Home >Documents >1.2 ASTMp31-58 new - Vogel .ASTM D-5580-00 Benzene, Toluene, Ethylbenzene, m/p-Xylene, o-Xylene,

1.2 ASTMp31-58 new - Vogel .ASTM D-5580-00 Benzene, Toluene, Ethylbenzene, m/p-Xylene, o-Xylene,

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  • ASTM D-5453 Total Sulfur in Light Hydrocarbons,Motor Fuels and Oils by Ultraviolet Fluorescence

    Fax 203-786-5287 Toll Free 800-442-5290 / 203-786-5290 Website www.accustandard.com

    ASTM

    Call your Distributor 31

    ASTM Standards

    D-5453

    Meets

    EPA Guidelines

    for

    RFG

    Analysis

    Method 544254435453

    ASTM D-5443 Paraffin, Naphthene, and Aromatic Hydrocarbon Type Analysis in(Reapproved 1998) Petroleum Distillates through 200C by Multi-dimensional GC

    Hydrocarbon Test MixtureD-5443-93-HTM $ 100 / 1 x 1 mLAt stated Wt. % 28 comps.

    ASTM D-5442 (Reapproved 1998) Analysis of Petroleum Waxes by GC

    Retention Time Standard Mix 1D-5442-RT1 $ 50 / 500 mgEqual parts by weight 12 comps.

    Retention Time Standard Mix 2D-5442-RT2 $ 55 / 500 mgEqual parts by weight 16 comps.

    n-Hexadecane (c16)n-Octadecane (c18)n-Eicosane (c20)n-Docosane(c22)n-Tetracosane (c24)n-Hexacosane (c26)

    Column ResolutionStandardD-5442-CR-PAK $ 40 / 5 x 1 mLAt stated Wt. % in Cyclohexane

    2 comps.

    Wt./Wt. %n-Eicosane 0.05n-Tetracontane 0.05

    n-Octacosane (c28)n-Triacontane (c30)n-Dotriacontane (c32)n-Hexatriacontane (c36)n-Tetracontane (c40)n-Tetratetracontane (c44)

    Quantitative Wax StandardD-5442-PAK $ 95 / 5 x 1 mLAt stated Wt. % in Cyclohexane 16 comps.

    n-Dodecane (c12)n-Tetradecane (c14)n-Hexadecane (c16)n-Octadecane (c18)n-Eicosane (c20)n-Docosane (c22)n-Tetracosane (c24)n-Hexacosane (c26)

    n-Octacosane (c28)n-Triacontane (c30)n-Dotriacontane (c32)n-Hexatriacontane (c36)n-Tetracontane (c40)n-Tetratetracontane (c44)n-Pentacontane (c50)n-Hexacontane (c60)

    NEW

    Wt./Wt. %Cyclopentane 1.00n-Pentane 1.00Cyclohexane 2.002,3-Dimethylbutane 2.00n-Hexane 2.00n-Hexene 1.50Methylcyclohexane 4.254-Methyl-1-hexene 1.50n-Heptane 3.50

    Wt./Wt. %1cis,2-Dimethylcyclohexane 5.00Isooctane 5.00n-Octane 5.001cis,2 cis,4-Trimethylcyclohexane 4.25n-Nonane 4.50n-Decane 4.25n-Undecane 3.50n-Dodecane 3.25Benzene 2.25Toluene 2.25

    Wt./Wt. %trans-Decahydronaphthelene 4.25n-Tetradecane 4.50Ethylbenzene 4.50o-Xylene 4.25n-Propylbenzene 5.001,2,4-Trimethylbenzene 4.501,2,3-Trimethylbenzene 5.001,2,4,5-Tetramethylbenzene 5.00Pentamethylbenzene 5.00

    Wt./Wt. %n-Tetracosane 0.10n-Hexacosane 0.12n-Octacosane 0.12n-Triacontane 0.10n-Dotriacontane 0.08

    Wt./Wt. %n-Dodecane 0.02n-Tetradecane 0.03n-Hexadecane 0.04n-Octadecane 0.05n-Eicosane 0.06n-Docosane 0.08

    Wt./Wt. %n-Hexatriacontane 0.06n-Tetracontane 0.05n-Tetratetracontane 0.04n-Pentacontane 0.03n-Hexacontane 0.02

    High Level Sulfur SetD-5453-HL-SET $ 90 / 5 x 2 mLThe set contains the following 5 standards in Isooctane

    Mid Level Sulfur SetD-5453-ML-SET $ 90 / 6 x 2 mLThe set contains the following 5 standards in Isooctane

    Low Level Sulfur SetD-5453-LL-SET $ 90 / 5 x 2 mLThe set contains the following 5 standards in Isooctane Real World Sulfur in Various

    Gasoline & FuelsQC SamplesSBPT-LSGAS $ 25 / 2 x 15 mLParameter Method Approx .Range

    Sulfur D-5453-00 0 - 50 g/g

    Cat. No. Description Unit

    D-5453-HL-BL Sulfur Blank 2 mLD-5453-HL-01 Sulfur @ 100 ng/L 2 mLD-5453-HL-02 Sulfur @ 250 ng/L 2 mLD-5453-HL-03 Sulfur @ 500 ng/L 2 mLD-5453-HL-04 Sulfur @ 1000 ng/L 2 mL

    Cat. No. Description Unit

    D-5453-ML-BL Sulfur Blank 2 mLD-5453-ML-01 Sulfur @ 5.0 ng/L 2 mLD-5453-ML-02 Sulfur @ 25 ng/L 2 mLD-5453-ML-03 Sulfur @ 50 ng/L 2 mLD-5453-ML-04 Sulfur @ 100 ng/L 2 mLD-5453-ML-05 Sulfur @ 200 ng/L 2 mL

    Cat. No. Description Unit

    D-5453-LL-BL Sulfur Blank 2 mLD-5453-LL-01 Sulfur @ 0.5 ng/L 2 mLD-5453-LL-02 Sulfur @ 2.5 ng/L 2 mLD-5453-LL-03 Sulfur @ 5.0 ng/L 2 mLD-5453-LL-04 Sulfur @ 10.0 ng/L 2 mL

    Originally designed forD-5442-93

    Originally designed forD-5443-93

    Originally designed forD-5453-00

    NEW

    Technical NoteDue to the wide variety ofrecommended solvents andstarting materials mentioned inthe preparation of the sulfurstandards, please review thecurrent product offering listedfor certified sulfur standards.Should AccuStandards currentsulfur standard line be missing,please contact us and indicateyour required formulation.For ppb Sulfur measurements,see page 6-11.

    Standards of InterestSee ASTM Methods D-3710,D-5307, D-6352 for additionalcalibration standards for hydro-carbon analysis or page 15 fornew proposed methods.

    Standards of InterestSee pages 6-11 for acomprehensive line of CertifiedSulfur Calibration Standards,Petrocheck, & Petrotest qualitycontrol products, pages 1-2.

    Member

  • ASTM D-5482 & D-5191 Vapor Pressure Standards

    ASTM D-5501 Ethanol Content of Denatured Fuel Ethanol by GC

    ASTM

    Quality System is Certified to comply with the International ISO 9001 Quality Standard32

    Vapor Pressure Quality Control Samples

    ASTM D-5580-00 Continuedon the Next Page

    ASTM Standards

    ASTM D-5580 Benzene, Toluene, Ethylbenzene, m/p-Xylene, o-Xylene, C9 andHeavier Aromatics, & Total Aromatics in Finished Gasoline by GC

    Analyte Std. 1 Std. 2 Std. 3 Std. 4 Std. 5Analyte Calibration range Wt. % Wt. % Wt. % Wt. % Wt. %

    Benzene 0.09 - 4.50 0.09 0.45 0.90 1.80 4.50Toluene 0.90 - 13.50 13.50 9.00 4.50 2.25 0.90Ethylbenzene 0.45 - 9.00 0.45 0.90 2.25 4.50 9.00o-Xylene 0.45 - 9.00 0.90 2.25 9.00 4.50 0.451,2,4-Trimethylbenzene 0.45 - 9.00 0.90 9.00 0.45 4.50 2.252-Hexanone (Internal Std.) 10.00 10.00 10.00 10.00 10.00Isooctane 74.16 68.40 72.90 72.45 72.90

    Analyte Std. 1 Std. 2 Std. 3 Std. 4 Std. 5Analyte Calibration range Wt. % Wt. % Wt. % Wt. % Wt. %

    Benzene 0.10 - 5.00 0.10 0.50 1.00 2.00 5.00Toluene 1.00 - 15.00 15.00 10.00 5.00 2.50 1.00Ethylbenzene 0.50 - 10.00 0.50 1.00 2.50 5.00 10.00o-Xylene 0.50 - 10.00 1.00 2.50 10.00 5.00 0.501,2,4-Trimethylbenzene 0.50 - 10.00 1.00 10.00 0.50 5.00 2.50Isooctane 82.40 76.00 81.00 80.50 81.00

    Denatured Fuel Ethanol Calibration SetD-5501-94-SET $ 75 / set of 7 x 1 mL

    Cat. No. Comp.1 Wt./ Wt.% Comp.2 Wt./ Wt.% Comp.3 Wt./ Wt.% Unit

    D-5501-94-01 Ethanol 92 Methanol 0.6 Heptane 7.4 1 x 1 mLD-5501-94-02 Ethanol 93 Methanol 0.5 Heptane 6.5 1 x 1 mLD-5501-94-03 Ethanol 94 Methanol 0.4 Heptane 5.6 1 x 1 mLD-5501-94-04 Ethanol 95 Methanol 0.3 Heptane 4.7 1 x 1 mLD-5501-94-05 Ethanol 96 Methanol 0.2 Heptane 3.8 1 x 1 mLD-5501-94-06 Ethanol 97 Methanol 0.1 Heptane 2.9 1 x 1 mLD-5501-94-07 Ethanol 98 Methanol 0.05 Heptane 1.95 1 x 1 mL

    Method 5480548255015580

    n-Dodecanen-Decanen-Undecane

    ASTM D-5480 Engine Oil Volatility by GC

    n-Octadecanen-Tetracosane

    n-Decanen-Dodecanen-Hexadecane

    Aromatics Quantitative Calibration Mixes (without Internal Standard)D-5580-95-CAL-SET-10ML $ 300 / set of 5 x 10 mL of 6 component mix

    Aromatics Quantitative Calibration Mixes (with Internal Standard)D-5580-95-CAL-IS-SET $ 100 / set of 5 x 1 mL of 7 component mix

    Tetracosane (Solution A)D-5480-C40-5ML $ 15 / 1 x 5 mLD-5480-C40-5ML-PAK SAVE 20% $ 60 / 5 x 5 mL500 g/mL in CS2

    n-Tetracosane

    Stock Column Resolution StandardD-5480-CR-PAK $ 40 / 5 x 1 mLEach comp. at 10 g/mL in CS2 5 comps.

    D-5480-CR-100X-PAK $ 50 / 5 x 1 mLEach comp. at 1000 g/mL in CS2 5 comps.

    Internal Standard SolutionD-5480-IS-5ML $ 30 / 1 x 5 mLD-5480-IS-5ML-PAK SAVE 20% $ 120 / 5 x 5 mLEach comp. at equal weights 3 comps.

    Cat. No. Vapor Pressure Price / Set of 10

    ASTM-P-124-01 68.3kPa (9.91 psi) $ 65 / 10 x 10 mLASTM-P-124-02 68.0kPa (9.86 psi) 75 / 10 x 10 mLASTM-P-124-03 51.1kPa (7.41 psi) 70 / 10 x 10 mLASTM-P-124-04 46.7kPa (6.77 psi) 125 / 10 x 10 mLASTM-P-124-05 22.5kPa (3.26 psi) 50 / 10 x 10 mLASTM-P-124-06 7.1kPa (1.03 psi) 50 / 10 x 10 mL

    Originally designed forD-5480-95

    Originally designed forD-5482-99 & D-5191-99

    Originally designed forD-5501-94

    Originally designed forD-5580-00

    Technical NoteAdditional Oxygenate calibra-tion, check standards, andindependent referencestandards can be found inASTM method D-4815 (page24) or D-5622-94 (page 37).The required QA/QCprocedures in EPA methodsstipulate a calibration checkstandard be used once peranalytical batch or per 10sample set. AccuStandard hasbulk packaged check standardsto meet this increased usage.

    Standards of InterestAlternative n-Paraffin stand-ards are available on page 15for further method developmentwork or more DetailedHydrocarbon Analysis (DHA).

    Technical NoteConsists ofpure solventswith knownvapor pressure.

    Member

  • ASTM D-5580-00 Benzene, Toluene, Ethylbenzene, m/p-Xylene, o-Xylene, C9 &Continued Heavier Aromatics, and Total Aromatics in Finished Gasoline by GC

    ASTM

    Call your Distributor 33

    Exclusive Aromatic Chemical Reference MaterialBenefits from AccuStandard

    Every analyte in each solution is individually weighed

    Actual weights and weight percents are available with allASTM/EPA solutions

    ASTM Standards

    Valve Timing Calibration Mix(without Internal Standard)M-GRA-VT-AS-10ML $ 100 / 1 x 10 mLM-GRA-VT-AS-10ML-PAK SAVE 20% $ 400 / 5 x 10 mLEach at stated conc. 5 comps.

    Wt./Wt. %Benzene 5.0Toluene 5.0Ethylbenzene 10.0o-Xylene 10.0Isooctane 70.0

    Internal StandardM-GRA-IS-AS-5ML $ 10 / 1 x 5 mLM-GRA-IS-AS-5ML-PAK SAVE 20% $ 40 / 5 x 5 mL

    2-Hexanone (Neat)

    Selectivity Check StandardM-GRA-SCS-AS $ 10 / 1 x 1 mLM-GRA-SCS-AS-PAK SAVE 20% $ 40 / 5 x 1 mLEach at stated conc. 2 comps.

    Wt./Wt. %n-Dodecane 1.5Isooctane 98.5

    Method 5580

    Wt./Wt. %Toluene 9Ethylbenzene 2p-Xylene 3o-Xylene 21,2,4-Trimethylbenzene 31,2,4,5-Tetramethylbenzene 1Naphthalene 1

    Wt./Wt. %n-Hexane 12n-Heptane 20n-Octane 15n-Decane 10n-Triadecane 1Isooctane 20Benzene 1

    Wt./Wt. %Toluene 9Ethylbenzene 2p-Xylene 3o-Xylene 21,2,4-Trimethylbenzene 31,2,4,5-Tetramethylbenzene 1Naphthalene 1

    Wt./Wt. %n-Hexane 12n-H

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