ANALYTICAL REPORT FOR WHITE SWAN LAUNDRY AND ...284-190 Unit 092 SS-092P2 284-191 Unit 093 SS-093...

198221

l l l l l l l l l i l l l l l l

ANALYTICAL REPORT

Prepared by LOCKHEED MARTIN, Inc.

White Swan Laundry & Cleaners/Sun Cleaners Area Vapor Intrusion Study Sea Girt, NJ

August 2009

EPA Work Assignment No. 0-284 LOCKHEED MARTIN Work Order EAC00284

EPA Contract No. EP-C-04-032

Submitted to R. Connell EPA-ERT

Analysis by: Columbia

Prepared by: Y. Mehra

Reviewed by: J. Soroka

0284-DAR-082509

Table of Contents

Topic

Introduction Case Narrative Summary of Abbreviations

Section I

Results of the Analysis for VOC (ppbv) in Air Table 1.1a Results of the Analysis for VOC (ug/m3) in Air Table 1.1b

Section II

Results of the Results of the

LCS Analysis for VOC in Air Duplicate Analysis for VOC in Air

Table 2.1 Table

2.2

Section III

Correspondence Chains of Custody

Appendices

Appendix A Data for VOC in Air U270

The appendix A will be furnished on request

0284-DAR-082509

Introduction

REAC personnel, in response to WA# 0-284, provided analytical support for environmental samples collected from the White Swan Laundry & Cleaners/ Sun Cleaners Area Vapor Intrusion Study Site located in Sea Girt, NJ, as described in the following table. The support also included QA/QC, data review and preparation of an analytical report containing analytical and QA/QC results.

coc# Number

of Samples

Sampling Date

Date Received Matrix

Analysis/ Method

Laboratory Data Package

0-284-07/10/09-0034 4 07/08/09 07/11/09 Air VOC/TO-15 (SIM)

Columbia • Analytical

Services1

U270

0-284-07/10/09-0035 4

VOC/TO-15 (SIM)

Columbia • Analytical

Services1

0-284-07/10/09-0036 4

0-284-07/10/09-0037 4

0-284-07/10/09-0038 4

0-284-07/10/09-0039 4

0-284-07/10/09-0040 4

CAS is NELAC certified for TO-15 analysis.

Case Narrative

The laboratory reported the data to two significant figures. Any other representation of the data is the responsibility of the user. All data validation flags have been inserted into the results tables. At the request of the WAM, the laboratory reported only eight chlorinated compounds.

VOC in Air Package U 270

The data package was examined and found to be acceptable.

0284-DAR-082509 1

Summary of Abbreviations

BFB Bromofluorobenzene C Centigrade CLP Contract Laboratory Program COC Chain of Custody cone concentration cont continued CRDL Contract Required Detection Limit CRQL Contract Required Quantitation Limit D (Surrogate Table) value is from a diluted sample and was not calculated Dioxin Polychlorinated dibenzo-p-dioxins (PCDD) and Polychlorinated dibenzofurans (PCDF) DFTPP Decafluorotriphenylphosphine EMPC Estimated maximum possible concentration GC/MS Gas Chromatography/ Mass Spectrometry IS . Internal Standard LCS Laboratory Control Sample LCSD Laboratory Control Sample Duplicate MDA Minimum Detectable Activity MS (BS)Matrix Spike (Blank Spike) MSD (BSD) Matrix Spike Duplicate (Blank Spike Duplicate) MW Molecular Weight NA Not Applicable or Not Available NAD Normalized Absolute Difference NC Not Calculated NR Not Requested/Not Reported NS Not Spiked % D Percent Difference % REC Percent Recovery SOP Standard Operating Procedure ppbv parts per billion by volume ppm parts per million pptv parts per trillion by volume PQL Practical Quantitation Limit QA/QC Quality Assurance/Quality Control QL Quantitation Limit REAC Response Engineering and Analytical Contract RL Reporting Limit RPD Relative Percent Difference RSD Relative Standard Deviation SIM Selected Ion Monitoring Sur Surrogate TIC Tentatively Identified Compound TCLP Toxicity Characteristic Leaching Procedure VOC Volatile Organic Compound * Value exceeds the acceptable QC limits.

m cubic meter microgram nanogram

uL Pg

gram microliter picogram

kg kilogram mg milligram pCi picocurie

L liter mL milliliter s sigma

Data Validation Flags

J Value is estimated R J+ Value is estimated high (metals only) U J- Value is estimated low (metals only) UJ N Presumptively present (Aroclors only) Rev. 1/14/09

Value is unusable Not detected Not detected and RL is. estimated

0284-DAR-082509 2

Table 1.1a Results of the Analysis for VOC (ppbv) in Air WA # 284 White Swan Laundry & Cleaners/Sun'Cleaners Area Vapor Intrusion Study

Method TO-15 Page 1 of 3

Sample Number Sample Location Sublocation

7/14/2009 Method Blank

284-188 Unit 091 SS-091

284-189 Unit 092

SS-092P1

284-190 Unit 092

SS-092P2

284-191 Unit 093 SS-093 •

Result RL Result RL Result RL Result RL Result RL Analyte ppbv ppbv Rpbv ppbv ppbv ppbv ppbv ppbv ppbv ppbv

Vinyl Chloride U 0.039 U 0.059 U 0.060 U 0.061 U 0.062 1,1-Dichloroethene U 0.025 U 0.038 U 0.039 U 0.039 U 0.040 trans-1,2-Dichloroethene U 0.025 U 0.038 U 0.039 U 0.039 U 0.040

1,1-Dichloroethane U 0.025 U 0.038 U ' 0.038 U 0.039 U 0.039 cis-1,2-Dichloroethene U 0.025 U 0.038 U 0.039 U 0.039 U 0.040 1,1,1-Trichloroethane U 0.018 U 0.028 U 0.028 0.036 0.029 0.053 0.029 Trichloroethene U 0.019 U 0.028 U 0.028 0.038 0.029 0.053 0.029 Tetrachloroethene U 0.015 4.5 0.022 0.047 0.023 0.15 0.023 0.090 0.023

Table 1.1a (cont) Results of the Analysis for VOC (ppbv) in Air WA # 284 White Swan Laundry & Cleaners/Sun Cleaners Area Vapor Intrusion Study

Method TO-15

Sample Number 284-192 284-193 284 :194 284-195 284-215 Sample Location Unit 094 Unit 095 Unit 096 Unit 096 Trip Blank Sublocation SS-094 SS-095 SS-096P1 SS-096P2

Result RL Result RL Result RL Result RL Result RL

Analyte ppbv ppbv ppbv ppbv ppbv ppbv ppbv ppbv ppbv ppbv

Vinyl Chloride U 0.063 U 0.060 U 0.049 U 0.068 U 0.039

1,1-Dichloroethene U 0.041. U 0.039 U 0.032 U 0.044 U 0.025

trans-1,2-Dichloroethene U 0.041 U 0.039 U 0.032 U 0.044 U 0.025

1,1-Dichloroethane U 0.040 U 0.038 U 0.031 U 0.043 U 0.025

cis-1,2-Dichloroethene U 0.041 U 0.039 U 0.032 U 0.044 U 0.025

1,1,1-Trichloroethane 0.032 0.030 U 0.028 0.023 0.023 U 0.032 U 0.018

Trichloroethene U 0.030 U 0.028 U 0.023 U 0.032 U 0.019

Tetrachloroethene 0.56 0.024 12 0.023 0.70 0.019 0.36 0.026 U 0.015

Method TO-15

Table 1.1 a (cont) Results of the Analysis for VOC (ppbv) in Air WA # 284 White Swan Laundry 8i Cleaners/Sun Cleaners Area Vapor Intrusion Study



284-196 Unit 097 SS-097

284-197 Unit 098 IA-098 -

284-198 Unit 098

AMB-098

284-199 Unit 099 SS-099

Result RL Result RL Result RL - Result RL Result RL


Vinyl Chloride U 0.039 U 0.063 U 0.064 U 0.060 U 0.060

1,1-Dichloroethene . U 0.025 U 0.040 U 0.041 U 0.039 U 0.039



cis-1,2-Dichloroethene U 0.025 1.0 0.040 U 0.041 U 0.039 U 0.039

1,1,1 -Trichloroethane U 0.018 0.034 0.029 ' U 0.030 U 0.028 0.099 0.028

Trichloroethene U 0.019 3.1 0.030 U 0.030 U 0.029 0.052 0.029

Tetrachloroethene U 0.015 230 0.47 0.13 0.024 0.037 0.023 45 0.23

0284-DAR-082509 3

Method TO-15

Table 1.1a (cont) Results of the Analysis for VOC (ppbv) in Air WA # 284 White Swan Laundry 81 Cleaners/Sun Cleaners Area Vapor Intrusion Study

Page 2 of 3


284-200 Unit 100

SS-100P1

284-201 Unit 100

SS-100P2

284-202 Unit 101 SS-101

284-203 Unit 102 SS-102

284-204 Unit 103 SS-103

Result RL Result RL Result RL Result RL Result RL Analyte ppbv ppbv ppbv ppbv ppbv ppbv ppbv ppbv ppbv ppbv

Vinyl Chloride U 0.061 U 0.063 U 0.052 U 0.058 U 0.060 1,1-Dichloroethene U 0.040 U 0.041 U 0.034 U 0.038 U 0.039 trans-1,2-Dichloroethene U 0.040 U 0.041 U 0.034 U 0.038 U 0.039 1,1-Dichloroethane U 0.039 U 0.040 U 0.033 U 0.037 U 0.038 cis-1,2-Dichloroethene U 0.040 U 0.041 U 0.034 U 0.038 U 0.039

1,1,1-Trichloroethane U 0.029 U 0.030 0.43 0.024 0.29 0.027 0.089 0.028

Trichloroethene U 0.029 U. 0.030 0.12 0.025 U 0.028 0.079 0.028 Tetrachloroethene 1.7 0.023 . 0.99 0.024 69 2.0 12 0.022 19 0.23

Method TO-15 (SIM)



284-205 Unit 104 SS-104

284-206 Unit 105 SS-105


284-207 Unit 105

AMB-105

284-208 Unit 106 SS-106



Vinyl Chloride U 0.07 U 0.061 U 0.039 U 0.058 U 0.058 1,1-Dichloroethene U 0.045 U 0.040 U 0.025 U 0.038 U 0.037


1,1-Dichloroethane U 0.044 U 0.039 U 0.025 U 0.037 U 0.036 cis-1,2-Dichloroethene U 0.045 U 0.040 U 0.025 U 0.038 U 0.037 1,1,1-Trichloroethane U 0.033 U 0.029 U 0.018 U 0.027 U 0.027 Trichloroethene 0.050 0.033 0.12 0.029 U 0.019 U 0.028 U 0.027 Tetrachloroethene 22 0.26 46 0.23 U 0.015 0.13 0.022 30 0.22

Method TO-15 (SIM)


Sample Number 284-209 284-210 284-211 284-212 284-213 Sample Location Unit 107 Unit 108 Unit 109 Unit 110 Unit 111 Sublocation SS-107 SS-108 SS-109 SS-110 SS-111



Vinyl Chloride U 0.055 U 0.056 U 0.061 U 0.051 U 0.060 1,1-Dichloroethene U 0.036 U 0.036 U 0.040 U 0.033 U 0.039

trans-1,2-Dichloroethene U 0.036 U 0.036 U 0.040 U 0.033 . U 0.039


cis-1,2-Dichloroethene U 0.036 U 0.036 U 0.040 U 0.033 U 0.039 1,1,1-Trichloroethane U 0.026 0.21 0.026 U 0.029 0.15 0.024 0.61 0.028

Trichloroethene U 0.026 U 0.027 U 0.029 U 0.024 0.12 0.029

Tetrachloroethene 8.5 0.021 0.48 0.021 0.29 0.023 2.4 0.019 0.73 0.023

0284-DAR-082509 4

Method TO-15 (SIM)


Page 3 of 3

Sample Number 284-•214 7/21/2009 Sample Location Unit 112 Method Blank Sublocation ss-112

Result RL Result RL Analyte ppbv ppbv ppbv ppbv

Vinyl Chloride U 0.060 U 0.039 1,1-Dichloroethene U 0.039 U 0.025 trans-1,2-Dichloroethene U 0.039 U 0.025 1,1-Dichloroethane U 0.038 U 0.025 cis-1,2-Dichloroethene U 0.039 U 0.025 1,1,1-Trichloroethane 0.029 0.028 U 0.018 Trichloroethene U 0.028 U 0.019 Tetrachloroethene 3.0 0.023 U 0.015

0284-DAR-082509 5

Table 1.1b Results of the Analysis for VOC (pg/m ) in Air WA # 284 White Swan Laundry & Cleaners/Sun Cleaners Area Vapor Intrusion Study

Method TO-15 v \H Page 1 of 3

; ' l l

V i - / , ' -r(. Sample Number 7/14/2009 •> 284-188 jg?) 284-189 1 284-190 284-191 Vi Sample Location Method Blank Unit 091 i " Unit 092 Unit 092 Unit 093 |/> Sublocation SS-091 SS-092P1 SS-092P2 SS-093 l -

- Result RL Result RL Result RL . Result RL Result RL

Analyte pg/m3 pg/m3 ug/m3 pg/m3 pg/m3 pg/m3 pg/m3 pg/m3 pg/m3 pg/m3

Vinyl Chloride U 0.10 U 0.15 U 0.15 U 0.16 U 0.16 1.1-Dichloroethene U 0.10 U 0.15 U 0.15 U 0.16 0 0.16 trans-1,2-Dichtoroethene U 0.10 . U 0.15 U 0.15 U" 0.16 U 0.16 1,1-Dichloroethane U 0.10 U 0.15 U 0.15 U 0.16 U 0.16 cis-1,2-Dichloroethene U 0.10 U 0.15 U 0.15 U 0.16 U 0.16 1,1,1-Trichloroethane • U 0.10 ,u 0.15 ' // U 0.15 0.20 0.16 0.29 0.16 Trichloroethene U 0.10 0.15 ' ^ / U 0.15 ' A20 0.16 / 0.28 0.16 Tetrachloroethene U 0.10 • . / 31 0.15 \ / 0 . 3 2 0.15 / 1.0 0.16 7 0.61 0.16

fr Table

WA # 284 White

Method TO-15


v l v w 0 284-192 Unit 094 SS-094

1.1b (cont) Results of the Analysis for VOC (pg/m ) in Air Swan Laundry & Cleaners/Sun Cleaners Area Vapor Intrusion Study

1 / 5 - j ^ . 284-193 Unit 095 SS-095

284-194 ' | Unit 096 / > - ^

SS-096P1

284-195 Unit 096

SS-096P2

Analyte

Result pg/m3

RL pg/m3

I Result.

i pg/m3 RL pg/m3

Result pg/m3

RL pg/m3

Result

pg/m3 RL I pg/m3 I

Result pg/m3

RL pg/m

Vinyl Chloride U 0.16 U 0.15 U 0.13 U 0.17 U 0.10 1,1-Dichloroethene U 0.16 U 0.15 U 0.13 u 0.17 U 0.10 trans-1,2-Dichloroethene U 0.16 U 0.15 U 0.13 U 0.17 U 0.10 1,1-Dichloroethane U 0.16 U 0.15 U 0.13 u 0.17 . U 0.10 cis-1,2-Dichloroethene 0.16 U 0.15 U 0.13 0.17 U 0.10 1,1,1-Trichloroethane ; i, 0.17 0.16 / U 0.15 0. 13 0.13 / u 0.17 U 0.10 Trichloroethene i . u 0.16 \ U 0.15 / U 0.13 y u 0.17 u 0.10 Tetrachloroethene 3.8 0.16 V 79 0.15 / 4.7 0.13 2.5 0.17 U 0.10

—* /

Table 1.1b (cont) Results of the Analysis for VOC (pg/m3) in Any 1 f WA # 284 White Swan Laundry & Cleaners/; Sun Cleaners Area Vapor Intrusion Study W

Method TO-15



284-196 Unit 097 SS-097

W4 • 284-197

RJ>. Unit 098 IA-098

i

284-198 Unit 098

AMB-098

284-199 Unit 099 SS-099

Analyte , Result

pg/m3 RL pg/m3

Result RL Result pg/m3 pg/m3 j pg/m3

RL Result RL ! Result RL pg/m3 pg/m3 pg/m3 1 pg/m3 pg/m3

0.16 U 0.15 1

U 0.15 0.16 U 0.15 U 0.15 0.16 U 0.15 U 0.15 0.16 U 0.15 U 0.15 0.16 / / U 0.15 U 0.15 0.16 1 U 0.15 0.54 0.15 0.16 " / U- 0.15 0.28 0.15 0.16 ' ' 0.25 0.15 300 1.5

Vinyl Chloride 1.1-Dichloroethene trans-1,2-Dichloroethene 1,1-Dichloroethane cis-1,2-Dichloroethene 1,1,1-Trichloroethane Trichloroethene Tetrachloroethene

U U U U U U U U 0.10

0.10 0.10 0.10 0.10 0.10 0.10 -J 0.10 \ /

o.io \J

U u u u

4.2 0.19

17

0.16 0.16 0.16 0.16 0.16 0.16 0.16 /

0284-DAR-082509 6

Table 1.1b (cont) Results of the Analysis for VOC (pg/m3) in Air P" WA # 284 White Swan Laundry & Cleaners/Sun Cleaners Area Vapor Intrusion Study

Method TO-15


Anaiyte

284-200 Unit 100

SS-100P1

Result RL pg/m3 pg/m3

284-201 Unit 100

SS-100P2

Result pg/m3

RL pg/m3

284-202 Unit 101 SS-101


/ O 0 / .

284-203 | J J Unit 102 SS-102


(2j 284-204 Unit 103 SS-103

Result RL [/ pg/m3 pg/m3

Vinyl Chloride 1,1-Dichloroethene trans-1,2-Dichloroethene 1,1-Dichloroethane cis-1,2-Dichloroethene 1,1,1-Trichloroethane Trichloroethene Tetrachloroethene

U U U U U U U

12

0.16 0.16 0.16 0.16 0.16 0.16 0.16 0.16

u 0.16 U 0.13 U 0.16 U 0.13

u 0.16 i /u 0.13

u 0.16 i / u 0.13 u 0.16 0.13 u 0.16 r 2.3 j 0.13 u 0.16 0.65 0.13

6.7 0.16 470 I 1.3

'Hug,1') o.i • j 0.43': 0.1 •I 130/ 1.5

0.15 0.15 0.15 0.15 0.15

5 5

5

Method TO-15

Sample Number ' Sample Location Sublocation

Analyte

Table 1.1b (cont) Results of the Analysis for VOC (pg/m3) in Air WA # 284 White Swan Laundry & Cleaners/Sun Cleaners Area Vapor Intrusion Study

284-205 i Unit 104

• 1 V SS-104


» 284-206 K « Unit 105

SS-105


'T\,

7/20/2009 MethocKBIank

Result pg/m3

RL pg/m3

284-207 Unit 105

AMB-105

Result RL ug/m3 ug/m3

284-208 ( Unit 106 • SS-106

Result RL

ug/m3 ug/m3

Vinyl Chloride 1,1-Dichloroethene trans-1,2-Dichloroethene 1,1-Dichloroethane -cis-1,2-Dichloroethene 1,1,1-Trichloroethane Trichloroethene Tetrachloroethene ^150.

•U , U M

0.18 U 0.16 U 0.10 0.18 U 0.16 U 0.10 0.18 U 0.16 U 0.10 0.18 / U 0.16 U 0.10 0.18 / U 0.16 U 0.10 0.18 V -U 0.16 U 0.10 0.18 '0.67 0.16 ' U 0.10 1.8 1 310 1.6 U 0.10

u 0.15 \ U 0.15 u 0.15 u 0.15 u 0.15 , u 0.15

, u 0.15 \ u 0.15

h 0.15 0.15 ' u 0.15 0.15 u 0.15 0.15

0ji8_ 0.15 I 200 1.5

Method TO-15


1 , , * * \ Table 1.1b (cont) Results of the Analysis for VOC (pg/m3) in Air f t i Y

WA # 284 White Swan Laundry & Cleaners/Sun Cleaners Area Vapor Intrusion Study —^t^ A

284-209 Unit 107 SS-107

'Villi j , 284-210 I NO Unit 108

SS-108

Result RL

284-211 1 Unit 109 SS-109

Result RL

-14-212 (OJ lit 110 '^•'J

284-! Unit 110 SS-110

bar

284-213 fi-fj Unit 111 SS-111

Result RL pg/m'

Vinyl Chloride U 0.14 U 0.14 > U 0.16 II

U 0.13 li • u 0.15 1,1-Dichloroethene U 0.14 U 0.14 , u 0.16 / U 0.13 •, u 0.15 trans-1,2-Dichloroethene U 0.14 U 0.14 U 0.16 l / U

0.13 •\ u 0^15 1,1-Dichloroethane U 0.14 / U 0.14 u 0.16 V u 0.13 * u 0.15 . cis-1,2-Dichloroethene y u 0.14 / U 0.14 I) 0.16 u 0.13 • u 0.15 1,1,1-Trichloroethane \ i u 0.14 t 1 1'1 0.14 0.16 • 0.82 0.13 • 3.3 0.15 Trichloroethene V u 0.14 y 0 0.14 V u 0.16 r U 0.13 ; 0.66 0.15 Tetrachloroethene 57 0.14 ; 3 3 0.14 2.0 0.16 : 1 6 0.13 ' 5.0 0.15

0284-DAR-082509 7

1 Method TO-15 (SIM)


Table 1.1b (cont) Results of the Analysis for VOC (pg/m3) in Air WA # 284 White Swan Laundry & Cleaners/Sun Cleaners Area Vapor Intrusion Study

Page 3 of 3

284-214 Unit 112 SS-112

7/21/2009 Method-Blank

Analyte

'Result pg/m3

RL pg/m3

Result pg/m3

RL pg/m3

Vinyl Chloride U 0.15 U 0.10 1,1-Dichloroethene U 0.15 U 0.10 trans-1,2-Dichloroethene / U 0.15 U 0.10 1,1-Dichloroethane / U 0.15 U 0.10 cis-1,2-Dichloroethene / U 0.15 U 0.10 1,1,1-Trichloroethane / 0.16 0.15 U 0.10 Trichloroethene \ ) u 0.15 u 0.10 Tetrachloroethene 21 0.15 u 0.10

0284-DAR-082509 8

Table 2.1 Results of the LCS Analysis for VOC in Air WA # 284 White Swan Laundry & Cleaners/Sun Cleaners Area Vapor Intrusion Study

Page 1 of 1

Date Analyzed 07/14/09

LCS LCS Spike Recovered QC Limits

Analyte ng ng % Recovery % Recovery

Vinyl Chloride 25.5 25.8 101 57-132 1,1-Dichloroethene 27.5 28.7 . 104 70-123 trans-1,2-Dichloroethene 26.8 29.2 109 69-125 1,1-Dichloroethane 26.8 29.0 108 72-130 cis-1,2-Dichloroethene 27.5 29.5 107 69-124 1,1,1-Trichloroethane 26.5 27.1 102 69-127 Trichloroethene 26.5 26.6 100 72-122 Tetrachloroethene 25.8 26.2 102 72-125



Analyte ng ng % Recovery % Recover

Vinyl Chloride 25.5 26.6 104 57-132 1,1-Dichloroethene 27.5 28.7 104 70-123 trans-1,2-Dichloroethene 26.8 29.6 110 69-125 1,1-Dichloroethane 26.8 29.2 109 72-130 cis-1,2-Dichloroethene 27.5 29.5 107 69-124 1,1,1-Trichloroethane 26.5 27.5 104 69-127 Trichloroethene 26.5 27.2 103 72-122 Tetrachloroethene 25.8 26.3 102 72-125


LCS Spike

Analyte ng

Vinyl Chloride 25.5 1,1-Dichloroethene 27.5 trans-1,2-Dichloroethene 26.8 1,1-Dichloroethane 26.8 cis-1,2-Dichloroethene 27.5 1,1,1-Trichloroethane 26.5 Trichloroethene 26.5 Tetrachloroethene 25.8

LCS Recovered QC Limits

ng % Recovery % Recovery

23.9 94 57-132 27.0 98 70-123 27.5 103 69-125 27.4 102 72-130 27.6 100 69-124 25.5 96 69-127 25.3 95 72-122 26.3 104 72-125



Analyte ng ng % Recovery % Recover

Vinyl Chloride 25.5 23.9 94 57-132 1,1-Dichloroethene 27.5 27.0 98 70-123 trans-1,2-Dichloroethene 26.8 27.4 102 69-125 1,1-Dichloroethane 26.8 27.2 101 72-130 cis-1,2-Dichloroethene 27.5 27.6 100 69-124 1,1,1-Trichloroethane 26.5 25.4 96 69-127 Trichloroethene 26.5 25.2 95 72-122 Tetrachloroethene 25.8 25.7 100 72-125

0284-DAR-082509 9

Table 2.2 Results of the Duplicate Analysis for VOC in Air WA # 284 White Swan Laundry & Cleaners/Sun Cleaners Area Vapor Intrusion Study

Page 1 of 1 Sample Number 284-189

Analyte Initial Analysis

ppbv Duplicate Analysis

ppbv RPD QC Limits

RPDS

Vinyl Chloride U U NC 25 1,1-Dichloroethene U U NC 25 trans-1,2-Dichloroethene U U NC 25 1,1-Dichloroethane U U NC 25 cis-1,2-Dichloroethene u U NC 25 1,1,1-Trichloroethane u U NC 25 Trichloroethene u u NC 25 Tetrachloroethene 0.0472 0.0458 3 25

Sampler Number 284-199

Analyte Initial Analysis

ppbv Duplicate Analysis

ppbv RPD QC Limits

RPDS

Vinyl Chloride U U NC 25 1,1-Dichloroethene U U NC 25 trans-1,2-Dichloroethene U U NC 25 1,1-Dichloroethane U U NC 25 cis-1,2-Dichloroethene U U NC 25 1,1,1-Trichloroethane 0.0994 0.109 9 25 Trichloroethene 0.0522 0.0568 8 25 Tetrachloroethene 44.9 45.6 2 ' - 25

0284-DAR-082509 10

Lockheed Martin Response Engineering Analytical Contract 2890 WoodbrMgc Avenue Building 209 Annex Edison, NJ 08837-3679 Telephone 732-321-4200 Facsimile 73M94-4021 LOCKHBED MARTIN

Columbia Analytical Services 2655 Park Center Dr. Suite A Simi Valley, CA 93065

Attn: Kelly Horiuchi . June 30,2009

As per Lockheed Martin / REAC Value Contract 46032343 or Project 0-284, please analyze samples according to the following parameters:

Analysis/Method Matrix #of samples

VOA/TO-15 (0.070 ppbv) See attached compound list Summa 30.

Data package: Package with Diskette Deliverable

Samples are expected to arrive at your laboratory on July10, 2009. All applicableQA/QC(eg: BS/BSD, LCS, Duplicates, and BlanKs) analysis as per method, will be performed on our sample matrix. Preliminary sample and QC result tables plus a signed copy of our Chain of Custody must be sent to BEi51lOJ^jnes.5.days after receipt of samples. The complete data package is due 15 business days after receipt of the samples. The complete data package must include all items on the deliverables checklist. The laboratory must provide documentation for individual summa canister and flow controller certification.

AH sample and QC results must be summarized in a tab delimited file diskette deliverable. Units must be in ppbv and ug/m3 in the electronic deliverable.

The summa canisters and preset orifices must arrive at REAC by July 6, 2009.

Please submit all reports concerning this project to John Johnson at (732) 321-4248 or [email protected]. Any contractual question, please call Joe Rosenberger (732) 321-4215.

Vinod Kansal Analytical Section Leader Lockheed Martin / REAC Project

VK:lm Attachments

cc. R. Singhvi V Kansal J. Rosenberger R. Connell Subcontracting File S. Thompson 0284\non\mem\0906\sub\0284Con5 J. Soroka

0284-DAR-082509 011

TO-15 Compound List for Project 0284 Vinyl Chloride 1,1-Dichloroethene (1,1-DCE) trans-1,2-Dichloroethene 1,1-Dichloroethane (1,1-DCA) cis-1,2-Dichloroethene 1,1,1 -Trichloroethane (TCA) Tetrachloroethene (PCE) Trichloroethene

* After normal dilution rate of 1-2x

Reporting Limit (ppbv) 0.070 0.070 0.070 0.070 0 070 0.070 0.070 0.070

0284-DAR-082509 012

o ro CO *. i

O > * o

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Lockheed Martin, Inc.

REAC, Edison, NJ

EPA Contract Number: EP-C-04-032

CHAIN OF CUSTODY RECORD

Site #: 0-284

Contact Name: John Johnson

Contact Phone; 732-321-4248

No: 0-284-07/10/09-0034

Lab: Columbia Analytical Services

Lab Contact: 2655 Park Center Drive

Special Instructions: TO-15 SIM 3® ŜAMPLES TRANSFERRED FROM | CHAIN OF CUSTODY iT

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REAC, Edison, NJ



Site #: 0-284


Contact Phone: 732-321-

N o : 0-284-07/10/03-0035

Lab: Columbia Analytical Service's


Lab#

tV.

Sample # ( Location

284-191 ]~Unii 093

284-192 ' Unit 094 i

284093 ~) Unit 095

284-194" ' ! Un¥696

Sub Location

SS-093

Matrix

Air

SS-094

SS^095 "~

SS-096pr

( Collected

i _ T7/8/2009

j 7/8/2009

T/8/2009

7/3/20C9

Container

SUMMA CANISTER

SUMMA CANISTER

SUMMA CANISTER

Pump # OrificelD Start ] Stop Pressure • Pressure ;

AC00782

AC007?a

; AC00705 j

i AC01011

| FC00194

; FC00514

"iFcooeos | ' FC00148

-3o;

-30 :

-30l

•30 j

-8 ! —n

Special Instructions: TO-15 SIM SAMPLES TRANSFERRED FROM CHAIN OF CUSTODY #

Items/Reason

:\y:'Jx>:...\

Received by Dale Time | Items/Reason Relinquished By I Dale Received by Date Time

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REAC. Edison, NJ



Site ff: 0-284


Contact Phone: 732-321-4248

No: 0-284-07/10/09-0036



j Lab #

©

0

Sample #

284~195

28TV96 "

284-197

28T l98"

Location T s u b Location

Unit 096

Unit'097

Unit 098

Unit~698

SS-096P2

SS-097

IA-098

AMB-098

Matrix

Air

Air

Air~

Air"

Collected

7/8/2009™

7/8/2009

7/8/2009"""

Container

7/8/2009

SUMMA CANISTER

SUMMA' ' - ' CANISTER

STJMMA CANISTER

SUMMA CANISTER

Pump #

AC01537

AC01527

| AC00919

AC01113

OrificelD

FC00598"

FC00163

FC00204''

FC00259"

j Start j Pressure

[ -30

""-30"

~~~ " - 3 0

J .

i Special Instructions: TO-15 SIM

Stop Pressure j

' " -10] _ i . . .. _s-

-9.5

._ _._

-w 1

< O

[SAMPLES TRANSFERRED FROM CHAIN OF CUSTODY #

Items/Reason Relinquished by I Date

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REAC, Edison, NJ



Site #:.0-284



No: 0-284-07/10/09-0037



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REAC. Edison, NJ



Site #: 0-284



No: 0,284-07/10/09-0038

Lab: Columbia Analytical Services Lab Contact: 2655 Park Center Drive

Start | Stop j Pressure | Pressure

-3

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REAC, Edison, NJ



Site #:• 0-284



No: 0-284-07/10/09-0039


Lab Contact: 2(555 Park Center Drive

L a b # S a m p l e # L o c a t i o n S u b L o c a t i o n Matr ix

£) 284-207 Unit 105 AMB-105 Air

& 284-208 Unit 106 SS-106 Air

284-209 Unit 107

S S - 1 0 7 ~ " Air

284-210 Unit 1 0 8 " " ss-i¥ Air

— I

' \ " —~

' .

" — - "

Co l lec ted Con ta ine r i P u m p #

7/8/2009 SUMMA j AC00667 CANISTER

] 7/8/2009 SUMMA | AC00486 CANISTER

7 , i /2009 "" SUMMA ; AC0G871 CANISTER t

7/6V2009~ SUMMA [ AC01257

OrificelD

FC0C110

?C00516 I !FC00539

FC00509

Start Pressure

-30

Stop I Pressure

-6.5 I

-30 ! -7 !

Special Instructions: TO-15 SIM

Items/Reason

SAMPLES TRANSFERRED FROM

CHAIN OF CUSTODY #

'/Sr. f ^ 1

elinquished by | Date Received by Date Time 1 I items/Reason Relinquished By I Date Received by Date Time

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ANALYTICAL REPORT FOR WHITE SWAN LAUNDRY AND ...284-190 Unit 092 SS-092P2 284-191 Unit 093 SS-093...

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