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14 Exploiting the Use of Compact Heat Exchangers on Preheating Trains

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    Exploiting the Use of Compact HeatExchangers on Preheating Trains

    (AIChE 2008 Spring Meeting 165d)

    PETROBRAS R&D Center CENPES

    Antonio V. S. de Castro*, M.Sc.

    Alan T. Vilas BoasClaudio L. M. Kuboski

    Diomedes C. da Silva, M.Sc.

    Roberto A. Oliveira, M.Sc.Washington de O. Geraldelli, Ph.D.

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    Introduction

    Higher prices of energy and oilCrude oil distillation unit is one of thehighest energy consumers in a refinery.

    Opportunities for heat integration:

    In revamps to process advantageous

    crudes Special Metallurgy higher heat recovery

    Threats:

    Special Metallurgy due to naphtenic acids- higher investments at preheating train

    increase on plot area due to increase onheat recovery - might be a constraint

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    Introduction

    Compact Welded Plate Heat Exchanger: Special Metallurgy (Titanium, SMO, etc.)

    leads to attractive costs compared to a S&T

    Compact (less plot area)

    Lower temperature approaches than S&T

    Innovative solution Refinery designers don't have enough

    information regarding the performance:

    Fouling Mechanical resistance

    Operational cautions, such as start-up and

    shut-down

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    PETROBRAS Experience

    End of 2001, PETROBRAS Engineersvisited a Refinery, in Europe, where aCompabloc CP75 was installed

    Overhead Condenser with Crude

    Special Metallurgy required due toChloride

    4 years without maintenance

    August, 2002. Service with two heavy

    fluids 13 exchangers at refinery since 1994

    Maintenance during winter shut-down

    Focus on Process Issues

    Visit to refinery with two parallel units(one stand-by) Sep,2005

    HVGO vs. Crude Oil (high temperature)

    Problems during the start-up (blocked

    pipe) Operating since November,2004

    Ref.: ALFA LAVAL

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    June,2002 ALFA LAVAL trained PETROBRAS

    Engineers how to design Compabloc using CAS200(ALFA LAVAL software)

    September,2006 Two-phase fluid ALFA LAVAL

    course, concerning crude oil vaporization Lack of data for temperature x shear stress x fouling rate

    May,2006 Visit to ALFA LAVAL factory in France:

    - Maintenance/Inspection/Cleaning Requirements

    - Manufacturing Process

    PETROBRAS Experience

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    P-68322A/B

    Feed pre-heater

    P-68323A/B

    Ovhd Condenser

    P-68324A/B

    Ovhd Gas

    Heater

    P-68325A/B

    Reboiler

    PETROBRAS Cases

    Sour WaterStripping Unit:

    Feed preheater Overhead

    Condenser

    Ovhd Gas Heater

    Reboiler

    Plot areaconstraints

    Fouling at Feedpre-heater

    Leakage at OvhdGas Heater

    CASE 1

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    Fouling at Feed preheater

    Inadequate H2S Stripping TowerOperation corrosion

    Actual Flow Rate (90m3/h) Design (160m3/h)

    Actual Shear Stress (22Pa) Design (60Pa)Mitigation:

    Increase passes number ( Shear Stress)

    Control Review (by-pass)

    Self-cleaning Strainers

    Leakage at Ovhd Gas Heater

    Material replacement:From Titanium to SMO

    PETROBRAS Cases

    CASE 1, cont.

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    Basic EngineeringDesign - Crude

    Distillation UnitRevamp:

    Increase FeedRate

    Heat Integration

    Plot AreaConstraints

    3 Services: MVGO(2) and VR

    220,000 bbl/d

    Start-up: 2011

    PETROBRAS Cases

    CASE 2

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    Conceptual Design

    (Revamp)140,000 bbl/d

    - MetallurgicalAdaptation(TAN=2.1)

    - OperationalDebottlenecking

    - Heat Integration

    Study PinchAnalysis

    - Plot Area and

    Shutdown timeconstraints

    - Full Compablocnew preheat trainsuggested.

    PETROBRAS Cases

    CASE 3

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    Compabloc Test at Refinery

    During conceptual design,necessity of a performancetest.

    A Compabloc CP30 unit hasbeen installed, in order toevaluate the performance ofthis equipment under unit

    conditions

    Vacuum Residue preheatingCrude before the Desalter

    Low Crude Temperature:~100 to 115C

    Operational and

    Maintenance experience

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    Compabloc Test at Refinery

    Vacuum Residue

    E-106D

    E-150

    Crude Oil

    103

    113

    172

    160

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    Compabloc Test at Refinery

    Similar to phase 1.3 months100%6

    b) Cleaning with hidroblasting.

    a) Open the equipment to check deposits;Cleaning5

    b) Equipment shut-down for 10 days and restart it.

    a) Check pressure drop;Fouling2 months25%4

    b) Auto cleaning capabity.

    a) Check pressure drop;Thermal performance

    and fouling

    2 months100%3

    if not, go to phase4.

    b) if fouling, go to phase 1;

    a) Check pressure dropFouling2 months50%2

    b) Compare design X operational data using CAS200.

    a) Check pressure drop;Thermal performance6 months100%1

    (design basis)

    ProcedureObjectivePeriodFlow rateStep

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    Compabloc Test at Refinery

    1st Phase Results: Crude side measured pressure drop was

    from 29 to 47% of calculated values byCAS200;

    VR side measured pressure drop was from123 a 167% of calculated values by CAS200;

    Difference in global heat transfer coefficients(HTC) was much lower. Measured valueswere from de 88 a 111% of calculated valuesby CAS200;

    Problems with Instrumentation could be thecause of such difference in pressure drop

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    Compabloc Test at Refinery

    Crude Inlet Vacuum Residue Inlet

    Compabloc Opening after 1st step (8 months)

    Deflected Baffle (mechanical resistance) it wasnot designed for that purpose

    C

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    Pressure drop results - phases 2, 3 and 4

    Compabloc Test at Refinery

    0.00

    0.20

    0.40

    0.60

    0.80

    1.00

    1.20

    1.40

    1.60

    1.80

    2.00

    1-Sep 2-Oct 2-Nov 3-Dec 3-Jan 3-Feb 6-Mar 6-Apr 7-May 7-Jun 8-Jul 8-Aug 8-Sep 9-Oct

    Period from 2006 up to 2007

    pressuredrop,

    kgf/cm

    CRUDE

    VACUUM RESIDUE

    50% flow rate 25% flow rate 100% flow rate

    C bl T R fi

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    Compabloc Test at Refinery

    Flow Rate Vacuum Residue vs CrudeAd-Hoc Trend

    01/08/05 00:00:00 20/09/07 00:00:002.14 Year(s)

    1210-FI-299

    M3/D

    1210-FI-298

    M3/D

    500

    1000

    1500

    2000

    2500

    0

    3000160.63

    28.689

    1210-FI-299

    M3/D

    1210-FI-298

    M3/D

    C bl T t t R fi

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    Compabloc Test at Refinery

    Positive Aspects:- Equipment kept its thermalperformance;

    - Design, Operational and

    Maintenance experience

    - No fouling observed

    Negative Aspects:

    - Mechanical Resistance(Leakage and Baffle);

    - Aspects not related to

    exchanger (instrumentation,flow fluctuation, )

    C bl T t t R fi

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    Compabloc Test at Refinery

    Crude Side

    Period: Jul/16/07 up toSep/20/07

    Zero Flow Rate forabout 3 weeks.

    No abnormal pressurevariation.

    Pressure

    Flow Rate

    Compabloc Test at Refinery

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    Compabloc Test at Refinery

    Vacuum Residue Side Period: 16/Jul/07 up to

    20/Sep/07

    Zero Flow Rate for 10 days. Significative pressure and

    flow rate variation.

    Pressure

    Flow Rate

    PressureSep/01 to 17

    Compabloc Test at Refinery

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    Compabloc Test at Refinery

    Inlet Pressure VR vs Crude (Accordeon Effect)

    Compabloc Test at Refinery

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    Compabloc Test at Refinery

    Problem Root Cause Consequense

    Leakage Joint Failure Vacuum Residue Leakage

    Baffle Deflection Overpressure or fatigue Thermal performance loss

    ALFA LAVAL: Development of new gasket;

    Adoption of reinforced baffles (for high viscous fluids);

    PETROBRAS: Avoid surge pressure (hydraulic hammer):

    Startup and shutdown procedures; Slow valve action;

    Drain the equipment, in case of several days of shutdown.

    Panels bolting hot retightening after startup Deposits prevention:

    Strainers;

    PETROBRAS Cases

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    Basic Engineering Design (Oct/07)

    Preheat Train before

    Desalter Carbon Steel

    Equivalent Cost

    Preheat Train betweenDesalter and PreFlashTower

    Crude Vaporization

    Special Metallurgy

    Parallel Arrangement

    PETROBRAS Cases

    CASE 3

    PETROBRAS Cases

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    Basic Engineering Design (Oct/07)After PreFlash Tower Preheat Train

    (High Temperature Special Metallurgy)

    SERVICE Shear (Pa) WALL TEMPERATURE (C)

    E-166 A/B (x HVGO) 112 264

    E-167 A/B (x HD) 113 289

    E-169 C/D (x BPA) 113 295

    PETROBRAS Cases

    CASE 3

    Petrobras Current Case

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    CS

    CS CS

    CS AE

    V

    V

    HT

    HT

    HT HT

    HT

    CB CB

    Petrobras Current Case

    CB CompablocCS Carbon Steel

    HT High TemperatureAE accordion Effect

    V Crude Vaporization

    CASE 4 Basic Engineering Design CDU Grass root Refinery

    PETROBRAS Current Case

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    COMPARISON OF EQUIPMENT COSTS

    SERVICE Compabloc (US$) Shell and Tube (US$)

    P-10 x ~ 5.6 x

    P-11 y ~ 3.8 y

    * Installation costs not included;

    * Equipment designed with the same allowablepressure drop;

    * Compabloc design and budget by Alfa Laval;

    * Shell and Tube budget by Aspen Icarus (Brazil

    Base)

    PETROBRAS Current Case

    CASE 4 Basic Engineering Design CDU

    Grass root Refinery

    Compabloc Design

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    Compabloc Design

    Design Parameters:

    Minimum Shear Stress

    Higher Pressure drop

    Countercurrent Pinch Analysis

    Strainers / Maintenance facilities Parallel Arrangement (flexibility)

    Accordeon Effect Crude Vaporization

    High temperature

    Next Compabloc Tests

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    Next Compabloc Tests

    Next Step at the same refinery:Operational practice and fouling at

    high temperatures;

    Service: Not defined yet;Wall temperature above 270C (target

    300C)

    Test at Case 2 refinery :

    Operational practice and fouling withcrude vaporization;

    Service: Not defined yet (desaltedcrude vs heavy diesel)

    Crude Temperature from 150C to220C

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    Thank you very much!

    Antonio V. S. de Castro, [email protected]

    Alan T. Vilas Boas

    Claudio L. M. Kuboski

    Diomedes C. da Silva

    Roberto A. OliveiraWashington de O. Geraldelli


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