ANALYTICAL REPORT 6 - Kentuckydep.gateway.ky.gov/publicfiles/Cabinet Records/Documents... ·...

ANALYTICAL REPORTTestAmerica Laboratories, Inc.TestAmerica St. Louis13715 Rider Trail NorthEarth City, MO 63045Tel: (314)298-8566

TestAmerica Job ID: 160-17284-1Client Project/Site: Blue Ridge Landfill

For:Commonwealth of Kentucky130 Eagle Nest DrivePaducah, Kentucky 42003

Attn: Gaye Brewer

Authorized for release by:6/13/2016 10:06:41 AM

Rhonda Ridenhower, Manager of Project Management(314)[email protected]

This report has been electronically signed and authorized by the signatory. Electronic signature isintended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

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Table of Contents

Client: Commonwealth of KentuckyProject/Site: Blue Ridge Landfill

TestAmerica Job ID: 160-17284-1

Page 2 of 66TestAmerica St. Louis

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Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1

Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2

Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3

Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6

Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12

Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13

Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14

Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15

Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16

QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 54

QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 61

Tracer Carrier Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 65

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Case NarrativeClient: Commonwealth of Kentucky TestAmerica Job ID: 160-17284-1Project/Site: Blue Ridge Landfill

Job ID: 160-17284-1

Laboratory: TestAmerica St. Louis

Narrative

CASE NARRATIVE

Client: Commonwealth of Kentucky

Project: Blue Ridge Landfill

Report Number: 160-17284-1

With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control

limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.

TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses

performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the application methods. TestAmerica’s operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data have been found to be compliant with laboratory protocols unless otherwise noted below.

The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions

to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory.

Calculations are performed before rounding to avoid round-off errors in calculated results.

All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.

All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a % solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and

disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the client.”

This laboratory report is confidential and is intended for the sole use of TestAmerica and its client.

RECEIPTThe samples were received on 05/06/2016; the samples arrived in good condition, properly preserved and on ice. The temperatures of

the 6 coolers at receipt time were 20.0º C, 20.0º C, 20.0º C, 20.0º C, 20.0º C and 22.0º C.

Receipt Exceptions: Samples ADS BRL-LT-LIQ and Leachate Effluent received with pH at 7. Added nitric. lot 832829 and pH remains at 7

for all sample bottles.

2XLP for MW-17R received with pH at 7. Added nitric, lot 832829 and pH is now below 2 for both bottles.

GROSS ALPHA AND GROSS BETA RADIOACTIVITY-Solids

Samples #7 FILTER CAKE (160-17284-12), ADS BRL-LT-SL (160-17284-16), POND 3 SEDIMENT (160-17284-20), POND 3 SEDIMENT

DUP (160-17284-22), DRY BRANCH CREEK UPSTREAM SED (160-17284-24), DRY BRANCH CREEK DOWNSTREAM SED (160-17284-26), DRY BRANCH CREEK DOWNSTREAM SED DUP (160-17284-27), POND 4 SEDIMENT (160-17284-30), POND 4 SED

SILT FENCE (160-17284-31), SED POND 1 SEDIMENT (160-17284-33) and POND 2 SEDIMENT (160-17284-38) were analyzed for Gross Alpha and Gross Beta Radioactivity in accordance with EPA 900.0. The samples were dried on 05/09/2016, prepared on 05/16/2016 and

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Job ID: 160-17284-1 (Continued)

Laboratory: TestAmerica St. Louis (Continued)

analyzed on 05/17/2016.

Gross Beta was detected in method blank MB 160-251280/1-A at a level exceeding the reporting limit. If the associated sample reported a

result above the MDL and/or RL, the result has been flagged. Refer to the QC report for details.

No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

GROSS ALPHA AND GROSS BETA RADIOACTIVITY-Waters

Samples MW-17R-AKGWA 8003-8393 (160-17284-1), MW-10-AKGWA 8001-0201 (160-17284-2), MW-13-AKGWA 8001-2025

(160-17284-3), MW-15R-AKGWA 8003-3579 (160-17284-4), MW-7-AKGWA 8001-0205 (160-17284-5), #1 UV EFFLUENT CHANNEL 37 DEGREES 42.086' (160-17284-6), #3 WWTP INFLUENT (160-17284-8), DRY BRANCH CREEK DOWNSTREAM DUP (160-17284-13),

POND 3 ABOVE OUTFALL (160-17284-14), ADS BRL-LT-LIQ (160-17284-15), ADS BRL UNDERDRAIN (160-17284-17), POND 3 (160-17284-18), POND 3 OUTFALL (160-17284-19), POND 3 DUP (160-17284-21), DRY BRANCH CREEK UPSTREAM (160-17284-23),

DRY BRANCH CREEK DOWNSTREAM (160-17284-25), OUTFALL 004 (160-17284-28), POND 4 (160-17284-29), SED POND 1

(160-17284-32), OUTFALL 001 (160-17284-34), LEACHATE EFFLEUNT (160-17284-35), POND 2 (160-17284-36) and POND 2 OUTFALL (160-17284-37) were analyzed for Gross Alpha and Gross Beta Radioactivity in accordance with USEPA Method 900.0. The samples were prepared on 06/03/2016 and analyzed on 06/09/2016.

Prep Batch 254725The gross alpha and gross beta detection goals were not met for the following samples due to a reduction of the sample size attributed to high residual mass: LEACHATE EFFLEUNT (160-17284-35) and POND 2 (160-17284-36). Analytical results are reported with the detection limit achieved.

The gross alpha detection goal was not met for the following samples due to a reduction of the sample size attributed to high residual mass: POND 2 OUTFALL (160-17284-37) and (160-17627-B-1-B DU). Analytical results are reported with the detection limit achieved.

Prep Batch 254724

The gross alpha and gross beta detection goals were not met for the following samples due to a reduction of the sample size attributed to high residual mass: MW-17R-AKGWA 8003-8393 (160-17284-1), MW-10-AKGWA 8001-0201 (160-17284-2), MW-13-AKGWA 8001-2025 (160-17284-3), MW-15R-AKGWA 8003-3579 (160-17284-4), MW-7-AKGWA 8001-0205 (160-17284-5), #3 WWTP INFLUENT (160-17284-8), POND 3 ABOVE OUTFALL (160-17284-14), ADS BRL-LT-LIQ (160-17284-15), ADS BRL UNDERDRAIN (160-17284-17), POND 3 (160-17284-18), POND 3 OUTFALL (160-17284-19) and POND 3 DUP (160-17284-21). Analytical results are reported with the

detection limit achieved.

The gross alpha detection goal was not met for the following samples due to a reduction of the sample size attributed to high residual mass: OUTFALL 004 (160-17284-28), POND 4 (160-17284-29), SED POND 1 (160-17284-32) and OUTFALL 001 (160-17284-34).

Analytical results are reported with the detection limit achieved.


RADIUM-226 BY GAMMA SPEC (21 DAY INGROWTH)

Samples #5 FILTER CAKE (160-17284-10), #6 FILTER CAKE (160-17284-11), ADS BRL-LT-SL (160-17284-16), POND 3 SEDIMENT (160-17284-20), POND 3 SEDIMENT DUP (160-17284-22), DRY BRANCH CREEK UPSTREAM SED (160-17284-24), DRY BRANCH

CREEK DOWNSTREAM SED (160-17284-26), DRY BRANCH CREEK DOWNSTREAM SED DUP (160-17284-27), POND 4 SEDIMENT

(160-17284-30), POND 4 SED SILT FENCE (160-17284-31), SED POND 1 SEDIMENT (160-17284-33) and POND 2 SEDIMENT (160-17284-38) were analyzed for Radium-226 by gamma spec (21 day ingrowth) in accordance with EPA 901.1. The samples were dried

on 05/09/2016, prepared on 05/12/2016 and analyzed on 06/02/2016.

Batch 250875

Insufficient samples were provided for the following samples to fill a tuna can geometry calibrated for Ra-226 analysis by gamma spectroscopy: #5 FILTER CAKE (160-17284-10) and #6 FILTER CAKE (160-17284-11). The use of a different geometry could potentially

bias the results low due to the loss of radon into the headspace of the container. Samples were placed in a 25mL geometry instead.



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Job ID: 160-17284-1 (Continued)

Laboratory: TestAmerica St. Louis (Continued)

RADIUM-226 (GFPC)

Samples MW-17R-AKGWA 8003-8393 (160-17284-1), MW-10-AKGWA 8001-0201 (160-17284-2), MW-13-AKGWA 8001-2025 (160-17284-3), MW-15R-AKGWA 8003-3579 (160-17284-4), MW-7-AKGWA 8001-0205 (160-17284-5), #2 UV EFFLUENT CHANNEL83

DEGREES 58.917 (160-17284-7), #4 WWTP INFLUENT (160-17284-9), DRY BRANCH CREEK DOWNSTREAM DUP (160-17284-13),

POND 3 ABOVE OUTFALL (160-17284-14), ADS BRL-LT-LIQ (160-17284-15), ADS BRL UNDERDRAIN (160-17284-17), POND 3 (160-17284-18), POND 3 OUTFALL (160-17284-19), POND 3 DUP (160-17284-21), DRY BRANCH CREEK UPSTREAM (160-17284-23),

DRY BRANCH CREEK DOWNSTREAM (160-17284-25), OUTFALL 004 (160-17284-28), POND 4 (160-17284-29), SED POND 1 (160-17284-32), OUTFALL 001 (160-17284-34), LEACHATE EFFLEUNT (160-17284-35), POND 2 (160-17284-36) and POND 2 OUTFALL

(160-17284-37) were analyzed for Radium-226 (GFPC) in accordance with EPA Method 903.0. The samples were prepared on 05/10/2016

and 05/17/2016 and analyzed on 06/01/2016, 06/02/2016 and 06/10/2016.

Prep Batch 250365The Laboratory Control Sample (LCS) spike recovery (140%) associated with the following samples is outside the upper QC limit of 137%

indicating a potential positive bias for that analyte : POND 2 (160-17284-36), POND 2 OUTFALL (160-17284-37), (LCS 160-250356/2-A),

(LCSD 160-250356/3-A). This analyte was not observed above the requested limit in the associated samples; therefore the sample data was not adversely affected by this excursion. The data have been qualified and reported.

Prep Batch 251589A deviation from the Standard Operating Procedure (SOP) occurred in preparation of the following samples: ADS BRL-LT-LIQ (160-17284-15) and LEACHATE EFFLEUNT (160-17284-35). The samples were deep brown to black in coloring with some sediment. Initial preparation of the samples left little to no barium sulfate following the analysis. Per instructions from the Technical Director, the samples were re-prepared at a reduced aliquot, cooked to dryness, muffled, and wet ashed to remove all organics interfering with normal

preparation. This was successful, and the samples behaved normally through the rest of the analysis. To avoid matrix interference with homogeneity, a laboratory control sample/ laboratory control sample duplicate (LCS/LCSD) were prepared instead of a sample duplicate (DUP).


RADIUM-228 (GFPC)Samples MW-17R-AKGWA 8003-8393 (160-17284-1), MW-10-AKGWA 8001-0201 (160-17284-2), MW-13-AKGWA 8001-2025 (160-17284-3), MW-15R-AKGWA 8003-3579 (160-17284-4), MW-7-AKGWA 8001-0205 (160-17284-5), #2 UV EFFLUENT CHANNEL83 DEGREES 58.917 (160-17284-7), #4 WWTP INFLUENT (160-17284-9), DRY BRANCH CREEK DOWNSTREAM DUP (160-17284-13),

POND 3 ABOVE OUTFALL (160-17284-14), ADS BRL-LT-LIQ (160-17284-15), ADS BRL UNDERDRAIN (160-17284-17), POND 3 (160-17284-18), POND 3 OUTFALL (160-17284-19), POND 3 DUP (160-17284-21), DRY BRANCH CREEK UPSTREAM (160-17284-23), DRY BRANCH CREEK DOWNSTREAM (160-17284-25), OUTFALL 004 (160-17284-28), POND 4 (160-17284-29), SED POND 1 (160-17284-32), OUTFALL 001 (160-17284-34), LEACHATE EFFLEUNT (160-17284-35), POND 2 (160-17284-36) and POND 2 OUTFALL

(160-17284-37) were analyzed for Radium-228 (GFPC) in accordance with EPA 904. The samples were prepared on 05/10/2016 and 05/19/2016 and analyzed on 05/17/2016 and 05/27/2016.

Prep Batch 250391The radium-228 MDC (2.19) did not meet the requested limit (1.00 pCi/L). However, the activity is well above the MDC achieved. In

addition, the barium recovery was low (40.7%) potentially increasing the MDC.#4 WWTP INFLUENT (160-17284-9)

Prep Batch 232055

A deviation from the Standard Operating Procedure (SOP) occurred in preparation of the following samples: ADS BRL-LT-LIQ (160-17284-15) and LEACHATE EFFLEUNT (160-17284-35). The samples were deep brown to black in coloring with some sediment.

Initial preparation of the samples left little to no barium sulfate following the analysis. Per instructions from the Technical Director, the samples were re-prepared at a reduced aliquot, cooked to dryness, muffled, and wet ashed to remove all organics interfering with normal

preparation. This was successful, and the samples behaved normally through the rest of the analysis. To avoid matrix interference with

homogeneity, a laboratory control sample/ laboratory control sample duplicate (LCS/LCSD) were prepared instead of a sample duplicate (DUP).



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Login Sample Receipt Checklist

Client: Commonwealth of Kentucky Job Number: 160-17284-1

Login Number: 17284

Question Answer Comment

Creator: Daniels, Brian J

List Source: TestAmerica St. Louis

List Number: 1

TrueRadioactivity wasn't checked or is </= background as measured by a survey meter.

TrueThe cooler's custody seal, if present, is intact.

N/ASample custody seals, if present, are intact.

TrueThe cooler or samples do not appear to have been compromised or tampered with.

N/ASamples were received on ice.

TrueCooler Temperature is acceptable.

TrueCooler Temperature is recorded.

TrueCOC is present.

TrueCOC is filled out in ink and legible.

TrueCOC is filled out with all pertinent information.

N/AIs the Field Sampler's name present on COC?

TrueThere are no discrepancies between the containers received and the COC.

TrueSamples are received within Holding Time (excluding tests with immediate HTs)

TrueSample containers have legible labels.

TrueContainers are not broken or leaking.

TrueSample collection date/times are provided.

TrueAppropriate sample containers are used.

TrueSample bottles are completely filled.

TrueSample Preservation Verified. Samples -1, -15, and -35 were received unpreserved. Nitric acid was added to

TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs

adjust pH. Sample -1 is now < 2 SU but samples -15 and-35 were unsuccessfully

N/AContainers requiring zero headspace have no headspace or bubble is <6mm (1/4").

adjusted and remain at 7.

TrueMultiphasic samples are not present.

TrueSamples do not require splitting or compositing.

N/AResidual Chlorine Checked.


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Definitions/GlossaryTestAmerica Job ID: 160-17284-1Client: Commonwealth of Kentucky

Project/Site: Blue Ridge Landfill

Qualifiers

Rad

Qualifier Description

G The Sample MDC is greater than the requested RL.

Qualifier

U Result is less than the sample detection limit.

* LCS or LCSD is outside acceptance limits.

Glossary

These commonly used abbreviations may or may not be present in this report.

¤ Listed under the "D" column to designate that the result is reported on a dry weight basis

Abbreviation

%R Percent Recovery

CFL Contains Free Liquid

CNF Contains no Free Liquid

DER Duplicate error ratio (normalized absolute difference)

Dil Fac Dilution Factor

DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample

DLC Decision level concentration

MDA Minimum detectable activity

EDL Estimated Detection Limit

MDC Minimum detectable concentration

MDL Method Detection Limit

ML Minimum Level (Dioxin)

NC Not Calculated

ND Not detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit

QC Quality Control

RER Relative error ratio

RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points

TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)

TestAmerica St. Louis

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Method SummaryTestAmerica Job ID: 160-17284-1Client: Commonwealth of Kentucky


Method Method Description LaboratoryProtocol

EPA900.0 Gross Alpha and Gross Beta Radioactivity TAL SL

EPA901.1 Radium-226 & Other Gamma Emitters (GS) TAL SL

EPA903.0 Radium-226 (GFPC) TAL SL

EPA904.0 Radium-228 (GFPC) TAL SL

Protocol References:

EPA = US Environmental Protection Agency

Laboratory References:

TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566


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Sample SummaryTestAmerica Job ID: 160-17284-1Client: Commonwealth of Kentucky


Lab Sample ID Client Sample ID ReceivedCollectedMatrix

160-17284-1 MW-17R-AKGWA 8003-8393 Water 05/03/16 10:45 05/06/16 09:10

160-17284-2 MW-10-AKGWA 8001-0201 Water 05/03/16 11:33 05/06/16 09:10

160-17284-3 MW-13-AKGWA 8001-2025 Water 05/03/16 14:46 05/06/16 09:10

160-17284-4 MW-15R-AKGWA 8003-3579 Water 05/03/16 15:45 05/06/16 09:10

160-17284-5 MW-7-AKGWA 8001-0205 Water 05/03/16 16:55 05/06/16 09:10

160-17284-6 #1 UV EFFLUENT CHANNEL 37 DEGREES 42.086' Water 05/03/16 11:05 05/06/16 09:10

160-17284-7 #2 UV EFFLUENT CHANNEL83 DEGREES 58.917 Water 05/03/16 11:05 05/06/16 09:10

160-17284-8 #3 WWTP INFLUENT Water 05/03/16 11:45 05/06/16 09:10

160-17284-9 #4 WWTP INFLUENT Water 05/03/16 11:45 05/06/16 09:10

160-17284-10 #5 FILTER CAKE Solid 05/03/16 12:10 05/06/16 09:10



160-17284-13 DRY BRANCH CREEK DOWNSTREAM DUP Water 05/03/16 18:35 05/06/16 09:10

160-17284-14 POND 3 ABOVE OUTFALL Water 05/03/16 17:25 05/06/16 09:10

160-17284-15 ADS BRL-LT-LIQ Water 05/03/16 11:10 05/06/16 09:10

160-17284-16 ADS BRL-LT-SL Solid 05/03/16 11:20 05/06/16 09:10

160-17284-17 ADS BRL UNDERDRAIN Water 05/03/16 16:20 05/06/16 09:10

160-17284-18 POND 3 Water 05/03/16 16:20 05/06/16 09:10

160-17284-19 POND 3 OUTFALL Water 05/03/16 16:50 05/06/16 09:10

160-17284-20 POND 3 SEDIMENT Solid 05/03/16 16:00 05/06/16 09:10

160-17284-21 POND 3 DUP Water 05/03/16 16:20 05/06/16 09:10

160-17284-22 POND 3 SEDIMENT DUP Solid 05/03/16 16:00 05/06/16 09:10

160-17284-23 DRY BRANCH CREEK UPSTREAM Water 05/03/16 17:53 05/06/16 09:10

160-17284-24 DRY BRANCH CREEK UPSTREAM SED Solid 05/03/16 17:58 05/06/16 09:10

160-17284-25 DRY BRANCH CREEK DOWNSTREAM Water 05/03/16 18:35 05/06/16 09:10

160-17284-26 DRY BRANCH CREEK DOWNSTREAM SED Solid 05/03/16 18:55 05/06/16 09:10

160-17284-27 DRY BRANCH CREEK DOWNSTREAM SED DUP Solid 05/03/16 18:55 05/06/16 09:10

160-17284-28 OUTFALL 004 Water 05/03/16 11:15 05/06/16 09:10

160-17284-29 POND 4 Water 05/03/16 11:30 05/06/16 09:10


160-17284-31 POND 4 SED SILT FENCE Solid 05/03/16 11:45 05/06/16 09:10

160-17284-32 SED POND 1 Water 05/03/16 14:10 05/06/16 09:10

160-17284-33 SED POND 1 SEDIMENT Solid 05/03/16 14:30 05/06/16 09:10

160-17284-34 OUTFALL 001 Water 05/03/16 14:45 05/06/16 09:10

160-17284-35 LEACHATE EFFLEUNT Water 05/03/16 15:00 05/06/16 09:10

160-17284-36 POND 2 Water 05/03/16 15:40 05/06/16 09:10

160-17284-37 POND 2 OUTFALL Water 05/03/16 16:00 05/06/16 09:10



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Client Sample ResultsTestAmerica Job ID: 160-17284-1Client: Commonwealth of Kentucky


Lab Sample ID: 160-17284-1Client Sample ID: MW-17R-AKGWA 8003-8393Matrix: WaterDate Collected: 05/03/16 10:45

Date Received: 05/06/16 09:10

Method: 900.0 - Gross Alpha and Gross Beta Radioactivity

Analyte

Gross Alpha 5.09 U G

(2σ+/-)

8.36

(2σ+/-)

106/09/16 07:5806/03/16 09:53pCi/L14.43.00

RL MDC

8.34

Dil FacAnalyzedPreparedUnitResult Qualifier

Count Total

Uncert. Uncert.

pCi/L 06/03/16 09:53 06/09/16 07:58 17.284.004.964.87G9.31Gross Beta

Method: 903.0 - Radium-226 (GFPC)

Analyte

Radium-226 3.87

(2σ+/-)

0.427

(2σ+/-)

106/01/16 07:3305/10/16 15:18pCi/L0.06201.00

RL MDC

0.247


Count Total

Uncert. Uncert.

Ba Carrier 40 - 110

Carrier

05/10/16 15:18 06/01/16 07:33 1

Dil FacAnalyzedPreparedQualifier Limits%Yield

85.5


Analyte

Radium-228 0.513

(2σ+/-)

0.313

(2σ+/-)

105/17/16 17:5605/10/16 17:22pCi/L0.4761.00

RL MDC

0.310


Count Total

Uncert. Uncert.

Ba Carrier 40 - 110

Carrier

05/10/16 17:22 05/17/16 17:56 1


85.5

Y Carrier 40 - 110 05/10/16 17:22 05/17/16 17:56 188.6


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Lab Sample ID: 160-17284-2Client Sample ID: MW-10-AKGWA 8001-0201Matrix: WaterDate Collected: 05/03/16 11:33



Analyte


(2σ+/-)

6.49

(2σ+/-)

106/09/16 07:5806/03/16 09:53pCi/L9.373.00

RL MDC

6.42


Count Total

Uncert. Uncert.

pCi/L 06/03/16 09:53 06/09/16 07:58 15.774.003.913.86G5.97Gross Beta


Analyte

Radium-226 3.58

(2σ+/-)

0.408

(2σ+/-)

106/01/16 07:3405/10/16 15:18pCi/L0.06791.00

RL MDC

0.250


Count Total

Uncert. Uncert.

Ba Carrier 40 - 110

Carrier

05/10/16 15:18 06/01/16 07:34 1


74.9


Analyte

Radium-228 0.446

(2σ+/-)

0.291

(2σ+/-)

105/17/16 17:5605/10/16 17:22pCi/L0.4401.00

RL MDC

0.288


Count Total

Uncert. Uncert.

Ba Carrier 40 - 110

Carrier

05/10/16 17:22 05/17/16 17:56 1


74.9

Y Carrier 40 - 110 05/10/16 17:22 05/17/16 17:56 187.1


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2

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4

5

6

7

8

9

10

11

12






Analyte

Gross Alpha 88.6 G

(2σ+/-)

47.6

(2σ+/-)

106/09/16 07:5806/03/16 09:53pCi/L57.03.00

RL MDC

46.5


Count Total

Uncert. Uncert.

pCi/L 06/03/16 09:53 06/09/16 07:58 130.54.0021.621.3G36.0Gross Beta


Analyte

Radium-226 1.29

(2σ+/-)

0.181

(2σ+/-)

106/01/16 07:3405/10/16 15:18pCi/L0.06521.00

RL MDC

0.140


Count Total

Uncert. Uncert.

Ba Carrier 40 - 110

Carrier

05/10/16 15:18 06/01/16 07:34 1


100


Analyte

Radium-228 0.114 U

(2σ+/-)

0.207

(2σ+/-)

105/17/16 17:5705/10/16 17:22pCi/L0.3521.00

RL MDC

0.207


Count Total

Uncert. Uncert.

Ba Carrier 40 - 110

Carrier

05/10/16 17:22 05/17/16 17:57 1


100

Y Carrier 40 - 110 05/10/16 17:22 05/17/16 17:57 186.4


Page 18 of 66 6/13/2016

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5

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7

8

9

10

11

12



Lab Sample ID: 160-17284-4Client Sample ID: MW-15R-AKGWA 8003-3579Matrix: WaterDate Collected: 05/03/16 15:45



Analyte

Gross Alpha 21.7 G

(2σ+/-)

9.97

(2σ+/-)

106/09/16 07:5906/03/16 09:53pCi/L10.83.00

RL MDC

9.66


Count Total

Uncert. Uncert.

pCi/L 06/03/16 09:53 06/09/16 07:59 16.194.004.794.64G11.6Gross Beta


Analyte

Radium-226 0.580

(2σ+/-)

0.112

(2σ+/-)

106/01/16 07:3405/10/16 15:18pCi/L0.05551.00

RL MDC

0.0994


Count Total

Uncert. Uncert.

Ba Carrier 40 - 110

Carrier

05/10/16 15:18 06/01/16 07:34 1


79.5


Analyte

Radium-228 0.289 U

(2σ+/-)

0.269

(2σ+/-)

105/17/16 17:5705/10/16 17:22pCi/L0.4301.00

RL MDC

0.267


Count Total

Uncert. Uncert.

Ba Carrier 40 - 110

Carrier

05/10/16 17:22 05/17/16 17:57 1


79.5

Y Carrier 40 - 110 05/10/16 17:22 05/17/16 17:57 187.1


Page 19 of 66 6/13/2016

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2

3

4

5

6

7

8

9

10

11

12






Analyte


(2σ+/-)

11.0

(2σ+/-)

106/09/16 07:5906/03/16 09:53pCi/L18.53.00

RL MDC

10.9


Count Total

Uncert. Uncert.

pCi/L 06/03/16 09:53 06/09/16 07:59 17.284.004.874.81G7.43Gross Beta


Analyte

Radium-226 2.96

(2σ+/-)

0.342

(2σ+/-)

106/01/16 07:3405/10/16 15:18pCi/L0.05951.00

RL MDC

0.215


Count Total

Uncert. Uncert.

Ba Carrier 40 - 110

Carrier

05/10/16 15:18 06/01/16 07:34 1


84.9


Analyte

Radium-228 0.189 U

(2σ+/-)

0.264

(2σ+/-)

105/17/16 17:5705/10/16 17:22pCi/L0.4401.00

RL MDC

0.263


Count Total

Uncert. Uncert.

Ba Carrier 40 - 110

Carrier

05/10/16 17:22 05/17/16 17:57 1


84.9

Y Carrier 40 - 110 05/10/16 17:22 05/17/16 17:57 184.5


Page 20 of 66 6/13/2016

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2

3

4

5

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7

8

9

10

11

12



Lab Sample ID: 160-17284-6Client Sample ID: #1 UV EFFLUENT CHANNEL 37 DEGREES

42.086'Matrix: WaterDate Collected: 05/03/16 11:05



Analyte

Gross Alpha 1.41 U

(2σ+/-)

1.64

(2σ+/-)

106/09/16 07:5906/03/16 09:53pCi/L2.653.00

RL MDC

1.63


Count Total

Uncert. Uncert.

pCi/L 06/03/16 09:53 06/09/16 07:59 11.484.001.581.407.23Gross Beta


Page 21 of 66 6/13/2016

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2

3

4

5

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7

8

9

10

11

12



Lab Sample ID: 160-17284-7Client Sample ID: #2 UV EFFLUENT CHANNEL83 DEGREES

58.917Matrix: WaterDate Collected: 05/03/16 11:05



Analyte

Radium-226 0.127

(2σ+/-)

0.0845

(2σ+/-)

106/01/16 07:3405/10/16 15:18pCi/L0.1141.00

RL MDC

0.0837


Count Total

Uncert. Uncert.

Ba Carrier 40 - 110

Carrier

05/10/16 15:18 06/01/16 07:34 1


82.1


Analyte

Radium-228 -0.406 U

(2σ+/-)

0.418

(2σ+/-)

105/17/16 17:5705/10/16 17:22pCi/L0.8301.00

RL MDC

0.416


Count Total

Uncert. Uncert.

Ba Carrier 40 - 110

Carrier

05/10/16 17:22 05/17/16 17:57 1


82.1

Y Carrier 40 - 110 05/10/16 17:22 05/17/16 17:57 189.3


Page 22 of 66 6/13/2016

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2

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4

5

6

7

8

9

10

11

12



Lab Sample ID: 160-17284-8Client Sample ID: #3 WWTP INFLUENTMatrix: WaterDate Collected: 05/03/16 11:45



Analyte

Gross Alpha 42.7 G

(2σ+/-)

15.3

(2σ+/-)

106/09/16 08:0006/03/16 09:53pCi/L14.53.00

RL MDC

14.5


Count Total

Uncert. Uncert.

pCi/L 06/03/16 09:53 06/09/16 08:00 18.944.009.878.72G46.3Gross Beta


Page 23 of 66 6/13/2016

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2

3

4

5

6

7

8

9

10

11

12



Lab Sample ID: 160-17284-9Client Sample ID: #4 WWTP INFLUENTMatrix: WaterDate Collected: 05/03/16 11:45



Analyte

Radium-226 2.56

(2σ+/-)

0.469

(2σ+/-)

106/01/16 07:3405/10/16 15:18pCi/L0.2971.00

RL MDC

0.409


Count Total

Uncert. Uncert.

Ba Carrier 40 - 110

Carrier

05/10/16 15:18 06/01/16 07:34 1


40.7


Analyte

Radium-228 3.22 G

(2σ+/-)

1.52

(2σ+/-)

105/17/16 17:5705/10/16 17:22pCi/L2.191.00

RL MDC

1.49


Count Total

Uncert. Uncert.

Ba Carrier 40 - 110

Carrier

05/10/16 17:22 05/17/16 17:57 1


40.7

Y Carrier 40 - 110 05/10/16 17:22 05/17/16 17:57 180.7


Page 24 of 66 6/13/2016

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2

3

4

5

6

7

8

9

10

11

12



Lab Sample ID: 160-17284-10Client Sample ID: #5 FILTER CAKEMatrix: SolidDate Collected: 05/03/16 12:10


Method: 901.1 - Radium-226 & Other Gamma Emitters (GS)

Analyte

Radium-226 0.885

(2σ+/-)

0.237

(2σ+/-)

106/02/16 09:2205/12/16 12:24pCi/g0.1901.00

RL MDC

0.221


Count Total

Uncert. Uncert.

pCi/g 05/12/16 12:24 06/02/16 09:22 10.4260.3630.3510.936Radium-228


Page 25 of 66 6/13/2016

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2

3

4

5

6

7

8

9

10

11

12






Analyte

Radium-226 0.000 U

(2σ+/-)

0.262

(2σ+/-)

106/02/16 11:4605/12/16 12:24pCi/g0.8081.00

RL MDC

0.262


Count Total

Uncert. Uncert.

pCi/g 05/12/16 12:24 06/02/16 11:46 10.6630.4990.495U0.585Radium-228


Page 26 of 66 6/13/2016

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2

3

4

5

6

7

8

9

10

11

12






Analyte

Gross Alpha 14.9

(2σ+/-)

6.20

(2σ+/-)

105/17/16 17:4605/16/16 15:33pCi/g7.3810.0

RL MDC

5.96


Count Total

Uncert. Uncert.

pCi/g 05/16/16 15:33 05/17/16 17:46 14.8310.04.524.1019.0Gross Beta


Page 27 of 66 6/13/2016

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2

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4

5

6

7

8

9

10

11

12



Lab Sample ID: 160-17284-13Client Sample ID: DRY BRANCH CREEK DOWNSTREAM DUPMatrix: WaterDate Collected: 05/03/16 18:35



Analyte

Gross Alpha 2.89

(2σ+/-)

1.63

(2σ+/-)

106/09/16 08:0006/03/16 09:53pCi/L2.033.00

RL MDC

1.59


Count Total

Uncert. Uncert.

pCi/L 06/03/16 09:53 06/09/16 08:00 11.034.000.7590.7421.61Gross Beta


Analyte

Radium-226 0.0844

(2σ+/-)

0.0488

(2σ+/-)

106/01/16 07:3405/10/16 15:18pCi/L0.06331.00

RL MDC

0.0482


Count Total

Uncert. Uncert.

Ba Carrier 40 - 110

Carrier

05/10/16 15:18 06/01/16 07:34 1


80.6


Analyte

Radium-228 0.226 U

(2σ+/-)

0.279

(2σ+/-)

105/17/16 17:5805/10/16 17:22pCi/L0.4611.00

RL MDC

0.278


Count Total

Uncert. Uncert.

Ba Carrier 40 - 110

Carrier

05/10/16 17:22 05/17/16 17:58 1


80.6

Y Carrier 40 - 110 05/10/16 17:22 05/17/16 17:58 189.3


Page 28 of 66 6/13/2016

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5

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7

8

9

10

11

12



Lab Sample ID: 160-17284-14Client Sample ID: POND 3 ABOVE OUTFALLMatrix: WaterDate Collected: 05/03/16 17:25



Analyte

Gross Alpha 26.8 G

(2σ+/-)

11.2

(2σ+/-)

106/09/16 08:0106/03/16 09:53pCi/L13.53.00

RL MDC

10.7


Count Total

Uncert. Uncert.

pCi/L 06/03/16 09:53 06/09/16 08:01 16.024.005.735.26G22.9Gross Beta


Analyte

Radium-226 1.65

(2σ+/-)

0.222

(2σ+/-)

106/01/16 07:3405/10/16 15:18pCi/L0.06231.00

RL MDC

0.166


Count Total

Uncert. Uncert.

Ba Carrier 40 - 110

Carrier

05/10/16 15:18 06/01/16 07:34 1


82.9


Analyte

Radium-228 0.384 U

(2σ+/-)

0.274

(2σ+/-)

105/17/16 17:5805/10/16 17:22pCi/L0.4241.00

RL MDC

0.272


Count Total

Uncert. Uncert.

Ba Carrier 40 - 110

Carrier

05/10/16 17:22 05/17/16 17:58 1


82.9

Y Carrier 40 - 110 05/10/16 17:22 05/17/16 17:58 190.1


Page 29 of 66 6/13/2016

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2

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5

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Lab Sample ID: 160-17284-15Client Sample ID: ADS BRL-LT-LIQMatrix: WaterDate Collected: 05/03/16 11:10



Analyte


(2σ+/-)

39.3

(2σ+/-)

106/09/16 08:0106/03/16 09:53pCi/L54.43.00

RL MDC

38.8


Count Total

Uncert. Uncert.

pCi/L 06/03/16 09:53 06/09/16 08:01 130.94.0066.145.4G480Gross Beta


Analyte

Radium-226 3.33

(2σ+/-)

0.443

(2σ+/-)

106/10/16 06:5505/17/16 15:37pCi/L0.1231.00

RL MDC

0.326


Count Total

Uncert. Uncert.

Ba Carrier 40 - 110

Carrier

05/17/16 15:37 06/10/16 06:55 1


87.7


Analyte

Radium-228 1.74

(2σ+/-)

0.611

(2σ+/-)

105/27/16 12:0605/19/16 14:12pCi/L0.7841.00

RL MDC

0.590


Count Total

Uncert. Uncert.

Ba Carrier 40 - 110

Carrier

05/19/16 14:12 05/27/16 12:06 1


87.7

Y Carrier 40 - 110 05/19/16 14:12 05/27/16 12:06 183.4


Page 30 of 66 6/13/2016

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5

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7

8

9

10

11

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Lab Sample ID: 160-17284-16Client Sample ID: ADS BRL-LT-SLMatrix: SolidDate Collected: 05/03/16 11:20



Analyte

Gross Alpha 28.9

(2σ+/-)

7.12

(2σ+/-)

105/17/16 17:4605/16/16 15:33pCi/g4.9510.0

RL MDC

6.31


Count Total

Uncert. Uncert.

pCi/g 05/16/16 15:33 05/17/16 17:46 13.1910.04.443.5027.4Gross Beta


Analyte

Radium-226 4.47

(2σ+/-)

0.767

(2σ+/-)

106/02/16 08:2905/12/16 12:24pCi/g0.2891.00

RL MDC

0.610


Count Total

Uncert. Uncert.

pCi/g 05/12/16 12:24 06/02/16 08:29 10.3100.6140.5682.28Radium-228


Page 31 of 66 6/13/2016

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2

3

4

5

6

7

8

9

10

11

12



Lab Sample ID: 160-17284-17Client Sample ID: ADS BRL UNDERDRAINMatrix: WaterDate Collected: 05/03/16 16:20



Analyte

Gross Alpha -2.75 U G

(2σ+/-)

24.4

(2σ+/-)

106/09/16 08:0206/03/16 09:53pCi/L46.73.00

RL MDC

24.4


Count Total

Uncert. Uncert.

pCi/L 06/03/16 09:53 06/09/16 08:02 116.84.0012.011.7G27.0Gross Beta


Analyte

Radium-226 0.751

(2σ+/-)

0.129

(2σ+/-)

106/01/16 18:1205/10/16 15:18pCi/L0.05891.00

RL MDC

0.110


Count Total

Uncert. Uncert.

Ba Carrier 40 - 110

Carrier

05/10/16 15:18 06/01/16 18:12 1


93.7


Analyte

Radium-228 0.506

(2σ+/-)

0.269

(2σ+/-)

105/17/16 17:5805/10/16 17:22pCi/L0.3921.00

RL MDC

0.265


Count Total

Uncert. Uncert.

Ba Carrier 40 - 110

Carrier

05/10/16 17:22 05/17/16 17:58 1


93.7

Y Carrier 40 - 110 05/10/16 17:22 05/17/16 17:58 185.6


Page 32 of 66 6/13/2016

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2

3

4

5

6

7

8

9

10

11

12



Lab Sample ID: 160-17284-18Client Sample ID: POND 3Matrix: WaterDate Collected: 05/03/16 16:20



Analyte


(2σ+/-)

8.03

(2σ+/-)

106/09/16 08:0206/03/16 09:53pCi/L11.93.00

RL MDC

7.94


Count Total

Uncert. Uncert.

pCi/L 06/03/16 09:53 06/09/16 08:02 15.404.005.675.02G26.5Gross Beta


Analyte

Radium-226 0.754

(2σ+/-)

0.144

(2σ+/-)

106/01/16 18:1205/10/16 15:18pCi/L0.09911.00

RL MDC

0.127


Count Total

Uncert. Uncert.

Ba Carrier 40 - 110

Carrier

05/10/16 15:18 06/01/16 18:12 1


76.9


Analyte

Radium-228 0.353 U

(2σ+/-)

0.290

(2σ+/-)

105/17/16 17:5905/10/16 17:22pCi/L0.4561.00

RL MDC

0.288


Count Total

Uncert. Uncert.

Ba Carrier 40 - 110

Carrier

05/10/16 17:22 05/17/16 17:59 1


76.9

Y Carrier 40 - 110 05/10/16 17:22 05/17/16 17:59 189.7


Page 33 of 66 6/13/2016

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2

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4

5

6

7

8

9

10

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Lab Sample ID: 160-17284-19Client Sample ID: POND 3 OUTFALLMatrix: WaterDate Collected: 05/03/16 16:50



Analyte


(2σ+/-)

7.21

(2σ+/-)

106/09/16 08:0206/03/16 09:53pCi/L10.93.00

RL MDC

7.14


Count Total

Uncert. Uncert.

pCi/L 06/03/16 09:53 06/09/16 08:02 15.324.005.955.15G29.7Gross Beta


Analyte

Radium-226 0.634

(2σ+/-)

0.127

(2σ+/-)

106/01/16 18:1205/10/16 15:18pCi/L0.09251.00

RL MDC

0.114


Count Total

Uncert. Uncert.

Ba Carrier 40 - 110

Carrier

05/10/16 15:18 06/01/16 18:12 1


80.6


Analyte

Radium-228 0.485

(2σ+/-)

0.308

(2σ+/-)

105/17/16 17:5905/10/16 17:22pCi/L0.4691.00

RL MDC

0.305


Count Total

Uncert. Uncert.

Ba Carrier 40 - 110

Carrier

05/10/16 17:22 05/17/16 17:59 1


80.6

Y Carrier 40 - 110 05/10/16 17:22 05/17/16 17:59 189.7


Page 34 of 66 6/13/2016

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2

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5

6

7

8

9

10

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Lab Sample ID: 160-17284-20Client Sample ID: POND 3 SEDIMENTMatrix: SolidDate Collected: 05/03/16 16:00



Analyte

Gross Alpha 30.9

(2σ+/-)

7.23

(2σ+/-)

105/17/16 17:4705/16/16 15:33pCi/g4.4910.0

RL MDC

6.31


Count Total

Uncert. Uncert.

pCi/g 05/16/16 15:33 05/17/16 17:47 12.7710.05.243.6337.8Gross Beta


Analyte

Radium-226 3.38

(2σ+/-)

0.611

(2σ+/-)

106/02/16 08:2805/12/16 12:24pCi/g0.2951.00

RL MDC

0.500


Count Total

Uncert. Uncert.

pCi/g 05/12/16 12:24 06/02/16 08:28 10.2620.4950.4292.41Radium-228


Page 35 of 66 6/13/2016

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4

5

6

7

8

9

10

11

12



Lab Sample ID: 160-17284-21Client Sample ID: POND 3 DUPMatrix: WaterDate Collected: 05/03/16 16:20



Analyte


(2σ+/-)

8.54

(2σ+/-)

106/09/16 08:0206/03/16 09:53pCi/L12.93.00

RL MDC

8.45


Count Total

Uncert. Uncert.

pCi/L 06/03/16 09:53 06/09/16 08:02 15.664.005.534.99G23.8Gross Beta


Analyte

Radium-226 0.735

(2σ+/-)

0.130

(2σ+/-)

106/01/16 12:2205/10/16 15:18pCi/L0.07881.00

RL MDC

0.112


Count Total

Uncert. Uncert.

Ba Carrier 40 - 110

Carrier

05/10/16 15:18 06/01/16 12:22 1


86.0


Analyte

Radium-228 0.383 U

(2σ+/-)

0.289

(2σ+/-)

105/17/16 18:0005/10/16 17:22pCi/L0.4521.00

RL MDC

0.286


Count Total

Uncert. Uncert.

Ba Carrier 40 - 110

Carrier

05/10/16 17:22 05/17/16 18:00 1


86.0

Y Carrier 40 - 110 05/10/16 17:22 05/17/16 18:00 190.1


Page 36 of 66 6/13/2016

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4

5

6

7

8

9

10

11

12



Lab Sample ID: 160-17284-22Client Sample ID: POND 3 SEDIMENT DUPMatrix: SolidDate Collected: 05/03/16 16:00



Analyte

Gross Alpha 40.5

(2σ+/-)

8.76

(2σ+/-)

105/17/16 17:4705/16/16 15:33pCi/g4.8710.0

RL MDC

7.44


Count Total

Uncert. Uncert.

pCi/g 05/16/16 15:33 05/17/16 17:47 13.8210.05.964.3640.6Gross Beta


Analyte

Radium-226 3.45

(2σ+/-)

0.585

(2σ+/-)

106/02/16 08:2905/12/16 12:24pCi/g0.3281.00

RL MDC

0.462


Count Total

Uncert. Uncert.

pCi/g 05/12/16 12:24 06/02/16 08:29 10.4020.5030.4691.79Radium-228


Page 37 of 66 6/13/2016

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5

6

7

8

9

10

11

12



Lab Sample ID: 160-17284-23Client Sample ID: DRY BRANCH CREEK UPSTREAMMatrix: WaterDate Collected: 05/03/16 17:53



Analyte

Gross Alpha 1.21 U

(2σ+/-)

1.48

(2σ+/-)

106/09/16 08:0206/03/16 09:53pCi/L2.423.00

RL MDC

1.47


Count Total

Uncert. Uncert.

pCi/L 06/03/16 09:53 06/09/16 08:02 11.144.000.8950.8642.35Gross Beta


Analyte

Radium-226 0.0618 U

(2σ+/-)

0.0507

(2σ+/-)

106/01/16 12:2305/10/16 15:18pCi/L0.07731.00

RL MDC

0.0504


Count Total

Uncert. Uncert.

Ba Carrier 40 - 110

Carrier

05/10/16 15:18 06/01/16 12:23 1


83.5


Analyte

Radium-228 0.268 U

(2σ+/-)

0.268

(2σ+/-)

105/17/16 18:0005/10/16 17:22pCi/L0.4331.00

RL MDC

0.267


Count Total

Uncert. Uncert.

Ba Carrier 40 - 110

Carrier

05/10/16 17:22 05/17/16 18:00 1


83.5

Y Carrier 40 - 110 05/10/16 17:22 05/17/16 18:00 188.6


Page 38 of 66 6/13/2016

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5

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Lab Sample ID: 160-17284-24Client Sample ID: DRY BRANCH CREEK UPSTREAM SEDMatrix: SolidDate Collected: 05/03/16 17:58



Analyte

Gross Alpha 29.8

(2σ+/-)

8.45

(2σ+/-)

105/17/16 17:4705/16/16 15:33pCi/g7.1710.0

RL MDC

7.74


Count Total

Uncert. Uncert.

pCi/g 05/16/16 15:33 05/17/16 17:47 15.4010.06.125.2431.7Gross Beta


Analyte

Radium-226 2.00

(2σ+/-)

0.325

(2σ+/-)

106/02/16 08:5905/12/16 12:24pCi/g0.1731.00

RL MDC

0.250


Count Total

Uncert. Uncert.

pCi/g 05/12/16 12:24 06/02/16 08:59 10.2060.2580.2191.35Radium-228


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Lab Sample ID: 160-17284-25Client Sample ID: DRY BRANCH CREEK DOWNSTREAMMatrix: WaterDate Collected: 05/03/16 18:35



Analyte

Gross Alpha 1.93 U

(2σ+/-)

1.83

(2σ+/-)

106/09/16 08:0206/03/16 09:53pCi/L2.813.00

RL MDC

1.81


Count Total

Uncert. Uncert.

pCi/L 06/03/16 09:53 06/09/16 08:02 10.9604.000.7260.7041.74Gross Beta


Analyte

Radium-226 0.106

(2σ+/-)

0.0564

(2σ+/-)

106/01/16 12:2405/10/16 15:18pCi/L0.07411.00

RL MDC

0.0556


Count Total

Uncert. Uncert.

Ba Carrier 40 - 110

Carrier

05/10/16 15:18 06/01/16 12:24 1


80.9


Analyte

Radium-228 0.0635 U

(2σ+/-)

0.231

(2σ+/-)

105/17/16 18:0105/10/16 17:22pCi/L0.4041.00

RL MDC

0.231


Count Total

Uncert. Uncert.

Ba Carrier 40 - 110

Carrier

05/10/16 17:22 05/17/16 18:01 1


80.9

Y Carrier 40 - 110 05/10/16 17:22 05/17/16 18:01 195.0


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Lab Sample ID: 160-17284-26Client Sample ID: DRY BRANCH CREEK DOWNSTREAM SEDMatrix: SolidDate Collected: 05/03/16 18:55



Analyte

Gross Alpha 30.0

(2σ+/-)

7.05

(2σ+/-)

105/17/16 17:4705/16/16 15:33pCi/g4.0310.0

RL MDC

6.17


Count Total

Uncert. Uncert.

pCi/g 05/16/16 15:33 05/17/16 17:47 13.2010.05.093.8533.3Gross Beta


Analyte

Radium-226 2.80

(2σ+/-)

0.382

(2σ+/-)

106/02/16 09:0205/12/16 12:24pCi/g0.1281.00

RL MDC

0.247


Count Total

Uncert. Uncert.

pCi/g 05/12/16 12:24 06/02/16 09:02 10.1850.2620.2261.30Radium-228


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Lab Sample ID: 160-17284-27Client Sample ID: DRY BRANCH CREEK DOWNSTREAM SED

DUPMatrix: SolidDate Collected: 05/03/16 18:55



Analyte

Gross Alpha 41.5

(2σ+/-)

8.89

(2σ+/-)

105/17/16 17:4705/16/16 15:33pCi/g4.8010.0

RL MDC

7.53


Count Total

Uncert. Uncert.

pCi/g 05/16/16 15:33 05/17/16 17:47 13.6710.04.913.9828.7Gross Beta


Analyte

Radium-226 3.32

(2σ+/-)

0.497

(2σ+/-)

106/02/16 09:2405/12/16 12:24pCi/g0.1781.00

RL MDC

0.357


Count Total

Uncert. Uncert.

pCi/g 05/12/16 12:24 06/02/16 09:24 10.2760.3100.2791.32Radium-228


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Lab Sample ID: 160-17284-28Client Sample ID: OUTFALL 004Matrix: WaterDate Collected: 05/03/16 11:15



Analyte

Gross Alpha 6.58 G

(2σ+/-)

3.59

(2σ+/-)

106/09/16 08:0206/03/16 09:53pCi/L4.123.00

RL MDC

3.51


Count Total

Uncert. Uncert.

pCi/L 06/03/16 09:53 06/09/16 08:02 12.724.002.021.974.50Gross Beta


Analyte

Radium-226 0.251

(2σ+/-)

0.0784

(2σ+/-)

106/01/16 12:2405/10/16 15:18pCi/L0.08111.00

RL MDC

0.0751


Count Total

Uncert. Uncert.

Ba Carrier 40 - 110

Carrier

05/10/16 15:18 06/01/16 12:24 1


84.3


Analyte

Radium-228 0.0587 U

(2σ+/-)

0.198

(2σ+/-)

105/17/16 18:0105/10/16 17:22pCi/L0.3491.00

RL MDC

0.198


Count Total

Uncert. Uncert.

Ba Carrier 40 - 110

Carrier

05/10/16 17:22 05/17/16 18:01 1


84.3

Y Carrier 40 - 110 05/10/16 17:22 05/17/16 18:01 190.5


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Analyte

Gross Alpha 4.43 G

(2σ+/-)

2.87

(2σ+/-)

106/09/16 08:0306/03/16 09:53pCi/L4.063.00

RL MDC

2.83


Count Total

Uncert. Uncert.

pCi/L 06/03/16 09:53 06/09/16 08:03 12.054.001.831.696.93Gross Beta


Analyte

Radium-226 0.164

(2σ+/-)

0.0697

(2σ+/-)

106/01/16 12:2405/10/16 15:18pCi/L0.07941.00

RL MDC

0.0681


Count Total

Uncert. Uncert.

Ba Carrier 40 - 110

Carrier

05/10/16 15:18 06/01/16 12:24 1


65.5


Analyte

Radium-228 0.0500 U

(2σ+/-)

0.276

(2σ+/-)

105/17/16 18:0105/10/16 17:22pCi/L0.4901.00

RL MDC

0.276


Count Total

Uncert. Uncert.

Ba Carrier 40 - 110

Carrier

05/10/16 17:22 05/17/16 18:01 1


65.5

Y Carrier 40 - 110 05/10/16 17:22 05/17/16 18:01 193.5


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Analyte

Gross Alpha 36.3

(2σ+/-)

8.38

(2σ+/-)

105/17/16 17:4805/16/16 15:33pCi/g4.7510.0

RL MDC

7.29


Count Total

Uncert. Uncert.

pCi/g 05/16/16 15:33 05/17/16 17:48 14.1510.05.944.6836.5Gross Beta


Analyte

Radium-226 3.37

(2σ+/-)

0.548

(2σ+/-)

106/02/16 09:2505/12/16 12:24pCi/g0.2671.00

RL MDC

0.422


Count Total

Uncert. Uncert.

pCi/g 05/12/16 12:24 06/02/16 09:25 10.4850.4670.4162.08Radium-228


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Lab Sample ID: 160-17284-31Client Sample ID: POND 4 SED SILT FENCEMatrix: SolidDate Collected: 05/03/16 11:45



Analyte

Gross Alpha 35.8

(2σ+/-)

9.30

(2σ+/-)

105/17/16 17:4905/16/16 15:33pCi/g7.8610.0

RL MDC

8.35


Count Total

Uncert. Uncert.

pCi/g 05/16/16 15:33 05/17/16 17:49 15.0910.06.025.0632.6Gross Beta


Analyte

Radium-226 3.41

(2σ+/-)

0.528

(2σ+/-)

106/02/16 09:4005/12/16 12:24pCi/g0.2311.00

RL MDC

0.392


Count Total

Uncert. Uncert.

pCi/g 05/12/16 12:24 06/02/16 09:40 10.2410.4650.4231.90Radium-228


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Lab Sample ID: 160-17284-32Client Sample ID: SED POND 1Matrix: WaterDate Collected: 05/03/16 14:10



Analyte


(2σ+/-)

4.07

(2σ+/-)

106/09/16 08:0306/03/16 09:53pCi/L5.943.00

RL MDC

4.02


Count Total

Uncert. Uncert.

pCi/L 06/03/16 09:53 06/09/16 08:03 13.154.002.542.418.00Gross Beta


Analyte

Radium-226 0.294

(2σ+/-)

0.0754

(2σ+/-)

106/01/16 12:2405/10/16 15:18pCi/L0.05681.00

RL MDC

0.0706


Count Total

Uncert. Uncert.

Ba Carrier 40 - 110

Carrier

05/10/16 15:18 06/01/16 12:24 1


96.9


Analyte

Radium-228 0.240 U

(2σ+/-)

0.215

(2σ+/-)

105/17/16 18:0205/10/16 17:22pCi/L0.3411.00

RL MDC

0.213


Count Total

Uncert. Uncert.

Ba Carrier 40 - 110

Carrier

05/10/16 17:22 05/17/16 18:02 1


96.9

Y Carrier 40 - 110 05/10/16 17:22 05/17/16 18:02 191.2


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Lab Sample ID: 160-17284-33Client Sample ID: SED POND 1 SEDIMENTMatrix: SolidDate Collected: 05/03/16 14:30



Analyte

Gross Alpha 26.6

(2σ+/-)

7.03

(2σ+/-)

105/17/16 17:4905/16/16 15:33pCi/g5.0810.0

RL MDC

6.34


Count Total

Uncert. Uncert.

pCi/g 05/16/16 15:33 05/17/16 17:49 13.7210.05.154.1330.7Gross Beta


Analyte

Radium-226 2.27

(2σ+/-)

0.433

(2σ+/-)

106/02/16 09:4105/12/16 12:24pCi/g0.2621.00

RL MDC

0.363


Count Total

Uncert. Uncert.

pCi/g 05/12/16 12:24 06/02/16 09:41 10.1570.3590.3321.33Radium-228


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Lab Sample ID: 160-17284-34Client Sample ID: OUTFALL 001Matrix: WaterDate Collected: 05/03/16 14:45



Analyte


(2σ+/-)

2.84

(2σ+/-)

106/09/16 08:0306/03/16 09:53pCi/L4.843.00

RL MDC

2.83


Count Total

Uncert. Uncert.

pCi/L 06/03/16 09:53 06/09/16 08:03 12.274.001.941.817.02Gross Beta


Analyte

Radium-226 0.305

(2σ+/-)

0.0842

(2σ+/-)

106/01/16 12:2405/10/16 15:18pCi/L0.06801.00

RL MDC

0.0796


Count Total

Uncert. Uncert.

Ba Carrier 40 - 110

Carrier

05/10/16 15:18 06/01/16 12:24 1


74.6


Analyte

Radium-228 -0.250 U

(2σ+/-)

0.279

(2σ+/-)

105/17/16 17:4505/10/16 17:22pCi/L0.5351.00

RL MDC

0.278


Count Total

Uncert. Uncert.

Ba Carrier 40 - 110

Carrier

05/10/16 17:22 05/17/16 17:45 1


74.5

Y Carrier 40 - 110 05/10/16 17:22 05/17/16 17:45 187.1


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Lab Sample ID: 160-17284-35Client Sample ID: LEACHATE EFFLEUNTMatrix: WaterDate Collected: 05/03/16 15:00



Analyte


(2σ+/-)

41.6

(2σ+/-)

106/09/16 08:1406/03/16 09:53pCi/L77.63.00

RL MDC

41.6


Count Total

Uncert. Uncert.

pCi/L 06/03/16 09:53 06/09/16 08:14 143.84.0074.653.3G521Gross Beta


Analyte

Radium-226 3.74

(2σ+/-)

0.490

(2σ+/-)

106/10/16 06:5505/17/16 15:37pCi/L0.1441.00

RL MDC

0.356


Count Total

Uncert. Uncert.

Ba Carrier 40 - 110

Carrier

05/17/16 15:37 06/10/16 06:55 1


88.0


Analyte

Radium-228 1.21

(2σ+/-)

0.537

(2σ+/-)

105/27/16 12:0605/19/16 14:12pCi/L0.7451.00

RL MDC

0.525


Count Total

Uncert. Uncert.

Ba Carrier 40 - 110

Carrier

05/19/16 14:12 05/27/16 12:06 1


88.0

Y Carrier 40 - 110 05/19/16 14:12 05/27/16 12:06 187.9


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Analyte

Gross Alpha 18.4 G

(2σ+/-)

8.35

(2σ+/-)

106/09/16 08:1506/03/16 09:53pCi/L9.643.00

RL MDC

8.08


Count Total

Uncert. Uncert.

pCi/L 06/03/16 09:53 06/09/16 08:15 14.894.004.454.11G17.0Gross Beta


Analyte

Radium-226 0.370 *

(2σ+/-)

0.0893

(2σ+/-)

106/02/16 13:5205/10/16 12:13pCi/L0.05681.00

RL MDC

0.0828


Count Total

Uncert. Uncert.

Ba Carrier 40 - 110

Carrier

05/10/16 12:13 06/02/16 13:52 1


82.6


Analyte

Radium-228 0.0952 U

(2σ+/-)

0.226

(2σ+/-)

105/17/16 12:4805/10/16 12:21pCi/L0.3891.00

RL MDC

0.226


Count Total

Uncert. Uncert.

Ba Carrier 40 - 110

Carrier

05/10/16 12:21 05/17/16 12:48 1


82.6

Y Carrier 40 - 110 05/10/16 12:21 05/17/16 12:48 192.3


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Lab Sample ID: 160-17284-37Client Sample ID: POND 2 OUTFALLMatrix: WaterDate Collected: 05/03/16 16:00



Analyte


(2σ+/-)

2.75

(2σ+/-)

106/09/16 08:1506/03/16 09:53pCi/L4.803.00

RL MDC

2.75


Count Total

Uncert. Uncert.

pCi/L 06/03/16 09:53 06/09/16 08:15 12.884.002.042.004.18Gross Beta


Analyte

Radium-226 0.0740 U *

(2σ+/-)

0.0594

(2σ+/-)

106/02/16 13:5205/10/16 12:13pCi/L0.09041.00

RL MDC

0.0590


Count Total

Uncert. Uncert.

Ba Carrier 40 - 110

Carrier

05/10/16 12:13 06/02/16 13:52 1


78.9


Analyte

Radium-228 -0.181 U

(2σ+/-)

0.174

(2σ+/-)

105/17/16 12:4805/10/16 12:21pCi/L0.3601.00

RL MDC

0.173


Count Total

Uncert. Uncert.

Ba Carrier 40 - 110

Carrier

05/10/16 12:21 05/17/16 12:48 1


78.9

Y Carrier 40 - 110 05/10/16 12:21 05/17/16 12:48 189.7


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Analyte

Gross Alpha 39.1

(2σ+/-)

8.63

(2σ+/-)

105/17/16 17:5005/16/16 15:33pCi/g4.8410.0

RL MDC

7.39


Count Total

Uncert. Uncert.

pCi/g 05/16/16 15:33 05/17/16 17:50 13.6110.06.014.5239.7Gross Beta


Analyte

Radium-226 4.75

(2σ+/-)

0.709

(2σ+/-)

106/02/16 10:0305/12/16 12:24pCi/g0.2721.00

RL MDC

0.509


Count Total

Uncert. Uncert.

pCi/g 05/12/16 12:24 06/02/16 10:03 10.3240.4550.4301.46Radium-228


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QC Sample ResultsTestAmerica Job ID: 160-17284-1Client: Commonwealth of Kentucky



Client Sample ID: Method BlankLab Sample ID: MB 160-251280/1-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 251461 Prep Batch: 251280

Gross Alpha

Analyte

U 105/17/16 17:4605/16/16 15:33pCi/g6.13

MDC

10.0

RL

3.263.26

(2σ+/-) (2σ+/-)

MB

0.4183

MB

Dil FacPrepared AnalyzedUnitResult Qualifier

Uncert.

Count

Uncert.

Total

105/17/16 17:4605/16/16 15:33pCi/g3.4110.02.332.294.357Gross Beta

Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-251280/2-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 251461 Prep Batch: 251280

Gross Alpha

Analyte

140-446417.3927.1 5.32 10.0 4.93

RL MDC(2σ+/-)

LCS LCS

pCi/g

UnitResult Qual %RecAdded

Spike

Limits

%Rec.Uncert.

Total

Gross Beta 26.8 23.11 3.60 10.0 2.44 pCi/g 86 38 - 130

Client Sample ID: Method BlankLab Sample ID: MB 160-254724/1-AMatrix: Water Prep Type: Total/NAAnalysis Batch: 255830 Prep Batch: 254724

Gross Alpha

Analyte

U 106/09/16 07:5806/03/16 09:53pCi/L0.890

MDC

3.00

RL

0.3430.340

(2σ+/-) (2σ+/-)

MB

-0.4251

MB


Uncert.

Count

Uncert.

Total

106/09/16 07:5806/03/16 09:53pCi/L0.8994.000.4910.491U-0.04452Gross Beta

Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-254724/2-AMatrix: Water Prep Type: Total/NAAnalysis Batch: 255830 Prep Batch: 254724

Gross Alpha

Analyte

133-738643.0850.0 6.45 3.00 1.25

RL MDC(2σ+/-)

LCS LCS

pCi/L


Spike

Limits

%Rec.Uncert.

Total

Client Sample ID: Lab Control SampleLab Sample ID: LCSB 160-254724/3-AMatrix: Water Prep Type: Total/NAAnalysis Batch: 255830 Prep Batch: 254724

Gross Beta

Analyte

125-759789.6192.7 9.49 4.00 0.893

RL MDC(2σ+/-)

LCSB LCSB

pCi/L


Spike

Limits

%Rec.Uncert.

Total

Client Sample ID: DRY BRANCH CREEK DOWNSTREAM DUPLab Sample ID: 160-17284-13 MSMatrix: Water Prep Type: Total/NAAnalysis Batch: 255830 Prep Batch: 254724

Gross Alpha

Analyte

140-608947.5350.02.89 7.19 3.00 1.79

RL MDC(2σ+/-)

MS MS

pCi/L


Spike

Result

Sample Sample

Qual Limits

%Rec.Uncert.

Total


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Method: 900.0 - Gross Alpha and Gross Beta Radioactivity (Continued)

Client Sample ID: DRY BRANCH CREEK DOWNSTREAM DUPLab Sample ID: 160-17284-13 MSBTMatrix: Water Prep Type: Total/NAAnalysis Batch: 255830 Prep Batch: 254724

Gross Beta

Analyte

140-609791.6892.71.61 9.71 4.00 1.06

RL MDC(2σ+/-)

MSBT MSBT

pCi/L


Spike

Result

Sample Sample

Qual Limits

%Rec.Uncert.

Total

Client Sample ID: DRY BRANCH CREEK DOWNSTREAM DUPLab Sample ID: 160-17284-13 DUMatrix: Water Prep Type: Total/NAAnalysis Batch: 255830 Prep Batch: 254724

Gross Alpha

Analyte

10.421.7102.89 1.18 3.00 1.62

RL MDC(2σ+/-)

DU DU

pCi/L

UnitResult Qual LimitResult

Sample Sample

Qual

Uncert.

Total

RER

RER

Gross Beta 1.61 1.864 0.804 4.00 1.11 pCi/L 0.16 1


Gross Alpha

Analyte

U 106/09/16 08:1406/03/16 09:53pCi/L1.09

MDC

3.00

RL

0.5720.572

(2σ+/-) (2σ+/-)

MB

0.0000

MB


Uncert.

Count

Uncert.

Total

106/09/16 08:1406/03/16 09:53pCi/L0.9704.000.5940.591U0.5397Gross Beta


Gross Alpha

Analyte

133-738944.6550.0 6.54 3.00 1.60

RL MDC(2σ+/-)

LCS LCS

pCi/L


Spike

Limits

%Rec.Uncert.

Total

Client Sample ID: Lab Control SampleLab Sample ID: LCSB 160-254725/3-AMatrix: Water Prep Type: Total/NAAnalysis Batch: 255829 Prep Batch: 254725

Gross Beta

Analyte

125-759890.4392.7 9.57 4.00 0.860

RL MDC(2σ+/-)

LCSB LCSB

pCi/L


Spike

Limits

%Rec.Uncert.

Total


Client Sample ID: Method BlankLab Sample ID: MB 160-250875/1-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 254484 Prep Batch: 250875

Radium-226

Analyte

U 106/02/16 08:2105/12/16 12:24pCi/g0.361

MDC

1.00

RL

0.08390.0837

(2σ+/-) (2σ+/-)

MB

-0.04844

MB


Uncert.

Count

Uncert.

Total

106/02/16 08:2105/12/16 12:24pCi/g0.2190.1510.151U0.06554Radium-228


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Method: 901.1 - Radium-226 & Other Gamma Emitters (GS) (Continued)

Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-250875/2-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 254482 Prep Batch: 250875

Americium-241

Analyte

116-879794.1497.1 9.87 0.990

RL MDC(2σ+/-)

LCS LCS

pCi/g


Spike

Limits

%Rec.Uncert.

Total

Cesium-137 29.7 27.87 2.95 0.165 pCi/g 94 87 - 120

Cobalt-60 17.2 15.68 1.62 0.123 pCi/g 91 87 - 115

Client Sample ID: ADS BRL-LT-SLLab Sample ID: 160-17284-16 DUMatrix: Solid Prep Type: Total/NAAnalysis Batch: 254534 Prep Batch: 250875

Radium-226

Analyte

10.224.8334.47 0.880 1.00 0.429

RL MDC(2σ+/-)

DU DU

pCi/g

UnitResult Qual LimitResult

Sample Sample

Qual

Uncert.

Total

RER

RER

Radium-228 2.28 1.870 0.724 0.754 pCi/g 0.31 1



Radium-226

Analyte

U 106/02/16 13:5205/10/16 12:13pCi/L0.0647

MDC

1.00

RL

0.04080.0407

(2σ+/-) (2σ+/-)

MB

0.03937

MB


Uncert.

Count

Uncert.

Total

Carrier

Ba Carrier 40 - 110 05/10/16 12:13 06/02/16 13:52 1

Dil FacPrepared AnalyzedQualifier Limits%Yield

86.9

MB MB


Radium-226

Analyte

137-68140*15.6611.2 1.50 1.00 0.0641

RL MDC(2σ+/-)

LCS LCS

pCi/L


Spike

Limits

%Rec.Uncert.

Total

Ba Carrier

Carrier

40 - 110

LCS

Qualifier Limits%Yield

81.8

LCS

Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 160-250356/3-AMatrix: Water Prep Type: Total/NAAnalysis Batch: 254506 Prep Batch: 250356

Radium-226

Analyte

10.21137-6813515.0411.2 1.44 1.00 0.0920

RL MDC(2σ+/-)

LCSD LCSD

pCi/L

UnitResult Qual %Rec LimitAdded

Spike

Limits

%Rec.Uncert.

Total

RER

RER


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Method: 903.0 - Radium-226 (GFPC) (Continued)


Ba Carrier

Carrier

40 - 110

LCSD


80.1

LCSD


Radium-226

Analyte

U 106/01/16 07:3305/10/16 15:18pCi/L0.0708

MDC

1.00

RL

0.03410.0341

(2σ+/-) (2σ+/-)

MB

-0.01042

MB


Uncert.

Count

Uncert.

Total

Carrier

Ba Carrier 40 - 110 05/10/16 15:18 06/01/16 07:33 1


86.3

MB MB


Radium-226

Analyte

137-6813214.6811.2 1.40 1.00 0.0799

RL MDC(2σ+/-)

LCS LCS

pCi/L


Spike

Limits

%Rec.Uncert.

Total

Ba Carrier

Carrier

40 - 110

LCS


86.3

LCS


Radium-226

Analyte

10.02137-6813214.7311.2 1.41 1.00 0.0669

RL MDC(2σ+/-)

LCSD LCSD

pCi/L


Spike

Limits

%Rec.Uncert.

Total

RER

RER

Ba Carrier

Carrier

40 - 110

LCSD


82.9

LCSD


Radium-226

Analyte

106/10/16 06:5505/17/16 15:37pCi/L0.126

MDC

1.00

RL

0.09330.0923

(2σ+/-) (2σ+/-)

MB

0.1529

MB


Uncert.

Count

Uncert.

Total

Carrier

Ba Carrier 40 - 110 05/17/16 15:37 06/10/16 06:55 1


92.9

MB MB


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Radium-226

Analyte

137-6812126.9822.3 2.59 1.00 0.119

RL MDC(2σ+/-)

LCS LCS

pCi/L


Spike

Limits

%Rec.Uncert.

Total

Ba Carrier

Carrier

40 - 110

LCS


93.4

LCS


Radium-226

Analyte

10.16137-6812527.8522.3 2.67 1.00 0.129

RL MDC(2σ+/-)

LCSD LCSD

pCi/L


Spike

Limits

%Rec.Uncert.

Total

RER

RER

Ba Carrier

Carrier

40 - 110

LCSD


92.3

LCSD



Radium-228

Analyte

U 105/17/16 12:4705/10/16 12:21pCi/L0.409

MDC

1.00

RL

0.2260.226

(2σ+/-) (2σ+/-)

MB

-0.03018

MB


Uncert.

Count

Uncert.

Total

Carrier

Ba Carrier 40 - 110 05/10/16 12:21 05/17/16 12:47 1


86.9

MB MB

05/10/16 12:21 05/17/16 12:47 1Y Carrier 91.6 40 - 110


Radium-228

Analyte

140-5612619.1215.2 2.01 1.00 0.450

RL MDC(2σ+/-)

LCS LCS

pCi/L


Spike

Limits

%Rec.Uncert.

Total

Ba Carrier

Carrier

40 - 110

LCS


81.8

LCS

Y Carrier 91.2 40 - 110


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Radium-228

Analyte

10.06140-5612518.9015.2 1.99 1.00 0.415

RL MDC(2σ+/-)

LCSD LCSD

pCi/L


Spike

Limits

%Rec.Uncert.

Total

RER

RER

Ba Carrier

Carrier

40 - 110

LCSD


80.1

LCSD

Y Carrier 92.3 40 - 110


Radium-228

Analyte

U 105/17/16 17:5605/10/16 17:22pCi/L0.400

MDC

1.00

RL

0.2240.224

(2σ+/-) (2σ+/-)

MB

0.01843

MB


Uncert.

Count

Uncert.

Total

Carrier

Ba Carrier 40 - 110 05/10/16 17:22 05/17/16 17:56 1


86.3

MB MB

05/10/16 17:22 05/17/16 17:56 1Y Carrier 88.6 40 - 110


Radium-228

Analyte

140-5611817.8615.2 1.89 1.00 0.404

RL MDC(2σ+/-)

LCS LCS

pCi/L


Spike

Limits

%Rec.Uncert.

Total

Ba Carrier

Carrier

40 - 110

LCS


86.3

LCS

Y Carrier 89.7 40 - 110


Radium-228

Analyte

10.11140-5611517.4615.2 1.86 1.00 0.395

RL MDC(2σ+/-)

LCSD LCSD

pCi/L


Spike

Limits

%Rec.Uncert.

Total

RER

RER

Ba Carrier

Carrier

40 - 110

LCSD


82.9

LCSD

Y Carrier 89.0 40 - 110


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Radium-228

Analyte

U 105/27/16 12:0505/19/16 14:12pCi/L0.793

MDC

1.00

RL

0.4460.446

(2σ+/-) (2σ+/-)

MB

-0.003885

MB


Uncert.

Count

Uncert.

Total

Carrier

Ba Carrier 40 - 110 05/19/16 14:12 05/27/16 12:05 1


92.9

MB MB

05/19/16 14:12 05/27/16 12:05 1Y Carrier 93.1 40 - 110


Radium-228

Analyte

140-5611935.8330.2 3.73 1.00 0.752

RL MDC(2σ+/-)

LCS LCS

pCi/L


Spike

Limits

%Rec.Uncert.

Total

Ba Carrier

Carrier

40 - 110

LCS


93.4

LCS

Y Carrier 91.6 40 - 110


Radium-228

Analyte

10.75140-5613941.8530.2 4.29 1.00 0.700

RL MDC(2σ+/-)

LCSD LCSD

pCi/L


Spike

Limits

%Rec.Uncert.

Total

RER

RER

Ba Carrier

Carrier

40 - 110

LCSD


92.3

LCSD

Y Carrier 87.9 40 - 110


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QC Association SummaryTestAmerica Job ID: 160-17284-1Client: Commonwealth of Kentucky


Rad

Leach Batch: 250107

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid Dry and Grind160-17284-10 #5 FILTER CAKE Total/NA



Solid Dry and Grind160-17284-16 ADS BRL-LT-SL Total/NA

Solid Dry and Grind160-17284-16 DU ADS BRL-LT-SL Total/NA

Solid Dry and Grind160-17284-20 POND 3 SEDIMENT Total/NA

Solid Dry and Grind160-17284-22 POND 3 SEDIMENT DUP Total/NA

Solid Dry and Grind160-17284-24 DRY BRANCH CREEK UPSTREAM SED Total/NA

Solid Dry and Grind160-17284-26 DRY BRANCH CREEK DOWNSTREAM SED Total/NA

Solid Dry and Grind160-17284-27 DRY BRANCH CREEK DOWNSTREAM SED DUPTotal/NA


Solid Dry and Grind160-17284-31 POND 4 SED SILT FENCE Total/NA

Solid Dry and Grind160-17284-33 SED POND 1 SEDIMENT Total/NA


Prep Batch: 250356


Water PrecSep-21160-17284-36 POND 2 Total/NA

Water PrecSep-21160-17284-37 POND 2 OUTFALL Total/NA

Water PrecSep-21LCS 160-250356/2-A Lab Control Sample Total/NA

Water PrecSep-21LCSD 160-250356/3-A Lab Control Sample Dup Total/NA

Water PrecSep-21MB 160-250356/1-A Method Blank Total/NA

Prep Batch: 250357


Water PrecSep_0160-17284-36 POND 2 Total/NA

Water PrecSep_0160-17284-37 POND 2 OUTFALL Total/NA

Water PrecSep_0LCS 160-250357/2-A Lab Control Sample Total/NA

Water PrecSep_0LCSD 160-250357/3-A Lab Control Sample Dup Total/NA

Water PrecSep_0MB 160-250357/1-A Method Blank Total/NA

Prep Batch: 250373


Water PrecSep-21160-17284-1 MW-17R-AKGWA 8003-8393 Total/NA

Water PrecSep-21160-17284-2 MW-10-AKGWA 8001-0201 Total/NA


Water PrecSep-21160-17284-4 MW-15R-AKGWA 8003-3579 Total/NA


Water PrecSep-21160-17284-7 #2 UV EFFLUENT CHANNEL83 DEGREES 58.917Total/NA

Water PrecSep-21160-17284-9 #4 WWTP INFLUENT Total/NA

Water PrecSep-21160-17284-13 DRY BRANCH CREEK DOWNSTREAM DUP Total/NA

Water PrecSep-21160-17284-14 POND 3 ABOVE OUTFALL Total/NA

Water PrecSep-21160-17284-17 ADS BRL UNDERDRAIN Total/NA


Water PrecSep-21160-17284-19 POND 3 OUTFALL Total/NA

Water PrecSep-21160-17284-21 POND 3 DUP Total/NA

Water PrecSep-21160-17284-23 DRY BRANCH CREEK UPSTREAM Total/NA

Water PrecSep-21160-17284-25 DRY BRANCH CREEK DOWNSTREAM Total/NA

Water PrecSep-21160-17284-28 OUTFALL 004 Total/NA


Water PrecSep-21160-17284-32 SED POND 1 Total/NA


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Rad (Continued)

Prep Batch: 250373 (Continued)


Water PrecSep-21160-17284-34 OUTFALL 001 Total/NA




Prep Batch: 250391


Water PrecSep_0160-17284-1 MW-17R-AKGWA 8003-8393 Total/NA

Water PrecSep_0160-17284-2 MW-10-AKGWA 8001-0201 Total/NA


Water PrecSep_0160-17284-4 MW-15R-AKGWA 8003-3579 Total/NA


Water PrecSep_0160-17284-7 #2 UV EFFLUENT CHANNEL83 DEGREES 58.917Total/NA

Water PrecSep_0160-17284-9 #4 WWTP INFLUENT Total/NA

Water PrecSep_0160-17284-13 DRY BRANCH CREEK DOWNSTREAM DUP Total/NA

Water PrecSep_0160-17284-14 POND 3 ABOVE OUTFALL Total/NA

Water PrecSep_0160-17284-17 ADS BRL UNDERDRAIN Total/NA


Water PrecSep_0160-17284-19 POND 3 OUTFALL Total/NA

Water PrecSep_0160-17284-21 POND 3 DUP Total/NA

Water PrecSep_0160-17284-23 DRY BRANCH CREEK UPSTREAM Total/NA

Water PrecSep_0160-17284-25 DRY BRANCH CREEK DOWNSTREAM Total/NA

Water PrecSep_0160-17284-28 OUTFALL 004 Total/NA


Water PrecSep_0160-17284-32 SED POND 1 Total/NA

Water PrecSep_0160-17284-34 OUTFALL 001 Total/NA




Prep Batch: 250875


Solid Fill_Geo-21 250107160-17284-10 #5 FILTER CAKE Total/NA

Solid Fill_Geo-21 250107160-17284-11 #6 FILTER CAKE Total/NA

Solid Fill_Geo-21 250107160-17284-16 ADS BRL-LT-SL Total/NA

Solid Fill_Geo-21 250107160-17284-16 DU ADS BRL-LT-SL Total/NA

Solid Fill_Geo-21 250107160-17284-20 POND 3 SEDIMENT Total/NA

Solid Fill_Geo-21 250107160-17284-22 POND 3 SEDIMENT DUP Total/NA

Solid Fill_Geo-21 250107160-17284-24 DRY BRANCH CREEK UPSTREAM SED Total/NA

Solid Fill_Geo-21 250107160-17284-26 DRY BRANCH CREEK DOWNSTREAM SED Total/NA

Solid Fill_Geo-21 250107160-17284-27 DRY BRANCH CREEK DOWNSTREAM SED DUPTotal/NA


Solid Fill_Geo-21 250107160-17284-31 POND 4 SED SILT FENCE Total/NA

Solid Fill_Geo-21 250107160-17284-33 SED POND 1 SEDIMENT Total/NA


Solid Fill_Geo-21LCS 160-250875/2-A Lab Control Sample Total/NA

Solid Fill_Geo-21MB 160-250875/1-A Method Blank Total/NA

Prep Batch: 251280


Solid Thin_Layer 250107160-17284-12 #7 FILTER CAKE Total/NA


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Rad (Continued)



Solid Thin_Layer 250107160-17284-16 ADS BRL-LT-SL Total/NA

Solid Thin_Layer 250107160-17284-20 POND 3 SEDIMENT Total/NA

Solid Thin_Layer 250107160-17284-22 POND 3 SEDIMENT DUP Total/NA

Solid Thin_Layer 250107160-17284-24 DRY BRANCH CREEK UPSTREAM SED Total/NA

Solid Thin_Layer 250107160-17284-26 DRY BRANCH CREEK DOWNSTREAM SED Total/NA

Solid Thin_Layer 250107160-17284-27 DRY BRANCH CREEK DOWNSTREAM SED DUPTotal/NA


Solid Thin_Layer 250107160-17284-31 POND 4 SED SILT FENCE Total/NA

Solid Thin_Layer 250107160-17284-33 SED POND 1 SEDIMENT Total/NA


Solid Thin_LayerLCS 160-251280/2-A Lab Control Sample Total/NA

Solid Thin_LayerMB 160-251280/1-A Method Blank Total/NA

Prep Batch: 251589


Water PrecSep-21160-17284-15 ADS BRL-LT-LIQ Total/NA

Water PrecSep-21160-17284-35 LEACHATE EFFLEUNT Total/NA




Prep Batch: 252055


Water PrecSep_0160-17284-15 ADS BRL-LT-LIQ Total/NA

Water PrecSep_0160-17284-35 LEACHATE EFFLEUNT Total/NA




Prep Batch: 254724


Water Evaporation160-17284-1 MW-17R-AKGWA 8003-8393 Total/NA

Water Evaporation160-17284-2 MW-10-AKGWA 8001-0201 Total/NA


Water Evaporation160-17284-4 MW-15R-AKGWA 8003-3579 Total/NA


Water Evaporation160-17284-6 #1 UV EFFLUENT CHANNEL 37 DEGREES 42.086'Total/NA

Water Evaporation160-17284-8 #3 WWTP INFLUENT Total/NA

Water Evaporation160-17284-13 DRY BRANCH CREEK DOWNSTREAM DUP Total/NA

Water Evaporation160-17284-13 DU DRY BRANCH CREEK DOWNSTREAM DUP Total/NA

Water Evaporation160-17284-13 MS DRY BRANCH CREEK DOWNSTREAM DUP Total/NA

Water Evaporation160-17284-13 MSBT DRY BRANCH CREEK DOWNSTREAM DUP Total/NA

Water Evaporation160-17284-14 POND 3 ABOVE OUTFALL Total/NA

Water Evaporation160-17284-15 ADS BRL-LT-LIQ Total/NA

Water Evaporation160-17284-17 ADS BRL UNDERDRAIN Total/NA

Water Evaporation160-17284-18 POND 3 Total/NA

Water Evaporation160-17284-19 POND 3 OUTFALL Total/NA

Water Evaporation160-17284-21 POND 3 DUP Total/NA

Water Evaporation160-17284-23 DRY BRANCH CREEK UPSTREAM Total/NA

Water Evaporation160-17284-25 DRY BRANCH CREEK DOWNSTREAM Total/NA

Water Evaporation160-17284-28 OUTFALL 004 Total/NA


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Rad (Continued)




Water Evaporation160-17284-32 SED POND 1 Total/NA

Water Evaporation160-17284-34 OUTFALL 001 Total/NA

Water EvaporationLCS 160-254724/2-A Lab Control Sample Total/NA

Water EvaporationLCSB 160-254724/3-A Lab Control Sample Total/NA

Water EvaporationMB 160-254724/1-A Method Blank Total/NA

Prep Batch: 254725


Water Evaporation160-17284-35 LEACHATE EFFLEUNT Total/NA


Water Evaporation160-17284-37 POND 2 OUTFALL Total/NA

Water EvaporationLCS 160-254725/2-A Lab Control Sample Total/NA

Water EvaporationLCSB 160-254725/3-A Lab Control Sample Total/NA

Water EvaporationMB 160-254725/1-A Method Blank Total/NA


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Tracer/Carrier SummaryTestAmerica Job ID: 160-17284-1Client: Commonwealth of Kentucky


Method: 903.0 - Radium-226 (GFPC)Prep Type: Total/NAMatrix: Water

Lab Sample ID Client Sample ID (40-110)

Ba

85.5160-17284-1

Percent Yield (Acceptance Limits)

MW-17R-AKGWA 8003-8393

74.9160-17284-2 MW-10-AKGWA 8001-0201

100160-17284-3 MW-13-AKGWA 8001-2025

79.5160-17284-4 MW-15R-AKGWA 8003-3579

84.9160-17284-5 MW-7-AKGWA 8001-0205

82.1160-17284-7 #2 UV EFFLUENT CHANNEL83

DEGREES 58.91740.7160-17284-9 #4 WWTP INFLUENT

80.6160-17284-13 DRY BRANCH CREEK

DOWNSTREAM DUP82.9160-17284-14 POND 3 ABOVE OUTFALL

87.7160-17284-15 ADS BRL-LT-LIQ

93.7160-17284-17 ADS BRL UNDERDRAIN

76.9160-17284-18 POND 3

80.6160-17284-19 POND 3 OUTFALL

86.0160-17284-21 POND 3 DUP

83.5160-17284-23 DRY BRANCH CREEK

UPSTREAM80.9160-17284-25 DRY BRANCH CREEK

DOWNSTREAM84.3160-17284-28 OUTFALL 004

65.5160-17284-29 POND 4

96.9160-17284-32 SED POND 1

74.6160-17284-34 OUTFALL 001

88.0160-17284-35 LEACHATE EFFLEUNT

82.6160-17284-36 POND 2

78.9160-17284-37 POND 2 OUTFALL

81.8LCS 160-250356/2-A Lab Control Sample



80.1LCSD 160-250356/3-A Lab Control Sample Dup



86.9MB 160-250356/1-A Method Blank



Tracer/Carrier Legend

Ba = Ba Carrier

Method: 904.0 - Radium-228 (GFPC)Prep Type: Total/NAMatrix: Water

Lab Sample ID Client Sample ID (40-110) (40-110)

Ba Y

85.5 88.6160-17284-1


MW-17R-AKGWA 8003-8393

74.9 87.1160-17284-2 MW-10-AKGWA 8001-0201

100 86.4160-17284-3 MW-13-AKGWA 8001-2025

79.5 87.1160-17284-4 MW-15R-AKGWA 8003-3579


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Tracer/Carrier SummaryTestAmerica Job ID: 160-17284-1Client: Commonwealth of Kentucky


Method: 904.0 - Radium-228 (GFPC) (Continued)Prep Type: Total/NAMatrix: Water

Lab Sample ID Client Sample ID (40-110) (40-110)

Ba Y

84.9 84.5160-17284-5


MW-7-AKGWA 8001-0205

82.1 89.3160-17284-7 #2 UV EFFLUENT CHANNEL83

DEGREES 58.91740.7 80.7160-17284-9 #4 WWTP INFLUENT

80.6 89.3160-17284-13 DRY BRANCH CREEK

DOWNSTREAM DUP82.9 90.1160-17284-14 POND 3 ABOVE OUTFALL

87.7 83.4160-17284-15 ADS BRL-LT-LIQ

93.7 85.6160-17284-17 ADS BRL UNDERDRAIN

76.9 89.7160-17284-18 POND 3

80.6 89.7160-17284-19 POND 3 OUTFALL

86.0 90.1160-17284-21 POND 3 DUP

83.5 88.6160-17284-23 DRY BRANCH CREEK

UPSTREAM80.9 95.0160-17284-25 DRY BRANCH CREEK

DOWNSTREAM84.3 90.5160-17284-28 OUTFALL 004

65.5 93.5160-17284-29 POND 4

96.9 91.2160-17284-32 SED POND 1

74.5 87.1160-17284-34 OUTFALL 001

88.0 87.9160-17284-35 LEACHATE EFFLEUNT

82.6 92.3160-17284-36 POND 2

78.9 89.7160-17284-37 POND 2 OUTFALL

81.8 91.2LCS 160-250357/2-A Lab Control Sample



80.1 92.3LCSD 160-250357/3-A Lab Control Sample Dup



86.9 91.6MB 160-250357/1-A Method Blank

86.3 88.6MB 160-250391/1-A Method Blank

92.9 93.1MB 160-252055/1-A Method Blank

Tracer/Carrier Legend

Ba = Ba Carrier

Y = Y Carrier


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Date post:	20-Jun-2020
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