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1. Standard Hydrogen Electrode 2. Sequestering agents 3...

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1 H. E Zagazig University Faculty of Pharmacy Clinical Pharmacy program Analytical Chemistry department Analytical Chemistry PC 306 Oral exam. 30/12/2012 ................ سم ا...... ..............جلوس الرقم ال............................................. .............. 1. Standard Hydrogen Electrode 2. Sequestering agents 3. Precision
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Page 1: 1. Standard Hydrogen Electrode 2. Sequestering agents 3 ...hishamezzat.weebly.com/uploads/9/0/6/0/9060375/oral_306_.pdf · Factors affecting on the Stability of complexes 3. Accuracy

1 H. E

Zagazig University

Faculty of Pharmacy

Clinical Pharmacy

program

Analytical Chemistry

department

Analytical Chemistry

PC 306

Oral exam.

30/12/2012

........................................................... الرقم الجلوس....................االسم ................

1. Standard Hydrogen Electrode

2. Sequestering agents

3. Precision

Page 2: 1. Standard Hydrogen Electrode 2. Sequestering agents 3 ...hishamezzat.weebly.com/uploads/9/0/6/0/9060375/oral_306_.pdf · Factors affecting on the Stability of complexes 3. Accuracy

2 H. E

Zagazig University

Faculty of Pharmacy

Clinical Pharmacy

program

Analytical Chemistry

department

Analytical Chemistry

PC 306

Oral exam.

30/12/2012

االسم ................................................................... الرقم الجلوس............................

1. Saturated calomel electrode(S.C.E.)

2. Factors affecting on the Stability of complexes

3. Accuracy

Page 3: 1. Standard Hydrogen Electrode 2. Sequestering agents 3 ...hishamezzat.weebly.com/uploads/9/0/6/0/9060375/oral_306_.pdf · Factors affecting on the Stability of complexes 3. Accuracy

3 H. E

Zagazig University

Faculty of Pharmacy

Clinical Pharmacy

program

Analytical Chemistry

department

Analytical Chemistry

PC 306

Oral exam.

30/12/2012

االسم ................................................................... الرقم الجلوس............................

1. Silver-silver chloride electrode

2. Complexones

3. Linearity

Page 4: 1. Standard Hydrogen Electrode 2. Sequestering agents 3 ...hishamezzat.weebly.com/uploads/9/0/6/0/9060375/oral_306_.pdf · Factors affecting on the Stability of complexes 3. Accuracy

4 H. E

Zagazig University

Faculty of Pharmacy

Clinical Pharmacy

program

Analytical Chemistry

department

Analytical Chemistry

PC 306

Oral exam.

30/12/2012

................................................... الرقم الجلوس............................االسم ................

1. Concentrated cell

2. General requirements for a good metal indicators

3. LOD

Page 5: 1. Standard Hydrogen Electrode 2. Sequestering agents 3 ...hishamezzat.weebly.com/uploads/9/0/6/0/9060375/oral_306_.pdf · Factors affecting on the Stability of complexes 3. Accuracy

5 H. E

Zagazig University

Faculty of Pharmacy

Clinical Pharmacy

program

Analytical Chemistry

department

Analytical Chemistry

PC 306

Oral exam.

30/12/2012

االسم ................................................................... الرقم الجلوس............................

1. Zimmermann’s reagent

2. Replacement and Back titration

3. LQD

Page 6: 1. Standard Hydrogen Electrode 2. Sequestering agents 3 ...hishamezzat.weebly.com/uploads/9/0/6/0/9060375/oral_306_.pdf · Factors affecting on the Stability of complexes 3. Accuracy

6 H. E

Zagazig University

Faculty of Pharmacy

Clinical Pharmacy

program

Analytical Chemistry

department

Analytical Chemistry

PC 306

Oral exam.

30/12/2012

.......... الرقم الجلوس............................االسم .........................................................

1. Effect of pH on oxidation potential of oxygenated system.

2. Indirect complexometric titration (determination of anions).

3. Methods of Validation

Page 7: 1. Standard Hydrogen Electrode 2. Sequestering agents 3 ...hishamezzat.weebly.com/uploads/9/0/6/0/9060375/oral_306_.pdf · Factors affecting on the Stability of complexes 3. Accuracy

7 H. E

Zagazig University

Faculty of Pharmacy

Clinical Pharmacy

program

Analytical Chemistry

department

Analytical Chemistry

PC 306

Oral exam.

30/12/2012

االسم ................................................................... الرقم الجلوس............................

1. Addition NaHCO3 before titration of arsenite with iodine.

2. Masking and Demasking.

3. Limit of detection

Page 8: 1. Standard Hydrogen Electrode 2. Sequestering agents 3 ...hishamezzat.weebly.com/uploads/9/0/6/0/9060375/oral_306_.pdf · Factors affecting on the Stability of complexes 3. Accuracy

8 H. E

Zagazig University

Faculty of Pharmacy

Clinical Pharmacy

program

Analytical Chemistry

department

Analytical Chemistry

PC 306

Oral exam.

30/12/2012

................................................................. الرقم الجلوس............................االسم ..

1. Desirable properties of redox indicators

2. Increasing selectivity of EDTA

3. Precision

Page 9: 1. Standard Hydrogen Electrode 2. Sequestering agents 3 ...hishamezzat.weebly.com/uploads/9/0/6/0/9060375/oral_306_.pdf · Factors affecting on the Stability of complexes 3. Accuracy

9 H. E

Zagazig University

Faculty of Pharmacy

Clinical Pharmacy

program

Analytical Chemistry

department

Analytical Chemistry

PC 306

Oral exam.

30/12/2012

االسم ................................................................... الرقم الجلوس............................

1. Diphenyamine.

2. Liebeg’s Method for determination of cyanide

3. Accuracy

Page 10: 1. Standard Hydrogen Electrode 2. Sequestering agents 3 ...hishamezzat.weebly.com/uploads/9/0/6/0/9060375/oral_306_.pdf · Factors affecting on the Stability of complexes 3. Accuracy

10 H. E

Zagazig University

Faculty of Pharmacy

Clinical Pharmacy

program

Analytical Chemistry

department

Analytical Chemistry

PC 306

Oral exam.

30/12/2012

.............................. الرقم الجلوس............................االسم .....................................

1. Iodometric methods

2. Denige’s modification

3. Methods of validation

Page 11: 1. Standard Hydrogen Electrode 2. Sequestering agents 3 ...hishamezzat.weebly.com/uploads/9/0/6/0/9060375/oral_306_.pdf · Factors affecting on the Stability of complexes 3. Accuracy

11 H. E

Zagazig University

Faculty of Pharmacy

Clinical Pharmacy

program

Analytical Chemistry

department

Analytical Chemistry

PC 306

Oral exam.

30/12/2012

االسم ................................................................... الرقم الجلوس............................

1. Iodimetric method,

2. Sequestering agents

3. LOD

Page 12: 1. Standard Hydrogen Electrode 2. Sequestering agents 3 ...hishamezzat.weebly.com/uploads/9/0/6/0/9060375/oral_306_.pdf · Factors affecting on the Stability of complexes 3. Accuracy

12 H. E

Zagazig University

Faculty of Pharmacy

Clinical Pharmacy

program

Analytical Chemistry

department

Analytical Chemistry

PC 306

Oral exam.

30/12/2012

االسم ................................................................... الرقم الجلوس............................

1. Precaution must be considered in case of using starch as

indicator in iodometric method

2. Factors affecting on the Stability of complexes

3. LQD

Page 13: 1. Standard Hydrogen Electrode 2. Sequestering agents 3 ...hishamezzat.weebly.com/uploads/9/0/6/0/9060375/oral_306_.pdf · Factors affecting on the Stability of complexes 3. Accuracy

13 H. E

Zagazig University

Faculty of Pharmacy

Clinical Pharmacy

program

Analytical Chemistry

department

Analytical Chemistry

PC 306

Oral exam.

30/12/2012

............................................................. الرقم الجلوس............................االسم ......

1. “Andrews Reaction”

2. Complexones

3. Method of validation

Page 14: 1. Standard Hydrogen Electrode 2. Sequestering agents 3 ...hishamezzat.weebly.com/uploads/9/0/6/0/9060375/oral_306_.pdf · Factors affecting on the Stability of complexes 3. Accuracy

14 H. E

Zagazig University

Faculty of Pharmacy

Clinical Pharmacy

program

Analytical Chemistry

department

Analytical Chemistry

PC 306

Oral exam.

30/12/2012

االسم ................................................................... الرقم الجلوس............................

1. Direct method for determination of Fe3+

2. Replacement and Back titration

3. Types of Error

Page 15: 1. Standard Hydrogen Electrode 2. Sequestering agents 3 ...hishamezzat.weebly.com/uploads/9/0/6/0/9060375/oral_306_.pdf · Factors affecting on the Stability of complexes 3. Accuracy

15 H. E

Zagazig University

Faculty of Pharmacy

Clinical Pharmacy

program

Analytical Chemistry

department

Analytical Chemistry

PC 306

Oral exam.

30/12/2012

االسم ................................................................... الرقم الجلوس............................

1. redox determination of PbO

2. Indirect complexometric titration (determination of anions).

3. H2O2 as oxidizing and reducing agent

Page 16: 1. Standard Hydrogen Electrode 2. Sequestering agents 3 ...hishamezzat.weebly.com/uploads/9/0/6/0/9060375/oral_306_.pdf · Factors affecting on the Stability of complexes 3. Accuracy

16 H. E

Zagazig University

Faculty of Pharmacy

Clinical Pharmacy

program

Analytical Chemistry

department

Analytical Chemistry

PC 306

Oral exam.

30/12/2012

االسم ................................................................... الرقم الجلوس............................

1. H2O2 as oxidizing and reducing agent

2. Masking and Demasking.

3. redox determination of PbO

Page 17: 1. Standard Hydrogen Electrode 2. Sequestering agents 3 ...hishamezzat.weebly.com/uploads/9/0/6/0/9060375/oral_306_.pdf · Factors affecting on the Stability of complexes 3. Accuracy

17 H. E

Zagazig University

Faculty of Pharmacy

Clinical Pharmacy

program

Analytical Chemistry

department

Analytical Chemistry

PC 306

Oral exam.

30/12/2012

.......... الرقم الجلوس............................االسم .........................................................

1. Karl Fischer reagent

2. Increasing selectivity of EDTA

3. Redox determination of Bleaching powder

Page 18: 1. Standard Hydrogen Electrode 2. Sequestering agents 3 ...hishamezzat.weebly.com/uploads/9/0/6/0/9060375/oral_306_.pdf · Factors affecting on the Stability of complexes 3. Accuracy

18 H. E

Zagazig University

Faculty of Pharmacy

Clinical Pharmacy

program

Analytical Chemistry

department

Analytical Chemistry

PC 306

Oral exam.

30/12/2012

................................................... الرقم الجلوس............................االسم ................

1. Redox determination of Bleaching powder

2. Liebeg’s Method for determination of cyanide

3. Karl Fischer reagent

Page 19: 1. Standard Hydrogen Electrode 2. Sequestering agents 3 ...hishamezzat.weebly.com/uploads/9/0/6/0/9060375/oral_306_.pdf · Factors affecting on the Stability of complexes 3. Accuracy

19 H. E

Zagazig University

Faculty of Pharmacy

Clinical Pharmacy

program

Analytical Chemistry

department

Analytical Chemistry

PC 306

Oral exam.

30/12/2012

االسم ................................................................... الرقم الجلوس............................

1. Redox detetrmination of mixture of Glucose & sucrose

2. Denige’s modification

3. Concentrated cell

Page 20: 1. Standard Hydrogen Electrode 2. Sequestering agents 3 ...hishamezzat.weebly.com/uploads/9/0/6/0/9060375/oral_306_.pdf · Factors affecting on the Stability of complexes 3. Accuracy

20 H. E

Zagazig University

Faculty of Pharmacy

Clinical Pharmacy

program

Analytical Chemistry

department

Analytical Chemistry

PC 306

Oral exam.

30/12/2012

االسم ................................................................... الرقم الجلوس............................

1. Redox determination of Phenol

2. Denige’s modification

3. NHE


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