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158 Ready Mix Paint Brushing,Bituminous Black Lead Free,Acid ,Alkali & Heat Resisting

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    IS:l!J s-1981I ndi an St andard

    SPECIFICATION FORREADY MIXED PAINT, BRUSHING,BITUMINOUS, BLACK, LEAD FREE, ACID,

    ALKALI ANil HEAT RESISTING( Thi rd Rev i si on)

    Second Reprint MAY 1990

    UDC 667.633 :667.637.23 :667.634.2

    ( Reaffirmed 1999 )

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    IS : 158 1981

    I ndi an St andardSPECIFICATION FORREADY MIXED PAINT, BRUSHING,

    BITUMINOUS, BLACK, LEAD FREE, ACID,ALKALI AND HEAT RESISTING

    / Thi rd Rev i si on)Paints and Allied Products Sectional Committee, CDC 8

    ChairntmiSHRI K. N. R. Sm

    MtT?h?i-S

    RepresentingDirecNc;t;e,eneral of Technical Development,

    Spnu R. D. KAWA~~A Altermte toSbri K. N. R. Sharma )Srmr BAL~TSINGH Bhagsons Paint Industries ( India ), New DelhiSHRIH.A~IXP INGH Alternate )Smu K. M. BANER~EE National Test House, CalcuttaSrrar V. M. BAVDEKAR Asian Paints ( India ) Ltd, Bombay

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    IS : 158 - 1981( Continued from page 1 )

    MembersSHRI M. PHIL IP

    Representing&RI P. N. PHADKE ( Alternate )

    Indian Aluminium Company Ltd. CalcuttaSHRI K. S. RAJ EEVALOCHANAM Heavy Engineering Co Ltd. RanchiSHRI D. P. MUK H~RJ EE Alternate )SHRI D. RAMAMURTHY Bharat Heavy Electricals Ltd, HyderabadSHRI N. D. GUPTA ( Al ternate I )SHRI R. C. MI SRA ( Ahernate I I )SHRI M. N. R.\ o Indian Paint Association, CalcuttaSHRI M. M. GHOSH ( Alternate )DR R. J . RATHI Sudershan Chemical Industries Ltd, PuneSHRI K . L. RATHI ( Alternate )SHIUP. SANANARAYANA Development Commissioner, Small Scale Industries,New Delhi

    DR S. K. Kamk ( Alternate )SC~ENI -IFIC DVISER TO THE CHIEF Naval Headquarters ( Ministry of Defence )OF THE NAVAL STAFFDR A. K. SEN Ministry of Defence ( DC1 )SHRI S . K. A~THANA ( Alternate )SENIORCHEMISTAND METALLURGIST Railway Board ( Ministry of Railways )AWSTAKT RE~@ARFH OFFICER (Alternate )SHRI R. R. SEQUERA Garware Paints Ltd, BombayDR P. G. CHAUDHARI Alternate ISHRI C. R. THUSa ( Alternate 11)DR S. M. S~NGH Cent~~or~~ding Research Institute ( CSIR ),

    SHRI R. S. SRIVASTAVA Alternate )DR M. A. SIVASAMBAN Regional Research Laboratory ( CSIR). HyderabadDR M. M. SHIRSALKAR Al ternate ) -

    CAPT V. SULIRAMANIAN The Shipping Corpqration of India Ltd. BombayCAPT S. K . KHURANA ( Alternate )

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    IS : 158 1981

    I ndian St andardSPECIFICATION FORREADY MIXED PAINT,, BRUSHING,

    BITUMINOUS, BLACK, LEAD FREE, ACID,ALKALI AND HEAT RESISTING

    ( Thi rd Rev i si on)0. FOREWORD

    0.1 This Indian Standard (Third Re,vision) was adopted by the IndianStandards.Institution on 15 July 1981, after the draft finalized by the Paintsand Allied Products Sectional Committee had been approved by the Chemi-cal Division Council.0.2 This standard was first published in 1950 and subsequently revisedin 1965 and 1968 and covered two types of the material. Material of Type 1was intended for use as acid, alkali, water and heat resistant paint, generallyused for chimneys, boilers, apparatus, etc. Type 2 was intendedfor use as acid, alkali and water resistant for general purposes,, parti-

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    IS : 158 - 19810.6 This standard contains clause 4.1 which calls for an agreement betweenthe purchaser and the supplier.0.7 For the purpose of deciding whether a particular requirement of thisstandard is complied with, the final value, observed or calculated, express-ing the results of a test or analysis, shall be rounded off in accordance withIS : 2-1960*. The number of significant places retained in the rounded offvalue should be the same as that of the specified v%lue in this standard.

    1. SCOPE1.1 This standard prescribes requirements, and methods of sampling andtest for ready mixed paint, brushing, bituminous, black, lead free, acid,alkali and heat resisting. c1.1.1 The material is used for the protection of funnels, boilers,apparatus and appliances connected with ammunition.2. TERMINOLOGY2.1 For the purpose of this standard, definitions given under 2 ofIS : IOI-1964t, IS : 1303-1963: and the following shall apply.

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    Is : 158 19813.4 Resistance to Heat - The material shall pass the test when testedas prescribed in Appendix A.3.5 The material shall also comply with the requirements given in Table 1.TABLE 1 REQUIREMENT FOR READY MlXED PAINT, BRUSHING. BITUMINOUS,BLACK, LEAD FREE, ACID, ALKALI AND HEAT RESISTING

    SL CHARACTERISTICNo.( Clauses 3.5 and 6.1 )

    REQUIREMENT METHOD OF TIZST,REF TO-Appendix Cl y;. m

    lOI-1464+

    (1) (2)i) Drying time - hard dryii) Consistency

    iii) Finishiv) Wet opacity

    (3)Not more than 8 hoursSmooth and uniform and suit-able for application by brush-ing without appreciable dragon the brushS;gstt and egg shell to semiBetween -10 percent and the+20 percent of the approved

    (4)--

    --

    (5)7.27.4

    7.510

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    Is : 158 - 19813.6 Lead Free Material -When lead free material is required in additionto the requirements stipulated in 3.1 to 3.5, it shall also be tested for freedomfrom lead in accordance with 29 of IS : lOI-1964*. When thus tested, thematerial shall not contain lead or lead compounds or a mixture of bothcalculated as metallic lead ( Pb ), exceeding 0.03 percent by mass.4. PACKING AND MARKING4.1 Packing-The material shall be packed as agreed to between thepurchaser and the supplier.4.2 Marking -The containers shall be marked with the following parti-culars :

    a) Name of the material;b) Manufacturers name and his recognized trade-mark, if any;c) Volume of the material;d) Batch No. or lot No. in code or otherwise; and 1e) Month and year of manufacture.

    4.2.1 The containers may also be marked *with the IS1 CertificationMark.

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    Is:lS-lsQu5.2 Number of Tests

    5.2.1 Individual samples shall be tested for mass in kg/l0 litres. Ifthey are found to be uniform and conforming to this specification, theindividual samples may be blended to make a composite sample.5.2.2 Tests for remaining characteristics of the material shall be con-ducted on the composite sample.

    5.3 Criteria for Conformity5.3.1 The lot shall be declared as conforming to the requirements ofthis specification if individual samples are uniform and conforming to thespecification limits of mass in kg/IO litres, and if the characteristics testedon composite sample satisfy the corresponding requirements given in thisspecification.6. TEST METHODS6.1 Tests shall be conducted as prescribed in IS : lOI-1964* and in Appen-dices A to C. Reference to relevant clauses of IS : IOl-1964* is given in3.2,3.3,3.6 and co1 5 of Table 1 and that of appendices in 3.4 and co1 4 ofTable 1.6.2 Quality of Reagents - Unless specified otherwise, pure chemicals

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    A-l. APPARATUSA-l.1 Electric Furnace With a maximum attainable temperature of900C. It is equipped with a 3 500 W heating element which operates on asingle phase alteof 240. in ating current of approximately 15 A of 50 c/s on a voltageThemin mum dimensions of the heating chamber are 380 x 150 x80 mm.

    A-2. PROCEDUREA-2.1 Apply acoating of thematerial by brushing to a 150 x 100 x @8 mmclean mild steel panel to give a dry film mass commensurate with the massin kg/l0 litres of the material as prescribed in 6A of IS : 101-1964*. Allowthe panel to air-dry in a horizontal position for 24 hours under standardconditions (2.4 of IS : lOl-1964* ). Heat the panel in a vertical position inan electrical furnace, the temperature of which is gradually raised fromroom temperature up. to a temperature of 3 000C in 14 hours time. Main-tain the panel at the maximum temperature of 3 000C for half an hour.Remove the panel from the fumace,cool to room temperature and immersein water at room temperature for 24 hours. Take out the panel and examineit after air-drying for one hour. .A-2.2 The material shall be deemed to have passed the test if the paintfilm remains firmly adherent and shows no sign of cracking, blisteringor flaking. Formation of hair-lines shall not be a cause for rejection. For

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    IS : 158 - 1981B-2. PROCEDUREB-2.1 Apply a coating of the material by brushing to a 150x 50 mm-clean glass panel to give a dry film mass commensurate with the mass inkg/IO litres of the material as specified in 6.4 of IS : lOl-1964*. Allow thepanel to air-dry in a horizontal position for 24 hours under standardconditions ( 2.4 of IS : lOl-1964* ). Immerse the panel partially in dilutesulphuric acid for 24 hours. Take out the panel, wash carefully and examinethe immersed portion of the film after drying for one hour.B-2.2 The material shall be deemed to have passed the test if the paintfilm on the panel shows not more than slight change in characteristic forsoftening, blistering, cracking, and colour.

    APPENDIX C[Table 1, hem (xi)]

    DETERMINATION OF RESISTANCEC-O. OUTLINE OF THE METHOD

    TO ALKALI

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    6UREA.U OF INDIAN STA-NDARDSHeedquerters: i *Manak Bhavan, 9 Bahadur Shah Zafar Marg, NEW DELHI 110002Telephones: 331 01 31, 331 13 76 Telegrams: Manakssnstha( Common to all Off i i )Regional Off ices: TelephmeCentral : Manak Bhavan, 9 Bahadur Shah Zafar Marg.

    I331 ni SlNEW DELHI 110002 331 1376

    *Eastern : 1 /i 4 C. I. T. Scheme VII M, V. I. P. Road. $8 24 99Maniktola, CALCUTTA 700064Northern : SC0 445-448, Sector 36-C,I

    21843CHANDIGARH 180038 3 1641

    (41 24 42Southern : C. I. T. Campus, MADRAS 800113 41 26 1941 2918tWostern : Manakalaya, E9 MIDC, Marol,, Andheri ( East ), 8 32 92 96BOMBAY 400093

    ranch Off ices:Pushpak, Nurmohamed Shaikh Marg, Khanpur,

    I2 83 48

    AHMADABAD 380001 2 83 49Peenya Industrial Prea 1 st Stage, Bangalore Tumkur Road 38 49 65BANGALORE 560068 I 38 49 65

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    AMENDMENT NO. 1 J ULY 1982TO

    I S: 158-1981 SPECI FI CATI ON FOR READY M XED PAI NT,BRUSHI NG, BI TUM NOUS, BLACK, LEAD FREE,ACI D, ALKALI ANDHEATRESISTING(Third Revision)

    Corrbendum- - - - -(Page 8, okwe A-2. 1, Zi ncs 7 and 8) - wti ttute300C far 3 OQOC at bo%h the places.

    (CM=8)Reprography Unit, BIS, New Delhi, India

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    AMENDMENT NO. 2 DECEMBER 1988TO

    IS I 158 - l!Ml SPECIFICATION FORREADY MIXED PAINT, BRUSHING, BITUMINOUS,BLACK, LEAD FREE, ACID, ALKALI AND

    HEAT RESISTING/ T h i r d Rev i r i o n /

    [ Puge 5, Tuble 1, Sf A%. ( iii ), co1 3 J - Substitute S~~ooth dremi-glow to glossy for the existing entries.

    (CDCE)Reprography Unit, 51.5, New Delhi, India


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