ANALYTICAL REPORT 6 - NRC: Home Page · 2017-10-11 · ANALYTICAL REPORT TestAmerica Laboratories,...

ANALYTICAL REPORTTestAmerica Laboratories, Inc.TestAmerica St. Louis13715 Rider Trail NorthEarth City, MO 63045Tel: (314)298-8566

TestAmerica Job ID: 160-15789-1Client Project/Site: HDP

For:Perma-Fix Environmental Services Inc.2800 Solway RoadKnoxville, Tennessee 37931

Attn: Brian Miller

Authorized for release by:1/29/2016 2:39:03 PMRhonda Ridenhower, Manager of Project [email protected] forIvan Vania, Project Manager II(314)[email protected]

This report has been electronically signed and authorized by the signatory. Electronic signature isintended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

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mailto:[email protected]

mailto:[email protected]

Table of ContentsClient: Perma-Fix Environmental Services Inc.Project/Site: HDP

TestAmerica Job ID: 160-15789-1

Page 2 of 46TestAmerica St. Louis

1/29/2016

Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 35QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 41Tracer Carrier Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 46

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Case NarrativeClient: Perma-Fix Environmental Services Inc. TestAmerica Job ID: 160-15789-1Project/Site: HDP

Job ID: 160-15789-1

Laboratory: TestAmerica St. Louis

Narrative

CASE NARRATIVE

Client: Perma-Fix Environmental Services Inc.

Project: HDP

Report Number: 160-15789-1

With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples,

the reporting limits are adjusted relative to the dilution required.

TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the application methods. TestAmerica’s operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data

have been found to be compliant with laboratory protocols unless otherwise noted below.

The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory.

Calculations are performed before rounding to avoid round-off errors in calculated results.

All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.

All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a %

solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the

client.”

This laboratory report is confidential and is intended for the sole use of TestAmerica and its client.

RECEIPT

The samples were received on 01/20/2016; the samples arrived in good condition, properly preserved and on ice. The temperatures of the 4 coolers at receipt time were 18.9º C, 18.9º C, 18.9º C and 18.9º C.

TECHNETIUM-99 (ICPMS)Samples B02-01-01-P-S-S-00 (160-15789-1), B02-01-02-P-R-S-00 (160-15789-2), B02-01-03-P-E-S-00 (160-15789-3),

B02-01-04-P-S-S-00 (160-15789-4), B02-01-05-P-R-S-00 (160-15789-5), B02-01-06-P-E-S-00 (160-15789-6), B02-01-07-P-S-S-00 (160-15789-7), B02-01-08-P-R-S-00 (160-15789-8), B02-01-09-P-E-S-00 (160-15789-9), B02-01-10-P-S-S-00 (160-15789-10),

B02-01-11-P-R-S-00 (160-15789-11), B02-01-12-P-E-S-00 (160-15789-12), B02-01-13-P-S-S-00 (160-15789-13), B02-01-14-P-R-S-00

(160-15789-14), B02-01-15-P-E-S-00 (160-15789-15), B02-01-16-P-S-S-00 (160-15789-16), B02-01-17-P-R-S-00 (160-15789-17), B02-01-18-P-E-S-00 (160-15789-18), B02-01-19-P-S-S-00 (160-15789-19), B02-01-20-P-R-S-00 (160-15789-20), B02-01-21-P-E-S-00

(160-15789-21), B02-01-22-P-S-S-00 (160-15789-22), B02-01-23-P-R-S-00 (160-15789-23), B02-01-24-P-E-S-00 (160-15789-24), B02-01-02-P-R-Q-00 (160-15789-25) and B02-01-10-P-S-Q-00 (160-15789-26) were analyzed for Technetium-99 (ICPMS) in accordance

with EPA SW-846 Method 6020A. The samples were prepared on 01/20/2016 and analyzed on 01/28/2016.

TestAmerica St. LouisPage 3 of 46 1/29/2016

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Case NarrativeClient: Perma-Fix Environmental Services Inc. TestAmerica Job ID: 160-15789-1Project/Site: HDP

Job ID: 160-15789-1 (Continued)

Laboratory: TestAmerica St. Louis (Continued)

No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

PERCENT SOLIDSSamples B02-01-01-P-S-S-00 (160-15789-1), B02-01-02-P-R-S-00 (160-15789-2), B02-01-03-P-E-S-00 (160-15789-3),

B02-01-04-P-S-S-00 (160-15789-4), B02-01-05-P-R-S-00 (160-15789-5), B02-01-06-P-E-S-00 (160-15789-6), B02-01-07-P-S-S-00 (160-15789-7), B02-01-08-P-R-S-00 (160-15789-8), B02-01-09-P-E-S-00 (160-15789-9), B02-01-10-P-S-S-00 (160-15789-10),

B02-01-11-P-R-S-00 (160-15789-11), B02-01-12-P-E-S-00 (160-15789-12), B02-01-13-P-S-S-00 (160-15789-13), B02-01-14-P-R-S-00

(160-15789-14), B02-01-15-P-E-S-00 (160-15789-15), B02-01-16-P-S-S-00 (160-15789-16), B02-01-17-P-R-S-00 (160-15789-17), B02-01-18-P-E-S-00 (160-15789-18), B02-01-19-P-S-S-00 (160-15789-19), B02-01-20-P-R-S-00 (160-15789-20), B02-01-21-P-E-S-00

(160-15789-21), B02-01-22-P-S-S-00 (160-15789-22), B02-01-23-P-R-S-00 (160-15789-23), B02-01-24-P-E-S-00 (160-15789-24), B02-01-02-P-R-Q-00 (160-15789-25) and B02-01-10-P-S-Q-00 (160-15789-26) were analyzed for percent solids in accordance with EPA

Method 160.3 MOD. The samples were analyzed on 01/20/2016.

No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

CESIUM-137 & OTHER GAMMA EMITTERS (GS)Samples B02-01-01-P-S-S-00 (160-15789-1), B02-01-02-P-R-S-00 (160-15789-2), B02-01-03-P-E-S-00 (160-15789-3), B02-01-04-P-S-S-00 (160-15789-4), B02-01-05-P-R-S-00 (160-15789-5), B02-01-06-P-E-S-00 (160-15789-6), B02-01-07-P-S-S-00 (160-15789-7), B02-01-08-P-R-S-00 (160-15789-8), B02-01-09-P-E-S-00 (160-15789-9), B02-01-10-P-S-S-00 (160-15789-10),

B02-01-11-P-R-S-00 (160-15789-11), B02-01-12-P-E-S-00 (160-15789-12), B02-01-13-P-S-S-00 (160-15789-13), B02-01-14-P-R-S-00 (160-15789-14), B02-01-15-P-E-S-00 (160-15789-15), B02-01-16-P-S-S-00 (160-15789-16), B02-01-17-P-R-S-00 (160-15789-17), B02-01-18-P-E-S-00 (160-15789-18), B02-01-19-P-S-S-00 (160-15789-19), B02-01-20-P-R-S-00 (160-15789-20), B02-01-21-P-E-S-00 (160-15789-21), B02-01-22-P-S-S-00 (160-15789-22), B02-01-23-P-R-S-00 (160-15789-23), B02-01-24-P-E-S-00 (160-15789-24), B02-01-02-P-R-Q-00 (160-15789-25) and B02-01-10-P-S-Q-00 (160-15789-26) were analyzed for Cesium-137 & Other Gamma Emitters

(GS) in accordance with DOE GA-01-R. The samples were dried on 01/20/2016, prepared on 01/22/2016 and analyzed on 01/24/2016.

Prep Batch 233605Radium-226 is reported in these samples at the clients request. Radium-226 is reported from the 609.31 keV line of bismuth-214. Because the samples have not had 21-days of ingrowth, the activity for radium-226 is an estimated value and may be biased low. This

bias is caused by the disruption of secular equilibrium between radium-226 and bismuth-214 by the loss of radon-222 during sample preparation. The samples are reported with the MDC achieved. B02-01-21-P-E-S-00 (160-15789-21), B02-01-22-P-S-S-00 (160-15789-22), B02-01-23-P-R-S-00 (160-15789-23), B02-01-24-P-E-S-00 (160-15789-24), B02-01-02-P-R-Q-00 (160-15789-25), B02-01-10-P-S-Q-00 (160-15789-26), (LCS 160-233605/2-A), (MB 160-233605/1-A) and (160-15789-A-21-D DU)

Prep Batch 233602Radium-226 is reported in these samples at the clients request. Radium-226 is reported from the 609.31 keV line of bismuth-214. Because the samples have not had 21-days of ingrowth, the activity for radium-226 is an estimated value and may be biased low. This

bias is caused by the disruption of secular equilibrium between radium-226 and bismuth-214 by the loss of radon-222 during sample preparation. The samples are reported with the MDC achieved. B02-01-01-P-S-S-00 (160-15789-1), B02-01-02-P-R-S-00 (160-15789-2),

B02-01-03-P-E-S-00 (160-15789-3), B02-01-04-P-S-S-00 (160-15789-4), B02-01-05-P-R-S-00 (160-15789-5), B02-01-06-P-E-S-00

(160-15789-6), B02-01-07-P-S-S-00 (160-15789-7), B02-01-08-P-R-S-00 (160-15789-8), B02-01-09-P-E-S-00 (160-15789-9), B02-01-10-P-S-S-00 (160-15789-10), B02-01-11-P-R-S-00 (160-15789-11), B02-01-12-P-E-S-00 (160-15789-12), B02-01-13-P-S-S-00

(160-15789-13), B02-01-14-P-R-S-00 (160-15789-14), B02-01-15-P-E-S-00 (160-15789-15), B02-01-16-P-S-S-00 (160-15789-16), B02-01-17-P-R-S-00 (160-15789-17), B02-01-18-P-E-S-00 (160-15789-18), B02-01-19-P-S-S-00 (160-15789-19), B02-01-20-P-R-S-00

(160-15789-20), (LCS 160-233602/2-A), (MB 160-233602/1-A) and (160-15789-A-1-F DU)

No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.


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TestAmerica St. Louis 13715 Rider Trail North

Earth City, MO 630l!5 phone 314.298.8566 fax

Clie'nt Contact Perrna-Fix Environmental Services 2800 Solway Road Knoxville, TN 37931 (865) 690-0501 Phone (865) 539-9868 FAX Project Na1ne: Hematite Decommissioning Project Site: Westinghouse Hematite, MO p 0#832953

Sample Identification

B02-01-01-P-S-S-OO

802-01-02-P-R-S-DO

802-01-03.-P-E·S-OO

802-01-04-P-s-S-Oo

Chain of Custody Record

Regulatory· Program: Dow ONPDES

Projecti Manager: Brian Miller Tel/Fax: (314) srn-3333

Analysis Turnaround Time 0 CA!!ENDAR DAYS 0 WORKING DAYS

TAT if different from Below

0 2weeks

0 1 week

0 2 days

0 1 day -MU•f'•-

Tiype Sample I Sample I (<>Comp, #of

Date ' Tirrie G=GrabJ Matrix cont.

12131/15 1150 c Soil 1

1/4/16 0925 c Soil 1

1/4/16 0935 c Soil 1

12129/15 0925 c Soil 1

0RCRA 0 Other:

Site Contact: Ellen Jakub Lab Contact: Ivan Vania

~1 ...... ~ z ~ I -- .l!l e z > :;:: - ...... .. Cl

>- c E .5

"' ~ -0 ::c ,gi ~ "' Ci)

,, Q. .... <> ., . .,.. ~"' "':::i () ~ tt ... 0 "'::: VI ..c "' Q. 'O E .. Cl "' fl) Ii "' .. s .5 ..

~ ~· ~ s ti ..c ="' . ~ ;t ... 11. 11. < Q

N x x x N x x x N x x x N x x x

Date: 1/1912016 Carrier: Courier

I I

CJ)

~ U1 -..i 00 co 0 ::r Ill s· ~

Test America THE LEADER IN ENVIRON MENT AL TE:.STlNG

TestAmerica Laboratories, Inc. COC No: 011916-FSS1 __ 1_._ of_3_ COCs

Sampler: For Lab Use Onfy:

Walk-in Client I I Lab Sampling:

Job I SDG No.:

Sample $pecific Notes:

Mark Shaffer

Marl< Shaffer

Mark Shaffer

Mark Shatti:f

802-01-05-P-R-S-OO 12/29/15 1030 c Soil 1 N x x x .------ ··. - -~,: ."f. Mark sn'affer

802-01-06-P-E·S-OO 12/29/15 1035 c Soil 1 N x x x Jahmai Williamis

802-01-07 -P-8·S-OO 12/29/15 1100 c Soil 1 N x x x Jahmai WiUiam5

802-01-08-P-R-S-OO 12/29/15 1130 c Soil 1 N x x x Jahmai Williams

802-01-09-P-E-S-OO 12129/15 1135 c Soil 1 N x x x Jahmal Williams

802-01-10cP-S-8-00 12131/15 1045 c Soil 1 N x x x Brian Miller

802-01-11-P-R-S-OO 12/31/15 1115 c Soil 1 N x x x Chris Chandler

802-01-12-P-E-S-OO 12/31/15 1125 C Soil 1

'~~Ii:<f~~\~~lfgg¥'.~l~i:i;':W,g~~~q~j\;i~~,g~~~ii~qij~%i:>Ji't<%}fi;\t}#?W~~;.11~mlii-'. Possible Hazard Identification: Sample Disposal (A fee may be assessed if samples are retained longer thim 1 month) Are any samples frdm a listed EPA Hazardous' Waste? Please List any EPA Waste Codes for the sample in the Comments• Section if the lab is to dispose of the sample.

0 Non-Hazard O Flammable 0 Skin InitBnt 0 Poison B 0 Unknown 0 Return to Oient 0 Disposal by Lab 0 ArthiVe fa- Months

Special Instructions/QC Requirements & Comments: Potential for Radiologil::al Contamination

Custody Seals Intact: 0 Yes ....-.0 No

Re~~~~~(7,~M3 ~~ l~y:<-/

~ Cvrai~

Custody Seal No. :

c~_ pany: ~/I/&> f~q-i·r Company:

Uro-~::S Company:

(\ !Cooler Temp. (0 C): Obs'd:

D~~ITi!¥: t-;'>;;fReqe1Vj:ld·by: {) • /f20J/(tp l~~Ji r~

Corr'd: Thenn ID Nb.:

Company: Grc.~5 '1'6-6.6'.;7

DatelTime: f-2CJ-/(,p 8' :55

Company:

114- OlL-Cornpany:

Date/Time:

1-020. /b -efiY /~0 Date/Time: <p h;ZIJ·t~

[ Hematite !Jecommioomg Project I Pem1afix (mr W-estinghouse) f'.fon-Propne!:af\~ CJa$S 3 I Procedtlf'e:HDP-PR-OA-000, Chait< of Custody r R.e\llsioo: ~ I '""' I I II : '. 1--. __

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1/29/2016

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TestAmerica St. Louis 13715 Rider Trail North

Earth City, MO 63045 phone 314.298.8566 fax

Client Contact Penna-Fix Environmental Services 2800 Solway Road Knoxville, TN 37931 (865) 690-0501 Phone (865) 539-9868 FAX Project Name: Hematite Decommissioning Project Site: Westinghouse Hematite, MO P0#832953


802-01-13-P-S-S-OO

802-01-14-P-R-S-OO

802-01-15-P-E-S-OO

802-01-16-P-S-S-OO

802-01-17-P-R-S-OO

802-01-18-P-E-S-OO

802-01-19-P-S-S-OO

802-01-20-P-R-S-OO

802-01-21-P-E-S-OO

802-01-22"P-S-S-OO

802-01-23-P-R-S-OO

802-01-24-P-E-S-00

Possible Hazard Identification:

·-----_.

Chain of Custody Record Test America THE LEADER IN ENVIRONMENTAL TESTING

Regulatory Program: 0 DW 0 NPDES 0 RCRA 0 other: -- - - - TestAmerica Laboratories, Inc.

Project Manager: Brian Miller Site Contact:. Ellen Jakub Date: 1/19/2016 COC No: 011916-FSS1 Tel/Fax: (314) 810-3333 Lab Contact: Ivan Vania Carrier: Courier 2 of 3 CO Cs

Analysis Turnaround Time i::' Sampler:

0 CALENDAR DAYS 0 WORKINGDAYS e For Lab Use Only: - "" :;: I TAT if different from Below z ~ l Walk-in Client:

0 - .s e Lab Sampling; I 2Weeks z > "" .. "" 0 l week >- ~ .5 c » 0 2days .!!! (/) ::c .. Job/SDG No.: ::

"~ ! ... Cl. ...... D 1 day E (/) .. "' " ~ill "' :: c. 0 "' __ ,,,,..._ rn rn .c c.

Type "' e "' g> II> II> Ii Sample Sample !!! .g E ·- .. ~ (C=Comp, #of l! eij .c

Date Time G=Grab) Matrix Cont. :. (; 3: c.

Li: :;;: 0 Sample Specific Notes:

1/18/16 1005 c Soil 1 N x x x Mark Shaffer

1/18/16 1045 c Soil 1 N x x x Chris Chandler

1118116 1050 c Soil 1 N x x x Mark Shaffer

12129/16 1520 c Soil 1 N x x x Mark Shaffer

12131/15 1020 c Soil 1 N x x x Chris Chandler '

12131/15 1030 c Soil 1 N x x x Mark Shaffer

1/18!16 1105 c Soil 1 N x x x Mark Shaffer



1/18/16 1315 c Soil 1 N v x x Mark Shaffer A



>.,::' :'J•C ~~~ ··" ... ,,,.,,, ,:,; Sample Disposal (A fee may be assessed if samples are retained longer than 1 month)

Are any samples from a listed EPA Hazardous Waste? Please List any EPA Waste Codes for the sample in the Comments Section if the lab is to dispose of the sample.

0 Non-Hazard 0Aammable D Skin Irritant 0 Poison B 0Unknown El Return to Client 0 Disposal by lab 0 Archive for Months

Special Instructions/QC Requirements & Comments: Potential tor Radiological Contamination

Custody Seals Intact: El Yes 0 No Custody Seal No.: Cooler Temp. (°C): Obs'd: Corr'd: Therm ID No.:

R,qzuished by: .~~v.D ~~ 0i/?O/l! ~~ Company: Datemme:

3';5;5 ,,,wefll(l. W<ub ¥1;£ (~'{Oqc)~ t~ltJ- /b

'~~:fj~\l'QJ1 ~ JJ ,,);?/~ Company: qi~rr~~:r&c!fJ '?Ji'@d by: ,d_ Company: Datemme:

~ ( -t_e /6 p; e_.~_,1 //tl-6/L- l.a2~·1&:i I~ ~elinquished by: I v Company: Oaternme: RE!ceived in Laboratory by: Company: Datemme:

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11·

TestAmerica St Louis 13715 Rider Trail North

Chain of Custody Record TestAmerica Earth City, MO 63045 phone 314.298.8566 fax

Client Contact Perma-Fix Environmental Services 2800 Solway Road Knoxville, TN 37931 (865) 690-0501 Phone (865) 539-9868 FAX Project Name: Hematite Decommissioning Project Site: Westinghouse Hematite, MO P0#832953


802-01-02-P-R-Q-OO

802-01-10-P-S-Q-OO

r----_

------- --------

Regulatory Program: D DW 0 NPDES

Project Manager: Brian Miller Tel/Fax: (314) 810-3333

Analysis Turnaround Time 0 CALENDARDAYS 0 WORKING DAYS

TAT if different from Below

0 2 weeks

0 l Week

0 2 days

D lday -~ ........

Type Sample I Sample I (C--Comp, #of

Date Time G=Grab) Matrix Cont.

114116 I 925 I c Soil 1

1.2131/15 I 1045 I c Soil 1

---+-------

'THE LEADER IN ENVIRONMENTAL TS:ST1NG

QRCRA 0 01!1er: TestAmerica Laboratories, Inc. Site Contact: Ellen Jakub !Date: 1/19/2016 COC No: 011916-FSS1 uib Contact: Ivan Vania !Carrier: Courier __ 3_ of_3_ COCs

t- Sampler: f! - ... f z ::i -- s Z> ~ -- .. Cl

>c E .5

"' >--(/) :c .. .!! :;: .. ;;- ~~ ... _ ... "'

~ E (/) "'::J ... ~ ~:;: ... 0 .. (/).:: ... .., E .. Cl "' UJ ~! "' .. E .E "' ~ s .g E 10 .c .. .. ...

~~ = m 0 3: < !::! u.. Q..

For Lab Use Only: Walk-in Client I I Lab Sampling:

Job I SDG No.:

Sample Specific Notes:

N x x x Mark Shaffer

N x x x Brian Miller

~

-------_J_H-J-1-1

--r-J-~~~~~~~~~~~~~~~~~~~1--~~-t-~~-t-~~-': N ____... . ... , ... I

· -· -· ~ .. ··········-·-· "--rt= I I I I I I I I I I I I' ~ N--W_

--------- N-+-L

--------- ------~ ~ 1~~~m~z~~~Jj\~JJ~~~-~~·~~~~~m~~~~~rit~f:~-zP:~f?~J~~1-~.}f~1~··: r~~-~~t1l§ ;~r~ _:~11; ·~~k ~~-Possible Hazard Identification: Sample Disposal ( A fee may be assessed if samples are retained longer than 1 month) Are any samples from a listed EPA Hazardous Waste? Please List any EPA Waste Codes for the sample in the Comments Section if the lab is to dispose of the sample.

0 Non-Hazard O Flammable 0 Skin Irritant 0 Poison B 0 Unknown 0 Return to Oient 0 Disposal by Lab 0 Archive fur Months

Special Instructions/QC Requirements & Comments: Potential for Radiological Contamination

Corr'd: Therm ID No.: Company: Datemme:

6~~5 CV'e55 .f'~P-t35 t -z.a- l<P Company: Datemme: 7-A sz_, 1-~,fb /030

Company:·· Date/Time:

I Hematite De-cammfoning; Praject I Permafi>; (for Westmgtm.ll!Se) Noo-Proprietaty ciass 3 I Procerlure:HD.0 -PR-OA-0(1'6, Chair. of Casiod!f I Re<.isron: 3

Login Sample Receipt Checklist

Client: Perma-Fix Environmental Services Inc. Job Number: 160-15789-1

Login Number: 15789

Question Answer Comment

Creator: Clarke, Jill C

List Source: TestAmerica St. Louis

List Number: 1

TrueRadioactivity wasn't checked or is </= background as measured by a survey meter.

TrueThe cooler's custody seal, if present, is intact.

N/ASample custody seals, if present, are intact.

TrueThe cooler or samples do not appear to have been compromised or tampered with.

N/ASamples were received on ice.

TrueCooler Temperature is acceptable.

TrueCooler Temperature is recorded.

TrueCOC is present.

TrueCOC is filled out in ink and legible.

TrueCOC is filled out with all pertinent information.

N/AIs the Field Sampler's name present on COC?

TrueThere are no discrepancies between the containers received and the COC.

TrueSamples are received within Holding Time (excluding tests with immediate HTs)

TrueSample containers have legible labels.

TrueContainers are not broken or leaking.

TrueSample collection date/times are provided.

TrueAppropriate sample containers are used.

TrueSample bottles are completely filled.

TrueSample Preservation Verified.

TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs

N/AContainers requiring zero headspace have no headspace or bubble is <6mm (1/4").

TrueMultiphasic samples are not present.

TrueSamples do not require splitting or compositing.

N/AResidual Chlorine Checked.


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101112

Definitions/GlossaryTestAmerica Job ID: 160-15789-1Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP

Qualifiers

Metals

Qualifier Description

J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.

Qualifier

Rad

Qualifier Description

U Result is less than the sample detection limit.

Qualifier

Glossary

These commonly used abbreviations may or may not be present in this report.

¤ Listed under the "D" column to designate that the result is reported on a dry weight basis

Abbreviation

%R Percent Recovery

CFL Contains Free Liquid

CNF Contains no Free Liquid

DER Duplicate error ratio (normalized absolute difference)

Dil Fac Dilution Factor

DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample

DLC Decision level concentration

MDA Minimum detectable activity

EDL Estimated Detection Limit

MDC Minimum detectable concentration

MDL Method Detection Limit

ML Minimum Level (Dioxin)

NC Not Calculated

ND Not detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit

QC Quality Control

RER Relative error ratio

RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points

TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)

TestAmerica St. Louis

Page 9 of 46 1/29/2016

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Method SummaryTestAmerica Job ID: 160-15789-1Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP

Method Method Description LaboratoryProtocol

SW8466020A Metals (ICP/MS), Tc-99 TAL SL

EPAMoisture Percent Moisture TAL SL

SW8466020A Metals (ICP/MS), Tc-99 in Activity TAL SL

DOEGA-01-R Cesium-137 & Other Gamma Emitters (GS) TAL SL

Protocol References:

DOE = U.S. Department of Energy

EPA = US Environmental Protection Agency

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

Laboratory References:

TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566


Page 10 of 46 1/29/2016

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Sample SummaryTestAmerica Job ID: 160-15789-1Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP

Lab Sample ID Client Sample ID ReceivedCollectedMatrix

160-15789-1 B02-01-01-P-S-S-00 Solid 12/31/15 11:50 01/20/16 10:30

160-15789-2 B02-01-02-P-R-S-00 Solid 01/04/16 09:25 01/20/16 10:30

160-15789-3 B02-01-03-P-E-S-00 Solid 01/04/16 09:35 01/20/16 10:30

160-15789-4 B02-01-04-P-S-S-00 Solid 12/29/15 09:25 01/20/16 10:30

160-15789-5 B02-01-05-P-R-S-00 Solid 12/29/15 10:30 01/20/16 10:30

160-15789-6 B02-01-06-P-E-S-00 Solid 12/29/15 10:35 01/20/16 10:30

160-15789-7 B02-01-07-P-S-S-00 Solid 12/29/15 11:00 01/20/16 10:30

160-15789-8 B02-01-08-P-R-S-00 Solid 12/29/15 11:30 01/20/16 10:30

160-15789-9 B02-01-09-P-E-S-00 Solid 12/29/15 11:35 01/20/16 10:30

160-15789-10 B02-01-10-P-S-S-00 Solid 12/31/15 10:45 01/20/16 10:30

160-15789-11 B02-01-11-P-R-S-00 Solid 12/31/15 11:15 01/20/16 10:30

160-15789-12 B02-01-12-P-E-S-00 Solid 12/31/15 11:25 01/20/16 10:30

160-15789-13 B02-01-13-P-S-S-00 Solid 01/18/16 10:05 01/20/16 10:30

160-15789-14 B02-01-14-P-R-S-00 Solid 01/18/16 10:45 01/20/16 10:30

160-15789-15 B02-01-15-P-E-S-00 Solid 01/18/16 10:50 01/20/16 10:30

160-15789-16 B02-01-16-P-S-S-00 Solid 12/29/15 15:20 01/20/16 10:30

160-15789-17 B02-01-17-P-R-S-00 Solid 12/31/15 10:20 01/20/16 10:30

160-15789-18 B02-01-18-P-E-S-00 Solid 12/31/15 10:30 01/20/16 10:30

160-15789-19 B02-01-19-P-S-S-00 Solid 01/18/16 11:05 01/20/16 10:30

160-15789-20 B02-01-20-P-R-S-00 Solid 01/18/16 11:20 01/20/16 10:30

160-15789-21 B02-01-21-P-E-S-00 Solid 01/18/16 11:25 01/20/16 10:30

160-15789-22 B02-01-22-P-S-S-00 Solid 01/18/16 13:15 01/20/16 10:30

160-15789-23 B02-01-23-P-R-S-00 Solid 01/18/16 13:40 01/20/16 10:30

160-15789-24 B02-01-24-P-E-S-00 Solid 01/18/16 13:45 01/20/16 10:30

160-15789-25 B02-01-02-P-R-Q-00 Solid 01/04/16 09:25 01/20/16 10:30

160-15789-26 B02-01-10-P-S-Q-00 Solid 12/31/15 10:45 01/20/16 10:30


Page 11 of 46 1/29/2016

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Client Sample ResultsTestAmerica Job ID: 160-15789-1Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP

Lab Sample ID: 160-15789-1Client Sample ID: B02-01-01-P-S-S-00Matrix: SolidDate Collected: 12/31/15 11:50

Date Received: 01/20/16 10:30

Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte

Actinium 228 0.117

(2σ+/-)

0.0406

(2σ+/-)

101/24/16 17:2001/22/16 09:43pCi/g0.0239

RL MDC

0.0388

Dil FacAnalyzedPreparedUnitResult Qualifier

Count Total

Uncert. Uncert.

pCi/g 01/22/16 09:43 01/24/16 17:20 10.03120.01870.0186U0.0109Americium 241

pCi/g 01/22/16 09:43 01/24/16 17:20 10.1830.1080.108U0.0687Bismuth 212

pCi/g 01/22/16 09:43 01/24/16 17:20 10.02040.03520.03100.159Bismuth 214

pCi/g 01/22/16 09:43 01/24/16 17:20 10.02360.02630.02290.0998Lead 212

pCi/g 01/22/16 09:43 01/24/16 17:20 10.03320.03640.03200.168Lead 214

pCi/g 01/22/16 09:43 01/24/16 17:20 10.1780.4550.3742.53Potassium 40

pCi/g 01/22/16 09:43 01/24/16 17:20 11.180.7260.724U0.532Protactinium 234m

pCi/g 01/22/16 09:43 01/24/16 17:20 10.3270.1900.189U0.0877Protactinium 231

pCi/g 01/22/16 09:43 01/24/16 17:20 10.02040.03520.03100.159Radium 226

pCi/g 01/22/16 09:43 01/24/16 17:20 10.3170.2510.2480.361Thorium 234

pCi/g 01/22/16 09:43 01/24/16 17:20 10.08240.04830.0483U0.0187Uranium 235

pCi/g 01/22/16 09:43 01/24/16 17:20 10.02390.04060.03880.117Thorium 232

Tl-208 0.0440 0.0137 0.0144 0.0117 pCi/g 01/22/16 09:43 01/24/16 17:20 1

(2σ+/-) (2σ+/-) MDCRL Dil FacAnalyzedPreparedUnitResult Qualifier

Count Total

Other Detected

Radionuclides

Uncert. Uncert.


Percent Solids: 90.9Date Received: 01/20/16 10:30

Method: 6020A - Metals (ICP/MS), Tc-99RL MDL

Technetium 99 ND 0.000054 0.000016 mg/Kg ☼ 01/20/16 16:10 01/28/16 21:15 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

Method: 6020A - Metals (ICP/MS), Tc-99 in Activity

Analyte

Technetium 99 -0.0261 U

(2σ+/-)

0.00953

(2σ+/-)

101/28/16 21:1501/20/16 16:10pCi/g0.1841.07

RL MDC

0.00923


Count Total

Uncert. Uncert.

Re 30 - 110

Carrier

01/20/16 16:10 01/28/16 21:15 1

Dil FacAnalyzedPreparedQualifier Limits%Yield

103

Lab Sample ID: 160-15789-2Client Sample ID: B02-01-02-P-R-S-00Matrix: SolidDate Collected: 01/04/16 09:25



Analyte

Actinium 228 1.09

(2σ+/-)

0.157

(2σ+/-)

101/24/16 17:2101/22/16 09:43pCi/g0.0862

RL MDC

0.113


Count Total

Uncert. Uncert.

pCi/g 01/22/16 09:43 01/24/16 17:21 10.09030.05390.0538U0.0155Americium 241

pCi/g 01/22/16 09:43 01/24/16 17:21 10.3210.3710.3521.16Bismuth 212

pCi/g 01/22/16 09:43 01/24/16 17:21 10.06220.1220.08930.805Bismuth 214

pCi/g 01/22/16 09:43 01/24/16 17:21 10.06240.1530.07341.04Lead 212


Page 12 of 46 1/29/2016

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Project/Site: HDP



Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)

Analyte

Lead 214 0.989

(2σ+/-)

0.128

(2σ+/-)

101/24/16 17:2101/22/16 09:43pCi/g0.0567

RL MDC

0.0764


Count Total

Uncert. Uncert.

pCi/g 01/22/16 09:43 01/24/16 17:21 10.2342.191.0119.3Potassium 40



pCi/g 01/22/16 09:43 01/24/16 17:21 10.06220.1220.08930.805Radium 226

pCi/g 01/22/16 09:43 01/24/16 17:21 10.7280.5890.5751.24Thorium 234

pCi/g 01/22/16 09:43 01/24/16 17:21 10.2160.1360.135U0.116Uranium 235

pCi/g 01/22/16 09:43 01/24/16 17:21 10.08620.1570.1131.09Thorium 232

Tl-208 0.348 0.0428 0.0558 0.0303 pCi/g 01/22/16 09:43 01/24/16 17:21 1


Count Total

Other Detected

Radionuclides

Uncert. Uncert.







Analyte

Technetium 99 0.111 U

(2σ+/-)

0.0747

(2σ+/-)

101/28/16 21:3801/20/16 16:10pCi/g0.2091.22

RL MDC

0.0740


Count Total

Uncert. Uncert.

Re 30 - 110

Carrier

01/20/16 16:10 01/28/16 21:38 1


100

Lab Sample ID: 160-15789-3Client Sample ID: B02-01-03-P-E-S-00Matrix: SolidDate Collected: 01/04/16 09:35



Analyte

Actinium 228 1.05

(2σ+/-)

0.158

(2σ+/-)

101/24/16 18:3501/22/16 09:43pCi/g0.110

RL MDC

0.116


Count Total

Uncert. Uncert.

pCi/g 01/22/16 09:43 01/24/16 18:35 10.09590.05670.0567U-0.00207Americium 241

pCi/g 01/22/16 09:43 01/24/16 18:35 10.4110.4580.4401.22Bismuth 212

pCi/g 01/22/16 09:43 01/24/16 18:35 10.07630.1530.1121.00Bismuth 214

pCi/g 01/22/16 09:43 01/24/16 18:35 10.06930.1650.08481.09Lead 212

pCi/g 01/22/16 09:43 01/24/16 18:35 10.07640.1330.08400.994Lead 214

pCi/g 01/22/16 09:43 01/24/16 18:35 10.3522.331.2419.2Potassium 40



pCi/g 01/22/16 09:43 01/24/16 18:35 10.07630.1530.1121.00Radium 226


Page 13 of 46 1/29/2016

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Project/Site: HDP




Analyte

Thorium 234 1.18

(2σ+/-)

0.528

(2σ+/-)

101/24/16 18:3501/22/16 09:43pCi/g0.809

RL MDC

0.514


Count Total

Uncert. Uncert.

pCi/g 01/22/16 09:43 01/24/16 18:35 10.2220.1470.146U0.154Uranium 235

pCi/g 01/22/16 09:43 01/24/16 18:35 10.1100.1580.1161.05Thorium 232

Tl-208 0.366 0.0500 0.0628 0.0372 pCi/g 01/22/16 09:43 01/24/16 18:35 1


Count Total

Other Detected

Radionuclides

Uncert. Uncert.







Analyte


(2σ+/-)

0.0152

(2σ+/-)

101/28/16 21:4201/20/16 16:10pCi/g0.2081.22

RL MDC

0.0152


Count Total

Uncert. Uncert.

Re 30 - 110

Carrier

01/20/16 16:10 01/28/16 21:42 1


101




Analyte

Actinium 228 0.0689

(2σ+/-)

0.0268

(2σ+/-)

101/24/16 18:3601/22/16 09:43pCi/g0.0597

RL MDC

0.0259


Count Total

Uncert. Uncert.

pCi/g 01/22/16 09:43 01/24/16 18:36 10.03160.2300.230U-0.00574Americium 241

pCi/g 01/22/16 09:43 01/24/16 18:36 10.1570.09370.0935U0.0612Bismuth 212

pCi/g 01/22/16 09:43 01/24/16 18:36 10.02780.03110.02940.0995Bismuth 214

pCi/g 01/22/16 09:43 01/24/16 18:36 10.02140.01850.01720.0521Lead 212

pCi/g 01/22/16 09:43 01/24/16 18:36 10.02610.03080.02780.127Lead 214

pCi/g 01/22/16 09:43 01/24/16 18:36 10.1780.3360.2801.85Potassium 40



pCi/g 01/22/16 09:43 01/24/16 18:36 10.02780.03110.02940.0995Radium 226

pCi/g 01/22/16 09:43 01/24/16 18:36 10.2480.1670.166U0.161Thorium 234

pCi/g 01/22/16 09:43 01/24/16 18:36 10.07480.04500.0449U0.0323Uranium 235

pCi/g 01/22/16 09:43 01/24/16 18:36 10.05970.02680.02590.0689Thorium 232


Page 14 of 46 1/29/2016

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Project/Site: HDP



Tl-208 0.0219 0.00902 0.00930 0.0109 pCi/g 01/22/16 09:43 01/24/16 18:36 1


Count Total

Other Detected

Radionuclides

Uncert. Uncert.







Analyte


(2σ+/-)

0.0207

(2σ+/-)

101/28/16 21:4601/20/16 16:10pCi/g0.1700.993

RL MDC

0.0207


Count Total

Uncert. Uncert.

Re 30 - 110

Carrier

01/20/16 16:10 01/28/16 21:46 1


105




Analyte

Actinium 228 0.658

(2σ+/-)

0.115

(2σ+/-)

101/24/16 18:3601/22/16 09:43pCi/g0.0756

RL MDC

0.0933


Count Total

Uncert. Uncert.

pCi/g 01/22/16 09:43 01/24/16 18:36 10.07620.04600.0459U-0.0263Americium 241

pCi/g 01/22/16 09:43 01/24/16 18:36 10.2690.3030.2910.813Bismuth 212

pCi/g 01/22/16 09:43 01/24/16 18:36 10.04290.09210.06710.607Bismuth 214

pCi/g 01/22/16 09:43 01/24/16 18:36 10.05130.1090.05900.710Lead 212

pCi/g 01/22/16 09:43 01/24/16 18:36 10.05220.09130.05800.679Lead 214

pCi/g 01/22/16 09:43 01/24/16 18:36 10.2181.570.80913.1Potassium 40



pCi/g 01/22/16 09:43 01/24/16 18:36 10.04290.09210.06710.607Radium 226

pCi/g 01/22/16 09:43 01/24/16 18:36 10.5630.2060.198U0.550Thorium 234

pCi/g 01/22/16 09:43 01/24/16 18:36 10.1660.1000.0996U0.0889Uranium 235

pCi/g 01/22/16 09:43 01/24/16 18:36 10.07560.1150.09330.658Thorium 232

Tl-208 0.222 0.0345 0.0415 0.0280 pCi/g 01/22/16 09:43 01/24/16 18:36 1


Count Total

Other Detected

Radionuclides

Uncert. Uncert.


Page 15 of 46 1/29/2016

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Project/Site: HDP







Analyte


(2σ+/-)

0.0436

(2σ+/-)

101/28/16 21:5001/20/16 16:10pCi/g0.1971.15

RL MDC

0.0435


Count Total

Uncert. Uncert.

Re 30 - 110

Carrier

01/20/16 16:10 01/28/16 21:50 1


102




Analyte

Actinium 228 1.16

(2σ+/-)

0.213

(2σ+/-)

101/24/16 18:3801/22/16 09:43pCi/g0.129

RL MDC

0.178


Count Total

Uncert. Uncert.

pCi/g 01/22/16 09:43 01/24/16 18:38 10.07770.05250.0523U0.0371Americium 241

pCi/g 01/22/16 09:43 01/24/16 18:38 10.4340.5240.5021.44Bismuth 212

pCi/g 01/22/16 09:43 01/24/16 18:38 10.08180.1580.1240.941Bismuth 214

pCi/g 01/22/16 09:43 01/24/16 18:38 10.08170.1600.09331.01Lead 212

pCi/g 01/22/16 09:43 01/24/16 18:38 10.07730.1430.1030.951Lead 214

pCi/g 01/22/16 09:43 01/24/16 18:38 10.2732.191.2817.3Potassium 40

pCi/g 01/22/16 09:43 01/24/16 18:38 16.833.723.72U-0.000967Protactinium 234m


pCi/g 01/22/16 09:43 01/24/16 18:38 10.08180.1580.1240.941Radium 226

pCi/g 01/22/16 09:43 01/24/16 18:38 10.9130.3330.322U0.829Thorium 234

pCi/g 01/22/16 09:43 01/24/16 18:38 10.2020.1440.1410.264Uranium 235

pCi/g 01/22/16 09:43 01/24/16 18:38 10.1290.2130.1781.16Thorium 232

Tl-208 0.410 0.0544 0.0691 0.0362 pCi/g 01/22/16 09:43 01/24/16 18:38 1


Count Total

Other Detected

Radionuclides

Uncert. Uncert.







Analyte


(2σ+/-)

0.0652

(2σ+/-)

101/28/16 21:5401/20/16 16:10pCi/g0.2131.25

RL MDC

0.0652


Count Total

Uncert. Uncert.


Page 16 of 46 1/29/2016

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Project/Site: HDP



Re 30 - 110

Carrier

01/20/16 16:10 01/28/16 21:54 1


101




Analyte

Actinium 228 0.104

(2σ+/-)

0.0344

(2σ+/-)

101/24/16 19:1301/22/16 09:43pCi/g0.0277

RL MDC

0.0327


Count Total

Uncert. Uncert.

pCi/g 01/22/16 09:43 01/24/16 19:13 10.03360.01990.0199U-0.00799Americium 241

pCi/g 01/22/16 09:43 01/24/16 19:13 10.1550.08880.0887U0.0400Bismuth 212

pCi/g 01/22/16 09:43 01/24/16 19:13 10.02220.03300.02970.139Bismuth 214

pCi/g 01/22/16 09:43 01/24/16 19:13 10.02230.02280.02000.0838Lead 212

pCi/g 01/22/16 09:43 01/24/16 19:13 10.03050.03340.02730.184Lead 214

pCi/g 01/22/16 09:43 01/24/16 19:13 10.1370.4620.3443.01Potassium 40



pCi/g 01/22/16 09:43 01/24/16 19:13 10.02220.03300.02970.139Radium 226

pCi/g 01/22/16 09:43 01/24/16 19:13 10.3370.09760.0968U0.121Thorium 234

pCi/g 01/22/16 09:43 01/24/16 19:13 10.07060.04310.0429U0.0375Uranium 235

pCi/g 01/22/16 09:43 01/24/16 19:13 10.02770.03440.03270.104Thorium 232

Tl-208 0.0303 0.0133 0.0137 0.0138 pCi/g 01/22/16 09:43 01/24/16 19:13 1


Count Total

Other Detected

Radionuclides

Uncert. Uncert.







Analyte


(2σ+/-)

0.0483

(2σ+/-)

101/28/16 21:5701/20/16 16:10pCi/g0.1751.02

RL MDC

0.0477


Count Total

Uncert. Uncert.

Re 30 - 110

Carrier

01/20/16 16:10 01/28/16 21:57 1


104


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Project/Site: HDP




Analyte

Actinium 228 0.723

(2σ+/-)

0.121

(2σ+/-)

101/24/16 19:1601/22/16 09:43pCi/g0.105

RL MDC

0.0963


Count Total

Uncert. Uncert.

pCi/g 01/22/16 09:43 01/24/16 19:16 10.07260.04320.0432U0.0130Americium 241

pCi/g 01/22/16 09:43 01/24/16 19:16 10.3390.3500.3380.867Bismuth 212

pCi/g 01/22/16 09:43 01/24/16 19:16 10.05510.1090.08180.690Bismuth 214

pCi/g 01/22/16 09:43 01/24/16 19:16 10.05290.1210.06450.791Lead 212

pCi/g 01/22/16 09:43 01/24/16 19:16 10.05350.09770.07040.651Lead 214

pCi/g 01/22/16 09:43 01/24/16 19:16 10.2151.750.96514.2Potassium 40



pCi/g 01/22/16 09:43 01/24/16 19:16 10.05510.1090.08180.690Radium 226

pCi/g 01/22/16 09:43 01/24/16 19:16 10.6650.2380.229U0.636Thorium 234

pCi/g 01/22/16 09:43 01/24/16 19:16 10.1930.1120.111U0.108Uranium 235

pCi/g 01/22/16 09:43 01/24/16 19:16 10.1050.1210.09630.723Thorium 232

Tl-208 0.242 0.0417 0.0487 0.0345 pCi/g 01/22/16 09:43 01/24/16 19:16 1


Count Total

Other Detected

Radionuclides

Uncert. Uncert.







Analyte


(2σ+/-)

0.0240

(2σ+/-)

101/28/16 22:0101/20/16 16:10pCi/g0.2081.21

RL MDC

0.0236


Count Total

Uncert. Uncert.

Re 30 - 110

Carrier

01/20/16 16:10 01/28/16 22:01 1


100




Analyte

Actinium 228 1.19

(2σ+/-)

0.175

(2σ+/-)

101/24/16 19:1501/22/16 09:43pCi/g0.104

RL MDC

0.128


Count Total

Uncert. Uncert.

pCi/g 01/22/16 09:43 01/24/16 19:15 10.1060.06260.0626U0.00334Americium 241

pCi/g 01/22/16 09:43 01/24/16 19:15 10.4630.5680.5451.57Bismuth 212

pCi/g 01/22/16 09:43 01/24/16 19:15 10.07570.1230.08640.849Bismuth 214

pCi/g 01/22/16 09:43 01/24/16 19:15 10.07560.1720.08681.15Lead 212


Page 18 of 46 1/29/2016

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Project/Site: HDP




Analyte

Lead 214 1.11

(2σ+/-)

0.147

(2σ+/-)

101/24/16 19:1501/22/16 09:43pCi/g0.0756

RL MDC

0.0904


Count Total

Uncert. Uncert.

pCi/g 01/22/16 09:43 01/24/16 19:15 10.2742.521.1722.2Potassium 40


pCi/g 01/22/16 09:43 01/24/16 19:15 11.200.7310.728U-0.558Protactinium 231

pCi/g 01/22/16 09:43 01/24/16 19:15 10.07570.1230.08640.849Radium 226

pCi/g 01/22/16 09:43 01/24/16 19:15 10.8310.3120.2960.915Thorium 234

pCi/g 01/22/16 09:43 01/24/16 19:15 10.2370.1300.130U0.115Uranium 235

pCi/g 01/22/16 09:43 01/24/16 19:15 10.1040.1750.1281.19Thorium 232

Tl-208 0.359 0.0493 0.0616 0.0406 pCi/g 01/22/16 09:43 01/24/16 19:15 1


Count Total

Other Detected

Radionuclides

Uncert. Uncert.







Analyte


(2σ+/-)

0.0149

(2σ+/-)

101/28/16 22:0501/20/16 16:10pCi/g0.2071.21

RL MDC

0.0138


Count Total

Uncert. Uncert.

Re 30 - 110

Carrier

01/20/16 16:10 01/28/16 22:05 1


101




Analyte

Actinium 228 0.0576

(2σ+/-)

0.0268

(2σ+/-)

101/24/16 19:1401/22/16 09:43pCi/g0.0438

RL MDC

0.0262


Count Total

Uncert. Uncert.

pCi/g 01/22/16 09:43 01/24/16 19:14 10.02920.01720.0172U-0.00578Americium 241

pCi/g 01/22/16 09:43 01/24/16 19:14 10.1970.1060.106U-0.0000829Bismuth 212

pCi/g 01/22/16 09:43 01/24/16 19:14 10.02330.03370.03040.140Bismuth 214

pCi/g 01/22/16 09:43 01/24/16 19:14 10.02310.02510.02270.0835Lead 212

pCi/g 01/22/16 09:43 01/24/16 19:14 10.02930.02920.02480.148Lead 214

pCi/g 01/22/16 09:43 01/24/16 19:14 10.1420.3910.3152.27Potassium 40



pCi/g 01/22/16 09:43 01/24/16 19:14 10.02330.03370.03040.140Radium 226


Page 19 of 46 1/29/2016

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Project/Site: HDP




Analyte

Thorium 234 0.187 U

(2σ+/-)

0.113

(2σ+/-)

101/24/16 19:1401/22/16 09:43pCi/g0.305

RL MDC

0.111


Count Total

Uncert. Uncert.

pCi/g 01/22/16 09:43 01/24/16 19:14 10.05990.03850.0383U0.0376Uranium 235

pCi/g 01/22/16 09:43 01/24/16 19:14 10.04380.02680.02620.0576Thorium 232

Tl-208 0.0315 0.0110 0.0115 0.00903 pCi/g 01/22/16 09:43 01/24/16 19:14 1


Count Total

Other Detected

Radionuclides

Uncert. Uncert.







Analyte


(2σ+/-)

0.0345

(2σ+/-)

101/28/16 22:0901/20/16 16:10pCi/g0.1791.05

RL MDC

0.0345


Count Total

Uncert. Uncert.

Re 30 - 110

Carrier

01/20/16 16:10 01/28/16 22:09 1


104




Analyte

Actinium 228 0.861

(2σ+/-)

0.174

(2σ+/-)

101/24/16 19:1601/22/16 09:43pCi/g0.0721

RL MDC

0.150


Count Total

Uncert. Uncert.

pCi/g 01/22/16 09:43 01/24/16 19:16 10.1020.06140.0613U0.0265Americium 241

pCi/g 01/22/16 09:43 01/24/16 19:16 10.4220.4220.4090.990Bismuth 212

pCi/g 01/22/16 09:43 01/24/16 19:16 10.06350.1310.1010.798Bismuth 214

pCi/g 01/22/16 09:43 01/24/16 19:16 10.06590.1430.08260.899Lead 212

pCi/g 01/22/16 09:43 01/24/16 19:16 10.06280.1230.09010.807Lead 214

pCi/g 01/22/16 09:43 01/24/16 19:16 10.3952.041.2415.8Potassium 40



pCi/g 01/22/16 09:43 01/24/16 19:16 10.06350.1310.1010.798Radium 226

pCi/g 01/22/16 09:43 01/24/16 19:16 10.7780.5300.5071.47Thorium 234

pCi/g 01/22/16 09:43 01/24/16 19:16 10.2430.1350.135U0.0887Uranium 235

pCi/g 01/22/16 09:43 01/24/16 19:16 10.07210.1740.1500.861Thorium 232


Page 20 of 46 1/29/2016

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Project/Site: HDP



Tl-208 0.302 0.0500 0.0590 0.0362 pCi/g 01/22/16 09:43 01/24/16 19:16 1


Count Total

Other Detected

Radionuclides

Uncert. Uncert.







Analyte


(2σ+/-)

0.00883

(2σ+/-)

101/28/16 22:1301/20/16 16:10pCi/g0.1991.16

RL MDC

0.00883


Count Total

Uncert. Uncert.

Re 30 - 110

Carrier

01/20/16 16:10 01/28/16 22:13 1


100




Analyte

Actinium 228 1.08

(2σ+/-)

0.159

(2σ+/-)

101/24/16 19:4901/22/16 09:43pCi/g0.0901

RL MDC

0.114


Count Total

Uncert. Uncert.

pCi/g 01/22/16 09:43 01/24/16 19:49 10.09460.05650.0565U0.0156Americium 241

pCi/g 01/22/16 09:43 01/24/16 19:49 10.3050.3340.3161.05Bismuth 212

pCi/g 01/22/16 09:43 01/24/16 19:49 10.06700.1350.09720.899Bismuth 214

pCi/g 01/22/16 09:43 01/24/16 19:49 10.06400.1510.07531.01Lead 212

pCi/g 01/22/16 09:43 01/24/16 19:49 10.06630.1320.07831.03Lead 214

pCi/g 01/22/16 09:43 01/24/16 19:49 10.3772.061.0517.3Potassium 40



pCi/g 01/22/16 09:43 01/24/16 19:49 10.06700.1350.09720.899Radium 226

pCi/g 01/22/16 09:43 01/24/16 19:49 10.7740.3110.2990.814Thorium 234

pCi/g 01/22/16 09:43 01/24/16 19:49 10.2160.1340.133U0.136Uranium 235

pCi/g 01/22/16 09:43 01/24/16 19:49 10.09010.1590.1141.08Thorium 232

Tl-208 0.343 0.0496 0.0611 0.0369 pCi/g 01/22/16 09:43 01/24/16 19:49 1


Count Total

Other Detected

Radionuclides

Uncert. Uncert.


Page 21 of 46 1/29/2016

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101112


Project/Site: HDP







Analyte


(2σ+/-)

0.0315

(2σ+/-)

101/28/16 22:2801/20/16 16:10pCi/g0.2141.25

RL MDC

0.0312


Count Total

Uncert. Uncert.

Re 30 - 110

Carrier

01/20/16 16:10 01/28/16 22:28 1


99




Analyte

Actinium 228 0.0969

(2σ+/-)

0.0352

(2σ+/-)

101/24/16 19:5001/22/16 09:43pCi/g0.0234

RL MDC

0.0337


Count Total

Uncert. Uncert.

pCi/g 01/22/16 09:43 01/24/16 19:50 10.02630.01560.0156U0.00804Americium 241

pCi/g 01/22/16 09:43 01/24/16 19:50 10.1790.1150.114U0.112Bismuth 212

pCi/g 01/22/16 09:43 01/24/16 19:50 10.02890.03720.03380.148Bismuth 214

pCi/g 01/22/16 09:43 01/24/16 19:50 10.02200.02350.02090.0834Lead 212

pCi/g 01/22/16 09:43 01/24/16 19:50 10.02140.03160.02630.168Lead 214

pCi/g 01/22/16 09:43 01/24/16 19:50 10.2110.4050.3442.09Potassium 40



pCi/g 01/22/16 09:43 01/24/16 19:50 10.02890.03720.03380.148Radium 226

pCi/g 01/22/16 09:43 01/24/16 19:50 10.2640.1550.154U0.134Thorium 234

pCi/g 01/22/16 09:43 01/24/16 19:50 10.09120.03380.0337U0.0233Uranium 235

pCi/g 01/22/16 09:43 01/24/16 19:50 10.02340.03520.03370.0969Thorium 232

Tl-208 0.0346 0.0115 0.0120 0.0106 pCi/g 01/22/16 09:43 01/24/16 19:50 1


Count Total

Other Detected

Radionuclides

Uncert. Uncert.







Analyte


(2σ+/-)

0.0248

(2σ+/-)

101/28/16 22:3201/20/16 16:10pCi/g0.1931.13

RL MDC

0.0248


Count Total

Uncert. Uncert.


Page 22 of 46 1/29/2016

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101112


Project/Site: HDP



Re 30 - 110

Carrier

01/20/16 16:10 01/28/16 22:32 1


101




Analyte

Actinium 228 1.03

(2σ+/-)

0.174

(2σ+/-)

101/24/16 19:5001/22/16 09:43pCi/g0.106

RL MDC

0.139


Count Total

Uncert. Uncert.

pCi/g 01/22/16 09:43 01/24/16 19:50 10.09000.05350.0535U0.0117Americium 241

pCi/g 01/22/16 09:43 01/24/16 19:50 10.2600.3670.3331.51Bismuth 212

pCi/g 01/22/16 09:43 01/24/16 19:50 10.06250.1190.08700.794Bismuth 214

pCi/g 01/22/16 09:43 01/24/16 19:50 10.06810.1390.07800.886Lead 212

pCi/g 01/22/16 09:43 01/24/16 19:50 10.06880.1270.08110.941Lead 214

pCi/g 01/22/16 09:43 01/24/16 19:50 10.3342.161.0418.8Potassium 40

pCi/g 01/22/16 09:43 01/24/16 19:50 12.312.702.626.63Protactinium 234m


pCi/g 01/22/16 09:43 01/24/16 19:50 10.06250.1190.08700.794Radium 226

pCi/g 01/22/16 09:43 01/24/16 19:50 10.7300.6090.5921.37Thorium 234

pCi/g 01/22/16 09:43 01/24/16 19:50 10.2220.1330.132U0.112Uranium 235

pCi/g 01/22/16 09:43 01/24/16 19:50 10.1060.1740.1391.03Thorium 232

Tl-208 0.302 0.0375 0.0487 0.0282 pCi/g 01/22/16 09:43 01/24/16 19:50 1


Count Total

Other Detected

Radionuclides

Uncert. Uncert.







Analyte


(2σ+/-)

0.0361

(2σ+/-)

101/28/16 19:5701/20/16 17:35pCi/g0.2181.28

RL MDC

0.0359


Count Total

Uncert. Uncert.

Re 30 - 110

Carrier

01/20/16 17:35 01/28/16 19:57 1


100


Page 23 of 46 1/29/2016

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101112


Project/Site: HDP




Analyte

Actinium 228 1.03

(2σ+/-)

0.162

(2σ+/-)

101/24/16 19:5201/22/16 09:43pCi/g0.0674

RL MDC

0.123


Count Total

Uncert. Uncert.

pCi/g 01/22/16 09:43 01/24/16 19:52 10.09280.05500.0550U-0.000866Americium 241

pCi/g 01/22/16 09:43 01/24/16 19:52 10.3300.3990.3731.38Bismuth 212

pCi/g 01/22/16 09:43 01/24/16 19:52 10.06090.1230.08840.825Bismuth 214

pCi/g 01/22/16 09:43 01/24/16 19:52 10.05050.1460.06631.01Lead 212

pCi/g 01/22/16 09:43 01/24/16 19:52 10.06090.1260.07710.960Lead 214

pCi/g 01/22/16 09:43 01/24/16 19:52 10.3212.041.0217.3Potassium 40



pCi/g 01/22/16 09:43 01/24/16 19:52 10.06090.1230.08840.825Radium 226

pCi/g 01/22/16 09:43 01/24/16 19:52 10.6670.2460.2350.709Thorium 234

pCi/g 01/22/16 09:43 01/24/16 19:52 10.2040.1200.120U0.0586Uranium 235

pCi/g 01/22/16 09:43 01/24/16 19:52 10.06740.1620.1231.03Thorium 232

Tl-208 0.335 0.0412 0.0539 0.0302 pCi/g 01/22/16 09:43 01/24/16 19:52 1


Count Total

Other Detected

Radionuclides

Uncert. Uncert.







Analyte


(2σ+/-)

0.0281

(2σ+/-)

101/28/16 20:0901/20/16 17:35pCi/g0.2101.22

RL MDC

0.0281


Count Total

Uncert. Uncert.

Re 30 - 110

Carrier

01/20/16 17:35 01/28/16 20:09 1


101




Analyte

Actinium 228 0.0730 U

(2σ+/-)

0.0478

(2σ+/-)

101/24/16 19:5301/22/16 09:43pCi/g0.0860

RL MDC

0.0473


Count Total

Uncert. Uncert.

pCi/g 01/22/16 09:43 01/24/16 19:53 10.03940.02300.0230U-0.00551Americium 241

pCi/g 01/22/16 09:43 01/24/16 19:53 10.2820.1600.160U0.0606Bismuth 212

pCi/g 01/22/16 09:43 01/24/16 19:53 10.02110.04200.03810.170Bismuth 214

pCi/g 01/22/16 09:43 01/24/16 19:53 10.02790.03370.02920.130Lead 212


Page 24 of 46 1/29/2016

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Project/Site: HDP




Analyte

Lead 214 0.206

(2σ+/-)

0.0422

(2σ+/-)

101/24/16 19:5301/22/16 09:43pCi/g0.0269

RL MDC

0.0364


Count Total

Uncert. Uncert.

pCi/g 01/22/16 09:43 01/24/16 19:53 10.2060.6390.5163.68Potassium 40



pCi/g 01/22/16 09:43 01/24/16 19:53 10.02110.04200.03810.170Radium 226

pCi/g 01/22/16 09:43 01/24/16 19:53 10.4000.1720.168U0.344Thorium 234

pCi/g 01/22/16 09:43 01/24/16 19:53 10.08010.02570.0257U0.00171Uranium 235

pCi/g 01/22/16 09:43 01/24/16 19:53 10.08600.04780.0473U0.0730Thorium 232

Tl-208 0.0403 0.0170 0.0175 0.0158 pCi/g 01/22/16 09:43 01/24/16 19:53 1


Count Total

Other Detected

Radionuclides

Uncert. Uncert.







Analyte


(2σ+/-)

0.0332

(2σ+/-)

101/28/16 20:1301/20/16 17:35pCi/g0.1761.03

RL MDC

0.0332


Count Total

Uncert. Uncert.

Re 30 - 110

Carrier

01/20/16 17:35 01/28/16 20:13 1


104




Analyte

Actinium 228 0.550

(2σ+/-)

0.0980

(2σ+/-)

101/24/16 20:2501/22/16 09:43pCi/g0.0662

RL MDC

0.0803


Count Total

Uncert. Uncert.

pCi/g 01/22/16 09:43 01/24/16 20:25 10.06750.04020.0402U0.00945Americium 241

pCi/g 01/22/16 09:43 01/24/16 20:25 10.2360.2830.2700.834Bismuth 212

pCi/g 01/22/16 09:43 01/24/16 20:25 10.04770.08120.06460.474Bismuth 214

pCi/g 01/22/16 09:43 01/24/16 20:25 10.04480.08530.04990.534Lead 212

pCi/g 01/22/16 09:43 01/24/16 20:25 10.04280.08190.05690.567Lead 214

pCi/g 01/22/16 09:43 01/24/16 20:25 10.1681.190.6739.56Potassium 40



pCi/g 01/22/16 09:43 01/24/16 20:25 10.04770.08120.06460.474Radium 226


Page 25 of 46 1/29/2016

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101112


Project/Site: HDP




Analyte

Thorium 234 0.510 U

(2σ+/-)

0.339

(2σ+/-)

101/24/16 20:2501/22/16 09:43pCi/g0.545

RL MDC

0.335


Count Total

Uncert. Uncert.

pCi/g 01/22/16 09:43 01/24/16 20:25 10.1480.09620.0958U0.0852Uranium 235

pCi/g 01/22/16 09:43 01/24/16 20:25 10.06620.09800.08030.550Thorium 232

Tl-208 0.180 0.0313 0.0365 0.0259 pCi/g 01/22/16 09:43 01/24/16 20:25 1


Count Total

Other Detected

Radionuclides

Uncert. Uncert.







Analyte


(2σ+/-)

0.0385

(2σ+/-)

101/28/16 20:1701/20/16 17:35pCi/g0.1791.05

RL MDC

0.0385


Count Total

Uncert. Uncert.

Re 30 - 110

Carrier

01/20/16 17:35 01/28/16 20:17 1


103




Analyte

Actinium 228 1.08

(2σ+/-)

0.170

(2σ+/-)

101/24/16 20:2601/22/16 09:43pCi/g0.0800

RL MDC

0.129


Count Total

Uncert. Uncert.

pCi/g 01/22/16 09:43 01/24/16 20:26 10.09160.05430.0543U0.00422Americium 241

pCi/g 01/22/16 09:43 01/24/16 20:26 10.3480.4430.4151.50Bismuth 212

pCi/g 01/22/16 09:43 01/24/16 20:26 10.06250.1220.08920.807Bismuth 214

pCi/g 01/22/16 09:43 01/24/16 20:26 10.06300.1500.07680.993Lead 212

pCi/g 01/22/16 09:43 01/24/16 20:26 10.07190.1380.09580.957Lead 214

pCi/g 01/22/16 09:43 01/24/16 20:26 10.2332.181.1418.2Potassium 40



pCi/g 01/22/16 09:43 01/24/16 20:26 10.06250.1220.08920.807Radium 226

pCi/g 01/22/16 09:43 01/24/16 20:26 10.7080.2700.2580.754Thorium 234

pCi/g 01/22/16 09:43 01/24/16 20:26 10.1380.07980.0792U0.101Uranium 235

pCi/g 01/22/16 09:43 01/24/16 20:26 10.08000.1700.1291.08Thorium 232


Page 26 of 46 1/29/2016

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Project/Site: HDP



Tl-208 0.375 0.0486 0.0623 0.0351 pCi/g 01/22/16 09:43 01/24/16 20:26 1


Count Total

Other Detected

Radionuclides

Uncert. Uncert.







Analyte


(2σ+/-)

0.00466

(2σ+/-)

101/28/16 20:2101/20/16 17:35pCi/g0.2031.19

RL MDC

0.00460


Count Total

Uncert. Uncert.

Re 30 - 110

Carrier

01/20/16 17:35 01/28/16 20:21 1


101




Analyte

Actinium 228 0.0773

(2σ+/-)

0.0395

(2σ+/-)

101/24/16 20:2701/22/16 09:43pCi/g0.0623

RL MDC

0.0387


Count Total

Uncert. Uncert.

pCi/g 01/22/16 09:43 01/24/16 20:27 10.02850.01600.0160U0.00149Americium 241

pCi/g 01/22/16 09:43 01/24/16 20:27 10.2170.1200.120U0.00896Bismuth 212

pCi/g 01/22/16 09:43 01/24/16 20:27 10.02380.03530.03100.164Bismuth 214

pCi/g 01/22/16 09:43 01/24/16 20:27 10.02150.02470.02110.0987Lead 212

pCi/g 01/22/16 09:43 01/24/16 20:27 10.02920.03110.02740.141Lead 214

pCi/g 01/22/16 09:43 01/24/16 20:27 10.1830.4620.3552.95Potassium 40



pCi/g 01/22/16 09:43 01/24/16 20:27 10.02380.03530.03100.164Radium 226

pCi/g 01/22/16 09:43 01/24/16 20:27 10.2830.1000.0994U0.140Thorium 234

pCi/g 01/22/16 09:43 01/24/16 20:27 10.06910.03280.0327U0.0297Uranium 235

pCi/g 01/22/16 09:43 01/24/16 20:27 10.06230.03950.03870.0773Thorium 232

Tl-208 0.0302 0.0106 0.0110 0.0120 pCi/g 01/22/16 09:43 01/24/16 20:27 1


Count Total

Other Detected

Radionuclides

Uncert. Uncert.


Page 27 of 46 1/29/2016

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101112


Project/Site: HDP







Analyte


(2σ+/-)

0.0440

(2σ+/-)

101/28/16 20:2501/20/16 17:35pCi/g0.1801.05

RL MDC

0.0440


Count Total

Uncert. Uncert.

Re 30 - 110

Carrier

01/20/16 17:35 01/28/16 20:25 1


103




Analyte

Actinium 228 0.780

(2σ+/-)

0.119

(2σ+/-)

101/24/16 20:2801/22/16 09:43pCi/g0.0658

RL MDC

0.0886


Count Total

Uncert. Uncert.

pCi/g 01/22/16 09:43 01/24/16 20:28 10.07930.04750.0474U-0.0165Americium 241

pCi/g 01/22/16 09:43 01/24/16 20:28 10.2980.3820.3581.31Bismuth 212

pCi/g 01/22/16 09:43 01/24/16 20:28 10.04900.09210.06950.582Bismuth 214

pCi/g 01/22/16 09:43 01/24/16 20:28 10.04860.1190.06090.791Lead 212

pCi/g 01/22/16 09:43 01/24/16 20:28 10.05210.1060.06630.790Lead 214

pCi/g 01/22/16 09:43 01/24/16 20:28 10.1781.700.87614.3Potassium 40



pCi/g 01/22/16 09:43 01/24/16 20:28 10.04900.09210.06950.582Radium 226

pCi/g 01/22/16 09:43 01/24/16 20:28 10.6600.4250.4140.922Thorium 234

pCi/g 01/22/16 09:43 01/24/16 20:28 10.1820.1100.110U0.0613Uranium 235

pCi/g 01/22/16 09:43 01/24/16 20:28 10.06580.1190.08860.780Thorium 232

Tl-208 0.257 0.0356 0.0444 0.0248 pCi/g 01/22/16 09:43 01/24/16 20:28 1


Count Total

Other Detected

Radionuclides

Uncert. Uncert.







Analyte


(2σ+/-)

0.0598

(2σ+/-)

101/28/16 20:2801/20/16 17:35pCi/g0.2011.17

RL MDC

0.0596


Count Total

Uncert. Uncert.


Page 28 of 46 1/29/2016

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101112


Project/Site: HDP



Re 30 - 110

Carrier

01/20/16 17:35 01/28/16 20:28 1


100




Analyte

Actinium 228 1.15

(2σ+/-)

0.214

(2σ+/-)

101/24/16 20:2901/22/16 10:00pCi/g0.128

RL MDC

0.179


Count Total

Uncert. Uncert.

pCi/g 01/22/16 10:00 01/24/16 20:29 10.1180.06980.0698U-0.00452Americium 241

pCi/g 01/22/16 10:00 01/24/16 20:29 10.4230.4100.3861.31Bismuth 212

pCi/g 01/22/16 10:00 01/24/16 20:29 10.08180.1740.1311.10Bismuth 214

pCi/g 01/22/16 10:00 01/24/16 20:29 10.08490.1670.09591.05Lead 212

pCi/g 01/22/16 10:00 01/24/16 20:29 10.08650.1580.1081.11Lead 214

pCi/g 01/22/16 10:00 01/24/16 20:29 10.4392.301.3917.9Potassium 40



pCi/g 01/22/16 10:00 01/24/16 20:29 10.08180.1740.1311.10Radium 226

pCi/g 01/22/16 10:00 01/24/16 20:29 10.9590.6210.6051.31Thorium 234

pCi/g 01/22/16 10:00 01/24/16 20:29 10.2450.1510.150U0.149Uranium 235

pCi/g 01/22/16 10:00 01/24/16 20:29 10.1280.2140.1791.15Thorium 232

Tl-208 0.428 0.0584 0.0734 0.0376 pCi/g 01/22/16 10:00 01/24/16 20:29 1


Count Total

Other Detected

Radionuclides

Uncert. Uncert.







Analyte


(2σ+/-)

0.0312

(2σ+/-)

101/28/16 20:3201/20/16 17:35pCi/g0.2131.24

RL MDC

0.0312


Count Total

Uncert. Uncert.

Re 30 - 110

Carrier

01/20/16 17:35 01/28/16 20:32 1


100


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Project/Site: HDP




Analyte

Actinium 228 0.220

(2σ+/-)

0.0606

(2σ+/-)

101/24/16 21:0601/22/16 10:00pCi/g0.0609

RL MDC

0.0564


Count Total

Uncert. Uncert.

pCi/g 01/22/16 10:00 01/24/16 21:06 10.04750.4380.438U-0.00669Americium 241

pCi/g 01/22/16 10:00 01/24/16 21:06 10.2490.1600.159U0.196Bismuth 212

pCi/g 01/22/16 10:00 01/24/16 21:06 10.03510.05520.04620.294Bismuth 214

pCi/g 01/22/16 10:00 01/24/16 21:06 10.03170.04800.03360.264Lead 212

pCi/g 01/22/16 10:00 01/24/16 21:06 10.03640.05480.04320.323Lead 214

pCi/g 01/22/16 10:00 01/24/16 21:06 10.1830.7410.4845.58Potassium 40



pCi/g 01/22/16 10:00 01/24/16 21:06 10.03510.05520.04620.294Radium 226

pCi/g 01/22/16 10:00 01/24/16 21:06 10.3590.1310.127U0.338Thorium 234

pCi/g 01/22/16 10:00 01/24/16 21:06 10.1230.07510.0746U0.0785Uranium 235

pCi/g 01/22/16 10:00 01/24/16 21:06 10.06090.06060.05640.220Thorium 232

Tl-208 0.0910 0.0195 0.0216 0.0166 pCi/g 01/22/16 10:00 01/24/16 21:06 1


Count Total

Other Detected

Radionuclides

Uncert. Uncert.




Technetium 99 0.000017 J 0.000053 0.000016 mg/Kg ☼ 01/20/16 17:35 01/28/16 20:48 1



Analyte

Technetium 99 0.288

(2σ+/-)

0.0419

(2σ+/-)

101/28/16 20:4801/20/16 17:35pCi/g0.1821.06

RL MDC

0.0324


Count Total

Uncert. Uncert.

Re 30 - 110

Carrier

01/20/16 17:35 01/28/16 20:48 1


102




Analyte

Actinium 228 0.894

(2σ+/-)

0.139

(2σ+/-)

101/24/16 21:0701/22/16 10:00pCi/g0.0970

RL MDC

0.104


Count Total

Uncert. Uncert.

pCi/g 01/22/16 10:00 01/24/16 21:07 10.08760.05300.0529U0.0336Americium 241

pCi/g 01/22/16 10:00 01/24/16 21:07 10.3120.3570.3381.11Bismuth 212

pCi/g 01/22/16 10:00 01/24/16 21:07 10.05880.1210.09000.783Bismuth 214

pCi/g 01/22/16 10:00 01/24/16 21:07 10.05410.1370.06750.918Lead 212


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Project/Site: HDP




Analyte

Lead 214 0.835

(2σ+/-)

0.114

(2σ+/-)

101/24/16 21:0701/22/16 10:00pCi/g0.0548

RL MDC

0.0741


Count Total

Uncert. Uncert.

pCi/g 01/22/16 10:00 01/24/16 21:07 10.3841.891.0215.6Potassium 40

pCi/g 01/22/16 10:00 01/24/16 21:07 14.152.062.014.71Protactinium 234m


pCi/g 01/22/16 10:00 01/24/16 21:07 10.05880.1210.09000.783Radium 226

pCi/g 01/22/16 10:00 01/24/16 21:07 10.6880.4700.4471.41Thorium 234

pCi/g 01/22/16 10:00 01/24/16 21:07 10.2010.1330.132U0.133Uranium 235

pCi/g 01/22/16 10:00 01/24/16 21:07 10.09700.1390.1040.894Thorium 232

Tl-208 0.319 0.0426 0.0540 0.0313 pCi/g 01/22/16 10:00 01/24/16 21:07 1


Count Total

Other Detected

Radionuclides

Uncert. Uncert.




Technetium 99 0.000027 J 0.000062 0.000019 mg/Kg ☼ 01/20/16 17:35 01/28/16 20:52 1



Analyte

Technetium 99 0.464

(2σ+/-)

0.0477

(2σ+/-)

101/28/16 20:5201/20/16 17:35pCi/g0.2141.25

RL MDC

0.0212


Count Total

Uncert. Uncert.

Re 30 - 110

Carrier

01/20/16 17:35 01/28/16 20:52 1


100




Analyte

Actinium 228 1.03

(2σ+/-)

0.151

(2σ+/-)

101/24/16 21:5501/22/16 10:00pCi/g0.110

RL MDC

0.108


Count Total

Uncert. Uncert.

pCi/g 01/22/16 10:00 01/24/16 21:55 10.09330.05570.0557U-0.0129Americium 241

pCi/g 01/22/16 10:00 01/24/16 21:55 10.3050.3620.3401.20Bismuth 212

pCi/g 01/22/16 10:00 01/24/16 21:55 10.05610.1200.08350.826Bismuth 214

pCi/g 01/22/16 10:00 01/24/16 21:55 10.05730.1490.07061.01Lead 212

pCi/g 01/22/16 10:00 01/24/16 21:55 10.05680.1190.07760.868Lead 214

pCi/g 01/22/16 10:00 01/24/16 21:55 10.3652.091.0417.7Potassium 40



pCi/g 01/22/16 10:00 01/24/16 21:55 10.05610.1200.08350.826Radium 226


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Analyte

Thorium 234 1.02

(2σ+/-)

0.285

(2σ+/-)

101/24/16 21:5501/22/16 10:00pCi/g0.716

RL MDC

0.265


Count Total

Uncert. Uncert.

pCi/g 01/22/16 10:00 01/24/16 21:55 10.2150.1210.121U0.131Uranium 235

pCi/g 01/22/16 10:00 01/24/16 21:55 10.1100.1510.1081.03Thorium 232

Tl-208 0.354 0.0454 0.0584 0.0336 pCi/g 01/22/16 10:00 01/24/16 21:55 1


Count Total

Other Detected

Radionuclides

Uncert. Uncert.







Analyte


(2σ+/-)

0.0252

(2σ+/-)

101/28/16 20:5501/20/16 17:35pCi/g0.2121.24

RL MDC

0.0249


Count Total

Uncert. Uncert.

Re 30 - 110

Carrier

01/20/16 17:35 01/28/16 20:55 1


101

Lab Sample ID: 160-15789-25Client Sample ID: B02-01-02-P-R-Q-00Matrix: SolidDate Collected: 01/04/16 09:25



Analyte

Actinium 228 0.638

(2σ+/-)

0.119

(2σ+/-)

101/24/16 21:5601/22/16 10:00pCi/g0.0719

RL MDC

0.0993


Count Total

Uncert. Uncert.

pCi/g 01/22/16 10:00 01/24/16 21:56 10.07130.02310.0231U0.000Americium 241

pCi/g 01/22/16 10:00 01/24/16 21:56 10.2110.3130.2921.08Bismuth 212

pCi/g 01/22/16 10:00 01/24/16 21:56 10.05200.09370.07520.538Bismuth 214

pCi/g 01/22/16 10:00 01/24/16 21:56 10.04550.09700.05720.605Lead 212

pCi/g 01/22/16 10:00 01/24/16 21:56 10.06770.09750.07270.624Lead 214

pCi/g 01/22/16 10:00 01/24/16 21:56 10.3071.460.90911.1Potassium 40



pCi/g 01/22/16 10:00 01/24/16 21:56 10.05200.09370.07520.538Radium 226

pCi/g 01/22/16 10:00 01/24/16 21:56 10.5900.3870.3770.832Thorium 234

pCi/g 01/22/16 10:00 01/24/16 21:56 10.1550.1170.1160.180Uranium 235

pCi/g 01/22/16 10:00 01/24/16 21:56 10.07190.1190.09930.638Thorium 232


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Project/Site: HDP



Tl-208 0.188 0.0323 0.0377 0.0239 pCi/g 01/22/16 10:00 01/24/16 21:56 1


Count Total

Other Detected

Radionuclides

Uncert. Uncert.







Analyte


(2σ+/-)

0.00323

(2σ+/-)

101/28/16 20:5901/20/16 17:35pCi/g0.2011.18

RL MDC

0.00294


Count Total

Uncert. Uncert.

Re 30 - 110

Carrier

01/20/16 17:35 01/28/16 20:59 1


101

Lab Sample ID: 160-15789-26Client Sample ID: B02-01-10-P-S-Q-00Matrix: SolidDate Collected: 12/31/15 10:45



Analyte

Actinium 228 0.156

(2σ+/-)

0.0485

(2σ+/-)

101/24/16 21:5701/22/16 10:00pCi/g0.0464

RL MDC

0.0459


Count Total

Uncert. Uncert.

pCi/g 01/22/16 10:00 01/24/16 21:57 10.03590.02940.0294U-0.00111Americium 241

pCi/g 01/22/16 10:00 01/24/16 21:57 10.1840.1040.104U0.0395Bismuth 212

pCi/g 01/22/16 10:00 01/24/16 21:57 10.02680.03690.03270.166Bismuth 214

pCi/g 01/22/16 10:00 01/24/16 21:57 10.02060.02680.02160.122Lead 212

pCi/g 01/22/16 10:00 01/24/16 21:57 10.03330.03430.02940.170Lead 214

pCi/g 01/22/16 10:00 01/24/16 21:57 10.2240.4790.3782.93Potassium 40



pCi/g 01/22/16 10:00 01/24/16 21:57 10.02680.03690.03270.166Radium 226

pCi/g 01/22/16 10:00 01/24/16 21:57 10.3130.2420.240U0.303Thorium 234

pCi/g 01/22/16 10:00 01/24/16 21:57 10.09550.04240.0423U0.0320Uranium 235

pCi/g 01/22/16 10:00 01/24/16 21:57 10.04640.04850.04590.156Thorium 232

Tl-208 0.0354 0.0117 0.0123 0.0128 pCi/g 01/22/16 10:00 01/24/16 21:57 1


Count Total

Other Detected

Radionuclides

Uncert. Uncert.


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Project/Site: HDP

Lab Sample ID: 160-15789-26Client Sample ID: B02-01-10-P-S-Q-00Matrix: SolidDate Collected: 12/31/15 10:45






Analyte


(2σ+/-)

0.00282

(2σ+/-)

101/28/16 21:0301/20/16 17:35pCi/g0.1921.12

RL MDC

0.00253


Count Total

Uncert. Uncert.

Re 30 - 110

Carrier

01/20/16 17:35 01/28/16 21:03 1


100


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QC Sample ResultsTestAmerica Job ID: 160-15789-1Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP

Method: 6020A - Metals (ICP/MS), Tc-99

Client Sample ID: Method BlankLab Sample ID: MB 160-233463/1-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 235007 Prep Batch: 233463

RL MDL

Technetium 99 ND 0.000048 0.000014 mg/Kg 01/20/16 16:10 01/28/16 21:07 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-233463/2-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 235007 Prep Batch: 233463

Technetium 99 0.00123 0.00111 mg/Kg 90 80 - 120

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

Client Sample ID: B02-01-01-P-S-S-00Lab Sample ID: 160-15789-1 MSMatrix: Solid Prep Type: Total/NAAnalysis Batch: 235007 Prep Batch: 233463

Technetium 99 ND 0.00135 0.00121 mg/Kg 90 75 - 125☼

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Client Sample ID: B02-01-01-P-S-S-00Lab Sample ID: 160-15789-1 MSDMatrix: Solid Prep Type: Total/NAAnalysis Batch: 235007 Prep Batch: 233463

Technetium 99 ND 0.00135 0.00122 mg/Kg 91 75 - 125 1 30☼

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD


RL MDL

Technetium 99 ND 0.000048 0.000014 mg/Kg 01/20/16 17:35 01/28/16 19:38 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier


Technetium 99 0.00123 0.00113 mg/Kg 92 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Client Sample ID: B02-01-14-P-R-S-00Lab Sample ID: 160-15789-14 MSMatrix: Solid Prep Type: Total/NAAnalysis Batch: 235007 Prep Batch: 233467

Technetium 99 ND 0.00157 0.00144 mg/Kg 91 75 - 125☼

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Client Sample ID: B02-01-14-P-R-S-00Lab Sample ID: 160-15789-14 MSDMatrix: Solid Prep Type: Total/NAAnalysis Batch: 235007 Prep Batch: 233467

Technetium 99 ND 0.00157 0.00142 mg/Kg 91 75 - 125 1 30☼

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD


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Technetium 99

Analyte

U 101/28/16 21:0701/20/16 16:10pCi/g0.164

MDC

0.959

RL

0.009060.00901

(2σ+/-) (2σ+/-)

MB

-0.009846

MB

Dil FacPrepared AnalyzedUnitResult Qualifier

Uncert.

Count

Uncert.

Total

Carrier

Re 30 - 110 01/20/16 16:10 01/28/16 21:07 1

Dil FacPrepared AnalyzedQualifier Limits%Yield

104

MB MB


Technetium 99

Analyte

120-809018.9421.0 1.92 0.955 0.164

RL MDC(2σ+/-)

LCS LCS

pCi/g

UnitResult Qual %RecAdded

Spike

Limits

%Rec.Uncert.

Total

Re

Carrier

30 - 110

LCS

Qualifier Limits%Yield

105

LCS

Client Sample ID: B02-01-01-P-S-S-00Lab Sample ID: 160-15789-1 MSMatrix: Solid Prep Type: Total/NAAnalysis Batch: 235008 Prep Batch: 233463

Technetium 99

Analyte

125-759020.7823.1-0.0261 U 1.96 1.08 0.185

RL MDC(2σ+/-)

MS MS

pCi/g


Spike

Result

Sample Sample

Qual Limits

%Rec.Uncert.

Total

Re

Carrier

30 - 110

MS


102

MS

Client Sample ID: B02-01-01-P-S-S-00Lab Sample ID: 160-15789-1 MSDMatrix: Solid Prep Type: Total/NAAnalysis Batch: 235008 Prep Batch: 233463

Technetium 99

Analyte

10.04125-759120.9523.1-0.0261 U 2.13 1.07 0.183

RL MDC(2σ+/-)

MSD MSD

pCi/g

UnitResult Qual %Rec LimitAdded

Spike

Result

Sample Sample

Qual Limits

%Rec.Uncert.

Total

RER

RER

Re

Carrier

30 - 110

MSD


103

MSD


Technetium 99

Analyte

U 101/28/16 19:3801/20/16 17:35pCi/g0.164

MDC

0.959

RL

0.004180.00259

(2σ+/-) (2σ+/-)

MB

-0.03562

MB


Uncert.

Count

Uncert.

Total


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Project/Site: HDP

Method: 6020A - Metals (ICP/MS), Tc-99 in Activity (Continued)


Carrier

Re 30 - 110 01/20/16 17:35 01/28/16 19:38 1

Dil FacPrepared AnalyzedQualifier Limits%Yield

104

MB MB


Technetium 99

Analyte

120-809219.4321.0 1.88 0.965 0.165

RL MDC(2σ+/-)

LCS LCS

pCi/g


Spike

Limits

%Rec.Uncert.

Total

Re

Carrier

30 - 110

LCS


104

LCS

Client Sample ID: B02-01-14-P-R-S-00Lab Sample ID: 160-15789-14 MSMatrix: Solid Prep Type: Total/NAAnalysis Batch: 235008 Prep Batch: 233467

Technetium 99

Analyte

125-759124.6026.90.0404 U 2.67 1.27 0.218

RL MDC(2σ+/-)

MS MS

pCi/g


Spike

Result

Sample Sample

Qual Limits

%Rec.Uncert.

Total

Re

Carrier

30 - 110

MS


101

MS

Client Sample ID: B02-01-14-P-R-S-00Lab Sample ID: 160-15789-14 MSDMatrix: Solid Prep Type: Total/NAAnalysis Batch: 235008 Prep Batch: 233467

Technetium 99

Analyte

10.06125-759124.3226.80.0404 U 2.31 1.28 0.219

RL MDC(2σ+/-)

MSD MSD

pCi/g

UnitResult Qual %Rec LimitAdded

Spike

Result

Sample Sample

Qual Limits

%Rec.Uncert.

Total

RER

RER

Re

Carrier

30 - 110

MSD


99

MSD



Actinium 228

Analyte

U 101/24/16 17:5901/22/16 09:43pCi/g0.0535

MDCRL

0.03090.0309

(2σ+/-) (2σ+/-)

MB

0.01798

MB


Uncert.

Count

Uncert.

Total

101/24/16 17:5901/22/16 09:43pCi/g0.02440.01330.0133U-0.0001374Americium 241

101/24/16 17:5901/22/16 09:43pCi/g0.2160.05510.0551U0.0000Bismuth 212

101/24/16 17:5901/22/16 09:43pCi/g0.04200.006740.00674U-0.0007974Bismuth 214


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Project/Site: HDP



Lead 212

Analyte

U 101/24/16 17:5901/22/16 09:43pCi/g0.0319

MDCRL

0.2940.294

(2σ+/-) (2σ+/-)

MB

-0.007355

MB


Uncert.

Count

Uncert.

Total

101/24/16 17:5901/22/16 09:43pCi/g0.03670.4880.488U-0.01219Lead 214

101/24/16 17:5901/22/16 09:43pCi/g0.2870.2090.209U-0.02888Potassium 40

101/24/16 17:5901/22/16 09:43pCi/g1.210.3300.330U0.0000Protactinium 234m

101/24/16 17:5901/22/16 09:43pCi/g0.3480.02040.0204U-0.008926Protactinium 231

101/24/16 17:5901/22/16 09:43pCi/g0.04200.006740.00674U-0.0007974Radium 226

101/24/16 17:5901/22/16 09:43pCi/g0.2370.02170.0217U0.007387Thorium 234

101/24/16 17:5901/22/16 09:43pCi/g0.06990.03910.0391U-0.007831Uranium 235

101/24/16 17:5901/22/16 09:43pCi/g0.05350.03090.0309U0.01798Thorium 232

Other Detected

Radionuclide

None

MB

(2σ+/-) (2σ+/-) MDCRL

pCi/g 01/22/16 09:43 01/24/16 17:59 1

MB


Uncert.

Count

Uncert.

Total

Radionuclides

Other Detected


Americium 241

Analyte

116-87106107.1101 11.2 0.529

RL MDC(2σ+/-)

LCS LCS

pCi/g


Spike

Limits

%Rec.Uncert.

Total

Cesium 137 34.2 37.48 3.87 0.200 0.159 pCi/g 109 87 - 120

Cobalt 60 32.5 34.86 3.46 0.0940 pCi/g 107 87 - 115

Client Sample ID: B02-01-01-P-S-S-00Lab Sample ID: 160-15789-1 DUMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233897 Prep Batch: 233602

Actinium 228

Analyte

10.660.067430.117 0.0338 0.0498

RL MDC(2σ+/-)

DU DU

pCi/g

UnitResult Qual LimitResult

Sample Sample

Qual

Uncert.

Total

RER

RER

Americium 241 0.0109 U -0.00429

4

U 0.0213 0.0362 pCi/g 0.38 1

Bismuth 212 0.0687 U 0.02679 U 0.0980 0.175 pCi/g 0.20 1

Bismuth 214 0.159 0.1795 0.0365 0.0197 pCi/g 0.28 1

Lead 212 0.0998 0.08508 0.0300 0.0305 pCi/g 0.26 1

Lead 214 0.168 0.1697 0.0305 0.0234 pCi/g 0.03 1

Potassium 40 2.53 2.270 0.381 0.140 pCi/g 0.31 1

Protactinium

234m

0.532 U 0.7488 U 0.769 1.64 pCi/g 0.14 1

Protactinium 231 0.0877 U 0.08078 U 0.102 0.335 pCi/g 0.02 1

Radium 226 0.159 0.1795 0.0365 0.0197 pCi/g 0.28 1

Thorium 234 0.361 0.1348 U 0.112 0.331 pCi/g 0.62 1

Uranium 235 0.0187 U 0.04920 U 0.0439 0.0699 pCi/g 0.33 1

Thorium 232 0.117 0.06743 0.0338 0.0498 pCi/g 0.66 1


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Project/Site: HDP

Tl-208 10.990.018990.0440 0.0108 0.0149

RL MDC(2σ+/-)

DU DU

pCi/g


Sample Sample

Qual

Uncert.

RER

RER

Total

Other Detected

Radionuclides


Actinium 228

Analyte

U 101/24/16 21:0301/22/16 10:00pCi/g0.0923

MDCRL

0.04750.0475

(2σ+/-) (2σ+/-)

MB

0.002995

MB


Uncert.

Count

Uncert.

Total

101/24/16 21:0301/22/16 10:00pCi/g0.02360.01260.0126U0.0000561

2

Americium 241

101/24/16 21:0301/22/16 10:00pCi/g0.1420.06030.0603U-0.005028Bismuth 212

101/24/16 21:0301/22/16 10:00pCi/g0.03760.02080.0208U0.008034Bismuth 214

101/24/16 21:0301/22/16 10:00pCi/g0.02830.01810.0181U-0.001672Lead 212

101/24/16 21:0301/22/16 10:00pCi/g0.03110.01610.0161U0.001416Lead 214

101/24/16 21:0301/22/16 10:00pCi/g0.2743.453.45U-0.08620Potassium 40

101/24/16 21:0301/22/16 10:00pCi/g4.168.178.17U-1.227Protactinium 234m

101/24/16 21:0301/22/16 10:00pCi/g0.4350.2400.240U0.05978Protactinium 231

101/24/16 21:0301/22/16 10:00pCi/g0.03760.02080.0208U0.008034Radium 226

101/24/16 21:0301/22/16 10:00pCi/g0.3120.3610.361U-0.07351Thorium 234

101/24/16 21:0301/22/16 10:00pCi/g0.06000.01880.0188U0.006843Uranium 235

101/24/16 21:0301/22/16 10:00pCi/g0.09230.04750.0475U0.002995Thorium 232

Other Detected

Radionuclide

None

MB

(2σ+/-) (2σ+/-) MDCRL

pCi/g 01/22/16 10:00 01/24/16 21:03 1

MB


Uncert.

Count

Uncert.

Total

Radionuclides

Other Detected


Americium 241

Analyte

116-87100101.0101 10.5 0.493

RL MDC(2σ+/-)

LCS LCS

pCi/g


Spike

Limits

%Rec.Uncert.

Total

Cesium 137 34.2 33.41 3.50 0.200 0.161 pCi/g 98 87 - 120

Cobalt 60 32.5 31.23 3.15 0.135 pCi/g 96 87 - 115

Client Sample ID: B02-01-21-P-E-S-00Lab Sample ID: 160-15789-21 DUMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233900 Prep Batch: 233605

Actinium 228

Analyte

10.430.99331.15 0.160 0.101

RL MDC(2σ+/-)

DU DU

pCi/g


Sample Sample

Qual

Uncert.

Total

RER

RER

Americium 241 -0.00452 U -0.00782

3

U 0.0568 0.0957 pCi/g 0.03 1

Bismuth 212 1.31 1.073 0.369 0.346 pCi/g 0.31 1

Bismuth 214 1.10 0.9712 0.148 0.0725 pCi/g 0.40 1

Lead 212 1.05 1.138 0.170 0.0680 pCi/g 0.25 1

Lead 214 1.11 1.058 0.149 0.0749 pCi/g 0.17 1

Potassium 40 17.9 18.42 2.27 0.434 pCi/g 0.12 1

Protactinium

234m

-1.61 U 3.044 U 2.29 7.62 pCi/g 0.32 1

Protactinium 231 0.579 U 0.2836 U 0.192 1.18 pCi/g 0.59 1


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Project/Site: HDP


Client Sample ID: B02-01-21-P-E-S-00Lab Sample ID: 160-15789-21 DUMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233900 Prep Batch: 233605

Radium 226

Analyte

10.400.97121.10 0.148 0.0725

RL MDC(2σ+/-)

DU DU

pCi/g


Sample Sample

Qual

Uncert.

Total

RER

RER

Thorium 234 1.31 1.079 0.689 0.908 pCi/g 0.18 1

Uranium 235 0.149 U 0.1499 U 0.127 0.169 pCi/g 0 1

Thorium 232 1.15 0.9933 0.160 0.101 pCi/g 0.43 1

Bi-210 10.451.1701.76 0.557 0.732

RL MDC(2σ+/-)

DU DU

pCi/g


Sample Sample

Qual

Uncert.

RER

RER

Total

Other Detected

Radionuclides

Eu-152 0.0375 U 0.1577 0.0903 0.103 pCi/g 0.71 1

Pb-210 1.76 1.170 0.557 0.732 pCi/g 0.45 1

Po-210 1.76 1.170 0.557 0.732 pCi/g 0.45

Ra-224 1.05 1.138 0.170 0.0680 pCi/g 0.25 1

Ra-228 1.15 0.9933 0.160 0.101 pCi/g 0.43 1

Sc-46 0.0673 0.07409 0.0230 0.0415 pCi/g 0.13 1

Sn-126 0.0458 U 0.4506 0.226 0.349 pCi/g 0.85 1

Ta-182 0.363 0.4135 0.128 0.149 pCi/g 0.18 1

Th-228 1.05 1.138 0.170 0.0680 pCi/g 0.25 1

Tl-208 0.428 0.3473 0.0660 0.0435 pCi/g 0.58 1

U-238 1.31 1.079 0.689 0.908 pCi/g 0.18 1


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QC Association SummaryTestAmerica Job ID: 160-15789-1Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP

Metals

Prep Batch: 233463

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid None160-15789-1 B02-01-01-P-S-S-00 Total/NA

Solid None160-15789-1 MS B02-01-01-P-S-S-00 Total/NA

Solid None160-15789-1 MSD B02-01-01-P-S-S-00 Total/NA

Solid None160-15789-2 B02-01-02-P-R-S-00 Total/NA

Solid None160-15789-3 B02-01-03-P-E-S-00 Total/NA











Solid NoneLCS 160-233463/2-A Lab Control Sample Total/NA

Solid NoneMB 160-233463/1-A Method Blank Total/NA

Prep Batch: 233467



Solid None160-15789-14 MS B02-01-14-P-R-S-00 Total/NA

Solid None160-15789-14 MSD B02-01-14-P-R-S-00 Total/NA











Solid None160-15789-25 B02-01-02-P-R-Q-00 Total/NA

Solid None160-15789-26 B02-01-10-P-S-Q-00 Total/NA



Analysis Batch: 235007


Solid 6020A 233463160-15789-1 B02-01-01-P-S-S-00 Total/NA

Solid 6020A 233463160-15789-1 MS B02-01-01-P-S-S-00 Total/NA

Solid 6020A 233463160-15789-1 MSD B02-01-01-P-S-S-00 Total/NA

Solid 6020A 233463160-15789-2 B02-01-02-P-R-S-00 Total/NA

Solid 6020A 233463160-15789-3 B02-01-03-P-E-S-00 Total/NA








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Project/Site: HDP

Metals (Continued)

Analysis Batch: 235007 (Continued)







Solid 6020A 233467160-15789-14 MS B02-01-14-P-R-S-00 Total/NA

Solid 6020A 233467160-15789-14 MSD B02-01-14-P-R-S-00 Total/NA











Solid 6020A 233467160-15789-25 B02-01-02-P-R-Q-00 Total/NA

Solid 6020A 233467160-15789-26 B02-01-10-P-S-Q-00 Total/NA

Solid 6020A 233463LCS 160-233463/2-A Lab Control Sample Total/NA

Solid 6020A 233467LCS 160-233467/2-A Lab Control Sample Total/NA

Solid 6020A 233463MB 160-233463/1-A Method Blank Total/NA

Solid 6020A 233467MB 160-233467/1-A Method Blank Total/NA

General Chemistry

Analysis Batch: 233335


Solid Moisture160-15789-1 B02-01-01-P-S-S-00 Total/NA

Solid Moisture160-15789-1 DU B02-01-01-P-S-S-00 Total/NA

Solid Moisture160-15789-2 B02-01-02-P-R-S-00 Total/NA

Solid Moisture160-15789-3 B02-01-03-P-E-S-00 Total/NA




















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101112


Project/Site: HDP

General Chemistry (Continued)

Analysis Batch: 233335 (Continued)





Solid Moisture160-15789-25 B02-01-02-P-R-Q-00 Total/NA

Solid Moisture160-15789-26 B02-01-10-P-S-Q-00 Total/NA

Solid Moisture160-15789-26 DU B02-01-10-P-S-Q-00 Total/NA

Rad

Leach Batch: 233330


Solid Dry and Grind160-15789-1 B02-01-01-P-S-S-00 Total/NA

Solid Dry and Grind160-15789-1 DU B02-01-01-P-S-S-00 Total/NA

Solid Dry and Grind160-15789-2 B02-01-02-P-R-S-00 Total/NA

Solid Dry and Grind160-15789-3 B02-01-03-P-E-S-00 Total/NA



















Solid Dry and Grind160-15789-21 DU B02-01-21-P-E-S-00 Total/NA




Solid Dry and Grind160-15789-25 B02-01-02-P-R-Q-00 Total/NA

Solid Dry and Grind160-15789-26 B02-01-10-P-S-Q-00 Total/NA

Prep Batch: 233463



Solid None160-15789-1 MS B02-01-01-P-S-S-00 Total/NA

Solid None160-15789-1 MSD B02-01-01-P-S-S-00 Total/NA







Page 43 of 46 1/29/2016

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Project/Site: HDP

Rad (Continued)

Prep Batch: 233463 (Continued)











Prep Batch: 233467



Solid None160-15789-14 MS B02-01-14-P-R-S-00 Total/NA

Solid None160-15789-14 MSD B02-01-14-P-R-S-00 Total/NA











Solid None160-15789-25 B02-01-02-P-R-Q-00 Total/NA

Solid None160-15789-26 B02-01-10-P-S-Q-00 Total/NA



Prep Batch: 233602


Solid Fill_Geo-0 233330160-15789-1 B02-01-01-P-S-S-00 Total/NA

Solid Fill_Geo-0 233330160-15789-1 DU B02-01-01-P-S-S-00 Total/NA

Solid Fill_Geo-0 233330160-15789-2 B02-01-02-P-R-S-00 Total/NA

Solid Fill_Geo-0 233330160-15789-3 B02-01-03-P-E-S-00 Total/NA

















Page 44 of 46 1/29/2016

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Project/Site: HDP

Rad (Continued)

Prep Batch: 233602 (Continued)




Solid Fill_Geo-0LCS 160-233602/2-A Lab Control Sample Total/NA

Solid Fill_Geo-0MB 160-233602/1-A Method Blank Total/NA

Prep Batch: 233605



Solid Fill_Geo-0 233330160-15789-21 DU B02-01-21-P-E-S-00 Total/NA




Solid Fill_Geo-0 233330160-15789-25 B02-01-02-P-R-Q-00 Total/NA

Solid Fill_Geo-0 233330160-15789-26 B02-01-10-P-S-Q-00 Total/NA

Solid Fill_Geo-0LCS 160-233605/2-A Lab Control Sample Total/NA

Solid Fill_Geo-0MB 160-233605/1-A Method Blank Total/NA


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Tracer/Carrier SummaryTestAmerica Job ID: 160-15789-1Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP

Method: 6020A - Metals (ICP/MS), Tc-99 in ActivityPrep Type: Total/NAMatrix: Solid

Lab Sample ID Client Sample ID (30-110)

Re

103160-15789-1

Percent Yield (Acceptance Limits)

B02-01-01-P-S-S-00

102160-15789-1 MS B02-01-01-P-S-S-00

103160-15789-1 MSD B02-01-01-P-S-S-00

100160-15789-2 B02-01-02-P-R-S-00

101160-15789-3 B02-01-03-P-E-S-00

105160-15789-4 B02-01-04-P-S-S-00

102160-15789-5 B02-01-05-P-R-S-00

101160-15789-6 B02-01-06-P-E-S-00

104160-15789-7 B02-01-07-P-S-S-00

100160-15789-8 B02-01-08-P-R-S-00

101160-15789-9 B02-01-09-P-E-S-00

104160-15789-10 B02-01-10-P-S-S-00

100160-15789-11 B02-01-11-P-R-S-00

99160-15789-12 B02-01-12-P-E-S-00

101160-15789-13 B02-01-13-P-S-S-00

100160-15789-14 B02-01-14-P-R-S-00

101160-15789-14 MS B02-01-14-P-R-S-00

99160-15789-14 MSD B02-01-14-P-R-S-00

101160-15789-15 B02-01-15-P-E-S-00

104160-15789-16 B02-01-16-P-S-S-00

103160-15789-17 B02-01-17-P-R-S-00

101160-15789-18 B02-01-18-P-E-S-00

103160-15789-19 B02-01-19-P-S-S-00

100160-15789-20 B02-01-20-P-R-S-00

100160-15789-21 B02-01-21-P-E-S-00

102160-15789-22 B02-01-22-P-S-S-00

100160-15789-23 B02-01-23-P-R-S-00

101160-15789-24 B02-01-24-P-E-S-00

101160-15789-25 B02-01-02-P-R-Q-00

100160-15789-26 B02-01-10-P-S-Q-00

105LCS 160-233463/2-A Lab Control Sample

104LCS 160-233467/2-A Lab Control Sample

104MB 160-233463/1-A Method Blank

104MB 160-233467/1-A Method Blank

Tracer/Carrier Legend

Re = Re


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