1C E?A SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS …O.SOJU O.SOJU 1.0JU 1.0JU FORM I PEST 1/87 Rev....

1C E?A SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET _______________

I CB<fX>3Qll6afa Name: YORK LABS/CT Contract: 68-W8-0021 I __________

YORK Case No.: 12512 SAS No.: SDG No.: C3Q02

atrix: (soil/water) WATER Lab Sample ID: 1496014

ample wt/vol: 1000 (g/mL) ML Lab File ID: >H5731

evel: (low/med) LOW Date Received: 08/23/89

Moisture: not dec. dec. Date Extracted: 08/24/89

xtraction: (SepF/Cont/Sor.c) SEPF Date Analyzed: 09/11/89

PC Cleanup: (Y/N) N pH: Dilution Factor: 1

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q

99-09-2 ——————— 3-Nitroaniline.83-32-9———————Acer.aohthene__51-28-5 ——————— 2,4-Dini trophenol.100-02-7 ——————— 4-Nitrophenol____132-64-9 ——————Dibenzofuran_____121-14-2 ——————— 2, 4-Dinitrotoluene.84-66-2————————Diethylphthalate__7005-72-3 —————— 4-Chl or opb.enyl-phenyl ether.86-73-7————————Fluorene________________100-01-6——————4-Ni troani 1 ine__________534-52-1———————4, 6-Dinitro-2-methylphenol.86-30-6———————N-Nitrosodiphenylamine (1}.101-55-3——————4-Bromophenyl-phenylether_118-74-1———————Hexachlorobenzene________87-86-5———————Pentachlorophenol________85-01-8 ———————— Phenanthrene_____________120-12-7———————Anthracene_______________84-74-2———————Di-n-butylphthalate.206-44-0 ——————— Fluoranthene______129-00-0———————Pyrene__________85-63-7———————Butylbenzylphthalate__91-94-1 ——————— 3,3 '-Dichlorobenzidine.56-55-3———————Benzo(a)arithracene___

I 218-01-9——————Chrysene_______________I 117-81-7——————bis(2-Ethylhexyl Jphthalate.117-84-0——————Di-n-octylphthalate.205-99-2———————Benzo(b)f luoranthene.207-08-9———————Benzo(k) f luoranthene.

I 50-32-8————————Benzo(a)pyrene________I 193-39-5 ——————— Indeno(l,2,3-cd)pyrene_I 53-70-3————————Dibenzo(a,h) anthracene.I 191-24-2———————SenzoCg,h, i )perylene__

50.00010.00050.00050.00010.00010.00010.00010.00010.00050.00050.00010.00010.00010.00050.00010.00010.0000.60010.00010.00010.00020.00010.00010.0009.00010.00010.00010.00010.00010.00010.00010.000

uuuuuuuuuuuuuuuuuJuuuuuuJBuuuuuuu

(1) - Cannot be separated from Diphenylamine

FORM I SV-2 1/87 Rev.

RR3065UI

ID EPA SAMPLE NO.PESTICIDE CRGANICS ANALYSIS DATA SHEET _______________


. Moisture: not dec. ____ dec. _____ Date Extracted: 08/25/89

xtraction: (SecF/Ccnt/Scnc) SEPF Date Analyzed: 09/01/89

:PC Cleanup: (Y/N) N pH: Dilution Factor: 1


319-S4-6——————— alpha-BHC_________319-35-7———————beta-BHC__________319-86-S— ———— delta-BHC________58-89-9---------gamma-BHC (Lindane).76-44-8————————Heotachlor_______'_309-00-2— ————— Aldrin____________1024-57-3—————Heptachlor eooxide959-98-8———————Endosulfan I_____60-57-1———————Dieldrin________72-55-9————————4, 4'-DDE__________72-20-8———————Endrin_________33213-65-9—————Endosulfan II____72-54-8—————————4,4'-DDD__________1031-07-8—————Endosulfan sulfate50-29-3————————4. 4'-DOT__________72-43-5—— — ——— Methoxychlor_____53494-70-5—————Endrin" ketone____5103-71-9---——alpha-Chlordane__5103-74-2-----—gamma-Chlordane___8001-35-2----——Toxaohene________12674-11-2—————Aroclor-1016_____11104-28-2—————A redo r-1221_____11141-16-5—————Aroclor-1232_____53469-21-9—————Aroclor-1242_____12672-29-6—————Arcclor-1248_____11097-69-1—————Aroclor-1254_____11096-82-5 ————— Arcclor-1260_____

0.050|UO.OSOJU0.050|UO.OSOJU0.050|UO.OSOJUO.OSOJUO.OSOJU0.10JU0.1OIU0.10JU0.10JU0.10JU0.10JU0.10JU0.50JU0.10IU0.50IU0.50JU1.0IU

0.50JU0.50IU0.50JU0.50!U0.50JUl.OJU1.0|U

i_____ i._

I

CBQ07 '.ab Name: YORK LABS/CT Contract: 68-W8-0021

.ab Code: YORK Case No.: 12512 SAS No.: _____ SDG No.: C8Q02

fatrix: (soil/water) WATER .Lab Sample ID: 1496O14

:amole wt/voL: 1000. (g/mL) ML Lab File ID: ________

FORM I PEST 1/87 Rev

AR3065142

13 E?A SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET ______________

t I C3Q08Name: YORK LA3S/CT Contract: 63-W8-0021 I_____ QOOJ2SCode: YORK Case No.: 12512 SAS No.: SDG No.: CBQ02

atrix: (soil/water) . WATER Lab Sample ID: 1496019




xtraction: (SepF/Cont/Sonc) SEPF Date Analyzed: 09/10/89



108-95-2 ———————— Phenol______________________111-44-4——————bis(2-Chloroethyl)ether____95-57-8 ——————— 2-Chlorophenol____________541-73-1 —————— 1,3-Dichlorobenzene_______106-46-7——————i, 4-Dichlorobenzene_______100-51-6———————Benzyl alcohol____________95-50-1 ———————— 1, 2-Dichlorobenzene________95-48-7————————2-Methyl phenol_____________108-60-1———————bis(2-Chloroisopropyl )ether_106-44-5 ——————— 4-Methyl phenol_____________621-64-7———————N-Nitroso-di-n-propylamine_67-72-1————————Hexachloroe thane___________98-95-3————————Nitrobenzene______________78-59-1 ———————— Isoohorone________________88-75-5———————2-Ni trophenol_____________105-67-9——————2,4-Dime thy 1 phenol________65-85-0———————Benzoic acid_____________111-91-1———————bis(2-Chloroethoxy) methane_120-83-2 ——————— 2 ,4-Dichlorophenol_________120-82-1 ——————— 1,2,4-Trichlorobenzene_____91-20-3———————Naphthalene______________106-47-8 ——————— 4-Chloroan.il ine___________87-68-3————————Hexachlorobutadiene________59-50-7 ———————— 4-Chloro-3-methyl phenol____91-57-6————————2-Methylnaphthalene_______77-47-4———————Kexachlorocyclopentadiene__88-Q6-2———————2,4,6-Trichlorophenol_____95-95-4 ———————— 2,4,5-Trichlorophenol______91-58-7 ———————— 2-Chloronaphthalene________33-74-4———————2-Nitroaniline____________131-11-3——————Dimethylphthalate_________208-96-8———————Acenaohthylene____________606-20-2 ——————— 2 ,6-Dinitrotoluene_________

I10.0001 U10.000! U0.4001 JB10.000! U10.000! U10.0001 U10.0001 U10.000! U10.0001 U10.000! U10.000! U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U50.0001 U10.0001 U10.000! U10.000! U10.0001 U10.000! U10.000! U10.0001 U10.0001 U10.0001 U10.000! U50.0001 U10.0001 U50.0001 U10.0001 U10.0001 U10.000! U

FORM I SV-1 APQn£Rb.3 1/87 Rev.

1C E?A SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET _______________.

I II C3Q08 00 01'-7

ab Name: YORK LA3S/CT Contract: 68-W8-0021 |____________wwwj,*.i

ab Code: YORK Case No.: 12512 SAS No.: SDG No.: CBQ02




Moisture.- not dec. dec. Date Extracted: 08/25/89




99-09-2 —————————83-32-9 —————————51-23-5 —————————100-02-7 ———————132-64-9 ————————121-14-2 ————————84-66-2 —————————7flnti— 7? T ______86-73-7 ————————100-01-6 ———————534-52-1 ————————86-30-6 —————————101-55-3 ————————118-74*-! ————————87-86-5 —————————85-01-8 —————————120-12-7 ————————84-74-2 —————————206-44-0 ————————129-00-0 ————————85-68-7 —————————91-94-1 —————————56-55-3 —————————218-01-9 ————————117 fl 1 "7

117-84-0 ———————

207-08-9 ————————50-32-8 —————————193-39-5 ————————^ "3 — 7fi "3 —• — — — —

3-Ni t-oan.il ineAcer-aahthene , „ , ,.,„2 , 4-Dini trooheno 14-NitroohenolDibenzof uran2 , 4-D in itro tolueneDiethylph thai ate4-Chl oropheny 1 -pheny 1 e therFluorene4-Mi troani 1 ine,, „4 , 6-Dini tro- 2 -methyl phenol _N-Ni trosodiphenylamine (1) _4 -Bromophenyl -pheny 1 ether __Hexachlorobenzene „,,Pentachl orooheno 1PhenanthreneAnthracene. ,„ ,.„, .Di— n— buty IphthalateFluoranthenePyreneButy Ibenzylohthal ate3 r 3 '-DichlorobenzidineBen2o(a)anthracene.,, ... ..Chrysenebis(2-Ethylhexyl )phthalateDi-n-octylphthalateBenzo ( b ) f luorantheneBenzo(k ) f luorantheneBenzo (a )pyreneIndeno( lf 2 f 3-cd)pyreneDiber.zo ( a y-h) anthracene, ,, ,,,, ..Benzo ( g , h , i )perylene

150.000!10.000150.000!50.000 !10.000110.000110.000!10.000110.000150.000150.000 |10.000 110.000110.000150.000!10.000 |10.00010.900110.000110.000110.000120.000 !10.000]10.00017.00010.300110.000110.000110.000110.000110.000110.0001

1

uuuuuuuuuuuuuu •uuuJuuuuuuJBJuuuuu



ID EPA SAMPLE NO.PESTICIDE ORGANICS ANALYSIS DATA SHEET _______________

Name: YORK LABS/CT Contract: 6S-W8-0021 CBQOS000677.ab Code: YORK Case No.: 12512 SAS No.: ______ SDG No.: C8Q02

latrix: (soil/water) WATER Lab Sample ID: 1496019

5amole wt/vol.: 1000. Cg/mL) ML Lab File ID: ________

.evel: (low/med) LOW Data Received: 08/24/89

; Moisture: not dec. ____ dec. _____ Date Extracted: 03/25/89

Ixtraction: (SeoF/Ccnt/Scnc) SEPF Date Analyzed: 09/01/89

iPC Cleanuo: (Y/N) N pH: Dilution Factor: 1


319-84-6 ——————— alpha-3HC_________319-85-7——————beta-3HC__________319-86-8——————delta-BKC________53-39-9-———__—gamma-BHC (Lindane).76-44-8———— ——Heotachlor________309-00-2- —————— Aldrin____________1024-57-3---———Heptachlor eooxide,959-98-8— ————— Endosulfan I_____60-57-1 ———————— Dieldrin_________72-55-9 ————————— 4. 4'-DDE__________72-20-8————————Endrin___________33213-65-9—————Endosulfan II____72-54-8—————————4.4'-DOD__________1031-07-8—-—--Endcsulfan sulfate50-29-3 ———————— 4,4'-DDT_________\72-43-5-----—--Methoxychlor_____53494-70-5----—Endrin ketone____5103-71-9——————aloha-Chlordane__5103-74-2----——gamma-Chlordane__8001-35-2—-----Toxaohene________12674-11-2—————Aroclor-1016______11104-28-2— ——— Aroclor-1221_____11141-16-5—————Aroclor-1232_____53469-21-9—————Aroclor-1242______12672-29-6—————Aroclor-1248______11097-69-1 ————— Aroclor-1254_____11096-82-5—————Aroclor-1260_____

O.OSOJUO.OSOJUO.OSOJUO.OSOJUO.OSOJUO.OSOJUO.OSOJUO.OSOJU0.10JU0.10JU0.10JU0.10!U0.10JU0.10JU0.10JUO.SOJU0.10JUO.SOJUO.SOJU1.0JU

O.SOJUO.SOJUO.SOJUO.SOJUO.SOJU1.0JU1.0JU


IS EPA SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET _________________

I CBQ09 |ab Name: YORK LABS/CT Contract: 68-W8-0021 t________o_£vr>d_h n——————U U U1 o oab Code: YORK Case No.: 12512 SAS No.: SDG No.: C3Q02


ample wt/vol: 1000 (g/mL) ML Lab File ID: >C4575






108-95-2 ———111 —4.-L— .4.— —

95-57-8 —————541-73-1 -——106-46-7 — —100-51-6 ———gc_ qn_l— __95-48-7 —————108-60-1 ————106-44-5 ————621-64-7 ————67-72-1 —————98-95-3 —————78-59-1 —— —88-75-5 —————105-67-9 ———65-85-0 —————111-91-1 ————120-83-2 ————120-82-1 ———91-20-3 —————106-47-8 ———87-68-3 —————c q_ e: n — 7 _____91-57-6 —————77-47-4 —————88-06-2 —————qc_ gc_4. __ __

91-58-7 —————88-74-4 —————131-11-3 ————

• 208-96-8 ———606-20-2 ————

——— Phenol——— bisf 2-Chloroethyl ) ether., .,,,,.—— -2-Chloroohenol „, „ ,, ,——— 1 e 3-Dichlorobenzene——— 1 r 4-Dichlorobenzene——— Benzyl alcohol——— 1 r 2-Dich.lorobenzene „.„,.,„„,„ ,.——— 2-Methylphenol——— bis ( 2-Chloroisopropyl ) ether_——— 4-Methvlphenol „, ,, .,——— N-Ni troso-di-n-prooy lamine——— Hexachloroethane——— Nitrobenzene,,.. ...——— Isoohorone——— 2-Ni troohenol „——— 2 f 4-Dimethylphenol , „. ..,, ,——— Benzoic acid.,. „——— bis ( 2-Chloroethoxy Jmethane——— 2 f 4-Dichlorophenol——— 1 . 2 f 4-Trichlorobenzene——— Naohtha 1 ene——— 4-Chloroanil ine——— Hexachlorobutadiene——— 4-Chl or o-3 -methyl phenol——— 2 -Methyl naphthalene——— Hexachlorocyclopentadiene __——— 2 f 4 f 6-Trichlorophenol——— 2,4 . 5-Trichloroohenol_——— 2-Chloronaphthalene .——— 2-Mitroani line , ,,.,——— Dimethylphthalate———— Acenaohthylene .,,.,,.,,,,,, ,,.,,.,—— -2 , fi-Dini trotoluene

110.000110.000 I10.000!10.000 I10.000 110.000 110.000110.000110.000110.000110.000110.000 |10.000110.000110.000!10.000150.000110.000110.000110.000 |10.000110.000!10.000!10.000 |10.000110.000110.000150.000110.000150.000110.000110.000110.000!

1

uuuuuuuuuuuuuuuuuuuuuuuuuuuuuuuu.u

FORM I SV-1 1/87 Rev,

AR3065I+6

1C ' E?A SAMPLE NO.SEMIVOLATILE CRGANIC5 ANALYSIS DATA SHEET _______________

II C3Q09 .

ab Name: YORK LA3S/CT Contract: 68-W8-0021 I_______ OGC1.'

: YORK Case No.: 12512 SAS No.: SDG No.: C3Q02






PC Cleanup: (Y/N) N pH: Dilution Factor:


83-32-9 — ———51-28-5 —————100-02-7 — —132-64-9 ———121-14-2 ———84-66-2 ————7005-72-3 ——86-73-7 ————100-01-6 ———f A M CO 4534-52-1 — —86-30-6 ————101-55-3 ———118-74-1 —— -87-86-5 — ——85-01-8 —————120-12-7 ————84-74-2 —————206-44-0 —— -129-00-0 ————85-68-7 —————

56-55-3 —————218-01-9 ————1^ •? a * ~r

117-84-0 ———2Q5 — QQ—.O — . — .

207-08-9 ————50-32-8 —————iqo "5Q_ C— '— _53-70-3 —————

——— 3-Ni troanil ine „ , ,, ,., ,,,„,———— Acenaah.th.en.e „— — 2 , 4-Dini troohenol „ _ , .,_,——— 4-Mi trooh.en.ol——— Diber.zof uran,. _„,_,„——— 2r4-Dinitrotoluene——— D i e thy 1 ph. tha late——— 4-Chlorophenyl -pheny 1 ether _——— Fluorene——— 4-Mi troani 1 ine „.,, ,.,,., „,„...„.——— 4 , 6-Dini tro-2-methyl phenol _——— N-Nitrosodiphenylamine (1) _——— 4-Sromopheny 1 -pheny 1 ether __——— Kexachlorobenzene „ ,——— Pentachloroohenol——— Phenanthrene _——— Anthracene .,— ! — Di-n-buty Iphtha late „——— F luoranthene ,.,.,__..——— Pyrene——— Sutylbenzylphthalate,——— 3 j. 3 '-Dichlorobenzidine _..——— Benzo (a ) anthracene ,, , „——— Chrysene- - bis(2-Ethylhexyl )phthalate_——— Di-n-octylphthalate, „ , ..,„,——— Berrzo(b)f luoranthene——— 3enzo ( k ) f luoranthene——— Benzo ( a ) pyrene——— Indenof 1 f 2 , 3-cd) pyrene ... „——— Diben.zo(arh) anthracene, , „.„. ,.,,..——— Benzof gfhf i )perylene

150.000110.000 I50.000150.000 I10.000110.000 110.000110.000110.000150.000150.000 |10.000110.000 I10.000150.000110.000110.000110.000110.000110.000!10.000!20.000110.000110.000 I3.000110.000110.000110.000110.000!10.000110.000110.000 |

1

uuuuuuuuuuuuuuuuuuuuuuuuJBuuuuuuu

- Cannot be separated from Diphenylamine


ID EPA SAMPLE NO.PESTICIDE CRGANICS ANALYSIS DATA SHEET ______________

Name: YORK LA8S/CT Contract: 6S-W8-0021C8Q09 0006

.ab Code: YORK Case No.: 12512 SAS No.: ______ SDG No.: C8Q02

tatrix: (soil/water) WATER Lab Sample ID: 1496002

;ample wt/voL: 1000. Cg/mL.) ML Lab File ID: ________

.evel: (low/med) LOW Date Received: 08/22/89

; Moisture: not dec. ____ dec. _____ ' Date Extracted: 08/24/89

Ixtracticn: fSeoF/Cont/Scnc) SEPF Date Analyzed: 08/30/89

;PC Cleanuo: (Y/N) N pH: Dilution Factor: 1


319-84-6 —— —— — aloha-SHC_________319-85-7———————beta-3HC____________319-86-8 ——————— delta-BHC_________58-39-9—— ————— gamma-3HC (Lindane).76-44-8———————Heotachlor___________3O9-00-2——————Aldrin_________1024-57-3———-—Heotachlor epoxide.959-9S-8--—-——Endcsulfan I_____60-57-1———————Dieldrin____________72-55-9 —— ——— — 4. 4'-DDE____________72-20-8————————Endrin______•33213-65-9---——Endosulfan II____72-54-8—————————4. 4'-ODD__________1031-07-3—————Endosulfan sulfate.50-29-3—————————4. 4'-DOT_________72-43-5-———————Methoxychlor______53494-70-5—————Endrin ketone____5103-71-9- ————— alpha-Chlordane__5103-74-2-------gamma-Chlordane_____8001-35-2- — — --Toxaohene__________12674-11-2—————Aroclor-1016______11104-28-2—————Aroclor-1221_____11141-16-5—————Aroclor-1232______53469-21-9—————Aroclor-1242_____12672-29-6—————Aroclor-1248_____11097-69-1 ————— Aroclor-1254______11096-82-5—————Arcclor-1260____

O.OSOJUO.OSOJUO.OSOJUO.OSOJUO.OSOJUO.OSOJUO.OSOJUO.OSOJU0.10IU0.10JU0.10JU0.10JU0.10JU0.10JU0.10JUO.SOJU0.10JUO.SOJUO.SOJUl.OJU

O.SOJUO.SOJUO.SOJUO.SOJUO.SOJUl.OJUl.OJU


IB EPA SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET _______________

I C3Q10 Iab Name: YORK LABS/CT Contract: 68-W8-0021 I ______________ I

e: YORK Case No.: 12512 SAS No.: SDG No.: C3Q02qp p -j f *~

iltrix: (soil/water) WATER Lab Sample ID: 1496010


svel: (low/med) LOW Date Received: 08/23/89


Ktraction; ( SepF/Cont/Sonc ) SEPF Date Analyzed: 09/11/89



108-95-2———————Phenol____________________I 10.000! U111-44-4———————bis(2-Chloroethyl)ether____1 10.0001 U95-57-8 ———— ——— 2-Chlorophenol____541-73-1 —————— 1, 3-Dichlorobenzene.106-46-7——————l, 4-Dichlorobenzene.100-51-6———————Benzyl alcohol____95-50-1 ——————— 1,2-Dichlorobenzene_______95-48-7———————2-Methylphenol___________108-60-1——————bis(2-Chloroisopropyl )ether_106-44-5 ——————— 4-Me thy 1 phenol____________621-64-7———————N-Ni troso-di-n-propylamine_67-72-1————————Hexachl or oe thane__________98-95-3————————Nitrobenzene______________78-59-1 ———————— Isophorone________________88-75-5 ———————— 2-Ni trophenol_____________105-67-9 ——————— 2 , 4-Dimethylphenol_________65-85-0———————Benzoic acid_____________111-91-1——————bis (2-Chloroethoxy) me thane_120-83-2 ——————— 2 , 4-Dichlorophenol_________120-82-1——————1,2,4-Tr ichlorobenzene_____91-20-3————————Naphthalene_______________106-47-8 ——————— 4-Chloroaniline___________87-68-3————————Hexachl orobutadiene________59-50-7 ———————— 4-Chloro-3-methylphenol____91-57-6————————2-Methylnaphthalene.77-47-4———————Hexachl or ocyclopent ad iene.88-06-2 ———————— 2 , 4 , 6-Tr ichlorophenol____95-95-4 ———————— 2 , 4 , 5-Tr ichlorophenol____91-58-7———————2-Chloronaphthalene_____88-74-4———————2-Ni troar.il ine_________131-11-3———————Dime thy Iphtha late_______208-96-8——————Acenaph thy Iene_________606-20-2 ——————— 2, 6-Dinitro toluene______

0.4001 JB10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.000! U10.000! U10.0001 U10.000! U10.0001 U10.0001 U10.000! U10.0001 U50.0001 U10.0001 U10.000! U10.0001 U10.000! U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U50.0001 U10.0001 U50.0001 U10.0001 U10.0001 U10.0001 u'___I_


&R30S5U9

1C EPA SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET _______________

I II C3Q10 I

ab Name: YORK LA3S/CT Contract: 68-W8-0021 I Ann 1ab Code: YORK Case No.: 12512 SAS No.: SDG No.: CBQ02





xtraction: (SepF/Cont/Sor.c) SEPF Date Analyzed: 09/11/89



%

I99-09-2 — -83-32-9 — -51-28-5 — -100-02-7 —132-64-9 —121-14-2 —84-66-2 — -7005-72-3-86-73-7 — -100-01-6 —534-52-1 —86-30-6 — -101-55-3 —118-74-1 —87-86-5 — -85-01-8 —— -120-12-7—84-74-2 — -206-44-0 —129-00-0 —85-63-7 — -Q 1 —Q 4. — 1 — -

56-55-3 — -218-01-9 —1 -t •? O 1 *7

117-84-0 —205-99-2 —207-08-9 —50-32-8 — -1 Q "i "3 Q S:

53-70-3 ——191-24-2 —

—————— 3-Mitroani 1 ine

—————— 2 f 4-Dini troohenol , „„ „ „—————— 4-Ni trooheno 1—————— Dibenzof uran- ————— 2 f 4-Dini trotoluene ,————— -Diethy Iph thai ate,,, ,. ,,„ ,„,_————— 4-Chlorophenyl -pheny 1 ether _—————— Fluorene,,—————— 4-Ni troani 1 ine————— 4 , 6-Dini tro-2-methy Iphenol _————— N-Ni tro sod i pheny lam ine ( 1 ) _— ———— 4-Bromophenyl -pheny 1 ether __- ————— Hexachlorobenzene,—————— P<=>ntachlorophenol—————— Phenanthrene—————— Anthracene—————— Di-n-buty Iphtha late—————— F luoranthene—————— Pyrene—————— Butylbenzy Iphtha late—————— 3 P3 '-Dichlorobenzidine—————— Benzo ( a ) anthracene—————— Chrysene————— bis(2-Ethylhexyl )ph thai ate _—————— Di-n-octylphthalate—————— Benzofb)f luoranthene—————— Benzo f k ) f luoranthene—————— Benzo f a ) pyrene—————— Indeno f 1 1 2 , 3-cd ) pyrene—————— D i benzo( a rh) anthracene.,—————— Benzof gfhf i )perylene

150.000110.000 I50.000150.000!10.000110.000 |10.000110.000 |10.000!50.000 |50.000110.000 |10.0001

. 10.000150.000110.000110.00010.800 |10.000110.000110.000120.000110,000!10.00015.00XDI10.000 |10.000110.000!10.000110.000 !10.000110.0001

I

uuuuuuuuuuuuuuuuuJuuuuuuJBuuuuuuu-


FORM I SV-2 1/87 Rev.i

AR306550

ID EPA SAMPLE NO,PESTICIDE ORGANICS ANALYSIS DATA SHEET _______________

Name: YORK LA8S/CT Contract: 6S-W8-0021csQio

.ab Code: YORK Case No.: 12512 SAS No.: ______ SOG No.: CBQ02


Sample wt/vol: 1000. (g/mL) ML Lab File ID: ________

.evel: (lcw/me.d) LOW Date Received: 08/23/89

'a Moisture: not dec. ____ dec. _____ Oats Extracted: 03/24/89

Extraction: (SepF/Cont/Scnc) SEPF Date Analyzed: 08/30/89

Clsanuo: (Y/N) N cH: Dilution Factor: 1

CONCENTRATION UNITS:CAS NO. COMPOUND Cug/L or ug/Kg) UG/L Q

319-84-6 —————— aicha-BHC________319-S5-7——————beta-3HC_________319-86-8——————delta-3HC________53-89-9--——---gamma-3HC (Lindane).76-44-8——-————Heotachlor________[309-00-2——————Aldrin____________1024-57-3--———Heotachlor eooxide959-98-8———————Endosulfan I_____'_60-57-1———————Dieldrin_________72-55-9——— ———— 4, 4 '-DDE__________72-20-8————————Endrin___________33213-65-9—————Endosulfan II____72-54-8————————4,4'-DDD_________1031-07-8————Endcsulfan sulfate.50-29-3————————4,4'-DDT__________72-43-5 ——— —— — Methoxychlor_____53494-70-5-————Endrin ketone____5103-71-9-————-alpha-Chlordane__5103-74-2—— ——— gamma-Chlordane__S001-35-2-------ToxaDhene________12674-11-2—————Aroclor-1016_____11104-28-2—————Aroclor-1221_____11141-.16-5—————Aroclor-1232_____53469-21-9—————Aroclor-1242_____12672-29-6—————Arcclor-1248_____11097-69-1————Aroclor-1254_____11096-82-5 ————— Aroclor-1260_____

O.OSOJUO.OSOJUO.OSOJUO.OSOJUO.OSOJUO.OSOJUO.OSOJUO.OSOJU0.10JU0.10JU0.10JU0.10JU0.10JU0.10JU0.10JUO.SOJU0.10JU0.043!J0.068JJ

l.OJUO.SOJUO.SOJUO.SOJUO.SOJUO.SOJUl.OJUl.OJU


[\R3Q6551

13 E?A SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET ________________

I II CBQ11 I

ab Name: YORK LA3S/CT Contract: 68-W8-0021 I______________I

ab Code: YORK Case No.: 12512 SAS No.: SDG No.: CBQ02^fl 0 1 J

atrix: (soil/water) WATER Lab Sample ID: 1496011 °! **'J-3




xtraccion: (SepF/Cont/Sonc) SEPF Date Analyzed: 09/11/89



108-95-2———————Phenol___________________111-44-4——————bis (2-Chloroethy 1) ether____95-57-8 ——————— 2-Chlorophenol____________541-73-1 ——————— 1, 3-Dichlorobenzene________106-46-7———————1, 4-Dichlorobenzene_______100-51-6——————Benzyl alcohol____________95-50-1 ———————— 1, 2-Dichlorobenzene___________95-48-7————————2-Methyl phenol____________108-60-1———————bis(2-Chloroisopropyl )ether_106-44-5 ——————— 4-Methyl phenol____________621-64-7———————N-Ni troso-di-n-propylamine_67-72-1————————Hexachl oroe thane__________98-95-3————————Nitrobenzene___________________78-59-1 ———————— Isoohorone___________________88-75-5 ——————— 2-Ni trophenol_____________105-67-9 —————— 2 , 4-Dimethylphenol_________65-85-0————————Benzole acid_____________111-91-1——————bis (2-Chloroethoxy) me thane_120-83-2 —————— 2 , 4-Dichlorophenol________120-82-1 ——————— 1, 2 , 4-Trichlorobenzene_____91-20-3———————Naphthalene______________106-47-8 ——————— 4-Chloroani 1 ine___________87-68-3———————Hexachl or obu tad iene________59-50-7 ———————— 4-Chloro-3-me thy 1 phenol____91-57-6 ———————— 2-Me thy 1 naphtha Iene__________77-47-4———————Hexach 1 or ocycl open tad iene__88-06-2 ———————— 2, 4, 6-Trichlorophenol________95-95-4 ———————— 2 , 4 , 5-Tr ichlorophenol______91-58-7———————-2-Chloronaphthalene_______88-74-4———————2-Nitroani line______________131-11-3——————Dime thy Iphtha late_________208-96-8———————Acenaph thy Iene____________606-20-2 ——————— 2 ,6-Dinitrotoluene________

10.0001 U10.000! U0.3001 JB10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.000! U10.0001 U10.0001 U10.000! U10.0001 U10.0001 U10.0001 U10.0001 U50.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.000! U10.000! U10.0001 U10.0001 U10.0001 U10.0001 U50.0001 U10.0001 U50.0001 U10.0001 U10.0001 U.10.0001 U

FORM I SV-1 _ 1/87 Rev.AR3065b2


I !I CBQ11 I

ab Name: YORK LABS/CT Contract: 63-W8-0021 I__________- .- -I _{»i i f,' T -..'• J o O 1 <j CCode: YORK. Case No.: 12512 SAS No.: SDG No.: CBQ02





Ktraction: (SepF/Cont/Scnc) SEPF Date Analyzed: 09/11/89

?C Cleanup: (Y/N) N pH: Dilution Factor: 1


99-09-2 ———— ——— 3-Nitroani 1 ine.83-32-9———————Acer.aohth.ene__51-28-5 ——————— 2,4-Dini trophenol_______100-02-7 —————— 4-Ni trophenol___________132-64-9——————Diber.zofuran____________121-14-2 ——————— 2, 4-Din.itrotoluene_______84-66-2———————Diethy Iphtha late_________7005-72-3——————4-Chlorophenyl-pheny 1 ether.86-73-7————————Fluorene_________________100-01-6——————4-Nitroani 1 ine__________534-52-1——————4,6-Dinitro-2-methylphenol_86-30-6———————N-Nitrosodiphenylamine (1)_101-55-3 ——————— 4-Bromophenyl -pheny 1 ether_118-74-1——————Hexachl orobenzene________87-86-5———————Pentachlorophenol_______85-01-8 ——————— Phenanthrene____________120-12-7——————Anthracene______________84-74-2————————Di-n-buty Iphtha late______206-44-0——————F luoranthene____________129-00-0——————Pyrene_________________85-68-7————————Butylben.zylph.thal ate_____91-94-1 ———————— 3 ,3 '-Dichlorobenzidine___56-55-3————————Benzo (a) anthracene_______218-01-9———————Chrysene________________117-81-7——————bis(2-Ethylhexyl)phthalate.117-84-0———————Di-n-octylphthalate______205-99-2———————Benzo (b)f luoranthene_____207-08-9——————Benzo(k)£ luoranthene_____50-32-8————————Benzo (a) pyrene———————————193-39-5 ——————— Indeno (1,2 ,3-cd)pyrene___53-70-3————————Dibenzo( a ,h) anthracene___191-24-2———————Ber.zo(g,h, i )perylene—————

I50.0001 U10.0001 U50.000! U50,0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U50.0001 U50.0001 U10.0001 U10.0001 U10.000! U50.0001 U10.0001 U10.0001 U0.7001 J10.0001 U10.0001 U10.0001 u20.000! U10.0001 U10.0001 U6.0001 JB10.0001 U10.000! U10.000! U10.0001 u10.000! U10.0001 u10.000 I U.



ID .EPA SAMPLE NO.PESTICIDE ORGANICS ANALYSIS DATA SHEET _____________

.ab Name: YORK LASS/CT Contract: 68-W8-0021C8Q11 0008$


tatrix: (soil/water) WATER Lab Sample ID: 1496011

Jamole wt/voL: 1000. (g/mL) ML Lab File ID: _________

.evel: (low/med.) LOW Data Received: 08/23/89

; Moisture: not dec. _____ dec. _____ Date Extracted: 08/25/89

."xtraction: CSeoF/Cont/Sonc.) SEPF Date Analyzed: 09/01/89



319-84-6 ——————— alcha-3HC_________319-85-7—— ———— beta-3HC_________319-86-8———————delta-3HC_________58-89-9———————gamma-8HC (Lindane).76-44-8 ———————— Heotachlor_______'309-00-2———————Aldrin______________1024-57-3—————Heotachlor eooxide959-98-8———————Endosulfan I_____60-57-1———————Dieldrin_________72-55-9————————4.4'-DDE_________72-20-8————————Endrin____________33213-65-9—————Endosulfan II____72-54-8————————4,4'-DDD___________1031-07-8-----—Endosulfan sulfate50-29-3————————4,4'-DDT_________'72-43-5-——————Methoxychlor_____53494-70-5————Endrin ketone____5103-71-9——————aloha-Chlordane___5103-74-2-------gamma-Chlordane___8001-35-2 —————— Toxaohene________12674-11-2—————Arcclor-1016_____11104-28-2—————Aroclor-1221_____11141-16-5————Aroclor-1232_____S3469-21-9————Aroclor-1242_____12672-29-6—————Aroclor-1248_____11097-69-1 ————— Aroclor-1254_____11096-82-5 — —— -A redo r-1260_____

O.OSOJUO.OSOJUO.OSOJUO.OSOJUO.OSOJUO.OSOJUO.OSOJU0.050 J U0.10JU0.10JU0.10JU0.10JU0.10JU0.10JU0.10JUO.SOJU0.10JUO.SOJUO.SOJUl.OJU



13 EPA SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET ' _______________

! I

ab Name: YORK LABS/CT Contract: 63-W8-0021 I C3Q12 QOGJ.TOYORK Case No.: 12512 SAS No.: SDG No.: CBQ02





xtraction: ( SepF/Cont/Sonc ) SEPF Date Analyzed: 09/10/89



1108-95-2 — —111-44-4 ———95-57-8 ————

106-46-7 ———100-51-6 ———95-50-1 —————Q s; A A "7 —— —

108-60-1 ———106-44-5 ———621-64-7 ———67-72-1 —————98-95-3 —————78-59-1 —————po 7C_ c:__ __

105-67-9 ———65-85-0 ————111-91-1 ———•ion P. *3 oi •? n P. •> t _ _

106-47-8 ———87-68-3 ————59-50-7 ————91-57-6 ————77-47-4 ————o o r\ f *\

QC. QC «_ _— ,—

Q 1 C. Q *7

£ P. "74. — d. — — — — —

131-11-3 ———o n p c\ fi p606-20-2 ———

p^«^.f^(^l«T**— »A_i»W*/1 ^ A 4» l>. A •"•

——— 2-Ch.lorocher..ol ,——— 1 , 3-Dichlorobenzene——— 1 . 4-Dich.lcrobenzene——— Her,zyl alcohol.,.. „- — -1 f 2-Dichlorobenzene,, ,. , _, , „„ ,———— 2 -Methyl phenol, , ,——— bis(2-Chloroisopropyl ) ether——— 4 -Me thy 1 phenol ,, ,, ., .——— N-Nitroso-di-n-propylamine——— Hexachloroethane——— Ni trobenzene——— Isoohorone , . ..——— 2-Nitrophenol——— 2f -Dimethylphenol. , ,,„.,„ „ „._„,.,.——— Benzoic acid——— bis(2-Chloroethoxy ) me thane _——— 2 , 4-Dichlorophenol „ , „,, „, . , ..——— l , 2 , 4-Tr ichlorobenzene _ . __——— Naphthalene——— 4-Ch.loroani 1 ine——— Hexachlorobutadiene——— 4-Ch.loro-3-methylph.enol., ,„ „„.——— 2-Methylnanhthalene., .,.„ .„„,. ,..,.,,——— Hexachlorocyclopentadiene __——— 2 r 4 f 6-Trichlorophenol——— 2 rir5-Tr ichlorophenol——— 2-Chloronaphthalene——— 7--Mit.roan.il ine———— Dimethylphthalate ... „ „———— Af-^nanhthy^ ene ,——— ?. , 6-Dini tvntoluene „ ,.

110.000110.000 10.400 110.000110.000!10.000110.000110.000110.000110.000!10.000110.000 110.000!10.000110.000110.000150.000110.000 I10.000110.000110.000110.000110.000110.000 I10.000110.000110.000150.000110.000150.000110.000 I10.000110.0001

1

uuJBuuuuuuuuuuuuuuuuuuuuuuuuuuuuuu


ftR306555

1C EPA SAMPLE NO.SEMIVOLATILE CRGANICS ANALYSIS DATA SHEET ______________

Ii CBQ12 nnni'ab Name: YORK LASS/CT Contract: 68-W8-0021 I________U U U li


atrix: (soil/water) , WATER Lab Sample ID: 1496020

ample wt/vol: 1000 (g/mL) ML Lab File ID: >HS710



xtraction: (SepF/Cont/Scr.c) SEPF Date Analyzed: 09/10/89



99-09-2 ————— -83-32-9 ————— -51 28-5 ————— -

——— 3-Mi troani 1 ine ,——— Acer.achthene

100-02-7 ———————— 4-Nitroohenol132-64-9 ———— -121-14-2 ——— -84-66-2 ————— -7005-72-3 —— -86-73-7 ————— -100-01-6 ———— -S"3A — <5 7 — 1 _ ___ -

86-30-6 ————— -101-55-3 ———— -118-74-1 ———— •87-86-5 ————— -85-01-8 ————— -120-12-7 ——— -84-74-2 ————— -206-44-0 ———— -129-00-0 ———— -85-68-7 ————— -91-94-1 ————— -56-55-3 ————— -218-01-9 ———— -11 7 *a 1 "7117-84-0 ———— -205-99-2 ———— -207-08-9 ———— -50-32-8 ————— -193-39-5 ———— -53-70-3 ————— -1 <5 1 — "> 4 — "> — — .— -

——— Dibenzofuran——— 2 t A-D in itro toluene——— Diethylphthalate——— 4-Chlorophenyl -pheny 1 ether _——— Fluorene——— 4-Ni troani 1 ine——— 4,6-Dini tro- 2 -methyl phenol _——— N-Nitrosodiphenylamine (1)——— 4 -Bromoohenyl -pheny 1 ether——— Hexachlorobenzene _——— Pentachlorophenol..——— Phenanthrene——— Anthracene——— Di-n-butylphthalate ..——— F luoranthene——— Pyrene——— Butylbenzylphthalate——— 3 .3 '-Dichlorobenzidine_

——— Chrysene——— bis(2-Ethylhexyl Jphthalate——— Di-n-octylnh thai ate——— 3enzo(b)f luoranthene——— Ben.zo(k)f luoranthene_ _.——— Benzo ( a } pyrene——— Indenofl ,2 f 3-cd )pyrene_ _——— Dibenzo ( a f h ) anthracene——— 3enzo(grhr. i Jperylene

150.000110.000 I50.000150.000!10.000110.000110.000110.000110.000150.000 |50.000]10.000110.000110.000 I50.000110.000110.00010.600110.060110.000!0.100120.000110.000110.000 I9.00010.400 !10.000110.000110.000110.000 !10.000!10.0001

1

uuuuuuuuuuuuuuuuuJuuJuuuJBJuuuuU -u


FORM I SV-2 i/87 Rev.AR306556

ID • EPA SAMPLE NO.PESTICIDE ORGANICS ANALYSIS DATA SHEET _______________

Name: YORK LA8S/CT Contract: 68-W8-0021CSQ12 000691

.ab Code: YORK Case No.: 12512 SAS No.: ______ SDG No.: C8Q02


Jample wt/vol: 1000. (g/mL) ML Lab File ID: ________


. Moisture: not dec. ____ dec. _____ Date Extracted: 08/25/89

•xtraction: (SeoF/Cont/Scnc) SEPF Date Analyzed: 09/01/89

;PC Cleanuo: (Y/N) N pH: Dilution Factor: 1


319-84-6 ——— ——— alDha-8HC._________319-85-7-- ————beta-3HC____________319-86-8———————delta-SHC_________58-89-9---------gamma-3HC (Lindane).76-44-8—— ————— Heptachlor________309-00-2———————Aldrin____________1024-57-3---———Heptachlor epoxide959-98-8——————Endosulfan I_____60-57-1———————Dieldrin________72-55-9————————4, 4 '-DDE__________72-20-8———————Endrin__________33213-65-9-————Endosulfan II____72-54-8—————————4,4'-DDD__________1031-07-8-----—Endosulfan sulfate.50-29-3—————————4, 4'-DOT_____'72-43-5 ———— - —— Methoxychlor_____53494-70-5- ———— Endrin ketone______5103-71-9—————aloha-Chlordane__5103-74-2---——gamma-Chlordane__8001-35-2———-Toxaohene________12674-11-2—————Aroclor-1016_____11104-28-2—————Arcclor-1221_____11141-16-5—————Aroclor-1232_____53469-21-9—————Aroclor-1242_____12672-29-6—————Arcclor-1248_____11097-69-1 ————— Aroclor-1254______11096-82-5—————Aroclor-1260_______

O.OSOJU0.050IUO.OSOJUO.OSOJUO.OSOJUO.OSOJUO.OSOJUO.OSOJU0.10JU0.10JU0.10JU0.10JU0.10JU0.10JU0.10JUO.SOJU0.10JUO.SOJUO.SOJUl.OJU

O.SOJUO.SOJU0.50JUo.soiuO.SOJUl.OJUl.OJU


AR30S557

1C EPA SAMPLE NO.SEMIVOLATILE CRGANICS ANALYSIS DATA SHEET _______________

I C3Q13ab Name: YORK LA3S/CT Contract: 68-W8-0021 I_______

ab Code: YORK Case No.: 12512 SAS No.: . SDG No.: CBQ02








99-09-2 — ——83-32-9 —————

1 51-28-5 —————100-02-7 ———132-64-9 ————121-14-2 ———84-66-2 —————7005—72—3— _86-73-7 —————

——— 3-Nitroani I ine

——— 2 , 4-Dini troohenol——— 4-Mi troohenol , , „ „ „ „ „ ,——— Dibenzofuran——— 2r 4-Dinitrotoluene——— Diethylphthalate .——— 4-Chl or ophenyl -pheny 1 ether _——— Fluorene

100-01-6 ——————— 4-Mi troani 1 ine534 52 186-30-6 —————101-55-3 ————118-74-1 ———87-86-5 —————85-01-8 —————120-12-7 ————84-74-2 —————206-44-0 ———129-00-0 ———P. f. Q "7

<5 1 — Q4. — 1 _ —56-55-3 ————218-01-9 ———117-81-7 ———117-84-0 ———7 OS — 3<3— -7 — — .— .—207-08-9 ———50-32-8 —————

53-70-3 —————191-24-2 ———

——— 4, 6-Dinitro-2 -methyl phenol——— N-Nitrosodiphenylamine (1)——— 4 -Bromophenyl -pheny 1 ether __——— Hexachl orobenzene——— Pentachlorophenol——— Phenanthrene——— Anthracene- —— Di-n-butylphthalate., , .„„ „——— F luoranthene,,,——— Pyrene——— Butylbenzylphthalate. .——— 3 ,3 '-Dichlorobenzidine——— Benzo ( a ) anthracene——— Chrysene——— bis ( 2-Ethylhexyl Jphthalate _——— Di-n-octylphthalate.,,.. ,„, , „——— Benzo (b ) f luoranthene——— Benzo(k) f luoranthene———— Benzo (a ) pyr-ene „„ ,.„ ., „——— Indeno ( 1 , 2 f 3 -cd ) pyr ene_ „ ,——— D i benzo ( a ,h) anthracene.. ..- —— Ren.zo(q,h., i ) per y Iene ,.,.„„, „

150.000110.000150.000!50.000 |10.000110.000 |0.300110.000!10.000!50.000150.000!10.0001

. 10.000110.000150.000!10.000110.00010.600110.000110.000110.000120.000110.000110.000!10.000!0.400110.000!10.000110.000110.000110.000110.0001

uuuuuuJuuuuuuuuuuJuuuuuuBJuuuuuu


rsv-2 flR306558


Name: YORK LABS/CT Contract: 63-WS-0021cadis. __ _n . jOQG8S4!


tatrix: (soil/water) WATER - Lab Sample ID: 1496021

Samole wt/vol: 1000. (g/mL) ML Lab File ID: _________



Extraction: (SenF/Cont/Scnc) SEPF Date Analyzed: 09/06/89

5PC Cleanup: (Y/N) N pH: Dilution Factor: 1


319-84-6 ——————— aloha-SHC.319-85-7———————beta-3HC_319-86-3——————delta-3HC53-89-9———————gamma-BHC (Lindane)76-44-8———————Heotachlor309-00-2——————Aldrin___________1024-57-3——————Heotachlor eooxide959-98-8——————Endosulfan I_____60-57-1———————Dieldrin________72-55-9———————-4.-' -DDE__________72-20-8————————Endrin___________33213-65-9—————Endosulfan II____72-54-8———— ——— 4. 4'-ODD__________1031-07-8—--——Endosulfan sulfate50-29-3 ———————— 4, 4'-DOT__________~72-43-5-——————Methoxychlor_____53494-70-5————Endrin ketone____5103-71-9—————aloha-Chlordane__5103-74-2-------gamma-Chlordane__8001-35-2---———Toxaohene_______12674-11-2—————Arcclor-1016_____11104-28-2—————Aroclor-1221_____11141-16-5—————Aroclor-1232_____53469-21-9—————Aroclor-1242_____12672-29-6—————Aroclor-1248_____11097-69-1—————Aroclor-1254_____11096-82-5- ———— A redo r-1260_____

O.OSOJUO.OSOJUO.OSOJUO.OSOJUO.OSOJUO.OSOJUO.OSOJUO.OSOJU0.10JU0.10 JU0.10JU0.10JU0.10JU0.10JU0.10JUO.SOJU0.10JUO.SOJUO.SOJUl.OJU



AR306559

1C EPA SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET _______________

I C3Q14 Iab Name: YORK LABS/CT Contract: 68-WS-0021 I_____________

ab Code: YORK Case No.: 12512 SAS No.: SDG No.:



^vel: (low/med) LOW . Date Received: 08/24/89


xtracticn: (SepF/Cont/Sonc) SEPF Date Analyzed: 09/10/89



11 99-09-2 ———— •1 83-32-9 ————— -1 51 28 5

——— 3-Nitroan.i 1 ine——— Acenanhthene ,

| 100-02-7 ———————— 4-Nitroohenol132-64-9 ——— •121-14-2 ———— •84-66-2 ————— •7005-72-3 —— •86-73-7 ————— -100-01-6 ———— -534-52-1 ——— -86-30-6 ————— •101-55-3 ———— -118-74-1 ———— •Q "7 O C. C

85-01-8 ————— -120-12-7 ——— -84-74-2 ————— •206-44-0 ———— -129-00-0 ———— -85-68-7 ————— -9T Q _1 1

56-55-3 ————— -218-01-9 ———— -11 "7 a 1 •?117-84-0 ———— •205-99-2 ———— •207-08-9 ———— •50-32-8 ———— •iq-j_-3q_c_ ___ .

53-70-3 ————— •191-24 — ? ____ .

——— Dibenzofuran——— 2 f 4-Din.itrotoluene——— D ie thy Inhtha late——— 4-Chl orooheny 1 -pheny 1 e ther——— Fluorene——— 4-Ni troani line ,,,,——— 4 , 6-Dinitro-2-methylphenol _——— N-Nitrosodiphenylamine (1) _——— 4-Sromopheny 1-phenylether __——— Hexachl or obenzene——— Pentachlorophenol——— Phenanthrene——— Anthracene——— Di-n-buty Iphtha late——— F luoranthene——— Pyrene——— Butyl benzy Iphtha late——— 3 f 3 '-Dichlorobenzidine——— Benzo ( a ) anthracene——— Chrysene——— bis(2-Ethylhexyl)phthalate _——— Di-n-octylphthalate ,, , ,— — Benzo (b) f luoranthene- —— Benzo ( k ) f luoranthene—— -Benzo (a) pyrene , ,„.„ .. .„ ,„,——— Indeno( 1 f 2 r 3 -cd) pyrene, . ., ,„—— -Dibenzo fa .hi anthracene——— Benzof q.h, i )perylene

150.000110.000 I50.000150.000!10.000110.00010.300110.000 I10.000150.000150.000110.000110.000110.000150.000110.000110.00010.700110.000110.000110.000!20.000110.000!10.00016.000110.000110.000110.000110.000110.000110.000110.0001

1

uuuuuuJuuuuuuuuuuJuuuuuuJBuuuuuuu-



AR306560

ID EPA SAMPLE NO.PESTICIDE ORGANICS ANALYSIS DATA SHEET _______________

Name: YORK LA8S/CT Contract: 6S-W8-0021CBQ14 OOQ6S;<

.ab Code: YORK Case No.: 12512 SAS No.: _____ SDG No.: CBQ02

latrix: (soil/water) WATER Lab Samole ID: 1496022

Jamole wt/vol: 1000. (g/mL) ML Lab File ID: ________



Ixtracticn: (SeoF/Cont/Sonc) SEPF Date Analyzed: 09/06/89

JPC Cleanuo: (Y/N) N pH: Dilution Factor: 1


319-34-6 —————— -alpha-3HC_________319-85-7———————beta-3HC__________319-86-8———————delta-BHC_________58-89-9—-----—gamma-BHC (Lindane).76-44-8———————Heotachlor_______309-00-2———————Aldrin____________1024-57-3—————Heptachlor eooxide959-98-8——————Endosulfan I_____60-57-1 ———————— Dieldrin_________72-55-9—————————4. 4'-DDE__________72-20-8———————Endrin____________33213-65-9—————Endosulfan II_____72-54-8 ————————— 4,4'-DDD__________1031-07-8-------Endosulfan sulfate.50-29-3————————4.4'-DDT_________\72-43-5—- ————Methoxychlor_____53494-70-5—————Endrin ketone______5103-71-9----—-alcha-Chlordane__5103-74-2-------gamma-Chlordane__8001-35-2---——Toxaohene_______12674-11-2—————Aroclor-1016_____11104-28-2—————Arcclor-1221_____11141-16-5—————Aroclor-1232_____53469-21-9—————Aroclor-1242_____12672-29-6 ————— Aroclor-1248_____11097-69-1——---Aroclor-1254_____11096-82-5 — — — Aroclor-1260______

O.OSOJUO.OSOJUO.OSOJUO.OSOJUO.OSOJUO.OSOJUO.OSOJUO.OSOJU0.10JU0.10JU0.10JU0.10 J U0.10JU0.10JU0.10JUO.SOJU0.10JUO.SOJUO.SOJUl.OJU


FORM I PEST 1/87 Rev,AR306561

IB EPA SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET ____________

I !I C3Q15

ab Name: YORK LASS/CT Contract: 68-W8-0021 I________n n 0

ab Code: YORK Case No.: 12512 SAS No.: . SDG No.: CBQ02





xtraciion: (Se?F/Cont/Sonc) SEPF Date Analyzed: 09/11/89

PC Cleanup.- (Y/N) N pH: ' Dilution Factor: 1


108-95-2 ———111-44-4 ———95-57-8 ————541-73-1 ———106-46-7 ———100-51-6 ———95 — SO 1 — — — —95-48-7 ————1 n Q fi n «i106-44-5 ———621-64-7 ———67-72-1 ————98-95-3 —————78-59-1 —————83-75-5 —————105-67-9 ———65-85-0 —————111-91-1 ———120-83-2 ———1*> n fl o 191-20-3 —————106-47-8 ———87-68-3 —————K Q — en— 7— __ ,__91-57-6 -----77-47-4 — ——88-06-2 —— ~95-95-4 ——— —91-58-7 — ———88-74-4 —————131-11-3 —— -208-96-8 ——— -606-20-2 ————

——— Phenol——— bis(2-Chloroethyl ) ether——— 2-Chloroohenol——— 1 f3-Dichlorobenzene_ ,„ ,,——— 1 f 4-Dichlorobenzene „ _ _„——— Benzyl alcohol——— 1 . 2-Dichlorobenzene——— 2 -Methyl phenol——— bis( 2-Chloroisopropyl ) ether_——— 4-Methylphenol , „, ,——— N-Nitroso-di-n-propylamine _——— Hexachl oroe thane——— Nitrobenzene——— Isoohorone——— 2-Nitroohenol——— 2 f 4-Dimethylphenol ... ,„ ...——— Benzoic acid——— bis (2-Chloroethoxy)me thane _——— 2 f 4-Dichlorophenol——— 1 . 2 f 4-Tr ichlorobenzene——— Naohthalene.——— 4-Chloroani 1 ine——— Hexachlorobutadiene——— 4-Chloro-3-methylphenol——— 2-Methylnaphthalene——— Hexachl orocycl open tadiene __——— 2 . 4.6-Trichlorophenol_——— 2 . 4 . 5-Trichlorophenol——— 2-Chloronaphthalene——— 2-Ni troani 1 ine——— Dime thy Iphtha late——— Acenaphthy 1 ene——— 2 f 6-Dini tr-otoluener... .

110.000 I10.000 I0.400110.000110.000110.000110.000110.000110.000!10.000110.000110.000!10.000110.000110.000110.000150.000110.000110.000110.000!10.000110.000110.000110.000110.000110.000110.000150.000110.000!50.000!10.000110.000110.0001

1

uuJBuuuuuuuuuuuuu-uuuuuuuuuuuuuuLI-LTu

FORM i sv-i AR306562 1/87

1C • ' E?A SAMPLE NO.SEMIVCLATILE ORGANICS ANALYSIS DATA SHEET _ _____________ _

I I1 CBQ15 I

»Name: YORK LASS/CT Contract: 68-W8-0021 1 ______________ !

Code: YORK Case No.: 12512 SAS No.: SDG No.:



»vel: (low/med) LOW Date Received: 08/23/89


•ctraction: (SepF/Cont/Scr.c ) SEPF Date Analyzed: 09/11/89



99-09-2 ——————— 3-Nitroaniline8 3-32-9 ———————Acer.aphthene51-28-5 ——————— 2, 4-Dini trophenol_________100-02-7 —————— 4-Ni trophenol____________132-64-9——————Diber.zofuran_____________121-14-2 ——————— 2 , 4-Dinitrotoluene_________84-66-2————————Diethy Iphtha late__________7005-72-3-—————4-Chloropheny1-pheny1ether_86-73-7———————Fluorene________________100-01-6——————4-Ni troar.il ine___________534-52-1——————4,6-Dinitro-2-methylphenol_86-30-6————————N-Nitrosodiphenylamine (1)_101-55-3——————4-3romophenyl-pheny 1 ether__118-74-1——————Hexachl orobenzene______•87-86-5 ——————— Pentachlorophenol_________85-01-8———————Phenanthrene_____________120-12-7——————Anthracene_______________84-74-2————————Di-n-buty Iphtha late________206-44-0 ——————— F luoranthene______________129-00-0———————Pyrene____________________85-68-7————————Butyl benzy Iphtha late_______91-94-1 ———————— 3 , 3 '-Dichlorobenzidine_____5 6-55-3 ———————Benzo (a) anthracene________218-01-9——————Chrysene.117-81-7——————bis(2-Ethylhexyl)phthalate_117-84-0——————Di-n-octylphthalate_______205-99-2———————Benzo (b)f luoranthene______207-08-9———————Benzo (k) f luoranthene______50-32-8————————Benzo (a ) pyrene____________193-39-5 ——————— Indeno( 1,2, 3-cd) pyrene_____'53-70-3 ———————Dibenzo (a, h) anthracene_____191-24-2———————3enzo(g,h,i)perylene———————

50.000! U10.0001 U50.0001 U50.0001 U10.0001 U10.0001 U10.0001 U10.000! U10.000! U50.0001 U50.0001 U10.0001 U10.0001 U10.0001 U50.0001 U10.0001 U10.0001 U1.0001 J10.0001 U10.0001 U10.0001 U20.0001 U10.0001 U10.0001 U13.0001 B10.0001 U10.0001 U10.000! U10.0001 U10.0001 U10.0001 U10.0001 U

(1) - Cannot be separated from Dipheny1amine

FORM I SV-2 1/87 Rev,AR306563

ID EPA SAMPLE NO.PESTICIDE ORGANICS ANALYSIS DATA SHEET ________________

.ab Name: YORK LA8S/CT Contract: 68-W8-00210007jrC8Q15 u%/y '•

.ab Code: YORK Case No.: 12512 SAS No.: _____ SDG No.: CBQ02


Sample wt/voL: 1000. (g/mL) ML Lab File ID: ________


j Moisture: not dec. ____ dec. _____ Date Extracted: 08/25/89

Extraction: (SeoF/Cont/Sonc) SEPF Date Analyzed: 09/01/89

5PC Cleanuo: (Y/N) N pH: Dilution Factor: 1

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg.) UG/L Q

319-84-6 — ————— aloha-BHC319-85-7——————beta-3HC__319-86-8———————delta-3HC53-89-9—- ——— — gamma-BHC ( Lindane).76-44-8————————Heotachlor________309-00-2———————Aldrin____________1024-57-3-————Heotachlor eooxide959-98-8———————Endosulfan I_____60-57-1———————Dieldrin_________72-55-9 ———————— 4,4'-DDE_________72-20-8 ———————— Endrin_______'33213-65-9—————Endcsulfan II_____72-54-8- ——————— 4,4'-ODD_________1031-07-8—————Endcsulfan sulfate.50-29-3————————4,4'-DDT_________\72-43-5 — —————— Methoxychlor_____53494-70-5 ————— Endrin ketone____5103-71-9—————aloha-Chlordane__5103-74-2—————gamma-Chlordane__8001-35-2—————foxaohene__________12674-11-2—————Arcclor-1016_____11104-28-2————Aroclor-1221_____11141-16-5—————Aroclor-1232_____53469-21-9—————Aroclor-1242_____12672-29-6 ————— Aroclor-1248_____11097-69-1- ———— Aroclor-1254_____11096-82-5—————Aroclor-1260_____

O.OSOJUO.OSOJUO.OSOJUO.OSOJUO.OSOJUO.OSOJUO.OSOJUO.OSOJU0.10JU0.10JU0.10JU0.10JU0.10JU0.10JU0.10JUO.SOJU0.10JUO.SOJUO.SOJUl.OJU


FORM I PEST 1/87 Rev• • AR30656I*

13 EPA SAMPLE NOSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET _______________

I CBQ16ab Name: YORK LABS/CT Contract: 68-W8-0021 I______

FCode: YORK Case No.: 12512 SAS No.: SDG No.: CBQ02








108-95-2——————Phenol_____________111-44-4——————bis(2-Chloroethyl)ether.95-57-8 ———————— 2-Chlorophenol____________541-73-1 ——————— 1, 3-Dichlorobenzene________106-46-7 ——————— 1,4-Dichlorobenzene________100-51-6———————Benzyl alcohol____________95-50-1 ———————— 1, 2-Dichlorobenzene________95-48-7————————2-Methylphenol_____________108-60-1———————bis ( 2-Chloroisopropyl) ether_106-44-5 —————— 4-Methylphenol___________621-64-7——————N-Nitroso-di-n-propylamine_67-72-1 ———————Hexachl oroe thane__________98-95-3 —————— -Nitrobenzene_____________78-59-1———————Isophorone_______________88-75-5 ———————— 2-Ni trophenol_____________105-67-9———————2 , 4-Dimethylphenol________65-85-0————————Benzoic acid______________111-91-1——————bis (2-Chloroethoxy) me thane_120-83-2 ——————— 2, 4-D ichlorophenol_________120-82-1 ——————— 1,2,4-Trichlorobenzene_____91-20-3————————Naphthalene_______________106-47-8———————4-Chloroani 1 ine___________87-68-3———————Hexachl or obu tad iene_______59-50-7———————4-Chl or o-3-methyl phenol____91-57-6———————2-Me thy Inaphtha Iene_______77-47-4———————Hexachl or ocyclopentad iene__88-06-2 ———————— 2 , 4 , 6-Trichlorophenol______95-95-4 ———————— 2 , 4 , 5-Tr ichlorophenol______91-58-7 ———————— 2-Chloronaphthalene________88-74-4————————2-Nitroani 1 ine____________131-11-3———————Dime thy Iphtha late__________208-96-8———————Acenaphthylene____________.606-20-2———————2 , 6-Dinitrotoluene_____________

I10.0001 U10.0001 U0.4001 JB10.0001 U10.0001 U10.0001 U10.000! U10.0001 U10.0001 U10.0001 U10.0001 u10.000! U10.0001 U10.0001 U10.0001 U10.0001 U50.000! U10.000! U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.000! U10.000! U50.000! U10.000! U50.000! U10.0001 U10.0001 U.10.0001 U

.1_______I.

FORM I SV-l nDonrirrc 1/87 Rev-Anoubbbb

1C E?A SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

I| C3Q16

ab Name: YORK LASS/CT Contract: 68-W8-0021 I_______

ab Code: YORK Case No.: 12512 SAS No.: SDG No.: CBQ02 ~J







•CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q

I99-09-2 —————83-32-9 -----51-28-5 ————— •100-02-7 — —132-64-9 ————121-14-2 ———— -84-66-2 ————— •7005-72-3 ——86-73-7 ————— •100-01-6 ———— •534-52-1 ———— •O £ *5 f\ £.86 — 30 — 6 — — ——— -101-55-3 ———— •118-74-1 ———— •87-86-5 ————— •85-01-8 ————— -120-12-7 ———— -84-74-2 ————— •206-44-0 ———— -129-00-0 ———— •85-68-7 ————— •91-94-1 ————— -56-55-3 ————— •218-01-9 ———— -117-81-7 ———— -117-84-0 ———— •205-99-2 — -207-08-9 ——— •50-32-8 ———— •193-39-5 ——— •53-70-3 ———— •191-24-2 ———

——— 3-Mitroani 1 ine——— Acenaohthene. . ,,.„,——— 2 , 4-Dini troohenol——— 4_Ni troohenol——— Diber-zof uran——— 2 , 4-Dini troto luene „ , ,——— Diethylphthalate——— 4-Chl or oohenyl -pheny 1 ether——— Fluorene——— 4-Ni troani 1 ine.,,,,,, ,„, ,_..——— 4 , 6-Dini tro-2-methylphenol _——— N-Ni trosodiphenylamine (1) _——— 4-Bromophenyl -pheny 1 ether __——— Hexachl or obenzene——— Pentachlorophenol——— Phenanthrene——— Anthracene——— Di-n-buty Iphtha late——— F luoranthene——— Pyrene——— Butyl benzy Iphtha late——— 3 f3 '-Dichlorobenzidine——— Benzo (a ) anthracene——— Chrysene,.,, ,_„——— bis( 2-Ethylhexyl Jphthalate _——— Di-n-octylphthalate,,,. .,,——— Benzorblf luoranthene——— Benzo f k ) f luoranthene——— Benzo ( a ) pyrene——— Indenor 1 .2 , 3 -cd) pyrene .. _——— Diber.zo(a,h)anthracene——— Benzof q,hf i )nerylene

150.000110.000150.000150.000!10.000110.000!10.000!10.000!10.000150.000150.000110.000110.000110.000150.000!10.000110.00010.500110.000110.000110.000120.000110.000!10.000!5.000110.000110.000110.000110.000 |10.000110.000110.000 I

1

uuuuuuuuuuuuuuuuuJuuuuuuJBuuuuuuu



AR306566


Name: YORK LA8S/CT Contract: 68-W8-0021C3G16

.ab Code: YORK Case No.: 12512 SAS No.: ' SDG No.: C


Sample wt/vol: 1000. (g/mL) ML Lab File ID: _____

.evel: (low/med.) LOW Date Received: 08/23/89


:xtraction: (SecF/Cont/Scnc) SEPF Date Analyzed: 09/01/89



319-84-6 ——————— alpha-3HC_________319-85-7———————beta-3HC__________319-86-8———————delta-3HC_________58-89-9------—-gamma-3HC (Lindane).76-44-8————————Heotachlor________309-00-2———————Aldrin____________1024-57-3—————Heptachlor epoxide959-98-8——————Endosulfan I_____60-57-1———————Dieldrin_________72-55-9————————4,4 '-DDE_________72-20-8———————Endrin^___________33213-65-9—————Endcsulfan II____72-54-8—————————4,4'-DDD__________1031-07-8---—--Endosulfan sulfate.50-29-3—————————4,4'-DDT__________72-43-5- —— -———Methcxychlor_____53494-70-5------Endrin ketone____5103-71-9---——-alpha-Chlordane__5103-74-2—————gamma-Chlordane__8001-35-2---———foxaohene_______12674-11-2—————Arcclor-1016_____11104-28-2————Aroclor-1221_____11141-16-5—————Aroclor-1232_____53469-21-9—————Aroclor-1242_____12672-29-6—————Aroclor-1248_____11097-69-1————Aroclor-1254_____11096-82-5—————Aroclor-1260_____

O.OSOJUO.OSOJUO.OSOJUO.OSOJUO.OSOJUO.OSOJUO.OSOJUO.OSOJU0.10JU0.10JU0.10JU0.10JU0.10JU0.10 J U0.10JUO.SOJU0.10JUO.SOJUO.SOJUl.OJU



13 EPA SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET _______________

I CBQ17 -.--- J.ab Name: YORK LA3S/CT Contract: 68-W8-0021 I_______LLLLllZ42

ab Code: YORK Case No.: 12512 SAS No.: SDG No.: C3Q02

mtrix: (soil/water) WATER Lab Sample ID: 1496003







541-73-1- —————— 1, 3-Dichlorobenzene________106-46-7——————1,4-Dichlorobenzene_______100-51-6———————Benzyl alcohol______________95-50-1 ———————— 1, 2-Dichlorobenzene________95-48-7————————2-Methyl phenol____________108-60-1——————bis(2-Chloroisopropyl )ether_106-44-5 ——————— 4-Me thy 1 phenol____________621-64-7——————N-Nitroso-di-n-propylamine_67-72-1————————Hexachl oroe thane__________98-95-3————————Nitrobenzene_____________78-59-1 ———————— Isoohorone________________

I I108-95-2———————Phenol____________________I 10.0001 U111-44-4———————bis(2-Chloroethyl)ether____1 10.0001 U95-57-8 ———————— 2-Chlorophenol_____________I 10.0001 U

10.0001 U10.000! U10.0001 U10.0001 U10.0001 U10.0001 U10.000! U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U50.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U50.0001 U10.000! U50.0001 U10.0001 U10.0001 U10.0001 U

88-75-5 ———— ——— 2-Ni trophenol_____________10S-67-9 ——————— 2 , 4-Dimethylphenol_________65-85-0—————•——Benzoic acid______________111-91-1——————bis(2-Chloroethoxy)me thane_120-83-2 ——————— 2, 4-Dichlorophenol_________120-82-1 ——————— 1, 2 , 4-Trichlorobenzene_____91-20-3————————Naphthalene_______________106-47-8——————4-Chloroani1 ine___________87-68-3———————Hexachl or obut ad iene________59-50-7———————4-Chloro-3-me thy 1 phenol____91-57-6———————2-Me thy Inaphtha Iene_______77-47-4———————Hexachl orocyclopentadiene__88-06-2———————2,4,6-Tr ichlorophenol_____95-95-4 ———————— 2, 4, 5-Tr ichlorophenol______91-58-7————————2-Chloronaphthalene________88-74-4 ———————— 2-Ni troani line____________131-11-3———————Dime thy Iphtha late_________208-96-8———————Acenaph thy Iene____________606-20-2 ——————— 2 , 6-Dinitrotoluene_________

FORM I SV-1 1/87 Rev.AR306568


I CBQ17 IName: YORK LABS/CT Contract: 63-W8-0021 I_________0 fi P A 3

rCode: YORK Case No.: 12512 SAS No.: SDG No.: C3Q02




Moisture: not dec.- dec. Date Extracted: 08/23/89

••ctraction: (SepF/Cont/Sonc) SEPF Date Analyzed: 09/09/89



1I 99-09-2 —83-32-9 —

1 51-28-5 —I 100-02-7-I 132-64-9-1 121-14-2-I 84-66-2 —1 7005-72-386-73-7 —100-01-6-5 '3 A. C •»

86-30-6 —101-55-3-118-74-1-87-86-5 —85-01-8 —120-12-7-84-74-2 —206-44-0-129-00-0-85-68-7 —91-94-1 —56-55-3 —218-01-9-117-81-7-117-84-0-205-99-2-207-08-9-50-32-8 —193-39-5-53-70-3 —191-24-2-

——————— 3-Mifoan.i 1 ine

- —————— 2 f A-Dini troohenol- —————— i-Mi tronheriol , , , , , ,——————— Dibenzofuran——————— 2 r 4-D in. itro toluene—————— Diethylphthalate ,--— -— 4-Chl or ophenyl -pheny 1 ether—————— Fluorene ,,——————— 4-Nitroani 1 ine————— 4,6-Dini tro- 2 -methyl phenol _—————— N-Nitrosodiphenylamine (1) _—————— 4 -Brcmophenyl -pheny 1 ether __——————— Hexachlorobenzene ,.,,„...„. , ,.—— ——— Pentachloroohenol,,——————— Phenanthrene-,, , „ . , , . ,——— —— Anthracene——————— Di-n.-butylphthalate .„, _——————— Fluo'-anthene——————— Pyrene „—————— Butylbenzy Iphtha late—————— 3,3 '-Dichlorobenzidine—————— Benzo (a ) anthracene _——————— Chrysene————— bis(2-Ethylhexyl)phthalate—————— Di-n-octylphthalate——————— Benzo ( b ) f luoranthene—————— Benzo ( k ) f luoranthene——————— 3enzo(a)pyrene._.., ,.—————— Indenof 1 , 2 P3-cd) pyrene—————— Dibenzo( a. hi anthracene—————— Benzo (q rhf i )perylene_

150.000 |10.000150.000150.000110.000110.000110.000110.000110.000150.000150.000110.000 I10.000110.000150.000110.000110.000110.000 110.000110.000110.000!20.000110.000110.000 I2.000110.000110.000110.000110.000110.000110.000110.0001

1

uuuuuuuuuuuuuuuuuuuuuuuuJBuuuuuuu



AR3Q6569


C8Q17ab Name: YORK LASS/CT Contract: 6S-WS-CC21

ao Coce: YORK Case No.: 12512 SAS No.: ______ SDG No.; C8Q02

atrix: (soil/water) WATER Lab Samole ID: 1496003

article wt/vol^ 1000. fa/mL) ML Lab File ID: _________

evel: (low/med) LOW Date Received: 03/22/S9

Moiscure: not dec. ____ dec. _______ Dace Extracted: 03/24/a

.xtraction: (SepF/Ccnt/Scnc) SEPF Date Analysed: 08/30/89

PC Cieanuc: (Y/N) N pH: Dilution Factor: 1

CONCENTRATION UNITS:CA3 NO. COMPOUND (ug/L or ug/!<g) UG/L G

7 t Q — O4 * — —wl^-tf-l-O— ~ —

31^-35-7---319-36-S ——•w w O * 7

~f\ Q — A A — "^— _ —

1024-57-3 —959-9S-S---60-57-1 ———"^ "^ — C 2 _ Q .

72-20-3 ———33213-65-9-T^—S. * _ C — — — —

1031-07-3 —50-29-3 ————72---3-S ———53-94-7O-5-3103-71-9--5103-74-2 —

* ^ .* *~f * < ^12o 74-11-2-11104-23-2-11141-16-5-53469-21-9-i *5 4 v^— *^c — — ; —JL—O /-.-.^C11097-69-1-t 7/%C_i._-.O'^«.C-_i1 iVÔCt<l"O™

Ci . ta/ i • d W «t W

-----beta-3HCce_ -3 cnu

-----camrna-SHC (Lincane)-----Hectachlor-----Alctrin- ---Heotachlor eooxide- ——— Sndosulfan I

W J. w _» W i _«• 1 1

— — -_.<_ '-DOE-----Encsrin- — --cndcsulfan II———— .i.A'-ODO-----Endcsulfan sul-fate———— 4._,'-DDT-----Metnoxvchlor-- — -Encrin kecone-----alDMa-Chiorciane-----camma-Chlordane-----Toxaohene-- — -Aroclo: — 1016

— '! W^wf JkA-4_JL

Ht w^XOi JL b *.

- —— -Aroclor-1242———— ArocIor-124S-----Aroclor-1254. ———— Arcclor-1260

I

0.050IU0.050IUO.OSOJUo.osoiuO.OSOJUo . 0.50 : uO.OSOJUO.OSOIU0.10JU0.10!U0.10JU0.10JU0.10JU0.10JU0.10JUO.SOJU0.10IUo.soiu0.501Ul.OJU

O.SOJUo . so : uO.SOJUo . so : uO.SOJUi . o : ul.OJU

1 1

FORHIPEST

IB EPA SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET ______________

t: I C3Q19 IName: YORK LABS/CT Contract: 68-W8-0021 I________n n r oirr -t

\J \J VJ fv «_• JL

aET Code: YORK Case No.: 12512 SAS No.: SDG No.: C3Q02








103-95-2 ——————— Phenol______________111-44-4——————bis(2-Chloroethyl)ether.95-57-8 ——————— 2-Chlorophenol___________541-73-1 —————— 1,3-Dichlorobenzene_______106-46-7 —————— l, 4-Dichlorobenzene_______100-51-6——————Benzyl alcohol____________95-50-1 ——————— 1,2-Dichlorobenzene_______95-48-7————————2-Methyl phenol________________108-60-1———————bis(2-Chloroisopropyl )ether_106-44-5——————4-Methylphenol____________621-64-7———————N-Nitroso-di-n-propylamine_67-72-1————————Hexachl or o ethane__________98-95-3————————Nitrobenzene______________78-59-1 ———————— Isoohorone________________88-75-5 ——————— 2-Ni trophenol____________105-67-9 ——————— 2 , 4-Dimethylphenol_________65-85-0———————Benzoic acid_;________________111-91-1——————bis(2-Chloroethoxy) me thane_120-83-2——————2,4-D ichlorophenol________120-82-1 —————— 1,2 , 4-Trichlorobenzene_____91-20-3———————Naphthalene______________106-47-8———————4-Chloroani 1 ine___________87-68-3————————Hexachlorobutadiene________59-50-7 ———————— 4-Chloro-3-methylphenol____91-57-6———————2-Methylnaphthalene_______77-47-4———————Hexachl orocyclopentadiene__88-06-2 ———————— 2 , 4 , 6-Tr ichlorophenol______95-95-4————————2 , 4 , 5-Tr ichlorophenol______91-58-7———————2-Chloronaphthalene_______88-74-4 ———————— 2-Nitroaniline____________131-11-3———————Dimethylphthalate___________208-96-8———————Acenaphthylene____———_______606-20-2 ——————— 2,6-Dinitrotoluene__________

I10.0001 U10.0001 U10.0001 U10.000! U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.000! U50.0001 U10.000! U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U50.0001 U10.000! U50.0001 U10.0001 U10.0001 U10.000! U

FORM i sv-i RR306571 i/87 Rev-

1C EPA SAMPLE NO.SEMIVOLATILE CRGANICS ANALYSIS DATA SHEET __________________

I CBQ19ab Name: YORK LABS/CT Contract: 68-WS-0021 I________

CGCML-ab Code: YORK Case No.: 12512 SAS No.: SDG No.: C3Q02 v m»-



>vel: (low/med) LOW Date Received: 08/23/89


<-raction: (SepF/Cont/Sor.c) SEPF Date Analyzed: 09/09/89



99-09-2 ———————— 3-Nitroani 1 ine____83-32-9————————Acenaphthene_____5 1-28-5 ———————— 2 , 4-Dini trophenol_100-02-7 ——————— 4-Ni trophenol_____132-64-9———————Dibenzofuran_____121-14-2———————2, 4-Dini trotoluene.84-66-2————————Die thy Iphtha late.7005-72-3——————4-Chlorophenyl-pheny 1 ether.86-73-7———————Fluorene________________100-01-6——————4-Nitroani 1 ine__________534-52-1——————4/6-Dinitro-2-methylphenol_86-30-6————————N-Nitrosodiphenylamine (1)_101-55-3——————4-Bromophen.yl -pheny 1 ether_118-74-1——————Hexachl orobenzene_______87-86-5———————Pentachlorophenol__________85-01-8———————Phenanthrene____________120-12-7———————Anthracene_______________84-74-2————————Di-n-buty Iphtha late_______206-44-0———————F luoranthene_____________129-00-0———————Pyrene___________________85-68-7————————Butylbenzy Iphtha late_____91-94-1—————•——3,3'-Dichlorobenzidine___56-55-3———————Benzo (a) anthracene________218-01-9——————Chrysene_______________117-81-7——————bis(2-Ethylhexyl)phthalate.117-84-0——————Di-n-octylphthalate______205-99-2——————3enzo(b)f luoranthene_____207-08-9———————Benzo ( k) f luoranthene_____50-32-8————————Benzo (a ) pyrene_____________193-39-5———————Indeno( 1, 2 , 3-cd) pyrene____'53-70-3————————Dibenzo(a,h)anthracene____191-24-2 ——————— Ber.zo(g,h, i Jperylene_____

50.0001 U10.0001 U50.0001 U50.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.000! U50.0001 U50.000! U10.0001 U10.0001 U10.0001 U50.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U20.0001 U10.000! U10.000! U7.0001 JB10.0001 U10.0001 U10.0001 U10.0001 U10.000! U10.0001 U .10.0001 U


FORM I SV-2 1/87 Rev.AR306572

ID £?A SAMPLE NO.PESTICIDE ORGANICS ANALYSIS DATA SHEET ' ______________

Name: YORK LA3S/CT Contract: 68-we-C021C3Q19 0007G3

ab Coae: YORK Case No.: 12512 SAS No.: ______ SDG No.: C3GO;

âtrix: (soil/water) WATER Lab Samole ID: 1496009

•ancle wc/vol.: 1000. (g/mL) ML Lab File ID: _______

evei: (low/med) LOW Date Received: 08/23/8

MQ'l-stura: net .-.ac. ._.„__ dec. ____ Date Extracted: 08/24/39

xtraction: (SecF/Ccnt/Sonc) SEPF Date Analyzed: 08/30/39

PC Cleanuo: (Y/N) N pH: Dilution Factor: 1

CONCENTRATION UNITS:CAS NO. COMPOUND fug/L or ug/Kg) UG/L Q

319-S4-6--------aIona-3KC____________319-35-7----- —— beca-SHC______________319-56-c- ————— delta-BHC________S3-39-9---------c3mma-BHC (Lindane)76-44-S----- — — Heotachlor _______

•Alarin1024-57-3-----—Heotachlor eooxide959-9S-3----——— Endosulfan I_____~60-57-1———————Disldrin________72-55-9----- — — 4. 4'-DOS____________72-20-S ———————— Encrin__________

T_.C. -0. •Endcsulfan II72-54-5—- ————— 4.4* _________1031-07-3-------EnccsuIfan sulfate50-29-3————————4.4'-DDT________'72-<-3-5---------Methoxychlor___53494-70-5————Endrin ketcne_3103-71-9-------aloha-Chlordane.5103-74-2-------gamma-ChIordane.SOOi-35-2- — - — -Tcxaohene _____12674-11-2—————Arcclcr-1016___11104-23-2—————Aroclor-1221___•11141-16-5—————Arcclor-1232 __53-16^-21-9 ———— -Aroclor-1242__12672-29-6 ————— Arocior-1243___11097-69-1---——Aroclor-1254___11096-32-5 ————— Arcclor-1260___

0.050IUO.OSOIU0.050IUO.OSOJU0.0501Uo.oso:u0.050IU0.050IU0.10IU0.10IU0.10IU0. 10 !U0.101UO.IO'.U0.10IU0 . 50 ! U0.10IUo . so : u0.50IUi . 0 ! U

0.501UO.SOJUO.SOIUo . so : uO.SOIU

1.0!U1.0IU

FORM I PEST 1/S7 Rev

AR306573

13 E?A SAMPLE NO.SEMIVCLATILE ORGANIC5 ANALYSIS DATA SHEET _________________

I C3Q20 !ab Name: YORK LABS/CT Contract: 68-W8-0021 I______________I









I 108-95-2 —— -111-44-4 ———

i 95-57-8 -----541-73-1 —— -106-46-7 — —100-51-6 ——— -95-50-1 —— —95-48-7 —————108-60-1 ————106-44-5 ————621-64-7 ———67-72-1 -----98-95-3 — ——78-59-1 —————ao —c. e _105-67-9 ———65-85-0 ————

120-83-2 —— -120-82-1 ————91-20-3 —————106-47-8 ————Q "7 £. Q "3

59-50-7 —————91-57-6 -----77 — 4.7 — 4. — —88-06-2 ————95— QC_4_ ____91-58-7 -----88-74-4 —— —131-11-3 — —208-96-8 — —606-20-2 ————

——— Phenol——— bis f 2-Chloroethy 1 ) ether——— 2-Chloroohenol——— 1,3-Dichlorobenzene ,——— 1 f 4-Dichlorobenzene, „——— Benzyl alcohol——— 1 , 2-Dichlorobenzene, ,,„..——— 2 -Methyl phenol ,, ,,. ...——— bis( 2-Chloroisopropyl )ether_——— 4-Methylphenol——— N-Nitroso-di-n-propylamine _——— Hexachl oroe thane——— Nitrobenzene .„, ,.——— Isophorone——— 2-Nitroohenol——— 2 . 4-Dimethylphenol——— Benzoic acid——— bis ( 2-Chloroethoxy )methane _——— 2 .4-Dichloroohenol _——— 1 . 2 , 4-Trichlorobenzene——— Naphthalene

——— Hexachlorobutadiene——— 4-Chloro-3-methylphenol——— 2-Methylnaphthalene——— Hexachl or ocyclopentadiene __——— 2 . 4 . 6-Trichlorophenol——— 2 . 4.5-Trichlorophenol_——— 2-Chloronaohthalene——— 2-Nitroani 1 ine.,,——— Dime thy Iphtha late——— Acenaoh thy Iene——— 2 , 6-Dinitrofcoluene

110.000110.000 |10.000!10.000110.000110.000110.000110.000 I10.000110.000110.000110.000110.000110.000110.000110.000150.000110.000110.000110.000110.000110.000!10.000110.000110.000110.000110.000150.000110.000150.000110.000!10.000110.000!

1

uuuuuuuuuuuuuuuuuuuuuuuuuuuuuuuuu'

FORM I SV-1 . 1/87 Rev.AR30657I*

1C EPA SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET ________________

I CBQ20 OOC231ib Name: YORK LA3S/CT Contract: 68-W8-0021 |______________I

FCode: YORK Case No.: 12512 SAS No.: SDG No.: C3Q02

itrix: (soil/water) WATER Lab Sample ID: 1496007




•ctraction: (SepF/Cont/Sonc) SEPF Date Analyzed: 09/09/89



99-09-2 — ——83-32-9 ———— •51-28-5 ————— •100-02-7 ————132-64-9 ———— -121-14-2 ———— •84-66-2 ————— •7005-72-3 ——— -86-73-7 ————— -100-01-6 ———— •534-52-1 ———— •86-30-6 ————— •101-55-3 ———— •118-74-1 ———— -87-86-5 ————— -85-01-8 ————— •120-12-7 ———— -

1 84-74-2 ————— •206-44-0 ———— -129-00-0 ———— •85-68-7 ————— -91-94-1 ————— -56-55-3 ————— -218-01-9 ———— -117-81-7 ———— -117-84-0 ———— -205-99-2 ———— -207-08-9 ———— -50-32-8 ————— -193-39-5 ———— -53-70-3 ————— -1 a 1 *> a. •?

—— - 3-Ni t--oani 1 ine——— Acenanhthene——— 2 f 4-Dini trophenol——— 4-Mi t-onhenol, _.„.„_.,——— Dibenzof uran,——— 2 f 4-Din.itrotoluene——— Diethylphthalate „,„,.„, , , ,,——— 4-Chl or ophenyl -pheny 1 ether _——— Fluorene „——— 4-Mi troani 1 ine ,, „„„„, „——— 4, 6-Dinitr o-2 -methyl phenol——— N-Nitrosodiphenylamine (1) _——— 4-3romophenyl -pheny 1 ether __——— Hexachl or obenzene——— Pentachlorophenol——— Phenanthrene——— Anthracene——— Di-n-buty Iphtha late——— Flu.oranth.ene,.,,——— Pyrsne——— Butylbenzy Iphtha late——— 3 t 3 '-Dichlorobenzidine.,,——— Benzo ( a ) anthracene——— Chrysene- — bis(2-Ethylhexyl )phthalate..,.——— Di-n-octylnhthalate——— Benzo ( b ) f luoranthene——— Benzo(k)f luoranthene——— Benzo(a)pyrene——— Indenofl f 2 ,3-cdl pyrene——— Dibenzo( a Ph) anthracene.——— Ben.zo(g rh, i )perylene

50.00010.00050.00050.00010.00010.00010.00010.00010.00050.00050.00010.00010.00010.00050.00010.00010.0000.40010.00010.00010.00020.00010.00010.00010.0002.00010.00010.00010.00010.00010.00010.000

uuuuuuuuuuuuuuuuuJuuuuuuuJuuuuuu .


FORM I SV-2 . 1/87 Rev.

AR30S575

ID EPA SAMPLE NO.PESTICIDE CRGANICS ANALYSIS DATA SHEET _____•___________

ab Name: YCRK LASS/CT Contract: 63-WS-OC21CSQ20

ab Coca: YORK Case No.: 12512 SAS No.: ______ ' SDG No.: C3C02

atrix: (soil/water^ WATER Lab Samole ID: 1496007

ancle wt/voL: 1000. Ca/mL) ML Lab File ID: _______

evel: (Icw/mecO LOW Date Received: 03/22/39

dcis-ura: net dec. ____ -_ec. ____ Date Extracted: 03/24/39.

xtracticn: ( SacF,'Ccnt/Sonc) SEPF Date Analyzed: 03/30/39

=C Cleanuo: CY/N") N oH: Dilution Factor: 1


31^-34-6----31^-35-7----_ iL • CO C53-39-9-----

309-00-2- ——1024-57-3 ——95<=>-93-3----60-57-1-----72-55-9-----— '^ —i /\ QTTÎ t—ji C — O— —

72-54-3 — — -1031-07-3---C/">_1Q— T— _— — —

72-43-5- — —53494-70-5 —5103-71-9 ——5103-74-2 ——•-» w .' ._ W W A.

1"ATA_1 1— *?_ —

11104-2S-2--11141-16-5 —

1 ~>Ji~l"*—. Q— ' — —

110'97-6<9-l--11096-32-5 —

----alor.a-SHC----aeta-3HC— --delta-BHC----aamma-BHC f'-indane)——— Heotachlcr----•aidrin— --Heotachlcr eooxide----Endcsulfan I----Dislcrin—— -4. -'-DOE----Endrin----Endcsulfan II——— 4.4'-DDD----Enccsulf an sulfate— --4.4'-DDT----Metnoxvchlor----Endrin ketone----aloha-Chlordane----gamma-Chlordane----Toxaohene——— Aroclor-1016- —— Aroclor-1221

A ^ __ __ ,-, __ * «» ^

MI at-itji __.— ^—— -Arcclor-1243----Aroclor-1254——— Aroclcr-1260

1

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O.SOIUO.SOIUO.SOIU0.50! UO.SOJUl.OJUl.OJU

1

FORM I PEST 1/37 K

2S68A RIVA ROADSUITE 300ANNAPOLIS. MD 21401PHONE 301 -266-9887

SESaNESS-CCNSUtTANrS

DATE: October 25, 1989

SUBJECT: Organic Data Validation for Case 12512Site: Keystone Sanitation

PROM: Mahboobeh Mecanic DonSr. inorganic Data Reviewer Organic Data Reviewer

TO: Theresa A. SimpsonESAT Deputy Project Officer

THRU: Richard D. DresserActing ESAT Team Manager

OVERVIEW

Case 12512 consisted of twenty (20) aqueous samples which were 'analyzed for semi-volatile and pesticide/PCB analyses. Includedin this case were two (2) field blanks and two (2) fieldduplicate pairs. The samples were analyzed as a ContractLaboratory Program (CLP) Routine Analytical Services (RAS) .

SUMMARY

All samples were successfully analyzed for all target compounds.All instrument and method sensitivities were according to theContract Laboratory Program (CLP) Routine Analytical Service(RAS) protocol.

MINOR PROBLEM

o Several compounds failed precision criteria for initial and/orcontinuing calibration. Therefore, positive results arequalified "J" and detection limits are qualified "UJ" for theaffected samples. (See Appendix F for affected samples).

NOTES ;

o Compound di-n-butylphthalate was found in samples CBQ03, CBQ07and their field duplicate pairs CBQ15 and CBQ16. The relativepercent differences (%RPD) between the samples and their fieldduplicate pairs is calculated below:

Concentration Concentration(ug/L) (ug/L)

CBO03 CB015 %RPD CBO07 CBQ16

29 1.0 J 187 0.6 J 0.5 J

AR30S577

Page 2 of 2

o The maximum concentrations of all compounds found in themethod or field blanks are listed below. All samples withconcentrations of common laboratory contaminants less than tentimes (10x), and concentrations of uncommon laboratorycontaminants less than five times (5x) the blank level havebeen qualified "B" on the data summary forms. (See AppendixF).

Compound Concentration (uq/LL

2-chlorophenol 0.4 Jdimethylphthalate* 0.7 Jdiethylphthalate* 0.4 Jbis (2-ethylhexyl)phthalate* 7.0 Jdi-n-octylphthalate* 2.0 J

* Common laboratory contaminant.

o The reported Tentatively Identified Compounds (TICS) ofAppendix D have been reviewed and corrected for blankcontamination during data validation.

All data for Case 12512 were reviewed in accordance with theFunctional Guidelines for Evaluating Organic Analyses withModifications for use within Region III. The text of this reportaddresses only those problems affecting usability.

ATTACHMENTS

1) Appendix A - Glossary of Data Qualifiers2) Appendix B - Data Summary. These include:

(a) All positive results for target compoundswith qualifier codes where applicable.

(b) All unusable detection limits (qualified "R").3) Appendix C - Results as Reported by the Laboratory for All

Target Compounds4) Appendix D - Reviewed and Corrected Tentatively Identified

Compounds5) Appendix E - DPO Report for Contractual Compliance6) Appendix F - Support Documentation

DCN: MM910A08.KEY

AR306578

Appendix A

Glossary of Data Qualifiers

flR306579

GLOSSARY OF DATA QUALIFIER CODES (ORGANIC)

CODES RELATING TO IDENTIFICATION(confidence concerning presence or absence of compounds):

U - Not detected. The associated number indicatesapproximate sample concentration necessary to bedetected.

(NO CODE) = Confirmed identification.

B — Not detected substantially above the level reportedin laboratory or field blanks.

R = Unreliable result. Analyte may or may not bepresent in the sample. Supporting data necessary toconfirm result.

N = Tentative identification. Consider present.Special methods may be needed to confirm itspresence or absence in future sampling efforts.

CODES RELATED TO QUANTITATION(can be used for both positive results and sample quantitationlimits):

J = Analyte present. Reported value may not be accurateor precise.

K = Analyte present. Reported value may be biased high.Actual value is expected to be lower.

L = Analyte present. Reported value may be biased low.Actual value is expected to be higher.

UJ = Not detected, quantitation limit may be inaccurateor imprecise.

UL = Not detected, quantitation limit is probably higher.

OTHER CODES

Q = No analytical result.

flR306580

Appendix B

Data Summary Forms

HR30S58

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COMPOUND

gu

•§cEl

e

bl»(2 Cli

toroel

hyljel

lief

o

o

c?_55cv

_,

* 1,3-Ulclilorolioiuene

e

* l.^-Dlchlorohoiuono

e

^

5•s.ca

e

1,2 U

lchlorobcnicna

e

•5

2cU

e

fcXô

m"oj|Urj_«»3

e

2

o

5

•|L5"E.co0.s

e

e£

oJ5~K•;

e

Nllrobcnzene

0

c§5I1

o

"S

5"

to

"5

acw

e

|

_g

"5Cts

R

blj(2 Cliloioellioxy)iiietli«ne

e

2,4 Ulchloroplionol

0

1.2,4-

filchloiobemerie

o

•

V

J"5

n

e

f Clil

oionii

llliio

e

" o2 ^

u_uiQUJQO•U

ou.

e

UJUJCO

at

e

ue

e"5eC

o

H

_5 u.

CM

CO

<2 W_. wffi un... <S cog t=u. uj

2COI

mO

cn

"c.nCO

«neaZ

o 3__ «co U

;

;

!

^

A

1

1

-

-

o S21 73

«e u.

tlco "25

"5

^^ CO

\ i-i 4-1 ca

Location

COMPOUND

13Q658SS§

Hexachlorobutadlene

e

4 Cliloro-3 melhylphenol

0

2 Melhyinaphthalena

o

t lexachtorocyclopentadlena

0

•5iT.o

1ni

o

"3I"5.o52iS«_-rCM

s

2-Chloronaphlhalene

o

1

s

2

£

|

O

t)

41-tie

2.6 Dln

lltolo

ltiene

o

o=

n

s

t>|

cie

"oi"cc

C

oin

V)

r-)

o>

f

s

I Dibenzoluran

e

I 2,4

DlnltrotoHlene

e

To

1S

e

te1"S.•5.i"i.• o•1U

o

Fluoiene

e

n

Tt_s

•cmoZ

s

Ij

~<ec

1<o-r

s

nit

'Action

Level

Exists

SEE

NARRATIVE

FOR bODE

DEFINITIONS

_a"oD>Q•OSerec~2ou

z!o

CO_0M

revised

i?

CO

co_ wCO -I

0.

<2 co _,*O -="?U. UJ CS.I i2COI

csCO

egZ

Hic73_£75

o. ,——————————j————————————.——p^————i——————————j O^

-3£croC

73nh.

Ou

C

U

ie

_s"acs

>-

•••«.

_.

73(S

cJO35

^

<|I

VL

_Jw

Location

COMPOUND

iu

N-Nltrosodtphenylamlne

o

C

Z

1"E.odp

o

'Hexachlorobonzene

o

73clio_,

73n_SQ.

o

Phenanlhrene

o

Anthracena

o

>->

•3-•Q

*-}

B

_:"3_CO

o

Fhloranthene

e

r?

v^

*>

e

^

|ai|"3

o

——— .

——— i

-. —————————————

3.3 Dlchlorobenzldlne

o

Denzofalanthracene

0

Ir

O

CQ

OO

t_E

"c

*5aK1

o

V^

O«i

c5aJ>—OCa

e

Benzo(b)l1uoranthene

e

e

c0_B

.£2£Q

e

t>£1•H,jtciQ

O

c£5

u

si1o

egc.

•

^M

jC

a

—— :.: — i ; . —

: ——— L-. ————————

Denrofq.h.Dperviene

e

s Is ^TJ_ e

U_ M

SM ">a oIBOOoou.Uf

ccrzUJUlCO

m_Su

1

ftR306590

§,_ __

II

I-CO

aOa.

QZ _

_j< C.

e 51u -J -c.

-, W' i ^

CO

UJ

a.

ou.> • £

Irstn

CS<0s

ere

e •>r: Bco o

r%-x.

tO

I

'J

2-4

SJ

•s.

I

«

•<

»

•v.

2

2

-*.

5

c

_O £2 73elfg-s5-240 _•

5

-ji

* f\ _,

•V 'i5r"--»» 1C, ^

2 >5

11•A

4>i

4i

>.\

nc

Location

t COMPOUND

592 gu

1

o5

oo

OB

7J

inOe

O51

inO

.•*om~3

_JM*

OEre

reC«

in0

k._o73(S— *5*«

ine

c•5

inoo

1u

1

inoo

Endosullan

1

inoo

iOfa

eo

1

tunV— r"

0

0

(I

oo

Endosulfan

II

1 0

o

— r

OO

Endosullan

Sulfale

•

oo

b—aqV

oe

uteO

"o

inO

Ctc

10

d

b

J

DJ5ww_s0R

"c<

ine

K

|

'Gamma-Clilordano

ine

eoc<t1

e

00

•_)

c<

inO

CNf

"S0<

ino

CM

CN

_OU0<

«ne

N-ri

73o<

mo

CS-rCNi

73o<

mo

— rtncv,

73o<

e"

(

Ocslev!

1<

e

_

CO -R u

oQ

COzO

aouou.

e:

xtu

f

£•eCun

gu

1

CO

gzZUJai I——————————————|ou

CO

aU

Hco

cOu.

I 1Q tfj

Q

a. uituCO

QZ S

< ICO _j*

CO <C E?UJ UJ .£,

0 I

(0

eTO2

c.—\ _?•••? "_.T —J

•

-_

s

dz__"a.nCO

r n

-•

r>Vj

_,

73£s

a

;q

03Q £1 V

U

3 nft.

Location

:OMPOUND

0 .

aB

a

inoo

oa

ine

Oa1•o

ine

*•— »

re•3

_J-•»•

0

C

c0

ine

v.

un"a.e

ino

e

I

ino

1c.uo—5Jl'S

ine

C

V*

•8

ine

S

-S

eo

UJ

2

-r

eo

•3CUl

eo

era"3o•-3

£

eo

nopV

eo

cresa1UJ

O

o

_.— Hs

eo

w

73Xo7?

ino

cS

ÛJ

oe

}|ilordane

rela<

ino

i-Chlordane

1a

me

esc.IBXo

0o1

_DUO<

ino

CMI

JD73o<

ino

nCM

_D73o<

in0

{M-rCM

JO7]o<

mo

esCvt_D7!<

.,o

— •inc\

"to<

5n

r-l2GO

7!

10'

ou.UJ

1

xUJ

uSi75Q

B

eaun

ou

Appendix C

Results as Reported by the Laboratoryfor all Target Compounds

AR306591*

13 EPA SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET _______________

I CBQOOJame: YORK LABS/C7 Contract: 68-W8-0021 I_____

ooooUab Code: YORK Case No.: 12512 SAS No.: SDG.No.: C3Q02



svel: , (low/med) LOW Date Received: 03/23/89


<traction: (SepF/Cont/Sonc) SEPF Date Analyzed: 09/09/89



108-95-2 ——————— Phenolbis(2-Chloroethyl ) ether

95-57-8 ———————— 2-Chlorophenol ____________541-73-1 ——————— 1 , 3-Dichlorobenzene ________106-46-7 —————— 1 , 4-Dichlorobenzene _______100-51-6 ——————— Benzyl alcohol ____________95-50-1 ——————— 1 , 2-Dichlorobenzene _______95-48-7 ———————— 2-Methylphenol ____________108-60-1 ——————— bis(2-Chloroisopropyl )ether_106-44-5 ——————— 4 -Me thy 1 phenol ____________621-64-7 —— ———— N-Nitroso-di-n-propy lamine _67-72-1 ———————— He xach 1 or o ethane __________98-95-3 ————— —— Nitrobenzene ______________73-59-1 ———————— Isophorone ________________88-75-5 ———————— 2-Ni trophenol _____________105-67-9 ——————— 2,4-Dimethylphenol _________65-85-0 ———————— Benzoic acid ______________111-91-1 —————— bis( 2-Chloroethoxy)methane _120-83-2 —————— 2 , 4-Dichlorophenol ________120-82-1 —————— 1 ,2,4-Trichlorobenzene _____91-20-3 ———————— Naphthalene _______________106-47-8 ——————— 4-Chloroaniline ___________87-68-3 ——————— Hexachl orobut ad iene _______59-50-7 ———————— 4-Chloro-3 -methyl phenol ____91-57-6———————2-Me thy Inaphtha Iene_____77-47-4———————Hexachl or ocyclopentad iene.88-06-2 ——————— 2,4,6-Trichlorophenol___95-95-4———————2 , 4 , 5-Tr ichlorophenol___91-58-7 ——————— 2-Chloronaphthalene_____88-74-4 ———————2-Ni troani 1 ine__________131-11-3———————Dime thy Iphtha late_______208-96-8————-•—Acenaph thy Iene__________606-20-2——————2, 6-Dinitro toluene______

I10.000! U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U50.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U50.0001 U10.0001 U50.0001 U10.0001 U10.0001 U10.0001 U

FORM I SV-1 RR^nCqqh 1/87 Rev.

Appendix D

Reviewed and CorrectedTentatively Identified Compounds

RR306596

SEMIVOLATILE ORGANICS ANALYSIS DATA SHEETI II CBQOO J

ab Name: YORK LA3S/CT Contract: 68-W8-0021 I_________U£LQjj43


fix: (soil/water) WATER Lab Sample ID: 1496008





JC Cleanup: (Y/N) N pH: Dilution Factor: 1

CONCENTRATION UNITS:Mumber TICs found: O (ug/L or ug/Kg) UG/L

CAS NUMBER

01.02.OJ.04.05.0(3.

:09.10.11.12.13.

. 14.1 15.1 16.1 17.1 18.i 19.20.21.22.23.24.25.26.27.28.29.30.

COMPOUND NAME,»„„, = ,„»„ = = = ,„„,

RT-..*,*,»

EST. CONC------------

Q

FORM I SV-TIC 1/87 Rev.

AR3Q6597

SEMIVCLATILE ORGANICS ANALYSIS DATA SHEET

! CBQ01ab Name: YORK LABS/CT Contract: 68-W8-0021 \.__________

ab Code: YORK Case No.: 12512 SAS No.: SDG No.: CBQ02 'GOo 3







CONCENTRATION UNITS:Mumber TICs found: £) (ug/L or ug/Kg) UG/L

1CAS NUMBER I COMPOUND NAME

._,***=>-*,,___, *,*._!- -,.„--..-* _.,..,..-,,,01. 102. 103. I04. 105. 106. 1 '07. tOS. !09. 110. 111. 112. 1 •13. 1

,14. 1! 15. 11 16. i1 17. 11 18. 1(19. !

20. i21. 122. I23. 124. 125. !26. !27. (23. 129. 130. 1

I

RT EST. CONC Q

FORM I SV-TIC 1/87 Rev,

AR306598

SEMI VOLATILE ORGANICS ANALYSIS DATA SHEETI II C3Q02 |

ab Name: YORK LABS/CT Contract: 68-W8-0021 I______________I

ab Code: YORK Case No.: 12512 SAS No.: SDG No.: CBQO-2 ' 0 0 S O

x: (soil/water) WATER Lab Sample ID: 1496004

ample wt/vol: 1000 (g/mL) ML. Lab File ID: >C4484

avel: (low/med) LOW Date Received: 08/22/89


<traction: (SepF/Cont/Soncj SEPF Date Analyzed: 09/09/89


, CONCENTRATION UNITS:dumber TICs found: Q (ug/L or ug/Kg) UG/L

CAS NUMBER

01.02.03.04.05.06.

:0-3.10.11.12.13.14.15.16.17.IS.19.20.21.22.23.24.25.26.27.26.2'3.JO .

COMPOUND NAME RT

•

EST. CONC Q


AR3Q6599

IF EPA SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET ._______________

I t1 CBQ03 |

ab Name: YORK LA3S/CT Contract: 68-W8-0021 1_______v








CONCENTRATION UNITS:Number TICs found:^ (ug/L or ug/Kg) UG/L

CGGOjo

CAS NUMBER 1

01.02 .03.04.05.06.07.OS.09.10.11.12.13.

, 14.I 15.! 16.I 17.1 18.1 19.20.21.22.23.24.25.26.27.28.29.30. '

COMPOUND NAME

•

1

1

11

-— ..

RT EST. CONC Q

1

|1•


AR306600

IF EPA SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET ________________

I II CBQ04 |

ab Name: YORK LABS/CT Contract: 68-W8-0021 I________n P O H O °U U U U o o«Code: YORK Case No.: 12512 SAS No.: SDG No.: CBQ02

ix: (soil/water) WATER Lab Sample ID: 1496005






CONCENTRATION UNITS:Number TICs found :Q (ug/L or ug/Kg) UG/L

CAS NUMBER,----*-- *--*a*-sa-.a-01.02.03.04.OS.«.:.09.10.11.12.13.

, 14.1 IS.1 16.1 17.I 18.! 19.20.21.22.23.24.25.26.27.28.29.30."-

COMPOUND NAME.._.,____. s-3_, ._»-,..-

RT EST. CONC«,=,- ,-.,.,-.

Q

II


AR3QS6CH

SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

1 C3Q05 |ab Name: YORK LABS/CT Contract: 63-W8-0021 I_________000095




2vel: (low/med) LOW Date Received: 08/22/89




CONCENTRATION UNITS:•Jumber TICs found: Q (ug/L or ug/Kg) UG/L

1CAS NUMBER 1 COMPOUND NAME RT

01. !02. I03. !04. !05. 106. 107. 108. 109. I10. I11. 11 2 . I - I13. 1 1

i 14. 11 15. 1 11 16. i 1I 17. 1 1I IS. !I 19. 1 i

20. ! 121. 122. 1 123. 1

_24. I..25. 126. 127. !28. 129. 130. I

1

EST. CONC Q


ftR306602

IF EPA SAMPLE NO.SEMI VOLATILE ORGANICS ANALYSIS DATA SHEET ____ . ____ . _______

I II CBQ06 |

ab Name: YORK LABS/CT Contract: 68-W8-0021 I ________ 000104

YORK Case No.: 12512 SAS No.: SDG No.: CBQ02

trix: (soil/water) WATER Lab Sample ID: 1496018


avel: (low/med) LOW Date Received: 08/24/89



?C Cleanup: (Y/N) N pH : Dilution Factor: 1

CONCENTRATION UNITS:Mumber TICs found: Q (ug/L or ug/Kg) UG/L

CAS NUMBER

01.02.03.04.05._g^jfl08.09.10.11.12.13.

. 14.1 15.1 16.1 17.I 18.i 19.20.21.22.23.24.25.26.27.

29.30.

1COMPOUND NAME

|.. .,- = _-- »*»*.-»,:..,:.RT

""" —EST. CONC Q


{\R306603

SSMIVCLATILE CRGANICS ANALYSIS DATA SHEET

| CBQ07ab Name: YORK LABS/CT Contract: 68-W8-0021 !______

ab Code: YORK Case No.: 12512 SAS No.: SDG No.: CB


ample wt/vol: 1000 (g/mL) ML- Lab File ID: >H5731





CONCENTRATION UNITS:Mumber TICs found: £) (ug/L or ug/Kg) UG/L

CAS NUMBER

01.02.03.04.05.06.07.08.09.10.11.12.13.14.15.16.17.18.19.20._21.22.23._24.25.26.27.28.29.30.

1COMPOUND NAME I RT EST. CONC .Q

FORM I SV-TIC 1/87

AR30660U

EPA SAMPLEANALYSIS DATA SHEET ' _________

f CBQ08ab Name: YORK LABS/CT Contract: 68-W8-0021 J_________,


a.rix: (soil/water) WATER Lab Sample ID: 1496019






CONCENTRATION UNITS:Mumber TICs found i (_) (ug/L or ug/Kg) UG/L

CAS NUMBER

01.02.03..04. .05.06.07.08.09.10.11.12.13.

. 14./ 15./ 16.1 17.i 13.t 19.20.21.22.23.24.25.26.27.28.29.30.

COMPOUND NAME RT EST. CONC

•

Q

i

iI

FORM I SV-TIC 1/87 Rev

(\R30S6Q5

ac.vu.vui-x4_-,-._. URGAiNiUi ANALYSIS DATA

ab Name: YORK LABS/CT Contract: 68-W8-0021 I______ 0 fi 0 "| 4"J


atrix: (soil/water) WATER Lab Sample ID: 1496002 ••

ample wt/vol: 1000 " (g/mL) ML Lab File ID: >C4575





CONCENTRATION UNITS:Number TICs found: Q (ug/L or ug/Kg) UG/L

ICAS NUMBER 1 COMPOUND NAME

»„--.** -.*«,,, .,..,3|,3*-., ,*..*_,__..»,._,.01. !02. 103. !04. 1OS. 106. I07. 1OS. 109. 110. I11. I12. 113. 114. !15. 116. 117. 118. 119. i20. !21. 122. 123. 124. [25. 126. 127. 128. 129. 130. 1

1

RT EST. CONC Q


AR306606

ab Name: YORK LA3S/CT Contract: 68-W8-0021


4feix: (soil/water) WATER Lab Sample ID: 1496010






- CONCENTRATION UNITS:Mumber TICs found: £) (ug/L or ug/Kg) UG/L

CAS NUMBER

01.02.03.04.05.06.

—————————10.11.12.13.

• 14.i 15.! 16.I 17.I 18.1 19.20.21.22.23.24.25.26.27.28.29.30.

11 COMPOUND NAME,..*___:,,.„,---*..--,,-

RT EST. CONC Q


RR306607

I I1 C3Q11 |

ab Name: YORK LA3S/CT Contract: 63-W8-0021 I______OOP 160

afa Code: YORK Case No.: 12512 SAS No.: SDG No.: CBQ02







CONCENTRATION UNITS:Mumber TICs found: / (ug/L or ug/Kg) UG/L

CAS NUMBER 1 COMPOUND NAME

Ul . -f-r- -i/ .-.7 *•/ —————— i — tsArO&C/iw -L — ••---02. 103. 104. tOS. 106. 107. !OS. 109. !10. !11. I12. 113. 1

, 14. 11 15. !1 16. I1 17. Ii 18. !I 19. 1

20. I21. 122. !23. 124. 125. 126. 127. 128. !29. f30. t

1

RT

" o//. o 4_

EST. CONC Q—TV* —-/A

FORM I SV-TIC 1/87 R

RR30S608

-EMIVOLATILE ORGAN I CS ANALYSIS DATA SHEET _______________________I 1I CBQ12 nnn. ,_,

ab Name: YORK LA3S/CT Contract: 6a-W8-0021 |.________UlHM /


•Bix: (soil/water) WATER Lab Sample ID: 1496020

ample wt/vol: 1000 (g/mLJ ML Lab File ID: >H5710





/. CONCENTRATION UNITS:Number TICs found: O (ug/L or ug/Kg) UG/L

CAS NUMBER

01.02.03.04.05.06.

•'

10.11.12.13.

. 14.15.16.17.18.19.20.21.22.23.24.25.26 .27.28.29.30.

COMPOUND NAME RT EST. CONC Q


AR306609

IF EPA SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET ______________

1 fI C3Q13 |

ib Name: YORK LA8S/CT Contract: 68-W8-0021 1______________I

ib Code: YORK Case No.: 12512 SAS No.: SDG No.: CBQ02 _____cowitrix: (soil/water) WATER Lab Sample ID: 1496021

ample wt/vol: 1000 (g/mL) ML Lab File ID: >H57ll

jvel: (low/med) LOW Date Received: 08/24/89



'•>C Cleanup: (Y/N) N pH: Dilution Factor: 1

_ CONCENTRATION UNITS:dumber TICs found: // (ug/L or ug/Kg) UG/L

CAS NUMBER

01.02.03.04.05.06.07.08.09.10.11.12.13.14.15.16.17.ia.1-3.20.21.22..23.24.25.26.27.28.29.-0.

1COMPOUND NAME

--

RT EST. CONC Q

i


AR306610

i CBQ14ab Name: YORK LABS/CT Contract: 68-W8-0021 1_________V/1> I <» J


•Hix: (soil/water) WATER Lab Sample ID: 1496022






CONCENTRATION UNITS:lumber TICs found: O (ug/L or ug/Kg) UG/L

CAS NUMBER

01.02.03.04.05.06.

*u~f .10.11.12.13.14.

1 15.1 16.1 17.1 18.1 19.20.21.22.23.24.25.26.27...28.29.30.

COMPOUND NAME

•

i

RT EST. CONC Q«----


AR30661 1

ir EPA s^-MfLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET ________________________

I CBQ15ab Name: YORK LABS/CT Contract: 68-W8-0021 'I._____

000ab Code: YORK Case No.: 12512 SAS No.: SDG No.: C3Q02

atrix: (soil/water) WATER Lab Sample ID: 1496013 •

ample wt/vol: 1000 Cg/mL) ML Lab File ID: >H5730





CONCENTRATION UNITS:Number TICs found: *___ (ug/L or ug/Kg) UG/L

210

CAS NUMBER

01 . \ t 1>o"L\ A02.03.04.05.06.07.08.09.10.11.12.13.14.

1 15.i 16.1 17.! 18.1 19.20.21.22.23.24.25.26._27.23._29.,30.

COMPOUND NAME333.X »J- X -1 3 3 * Z

•uW D t_ i' A w £L,fs;K.No\v *^ & ftl^-ft &£"

'

RT,,,!,.) „ g ———

k 1 • O-J

3?. oa

EST. CONC_

14

Q

-¥sr-T".


RR30G612

SEMI VOLATILE ORGANICS ANALYSIS DATA SHEETt II C3Q16 |

ab Name: YORK LA3S/CT Contract: 68-W8-0021 |_________0 0 G 2 S 3


HPix: (soil/water) WATER Lab Sample ID: 1496015

ample wt/vol: 1000 (g/mL) ML Lab File' ID: >H5732





^ CONCENTRATION UNITS:lumber TICs found:^/ (ug/L or ug/Kg) UG/L

CAS NUMBER

01.02.03.04.05.-06-Af.09.10.11.12.13.

. 14.IS.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

11 COMPOUND NAME RT EST. CONC

=,=.=.=, 3 -«,-,.-

Q


AR306613

SEMIVOLATILE ORGANIC3 ANALYSIS DATA SHEET

1 CBQ017ab Name: YORK LABS/CT Contract: 68-W3-0021 {_______


ttrix: isoil/water) WATER Lab Sample ID: 1496003




-ctraction: tSepF/Cont/Scnc) SEPF Date Analyzed: 09/09/89

?C Cleanup: fY/N) N pH: Dilution Factor: 1

CONCENTRATION UNITS:Mumber TICs found: /y Iug/L or ug/Kg) UG/L

CAS NUMBER

01.02.03.04.05.06.07.06.09.10.11.12.13.14.15.16.17.16.

20.21.22.23.24.25.26.27.28.29.30.

1COMPOUND NAME RT EST. CONC .Q

||i*

, ,


flR3066|if

IF EPA SAMPLE NO.SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET _______________.

1 !I CBQ19 I

ab Name: YORK LABS/CT Contract: 68-W8-0021 I______________I

JjkCode: YORK Case No.: 12512 SAS No.: SDG No.: CBQO



evel: (iow/med) LOW Date Received: 08/23/89




/-, CONCENTRATION UNITS:Number TICs found: (_J (ug/L or ug/Kg) UG/L

CAS NUMBER= = = = = = = = = = ===, = = = = =,„

01.02.0.3.04.«-

:08.09.10.11.12.13.14.15.16.17.13.19.20.21.22.23.24.25.26.27.26.29.,10m

COMPOUND NAME

•

RT EST. CONC Q


AR30S6i5

SEM_VOJLAii_,_; ORGANIC^ ANALYSIS DATA SHaiT

! CBQ20ab Name: YORK LA3S/CT Contract: 68-W8-0021 i




*vel: (low/med) LOW Date Received: 08/22/89


ctraction: (SepF/Cont/Sonc) SEPF Date Analyzed: 09/09/89

?C Cleanup: (Y/N) N pH : Dilution Factor: 1

CONCENTRATION UNITS:dumber TICs found :O (ug/L or ug/Kg) UG/L

1 1GAS NUMBER COMPOUND NAME

01.02.03.04.OS.06.07.0£.09.10. 111.12.13. 114.

i 15. iI 16. f1 17. 1! 18. 11 19.20..21.22.23.24.25.26.27.28.29.30.

!RT EST. CONC Q

yn


AR306616

Appendix EDPO Report for Contractual Compliance

AR3066I7

of 2

ORGANIC DATA VALIDATION SUMMARY

Date Review Completed: 10/24/89 Contract Lab.: 3RIVERCase No.: 12512 Contract No.: 68-W8-0021Site Name: Keystone Sanitation Lab DPO: Deborah SzaroSample Nos.: CBOOO-CB017 Reviewer: M. Mecanic

CB019-CB020 From: Region III/ESATPhone: (301) 266-9887

CONCENTRATIONMATRIX ! low ! med ! hiah ! MATRIX RELATED COMMENTS{ soil/solid |{ aoueous ! 20 !other ! !

! 1 1i— — i ———— i> i 11 • - - ! - - • - - iI i 1

j |i 1, ....... __ . ... ————————————————————————————————— ___!_

| j

SEMI-VOLATILES{GC/MS tunina — DFTPP jInitial CalibrationContinuing Calibration[ Surroaate Recovery !Matrix SDikes

j Reaaent Blanks{Holdina Times

I Y 'i —— & ——— ii 1i 1i ———————i———————i —————— Ix !

i i- ....... i1 Y Ii — - —— i1 Y ': —— & —— — . |l x !1 Y 11 ——— — ———— 11 Y 'i —— £ ——— i

1 1: ————————— 11 1—————————

i1 ————————— 11 1

! 1——————————————————————————— j.

! See note 1i See note 1 j! See note 2 j| See note 3 {j See note 4 j

PESTICIDES! Instrument PerformanceInitial CalibrationContinuina Calibration

j Surroaate RecoveryMatrix SDikes

J Reaaent Blanksj Holdina Times

OVERALL CASEjComcound Identification1 Data Completeness

Y 1 1•*•- t— - -•! - H

i Y '———————— i ——— & ———— i ————————i Y 1———————— I ——— £ ———— 1 ————————1 Y 1————————— j ——— A ———— t —————————

Y ' i——— £ ————— I ————————— 1 _______Y 1 1i —— £ ——— ! ——————— i ———————Y 1 1

T t

OK i FYI 'ActionY ' 1——— A ————— , ————————— , —————————X

1See note 5See note 6See note 7—————————————— i—————————————— i

——————————————

REVIEWER'S COMMENTS;

DOCUMENTATION ATTACHED (see following pages)

fiR3066i8

Case 12512Site: Keystone Sanitation Page 2 of 2

ORGANIC DATA VALIDATION SUMMARY

Note 1 - The %RSD and %D values for several compounds exceededprecision criteria in the initial and/or continuingcalibrations. (See Table 1 of Appendix F).

Note 2 - The semi-volatile analyses of several samples had oneacid surrogate recovery above the QC limit. (SeeAppendix F, Form II SV-1).

Note 3 - The semi-volatile MS/MSD analyses of sample CBQ09 hadone (1) out of eleven (11) relative percent differences(%RPD) and three (3) out of twenty-two (22) recoveries(%R) outside the QC limits. (See Appendix F, Form IIISV-l).

Note 4 - The maximum concentration of the following compoundswere found in the laboratory method blanks.

Compound Concentration fua/LV

2-chlorophenol 0.4 Jdimethylphthalate * 0.7 Jdiethylphthalate * 0.4 Jbis (2-ethylhexyl) phthalate* 6.0 J

* Common laboratory contaminant

Note 5 - The pesticide/PCB initial calibration linearity checkhad the %RSD greater than ten percent (>10%) for 4,4'-DDT on the quantitation column. No DOT was detected inany of the samples. (See Appendix F, Forms VIII PEST-1).

Note 6 - The pesticide/PCB continuing calibration of severalcompounds had %Ds greater than 15% on the quantitationcolumn and greater than 20% on the confirmation column.No data was affected. (See Appendix F, Forms IX PEST) .

Note 7 - The pesticide/PCB analysis of sample CBQ04 hadsurrogate recovery above the QC advisory limit. (SeeAppendix F, Form II PEST-1).

AR3066I9

Appendix F

Support Documentation

AR306620

TA3L5 I P*3«J_of.exviZOM-SMTAL PÔTECTIOH ASSMCT XESIOM c:i

CAUI3«ATIO« QUT.IS2SSSMIVOLATILS US. COMPOUNDS (Pare 1 of 2)

CASs/SAS Mo. I 3 5*1 ? _________C3HTaACTOi» _____£\

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AR30S62

TA3LS I pag«____ofPROTECTION AGsNCY ZSStOH H

CALISaATIOH OUTLIERSSs.irvot.ATI LS HSL CCMPOUX3S '(Pars 2 at 2)

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AR30G623

TA3L5 I P» 9 •____,« *____.HJT/I JCXKSK7AL PIOTE-TICX ASSMC? ZSStOH III

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AR30662I*

TA3LE I P*3«_3 ofEMVIZONMSJITAL PROTECTION AGESCT USSION III

CALIBRATION OUTLIERSSsMIVOLATILS HSL C3XPCUNOS {Pars 1 of 2)

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l a s t saa- of t h ? > t a b t g far Q g F t H T T t O M o p ca8SS._

AR306625

TA3L5 t P»S«____af_j__S3T/I RONH5STAL PROTECTION ASESCT RSSION III

CALISRATION OUTLIERSSsKtVOLATILS HSL C3HPOUNQS (Part 2 at 23

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flR306626

p-ae

OSMUITION OF COOES USSO IM TA3LE I

t » 5RS3 exceeded 305 in the initial calibration, positiveresults are qualified "J», and quantisation limits artqualified

C * S3 «xe«*d«_ 255 in tht continuing calibration. Posttivt.results art qualified "J" and quaneitacion Units art qualified"UJ".

F » RF less than O.QS in all calibrations. All quantitacion limitsarc qualified "R".

* * The "3" qualifier denoting blank contamination supersedes thequalifier issued in this table.

AR306627

63ScMIYCLATILE CRGANICS INITIAL CALIBRATION DATA

ah Name: YORK LA3S/CT Contract: 63-WS-002!


r.s-rurner.t ID: C Calibration. Date(s): 09/08/89 09/08/89

in RRF for S?CC(#) - O.OSO Max *RSD for CCC(«) - 30.0%

LAB FILE ID: RRF020- >C4474 RRF050- >CD397?.RFC30« >C4469 RRF120- >C4468 RRF160- >C4467

!1 COMPOUND

Phenol-:»is( 2-Chlorcethyl jether2-Chlorophenoll,3-Dichlcrober._er.e1,4-Dichlorobenzer.eSer.-yl alcoholL, 2-Dichlorobenzene.2-Me thvIoheno1____oisf2-ChloroisopropylJetheri 14 -Me thy 1 pher.o 1_M-Nitroso-di-n-propylamir.9_*.•iexachl or o ethaneMi trobenzene_____Isophorone_______2-Ni trophenol_____2,4-DimethylphenolBenzoic acid_____2 is (2 -Ch 1oro e tho xy}me thane_2,4-Dichioropheno11,2,4-TrichlorobenseneNaphthalene__________

, 4-Chloroani1ine______Hexachlorobutadlene4-Chlcro- 3 -methyl phenol2-MethylnaphthaleneHexachlorocycloper.tadiene_*2, 4,6-Trichlorophenol____*2,4, 5-Trichlorophenol2-Chloronaphthalene2-Ni troani1ine____Dime thyIphthalateAcenachthylene___2, 6-Dinitrotoluene3-Nitroaniline___^cer.aohthene_____2,4-Dini trophenol4-Mi troohenol

RRFQ20!RRFOSO|RRF080!RRF120|RRF160

1/87 Rev.

AR306628

6CSEMI VOLATILE CRGANICS INITIAL CALIBRATION DATA

»• Name: YORK LA3S/CT Contract: 68-W8-0021 QQ02/1

Cede: YORK Case No.: 12512 SAS No.: SDG No.: C3Q02

r.strumer.t ID: C Calibration Date(s): 09/08/89 09/08/89

in RRF for S?CC(#) - 0.050 Max %RSD for CCC(«) « 30.0%

LAS FILE I D : R R F 0 2 0 - > C 4 4 7 4 R R F 0 5 0 - >CD397RRF080» >C4469 RRF120- >C4463 RRF150- >C4467

COMPOUNDI I I I

RRF020IRRF050IRRF080IRRF120IRRF160.,,a_,|......|.,,,..!--,.,.[.._.,.

1.8661 2.0231 1.943! 1.7021 1.4960.464! 0.4921 0.540! 0.491! 0.5131.9941 1.8601 1.9111 1.560! 1.4130.8461 0.9071 0.915! 0.7911 0.7961.6491 1.6481 1.5621 1.3291 1.3330.000! 0.1421 0.0231 0.029! 0.0590.0001 0.0921 0.1211 0.132! 0.131

RRF

Dibenzofuran______________2., 4-Dinitrotoluene________Die thy1phthai a t e_________4-Chlorophenyl-pheny lether_Fluorene_________________4-Mi troar.il ine___________4, 6-Dinitro-2-methylpher.cl_M-Nitrosodiphenylamine (1)_* 0.337* 0.407* 0.395* 0.348* 0.373* 04-Bromophenyl -phenylether _riexaehlorober.zsne _________

0.2261 0.247! 0.2591 0.240! 0.210! 00.3041 0.297! 0.3231 0.3131 0.2321 0.304

Pentachlorophenol_________* 0.000* 0.176* 0.210* 0.216* 0.209* 0.203*inanthrene_____________1 0.9701 0.9771 0.973! 0.8471 0.6921 0hracene_______________! 0.963

DT-n-butylphthalate_______1 1.055Fluoranthene_____________* 0.990* 0.920* 1.058* 0.903* 0.724* 0.919* 13.6*Pyrene__________________I 1.701Butyibenzy Iphthalate______I 0.6693 ,3'-Dichlorobenzidine_____I 0.342Benzo (a) anthracene_______I 1.092Chrysene_________________I 1.010,bis(2-Ethylhexyl)phthalate_! 0.893Di-n-octylphthalate______•* 1.836* .2 . 296* 1.991* 1.582* 113enzo(b)f luoranthene_____! 1.069! Benzo (k) fiuoranthene_____I 1.3033enzoCa)pyrene____________* 0.945* 0.983* 1.121* 1.017* 1.090*! Inceno( 1, 2 ,3-cd) pyrene____I 0.878Dibenzo(a,h)anthracene____1 0 .7023enzo(g,h, i )perylene______I 0.742

0.9941 0.967| 0.8651 0.67411.2411 1.0441 0.8911 0.6761 0.9821 21.5

2.7411 2.3521 2.34510.8281 0.8421 0.808!0.2451 0.349! 0.343!1.1521 1.1971 1.20511.0681 1.1071 1.090!0.9371 0.9981 0.943!

1.2231 1.247| 1.3731 1.1431.4031 1.0431 0.815! 1.121

0.949! 1.2601 1.2221 1.7101 10.6951 0.996! 0.9511 1.3371 00.796! 1.0691 0.6931 1.5051 0.962

Mitrobenzene-d5___________I 0.2342—Fluorobipheny 1_________I 0.702Terphenyl-dl4____________I 1.784Phenol-dS_______________I 1.5602-Flucrophenol___________! 1.2032,4,6-Tribromochenol_____I 0.563

0.238] 0.2711 0.2471 0.2531 0.2491 5.90.6731 0.726J 0.7031 0.7421 0.7101 3.72.7691 2.2001 2.2471 1.7641 2.1541 19.11.3811 1.5951 1.5081 1.4991 1.5091 5.41.1511 1.2241 1.2201 1.2291 1.2061 2.70.6371 0.8231 0.7901 0.7321 0.7091 15.2_____I______I______I______I______i_____

^ v.1annot be separated from Diphenylamine

FORM VI SV-2 1/87 Rev,AR30S629

0*1

63' 3EMIVOLATILS ORGANICS INITIAL CALIBRATION DATA


ab Cods: YORK Case No.: 12512 SAS No.: SDG No.: C3Q02

nstrument ID: C Calibration Date(s): 09/15/39 09/16/89

in RRF for S?CC(*j « 0.050 Max *.RSD for CCC(*} « 30.0%

L A B FILE I D : R R F 0 2 0 - > C 4 5 7 0 R R F 0 5 0 - > C D 4 1 9 13.S.FC80- >C45o4 RRF120* >C4S63 RRF160- >C4562 1

COMPOUND! i I I i __ I *• !

RRF020!RRFOSO!RRF080IRRF1201RRF160! RRF I RSD 1

?h*noi _________________ * 1.304* 1.262* 1.355* 1.213* 1.261* 1.279* 4.2*bis(2-ChLoroe.h.yl ) ether2-Ch 1 or opheno 11,3-Dichiorobenzene1,4-Dichlorobenzene3er.cyl alcohol

, 2-Dichlorobenzene.2 -Me chy 1 pher.o _ ____ _bis(2-Chloroiscpropyljether4-Me thy 1 pher.o 1M-Nitroso-di-n-prooylamine_*Hexachl oroe thane__________1Ni trobenzene_____________1Isophorone______________12—Ni tropheno 1____________*2 , 4-Dimethy 1 phenol________!Benzoic acid.bis(2-Chloroethoxy)methane_!2 , 4-Dichlorophenol________*1, 2,4-Trichlorobenzene____1. Naphthalene______________11 4—Chloroani 1 ine___________!I Hexachlorobutadiene______*I 4-Chloro-3-methylphenol___*1 2-Methyl naphtha Iene_______IIKexachlorocyclopentadiene_*2,4 , 6-Tr ichlorophenol_____*2,4,5 -Tr i chl orcphenol_____ I2-Ch 1 oronaphtha 1 ene______!2-Ni t roan i line__________1Dime thy Iphtha late________IAcer.aphthylene___________I2 f 6-Dinitro toluene_______t3—Ni troani 1 ine____________ IAcenaphthene ______________ * 1.374* 1.464* 1.525* .2,4-Dinitrophenol ________ _* 0.000* 0.146* 0.214* 0.263* 0.264* 0.222* 25.1*4-Nitrophenol _____________ .* O.OQO* 0.206* 0.234* 0.252* 0.246* 0.235*

FORM VI SV-i 1/87 Rev>

AR306630

6CSET-tlVOLATILE ORGANICS INITIAL CALIBRATION DATA

000273Name: YORK LA3S/CT Contract: 68-W8-0021

Cede: YORK Case No.: 12512 SAS No.: SDG No.: C3Q02

nstrument ID: C Calibration Date(s): 09/15/89 09/16/89

in RRF for S?CC(») - 0.050 Max %RSD for CCC(«) - 30.0%

LAS FILE I D : R R F 0 2 0 - > C 4 5 7 0 R R F 0 5 0 - >CD419REF030- >C4564 RRF120- >C4563 RRF160'- >C4S62

COMPOUND RRF0201RRF0501RRF0801RRF120

Dibenzofuran_____________2,4-Dinitrotoluene________Diethylphthaiate_________4—Chlorooheny 1—pheny 1 ether_Fluorene______________________4-Nitroani1ine__________4,6-Dinitro-2-methylphenoi_M—Nitrosodipher.ylamine (1)_4-3rotr.ophenyl -phenylether_Hexachiorobenzene________Pencachlorophenol________

1.9480 .4382.0790.773

2.152!0 .599!2.235 I0.8651

1.6701 1.771!0.000! 0.238!0.0001 0.12710.466* 0.517*0.209! 0.21810.268! 0.28010.000* 0.163*

•nanthrene.(hracene.-r.-buty Iphtha late.

0.9991.0371.269

Fluoranthene____________* 1.054* 1.215*2.7631.1600.2731.5341.4121.417

Pyrene___________________ 1.955Sutylbenzyiphthalate_____ 0.8223,3' -Dichlorobenzidine____ .0 .3743enzo (a)anthracene_______ 1.087Jhrysene________________ 1.091

. bis(2-Ethylhexyl )phthalate_ 1.027! Di-n-octylphthalate______* 2.494!Benzo(b)f iuoranthene_____ 1.402|Benzo(k)f luoranthene._____ 1.356

2.494* 2.781* 31.7241.203

I Benzo (a) pyrene___________* 1.038* 1.263* 1Indeno :. 1, 2 , 3 -cd) pyrene.Di benzo(a,h)anthracene.Benzo(g,h,i Jperylene

0.7410.533

1.0601.1111.322

1.1270.851

0.6031 0.925

1.1980.9480.986

Nitrobenzene—d5____2-Fluorobipheny1___rerphenyl-d!4______Pheno1-d5_________.-Fluorophenol_____2,4,5-Tribromcphenol.

0.2711 0.3471.2191 1.3151.1331 1.6071.5821 1.6341.238! 1.2760.3771 0.351

0.3411.3811.4551.6311.3670.451

0.3371 0.3601.2411 1.0161.633! 1.6821.478! 1.5861.2421 1.2190.4881 0.454

0.3321 10.51.2351 11.21.5031 14.81.5831 4.01.2691 4.60.4251 13.6

ar.not be seoarated from Diphenylamine

FORM VI SV-2 1/87 Rev.

flR30663i

OSSEMI VOLATILE ORGAMICS INITIAL CALIBRATION DATA

ab Name: ' YORK LA3S/CT Contract: 63-W8-0021 00027.4


instrument ID: C Calibration Date(s): 09/17/89 09/17/89

in RRF for S?CC(#) « 0.050 Max %RSD for CCCC*) - 30.0%

*

LAB FILE ID: RRF020- >C4592 RRF050- >CD421?.RF030» >C4590 RRF120- >C4537 RRF160- >C453S

I I I i f I ___COMPOUND IRRF0201RRFOSOIRRF080!RRF120IRRF160I RRF RSD I

Phenol _________________ * 1.335* 1.299* 1.431* 1.221* 1.305* 1.319* 5.8*ois(2-Cr.loroethyl jether___! 0.8701 1.139! 1.2441 1.244! 1.2541 1.1512-Chlorophenoi____________i 1.2371 1.227! 1.290! 1.165! 1.207! 1.2361, 3-Dichlorobenzsne_________\1, 4-Dichlorobenzene_______*Senzyl alcohol___________11, 2-Dichlorobenzene_______!2— Methyl pher.o i_____________I

14.3 t4.4!

bis(2-Chloroi3opropyl]ether 14—Methyl pher.o L___________1N—Ni troso-di-n-procylamine_*.-iexacr. loroe thane__________IDXI trobenzene_____________1Isophorone_______________ I2—Ni trophenol___________*2 ,4-Dimethylphenol________IBenzoic acid_____________i_>is( 2-Chloroethoxy }methar.e_i2, 4-Dichlorochenol_______*1,2,4-Trichlorobenzene.Naphthalene___________4-Chloroaniline_______Hexachlorobutadiene___4-Ch 1 oro- 3 -me thy 1 pher.o 1.2— M-sthvlnaohthai ene___Hexach 1 or ocy eloper, tad iene_*2,4, 6-7r ichlorophenol_____*2,4, 5-Trichlorophenol____2—Chloronaphthai ene______2-Nitroar.il ine___________Dime thyIphthalateAcenaph thy i ene2, 6-Dinitrotoluene.3—Nitroaniline_____Acenaohthene_____________*2,4-Dinitrophenol_________**4-Nitrophenol____________*

FORM VI SV-1 1/87 Rev,AR306632

•6C

SEMIVOLATILE CRGANIC5 INITIAL CALIBRATION DATA

QOG275YORK LA3S/CT Contract: 68-W3-0021


nstrunent ID: C Calibration Date(s): 09/17/89 09/17/89

in RRF for S?CC(*) » 0.050 Max %RSD for CCC(*) » 30.0%

LAS FILE ID: RRF020- >C4592 RRF050- >CD42lERFOSO- >C4590 RSF120- >C4587 RRF160- >C4535

COMPOUND RRF0201RRF050I 1 I

RRF080IRRF1201RRF160

D ibenzofuran_____________2.4-Dini trotoluene________DiethyIphthalate_________4-Ch1o ropheny1-pheny1e ther_Fiuorer.e________________4-Mitroar.i 1 in-e___________4, 6 -D i n i t r c - 2 -me thy 1 pher.o 1_

4-Sromopheny 1 -pheny 1 ether _He xach lore benzene _________Pentachlorocheno i

nracene.Di-n-butyIphthalate_Fluoranthene_______Pyrene____________3utylbenzylphthalate_3,3'-Dichlorobenz idine.Benso (a) anthracene_______Chrysene________________.bis(2-Ethylhexyl)phthalate_i Di-n-octylphthalate______! Benzo (b) f luoranthene______I Senzo f k ) f luoranthene______

0,1720.2190 .0000.8530.9091.111

2.1130.5252.1010.8841.6460.1920.1390.4710. 2340.2980 .1761.0871.1021.426

0.967* 1.3111.2800.6440.4141.0000.9451.0592.2491.0900.976

1 Benzo(a)pyrene___________* 0.895I Indeno( 1, 2 , 3-cd) pyrene____I 0.816Diber.zo (a,h) anthracene.Senzof ?,h,iJperylene__

0.6000.620

1.8330.9530.4011.3151.2891.2623.3771.5221.4551.2570.9870.7900.778

1.79310.50911.70810.733!1.45017.29010.147!0.519*0.24010.310|0.181*1.04211.031!1.08511.153*1.91110.99810.37311.40211.26111.37712.926*1.35411.45411.244*1.097]0.8570.841

Nitrobenzene-d5_2—Fluor obi pheny 1.Terpheny1-dl4___Pheno1-d5______2-F1uoro oheno1__2,4,6-Tribromophenol.

0.2361.0730.8501.6491.2680.402

0.3221.4011.2781.6391 .2460.400

0.3341.4531.2491.7831.3430.414

0.3381 0.3311 0.3131 13.7|1.3551 1.1991 1.2971 12.111.1121 1.0431 1.1071 15.611.5661 1.5731 1.6431 5.311.2021 1.2751 1.267] 4.1!0.5231 0.4671 0.4421 12.01————— I_____!_____I____I

t be separated from Diphenylamine

FORM VI SV-2 m-+-.n-mn 1/87 Rev.

63SEMIVOLATILE CRGANICS INITIAL CALIBRATION DATA

P APO"? <"»vUc~:; oab Name: YORK LA3S/CT Contract: 63-W8-0021 ^k

ab Code: YORK Case No.: 12512 SAS No.: . SDG No.: C3Q02

nstruner.t ID: H Calibration Date(s): 09/02/39 09/02/89

in RRF for SPCCC*} - 0.050 Max %RSD for CCC(*) - 30.0%

L A S FILE I D : R R F 0 2 0 - > H 5 5 7 4 R R F O S O - >HD223>H5372 RRF120- >H5570 RRF160- >H5563

I 1 I ! I ! __COMPOUND JRRF020iRRFOSOIRRF0801RRF120IRRF1601 RRF

,«>.*,»-,,.,.,-.,--,._,,-.,[..,.,«|......| ------|_-,--.| ...... | ..,-..|---.-iPhenol_____________________* 2.130* 1.813* 1.662* 1.588* 1.473* 1.734* 14.7*3isi2-Ch!oroe.ayi)ether___t 1.923! 1.797! 1.623! 1.7071 1.5901 1.730 8.01_-Chiorocher.oi__I__________1 1.602! 1.4121 1.313! 1.292! 1.169! 1.353 12.011,3-Dichlorcbenzene_______! 1.7331 1.531! 1.325! 1.196! 1.1031 1.378 18.611,4-Dichlorobenzene_______* 1.735* 1.507* 1.322* 1.205* 1.072* 1.369* 19.0*3enzyl alcohol____________I 0.903! 0.815! 0.751! 0.554 0.606! 0.746 16.1!1,2-Dichlorobenzene_______1 1.637! 1.413! 1.2031 0.963 0.8221 1.213 23.512-Me thy Ipheno i____________I 1.667! 1.446! 1.3151 1.235 1.187! 1.371 14.11bi3(2-ChloroisooropyiJetherl 4.503! 4.002! 4.007! 3.829 3.7281 4.014 7.514-Meth.ylaheriol ______1 1.552! 1.3871 1.307! 1.253 1.1831 1.338 10.51N-Nitroso-di-n-propylamine_* 1.618* 1.474* 1.375* 1.203* 1.027* 1.340* 17.3_*HexachloroethaneNitrobenzeneIsophorone2—Ni trophenol2,4-DimethyIphenoBenzoic acidbis(2-Chlorcethoxy)methane_

•0.775! 0.6371 0.619! 0.494! 0.4111 0.5981 240.511! 0.4711 0.4321 0.3991 0.3821 0.4401 121.0161 0.904! 0.809! 0.7401 0.705! 0.8351 15.2!0.231* 0.218* 0.215* 0.203* 0.189* 0.212* 7.6*0.4671 0.3901 0.3781 0.3611 0.331! 0.3861 13.2!0.0001 0.1221 0.160! 0.1831 0.2041 0.163! 21.110.5831 C.525I 0.4741 0.4481 0.4201 0.4901 13.31

2,4-Dichlorophenol________* 0.374* 0.317* 0.293* 0.271* 0.242* 0.300* 16.8*1,2,4-Trichlorobenzene____! 0.392! 0.362! 0.3131 0.283! 0.2631 0.323! 16.7|.Naphthalene_______________1 1.179! 0.979! 0.875! 0.7371 0.6751 0.8891 2.3 .fij^14-Chloroar.il ine___________! 0.4561 .0.395! 0.3371 0.2431 0.2031 0 . 323 isQli.Jj)i Hexachlorobutadlene______* 0.214* 0.196* 0.172* 0.149* 0.137* 0.174*T3T4*I4-Chloro-3-methylphenol___* 0.452* 0.379* 0.373* 0.347* 0.312* 0.373* 13.9*[ 2-Methylnaphthaler.e_______i 0.753! 0.652! 0.569! 0.4921 0.444! 0.5821 21.31"Hexachlorocyclopentadiene_* 0.351* 0.433* 0.373* 0.361* 0.358* 0.377* 8.9*2,4,6-Trichlorophenol_____* 0.529* 0.490* 0.429* 0.407* 0.356* 0.443* 15.4*2,4,5-Trichloroohenol_____i 0.0002-Chiorona?hthaiene______\ 1.4702-Nitroaniline___________! 0.000Dimethyiphthaiate________1 1.886Acenaphthylene___________I 2.5262,6-Dir.itrotoluer.e_______I 0.4553-Nltroar.il ine____________1 0.000

0.572! 0.496! 0.4761 0.407 0.483 13.91.3911 1.134! 1.0231 0.937 1.202 19.10.6141 0.6221 0.5521 0.552 0.586 6.61.831! 1.5651 1.4061 1.344 1.607 15.32.272! 1.9511 1.602! 1.430 1.968 22.30.4981 0.436! 0,408! 0.395 0.439 9.30.3151 0.217! 0.145! 0.1711 0.2121 (3$~T&

Acenashthene______________* 1.620* 1.407* 1.193* 1.011* 0.893* 1.225* 24.1*2,4-Dinitrophenol_________* 0.000* 0.259* 0.248* 0.267* 0.249* 0.256* 3. *4-Nitrooher.ol______________* 0.000* 0.172* 0.194* 0.186* 0.171* 0.131*_______1________________\_______1______I______1______1—____I______1.

SEMIVOLATILE ORGANICS INITIAL CALIBRATION DATA QQG2'/ f

,Name: YORK LA22/CT Contract: 63-W8-0021

afc Code: YORK Case No,: 12512 SAS No.: SDG No.: C3Q02

nstrumer.t ID: H Calibration Date(s): 09/02/39 09/02/89

in RRF for S?CC(#) - 0.050 Max %RSD for CCC(*) - 30.0%

L A S FILE I D : R R F 0 2 0 - > H 5 5 7 4 R R F 0 5 0 » > H D 2 2 3 I2.RF080- >H5572 RRF120- >H5570 RRF160» >H5568 I

COMPOUND RRF020I I i I ___ 1 %

RRF0501RRF0801RRF120IRRF160I RRF I RSD

Dibenzofuran______________,4-Dinitrotoluene________Die thy1phtha1a t e_________~—Ch1oropheny1-pheny1e ther_Fluorene__________________—Ni troar. i 1 ine____________4,6-Dinitro-2-methylphenol_

2.2920.6291 .9490.8301.7400 .0000 .000

2.0791 1.7471 1.5241 1.3701 1.8031 21.20.6391 0.6121 0.601! 0.5391 0.624! 6.31.8081 1.5501 1.3251 1.162! 1.5591 20.90.753! 0.53SI 0.4331 0.4071 0.6131 29.21.4531 1.1771 0.9071 0.724! 1. 2 0 0 I <_,_____Q0.1731 0.058! 0.047! 0.063! 0.0870.1911 0.1791 0.181! 0.1691 0.1301 4.9

.\r-Nitrosodioher.ylamine (1)_* 0.431* 0.379* 0.365* 0.326* 0.281* 0.367* 20.3*i-3romochenyi-?henvlether_ 0.253! 0.2241 0.2091 0.189! 0.163! 0.209! 15.6!-:exachlorobenzene_________ 0.3591 0.317| 0.2901 0.256! 0.2371 0.2921 16.6!sgntachloropher.ol________* 0.000* 0.218* 0.209* 0.208* 0.177* 0.203* 8.8*J^nanthrene______________I 1.3001 1.0481 0.9321 0.8051 0.724! 0.9621 23.51sKsiracene________________I 1.2761 1.0791 0.957| 0.8221 0.6941 0.966! 23.41M-n-butylphthalate_______I 1.6951 1.4371 1.3001 1.177! 1.0421 1.3301 18.91Fluoranthene______________* 1.501* 1.272* 1.144* 1.023* 0.912* 1.171* 19.5*Pyrene____________________I 1.5971 1.3761 1.2501 1Butyibenzylphthalate______! 0.8361 0.6671 0.7093,3 '-Dichlorobenzidine.3enzo ( a ) anthraceneThrysene

, t>is( 2-Ethylhexyl } phtha late_Di-n-octylphthalate_______* 1.831* 1.574*Benzo ( b ) f iuoran theneBenzo ( k ) f luorantheneBenzo ( a ) pyrene _______Incer.o (1,2 , 3-cd ) pyrene.Di benzo ( a, h) anthracene.3enzo(g,h, i ) per y Iene __

0.493! 0.4341 0.4031.3671 1.2351.4061 1.2351.3071 1.030

1.386! 1.24411.1111 1.12911.183* 1.122* 11.3271 1.095! 01.0301 0.8771 0.6671.0281 0.8331 0.465

1.1230.7290.391 I

266 .0.946 I0.9971826*

1.0901.0381

Mitrobenzene-d5____2—Fluorobipheny1___Eerpheny1-dl4______?h.enol-c5__________i—Fluorophenol______2,4,6-Tribromophenol.

^T C

0.4901 0.4531 0.4391 0.4131 0.4021 0.4401.8121 1.6201 1.3341 1.1431 1.0581 1.3951.1891 0.992! 0.912! 0.9151 0.8631 0.9752.3261 2.0951 1.9521 1.8761 1.7951 2.0091.568! 1.438! 1.3531 1.2921 1.2461 1.3800.5471 0.4811 0.4501 0.4251 0.3841 0.458

_____I_____I_____1_____!_____

7.9!22.8113.2110.4!9.21

13.51

Cannot be separated from Diphenylamine £|^ ^ *•&$ "^"C y O T ^y ( J«« _(*•

Cp^

FORMVisv-2 CB9H flR3QS635~

I d

73SEMIVCLATILS CONTINUING CALIBRATION CHECK _.

0004S3ab Name: YORK LA3S/CT Contract: 63-W8-OC21

ab Code: YORK Case No.: 12512 SAS No.: • SDG No.: C3Q02

astrument ID: C Calibration Date: 09/09/39 Time: 11:34 •

ab File ID: >C340l Init. Calib. Date(s): 09/08/89 09/08/89

in RRF50 for S?CC(*) - 0.050 Max %D for CCCC*) - 25.0%

COMPOUND 1 RRF IRRF50 1 %D I».««._»«>...».«,»__.m»._».|_--__-|_.««.,|«._.._,| £3 _0 CO

Phenol ___________________ *bisc 2-Chloroethyl } ether ___ t2-Chlorophenol ____________ !

1Iscphorone_______1 2-Nitrophenol____f 2,4-Dimethyl?henol.ISenzoic acid_____b is(2-Chloroethoxy)methane.2,4-Dichlorochenol_______1,2,4-Trichlorobenzene.Nash thai ene________'4-Chloroar.il ine__________tHexachlorobutadlene______*4-Chloro-3-methy Ipheno i___*2-Methyl naphtha Iene______IKexach 1 orocyc1opentad i ene_*2,4, 6-Trichlcropheno 1_____*2,4,5-Trichlorophenol____2-Chlor©naphthalene______2-Ni troani1ine___________DimethyIphthalate________Ac e naoh thv1ene___________2,6-Dinitrotoluene.3-Nitroaniline___Acenaohthene_____2,4-Dini trophenol.4-Ni troohenol___

I 1 ,3-Dichlorobenzene _______ 1 . . . r R OI 1 ,4-Dichlorobenzene _______ * 1.352* 1.302* 3.6*i Benzyl alcohol ____________ I 0.6751 0.6901 2.1 C£<5> IT! 1 , 2-Dichiorobenzene ______ ! 1.2441 1.2501 1.2 Cg<9 (î 2-Methylpher.cl ____________ 1 1.0731 0.972! 9.9 Ce>o - _,i bis(2-Chloroisopropyl Jetherl 1.9061 1.6711 12.3i 4 -Me thy 1 pher.o I ___________ \ 0.937| 0.8941 4.5 C£0 0*1 - I!N-.Mitroso-di-n-propylamine_* ~ ~~'" " " ' " " ' -'1 Kexachloroethane _________ INitrobenzene _____________ 1 0.2361 0.2891 0.9 4fe

VII SV-1

. 7CSEMIVCLATILE CONTINUING CALIBRATION CHECK

000453__> Name: YORK LA3S/CT Contract: 63-W3-0021

Code: YORK Case No.: 12512 SAS No.: • SDG No.: CBQ02

nstrument ID: C . Calibration Date: 09/09/89 Time: 11:34

ab File ID: >CD401 Init. Calib. Date(s): 09/08/89 09/08/89

in RRF50 for's?CC(*) - 0.050 Max %D for CCC(«) - 25.0%

COMPOUND

Dibensofurar.2 . 4-Din.itrotoiuen.eDie thv 1 sht ha late4-Chiorophenyl -pheny lether_Fluorene4-:; itroar.il ine4 , 6-Dinitro-2-methylphenol_N-Ni trosodiphenylamine (!)_'4 -Bromophenyl -phenylether _Kexachlorober.zen.e , , ,Psn.tachlorochen.ol iPher-anthrer-eAnthraceneDi-r.-butylohthalateFlucranthenePyreneButyl benzyl phtha late3 f 3 ' -DichlorobenzidineBenzo ( a) anthraceneChrysenebis ( 2-Ethylhexyl )phthalate_Di-n-octylphthalateBenzo ( b ) f luoranthene ,.„„._„ , ,.Benzof k) f luorantheneBer.zo(a)pvrene iIndeno(l r2 ,3-cd ) pyrene ,Di benzo ( a rh) anthracene ,,.Benzo (g,h,. i ) cerylene „ „ , ,, ,

Mi tr-obenzer.e-dS2-FluorobiphenylTerr3h.en.yl-d 14Phenol -d52 - F 1 uorochen.o 1"> '- , 4 , -Tr iferomors'nen.ol IMI . ., , ,,

I ___RRF......1.8060.5001.7490.8511.5050.0640.119

* 0.332*0.2370.304

« 0.203*0.8920.8930.982

* 0.919*2.2160.7850.3161.1601.0810.950

* 1.835*1.2121.137

* 1.031*1.2040.9360.962

0.2490.7102.1541.5091.2060.709

RRF 30

1.9710 5081.9670.9241.6820.1070.119

t 0.400*0.2480.279

t 0.174*0.9800.9831.282

t 0.932*2.9060.8650.2591.0691.0740.840

r 2.065*1.2931.239

t 1.060*0.9680.8421.123

0.2630.7072.9081.4511.1480.646

I%D |

9.111.5 1

12.418.51

11 PI2J__iC6J.J3:

0.6I* 4.5*

4. 718.41

* 14.1*9.81

10_0 1/-*" "Q_L_Sx?* 1 3 *CHIP

10.218.07.80.6

11.4« 12.5*

6.613.3

* 2.7*19.610.016.7

5.60.3

C_35_JD33.84,8

1 8.91

(1) Cannot be separated from Diphenylamine

FORM VII SV-2 AR30S637 1/87 ReV'

73SEMI VOLATILE CONTINUING CALIBRATION CHECK

OOOcOOab Name: YORK LA3S/CT Contract: 68-W8-0021


nstrument ID: C Calibration Date: 09/16/89 Time: 09:39


in RRF50 for-SPCCC*) - 0.050 Max %D for CCC(*} « 25.0%

ICOMPOUND ! RRF IRRF50

bis(2-Chlcroe.hyl)ether___t 1.130! 1.1882-Chlorophenol____________1 1.2201 1.1291,3-Dicr.lorobenzene_______1 1.494! 1.409

I%D

t Phenol___________________* 1.279* 1.302* 1.7*0.6 t7.415.61

1, 4-Dichlorobenzene_______* 1.501* 1.540* 2.6*Benzyl alcohol___________! 0.642! 0.6531 1.611,2-Dichlorobenzene_______I 1.439! 1.4711 2.2!2-Me thy 1 pher.o 1____________1 1.1171 1.114! 0.2!bis(2-Chloroisopropyljether1 1.6001 1.510! 5.614 -Me thy 1 pher.o l_l___________I 0.9821 0.994! 1.1!N-Nitroso-di-r.-?ropylamine_* 0.872* 0.795* 8.8*Hexachloroethane__________I 0.6181 0.634! 2.51Nitrobenzene_____________! 0.3491 0.349! 0.0Isophorone________________! 0.691! 0,7151 3.42-Nitrophenol_____________* 0.189* 0.182* 3.6*2,4-Dimethylphenol________1 0.387! 0.382! 1.3Senzoic acid______________1 0.245! 0.233bis(2-Chloroethoxy)methane_l 0.4021 0.3902 , 4-Dichloroohenol________* 0.335* 0.338* 0.81,2,4-Trichlorobenzene____1 0.374! 0.368Naphthalene______________1 0.9561 0.974

4.72.7

. 1.6. 1.810.94-Chloroaniline___________I 0.327! 0.363

Hexachlorobutadiene_______* 0.231* 0.222* 4.0*4-Chloro-3-methylphenol___* 0.384* 0.397* 3.2*2-Methylnaphthalene_______1 0.699! 0.7181 2.71Hexachlorocyclopentadiene_* 0.321* 0.329* 2.5*2,4,6-Trichlorophenol_____* 0.513* 0.462* 9.9*2,4,5-Trichlorophenol_____1 0.6211 0.624! 0.52-Chloronaphthalene_______I 1.1861 1.300! 9.52-Ni troani line____________\ 0.409! 0.393! 3.9Dimethylphthalate_________I 1.6671 1.987J 19.2Acenaphthylene____________I 1.779! 2.1771 22.42,6-Dinitrotoluene________[ 0.4141 0.4071 1.63-Mi troani line____________! 0.3261 0.3521 7.8Acenaphthene______________* 1.364* 1.485* 8.8*2, 4-Dini trophenol________# 0.222* 0.172* 22.4*4-Nitroohenol_____________# 0.235* 0.224* 4.7*

FORM VII SV-1 1/87 Rev,

AR306638

7CSEMIVCLATILE CONTINUING CALIBRATION CHECK

000501»Name: YORK LABS/CT Contract: 68-W3-0021

Code: YORK Case No.: 12512 SAS No.: - SDG No.: C3Q02

nstrument ID: C Calibration Date: 09/16/39 Time: 09:39


in RRF50 for's?CC(*) - 0.050 Max %D for CCC(*) « 25.0%

(l) Cannot be separated from Diphenylamine

COMPOUND

D i benzo furar.2 . i-Dinitrotolusn.eDiethvlchthaiate , „. ,4 -Ch i or opheny i -pheny 1 e ther_

1 Fluorene4-Ni troar.i line4 , 6-Dinitro-2-methylphenol_M'-N'i trosodiphenylamine ( 1 )_4- Bromo pheny i -phenylether _riexaehlorober-zeR-e., „. ,., ,,,Pentachloroohenol., , , , ,, , ,*PhenanthreneAnthraceneDi-n-butylohthalateFluoranthene *PyreneButylbenzy Iphtha late3.3' -Dichlorobenzidirie,,, .„,, „.,,Benzo f a ) anthraceneChrvsenebis ( 2-Ethylhexyl )phthalate_Di-n-octylohthalate >Benzo ( b 1 f luorantheneBenzo ( k } f luorantheneBenzo(a)oyrene *Indeno( 1 , 2 ,3-cd) pyrene. , , , „D i benzo ( a, h) anthracene. .,Benzo (g rhr i }perylene

Mi trofaen.zen.e-d5.,2-Fluorobinhen.ylTerahenvl-dl4 , ... „ , ,....Phenol -dS2 - F 1 vi o rooh.en.0 1 ,">- ,6- t fi-T-ri h»-omonhen.ol

RRF

1.7470.5711.7660.7911.5450.2210.145

« 0.4900.2230.272

* 0.1730.9040.9150.992

* 0.9532.3621.0500.3191.3741.3001.237

* 2.6111.4781.404

» 1.2711.3281.0171.121

0.3321.2351.5031.5831.2690.425

RRF 50

2.1220.5982.1750.803

1 1.6310.2520.130

* 0.4940.2260.257

* 0.172*1.155

1 1.2211.382

* 1.036*3.5691.0810.2741.2611.2041.205

* 1.962:1.207

! 1.360* 1.152*

1.5971.2531,414

0.3201.3941.7791.5951.2970.378

%D,-.,-.

21.44.7

23.11.46.9

13.610.6

r 0.81.45.3

* 0.?*rj7_ 7Jda^ -, j-^— — * "*•C39.3J

t JLJL_<_Ti.Q-

2.914.08.27.4

' 6.4* 24. Q*

18.23.0

^ 9.3*20.223__2

_--_— -" w

0S.JJ

3.512.818.30.72.2

11.0

FORM vii sv-2 AR306639 1/87 Rev-

73SEMIVOLATILE CONTINUING CALIBRATION CHECK nnn^nU U U \»« J


ab Code: YORK " Case No.: 12512 SAS No.: . SDG No.: C3Q02

nstrument ID: H Calibration Date: 09/09/89 Time: 15:40

ab File ID: >HD237 Init. Calib. Date(s): 09/02/89 09/02/89

in RRF50 for-S?CC(#) - 0.050 Max %D for CCC(*) - 25.0%

COMPOUND 1 RRF

Phenol_______________b is(2-Chlorce.hyl)ether.2-Chlorochenol________1,3—Dichlorobenzene.t,4-Dichlorobenzene.Eenzvl alcohol_____1,2-Dichlorobenzene.2 —Me «hv 1 cher.o 1________b i s t 2-Chlorciscpropyi)ether 14 -Me thy 1 pher.o I____________ IN-Wi troso-di-n-propylamine_*K exach i or o ethane_________1Ni trobenzene_____________1Iscphorone_______________!2-Ni trophenol_____________*2 , 4—Dimethyl phenol________1Benzoic acid_____________Ibis(2-Chloroethoxy)methane_|2 , 4-Dichlorcphenol________*1,2, 4-Tr ichlorobenzene____!Naph tha 1 ene_____________ 14-Chloroani 1 ine__________ 1Kexachlorobutadiene________*4-Chloro-3-methyl phenol___*2 -Me thy 1 naphtha 1 ene_______ 1Kexach1orocyclopentadiene_*2,4, 6-Trichlorophenol_____*2,4,5-Trichlorophenol____2-Chloronaphthalene______2-Nitroaniline___________DimethyIphthalate________Acenaohthvlene__________2,6-Dinitrotoluene.3-Ni troani line_____Acenaphthene_____2 , 4-Dini tropheno 1.4-Ni troohenol___

313 1C228*248*183*

FORM VII SV-1 i/87 Rev

7CSEMIVOLATILE CONTINUING CALIBRATION CHECK •

Name: YORK LA3S/CT Contract: 63-W3-0021

Code: YORK Case No.: 12512 SAS No.: . SDG No.: CBQ02



in RRF50 for's?CC(*) » 0.050 Max %D for CCC(*) - 25.0%


1COMPOUND 1

Di benzo fur an 12 , 4-Din.i trotoluene ,, .„„.„,.,, ,.,,. 1Dieihy Iphtha late I4-Ch 1 o ro pheny 1 -pheny 1 e ther_ 1Fiucrsne 1f= -Mi troani line 14, 6-Dinitro-2-methylphenol_tM-Ni trosocichenylamine (1)_*4 -Bromophenvi-ohenv lather 1Hexachlorobenzene 1Pentachloroohenol *Phenanthrer.e 1Anthracene ID i -n.-but y 1 chtha late ,__ __ .._. , 1Fluoranthene *Pyrene !Sutvlbenzvlchthalate 13 , 3 '-Dichlorobenzidine 1Benzo f a 1 anthracene 1Chrvsene 1bi s f 2-Ethylhexyl ) phthalate_|Di-n-octylchthalate .*Benzo (b)f luoranthene 1Benzo ( k) f luoranthene .... , ,„„. 1Senzof a)ovren.e *Inden.0 ( 1 f 2 , 3-cd)pvrene ... 1Di benzo (a, h) anthracene ISen.20 ( gfh.r i )oerylen.e ,!

Mit.roben.zene-d5 , 12-Fluorobiphenyl 1Terph.en.yl-d! 4 1Phenol -dS 1•l-=*luorophan.ol 1

1

___ 1RRF | =

1.803!0.62411.559!0.61311.20010.087!0.180!0.367*0.20910.29210.203*0.962!0.966 |1.33011.171*1.31910.73810.426!1.28311.14211.086!1.748*1.22411.03811.074*0.810!0.686 I0.5541

0.440!1.39510.97512.00911.38010.4581

1

IIRF50 1.»..». I -1.83910.55911.543!0.64711.33110.1381 «0.17410.366*0.17310.182 10.153*0.990 |1.036!1.40111.125*1.412!0.88410.371!1.240!1.156!1.221!2.105*1.260!1.05311.077*1.07710.868! <0.871K------|-0.306!0.829 I1.15711.94511.30010.2481

I

I%D I

1.9110.4!1.015.51

1_U5JC5JL-i''i

3.410.1*17.3 !

<C%7 _4-t24.7*2.9!7.215.313.9*7.0119.7112.913.311.21

' 12.4120.3*2.9|1.410.2*

dTj-i-1"ifeTAJ~~57 2-r vrrc_~b._r^_tO 518.63.15 .7

( 45 7~V * ~f • *

FORM VII SV-2 AR3066U 1/87 Rev,

73SEMIVOLATILE CONTINUING CALIBRATION CHECK

\J

ab Name: YORK LA3S/CT Contract: 6S-W8-0021


nstrument 'ID: K Calibration Date: 09/11/39 Time: 12:17


in RRF50 for-S?CC(*) - 0.050 Max %D for CCC(*) - 25.0%

COMPOUND i RRF 1RRF50

Phenol___________________* 1.734* 1.656*1.7301 1.453

1 2-Chlorophenol! 1,3-Dichlorobenzene[i,4-DichlorobenzeneiBenzvl alcohol-, 2-Dichlorobenzene.

1.358! 1.3511.3781 1.3071.369* 1.303*0.746! 0.7291.2181 1.141!1.3711 1.3054.0141 2.3381.333! 1.295

N'-Nitroso-di-n-?ropylamine_# 1.340* 0.937*Hexachl oroe thane__________ 0.5981 0.547

0.4401 0.3450.835! 0.6620.212* 0.245*0.3861 0.367

I 2-Me -.hy 1 pher.o 1 ___________i bi s(2-Chloroi sopropy1)ether1 4-Me thv1sheno1___________

M. i trober.zer.e____________Isophorone______________2-Ni trophenoi_____________2 . 4-Dimethylphenol_______Benzoic acid_____________b i s C 2-Chloroethoxy)methane_

0.1630.490

2 , 4-Diqhiorophenol________* 0.300* 0.313* 4.5*1,2, 4-Trichlorobenzene____[ 0.323Naphthalene______________1 0.8894-Chloroaniline__________1 0.328

0.2510.399

0.293! 9.310.816! .8.210.2631 13.21

Hexachiorobutadiene _______ * 0.174* 0.137* 21.3*4-Chloro-3-methylphenol ___ * 0.373* 0.358* 4.0*2-M.ethylnaphthalene _______ f 0.532! 0.539! 7.51Hexachlorocycloper.tadiene _ * 0.377* 0.340* 9.6*2 , 4 , 6-Trichlorophenol _____ * 0.443* 0.441* 0.4*2 ,4,5-Trichlorophenol _____ I 0.438! 0.5081 4.02-Chloronaphthalene _______ 1 1.2021 1.1281 6.12-Ni troar.il ine ___________ 1 0.586! 0.4661 20.3Dimethylphthalate _________ I 1.607) 1.5041 6.3Acenaphthylene ____________ 1 1.968! 1.8051 8.32,6-Dinitrotoluene ________ ! 0.439! 0.3971 9.53-Mitroaniline ____________ ! 0.212! 0.2991Acenaphthene _____________ * 1.225* 1.106*2, 4-Dini troohenol _________ * 0.256* 0.355*4-Nitrophenol _____________ * 0.181* 0.219* 20.6*


AR3066U2

7CSEMIVCLATILE CONTINUING CALIBRATION CHECK nnn=.nV d \_, t_' a i

Name: YORK LA3S/CT Contract: 63-WS-0021

Code: YORK Case No.: 12512 SAS No.: . SDG No.: C3Q02


ab File ID: X-ID239 Init. Calib. Date(s): 09/02/89 09/02/89 •

in RRF50 for'S?CC(*) * 0.050 Max %D for CCC(«) « 25.0%

! COMPOUND

Dibenzofuran2 . 4-Dini trotolueneD i e th v 1 oh tha late,4 -Ch 1 or opheny 1 -pheny 1 e ther_Fluorene4-Ni troar.i 1 ine4 , 6-Dini tro-2-me thy Ipheno 1_N-Ni trosodichenylamine ( 1 )_4 -Sromophenyl -phenylether _Hexachl or ober.z enePentachloroohenol .. *FhenanthreneAnthraceneDi-n-butvlnhthalateF luoranthene :PvreneSutvlbenzvlohthalate3.3' -Dichlorobenzidine,,, „,..,. ,,,Benzo fa) anthracene ,,,„. ..,Chrvsenebis(2-Ethylhexyl )phthalate_Di-n-octvlshthalate, , *Benzo f b ) f luorantheneBenzo f k ) f luorantheneBenzo (a)pvrene iIndeno( 1,2, 3 -cd) pyrene,,. ,, .„ .D i benzo ( a, h) anthraceneBer.zo(cfh, i Icerylerie

Ni trobenzene-d5_. .2 -F luor obi cherry 1Terrshenyl-dl4Phenol -d52-F luoroohenol2 ,. 4 , S-T-rihromooh.en.ol

1 _1 R

11 01

1 0100

* 000

* 0001

Ir 1100111

* 111

* 1000

010210

RF

.803

.624

.559

.613

.200

.087

.180

.367

.209

.292

.203

.962

.966

.330

.171

.319

.738

.426

.283

.142

.086

.743

.224

.038

.074

.810

.636

.554

.440

.395

.975

.009

.380

.458

11RR1 --1 1! 0! 1I 01 11 o1 0* 01 oi o* 01 01 01 1* 11 11 oI 01 11 11 1* 1l oI 0* 01 o1 01 01..\ oI 11 01 11 1I 0

F50

.634

.572

.452

.608

.193

.170

.215

.343*

.165

.185

.178*

.924

.956

.354

.090*

.272

.789

.472

.097

.062

.123

.780*

.977

.925

.921*

.993

.877

.959

.370

.329

.861

.940

.294

.281

%D..«»

636Ca

(95^ 1. —19

r 520

C36* 12

411

* 6' 3610146

• 3* 1

2010

* -142.222.C.Z3

154

1136

.6

.3,8.8

.01

.1*

.8

.5*,0.0.7.8*.5.8.7.4.9.3.8*.1.8.2*6~ NHfj,

.2,1

.7

.6

.6

.4-JU^


CJf 02

FORM VII SV-2 RDOn6f;ii9 1/87 Rev.

7BSEMI VOLATILE CONTINUING CALIBRATION CHECK 00050 G


ab Code: YORK Case No.: 12512 SA5 No.: SDG No.: C3Q02

nstrument ID: C . Calibration Date: 09/17/89 Time: 20:54 •

ab File ID: >C4594 Init. Calib. Date(s): 09/17/89 09/17/89

in RRF50 for's?CC(*) » 0.050 Max %D for CCC(*J - 25.0%

COMPOUND ! RRF 1RRF50

Phenol ___________________ * 1.319* 1.206* 8.5* 58LK71bis( 2-Chloroe.hyl ) ether ___ I 1.1511 1.1842-Chlorophenol ___________ I 1.236! 1.1691 . 3-Dichlorobenzene _______ ! 1.417! 1.4701 , 4-Dichlorobenzene _______ * 1.438* 1.467*Benzyl alcohol ____________ 1 0.5251 0.4041,2-Dichlorobenzene _______ I 1.375! 1.4382 -Me thy 1 pher.o 1 ____________ i 1.1471 1.116bis( 2-Chloroisopropyl ) ether 1 1.6361 1.6714 -Methyl phenol ___________ \ 1.0371 0.966N-Ni troso-di-n-?rooylamine_* 0.916* 0.900*

1 Hexachl oroethane _________ 1 0.5311 0.611Nitrobenzene ______________ I 0.3241 0.321Isophorone _______________ I 0.6911 0.7102-Ni trophenol _____________ * 0.198* 0.193*2,4-Dimethylphenol ___________ I 0.4031 0.382!Benzoic acid _____________ 1 0.237! 0.1931bis(2-Chlorcethoxy)methane__! 0.3751 0.39212 , 4-Dichlorophenol ____ ____* 0.343* 0.337*1 ,2 , 4-Trichioro benzene ____ | 0.3571 0.3511Naphthalene _______________ \ 0.867! 0.99114-Chloroaniline __________ I 0.2861 0.2991Hexachlorobutadiene _______ * 0.229* 0.227*4-Chioro-3-methylphenol ___ * 0.376* 0.365*

1 2-Methylnaphthalene _______ I 0.661! 0.6451I Hexachlorocycloper.tadiene _ * 0.325* 0.316*I 2 . 4 . 6-Trichlorophenol • * 0.516* 0.473*i 2, 4,5-Trichlorophenol _____ I 0.617! 0.6242 -Ch i oronaphtha 1 ene2-Ni troani 1 ineDimethylphthalate __Acenaphthylene2 , 6 -Dinitro toluene3-Ni troani 1 ine

1.2061 1.3100.4021 0.4431.7191 2.0011.8091 2.1480.3931 0.4710.278! 0.356

Acenaphthene_________________* 1.354* 1.518*2,4-Dinitrophenol_________# 0.198* 0.147*4-Ni trophenoi____________* 0.216* 0.222*

FORM VII SV-1 1/87 Rev

7CSSMIVOLATILE CONTINUING CALIBRATION CHECK

OOG50iab Name: YORK LA3S/CT Contract: 63-W8-0021

dfecode: YORK Case No.: 12512 SAS No.: SDG No.: C3Q02

nstrumer.t ID: C Calibration Date: 09/17/39 Time: 20:54 •

ab File ID: >C4594 Ir.it. Calib. Date(s): 09/17/89 09/17/89

in RRF50 for'SPCCC*} « 0.050 Max %D for CCCl*) - 25.0%

I —— I 1 ICOMPOUND I RRF IRRF50 | %D I

,.-...,.,.._.........._....|.,,...I......|......ID i b er.zo f ur an_____________ 12 , 4-Dini trotoluene________!D i e thy 1 phtha 1 a t e__________ 14-Chlorophenyl-phenylether_!Fluorene_________________I4-Ni troani1ine4,6-Dinitro-2-methylphenol_|N-Mitrosociphenylamine (1)_*4-S romopheny1-pheny1 ether_ IHexachl orobenzene________!Pentachloropheno 1________*Pher.ar.threr.e___________Anthracene____________Di-n-butyIphthalate______Fluoranthene____________Pvrene_________________Butylbenzylphthalate__3,3'-Dichlorobenzidine.Ber.zo ( a } anthracene____Chrvsene____________bis(2-Ethylhexyl)phthalate_D i-n-oc ty1phtha1a t e_______Benzo(b j fluoranthene______Benzo(k)fluoranthene______Benzo (a) pyrene.Inceno(1,2,3-cd)pyrene.D i benzo(a,h)anthracene.Senzo(g,h,i)perylene

Ni trobenzen,e-d5_2-Fluorobiphenyl.Terpheny1-dl4__Pher.o 1 -dS______2-Fluorophenol_____2,4,6-Tribromophenol.

1.4801.2181.5481.1720.427



000017ab Name: YORK LA3S/CT Contract: 63-W8-0021 --..

afa Code: YORK Case No.: 12512 SAS No.: SDG No.: CBQ02

020304CS0607;os:091C1 t

12!131415

20

232412526127|281291301.

E?A SISAMPLE NO. (N3Z)*

S3LK31 79C3Q09MS 94C3Q09MSD 84C3Q09 72C3Q17 83C3Q02 73C3Q04 76C3Q05 35C3Q20 85C3QOO 75C3Q19 71SBLK83 69C3Q01 91C3Q06 102C3QC8 83C3Q12 43C3Q13 85C3Q14 85S3LK32 69C3Q10 47C3Q11 72C3Q03 66C3Q1S 63C3Q07 72CSQ16 65

S2(F3P)#

80143*131*80131*137*132*141*146*130*123*76129*140*134*74127*132*76537776708175

S3(T?H)#

11458517650525640S344529277778150348594•6995981009491

S4(PHL)#

24292324332731262929273033333230293029312727252728

1

S5(2FP)*

40473743494349434545464543504545434444464143394243

S3(TBP)*

547350434349 |48 |424346475472726769636457585353535257

1

OTHER TOTOUT

0110111111l'01110110

°M<f0*000

QC LIMITSSI (NBZ) Nitrobenzene-dS (35-114)S2 (F3P) 2-Fluorobiphenyl (43-116)S3 (TPH) Terphenyl-dl4 (33-141)S4 (PHL) Phenol-d5 (10-94)S5 (2F?) 2-Fluorophenol (21-100)S6 (TB?) 2,4,6-Tribromophenol (10-123)

# Column to be used to flag recovery values* Values outside of contract required QC limitsD Surrogates diluted out

age 1 of 1FORM II SV-1

ab Name: YORK LASS/CT Contract: 63-W8-0021


x Spike - EPA Sample No.: C3Q09

COMPOUND,,.---.,.,--.».».-»-.-.-Phenol2 -Ch. 1 oronher.o 11 , 4-Dichlorobenzene ___N-Mitroso-di-n-prop . ( 1 )1,2 ,4-Trichlorobenzene_4 -Ch i or o-3 -methyl phenolAcer.achthene „ . „4-Mi troohenol2 , 4-Dini trot o luer.e ____Pentach lorocheno 1 _. „ ..„.„_,.Pyrsne

SPIKEADDED(ug/L)

200.000200.000100.000100.000100.000200.000100.000200.000100.000200.000100.000

SAMPLE'CONCENTRATION

(ug/L)

0.0000.0000.0000.0000.0000.0000.0000.0000.0000.0000.000

MSCONCENTRATION

(ug/L)

78.000180.00082.00082.00093.000200.00088.00075.000110.000150.00076.000

MS I QC I*. I LIMITS |

REC #1 REC. I

39 112- 89190 [27-123!82 136- 97!82 141-116193 139- 981100*123- 97]38 146-118137 110- 801109*124- 96175 19-103 176 126-1271

I 1

11

COMPOUND I».« --.-_--__.»_..--_-:. |

j Keno 1 I" -Ch 1 oropherio 1 _„_, ... , 11 ,4-Dichlorobenzene ___ IN-Mi troso-di-n-prop .(1)11,2, 4-Trichlorobenzene_!4-Chloro-3-methylphenol 1Acer.a=hthene 14-Mi trophenol , 12,4-Dinitrotoluene 1Pentachlorooher.ol 1Pyrene 1

1

SPIKEADDED(ug/L).----._.-200.000200.000100.000100.000100.000200.000100.000200.000100.000200.000100.000

MSD 1CONCENTRATION!

(ug/L) 1

63140848182150334311011079

.0001

.000!

.0001

.000!

.0001

.0001

.0001

.0001

.0001

.0001

.00011

MSD%REC #

3170848182758321109*5579

%RPD #

232521

13296

55*0314

QCRPD

424028382842

. 315038SO31

1LIMITS 1

1 REC. 1.(......

112- 89[27-1231 36- 971 41-116139- 98123- 97146-118110- 80124- 9619-103126-1271

(1) N-Nitroso—di-n-propylamine

Column to be used to flag recovery and RPD values with an asteriskValues outside of QC limits

PD: 1 out of 11 outside limitspike Recovery: 3 out of 22 outside limits

OMMENTS:

FORM III SV-1 1/87 Rev.

AR30S6i*7

so C00718PESTICIDE EVALUATION STANDARDS SUMMARY ~

.ab Name: YORK LA8S/CT 'Contract: 63-W8-0021

.ab Code: YORK Case No.: 12512 SAS No.: _________ SDG No.: .C3Q02

Instrument ID: GC4A GO Column ID: 2250/2401

>ates of Analyses: 09/01/39 to 09/01/89

Evaluation Check for Linearity

PESTICIDE •

AldrinEndrin4,4'-DDTDBC

_

' CALIBRATIONFACTOR

EVAL MIX A

25305500143134201034233616651950

CALIBRATIONFACTOR

EVAL MIX B

26084650151810901201976816230680

CALIBRATIONFACTOREVAL MIX C

23664070147673551298863015534800

%RSD J«/= !10.0%)!«--»-»«•-•«.. 1

4.9|

i

(1) If > 10.0% RSD, plot a standard curve and determine the ngfor each sample in that set from the curve.

Evaluation Check for 4,4'-DDT/Endrin Breakdown(percent breakdown expressed as total degradation)

01!02!03!04J05!06!07!08,'09}10!ll!12!13!14!

INITIALEVAL MIX BEVAL MIX BEVAL MIX 8EVAL MIX 8EVAL MIX BEVAL MIX BEVAL MIX 8EVAL MIX BEVAL MIX BEVAL MIX 8EVAL MIX BEVAL MIX BEVAL MIX 8EVAL MIX B

DATEANALYZED

09/01/8909/01/89

TIMEANALYZED

08:0218:19

ENDRIN

0.00.0

4,4'-DDT

7.411.3

COMBINED(2)

-

,

(2) See Form instructions.

FORM VIII PEST-1 nn 8/87 Rev.AR3066148

000720

soPESTICIDE EVALUATION STANDARDS SUMMARY

.ab Name: YORK LA8S/CT Contract: 68-W3-0021

.ab Code: YORK Case No.: 12512 SAS No.: _____ SDG No.: C8Q02•

Instrument ID: GC4A GO Column ID: 225O/2401

>ates of Analyses: 09/06/89 to 09/07/89

Evaluation Check for Linearity

PESTICIDE

AldrinEndrin4,4'-DDTD8C

CALIBRATIONFACTOR

EVAL MIX A

296542SO16355330112027841S660770

CALIBRATIONFACTOR

EVAL MIX 8

28950340165022701363305218390750

CALIBRATIONFACTOREVAL MIX C

28360685177704971593662017490270

%RSD iC</= !io.o%) j

2.2!4.6!

C17.4J,3.4!

i

(1)

(1) If > 10.0% RSD, plot a standard curve and determine the ngfor each sample in that set from the curve.

Evaluation Check for 4,4'-DDT/Endrin Breakdown(percent breakdown expressed as total degradation)

01!02!03!04J05!06!07!os;09J10!li!12!13!14!

INITIALEVAL MIX BEVAL MIX 8EVAL MIX BEVAL MIX 8EVAL MIX BEVAL MIX BEVAL MIX BEVAL MIX BEVAL MIX BEVAL MIX 8EVAL MIX BEVAL MIX BEVAL MIX BEVAL MIX 8

DATEANALYZED

09/06/8909/06/8909/07/8909/07/89

TIMEANALYZED

07:1616:1402:4710:28

ENDRIN

0.00.00.00.0

-

4, 4 '-DOT. •

6.510.06.712.0

COMBINED(2)

(2) See Form instructions.

8/87 Rev.

9PESTICIDE/PCS STANDARDS SUMMARY

ab Name: YCRK LA3S/CT Ccntract: 63-WS-002I

ab C-rda: YORK Case No.: 12512 SAS No.: ______ EDG Mo.: C2CGZ

ns-rumen. ID: GC4£ GC 'Column ID: 2250/2401

CC.-PCL'NO

- * — - > - _ 2 •_!,••»-1__'. id _/. .'_•

beta-EHC•ielt.a-£HCcami7ia-cHCHeotachior-* "* *4 *- - —•r-t __, \_. . M i i

He_t. aooxiceEn<_c £-.' _ "<si". IDieloJrin4.4--C.CEEr.drinEndcsulfan II4, 4 '-000=,r.co. sulrjita4. -S. * -.~;.~-T

Me thoxychicrEiioli'in Xs-cr.a^. Chlorcfane'_. ChlcrdaneTexas hensAi-oclor-1016Aroclor-1221Arocior-1232.*.«*-> * __ • *^ 4 ^-t i w;_ _C " ~ __.4_Arcclor-124SArcclcr-i254•-t i" c _ 1 G r - 1 26 0

DA7SCS) C? FROM; CS/29/37ANALYSIS TC: 03/29/29TIDE'S; C" FROM: 17:40ANALYSIS TO: 21:27

R7

.2 . - 9W • *•"• >v

3.7.33. OS-_•.'_•

-.47i .-i?£.099.76— '—.'—'1 1 . 76t * /* »13 . 3621 . 71

27.0?27 . 337 . 7-~* • «•> w^ * '~.* * w •_.

3.642.303.603.643.6311.1512.43

RTWINDOW

-?-:M : TO2.--w • w *T /•* "•w • ?w

3.053.70,« 44

W • *™ '*

S.Cs7.71

* • •» •i.- . : -\ " or13.2321.61

25 . £3— «*— > • "C_. * . JL s— -

7.697. OS9.593 .592.273.573.533.6011 . 1312.*31

*^ C t-_. . 5^^ * ™f .*A . 033.113.76- SO6. SiS.12/_ C '

G O"1* • W^ •_>

1 i . S i• .< . -•_•-• . —«-•13.44*•* » c i«_.-»• / <k

li 1029 . 35TC 4,3•• •' * ~~ *!.»

7.797.139.653.69*-» --»"->-t. *~ w w

3.63C.7C3 . 6611.1712 . 55

CALIsSATIONFACTOR

66291002520930•496007S5=167003=3=7756030 73i * * s .*^ ! ; **

371347033535003623900"* "" T 4 "T T .-*,%.*<».««_'•*' <M V

6127060471739027994773332527246765354«52420372666052349501336010£3"'30542433420-779177293073352734594632S63576

DATE Cr ANALYSIS OS/31/S?TIME OF ANALYSIS 02:29EPA SAMPLE NO.C STANDARD) IND2

RT

2.433.413.96

3 . 93« T T '.__./!,

• -> —r><.it — * . W W

21.62

27. 177.717.09

CALIBRATIONFACTOR

722637527543503356330

63344303730420

3430655-_*_. c w i-4w

6-wt rr • a T1 *s--w **T*wO

. '64697955379035

CNTV/iS

YYY

,

1 1 1

V

Y

YY

YYY

.» .—i-

o 99.312.0

i i

1Z.5_s* _, — "*^ __jj| Lx

12.6

1Z._11. C« ^JL • • •-/

nder QN" Y/N: enter Y if auanti ta tion was psrformsd, N if not performed.0 must be less zr.aii cr ecu»l tc 15.0-\ for cuancitation, and less thanr ec_al to 2O.C-. for c-_nf ir.T.ation .

ote: Ds termini ng that no ccmc-cunds we.-s found above the CRCL is a form o*uantitAtion. _.nd t:*ie.'«* _re at least ons column must meet the 15.0?i critsrii,

or rr.ul iiccmccnent analyses, the sin<gle largest pea!-; that isf ths comconent Ehculd --3 uss-d to establish retention time and %D. ,dentificaticn of such analytss is based primarily on pattern reccgnifci

age 2 of 5FCP.M ix PEST A R 3 0 6 6 5 0 5/37 fia"

i

9PESTICIDE/PC3 STANDARDS SUMMARY

000737.ab Name: YORK LASS/CT Contract: 68-W8-0021

^fe Code: YORK Case No.: 12512 SAS No.: ______ SDG No.: CSG02

Cnstrument ID: GC2 GO Column ID: OV-1

1

COMPOUND

:alpha-3HC'beta-3HC:delta-8HCgamma-3HC: HeptachlorAldrin!Heot. epoxideEndosulfan IIDieldrin'4,4'-DDE! Endrin; Endosulfan II

Pfdo. sulfata! 4, 4 '-DOTiMethoxychlor[Endrin ketone,'a. Chlordane!g. ChlordaneJToxaphene[Aroclor-1016!Aroclor-1221! Aroclor-1232: Aroclor-1242:Aroclor-1248Aroclor-1254: Aroclor-1260

! DATE(S) OF FROM: 09/01/89 ! DATE OF ANALYSIS '09/02/89ANALYSIS TO: 09/02/89 | TIME OF ANALYSIS 16:27TIME(S) OF FROM: 22:21 ! EPA SAMPLE NO.ANALYSIS TO: 00:36 | (STANDARD) IND8

ii p^j i t

RT ! WINDOW ! CALIBRATION! RT! FROM ! TO ! FACTOR }

2.16J 2.13! 2.19J 4412962! 2.182.36! 2.33J 2.39J 1132955! 2.372.68J 2.65! 2.71! 2332537! 2.702.57! 2.54! 2.60! 251370O!4.20! 4.14! 4.26! 2530012!5.24! 5.13! 5.30! 2654975!6.46! 6.38! 6.54! 24463O5 i8.10! 8.01! 8.19! 2386325!9.53! 9.39! 9.67! 2997520!9.60! 9.43! 9.72J 2370080 J 9.6610.66! 10.51! 10.81! 2380930! 10.7210.93! 10.76! 11.10! 2035710!12.24J 12.07! 12.41! 1764890J 12.3214.24,' 14.04! 14.44J 970218 J 14.3316.16! 15.95! 16.37! 1410047J24.53! 24.20! 24.86! 681009}18.40! 18.14! -18.66! 2025832! 18.518.28! 8.16! 8.4O! 2429952!7.45! 7. 34J 7.56! 2342417! 7.49

3.68! 3.63! 3.73! 325242!

! I ! !3.68! 3.65! 3.71! 294274 }

i i i ii i i i

14.16! 13.99! 14.33! 1288419!i i i i

CALIBRATIONFACTOR

335826211305902549O37

24705452509695

19665901427153

2427167

2533032

QNTY/N

NN

——

NN

NN

N

N

———

%D

S 7. ••• V.

<33.9j4.49.3

4725.4

11. 4^(27-i

19.8

8.1

Jnder GNT Y/N: enter Y if quantitation was performed, N if not performed.jD must be less than or equal to 15.O% for quantitation, and less thanjr equal.to 2O.O% for confirmation.

lota: Determining that no compounds were found above the CRQL is a form ofquantitation, and therefore at least one column must meet the 15.0% criteria.

•"or multicomponent analytes, the single largest peak that is characteristiccomponent should be used to establish retention time and %D.

iification of such analytes is based primarily on pattern recognition

jage 2 of 5FORM IX PEST . 8/87 Rev.

flR3066

9PESTICIDE/PCS STANDARDS SUMMARY

000733.ab Name: YORK LA8S/CT Contract: 63-W8-OO21

.ab Coda: YORK Case No.: 12512 SAS No.: ______ SOG No.: C8G02

Instrument ID: GC2 GC Column ID: OV-1

COMPOUND

alpha-3HCbeta-BHCdelta-BHCgamma-3HCHeptachlorAldrinHeot. eooxideEndcsulfan IDieldrin4, 4 '-DDEEndrinEndcsulfan II4.4'-DDDEndo. sulfate4, 4 '-DOTMethoxychlorEndrin ketone[a. ChlordaneJg. Chlordane! ToxaphenejAroclor-1016!Aroclor-1221!Aroclor-1232Arocloi — 1242Aroclor-1248Aroclor-1254Aroclor-1260

DATE(S) OF FROM: 09/01/89 ! DATE OF ANALYSIS 09/02/89ANALYSIS TO: 09/02/89 } TIME OF ANALYSIS 17:12TIME(S) OF FROM: 22:21 ! EPA SAMPLE NO.ANALYSIS TO: 00:36 j (STANDARD) INDA

ii j^— • i i

RT ! WINDOW [CALIBRATION! RT! FROM ! TO ', FACTOR ',

2.16J 2.13! 2.19! 4412962!2.36J 2.33J 2.39! 1132955!2.63! 2.65! 2.71! 2332537!2.57! 2.54[ 2.60J 2513700! 2.594.20J 4.14J 4.26! 2530012! 4.235.24! 5.18! 5.30! 2654975! 5.236.46! 6.33! 6.54J 2446305! 6.508.10! 8.01! 8.19J 2336325! 8.169.53! 9.39! 9.67! 2997520! 9.599.60! 9.48! 9.72! 2370080!10.66! 10.51! 10.81! 2380930!10.93! 10.76! 11.10! 2035710', 11.0112.24! 12.07! 12.41! 1764890!14.24! 14.04! 14.44! 970218!16.16J 15.95! 16.37J 1410047! 16-J27.24.53J 24.20! 24.86! 681009 ! C27. 70,18.40! 18.14! 18.66! 2025832!8.28! 8.16! 8.40! 2429952!7.45! 7.34! 7.56! 2342417!

i i i i3.68! 3.63! 3.73! 325242!

i i i i————— i ————— i ————— i ti i i i

3.68! 3.65! 3.71! 294274!i i i ii i i i

14.16! 13.99! 14.33! 1288419!i i i t

CALIBRATIONFACTOR

315612533220873048700234364528092453099775

2602865

1767647> 1049470

GNTY/Nsz_

NNNNNN

N

NN

——

%D

3132ffJ. ** • w

16.217.73.4

,—»• —— *-\ M-C25.A•CsTTiv-- ——

Jnder GNT Y/N: enter Y if quantitation was performed, N if not performed.;D must be less than or equal to 15.0% for quantitation, and lass thanjr equal to 2O.O% for confirmation.

Iota: Determining that no compounds were found above the CRGL is a form ofluantitation, and therefore at least one column must meet the 15.0% criteria.

"or multiccmponent analytes, the single largest peak that is characteristic>f the component should be used to establish retention time and %D. ^^'dentification of such analytas is based primarily on pattern recognitiorflB

•age 3 of 5FORM IX PEST 8/87 Rev

flR30S652

2£WATER PESTICIDE SURROGATE RECOVERY DAr/*-"

.ab Name: YORK LA3S/C7 Contract: 6S-W8-0021

Code: YORK Case No.: 12512 SAS No.: ______ SOG No.: C8G02

! EPA! SAMPLE NO.

01IP3LK3902 ! P3LK4003IC3SCO04JC3C0105!C2G02C6IC3C0307IC3C04os:c3cos09JC3CC610IC3G07li!C3G0312IC3G0913|C3C09MS14IC3CG9MSD151C3G1016!C3G1117JC3G121SJC3G1319JC3G1420IC3G1521IC3G1622IC3G1723IC3C19241CSG2025!26!27!23!29!30!

SICDBC)*

1019493969593 j

( 226 **v-=_—--*

949292989399839295931009494

• 959289

OTHER

, :

^

ADVISORY. ' ' CO LIMITS

Si (D8C) = Dibutylchlcrendata (24-154)

* Column used to flag recovery values

* Values outside of CO limits

D Surrccatas diluted out

>age 1 of 1FORM II PEST-1 1/S7 Ra

&R3QS653

la c.-'rt. _x-vur.ue.SEMI VOLATILE ORGANICS ANALYSIS DATA SHEET .___________

II SBLK81

ab Name: YORK LASS/CT Contract: 68-W8-0021 I_______V/ "O \J X* -.

ab Code: YORK Case No.: 12512 SAS No.: SDG No.: CBQ02 ^^

atrix: (soil/water) WATER Lab Sample ID: 08/23-B02 ^^


evel: (low/medj LOW Date Received:


xtraction: (SepF/Cont/Soncj SEPF Date Analyzed: 09/17/89


CONCENTRATION UNITS:CA5 NO. COMPOUND (ug/L or ug/Kg) UG/L Q

iI 108-95-2 - ——i 111-44-4 — —[ 95-57-3 —————I 541-73-1 ———I 106-46-7 ————I 100-51-6 ———1 95-50-1 —————I 95-48-7 —————I 108-60-1 ————i 106-44-5 ————,621-64-7 ————67-72-1 —————98-95-3 —————78-59-1 —————88-75-5 —————105-67-9 ————65-85-0 —————1*1 _Q 1—1

120-83-2 ———1 •'/ r\ a •? t91-20-3 —————106-47-8 ———87-68-3 —————

91-57-6 —————77 — 4.7 4. —oci f\a oqe o«_4. ____91 ^ O "7

83-74-4 —————131-11-3 ————208-96-8 ————606-20-2 ———

————— PVISMI

—— -2-ChIoroohenol— — -1 f 3-Dichlorobenzene—— -1 r 4-Dichlorobenzene— — Bensvl alcohol——— 1 , 2-Dichlorobenzene———— 2 -Methyl phenol . „——— bis(2-Chloroisopropyl )ether_——— 4-Methv Ipheno 1——— N-Ni troso-di-n-propy lamine _——— Hexachloroenhane, „,——— Nitrobenzene——— Tsonhorone———— 2-Ni trophenol ,,,,,,.,——— 2 . 4-Dimethy Ipheno 1——— Benzo ic acid, „,.„,„.._,——— bis ( 2-Chloroethoxy )methane _——— 2 e 4-Dichlorophenol ,„_. , „,„.,,„„---- i f 2 f 4-Trichlorcbenzene——— Naphthalene——— 4-Chloroani 1 ine——— Hexachlorobutadiene——— 4-Chloro-3-methylphenol——— 2-Methylnaphthalene , „',,.——— Hexachlorocyclopentadiene __——— 2 r 4 r 6-Tr ichlorophenol——— 2 f 4 r 5 -Tr ichlorophenol——— 2-Chloronaohthalene , ,,— —— 2-Ni troani 1 ine———— Dimethy 1 phfckala te..,_———— Acenas'nthy 1 ene——— 2 , 6-Dini t»-otolu.ene

110.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.000! U10.000! U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U50.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U50.0001 U10.0001 U50.000! U10.0001 U10.000! U-10.0001 U

1

FOEIM I SV-1 1/8

m

•7 Rev.

AR30665U

1C E?A SAW-'-..; NO,ScMIVOLATILE ORGANICS ANALYSIS DATA SHEET

! iI S3LK81 }

ab Name: YORK LA3S/CT Contract: 68-W8-0021 ! _________ n Q P. £>T T•_/ w v •-_> —» •

e: YORK Case No.: 12512 SAS No.: SDG No.: CBQ02

(soil/water) WATER Lab Sample ID: 08/23-B02


*vel: (low/med) LOW Date Received:


•<traction: (SepF/Cont/Sonc) SEPF Date Analyzed: 09/17/89


CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg ) UG/L Q

99-09-2 ——————— 3-Nitroaniline____________I 50.000! U83-32-9———————Acer.aphth.ene_____________I 10.0001 U51-28-5 ———————— 2, 4-Dini trophenol_________I 50.0001 U100-02-7 ——————— 4-Nitrochenol______________I 50.0001 U132-64-9———————Di benzo fur an______________121-14-2 ——————— 2 , 4-Dinitrotoluer.e_________84-66-2————————Diethylph thai ate___________7005-72-3 —————— 4-Chlorophenyl-phenylether_86-73-7————————Fluorene__________________100-01-6——————4-Nitroani 1 ine____________534-52-1-—————4,6-Dinitro-2-methylphenol_86-30-6————————N-Nitrosodiphenylamine (1)_101-55-3 ——————— 4-Bromophenyl-phenylether__118-74-1———————Hexachl orobenzene_________87-86-5———————Pentachlorophenol_________85-01-8———————Ph.enanth.rene_____________120-12-7———————Anthracene_______________________84-74-2————————Di-n-buty Iphtha late________206-44-0 — ————F luoranthene______________129-00-0———————Pyrene____________________85-68-7———————Butylbenzy Iphtha late______91-94-1———————3,3'-Dichlorcbenzidine_____56-55-3———————Benzo (a) anthracene________218-01-9———————Chrysene__________________117-81-7———————bis(2-Ethylhexyl ) phtha late_117-84-0———————Di-n-octylphthalate________205-99-2———————Benzo(b)f luoranthene_______207-08-9 ——————Benzo(k ) f luoranthene_______50-32-8————————Benzo (a)pyrene_____________193-39-5 ——————— Indeno( 1,2 ,3-cd) pyrene_____53-70-3———————D i benzo( a, h) anthracene_____

I 191-24-2———————Benzo(g,h, i )perylene.

10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U50.000! U50.000! U10.0001 U10.000! U10.0001 U50.0001 U10.0001 U10.0001 U10.000! U10.0001 U10.0001 U10.000! U20.0001 U10.0001 U10.0001 U6.0001 J

io.oooi u10.000! U10.0001 U10.0001 U10.0001 U10.0001 U10.000! U -



fiR306655 .

IF E?A SAMPLE NO.SSMIVOLATILc CRGANICS ANALYSIS DATA SHEET _________._______

I 1I S3LK31 |

afa Name: YORK LA3S/CT Contract: 68-W8-0021 I__________ IrrtRTgiiib Code: YORK Case No.: 12512 SAS No.: SDG No.: C3Q02~ jjjL

atrix: (soil/water) WATER Lab Sample ID: 08/23-B02


svel: (low/med) LOW Date Received:




^ CONCENTRATION UNITS:dumber TICs found: <_,/ (ug/L or ug/Kg) UG/L

CAS NUMBER

01.02.03.04.05.06.07.08.09.10.11.12.13.

! 14.I 15.I 16.I 17.l 18.19.20.21.22.23.24.25.

' 26.27.28.29.30.

COMPOUND NAME

'

RT EST. CONC Q•

____ i


AR3Q6656


| S3LK82 Iab Name: YORK LABS/CT Contract: 68-W8-0021 I_______0 Q 0 S G'8

«Code: YORK Case No.: 12512 SAS No.: SDG No.: CBQ02

ix: (soil/water) WATER Lab Sample ID: 0824-B02




xtracticn: (Se?F/Cont/Sor.c) SEPF Date Analyzed: 09/11/89



I I108-95-2———————Phenol____________________I 10.0001 U

10.0001 U111-44-4———————bis(2-Chloroethyl) ether.95-57-8 ———————— 2-Chloroohenol________541-73-1 —————— 1, 3-Dichlorobenzene_______106-46-7 —————— 1, 4-Dichlorobenzene_______100-51-6——————Benzyl alcohol___________95-50-1 ——————— 1, 2-Dichlorobenzene_______95-48-7———————2-Methyl phenol___________108-60-1——————bis(2-Chloroisopropyl )ether_106-44-5 ——————— 4-Me thy 1 phenol____________621-64-7———————N-Nitroso-di-n-propy lamine_'67-72-1————————Hexachl oroe thane__________93-95-3————————Nitrobenzene______________78-59-1 ———————— Isoohorone________________88-75-5 ———————— 2-Ni trophenol_____________105-67-9 ——————— 2,4-Dimethylphenol_________65-85-0————————Benzoic acid______________111-91-1——————bis(2-Chloroethoxy)methane_120-83-2 ——————— 2 , 4-Dichlorophenol_________120-82-1 ——————— 1, 2,4-Trichlorobenzene_____91-20-3————————Naphthalene_______________106-47-8———————4-Chloroani 1 ine______________

i 87-68-3————————Hexachlorobutadiene.59-50-7 ———————— 4-Chl oro-3-me thy Ipheno 1__91-57-6 ———————— 2-Methyl naphtha Iene_____77-47-4———————Hexachl orocyclopentadi ene.88-06-2 ———————— 2 ,4,6-Trichlorophenol____95-95-4 ———————— 2, 4, 5-Tr ichlorophenol____91-58-7 ——————— 2-Chloronaphthalene_____88-74-4 ———————— 2-Nitroani 1 ine__________131-11-3——————Dime thy Iphtha late.__________208-96-8———————Acenaph thy Iene__________606-20-2 ——————— 2, 6-Dinitrotoluene.________

0.400! J10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.000! U10.000! U10.0001 U10.0001 U10.0001 U50.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.000! U10.0001 U10.0001 U10.0001 U10.0001 U50.0001 U10.0001 U50.0001 U0.7001 J10.0001 u10.0001 u


ftR306657

SEMIVCLATILS CRGANICS ANALYSIS DATA SHEET

I SBLK32ab Name: YORK LA3S/CT Contract: 68-W8-0021 I

ab Code: YORK Case No.: 12512 SAS No.: SDG No.: CBQO

atrix: (soil/water) WATER Lab Sample ID: 0824-B02







99-09-2 ————— •83-32-9 ————— -51-28-5 ————— -100-02-7 ——— -132-64-9 ———— -121-14-2 ——— -84-66-2 ————— •7005-72 3 — -86-73-7 ————— -100-01-6 ———— •5-5 4,_ •) 1 ___ .

86-30-6 ————— •101-55-3 ——— -118-74-1 ———— -87-86-5 ————— -85-01-8 ————— -

——— 3-Ni troani 1 ine——— Acenachthene——— 2 f 4-Dini trophenol ,, ,.,——— 4-Ni trcnhenol——— Dibenzof u-an——— 2 . 4-Dini tro toluene——— Diethylphthalate

——— Fluorene——— 4-Ni troani 1 ine——— 4 , 6-Dini tro-2-methylphenol——— N-Ni trosodipheny lamine ( 1 ) _——— 4 -Bromophenyl -phenylether __——— Hexachl or obenz ene- —— Pentachloroohenol- ——— ?h^nan.th.T-ene

120-12-7 ——————— Anthracene84-74-2 ————— -206-44-0 ———— -129-00-0 ———— •85-68-7 ————— -SI —Q4. 1 _ — — .

218-01-9 ———— •117 fl 1 *7

117-84-0 ———— -205-99-2 ———— -207-08-9 ———— •50-32-8 ————— •i q o o q c __ _ .

——— Di-n-butylohthalate——— F luoranthene——— Pyrene——— Butyl benzyl phtha late——— 3 . 3 '-Dich lor obenz id ine——— Benzo ( a ) anthracene——— Chrysene——— bis(2-Ethylhexyl )phthalate _——— Di-n-octylphthalate——— Benzo (b) f luoranthene „,,., ..——— Benzo ( k ) f luoranthene——— Benzo ( a ) ny-ene ,——— Tndeno ( 1 t 2 f 3-cd ) pyrene

191-24-2 —————— Benzofa.h. i loerylene

150.0001 U10.0001 U50.0001 U50.0001 U10.0001 U10.0001 U0.4001 J10.0001 U10.0001 U50.0001 U50.0001 U10.0001 U10.000! U10.0001 U50.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U

1 JZ-rU-T. | J<4.20.0001 U10.0001 u10.0001 U6.0001 J10.0001 U10.0001 U10.0001 U10.0001 u10.0001 U10.0001 U10.0001 u.

1(1) - Cannot be separated from Diphenylamine


AR306658

ScMI VOLATILE ORGANICS ANALYSIS DATA SHEET ________________I I| SBLK82 1

ab Name: YORK LABS/CT Contract: 6S-W8-0021 I______________I

«Code: YORK Case No.: 12512 SAS No.: SDG No.: CBQ02

ix: (soil/water) WATER Lab Sample ID: 0824-BO-}Q081G






CONCENTRATION UNITS:lumber TICs found : / (ug/L or ug/Kg) UG/L

CAS NUMBER

01. M-2.C1.lH02.-03.04.05.

09.10.11.12.13.

. 14.15.16.17.18.19.20.21.22.23.24.25..26.27.28.29.30.._«_

1COMPOUND NAME

Vj\Nj5eCAW_:

RT

U,<hEST. CONC

1C

•Q

J

1-


AR3QS659


| S3LK83ab Name: YORK LA3S/CT Contract: 68-W8-0021 I

ab Code: YORK Case No.: 12512 ' SAS No.: SDG No.: CBQ02

atrix: (soil/water) WATER Lab Sample ID: 0825-B02


evel: (low/med) LOW Date Received:




CONCENTRATION UNITS:CA5 NO. COMPOUND (ug/L or ug/Kg) UG/L Q

108-95-2———————Phenol______________111-44-4——————bis (2-Chloroethyl) ether.95-57-8————————2-Chlorophenol____________541-73-1 ——————— 1, 3-Dichlorobenzene________

100-5 1-6-——————Benzyl alcohol_____________95-50-1 ——————— 1, 2-Dichlorobenzene_______95-43-7 ———————— 2-Methyl phenol____________108-60-1———————bis(2-Chloroisopropyl )ether_106-44-5 ——————— 4-Me thy 1 phenol____________621-64-7——————N-Nitroso-di-n-propy lamine_67-72-1————————Hexachl oroe thane__________98-95-3————————Nitrobenzene______________78-59-1 ———————— Isoohorone________________88-75-5 ———————— 2-Ni trophenol____________105-67-9 ——————— 2 , 4-Dimethy 1 phenol_______65-85-0————————Benzoic acid_____________________111-91-1——————bis(2-Chloroethoxy) methane.120-83-2 ——————— 2, 4-Dichlorophenol_______120-82-1 ——————— 1,2, 4-Trich lor obenz ene____91-20-3———————Naphthalene_____________106-47-8 ——————— 4-Chloroani 1 ine__________87-68-3———————Hexachlorobutadlene______59-50-7————————4-Chloro-3-me thy Ipheno 1___91-57-6————————2-Me thy Inaphtha Iene.77-47-4———————Hexachlorocyclopentadiene.88-06-2 ———————— 2 , 4 , 6-Trichlorophenol____95-95-4————————2 , 4 , 5-Trichlorophenol___91-58-7 ———————— 2 -Ch lor ©naphthalene_____88-74-4————————2-Ni troani 1 ine__________131-11-3———————Dimet-hylphthalate_______208-96-8———————Acenaphthy Iene__________606-20-2 ——————— 2 , 6-Dinitrotoluene______

10.0001 U10.0001 U0.4001 J10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.000! U10.0001 U10.000! U10.000! U10.0001 U10.0001 U10.0001 U10.0001 U50.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 u50.0001 U10.000! U50.0001 U10.0001 U10.0001 u10.0001 U


AR306660

SEMIVOLATILE CRGANICS ANALYSIS DATA SHEETII S3LK83 0005

ab Name: YORK LABS/CT Contract: 63-W8-0021 !______________I

»Code: YORK Case No.: 12512 SAS No.: SDG No.: CBQ02

ix: (soil/water) WATER Lab Sample ID: 0825-B02


evel: (low/med) LOW Date Received:•





99-09-2 ——————— 3-Nitroani 1 ine.83-32-9———————Acsnaohthene__51-28-5 ———————— 2 , 4-Dinitrophenol.100-02-7 ——————— 4-Ni trophenol___132-64-9———————Di benzo fur an______121-14-2 ——————— 2 ,4-Dinitrotoluene_______84-66-2————————Diethy Iphtha late_________7005-72-3 —————— 4-Ch 1 or ophenyl-phenylether.86-73-7———————Fluorene_______________100-01-6———————4-Nitroani line__________534-52-1——————4,6-Dinitro-2-me thy Ipheno 1.86-30-6————————N-Nitrosodiphenylamine (1).101-55-3——————4-3romophenyl-phenylether_118-74-1——————Hexachl or obenz ene________87-86-5———————Pentachlorophenol________

! 85-01-8———————Phenanthrene

i120-12-7———————Anthracene_______________________84-74-2————————Di-n-buty Iphtha late______206-44-0 ——————— F luoranthene_____________129-00-0———————Pyrene__________________85-63-7————————Butyl benzylphthalate_____91-94-1 ———————— 3,3'-Dichlorobenzidine___56-55-3————————Benzo (a) anthracene_______213-01-9———————Chrysene________________117-81-7———————bis(2-Ethylhexyl)phthalate.117-84-0———————Di-n-octylphthalate______205-99-2———————Benzo (b)f luoranthene_____207-08-9 ——————— Benzo(k) f luoranthene_____50-32-8———————Benzo (a) pyrene__________193-39-5 ——————— Indeno (1,2 t 3-cdl pyrene53-70-3————————D i benzo (a, h) anthracene___191-24-2———————Benzo(g,h/ i )perylene______

I50.0001 U10.0001 U50.0001 U50.0001 U10.0001 U10.0001 U10.0001 U10.000! U10.000! U50.0001 U50.0001 U10.0001 U10.0001 U10.0001 U50.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.000! U20.0001 U10.0001 U10.0001 U2.0001 J10.000! U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U10.0001 U



AR30666I

ac. .i YOU-.- __<c <jy.UAN.LU-5 AJNri—i!3i3 OATA an_.i_ _________________I I| S3LK83 |

ab Name: YORK LA3S/CT Contract: 68-W8-0021 I_________r ~ - -J.-.u V w "• "-1ab Code: YORK Case No.: 12512 SAS No.: SDG No.: C3Q02

atrix: (soil/water) WATER Lab Sample ID: 0825-302


evel: (low/med) LOW Date Received:


xtrac.ion: (SepF/Cont/Sonc) SEPF Date Analyzed: 09/11/89


CONCENTRATION UNITS:Number TICs found: 7- (ug/L or ug/Kg) UG/L

CAS NUMBER

01.02.03.04.05.06.07.oa.09.10.11.12.13.14.

1 15.! 16.I 17.! 18.1 19.20.21.22.23.24.25.26.27.28.29.30.

COMPOUND NAME

v/xocNOvN^ AL<$/v£uNK,\iOiA;N /i_.<rt,VE.

RT

'/.<*. !H

EST. CONC

S°\

,

Q

T\

ft


ftR3Q6662

ID EPA SAMPLE NO.PESTICIDE ORGANICS ANALYSIS DATA SHEET ______________.

PBLK39 J.ab Name: YORK LA8S/CT Contract: 68-W8-0021

Cede: YORK Case No.: 12512 SAS No.: _____ SDG No.:

•tatrix: (soil/water.) WATER Lab Sample ID: OS24-B03

Samole wt/vol: 1000. (g/mL) ML Lab File ID:

.evel: (low/med) LOW Date Received: _______

', Moisture: net dec. ____ dec. _____ Date Extracted: OS/24/S9

-rxtracticn: (SecF/Ccnt/Scnc) SEPF Date Analyzed: OS/30/89

3PC Cleanuo: (Y/N) N pH: Dilution Factor: 1

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L Or ug/Kg) UG/L Q

319-84-6 ——————— aloha-SHC_________319-SS-7- —— ——— beta-3HC___________319-S6-S —— ———— delta-BHC__________58-S9-9-------—gamma-SHC (Lindane),76-44-8———————Heotachlor__________309-00-2———————Aldrin____________1024-57-3—————Heptachlor epoxide959-98-8——————Endosulfan I_____60-57-1———————Dieldrin_________72-55-9————————4. 4'-DDE_________72-20-8 ———————— Endrin___________33213-65-9—————Endcsulfan II_____72-54-8 ————————— 4,4'-DDD________1031-07-8- ————— Endcsulfan sulfate50-29-3—————————4,4'-DDT__________72-43-5—--————Methoxychlor_____53494-70-5— ——— Endrin ketone_____5103-71-9—————a'loha-Chlordane__5103-74-2——--—camma-Chlordane__8001-35-2-—————Toxaohene________12674-11-2—————Aroclor-1016______11104-23-2—————Aroclor-1221_____11141-16-5 ————— Aroclor-1232_____53469-21-9—————Aroclor-1242______12672-29-6—————Aroclor-1248______11097-69-1—————Aroclor-1254_____11096-82-5—————Arcclor-1260______

o.osoiuo.osoiuo.osoiuo.osoiuo.osoiuo.osoiuo.osoiuO.OSOJU0.10JU0.10IU0.10|U0.10IU0.10|U0.10JU0.10JUO.SOIU0.10IUO.SOIUO.SOIU1.0JU

O.SOIUO.SOIU0.50 IUO.SOIUO.SOIUi.o |ul.OJU

FORM I PEST

AR30S663

ID EPA SAMPLE NO.PESTICIDE CRGANICS ANALYSIS DATA SHEET _______________:

.ab Name: YORK LA3S/CT Contract: 6S-W8-0021P8LK40

.ab Code: YORK Case No.: 12512 SAS No.: _____ SDG No.: C8G02

latrix: (soil/water) WATER Lab Sample ID: 0825-B01

:amole wt/vol: 1000. (g/mL) ML Lab File ID: ________

.evel: (low/med) LOW Date Received: ______

i Moisture: not dec. ____ dec. _____ Date Extracted: 08/25/89

Ixtraction: (SeoF/Ccnt/Scr.c) SEPF Date Analyzed: 09/01/89

•PC Cleanuo: (Y/N) N pH: Dilution Factor: 1

CONCENTRATION UNITS:CAS NO. COMPOUND x (ug/L or ug/Kg) UG/L Q

319-84-6 ——————— aloha-BHC_________319-85-7———————beta-3HC__________319-86-8——————delta-BHC_________58-89-9------—-gamma-BHC (Lindane).76-44-8——- ———— Heotachlor________309-00-2———————Aldrin____________1024-57-3-————Heotachlor epoxide,959-98-3———————Endcsulfan I_____60-57-1--—---—Dieldrin_________72-55-9—————————4, 4'-DDE__________72-20-8—— — —— -Endrin___________33213-65-9—————Endosulfan II____72-54-8—————————4.4'-DDD__________1031-07-8—— ——— Endosulfan sulfate.50-29-3—————————4,4'-DOT__________72-43-5 — ———— — Methoxychlor______53494-70-5—————Endrin ketone____5103-71-9—--——aloha-Chlordane___5103-74-2- — ——— gamma-Ohio rdane__8001-35-2--—-—Toxaohene________12674-11-2—————Aroclor-1016______11104-28-2—————Aroclor-1221_____11141-16-5—————Aroclor-1232_____53469-21-9—————Aroclor-1242______12672-29-6- ———— Arcclor-1248_____11097-69-1 ————— Aroclor-1254_____11096-82-5 ————— Aroclor-1260____

o.osoiuo.osoiuo.osoiuo.osoiu0.050 IUo.osoiuo.osoiuo.osoiuo.ioiuo.ioiu0.10JUo.ioiu0.10|UO.IO'.Uo.ioiuO.SOJU0.10JU0.50|U0.50|U

1.0IU0.50JU0.50|U0.50|U0.50|U0.50|U1.0|U1.0|U

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1C E?A SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS …O.SOJU O.SOJU 1.0JU 1.0JU FORM I PEST 1/87 Rev....

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