Martin Andersson, Application Specialist, FOSS · Martin Andersson, Application Specialist, FOSS...

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Martin Andersson, Application Specialist, FOSS

”We deliver rapid, reliable and dedicated analytical solutions for routine testing to allow for fast decisions on how to maximise value of production of agricultural food products”

Improved predictability and control of manufacturing processes

Safe products and compliance with regulatory requirements

Supplier Receiving points

At-line/In-line production

Quality Control Laboratories

Finished products

Payment, segregation and quality control of raw material

Customer

Customer is using the same analytical system as the supplier

• Hit the target• Understand your yield

• Traceability• Fair trade

Chemical analysis using near infrared: How?

• Spectroscopy is the study of absorption of near infrared light (energy) by molecules

• Near infrared ranges from 780 – 2500 nm• It is a part of molecular spectroscopy

where interaction between light (energy) and matter (molecules).

NIR

• Atoms vibrate with a frequency specific to the molecular bond

• When light hits the vibrating bond, it is just passing through when it does not match the frequency

• When light hits the bond with a matching frequency, the light is absorbed and the vibration intensifies

• Organic bonds absorb NIR light.

400 nm

Color & chemical compositionincluding

-OH-NH-CH

780 nm 2500 nm

T H E L U C K Y R E G I O N

1100 1300 1500 1700 1900 2100 2300 2500Wavelength / nm

Abso

rban

ce (d

ashe

d)1st

deriv

ative

(soli

d)

1100 1300 1500 1700 1900 2100 2300 2500Wavelength / nm

Abso

rban

ce (d

ashe

d)1st

deriv

ative

(soli

d)

1100 1300 1500 1700 1900 2100 2300 2500Wavelength / nm

Abso

rban

ce (d

ashe

d)1st

deriv

ative

(soli

d)

1100 1300 1500 1700 1900 2100 2300 2500Wavelength / nm

Abso

rban

ce (d

ashe

d)1st

deriv

ative

(soli

d)

Water Fat

Protein Starch

• Moisture• Protein• Water Absorbtion• Maltose• Ash• Color L (L*, a*, b*)• Rice Amylose

2019年10月7日 10

Protein

7

8

9

10

11

12

13

14

15

16

7 8 9 10 11 12 13 14 15 16

0.1

7SEP

-

0.0

2

Bias

Infra

tec

LAB

Moisture

8

9

10

11

12

13

14

15

16

8 9 10 11 12 13 14 15 16

0.1

2SEP

-

0.0

4

Bias

LAB

Infra

tec

Color Value

58

59

60

61

62

63

64

65

66

67

68

58 59 60 61 62 63 64 65 66 67 68

0.3

3SEC

0.0

1Bias

Infra

tec

LAB

Maltose

150

200

250

300

350

400

150 200 250 300 350 400

15.

5SEC

-

0.3Bias

Infra

tec

LAB

Raw material reception

production Quality Control Laboratories

Finished products

Improved control of feed manufacturing process

Safe products and compliancewith regulatory requirements

Supplier’s payment, segregationand quality control of raw material

Usually good…

But too late

Raw material reception

Quality Control Laboratories

Finished products

Safe products and compliancewith regulatory requirements

Supplier’s payment, segregationand quality control of raw material

production

Improved control of feed manufacturing process

1 2

3

1. Windows reflectance

2. Direct light

3. Powder probe

4. Lateral Transmittance

probe4

Fine sticky powdersNIR range: 1100 – 1650 nm

• Whole milk powder• Skim milk powder• Whey powder• Infant formula powder• Caseinate powder• Starch powder• Corn/wheat gluten powder

Solids on open conveyor in reflectanceNIR range: 1100 – 1650 nm

• Feed ingredients• Feed pellets• Minced meat• Pasta• Chips

For liquid & slurriesNIR range: 850 – 1050 nm

• Soy Milk• Butter• Mozzarella• WPC / MPC• Cream• Fresh Cheese• Processed Cheese• Mechanical Debone Meat• Wet Pet Food• Whole Grain• Gluten/starch slurries

Fluid PowdersNIR range: 1100 – 1650 nm

• Feed ingredients• Feed mix• Feed pellets• Soy/rape meal• Whole Wheat• Whole Corn• Flour• Cocoa liquor • Etc.

30° 45° 80°

Limit of responsibilityNote: the Kepware license will be needed with ISIscan Nova and Beckhoff

Graph view of noisy measurements with batch average as a thick red line, and moving average as thick black line.

New interface

8. Optimizing samples for reference analyses

3. Back up sample data and instrument data

2. Instrument downtime,

1. Instrument management 4. Monitoring and optimizing instrument performance

5. Securing basic Standard Operation Procedures are followed

6. Maintenance plan for your instrument

7. Calibration accuracy on your instrument

9. Documenation for audit trail?

11. ANN

10. Best possible performance for all your samples

12. Complete backup and auto-documentation

FossManager (Pro) FossAssure ProFossAssure

FREE 90 days trial

FossCalibrator (Pro)

FREE 90 days trial

”A challenge I have often encountered is that when you are working within the plant, and the instrument seems to be working OK, then everyone is happy. However, when you start getting out of spec results, you get challenged. Is it the process or the instrument? With FossAssure, we can point to and demonstrate that the instrument is not the source of the issue. It gives peace of mind because I know that someone with the right education is keeping an eye on the instruments and how they are running.”

Jennifer Robinson, VP of Corporate Quality Assurance