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6390 Joyce Drive # 100 Golden, CO 80403 Phone 303-940-0033 Fax 866-283-0269 www.phenova.com October 16, 2020 Mrs. Erin Briggs Bio-Analytical Laboratories 3240 Spurgin Road Doyline, LA 71023 USA Dear Erin, Thank you for participating in the DMRQA40-WET DMRQA PT Study. Enclosed is your final report, which has been carefully reviewed by the PT specialists at Phenova. For any analyte falling outside the established acceptance limits, our PT management staff would like to assist you in determining the most appropriate course of corrective action for your facility. Please contact us at any time if we may be of service to you. A final report for your laboratory will be sent to all accrediting agencies you requested at the time of data submittal. Thank you again for participating in the DMRQA40-WET DMRQA PT Study. We appreciate working with you and look forward to our next study. If you have any questions, please call us at 303-940-0033.
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Page 1: 6390 Joyce Drive Phone 303-940-0033

6390 Joyce Drive

# 100

Golden, CO 80403

Phone 303-940-0033

Fax 866-283-0269

www.phenova.com

October 16, 2020

Mrs. Erin BriggsBio-Analytical Laboratories3240 Spurgin RoadDoyline, LA 71023USA

Dear Erin,

Thank you for participating in the DMRQA40-WET DMRQA PT Study. Enclosed is your finalreport, which has been carefully reviewed by the PT specialists at Phenova.

For any analyte falling outside the established acceptance limits, our PT management staffwould like to assist you in determining the most appropriate course of corrective action foryour facility. Please contact us at any time if we may be of service to you. A final reportfor your laboratory will be sent to all accrediting agencies you requested at the time ofdata submittal.

Thank you again for participating in the DMRQA40-WET DMRQA PT Study. We appreciateworking with you and look forward to our next study. If you have any questions, please callus at 303-940-0033.

Page 2: 6390 Joyce Drive Phone 303-940-0033

6390 Joyce Drive

# 100

Golden, CO 80403

Report Definitions:

Phone 303-940-0033

Fax 866-283-0269

www.phenova.com

The Assigned Value is determined from the study mean, gravimetric

and volumetric true concentration of an analyte to be analyzed,

calculation and/or an appropriate reference value as stipulated in the

EPA National Standards for Water Proficiency Testing Studies Criteria

Document (current version), the National Environmental Laboratory

Accreditation Conference (NELAC) criteria (ref: NELAC FOT tables,

NELAC PT Committee) and other documents distributed by accrediting

agencies as applicable.

Assigned Value

Evaluation Limits Acceptance Limits are derived from fixed limits, coefficients, constants

and calculations stipulated in the EPA National Standards for Water

Proficiency Testing Studies Criteria Documents (current version), the

National Environmental Laboratory Accreditation Conference (NELAC)

criteria (ref: NELAC PT FOT tables, NELAC PT Committee) and other

documents distributed by accrediting agencies as applicable.

Evaluation

Acceptable The reported value falls within the Acceptance Limits.

No Evaluation

NR

The reported value is non-numeric and can not be evaluated.

As required by the NELAC standards and requested by state

authorities, any analyte purchased but not reported by your facility is

listed as NR (Not Reported).

Not Acceptable The reported value falls outside the Acceptance Limits.

This report must not be reproduced except in full, without the written approval of Phenova.

This report must not be used to claim product certification, approval, or endorsement by the American Association for Laboratory

Accreditation (A2LA) or any agency of the federal government.

Page 3: 6390 Joyce Drive Phone 303-940-0033

6390 Joyce Drive

# 100

Golden, CO 80403

Final Report - DMRQA PT

Study: DMRQA40-WET

Facility: Contact:

EPA Lab ID: LA00917

Bio-Analytical Laboratories

3240 Spurgin Road

Doyline, LA 71023

USA

Mrs. Erin Briggs, Technical Director

(318) 745-2772

Opening Date: March 20, 2020 - Closing Date: September 18, 2020

NPDES Permit ID:

Phone 303-940-0033

Fax 866-283-0269

www.phenova.com

Fathead Minnow Method 13 (PT-13-WET) Lot #: 8548-13NELAC

Code

Analyte Method Code Units Assigned

Value

Result Acceptance

Limits

EvaluationMethod Description

3410 Fathead Minnow Acute MHSF 25° - LC50 EPA 2000.0 - Fathead

Minnow Acute Toxicity

2002

S.U. 38.0 17.68 25.7 - 50.4 Not Acceptable10264809

Fathead Minnow Method 15 (PT-15-WET) Lot #: 8548-15NELAC

Code

Analyte Method Code Units Assigned

Value

Result Acceptance

Limits

EvaluationMethod Description

3410 Fathead Minnow Chronic MHSF - Survival NOEC EPA 1000.0 - Fathead

Minnow Chronic Toxicity

2002

S.U. 50 50.0 25 - 100 Acceptable10252605

3410 Fathead Minnow Chronic MHSF - Growth IC25 (ON) EPA 1000.0 - Fathead

Minnow Chronic Toxicity

2002

S.U. 46.1 41.75 25.5 - 66.8 Acceptable10252605

3410 Fathead Minnow Chronic MHSF - Growth NOEC (ON) EPA 1000.0 - Fathead

Minnow Chronic Toxicity

2002

S.U. 25 25.0 12.5 - 50 Acceptable10252605

Ceriodaphnia Method 19 (PT-19-WET) Lot #: 8548-19NELAC

Code

Analyte Method Code Units Assigned

Value

Result Acceptance

Limits

EvaluationMethod Description

3315 Ceriodaphnia Acute MHSF 25° - LC50 EPA 2002.0 -

Ceriodaphnia Acute

Toxicity 2002

S.U. 39.9 45.06 17.3 - 62.4 Acceptable10214581

Report Issue Date - 10/16/2020 Page 1 of 3

Page 4: 6390 Joyce Drive Phone 303-940-0033

6390 Joyce Drive

# 100

Golden, CO 80403

Final Report - DMRQA PT

Study: DMRQA40-WET

Facility: Contact:

EPA Lab ID: LA00917

Bio-Analytical Laboratories

3240 Spurgin Road

Doyline, LA 71023

USA

Mrs. Erin Briggs, Technical Director

(318) 745-2772

Opening Date: March 20, 2020 - Closing Date: September 18, 2020

NPDES Permit ID:

Phone 303-940-0033

Fax 866-283-0269

www.phenova.com

Ceriodaphnia Method 21 (PT-21-WET) Lot #: 8548-21NELAC

Code

Analyte Method Code Units Assigned

Value

Result Acceptance

Limits

EvaluationMethod Description

3315 Ceriodaphnia Chronic MHSF - Survival NOEC EPA 1002.0 -

Ceriodaphnia dubia

Chronic Toxicity

S.U. 25 12.5 12.5 - 50 Acceptable10253006

3315 Ceriodaphnia Chronic MHSF - Reproduction IC25 EPA 1002.0 -

Ceriodaphnia dubia

Chronic Toxicity

S.U. 26.5 22.44 15.1 - 37.9 Acceptable10253006

3315 Ceriodaphnia Chronic MHSF - Reproduction NOEC EPA 1002.0 -

Ceriodaphnia dubia

Chronic Toxicity

S.U. 25 12.5 12.5 - 50 Acceptable10253006

Daphnia Method 32 (PT-32-WET) Lot #: 8548-32NELAC

Code

Analyte Method Code Units Assigned

Value

Result Acceptance

Limits

EvaluationMethod Description

3350 Daphnia Magna Acute MHSF 25° - LC50 EPA 2021 Daphnia

magna Acute MHSF

S.U. 58.0 69.11 32.6 - 83.3 Acceptable10215415

Daphnia Method 38 (PT-38-WET) Lot #: 8548-38NELAC

Code

Analyte Method Code Units Assigned

Value

Result Acceptance

Limits

EvaluationMethod Description

3355 Daphnia Pulex Acute MHSF 25° - LC50 EPA 2021 Daphnia

pulex Acute MHSF

S.U. 60.4 53.19 43.8 - 76.9 Acceptable10215619

Mysid Method 42 (PT-42-WET) Lot #: 8548-42NELAC

Code

Analyte Method Code Units Assigned

Value

Result Acceptance

Limits

EvaluationMethod Description

3395 Mysid Acute SSW 25° - LC50 EPA 2007.0 - Mysid

Acute Toxicity 2002

S.U. 37.6 28.98 <6.25 - 70.2 Acceptable10216010

Report Issue Date - 10/16/2020 Page 2 of 3

Page 5: 6390 Joyce Drive Phone 303-940-0033

6390 Joyce Drive

# 100

Golden, CO 80403

Final Report - DMRQA PT

Study: DMRQA40-WET

Facility: Contact:

EPA Lab ID: LA00917

Bio-Analytical Laboratories

3240 Spurgin Road

Doyline, LA 71023

USA

Mrs. Erin Briggs, Technical Director

(318) 745-2772

Opening Date: March 20, 2020 - Closing Date: September 18, 2020

NPDES Permit ID:

Phone 303-940-0033

Fax 866-283-0269

www.phenova.com

Menidia Method 44 (PT-44-WET) Lot #: 8548-44NELAC

Code

Analyte Method Code Units Assigned

Value

Result Acceptance

Limits

EvaluationMethod Description

3380 Menidia Acute SSW 25° - LC50 EPA 2006.0 - Inland

Silverside, 48-hr Acute,

nonrenewal,

40-fathoms SW 25°C

2002

S.U. 42.2 35.36 28.8 - 55.6 Acceptable10216407

Sheepshead Minnow Method 46 (PT-46-WET) Lot #: 8548-46NELAC

Code

Analyte Method Code Units Assigned

Value

Result Acceptance

Limits

EvaluationMethod Description

3345 Sheepshead Minnow Acute SSW 25° - LC50 EPA 2004.0 -

Sheepshead Minnow

Acute Toxicity 2002

S.U. 25.6 17.68 7.96 - 43.3 Acceptable10216612

Report Issue Date - 10/16/2020 Page 3 of 3

Page 6: 6390 Joyce Drive Phone 303-940-0033

Erin Ginger BriggsBio-Analytical Laboratories3240 Spurgin RdDoyline, LA 71023USA

102320N Final Report

Project # :102320N

Ver. 1Page 1 of 7

Page 7: 6390 Joyce Drive Phone 303-940-0033

November 1, 2020

Erin Ginger BriggsBio-Analytical Laboratories3240 Spurgin RdDoyline, LA 71023

Fax: 318-745-2773

Enclosed is your final report for ERA's QuiK™Response program. Your final report includes an evaluation of all results submitted by your laboratory to ERA. The assigned value(s) and acceptance limits were not available to your laboratory at or before the time of reporting. All analytes in ERA's QuiK™Response program are evaluated using the following tiered approach. If the analyte is listed in the most current TNI Fields of Proficiency Testing (FoPT) tables the evaluation was completed by comparing the reported result to the acceptance limits generated using the criteria contained in the tables and the evaluation criteria contained in the 2016 TNI Standard, Volume 3. If the analyte is not included in the TNI FoPT tables, the reported result has been evaluated using the procedures outlined in ERA's Standard Operating Procedure for the Generation of Performance Acceptance Limits (SOP 730002268). All analytes are included in ERA's A2LA accreditation, certification number 1539.01.

All activities associated with this QuiK™Response project were performed by Waters/ERA with the exception of these samples/products which were manufactured for Waters/ERA by a subcontractor: Microbiology products with the following catalog numbers; 081, 084, 085, 078, 078A, 083, 083A and Volatiles in Gas Cylinder, catalog number 1100. As part of your accreditation(s), you may be required to identify the root cause of any "Not Acceptable" results, implement the necessary corrective actions, and then satisfy your PT requirements by participating in a supplemental (QuiK™Response) or future ERA PT study. ERA's technical staff is available to help your laboratory resolve any technical issues that may be impairing your PT performance and possibly affecting the quality of your routine data.

The data contained herein are confidential and intended for your use only.

If you are using this report for DMRQA Corrective Action, please note the following: permittees must submit a copy of this report to your DMR-QA Coordinator, along with your corrective action documentation. Contract Laboratories should send a copy of this report to your permittees upon receipt.

Thank you for your participation in ERA's QuiK™Response program. If you have any questions, please contact our Proficiency Testing Department at 1-800-372-0122.

Sincerely,

Matthew SeebeckQuality Officer

cc: Project File Number 102320N

16341 Table Mountain Pkwy • Golden, CO 80403 • 800.372.0122 • 303.431.8454 • fax 303.421.0159 • www.eraqc.com Project # : 102320N

Ver. 1Page 2 of 7

Page 8: 6390 Joyce Drive Phone 303-940-0033

Report Recipient Contact/Phone Number Reporting Type

No Recipients Selected

Project # : 102320N

Ver. 1Page 3 of 7

Page 9: 6390 Joyce Drive Phone 303-940-0033

Not Acceptable EvaluationsThere were no Not Acceptable evaluations for this study.

16341 Table Mountain Pkwy • Golden, CO 80403 • 800.372.0122 • 303.431.8454 • fax 303.421.0159 • www.eraqc.com Project # : 102320N

This report is scored by the criteria in the 2016 TNI Standard, Volume 3, instead of by the criteria in the 2009 TNI Standard to which the Proficiency Testing Provider is accredited. This is a planned change and is endorsed by the TNI Proficiency Testing Program Executive Committee for transition to the 2016 TNI Standard.

Erin Ginger BriggsTechnical DirectorBio-Analytical Laboratories3240 Spurgin RdDoyline, LA 71023318-745-2772

EPA ID:ERA Customer Number:

LA00917B353101

102320N Laboratory Exception Report

Ver. 1Page 4 of 7

Page 10: 6390 Joyce Drive Phone 303-940-0033

Final Report Results For Laboratory Bio-Analytical Laboratories

16341 Table Mountain Pkwy • Golden, CO 80403 • 800.372.0122 • 303.431.8454 • fax 303.421.0159 • www.eraqc.com Project # : 102320N

Ver. 1Page 5 of 7

Page 11: 6390 Joyce Drive Phone 303-940-0033

Project Number:

ERA Customer Number:

Laboratory Name:

102320N

B353101

Bio-Analytical Laboratories

WET Results

Final Evaluation Report

16341 Table Mountain Pkwy • Golden, CO 80403 • 800.372.0122 • 303.431.8454 • fax 303.421.0159 • www.eraqc.com Project # : 102320N

Ver. 1Page 6 of 7

Page 12: 6390 Joyce Drive Phone 303-940-0033

Erin Ginger BriggsTechnical DirectorBio-Analytical Laboratories3240 Spurgin RdDoyline, LA 71023318-745-2772

EPA ID:ERA Customer Number:

LA00917B353101

102320N Final Report

AnalyteCode Test End Point Reported

ValueAssigned Value %

Acceptance Limits %

Performance Evaluation Method Description Analysis

Date Z Score Study Mean

Study Standard Deviation

Analyst Name

DMRWet Fathead minnow (Test Code 13) (cat# AQC002, lot# 102320N) Study Dates: 10/23/20 - 11/01/2048Hr., Acute, Non-Renewal, 25° C, MHSFPotassium chloride

0754 LC50 58.50 45.2 24.7 - 65.6 Acceptable 10264809 2002 10/30/2020 1.31 45.2 10.2

16341 Table Mountain Pkwy • Golden, CO 80403 • 800.372.0122 • 303.431.8454 • fax 303.421.0159 • www.eraqc.com Project # : 102320N

This report is scored by the criteria in the 2016 TNI Standard, Volume 3, instead of by the criteria in the 2009 TNI Standard to which the Proficiency Testing Provider is accredited. This is a planned change and is endorsed by the TNI Proficiency Testing Program Executive Committee for transition to the 2016 TNI Standard.

Ver. 1Page 7 of 7


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