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2009 Table of Contents Product-Method List by Section
Method Latest Section A: Vegetable Oil Source Materials number
issue Cottonseed
Sampling Foreign Matter Moisture and Volatile Matter Oil Content
Protein Protein " Conversion Table for Nitrogen-Ammonia-Protein
Free FarryAcids Residual Lint Aflatoxins Aflatoxins, Confirmation
by TLC Aflatoxins in Corn and Peanut by TIC Aflatoxin Standards
(preparation) Aflatoxin Detection by PHRED
Peanuts (Grcundnurs) Sampling Moisture and Volatile Marter Oil
Content Protein Protein Free Fatty Acids Aflatoxins Aflatoxins
(affinity oolumn)
Also see Also see
Soybeans . Sampling Moisture and Volatile Mauer Oil Content
Protein Protein Free Fatty Acids
Tung Fruit Sampling Moisture and Volatile Matter Oil Content
(whole tung fruit) Physical Analysis (kernel content) Oil Content
(tung kernels) Oil Content (hulled tung fruit)
Castor Beans Moisture and Volatile Matter Oil Content Free Fatty
Acids
Flaxseed Sampling Moisture and Volatile Mauer Oil Content
SaflIower Seed Oil Content
Copra Aflatoxins
*Surplus method
.Aa I
.Aa 2 , .Aa 3
.Aa4
.Aa 5
.Aa 5 Aa 5 .Aa 6 .Aa 7 Aa 8 .Aa 9 .Aa9a Aa 10 .Aa II
.Ab 1
.Ab 2
.Ab 3
.Ab 4
.Ab 4
.Ab 5
.Ab 6 Ab 7 .Aa 9 .Aa 10
.Ac I
.k 2
.Ac 3
.Ac 4
.Ac 4
.Ac 5
.Ad I
.Ad2
.Ad 3
.Ad4
.Ad 5
.Ad 6
k 2 .AJ: 3 .Ae 4
.Af I
.AI 2
.Af 3
Ag 1
.Ah 1
Pagelofl0
-38 (09) -38 (09) -38 (09) -38 (09) -38 (89) • -91 (09) -91 (09)
-38 (09) -55 (09) -83 (09) -86 (09) -97 (09) -88 (09) --j)5
(09)
-49 (09) -49 (09) -49 (09) -50 (89) • -91 (09) -49 (09) --68
(09) -91 (09) -86 (09) -88 (09)
-45 (09) -41 (09) -44 (09) -41 (89)' -91 (09) -41 (09)
-48 (09) -52 (09) -52 (09) -52 (09) -52 (09) -52 (09)
-52 (09) -52 (09) -52 (09)
-54 (93)' -54 (97)' -54 (95)'
--65 (09)
-72 (09)
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--"un'!",..." Se«1 '>.tll,pling. . . Moi",,,, .,,,,j
Vul.1tilo Manu_. Oil Conti'''''' ._._ Protoin. Protein.. . .
G'm AJlarn, md l'""nu, B,.".t.. Ailacoxin.' BL_ B 'nd G, in Corn
hy F.US,~.....................r
Rap"e
-
l_~ _ -~~ ""..be, _
Oil ('"m,m (,,,,,,,,,,.,,a bulb) __.Jll> 2 -JIl (09) _____ ,
Db,\ --47 (0'»)
Sor Flo". S.ml'l;,,~_._.,_,.,. __ _ ...........Bo I _~O(~)
.'do;",,'. 'nd Vola'il' Maner . . Bc2 -A~ (0')) oa Coo«,,,. . ,__
... I\e 3 --4~ (1)9)P",,,m ,_ ___ . _ .,B< 4 --4~ (~9)' ho«in,
Ti"''''"Jn Dioxid I" F,,, and Oil, ........... c.;>o ---{l2
(O')) Sol,,!>I, Min u,o,!>lncd .. Mine,.aJ S -52 (09)
o.p,,"o'
-
[0("'''0 ",rrnOD U" BY SL(lIO~
Tmc~ M«"I., by AAS . ................................c. l~ -?5
(09) Sodilll1l ""d Calcium by AAS . ................. . C. i5b_B?
(09) Polycrhylcn< i" F", >n .. . . C. i(, -7.5 (09) J lice
£Icm, If01 0"". CC IZ -S9Ih9) C",I",
FAC M"ch
-
L__ 111_ , ""mbo, I.....
Iodin< Vo1'-92 (09) Hydro"}"! Volue (d"
-
F~U_MI IHOI) lIST"' .""'D'
~"""'..... ;"." E",cic IIdd in Oi[, and F,,,.. ....
,..,.,..,.,.,.,.,.,.... ,.CI, Oil>and fm by HPLC ,.,., ,. . u 8
---1'') (09) il-C,n"'~, I" Margarine> , ,.,..,.,.,..... .
,..,.,.,.,., , Co " --. Cr>mpari.>~n PI' AOes & ASTM
,I,f",hod, .. . D- j _9'> (09)
~'mpJir'1l ,.,.,.,.,.,. . Da j -I; W9} M",,,uc< and Volatile
M,tter, Air 0.oJoblc ami Akohol-Jn""l~bl< M., [k M.acr.
.....,..,.,.,., ... ...".,.,.,., ,.,.,., 0. 7 -I8109}
'fot31Anhydro~. S'''I' .".1 C.. ",hlned Alkali .. ,.,.,.,.,
,.,.,.,., Oa 8 --4R 1fl9} Chlorides .,...... . . ..., ,., 0.9 --48
(I)'}) Urno.poniliccl J>1\l.l U.....po~ifi.bl< M,tt« .. . 0.
10 --4~ fiJ'J) Umaponifiahl, M"'
·Swpl"" mcmoo ~'II" 60ilO
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----------
I:Iom... ""....... . " _ , " "".,,0., 17 -52 (09) A1b]in"
Silica[Ibonat"', Gr"i,,,",,,, Ab>orptioll M"tI",d. ..
".......... . ., D. t 9' -42 (09) C,,~""""'. Volumetric E,oh"ion
Method _ .D, 1%-\2 109) PI,r"'pb",,, (yavim«ric m",hod) " _ Da 20a
-48 109) I'I,r.'>n< . "........... .1J, 26 ---42 (1)9)
Comhinro Sodium .".1 rUl.«iLlm Orid 5 --48 \O'JI Toralllnhydrvl'.,
s."p. .. .. ............ "........ .. Ob 6 ---48 (O'Jl ChIorid",
(ind,""o' m"uwd) .. .. " Ob 7 ---48 (O'J) Chlorid
-
_______-==~=:J 5 in Loo;,I,I" Cooe
-
__________________________ ________________________
__________
______
,~'-------------:::==----::c-lPRODLCT _Mm IO~ ,,,, L"-
",:.l"",N
(;"d".,'.1",-- """, ,_ f1"'''kfodd Vi,oosiTY "" , " Vi>co,i,y
"fTran. by BuW", Time M"hnd Lodthi" c,~ Pm,Ju,", Towph""I, ill
l"'imin r.y HI'lC Iodin, V,I,," in I",:irh;n, \,iii, Mcd",d , "
Sedi"" 1.4, Eval..~lioo ....d Design of Yest Melhod5 Preci,;on
&f Anol)"ig~n Produm
Fatty Ami"", .. FaIry Amidoomin",... . , . faIry Quaternary
Anllnoniuo, Colacuum O'I'en) "."
Color Gardnel .... " PI"inum-Cob,lt Sc.ol< Commercial F.tty
i\.c·,d, hrry Acid> (:ili~r h"'l;n!\.'
ill:id Value Commercial Fmy i\£id.. . Polym~'izd Fa,')'
i'u:id.< . Drying oa.. .. .. Fo"y Q'ur~rn.ry Ammonium ChloriJ«
\i"cluding free amino nIno} Di!>,,';' .~,id,.
Amin
-
G''''p'''i[ior, Prim,,,, ,'uT1;,,< (;~mpo,i[ion by Gl.C .
CompO>.irio" ul O;,,,,,r Add! by HPI£:
1,,,lino VaJu< Wij., Method (g~, and F.rry DI""',,.. Hyd,~ryl
Voln
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2009 Table of Contents AI"""bctinllnd~.
....ho>
~n ~~I''' ",,-t Cop.. MraI...................... .. .Ab I -r:
(.11'''''y wlu","'), ...AI> 7 _OJ ({\~) In P.~""" i
-
-- .. .....,..., i..... Am,ne, Te,L'
I,,, ta,C)' Quatern.ry A""Mnium CliloTide.,. "-" P,;m.'Y Ami"es,
by (;~, C~romatograpi,y .. lur PrimalJ'" S
..........T < 3, . rrs,
, Tl' ,la
---i>-I fO'J) _77 (09) ---M 1.09)
Amill< Value F,,'l' Quotern.,')' Ammonium Ch!rid« .
Pri"','}', Src~ndary, m,d T en:iaI}' I"dieato' Fmy Amin
S 4d 5 4<
--4 (09) ----I>l [l\"\
hor Fclcin T",r., ,,, . .. ,Ca7 -35 (901 • 1l,nm(,jpJ'Il'ne in
Wible au, and I'm.... . .. . Cd 21 -Y1 (O~j jj;,,,I,,,,,,,1
F«cklOck>.......... . . ...Ck 1 ---..-.:I1 .. . , ..Cc ~~ -52
(09) f"r s"y"",n Oillmodilied ,.,,,-',...... . CC& ---
-
-- -AlPIIMl''-A11Nv,,1
M.""xI 1.1,... Chloride<
i" G)Vco,in «",doapJ>rod""'> . D" 27 --48 (09) by FAC
Mcmoo. . . ....u 13>.--43 (09) br Fmy Add, ic~mm"oi.J).." .
..."............ ..Td 2. --64 (09) h;- Garon« fo' lodu'''iol OiLs .
.............. ..Td l> --64 (119) Colo, (Automated M",lwdi , Co
13; -97 iV'l) by Gudnc' fo' l-45 (0')1
Composi,io", of Di"",;, ""'i
-
~......... Dime Val,," of D'Yin~'Jil> _ _ _______ Th 1•
...,(>4 (09) Dienoic Acid, ;0 Ochydrawl C,,"or Oil and A,iJ,'.
__ Tl h --64 (,I'l' Djl..ommic Me,)",,1 for Solid Fat h,d G.l1O -,7
(97)' Dm,,' Adds, Com!,,-,'''ion by HPLC ...".._TF5 -91 (09)
Dm,,,,l.ylpolysiloxan and 0;1,) hy GtC .
.....Cd 24 -95 (U9) __________ Cd 2'; -% (09)
O16 {951' f.»
-
r _ ..- ....... ""mb ,,,,I Oil,._ in en,,)" V~."hl< 0;1, by
COC _ ;n P._ ,_._
fumQnwn, B, .ndB,;o CDrn by LC , ;n Corn by Le...
(;Ioco'inola"" (rape=Jj, (;Iy""i", TOIal and Organic ~.,id"e..
Gy_",;"e, Free, by l-IHCiFI.sn . Glycc'ul Lv P.~by NUL. .
"................. (',1",1.",1 from GLC Cyd"h"","e Memo..:l... ..
Cyd " l,e, . " e_A",ric Arid 1-1.-Q? 109)
..........................H M -%(09)
..................... R, 1:\ ~7 (09) ..............J, J -~7
(09)
.........Ca .'lb ----87 (09) ........... Ba 14 -81 t(l~)
. Ca 6c ~5 (09) . ])-.16 ---'i2 (;!'II
.............................. ...Cd 27 -% \Ii'll
........................... T, [;, -78 (M)
........................T, II, -79 (O?)
. T.la ---66 (09) .. Cd 4 --40 (99)"
. Cd n ---.(0) «(1'1) .. .Am 4 -{l~ (Il~l
. F 6 --11 (O~)
C, J., --46 (091 .. Jo ~ -H7 (M)
.. Fron' M.tter
........Cd Ie ---fll (09) .ca Ie -85 (09)
. .., Cd;b ----87 (09.' Cd;d _0"(09) TB I ..(,( (09)
-
__
__
of Fars and Oil, of fatty lind, "I' p",)' Am,n" Dl.mine>,
"0'\ Amidoamin",.. ,.( I'm)' Quaternary Amm""ium Chloride'
f"l«-i,llln. "fSoap and Soap P,oduct>...
1""0, Trace A",('urn.' in U~, byAAS .. hy A!l.'i with Cmphil<
fum",.
I"'rr~l'yl Alcohol, Sf"CihC:uio,,-, __ Joinba Oil
AcidV.h". ."."........... 1)"'ectionofT'iglya:rid,Mol"',"uon"
.~«
-
Al!"IA"fTIrAlIND~ -... L""'" ........., i.....
brryAejd" . , " Th j" ...(,.; (09) Mc..Lh ( ,,,d Oil, .........
"..... ............... .....Ca 2a ----H ((I'll in Fa[t;' Al~yl
:;ulfa« 1',0dlc, MoLb.-:J in Alkylbenzenc Sul(o,u« P[~dum "" .....
" . . oa a, _,~(~o)' in Fat, ."d ou;... . Ca 2< _~ ill'J) in
Fa'" N"",~ ---87 (09)
M"I.cular Weight ('",rag.) of fam' Qu".. . .....C. 'If -» i(l'I)
j" Soap $[",,, (Wl"'po"'O ....1< "'-"«rial), ...G ~
----lOW9)
:. i[rogt'n-Am m"" ia_ P,~[oin Con"ol>i"" T,h(e ........
"..... ,....... ,A., 5 -91 (0") Copper Sv!["< C,llaly>[....
,............ . . .....&-11.> ---87 (90) • G:>pp'"
S"lt',e Plu., l'imliull1 Dit,'id' C.r.L1y>l " -90 (1l9) in
C,tlon>« (gronllJ"u,- -52 (09) in C,,[01 r~m.c". -52 (0'1) i"
C'1lI1 Genn Ai 4'" ----S9 (0'1) in C""o"",oo k' _}8 (119) in
Fl.",,,,,,d , " . ........... " ... Af'} -54(95)' in Lore'"
(OJ"""..",d huJ[,). ....,BI.> ;: -3R IOQ)
'Surplw metkd ~"llC 7 0/ 12
-
-------C_=~"'OC_"J nu"'bOcil1""'ir,,,, .................H 3 --45
(09) Forocd Drm, 51'",;"""[io,,. . V.coum. SpcciHc.aliom .
... ..................
., . _
H 1 H 4
_.N (tNI--4, (U~I
O,id;zed Pa"y Add.< in Sw.p S'oe"" , GJ -'i-l (u·))
O,ih",pho,"~ 1I"',,,io Ah."'fption Spccr:rOllcopy .. ..C.llb-~l{(9)
Ph""pnom,
il\ k,ilni~ ('a,oIi .. Ji'i -55 (89)' il\ Oil, . . c. 12 _j~
(09) ,,, O;L, ilSO M,thadi .............................Ca 12.J.
---1Jl (U~) ,n 0;1 by Icr·QE~ . . Ca 20 -':I'J (O~)
Photo",,,ri< Ind. . GI10 -91 (O?) Pclycthrknc in Pal• .00
Oil, .' ', '.'"",' ..' ,., ,.,., ,., , , ,.,.,., Ca 16 -7:>
IO?)
·Sutplu.< n'e,hod
-
.'l"HA"",cA' ';;DE;I ~"~ "U"'..... .......
l'olym. M""I, GkJW1dnut» . ...............................AI,4
_0; ,-O~J ;0 S~'" F1au"'/Cmola Flout> . .. .. " Ilc 4 _91109) j"
"""'citL< .. .. .N:.4 -91 (09) !'To"'i,, Dlip (PDT) (.",yhJy" .
. B,4b -B7 (90)" wi,h Copper SuI!>!< Plu; T;"""'nl Dio,"d<
c.tal}"'t ... .................Ba4d -90 (09i
kd,,,""""",«:1, hpdlc' Soybean Oil ..".. C,9. ~~2(0'i)
D"!:"",,,,«:I, Hyd4 (09) Fae< and QU... . . . . . .. . CO 7 -15
(09) Far']' ildd.!, 1::,'mm",0,1.. . . Tp la ~(o9)
R"ic),.tr_Mei..1V.Ju, .. . . Cc1 5 -'10 (ll')) Rr~idu"1 ],;",
iI, C''''"''''',,d .. .. A. 7 -55 1l'9\ R
-
- ...,.., """,t- i_
of 1'olym ---64 (09) "f -'12 (09) ~iip P",,,.
H.,d F,,, (palm oa) ,.. .. -. " ce 3 -25 (()OJ; Soft F"". . u 4
-2\ IB~i'
Smoke, fl.,IL ""d file Poin" Cbd.nd aI''''' Cup M",bod
"......... ...u 9a -181("!] Soap in Oil
by c"OdUClivi') Met~od.. .. .-................. . \:" 15 ---0
(B9) • by Tj"ime"io M",hod .. , C'" 17 -95 (O?)
W;nm Jllkylbenun< SuIlOn hy VI".Yi"k, Abso'l"io" .Dd 3 ---0
(09) W;um and Calcium br AAS . 0. '~b-ll7 (09) S" in F,t> "nd
Oil, . Cd 6 -38 (R~)' Soluble Min",,] M."., ,nd FaayMJ< Combim:d
"" Min...,1 ""'-p.. . . .. 0. 4 -25 (O~; ~pccificatio",
-..................... . 0;." S=ion H ,pccif,c Gravi')'
Drying OiL....... . "............................... ... Tc. Ib
-64 (09) Fmy Acid" Comm«ciol.................. . . ,T" 1.1 --G4
(09) "1,,,,,,iLl.. . . Ea 7 -?5 (09) 1"'I',id Oil, and fa" . u
10,_1) (95)' S"lid F"" .nd Wax". .. . u 10\>---15 (09)
Spread.bili'}' .. Cj 4 ---fIn (M' Srability ,nd Q".Ji'.1' of
F,,,.
-
--~nn_. I..... S,andard Sol,,'I"'"
Alcoholic P~"..iu", llyd""iJo , ,.,." , , . .. H J5 -~~ ((lQ\
Hvdm by Cl.C. . CC 10 ----B9 (9~)' ".Ins Composilion of Parti.Jly
Hycl~)~",,,,,l all, by GLC-IR. .. .. Cd 14f>-93 (9.5)' ,,"'"
loom"'" (1,01a,«I) by ITI/( . . Cd 14 -95 (09) ,,"'" 1",0"(8 by
Capillary GLC. , Cd 14
-
"' ..... ......., ' ... in Fat>0' Hy,iml)'Ud 1-." , ,., ,..
...............Ca 5b ,-71 ((l~) in F.tty A'ids, Comm~rcw . .. Tk ta
-6-1 (O~l in Fatty Add" 1'"1,,,,«,,00.. , . ................ ...-n
1a ,-6-1 (O~) in Soap and S...... p rmduw.. .....D. 11 ---. 110m,.
and 11,;11 fe,,!j . . . B. 9 -~8 (OY) Vill,v=hi" Te" [or S=rnc Oil,
Modili..:!. .. .. o, 2 ,--40 (~9) >'i"""icy
Drying Oil., BuhbleTin,( M'thod . . Tq 1. ,---f.
.......................01,4 ---4~ (09)
W,.. Come", . . .. ........" c, a ,-02109) Wil
