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FORENSIC CHEMISTRY FORENSIC CHEMISTRY AS SCIENTIFIC AND EDUCATIONAL AS SCIENTIFIC AND EDUCATIONAL
SPECIALISATION SPECIALISATION AT THE JAGIELLONIAN UNIVERSITYAT THE JAGIELLONIAN UNIVERSITY
Paweł Kościelniak
JAGIELLONIAN UNIVERSITY, Faculty of Chemistry
INSTITUTE OF FORENSIC RESEARCHCracow, Poland
Jagiellonian University (1364)
Faculty of Law and Administration
Faculty of Philosophy
Faculty of History
Faculty of Philology
Fac. of Math., Phys. and Comp. Sciences
Faculty of Biology and Earth Sciences
Faculty of Biotechnology
Faculty of Chemistry
Fac. of Management and Social Comm.
Fac. of Internat. and Political Studies
Collegium Medicum
Fac. of Medicine & Div. of Dentistry
Fac. of Pharmacy & Div. of Medical Anal.
Faculty of Health Care
Jagiellonian University
Students
Total: 44 214
Regular studies: 27 653
Extramural studies: 15 552
External studies: 1 099
Postgraduate studies: 2 091
Academic staff
total: 6 710
academic teachers: 3 605
professors: 486
doctores habilitati: 503
JU in numbers (2006)
Faculty of Chemistry
Karol Olszewski (1846-1915) Chemist, physicist and expert of low Chemist, physicist and expert of low
temperatures; the first scholar who liquefied temperatures; the first scholar who liquefied nitrogen and oxygen; he also discovered a nitrogen and oxygen; he also discovered a
method of hydrogen liquefaction and method of hydrogen liquefaction and constructed machinery for that purpose, constructed machinery for that purpose,
which enabled him to reach the then-lowest which enabled him to reach the then-lowest world temperature, -225 C. world temperature, -225 C.
191950-5250-52
Faculty of Chemistry
Department of Inorganic Chemistry
Department of Organic Chemistry
Department of Analytical Chemistry
Department of Physical Chemistry
Department of Chemical Physics
Department of Theoretical Chemistry
Department of Crystal Chemistry
Department of Chemical Technology
Department of Chemical Education
Department of Computational Methods in Chemistry
DEPARTMENT OFANALYTICAL CHEMISTRY
(25)
LABORATORY FOR
FORENSIC CHEMISTRY(11)
GROUP OF ANALYTICAL FLOW TECHNIQUES
(10)
GROUP OF CHEMOMETRICS
(4)
Pure analytical chemistry & Flow Analysis
Optimization of analytical conditionsDevelopment of calibration methods Examination of interference effects
Analytical techniques
Atomic absorption spectrometryAtomic fluorescence spectrometry
UV/VIS spectrophotometryElectrochemical techniques
Capillary electrophoresisLiquid chromatography
Forensic Chemistry
Development of analytical methods and procedures for forensic purposes
Chemistry
undergraduate study graduate study
Organic
synthesisCatalysis Forensic
chemistry
EDUCATIONAL STRUCTURE
19291929
It is the only research centre of its kind in Poland, working under the aegis of the Ministry of Justice. Its statutory duties include: - research in the field of forensic science, - preparation of expert opinions for courts and public prosecutor's offices in criminal and civil cases,- the development and promotion of the forensic sciences.
The Institute carries out expert investigations and research in the following units:
Department of Forensic Toxicology Department of Criminalistics Department of Road Accidents Department of Forensic Psychology Forensic Genetics Section
Institute of Forensic Research
before 1997 – informal collaboration between FCh JU and IFR 1997 – common idea of educational module called „forensic chemistry” as one of
objectives of the TEMPUS project „Transformation of University Chemistry Studies at the Jagiellonian University”(TRUCS),
1997/98 – formal introduction of this module to the chemical study at FCh JU 2000 – establishment of the Laboratory for Forensic Chemistry at FCh JU as one
of the objectives of the TEMPUS project „National Training Program for Forensic Science Experts” (NATFOSE),
2001 – formal agreement between FCh JU and IFR in the field of forensic
chemistry
2000/2001 – modification of the curriculum of module „forensic chemistry”
from 2002 – teaching of „forensic chemistry” according to new curriculum
MILESTONES
LABORATORY FOR FORENSIC CHEMISTRY
- system for capillary electrophoresis (PrinCe 550 CSD, Prince)
- HPLC system (LaChrom, Merck)
- atomic fluorescence spectrometer with the flow system for hydride generation (AFS 230, Beijing Haiguang Instrument
Co.)
- system for microwave digestion (MARS 5X, CEM), - audiovisual equipment (video-projectors, digital photo-cameras, video-camera, video-recorders)
founded in 2000
Sem. SubjectNo. of hours
lectures classes seminars total
VIElectronics and automatics 30 30Optional 60 60
Total 90 90
VII
Electronics and automatics 60 60
Advanced analytical chemistry 45 45
Chemometrics and biometrics 30 15 45
Analysis in forensic chemistry 15 15
Radiometric analysis 30 30
Toxicology 30 30
Flow analysis 15 15
Optional 60 60
Total 225 60 15 300
Sem. SubjectNo. of hours
lectures classes seminars total
VIII
Radiometric analysis 45 45Forensic toxicology 60 15 75Criminalistics 15 60 15 90Low aspects of the forensic expert work 15 15
Student’s report 30 30Optional 60 60
Total 100 100 100 315
IXiX
Laboratory for master thesis 450 450
Seminar for master thesis 60 60Clinical toxicology 15 15GLP 15 15
Optional 60 60Total 90 450 60 600
No. Place
1 Toxicological analysis of drugs IFR2 Ethanol- selected toxicological and analytical aspects IFR3 Application of the GC/MS method to analysis of medicines in
biological materialsIFR
4 Determination of inorganic toxicants in biological material IFR5 Chemical examinations of car paints IFR6 Chemical examinations of fibers IFR7 Chemical examinations of gun-shot residuals IFR8 Chemical examination of inks by TLC IFR9 Chemical analysis of inks by CE JU
10 Determination of Se and As in biological materials by AFS-HG JU11 Comparative examination of psychotropic medicines by HPLC
and CEJU
12 Profiling of drugs – physicochemical and chemometric examination
JU
LABORATORY CLASSES
SubjectAnalytical method
FCh JU IFR
Examination of questioned documents on the basis of identification of chemical composition of inks CE
FTIR, TLC, RAMAN
Development of analytical procedures for determination of psychotropic drugs, particularly of phenotiazines and tricyclic antidepressants
HPLC, CE GC/MS
Development of analytical procedures for determination of selenium and arsenic in biological materials (blood, urine, hair, body tissues)
AFS, AAS UV/VIS
Identification and discrimination of car traces (paint, oil) - physicochemical and chemometric examinations
ASA FTIR, XRF
Profiling of amphetamine - physicochemical and chemometric examinations
TLC GC/MS
RESERCH SUBJECTS
PUBLICATIONS
- J. Zięba-Palus, P. Kościelniak, An Analysis of the Similarity of Motor Oils on the Basis of Their Elemental Composition, Forensic Sci. Int., 112, 81-90 (2000).
- J. Zięba-Palus, P. Kościelniak, M. Łącki, Differentiation of Motor Oils on the Basis of Their IR Spectra with Application of the Cluster Analysis, J. Molec. Struct., 596, 221-228 (2001).
- J. Zięba-Palus, P. Kościelniak, M. Łącki, Differentiation of Motor Used Oils on the Basis of Their IR Spectra with Application of the Correlation Method, Forensic Sci. Int., 122, 35-42 (2001).
- K. Madej, Capillary Electrophoresis as a New Tool in Forensic Toxicological Analysis, Problems of Forensic Sciences, 48, 31-52 (2001).
- R. Wietecha, R. Stanaszek, Determination of Morfine, Codeine and 6-monoacetylomorphine in Hair of Addicted Persons, Problems of Forensic Sciences, 49, 38-45 (2002).
- J. Mania, K. Madej, P. Kościelniak, Inks Analysis by Capillary Electrophoresis – Analytical Conditions Optimisation, Chem. Anal., 47, 585-594 (2002).
- P. Kościelniak, W. Piekoszewski, (ed.) Forensic Chemistry (in Polish), IFR, Kraków 2002.
- Z. Chłobowska, E. Chudzikiewicz, P. Kościelniak, W. Piekoszewski, A. Stolarz, Application of Gas Chromatography with NPD Detection to the Analysis of Tricyclic Antidepressants in Blood, Chem. Anal. 48, 255-263 (2003).
PUBLICATIONS
- J. Zięba-Palus, P. Kościelniak, Differentation Between Used Motor Oils on the Basis of Their IR Spectra for Criminalistic Purposes, The Forensic Scientist, 1, 23-28 (2003).
- R. Wietecha, P. Kościelniak, T. Lech, M. Rymanowski, Determination of Selenium in Human Blood Using Atomic Fluorescence Spectrometry, Problems of Forensic Sciences, 52, 21-30 (2003).
- Z. Chłobowska, Cz. Świegoda, P. Kościelniak, W. Piekoszewski, Identification and Determination of Flunitrazepam and Its Metabolites in Blood by Gas Chromatography, Chem. Anal., 49, 71-77 (2004).
- R. Wietecha, P. Kościelniak, T. Lech, T. Kielar, Simple Method for Simultaneous Determination of Selenium and Arsenic in Human Hair by Means of Atomic Fluorescence Spectrometry with Hydride Generation Technique, Microchim. Acta, 149, 137-144 (2005).
- K. Madej, M. Woźniakiewicz, M. Kała, Method for Screening and Quantification of Seven Phenothiazines in Whole Blood Samples by Non-aqueous Capillary Electrophoresis, Chromatographia, 61, 259-263 (2005).
- K. Madej, M. Kała, M Woźniakiewicz Application of Liquid Chromatography and Non-aqueous Capillary Electrophoresis to the Determination of Phenothiazines in Six Cases of Poisonings: Comparative Analysis, Chromatographia, 62, 533-538 (2005).
- R. Wietecha, J. Dobrowolska, P. Kościelniak, Simple Analytical Method for Determination of Selenium and Arsenic in Human Urine, 39, 2787-2796 (2006).
PROJECTS
TEMPUS program, project no. 12236/97 „Transformation of University Chemistry Studies at the Jagiellonian University” (TRUCS); 1997-2000
TEMPUS program, project no. 13514/98 „National Training Program for Forensic Science Experts” (NATFOSE); 1998-2001
LEONARDO DA VINCI program, project PL/01/A/Exd/14054 „Vocational Training System in Forensic Sciences - Exchange of Educational Experiences”
(VITSFOS-E); 2001-2003
NATO program, project no. PST.CLG.980067 “Sensors for Chemical Weapons Detection Based on Molecularly Imprinted Polymers”; 2004-2005
TEMPUS program, project no. 41105 - 2006„Education System In Forensic Sciences for the Republic of Macedonia” ”
(EDUFORMAK); 2007-2009
Ph.D. STUDYStudent Subject Defense
Renata WietechaDevelopment of the analytical procedure for the selenium determination in human tissues by the AFS-HG technique
2004
Rafał Borusiewicz Examination of arson traces 2004
Joanna Mania Examination of inks by capillary electrophoresis 2005
Małgorzata Świst Profiling of drugs 2005
Maria Pawluk-Kołc Classification and discrimination of glass traces 2005
Agnieszka Skulska Profiling of drugs 2006
Agnieszka Zakrzewska Profiling of drugs 2006
Maciej Kochanowski Analytical examination of illicit drugs 2007
Michał Woźniakiewicz Analysis of psychotropic drugs by HPLC and CE 2008
Justyna Dobrowolska Elemental analysis of biological materials 2008
Jakub Mielczarek Classification and discrimination of car paint traces 2008
FUTURE
• to make specialisation in forensic chemistry more and more attractive (e.g. to organise „artificial” trials, to prepare new interactive classes with the use of audiovisual and computer tools),
• to organise and open post-graduate study in the field of
forensic chemistry,
• to organise and open the „forensic” courses in the frame of „virtual university”
• to increase the scientific level of the forensic research performed,
• to expand the collaboration with national and foreign forensic/analytical centres
„FORENSIC CHEMISTRY” IN NUMBERS
• first and still only one activity of this kind in Poland
• 2 years of studying (4th and 5yh year of chemical study)
• 10 years of activity (since 1997/78)
• 12 - 14 students a year
• 31 publications (with the student contribution)
• 34 master’s theses
• 82 graduates
• a lot of students interested in the subject every year