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[email protected] www.magnaiv.com Canada United States Chile Engineering & Technical Field Services CARGILL LIMITED 2016 Transformer Oil Sampling and Analysis June 7, 2016 File: C3330-10 Project Manager: George Shehata, P.Eng. Superior client service. Electrical confidence.
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Page 1: 2016 Transformer Oil Sampling and Analysis · 2016 Transformer Oil Sampling and Analysis June 7, 2016 File: ... Close observation of dissolved gases in the oil, ... 12 2 / OIL-/ ESTER

[email protected]

www.magnaiv.com

Canada

United States

Chile

Engineering & Technical Field Services

CARGILL LIMITED

2016 Transformer Oil Sampling

and

Analysis

June 7, 2016 File: C3330-10

Project Manager: George Shehata, P.Eng.

Superior client serv ice. Electrical confidence.

Page 2: 2016 Transformer Oil Sampling and Analysis · 2016 Transformer Oil Sampling and Analysis June 7, 2016 File: ... Close observation of dissolved gases in the oil, ... 12 2 / OIL-/ ESTER

1103 Parsons Road SW

Edmonton, AB T6X 0X2

p 780.462.3111 f 780.462.9799 tf 800.462.3157 Superior client serv ice. Electrical confidence.

[email protected]

www.magnaiv.com

Canada

United States

Chile

Engineering & Technical Field Services

File: C3330-10

June 28, 2016

CARGILL LIMITED

801 LOW LEVEL ROAD

NORTH VANCOUVER, BC V7L 1A7

Attention: Mr. Ron Ludwig

Supervisor, Electrical

Dear Sir:

Re: Oil Sampling and Analysis – North Vancouver Facility

We are pleased to submit the insulating fluid report and test sheets for the three (3) transformers

and one (1) OCB located at the North Vancouver facility. The transformer sampling was

performed by James Powell on June 7, 2016 in accordance with ASTM D923 and D3613

standards. The laboratory testing was completed by The Chemlab of Calgary. Review of results

and analysis was provided by the undersigned.

Based on the analysis of the laboratory results, all equipment is in good condition and suitable

for continued service. Once again, both the East and West transformers are showing elevated

Ethylene indicating higher temperature internal heating however, since there has been no

significant generation and all other dissolved gases and standard fluid quality tests are within

IEEE acceptable limits for in-service equipment, the units are of no immediate concern. Annual

sampling is highly recommended to monitor any further generation. The Sub 2 transformer is

filled with Natural Ester (FR3) – it appears there is elevated Ethane however, the limits indicated

are for mineral oil only. Natural ester generates Ethane under normal operation (test limit is

400PPM) therefore the current value is within acceptable limits. In addition, the interfacial

tension appears low however, the test limit is 18 for Natural ester. As such all values meet the

recommended test limits for natural ester. The OCB is showing all dissolved gases and tested

fluid quality properties to be within acceptable limits. All equipment is classified as category

Type 1. Equipment in this category shows acceptable test results, with some showing minor

elevated gas levels. Close observation of dissolved gases in the oil, along with the fluid quality

properties, provides the most valuable information about your equipment health. All units are

recommended for annual resampling with electrical tests performed at 2 year intervals. This

testing schedule will allow us to maintain a comprehensive trend of all properties, and provide

accurate analysis on the condition and operational reliability of your equipment. Please see

Section 3.0 – Summary of Results and Deficiencies for a complete breakdown.

Via: email

fax

mail

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3 | Pa ge

We trust this report meets with your approval and requirements. Should you need further

information or assistance, please do not hesitate to contact us. Thank you for retaining the

services of Magna IV Engineering. We look forward to being of service to you again in the future.

Yours Truly,

MAGNA IV ENGINEERING

Stephanie Parsons

Oil Analysis Project Manager

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4 | Pa ge

INDEX

1.0. SCOPE OF WORK .......................................................................................................................... 5

2.0. SUMMARY OF TESTS ....................................................................................................................... 6

3.0. SUMMARY OF RESULTS AND DEFICIENCIES ................................................................................ 8

4.0. TEST RESULTS ................................................................................................................................... 9

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5 | Pa ge

1.0. SCOPE OF WORK

As per Magna IV Engineering’s standard practices for transformer oil sampling, our scope of work consisted of:

Providing Transformer Inspection

Recording Nameplate Data

Reading and resetting Gauges

Providing Inspection Report

Procurement of oil samples in accordance with ASTM D923 & D3613

- obtain one syringe for gas-in-oil analysis & moisture content

- obtain bottle sample for fluid quality tests

The Chemlab of Calgary performs all analytical tests, consisting of:

Gas Analysis (DGA) D-3612

Moisture Content D-1533B

Interfacial Tension D-971

Acid Number D-974

Color Number D-1500

Visual Examination D-1524

Dielectric Breakdown D1816 @ 1mm

The Chemlab is responsible for proper disposal of samples.

Analysis of Laboratory results by Magna IV Engineering. Tools utilized:

Duval Triangle

GA Key Gas Method

DGA Rogers Ratio Method

DGA Cellulose

DGA IEEE/ANSI

Specific History and Trending (Generation vs. Time)

Document, interpret and evaluate results, and recommend corrective or follow up

action.

Prepare traditional summary sheets and lifetime trending graphs.

Prepare report detailing findings, recommendations and corrective action as

required.

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6 | Pa ge

2.0. SUMMARY OF TESTS

For your reference and confirmation of the specific tests performed and their analytical

value, we provide the following highlight information. All transformer tests were

performed as per the latest ASTM standards.

Specific tests performed include:

ASTM D1816 - Liquid Dielectric Test

The dielectric breakdown voltage of an insulating liquid is important as a measure of

the liquid’s ability to withstand electric stress without failure. It serves to indicate the presence of contaminating agents, such as water, dirt, moisture, cellulosic fibers or

conducting particles in the liquid, one or more of which may be present in significant

concentrations when low dielectric breakdown values are found by test. However, a

high dielectric breakdown voltage does not indicate that the concentrations of

contaminants that are present in the liquid between the electrodes are not large

enough to negatively affect the average breakdown voltage of the liquid when

tested by this method.

ASTM D971 - Interfacial Tension

This method has been shown by practice to give a reliable indication of the presence

of hydrophilic compounds. When certain contaminants such as soaps, paints

varnishes and oxidation products are present in the oil, the film strength of the oil is

weakened, thus requiring less force to rupture. For oils in service, a decreasing value

indicates the accumulation of contaminants and oxidation products, which may

attack the insulation and interfere with the cooling of transformer windings.

ASTM D1533 - Moisture Content

The electrical characteristics of an insulating liquid are deleteriously affected by its

water content. A high water content may make a dielectric liquid unsuitable for some

applications because a deterioration in properties such as dielectric breakdown

voltage may occur. This test is suitable for use in acceptance specifications, in control

of processing and in evaluating the condition of dielectric liquids in service.

ASTM D974 - Neutralization Number

The acid number of an oil is a measure of the amount of acidic materials present. As

oils age in service the acidity, and therefore the acid number, increases. A used oil

having a high acid number indicates the oil is either oxidized or contaminated with

materials such as varnish, paint or other foreign matter. This test serves as an indicator

of the potential of the oil to form sludge.

ASTM D1500 – Color Number

The color of a new oil is generally accepted as an index of the degree of

refinement. For oils in service, an increasing or high color number is an indication of

contamination, deterioration or both.

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7 | Pa ge

ASTM D3612 - Dissolved Gas Analysis

Gas analysis is based upon the fact that both electrical insulating oil and cellulosic

insulation break down under abnormal thermal or electrical stress. The results of these

stresses are both volatile and non-volatile gases, known as fault gases. Gas analysis is

the technique that identifies fault gases, relates their quantity, generation rate and

relevant ratios to type and severity of fault.

Typical fault gases analyzed are:

Hydrogen H2

Methane CH4

Ethane C2H6

Ethylene C2H4

Acetylene C2H2

Carbon Monoxide CO

Carbon Dioxide CO2

Typical types of transformer problems that can be detected are:

thermal degradation

- low temperature

- high temperature (hot spot)

arcing

partial discharges

degradation of paper insulation

Increased frequency or periodic testing will significantly increase the value and

accuracy of fault gas analysis.

Page 8: 2016 Transformer Oil Sampling and Analysis · 2016 Transformer Oil Sampling and Analysis June 7, 2016 File: ... Close observation of dissolved gases in the oil, ... 12 2 / OIL-/ ESTER

8 | Pa ge

3.0. SUMMARY OF RESULTS AND DEFICIENCIES

Transformers typically can be broken down into the following categories:

Type 1 Transformers in this category show acceptable test results, with a few

transformers showing signs of minor non-serious overheating (re-test

recommended in one year). Variations of Type 1 transformers may exist

pending past records and age of units.

Type 2 This category covers any transformer showing test results where some concern

is evident (re-test recommended in six months).

Type 3 Transformers in this category show signs of serious fault gas concentrations or

very poor chemical properties (prompt re-tests or further investigations are

required).

Type 4 Mechanical deficiencies (corrective action to be taken as soon as possible or

as recommended).

Please refer to the test sheets (5 pages) for a detailed breakdown of results and

recommendations. Following is the Summary of Results and Deficiencies.

Transformer

Identification /

Serial Number

Year

Manufactured

Analysis

Type

Recommended

Retest Comments

East TX

293639

1967 1 1 Year

Slight elevation in Ethylene – higher

temperature internal heating – no

immediate concern. All other dissolved

gases and tested fluid properties within

acceptable limits. Annual sampling highly

recommended to monitor any further

generation. Check loading conditions and

cooling means. No major deficiencies

noted.

West TX

293638

1967 1 1 Year

Slight elevation in Ethylene – higher

temperature internal heating – no

immediate concern. All other dissolved

gases and tested fluid properties within

acceptable limits. Annual sampling highly

recommended to monitor any further

generation. Check loading conditions and

cooling means. No major deficiencies

noted.

Sub 2

1059001354

2010 1 1 Year

All dissolved gases and standard fluid quality

properties within acceptable limits for

Natural Ester Insulating fluid. Annual

sampling should be maintained. No major

deficiencies noted.

6OCB1

60503

1967 1 1 Year

All dissolved gases and standard fluid quality

properties within acceptable limits showing

no significant change. Annual sampling

should be maintained. No major

deficiencies noted.

Page 9: 2016 Transformer Oil Sampling and Analysis · 2016 Transformer Oil Sampling and Analysis June 7, 2016 File: ... Close observation of dissolved gases in the oil, ... 12 2 / OIL-/ ESTER

9 | Pa ge

4.0. TEST RESULTS

Following is a copy of all individual test results. We recommend you review the results

and graphs at your convenience to better understand our analysis and the condition of

your equipment.

Each piece of equipment consists of the following 4 pages of documentation:

Page 1 Transformer nameplate, identification name, oil and gas results and any

notable comments and deficiencies.

Pages 2&3 Graphs for all generated gases and chemical analysis tests. This provides a

more visual idea of determining the trending of these gases. All limits are

based upon standards widely accepted throughout the industry.

Page 4 Inspection sheet, nameplate data, gauge recordings.

Page 10: 2016 Transformer Oil Sampling and Analysis · 2016 Transformer Oil Sampling and Analysis June 7, 2016 File: ... Close observation of dissolved gases in the oil, ... 12 2 / OIL-/ ESTER

Cargill Terminal

East - TX

S/N: 293639

C3330-10

Oil & Gas Results

Nameplate Information

Page 11: 2016 Transformer Oil Sampling and Analysis · 2016 Transformer Oil Sampling and Analysis June 7, 2016 File: ... Close observation of dissolved gases in the oil, ... 12 2 / OIL-/ ESTER

Cargill Limited

Cargill TerminalFluid Test Report

Maintenance

Nameplate Information

Serial Number: 293639

Sample Date:

Job Number:

Nitrogen (N₂)

Total Dissolved Combustible Gas

Total Gas Content (%)

kVA Rating: 4000

Fluid Type: OIL

Designation: East - TXkV Rating: 72.000/0.575

Dissolved Gas Analysis

Fluid Quality Analysis Limits

Additional Fluid Quality Tests

Notes:

D3612-C

Apparatus Type: TRN Manufacturer: WESTINGHOUSE

Year Manufactured: 1967 Fluid Capacity (G): 750

Expressed in PPM

Voltage Class >69kV - <230kV

Hydrogen (H₂)

Methane (CH₄)

Ethane (C₂H₆)

Ethylene (C₂H₄)

Acetylene (C₂H₂)

Carbon Monoxide (CO)

Carbon Dioxide (CO₂)

100

120

65.0

50.0

2.0

1000

10000

Limits

Moisture Content D1533 (ppm)

Interfacial Tension D971 (mN/m)

Acid Number D974 (mg KOH/g)

Color Number D1500 (Relative)

Visual Examination D1524 (Relative)

Dielectric Breakdown @ 1mm D1816 (kV)

Dielectric Breakdown D877 (kV)

25

30.0

0.150

3.5

CLEAR

28

26

PCB D4059 (ppm)

Specific Gravity D4052 (Relative)

Power Factor @ 25°C D924 (%)

Oxidation Inhibitor D2668 (%)

2.0

0.91

0.5

0.08 - 0.3

Limits

Power Factor @ 100°C D924 (%) 5.0

Oxygen (O₂)

16

31.8

33

0.018

L1.5

CLEAR

17

32.4

40

0.022

1.5

CLEAR

4

29000

66800

3

146

7180

3.2

62.0

0.0

218

10.320

5

27500

71200

3

194

7550

3.1

58.2

0.0

263

10.660

Jun-7-2016

C3330-10

Jun-10-2015

C3330-7

- 3.7

Page 1 of 3Serial Number: 293639Magna IV Engineering

Page 12: 2016 Transformer Oil Sampling and Analysis · 2016 Transformer Oil Sampling and Analysis June 7, 2016 File: ... Close observation of dissolved gases in the oil, ... 12 2 / OIL-/ ESTER

Cargill Limited

Cargill TerminalFluid Test Report

Maintenance

Historic Graphs and Diagnostic Charts

Combustible Gases

Total Gas Content (%)

(All Gases)

0

2

4

6

8

10

12

Ju

n-1

6

Ju

n-1

5

Key Gas Comparison (ppm)

0

20

40

60

80

100

120

140

160

CO - H2 - Meth - Eth - Ethy - Ace

Methane (CH4)

0

0.5

1

1.5

2

2.5

3

3.5

Ju

n-1

6

Ju

n-1

5

Pa

rts

Pe

r M

illio

n

Ethane (C2H6)

0

0.5

1

1.5

2

2.5

3

3.5

Ju

n-1

6

Ju

n-1

5

Pa

rts

Pe

r M

illio

n

Acetylene (C2H2)

0

0.1

0.2

0.3

0.4

0.5

0.6

0.7

0.8

0.9

1

Ju

n-1

6

Ju

n-1

5

Pa

rts

Pe

r M

illio

n

Ethylene (C2H4)

0

10

20

30

40

50

60

70

Ju

n-1

6

Ju

n-1

5

Pa

rts

Pe

r M

illio

n

Hydrogen (H2)

0

1

2

3

4

5

6

Ju

n-1

6

Ju

n-1

5

Pa

rts

Pe

r M

illio

n

Carbon Monoxide (CO)

0

50

100

150

200

250

Ju

n-1

6

Ju

n-1

5

Pa

rts

Pe

r M

illio

n

Non-Combustible Gases

Carbon Dioxide (CO2)

0

1000

2000

3000

4000

5000

6000

7000

8000

Ju

n-1

6

Ju

n-1

5

Pa

rts

Pe

r M

illio

n

Nitrogen (N2)

0

10

20

30

40

50

60

70

80

Ju

n-1

6

Ju

n-1

5

Thousands

Pa

rts

Pe

r M

illio

n

Oxygen (O2)

0

5

10

15

20

25

30

35

Ju

n-1

6

Ju

n-1

5

Thousands

Pa

rts

Pe

r M

illio

n

Page 2 of 3Serial Number: 293639Magna IV Engineering

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Cargill Limited

Cargill TerminalFluid Test Report

Maintenance

Fluid Analysis

Moisture Content

(Should be <Limit)

0

5

10

15

20

25

30

Jun

-16

Jun

-15

Pa

rts

Pe

r M

illio

n

Interfacial Tension

(Should be >Limit)

0

5

10

15

20

25

30

35

Jun

-16

Jun

-15

mN

/m

Acid Number

(Should <Limit)

0

0.02

0.04

0.06

0.08

0.1

0.12

0.14

0.16

Jun

-16

Jun

-15

mg

KO

H/g

Color Number

(Should be <Limit)

0

0.5

1

1.5

2

2.5

3

3.5

4

Jun

-16

Jun

-15

Dielectric Breakdown D877

(Should be >Limit)

Actual Values

Acceptable Limits

Dielectric Breakdown D1816

(Should be >Limit)

0

5

10

15

20

25

30

35

40

45

Jun

-16

Jun

-15

kV

Page 3 of 3Serial Number: 293639Magna IV Engineering

Page 14: 2016 Transformer Oil Sampling and Analysis · 2016 Transformer Oil Sampling and Analysis June 7, 2016 File: ... Close observation of dissolved gases in the oil, ... 12 2 / OIL-/ ESTER

/

WEIGHT

TEMP RISE

PSI

PO# for Sampling Lab:

REPORT RUSH:

� DGA D3612C � Dielectric 1.0mm D1816 Oxidation Inhibitor D2668 NOTES:

� Moisture in Oil D1533B Dielectric 2.0mm D1816 Furfurals (paper degradation) 1. NO WINDING TEMP GAUGE

� Interfacial Tension D971 Power Factor 25°C D924 Metals D3635ICP TRANSFORMER IS IN A VAULT

� Acid Number D974 Power Factor 100°C D924 Viscosity D88

� Color/Visual D1500, D1524 Specific Gravity D1298 Other:

Dielectric 2.5mm D877 PCB

BREATHERS

GAUGE DOCUMENTATION

DESCRIPTION YES DESCRIPTION OK

DUSTY

40 °C

COMMENTS

NITROGEN ADDED

NO

RADIATORS INSTALLED

CONSERVATOR TANK

BLUE

HV BUSHINGS ACCESSIBLE HV BUSHING CONDITION �

RELIEF VALVE INSTALLED

GROUNDING (2 LOCATIONS) �

PHYSICAL DAMAGE

NO

DIRT ACCUMULATION

750

PROPER LEVEL

NO

OIL LEAKS (WHERE)

DUSTY

FAIL

CORROSION / RUST ACCUMULATION � PAINT IS GOOD

� DUSTY

COMMENTS

3.7 PPM

LV BUSHING CONDITION �

DM 635 1006975

RADIATOR CONDITION N/A

50 °C

� SILICA DESICANT CONDITION �

NO

INSPECTIONS

CRITERIA

ADEQUATE CLEARANCE

TANK PRESSURE (Min: -1 Psi (-6.89 kPa))

LOW OIL LEVEL (GAUGE @ LOW)

LV BUSHINGS ACCESSIBLE

Tests Required (Internal Purposes Only)

CRITERIAYES

Sampler: JMP

78 %

27.0 °C

BOTTOM VALVE

Syringe #:

KPA

READING

SEE DIAGRAM AT RIGHT

HUMIDITY

AMB. TEMP

SEDIMENT

SAMPLE POINT

� OK

SO# 293639 AMPS

PRE-SAMPLING CHECKLIST

CAPACITY GALSLTRS

NO

RESET GAUGE

OIL LEVEL

PRESSURE

GAUGE READING DRAGHAND

OIL TEMP

N/A

SAMPLE COLOR

SAMPLE DATA

NO

YES / NOWINDING TEMP

ONAN SEC VOLTS 575 %IMPED

WESTINGHOUSE PRI VOLTS 72KV 3 3

PREPARED FOR

CARGILL

AREA

SITE

WO#

MAIN SUB

CARGILL TERMINAL

C3330-10 DATE

TEST BY

APPROVED BY

EAST TX

JMP

STANDARD MAINTENANCE

OIL FILLED EQUIPMENT INSPECTION SHEETTAG #

CANF-5E006

LEMON YELLOW

STRAW YELLOW

STRAW WHITE

BROWN

REDDISH ORANGE

ORANGE BLACK

OTHER:

OIL TYPE MINERAL SYSTEM BREATHING

DATE OF LAST OIL CHANGE (IF KNOWN) UNKNOWN

NAMEPLATE DATA

June 7, 2016

PCB CONTAMINATED

# OF TAPS

TAP FOUND/LEFT

YES

5EQUIPMENT TX KVA 4000

MANUF.

YEAR 1967

3.70%TYPE

East Tx Oil Filled Equipment Inspection Page 1 of 1

Page 15: 2016 Transformer Oil Sampling and Analysis · 2016 Transformer Oil Sampling and Analysis June 7, 2016 File: ... Close observation of dissolved gases in the oil, ... 12 2 / OIL-/ ESTER

Cargill Terminal

West - TX

S/N: 293638

C3330-10

Oil & Gas Results

Nameplate Information

Page 16: 2016 Transformer Oil Sampling and Analysis · 2016 Transformer Oil Sampling and Analysis June 7, 2016 File: ... Close observation of dissolved gases in the oil, ... 12 2 / OIL-/ ESTER

Cargill Limited

Cargill TerminalFluid Test Report

Maintenance

Nameplate Information

Serial Number: 293638

Sample Date:

Job Number:

Nitrogen (N₂)

Total Dissolved Combustible Gas

Total Gas Content (%)

kVA Rating: 4000

Fluid Type: OIL

Designation: West - TXkV Rating: 72.000/0.575

Dissolved Gas Analysis

Fluid Quality Analysis Limits

Additional Fluid Quality Tests

Notes:

D3612-C

Apparatus Type: TRN Manufacturer: WESTINGHOUSE

Year Manufactured: 1967 Fluid Capacity (G): 750

Expressed in PPM

Voltage Class >69kV - <230kV

Hydrogen (H₂)

Methane (CH₄)

Ethane (C₂H₆)

Ethylene (C₂H₄)

Acetylene (C₂H₂)

Carbon Monoxide (CO)

Carbon Dioxide (CO₂)

100

120

65.0

50.0

2.0

1000

10000

Limits

Moisture Content D1533 (ppm)

Interfacial Tension D971 (mN/m)

Acid Number D974 (mg KOH/g)

Color Number D1500 (Relative)

Visual Examination D1524 (Relative)

Dielectric Breakdown @ 1mm D1816 (kV)

Dielectric Breakdown D877 (kV)

25

30.0

0.150

3.5

CLEAR

28

26

PCB D4059 (ppm)

Specific Gravity D4052 (Relative)

Power Factor @ 25°C D924 (%)

Oxidation Inhibitor D2668 (%)

2.0

0.91

0.5

0.08 - 0.3

Limits

Power Factor @ 100°C D924 (%) 5.0

Oxygen (O₂)

13

32.3

39

0.014

L2.0

CLEAR

7

32.8

36

0.014

2

CLEAR

7

28300

74300

5

212

4880

4.3

71.9

0.0

300

10.780

8

24300

68400

5

231

4640

4.1

64.8

0.0

313

9.770

Jun-7-2016

C3330-10

Jun-10-2015

C3330-7

- 6

Page 1 of 3Serial Number: 293638Magna IV Engineering

Page 17: 2016 Transformer Oil Sampling and Analysis · 2016 Transformer Oil Sampling and Analysis June 7, 2016 File: ... Close observation of dissolved gases in the oil, ... 12 2 / OIL-/ ESTER

Cargill Limited

Cargill TerminalFluid Test Report

Maintenance

Historic Graphs and Diagnostic Charts

Combustible Gases

Total Gas Content (%)

(All Gases)

0

2

4

6

8

10

12

Ju

n-1

6

Ju

n-1

5

Key Gas Comparison (ppm)

0

50

100

150

200

250

CO - H2 - Meth - Eth - Ethy - Ace

Methane (CH4)

0

1

2

3

4

5

6

Ju

n-1

6

Ju

n-1

5

Pa

rts

Pe

r M

illio

n

Ethane (C2H6)

0

1

2

3

4

5

Ju

n-1

6

Ju

n-1

5

Pa

rts

Pe

r M

illio

n

Acetylene (C2H2)

0

0.1

0.2

0.3

0.4

0.5

0.6

0.7

0.8

0.9

1

Ju

n-1

6

Ju

n-1

5

Pa

rts

Pe

r M

illio

n

Ethylene (C2H4)

0

10

20

30

40

50

60

70

80

Ju

n-1

6

Ju

n-1

5

Pa

rts

Pe

r M

illio

n

Hydrogen (H2)

0

1

2

3

4

5

6

7

8

9

Ju

n-1

6

Ju

n-1

5

Pa

rts

Pe

r M

illio

n

Carbon Monoxide (CO)

0

50

100

150

200

250

Ju

n-1

6

Ju

n-1

5

Pa

rts

Pe

r M

illio

n

Non-Combustible Gases

Carbon Dioxide (CO2)

0

1000

2000

3000

4000

5000

6000

Ju

n-1

6

Ju

n-1

5

Pa

rts

Pe

r M

illio

n

Nitrogen (N2)

0

10

20

30

40

50

60

70

80

Ju

n-1

6

Ju

n-1

5

Thousands

Pa

rts

Pe

r M

illio

n

Oxygen (O2)

0

5

10

15

20

25

30

Ju

n-1

6

Ju

n-1

5

Thousands

Pa

rts

Pe

r M

illio

n

Page 2 of 3Serial Number: 293638Magna IV Engineering

Page 18: 2016 Transformer Oil Sampling and Analysis · 2016 Transformer Oil Sampling and Analysis June 7, 2016 File: ... Close observation of dissolved gases in the oil, ... 12 2 / OIL-/ ESTER

Cargill Limited

Cargill TerminalFluid Test Report

Maintenance

Fluid Analysis

Moisture Content

(Should be <Limit)

0

5

10

15

20

25

30

Jun

-16

Jun

-15

Pa

rts

Pe

r M

illio

n

Interfacial Tension

(Should be >Limit)

0

5

10

15

20

25

30

35

Jun

-16

Jun

-15

mN

/m

Acid Number

(Should <Limit)

0

0.02

0.04

0.06

0.08

0.1

0.12

0.14

0.16

Jun

-16

Jun

-15

mg

KO

H/g

Color Number

(Should be <Limit)

0

0.5

1

1.5

2

2.5

3

3.5

4

Jun

-16

Jun

-15

Dielectric Breakdown D877

(Should be >Limit)

Actual Values

Acceptable Limits

Dielectric Breakdown D1816

(Should be >Limit)

0

5

10

15

20

25

30

35

40

45

Jun

-16

Jun

-15

kV

Page 3 of 3Serial Number: 293638Magna IV Engineering

Page 19: 2016 Transformer Oil Sampling and Analysis · 2016 Transformer Oil Sampling and Analysis June 7, 2016 File: ... Close observation of dissolved gases in the oil, ... 12 2 / OIL-/ ESTER

/

WEIGHT

TEMP RISE

PSI

PO# for Sampling Lab:

REPORT RUSH:

� DGA D3612C � Dielectric 1.0mm D1816 Oxidation Inhibitor D2668 NOTES:

� Moisture in Oil D1533B Dielectric 2.0mm D1816 Furfurals (paper degradation) 1. NO WINDING TEMP GAUGE

� Interfacial Tension D971 Power Factor 25°C D924 Metals D3635ICP TRANSFORMER IS IN VAULT.

� Acid Number D974 Power Factor 100°C D924 Viscosity D88 2. IMPERIAL GALLONS

� Color/Visual D1500, D1524 Specific Gravity D1298 Other:

Dielectric 2.5mm D877 PCB

OIL TYPE MINERAL SYSTEM BREATHING

DATE OF LAST OIL CHANGE (IF KNOWN) UNKNOWN

NAMEPLATE DATA

June 7, 2016

PCB CONTAMINATED

# OF TAPS

TAP FOUND/LEFT

YES

5EQUIPMENT TX KVA 4000

MANUF.

YEAR 1967

3.70%TYPE

LEMON YELLOW

STRAW YELLOW

STRAW WHITE

BROWN

REDDISH ORANGE

ORANGE BLACK

OTHER:

PREPARED FOR

CARGILL

AREA

SITE

WO#

MAIN SUB

CARGILL TERMINAL

C3330-10 DATE

TEST BY

APPROVED BY

WEST TX

JMP

STANDARD MAINTENANCE

OIL FILLED EQUIPMENT INSPECTION SHEETTAG #

CANF-5E006

ONAN SEC VOLTS 575 %IMPED

WESTINGHOUSE PRI VOLTS 72KV 3 3

SO# 293638 AMPS

PRE-SAMPLING CHECKLIST

CAPACITY GALSLTRS

NO

RESET GAUGE

OIL LEVEL

PRESSURE

GAUGE READING DRAGHAND

OIL TEMP

N/A

SAMPLE COLOR

SAMPLE DATA

NO

YES / NOWINDING TEMP

Tests Required (Internal Purposes Only)

CRITERIAYES

Sampler: JMP

78 %

26.0 °C

BOTTOM VALVE

Syringe #:

KPA

READING

SEE DIAGRAM AT RIGHT

HUMIDITY

AMB. TEMP

SEDIMENT

SAMPLE POINT

� OK

NO

INSPECTIONS

CRITERIA

ADEQUATE CLEARANCE

TANK PRESSURE (Min: -1 Psi (-6.89 kPa))

LOW OIL LEVEL (GAUGE @ LOW)

LV BUSHINGS ACCESSIBLE

CO 376 1006975

RADIATOR CONDITION N/A

40 °C

� SILICA DESICANT CONDITION �

NO

DIRT ACCUMULATION

750

PROPER LEVEL

NO

OIL LEAKS (WHERE)

DUSTY

FAIL

CORROSION / RUST ACCUMULATION � PAINT IS GOOD

� DUSTY

COMMENTS

6 PPM

LV BUSHING CONDITION �

35 °C

COMMENTS

NITROGEN ADDED

NO

RADIATORS INSTALLED

CONSERVATOR TANK

BLUE

HV BUSHINGS ACCESSIBLE HV BUSHING CONDITION �

RELIEF VALVE INSTALLED

GROUNDING (2 LOCATIONS) �

PHYSICAL DAMAGE

BREATHERS

GAUGE DOCUMENTATION

DESCRIPTION YES DESCRIPTION OK

DUSTY

West Tx Oil Filled Equipment Inspection Page 1 of 1

Page 20: 2016 Transformer Oil Sampling and Analysis · 2016 Transformer Oil Sampling and Analysis June 7, 2016 File: ... Close observation of dissolved gases in the oil, ... 12 2 / OIL-/ ESTER

Cargill Terminal

Sub 2

S/N: 1059001354

C3330-10

Oil & Gas Results

Nameplate Information

Page 21: 2016 Transformer Oil Sampling and Analysis · 2016 Transformer Oil Sampling and Analysis June 7, 2016 File: ... Close observation of dissolved gases in the oil, ... 12 2 / OIL-/ ESTER

Cargill Limited

Cargill TerminalFluid Test Report

Maintenance

Nameplate Information

Serial Number: 1059001354

Sample Date:

Job Number:

Nitrogen (N₂)

Total Dissolved Combustible Gas

Total Gas Content (%)

kVA Rating: 3000

Fluid Type: ESTER

Designation: Sub 2kV Rating: 12.400/0.575

Dissolved Gas Analysis

Fluid Quality Analysis Limits

Additional Fluid Quality Tests

Notes:

D3612-C

Apparatus Type: TRN Manufacturer: COOPER

Year Manufactured: 2010 Fluid Capacity (L): 1250

Expressed in PPM

Voltage Class ≤69kV

Hydrogen (H₂)

Methane (CH₄)

Ethane (C₂H₆)

Ethylene (C₂H₄)

Acetylene (C₂H₂)

Carbon Monoxide (CO)

Carbon Dioxide (CO₂)

100

120

65.0

50.0

2.0

1000

10000

Limits

Moisture Content D1533 (ppm)

Interfacial Tension D971 (mN/m)

Acid Number D974 (mg KOH/g)

Color Number D1500 (Relative)

Visual Examination D1524 (Relative)

Dielectric Breakdown @ 1mm D1816 (kV)

Dielectric Breakdown D877 (kV)

35

25.0

0.200

3.5

CLEAR

23

26

PCB D4059 (ppm)

Specific Gravity D4052 (Relative)

Power Factor @ 25°C D924 (%)

Oxidation Inhibitor D2668 (%)

2.0

0.91

0.5

0.08 - 0.3

Limits

Power Factor @ 100°C D924 (%) 5.0

Oxygen (O₂)

12

23.3

37

0.020

CLEAR

15

22.9

47

0.024

CLEAR

36

1500

67600

6

36

310

192.9

6.3

0.0

277

6.970

36

2400

66000

6

38

330

195.6

8.2

0.0

284

6.900

Jun-7-2016

C3330-10

Jun-10-2015

C3330-7

- <0.5

Limits based on Mineral Oil Insulating Fluid.

All Results considered normal for Natural Ester Insulating Fluid.

07/06/2016 :

Page 1 of 3Serial Number: 1059001354Magna IV Engineering

Page 22: 2016 Transformer Oil Sampling and Analysis · 2016 Transformer Oil Sampling and Analysis June 7, 2016 File: ... Close observation of dissolved gases in the oil, ... 12 2 / OIL-/ ESTER

Cargill Limited

Cargill TerminalFluid Test Report

Maintenance

Historic Graphs and Diagnostic Charts

Combustible Gases

Total Gas Content (%)

(All Gases)

0

1

2

3

4

5

6

7

8

Ju

n-1

6

Ju

n-1

5

Key Gas Comparison (ppm)

0

50

100

150

200

250

CO - H2 - Meth - Eth - Ethy - Ace

Methane (CH4)

0

1

2

3

4

5

6

7

Ju

n-1

6

Ju

n-1

5

Pa

rts

Pe

r M

illio

n

Ethane (C2H6)

0

50

100

150

200

250

Ju

n-1

6

Ju

n-1

5

Pa

rts

Pe

r M

illio

n

Acetylene (C2H2)

0

0.1

0.2

0.3

0.4

0.5

0.6

0.7

0.8

0.9

1

Ju

n-1

6

Ju

n-1

5

Pa

rts

Pe

r M

illio

n

Ethylene (C2H4)

0

1

2

3

4

5

6

7

8

9

Ju

n-1

6

Ju

n-1

5

Pa

rts

Pe

r M

illio

n

Hydrogen (H2)

0

5

10

15

20

25

30

35

40

Ju

n-1

6

Ju

n-1

5

Pa

rts

Pe

r M

illio

n

Carbon Monoxide (CO)

0

5

10

15

20

25

30

35

40

Ju

n-1

6

Ju

n-1

5

Pa

rts

Pe

r M

illio

n

Non-Combustible Gases

Carbon Dioxide (CO2)

0

50

100

150

200

250

300

350

Ju

n-1

6

Ju

n-1

5

Pa

rts

Pe

r M

illio

n

Nitrogen (N2)

0

10

20

30

40

50

60

70

80

Ju

n-1

6

Ju

n-1

5

Thousands

Pa

rts

Pe

r M

illio

n

Oxygen (O2)

0

0.5

1

1.5

2

2.5

3

Ju

n-1

6

Ju

n-1

5

Thousands

Pa

rts

Pe

r M

illio

n

Page 2 of 3Serial Number: 1059001354Magna IV Engineering

Page 23: 2016 Transformer Oil Sampling and Analysis · 2016 Transformer Oil Sampling and Analysis June 7, 2016 File: ... Close observation of dissolved gases in the oil, ... 12 2 / OIL-/ ESTER

Cargill Limited

Cargill TerminalFluid Test Report

Maintenance

Fluid Analysis

Moisture Content

(Should be <Limit)

0

5

10

15

20

25

30

35

40

Jun

-16

Jun

-15

Pa

rts

Pe

r M

illio

n

Interfacial Tension

(Should be >Limit)

0

5

10

15

20

25

30

Jun

-16

Jun

-15

mN

/m

Acid Number

(Should be <Limit)

0

0.05

0.1

0.15

0.2

0.25

Jun

-16

Jun

-15

mg

KO

H/g

Color Number

(Should be <Limit)

Dielectric Breakdown D877

(Should be >Limit)

Actual Values

Acceptable Limits

Dielectric Breakdown D1816

(Should be >Limit)

0

5

10

15

20

2530

35

40

45

50

Jun

-16

Jun

-15

kV

Page 3 of 3Serial Number: 1059001354Magna IV Engineering

Page 24: 2016 Transformer Oil Sampling and Analysis · 2016 Transformer Oil Sampling and Analysis June 7, 2016 File: ... Close observation of dissolved gases in the oil, ... 12 2 / OIL-/ ESTER

/

WEIGHT

TEMP RISE

PSI

PO# for Sampling Lab:

REPORT RUSH:

� DGA D3612C � Dielectric 1.0mm D1816 Oxidation Inhibitor D2668 NOTES:

� Moisture in Oil D1533B Dielectric 2.0mm D1816 Furfurals (paper degradation) 1. NO WINDING TEMP GAUGE

� Interfacial Tension D971 Power Factor 25°C D924 Metals D3635ICP TRANSFORMER IS IN A VAULT

� Acid Number D974 Power Factor 100°C D924 Viscosity D88

� Color/Visual D1500, D1524 Specific Gravity D1298 Other:

Dielectric 2.5mm D877 PCB

OIL TYPE FR3 SYSTEM BREATHING

DATE OF LAST OIL CHANGE (IF KNOWN) NEW TRANSFORMER

NAMEPLATE DATA

June 7, 2016

PCB CONTAMINATED

# OF TAPS

TAP FOUND/LEFT

YES

5EQUIPMENT TX KVA 3000

MANUF.

YEAR 2010

TYPE

LEMON YELLOW

STRAW YELLOW

STRAW WHITE

BROWN

REDDISH ORANGE

ORANGE BLACK

OTHER:

PREPARED FOR

CARGILL

AREA

SITE

WO#

SUB 2

CARGILL TERMINAL

C3330-10 DATE

TEST BY

APPROVED BY

SUBSTATION 2

SB

STANDARD MAINTENANCE

OIL FILLED EQUIPMENT INSPECTION SHEETTAG #

CANF-5E006

ONAN SEC VOLTS 575 %IMPED

COOPER PRI VOLTS 12.4Kv 3 3

SO# 1059001354 AMPS

PRE-SAMPLING CHECKLIST

CAPACITY GALSLTRS

NO

RESET GAUGE

OIL LEVEL

PRESSURE

GAUGE READING DRAGHAND

OIL TEMP

N/A

SAMPLE COLOR

SAMPLE DATA

NO

YES / NOWINDING TEMP

Tests Required (Internal Purposes Only)

CRITERIAYES

Sampler: SB

40 %

26.0 °C

BOTTOM VALVE

Syringe #:

KPA

READING

SEE DIAGRAM AT RIGHT

1

HUMIDITY

AMB. TEMP

SEDIMENT

SAMPLE POINT

� OK

NO

INSPECTIONS

CRITERIA

ADEQUATE CLEARANCE

TANK PRESSURE (Min: -1 Psi (-6.89 kPa))

LOW OIL LEVEL (GAUGE @ LOW)

LV BUSHINGS ACCESSIBLE

DS 264 1006975

RADIATOR CONDITION � OK

40 °C

SILICA DESICANT CONDITION

NO

DIRT ACCUMULATION

1250

PROPER LEVEL

NO

OIL LEAKS (WHERE)

FAIL

CORROSION / RUST ACCUMULATION � PAINT IS GOOD

� DUSTY

COMMENTS

UNKNOWN

LV BUSHING CONDITION

40 °C

COMMENTS

NITROGEN ADDED

NO

RADIATORS INSTALLED

CONSERVATOR TANK

NOT USED

HV BUSHINGS ACCESSIBLE HV BUSHING CONDITION

RELIEF VALVE INSTALLED

GROUNDING (2 LOCATIONS) �

PHYSICAL DAMAGE

BREATHERS

GAUGE DOCUMENTATION

DESCRIPTION YES DESCRIPTION OK

Substation 2 Oil Filled Equipment Inspection Page 1 of 1

Page 25: 2016 Transformer Oil Sampling and Analysis · 2016 Transformer Oil Sampling and Analysis June 7, 2016 File: ... Close observation of dissolved gases in the oil, ... 12 2 / OIL-/ ESTER

Cargill Terminal6OCB1

S/N: 60503

C3330-10Oil & Gas Results

Nameplate Information

Page 26: 2016 Transformer Oil Sampling and Analysis · 2016 Transformer Oil Sampling and Analysis June 7, 2016 File: ... Close observation of dissolved gases in the oil, ... 12 2 / OIL-/ ESTER

Cargill LimitedCargill Terminal

Fluid Test ReportMaintenance

Nameplate InformationSerial Number: 60503

Sample Date:

Job Number:

Nitrogen (N₂)Total Dissolved Combustible Gas

Total Gas Content (%)

kVA Rating:Fluid Type: OIL

Designation: 6OCB1kV Rating: 72.000

Dissolved Gas Analysis

Fluid Quality Analysis Limits

Additional Fluid Quality Tests

Notes:

D3612-C

Apparatus Type: OCB Manufacturer: GEYear Manufactured: 1967 Fluid Capacity (G): 575

Expressed in PPM

Voltage Class >69kV - <230kV

Hydrogen (H₂)Methane (CH₄)Ethane (C₂H₆)Ethylene (C₂H₄)Acetylene (C₂H₂)Carbon Monoxide (CO)

Carbon Dioxide (CO₂)

100

120

65.0

50.0

2.0

1000

10000

Limits

Moisture Content D1533 (ppm)

Interfacial Tension D971 (mN/m)

Acid Number D974 (mg KOH/g)

Color Number D1500 (Relative)

Visual Examination D1524 (Relative)

Dielectric Breakdown @ 1mm D1816 (kV)

Dielectric Breakdown D877 (kV)

25

30.0

0.150

3.5

CLEAR

28

26

PCB D4059 (ppm)

Specific Gravity D4052 (Relative)

Power Factor @ 25°C D924 (%)

Oxidation Inhibitor D2668 (%)

2.0

0.91

0.5

0.08 - 0.3

Limits

Power Factor @ 100°C D924 (%) 5.0

Oxygen (O₂)

32.0

32

0.022

L1.5

CLEAR

32.5

36

0.025

1.5

CLEAR

0

30300

65500

1

25

560

0.0

0.8

0.0

27

9.630

1

27400

63900

1

31

580

0.0

0.7

0.0

34

9.200

Jun-7-2016

C3330-10

Jun-10-2015

C3330-7

- <0.5

All results considered normal for OCB operation2016-06-07 :

Page 1 of 3Serial Number: 60503Magna IV Engineering

Page 27: 2016 Transformer Oil Sampling and Analysis · 2016 Transformer Oil Sampling and Analysis June 7, 2016 File: ... Close observation of dissolved gases in the oil, ... 12 2 / OIL-/ ESTER

Cargill LimitedCargill Terminal

Fluid Test ReportMaintenance

Historic Graphs and Diagnostic Charts

Combustible Gases

Total Gas Content (%)(All Gases)

0

2

4

6

8

10

12

Jun-

16

Jun-

15

Key Gas Comparison (ppm)

0

5

10

15

20

25

30

CO - H2 - Meth - Eth - Ethy - Ace

Methane (CH4)

0

0.2

0.4

0.6

0.8

1

1.2

Jun-

16

Jun-

15

Parts

Per

Milli

on

Ethane (C2H6)

0

0.2

0.4

0.6

0.8

1

Jun-

16

Jun-

15

Parts

Per

Milli

on

Acetylene (C2H2)

00.10.20.30.40.50.60.70.80.9

1

Jun-

16

Jun-

15

Parts

Per

Milli

on

Ethylene (C2H4)

00.10.20.30.40.50.60.70.80.9

Jun-

16

Jun-

15

Parts

Per

Milli

on

Hydrogen (H2)

0

0.2

0.4

0.6

0.8

1

1.2

Jun-

16

Jun-

15

Parts

Per

Milli

on

Carbon Monoxide (CO)

0

5

10

15

20

25

30

35

Jun-

16

Jun-

15

Parts

Per

Milli

on

Non-Combustible GasesCarbon Dioxide (CO2)

0

100

200

300

400

500

600

700

Jun-

16

Jun-

15

Parts

Per

Milli

on

Nitrogen (N2)

0

10

20

30

40

50

60

70

Jun-

16

Jun-

15

Thousands

Parts

Per

Milli

on

Oxygen (O2)

0

5

10

15

20

25

30

35

Jun-

16

Jun-

15

Thousands

Parts

Per

Milli

on

Page 2 of 3Serial Number: 60503Magna IV Engineering

Page 28: 2016 Transformer Oil Sampling and Analysis · 2016 Transformer Oil Sampling and Analysis June 7, 2016 File: ... Close observation of dissolved gases in the oil, ... 12 2 / OIL-/ ESTER

Cargill LimitedCargill Terminal

Fluid Test ReportMaintenance

Fluid AnalysisMoisture Content

(Should be <Limit)Interfacial Tension(Should be >Limit)

0

5

10

15

20

25

30

35

Jun-

16

Jun-

15

mN

/m

Acid Number(Should <Limit)

00.020.040.060.080.1

0.120.140.16

Jun-

16

Jun-

15

mg

KOH/

g

Color Number(Should be <Limit)

0

0.51

1.5

2

2.53

3.5

4

Jun-

16

Jun-

15

Dielectric Breakdown D877(Should be >Limit)

Actual ValuesAcceptable Limits

Dielectric Breakdown D1816(Should be >Limit)

05

10152025303540

Jun-

16

Jun-

15

kV

Page 3 of 3Serial Number: 60503Magna IV Engineering

Page 29: 2016 Transformer Oil Sampling and Analysis · 2016 Transformer Oil Sampling and Analysis June 7, 2016 File: ... Close observation of dissolved gases in the oil, ... 12 2 / OIL-/ ESTER

/

WEIGHT

TEMP RISE

PSI

PO# for Sampling Lab:

REPORT RUSH:

� DGA D3612C � Dielectric 1.0mm D1816 Oxidation Inhibitor D2668 NOTES:

� Moisture in Oil D1533B Dielectric 2.0mm D1816 Furfurals (paper degradation)

� Interfacial Tension D971 Power Factor 25°C D924 Metals D3635ICP

� Acid Number D974 Power Factor 100°C D924 Viscosity D88

� Color/Visual D1500, D1524 Specific Gravity D1298 Other:

Dielectric 2.5mm D877 PCB

OIL TYPE MINERAL SYSTEM BREATHING

DATE OF LAST OIL CHANGE (IF KNOWN) UNKNOWN

NAMEPLATE DATA

June 7, 2016

PCB CONTAMINATED

# OF TAPS

TAP FOUND/LEFT

YES

N/AEQUIPMENT OCB KVA

MANUF.

N/AYEAR 1967

N/ATYPE

LEMON YELLOW

STRAW YELLOW

STRAW WHITE

BROWN

REDDISH ORANGE

ORANGE BLACK

OTHER:

PREPARED FOR

CARGILL

AREA

SITE

WO#

MAIN SUB

CARGILL TERMINAL

C3330-10 DATE

TEST BY

APPROVED BY

6 OCB1

JMP

STANDARD MAINTENANCE

OIL FILLED EQUIPMENT INSPECTION SHEETTAG #

CANF-5E006

WSO SEC VOLTS %IMPED

GE PRI VOLTS 72KV

SO# 60503 AMPS 1200

PRE-SAMPLING CHECKLIST

CAPACITY GALSLTRS

NO

RESET GAUGE

OIL LEVEL

PRESSURE

GAUGE READING DRAGHAND

OIL TEMP

SAMPLE COLOR

SAMPLE DATA

YES / NO

YES / NOWINDING TEMP

Tests Required (Internal Purposes Only)

CRITERIAYES

Sampler: JMP

78 %

23.0 °C

BOTTOM VALVE

Syringe #:

KPA

READING

SEE DIAGRAM AT RIGHT

HUMIDITY

AMB. TEMP

SEDIMENT

SAMPLE POINT

� OK

NO

INSPECTIONS

CRITERIA

ADEQUATE CLEARANCE

TANK PRESSURE (Min: -1 Psi (-6.89 kPa))

LOW OIL LEVEL (GAUGE @ LOW)

LV BUSHINGS ACCESSIBLE

DS 901 1006975

RADIATOR CONDITION N/A

� SILICA DESICANT CONDITION

YES / NO

DIRT ACCUMULATION

575

NO GAUGE

NO

OIL LEAKS (WHERE)

SOME CHIPS

FAIL

CORROSION / RUST ACCUMULATION � PAINT IS POOR

� NONE VISIBLE

COMMENTS

< 0.5 PPM

LV BUSHING CONDITION

26 °C

COMMENTS

NITROGEN ADDED

NO

RADIATORS INSTALLED

CONSERVATOR TANK

NOT USED

HV BUSHINGS ACCESSIBLE HV BUSHING CONDITION

RELIEF VALVE INSTALLED

GROUNDING (2 LOCATIONS) �

PHYSICAL DAMAGE

BREATHERS

GAUGE DOCUMENTATION

DESCRIPTION YES DESCRIPTION OK

N/A

6 OCB1 Oil Filled Equipment Inspection Page 1 of 1


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