e CDM ~ ~ SCrel!l&t/3. ~ & msM~ ~

August 11, 1986

Mr. John Cochnm U.S. Environmental Protection Agency First International Suilding 1201 Elm Street Dallas, TX 7S270

IE& CLP Data at Koppers/Texarkana Site

Ooc. Ctrl. No.: 142-TSl-EP-DCPN-1

Dear John:

CAMP DRESSER & McKEE INC.

9U2 CaOilal Of Texas ~ay !-lotll'I A.ll)Qr8'Cm Plaza rwo, Sule 400 Au9llr'I. Texas 78759 s,2 3"5-6861

Per your request ( letter dated July 22, 1986), I am sending a copy of the analytical results from split samples at the Koppers/I'exarkana Site.

TWo of the CLP samples (CLP IMFC214 and iMf'C216) sent to Cambridge Analytical are still in the system. We are awaiting the results.

An extra copy of the data are included for transmission to Koppers. If you have any questions, do not hesitate to contact me.

Sincerely,

~X--ll Yl/curf'-i> --. .,,,, , / "Cv ~ . . I I

(

S. Lynn Mays Site Manager

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(Page 1 J

• •':ioritOl'y Na-ne ~OUTHWE.fil lf..BORATORY OF' OKLA.

..... b S1 "l"lple 10 No ---~--_c._· _7_7-_____ _ C1uNo

QC Report No SI~ t.e.t,11. ~q_._f ____ _ Contr1:1 No §_8-01~7168/JA 68-01-7168/2~­01u Jt..luu Aut~orized By ¼J!YeOt S_hri nr:,arpure Date Sample Reeeived '2.- '2-/ - ~ 6

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c1-11o•ome1"•"e

: Volatile Compounds ,/"7--... Concentr111ori . ...__..,o~· Medium (C1tele One}

Date E1e1r1c1td /Prepared

Date .4.nalV?ed

Cone 10,1 Factor __ ~ ___ pH __ :t..i-....·9 .... , __

Percent Moisture {No1 Dec11nted) _____ l_8--... __ _

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CAS Number ,a e1.s

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laborinory Name SOUTHWEST , 9no~Y OF OKLA. s-c;{-/_ Cue No

Sample Number

Contract N 68-01~7168/~A 68•0blJiWil~ Analysis Data Sheet (Page 2)

Fe. 807

Semivolatile Compounds

Date AN tvz,ed

Cone/0,t Factor I Percent Moisture (Oecanted) ___ /_f?.._ ___ _

CAS NumMr 108-95-2 ,1,.44.4

95-57-8 541.73.1

106-46-7 100-51-6 95.50., 95-48-' ~

"38-32-9 4..4-S

-6A-7 .. 67-72-1 98-95-3 78-59•1 es-n.s 105-67-9 65-85-0 . ---

111,91-1 -

t20·83·2 120-82·1 91-20-3 106•41-B

e::.6s-3 59-S0-7 91.57.g

'147◄ 99.1'.)6.J 95.95., 9_1-58-? es.,, .• 131-U,3

"·96-B .. .J9,2

P1'enol

b•t' -2· Cl'\lo,oe1"iv1JE 11'\er 2•Chlorop"ienol

1 3-0,cn!orob!-ite"e

1 4•Drchlo,ob!l'ltf'"lf'

Be~tvl A.lcotiol , 2-0ichlorobenzpne

2-Me•"v'p"'e:1101 ..

b1S(2 •Cl-iloro1sop•opvl)E U,tr

4-Metl)vlp"'leno

N. N11roso-D••n-P1opvl&rT11ne

Mu.11ct-iI0,oeIhane

NrHobef\.te'"lf'

lsoo"iorone

2 -N1trop"ie nol

2 4-0ime!hylphtnol

Bentoic Acid

b,s, · 2 •Chloroe1holvlMe11-i11 rie 2 4-0u:t-ilorop,.,enol . 1. 2. 4-Trichlorobel"izene

.. ---

Naphrha le tie

4 ,C'1I0roan1hne

He11.achl~robu111~1e l'lt

4-Ctiloro-3 •Me_thylphel'lo1

2•Me1hrln•phIh1te11_e

Hell&chloroevclo~r11ad1ene

2. A. 6•Tr1chloroi,hen0I

2 . •. S-Tuchlorophef'IOI

2,Chlorott1phthale_iie

2-~11,oar11hn-e

O,methvl "'~1ha111e . -

Acenaphthvl•".le

3•N•ttoanihne

ug110~ (Ci,~

330 U 330 U 111'1 II 33_0 U 1':W " 330 U .. 330_U 330 U 330 11 330 U 110 II

3~0 II

-- 330 U_ 330 U 330 U 330 U

u;no 11

330 U ~-!JU U

330 U 330 U 11n II j:lfl II 330 U 330 U 330 U 3;m u

1600 II 3~0 ll --

H,nn II ~-:in ti

_ 330 U , ,:;nn 11

GPC Cleanup 0Yes ~No

Separatorv Funnel Exuae1iori OYes

Continuous L1Quid • LiQuid Eic1rac1,on OYes

CAS Numtar

83-32·9 51-28-S 100-02., 132-64 9 121.14.2

606-20-2 8--4 ·66-2 7005-72•3 86-?J., 100.01 ·6 534-52-1

86-30·6 101.55.3 118-?4-t

87•86·5

85-01-8 120-12-7 64.74.2 206,44-0 129-00-0 BS-68-7 91-94• 1 56-55-3 ,,,.e1.1

121 B-01-9 117,84-0 205.99.2 20?,08-9 )0·32-8 193.39.5, 53-10-3 19t2•-2

---AcMap"lt,-.ene

2. ••D1n1trophenol

4-Nitropheriol

D1be"llOfuran

2 il-01n1tro1oruene

2 6•01nitro1oluene

Diet hylpht ha la le

4-Ct-,loropl-ienvt-pt-ief'l}'.lf!tt-ier

Fluorene

4-Nittoanil,ne

4. 6-_0m1tr0·2·Metliylplienof

N-N ,troSodJt>l-ienvra~ine fl I 4 •8rornop"ienv)•Pl-ienvlett-ie~

~ellachlorobenre,,e

Pentac'1 lor opl-i ertol

Phen1,'11hrene

Anthr•cene

01-n-Bu~yJp1·oh111111e

Fluor•nthene

Pyrenl!!

Butylb,e r\tylphtha late

3. 3 ·.01chlorobenz1d1r11!

DenzO(&fAnthraeene

b~Sl2:Ethylhoyl)Phtti_atate

Chrvae~ 01,n,(xtyl Phthol1te

Sento(b)Fluorant~~

Bento(k~ I uorat1tl'IG1ie Ber,_rO(•)Pvrel'\O lndenoc,. 2. 3--cd_~•~ 01bel'lt!i hJAnt~r•e•~ Benra1.o h. ilPervlen~

(\J

0 Ug 110~ f'-­

(C1tc~

:-no n 1600 U 1 f.(\O II 330 U 330 U :lJO l/ 330 U JjU U

330 ll 1600 U lbUU U ·nn 11

1~n II 330_U

1600 U 330 U 310 II 330 U 330 U

330 II 330 U 6~0 U ':l.'V1 II

~nn 11 330 U 330 U 330 II ..

330 11 330 U 3~n II ~'.tn II 330 II

7:85

r-e 0

La~o• •tof~ ,._,.,,.,t . SOUTHWEST .AJORY Of ,ill'J,AHOM~ t;: ~ t (

Cut ~o --------------~--Contract t 68·01-7168/lA or 2AO • A , · 0 t Sh t - rgan,cs na v11s I a ee

(Page 3}

Pt1ticidelPCBs

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Co--,ief"Tt"•:,o.., Low Mtd,ut'tl (C,,cle Onet ~ GPC Clunup C)'r'est'JNo

St"n"le "-u: F\t,er r~ r ( - V (- ~I

Datt [xtractt-d 'Prt;,ared ')- .2... { ~ -~ ( Datt A.l'\ITyzt-d ____ --i.__-_~..,-.......... -_~..;,:..--..;:{ ___ _

' ~I~ .--c

Se;,s,a,1orv Fu~nt1 Ertr,et,on :,,vu Continuous liQuid. LiQvid Er1rac1,on 0Yes

CAS Nul'l'lber

3, 9 84-6

319 85-? 3'1~•86-B

i$8 89·9 16-4.4-8 )09 00-2 1024,57-3 ig59 98·8 60-51-1

12-55-9

72·20·8 332\3-E:5 9 '2·S4·8 l031-07-S !)0 29 3 72-43-S

Sl49-'·'0-!i S. ,. "14-9 8Xll -35 2 12674-11•2 \ U04-28 2 111'1-16 5 ~3469-2\-9 '2Ei72·29-6 1109'1-69-1 1109682,!

--

Alp"ia sMr 6flll 8'"4(

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1-itt)lJCl\ior

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D,era,,n

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E"'dCS.i•f,t"I II

4. • -000 fl'ldosul!a" S.Jiia,~,

4 4 -DOT Metho•vc..,lo• E nd•,ri 11'.e'.o"le

Ci-tr,... csa rir Toup..,erie A•oclot-1016

A•octo••l221

A1oclot-1ll2 A1oclot• 12'2 A10tlot.1248

Aroclor,1254 A,oc10,,t260

--·-

·-

ug'fo~ CC•tc~

R n IJ 8.0 U R n II 8 O 11 a.o u _8 n II 6.0 U 8.0 U

16.0 U 16.0 U 16.0 \J

_ 16.0 U 16.0 U lf; 0 H

16.0 U 80.0 U 16.0 U 80.0 U

lliO n II 80.0 U 80.0 U HO,O U 80.0 U 80.0 U

160.0 U 160.0 u

V1 • vorume of t1tttaet u,Je~ted (ut)

v, • Voluf'ht or w11e1 t11ree1ed (ml)

W0 • Wt•ghl of iU"'plt eatracttd (g1

Vt ,. Vofumt of 101a1 t1trat1 (ult

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t..eboratorv Name SOUTHWEST LABr._or OKLA. CueNo S-~ I _

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Organics Anatysis Data Sheet (Page 4)

tentatively Identified Compounds

N....,..._ Compound N•rrHt Fraction

t.+c.J- 7C ·· 1 Ace he C,1___{_.A. J "h-1€ -f/4,., /es 1-<v Gtv1i -2. .-- (,<,..J<._ YL(J""t.Vi.L__ t.

J. - r~ vt k. 'vtou__ '11.. 1-1.8 ,.J 'J,--c < &<. v Lerv1 t,

,_q·3c .. (g .. :,- '2 - C 'i C ( b j, (! ',£ ( ">1 - I o---n a.... 1'1

g_ ,..- Uh k 'n c, I) . .! 11 Ji~~,,./.-,--;; r __,., 'k, ('-'IA LI

6. 0 ..

7.

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9. ,o. 11.

12. . 13 ,

15.

16 ,,. . ..

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20. ---

21.

22. --

23

24. --

25. ---

28 27.

28. ---

21. -30. - -- -

form 1. f'art D

-:r..

Sample Number

F=C. t?bl-

11:T CH Scan f•tim1t&d Numbttt Conc•ntr1tiD"

fug If or~'~!,

4tr;, 3~/';; f~ /

$77 CJ¥-!<. - - I ' C/6 4-0i1 C. 3'1-- /& J '(t)

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@·_SAMPLE CONCENTRATION-___ . . " - (Checl: One) · .

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@ -~MATRIX_-(Check One)

_..:.__ Water · ~ Soil/Sediment

_, ~Number

-J!.C868 _:~

@ Ship To: . ·: .. _ _ _ _ _5r:,..1••r11~>7"~rJ Lal~~-ld ~ 1u92t, f. :S5,J. Pl.

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1==::.::::=:;:;====..::.:::.:==~============~~-·:~-=====::::::=::;::::===========:::.:::;: ® Regional Office: \L 1• @ For ea.ch sample collecied specify number @ Anal Sampling Personnel: of containers used and mark volume level Rec'd by: .Joo<:J~-1-----,--

on each bottle. Date Rec'd: _,_.Jc.-/ __

,,- 12) (Phone)

Sampling Date: -, I- I.,;_(. --.;; L - I -!

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( "hipping Information

"f'~ ,.,.. l- ,,,_ - ·. r .~ I ,. x 6 1 • ..:. - r .

Name of Carrier

Date Shipped:

Airbill Number:

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(Extractable)

Water (VOA)

Boll/Sadiment ~a.ota.ble)

Boll/Sediment ~)

Other

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I I

I

Sample Condition on Receipt (e.g., brol:.en, no ice, Chain-of.Custody, etc.)

ND

. @ Sample Location

~1mple Num~

Organic, Anafyai, Data Sheet · (Page 1)

r=-c ~ (e J 'be;;,(~

• -~ritory Na~e SOUTHWEST LABORATORY OF OKLA.

L..0 Sa~le 10 No __ ?-i_, ..... r-.... - -_? ..... (..__-. _____ _ OC Report No _____ r ________ _

Sa~ Matri1. ____ Sr _____ ._;_f _____ _ Con1r1et No 68~01-:7l68!1A 68-0l-7168L2h_

01t1 f!WNu A.uthorired By Jax:ant Shri n.3e,r0;ure Uate Sample Received 2.- 2 )- b c~

,,.e,.3 74.93.9 1$-01-4

7S-00-3 -. ~-2 64-1 ~ 5-0

S-35-4 ,s-34-3 156-60-S

67-66-3 -107-06,2-

78-93·3 '11.55.g

!,6 2J-!, 108-05-4 ?S-21-4 -

Volatile Compounds.

Concentr11ion. e Medium (Circle One)

Date h1r1etedlPrep1red --Date Analyzed

Cone/Oil F•e1or _ u s;s-------"" -------

Percent Moisture (Nol Decentedl---2._c;-_· __ _

..,g 1fo~ CAS (Ci~~ Numbti,

Chloro,,.,e!"itl'le 10 U 76-8?-S 1 2 · 0•c: ,.,,o,op•op;, ... ,

e,o,,.,omet"arie 10 U 10061-02-6 Tta"ls 1 3-01C:l'llorop•ope"'le

V1nv1 Chlo••~ 10 U ?9-01 -6 Tr,clllOrMthf"'lf'

Chloroefl\81'\£' 10 U 124-48- 1 b 1br O'f'IOC hlo1 ome1h11 "le

Mt!"iyle"lf Ct\lOrtde 5 U '19,CXH, 1 1. 2-Trichloroetl-\ant

Ace,ol'le 10 II 71-•3-2 Bel'ltene

Ct•bon 0,1 ulr1de 5 II 1oos, .o, .s c,,.,. 3•01chlo•Jo1oc,ef'le

1.1-01tl\lori>rt'1trte t; l I 110-75-8 2-ChlO•Olthvlv•:"lvlethe,

1. 1-0,el'llo•oet"'•"" 5 U 75-25-2 81ornoform

Tr•l'ls• 1. 2•01el'\Jor~thel'lt 5 U 591-78,6 4-Me,"'vl-2-Pe"'lt&l'IO'lf

C/'\foroform 5 II 108 10-1 2•Mhll1'10t\f

, ' 2-011:hfo1oethll'II!' 5 U 127-16-4 T ~tr ae'11o•oet"e-"e

2•Bu1enol'le 10 U '19-34-S 1. 1. 2 2-Tetrac"ilorM-t"il"lf

1. t. I •Tr.c"iloroet'18rtt 5 U 108-86-3 To!uerit

Carbot-i Tttttc:Moride 5 U 108-90 7 C~loro~nie-nt

V,n~I Ac:elltt 10 U 100-41 ., ftl'lvl~n.z•"' -8 •o'T'IOd1el-\lo1omtthal'le 5 lJ 100-41-5 Stvrent

Total_X\·lef'll!'S

011a C!:t;i,o,,•"9 (wtlrf,_,t

eo, 1Spol'l1flt ._,11111 to £11.l t1't fe/lew,'IQ ,a~~IU ,.,11rf,e11 ••• l!lltO Adid•hOP\AI fllQl O• fOOl"iO!illl t!ll)la,1\11\Q 1fl111t, 11t O~o1,1<IQd tco-,..., tl'llt -,.i,1\11 IO".,,, ••th fl.I; ft'll,/Sl tal ♦J,lifJCr1

5 U 5 U 5 U 5 II 5 U 5 U 5 U

10 U 5 II

IO IJ 10 U 5 U 5 U 5 IJ 5 U 5 IJ 5 U 5 ll

W.. • .._ IW""1 11 a nl..it t•Ult• ffli" .. t,alJotl kl tf'lt CMlffllOl'l ""°'11 C . ..f'l'O" ttif 119 li,t

II Wc.,iaa lO""OOu"CI lltU tf\tlr1td fo, t>111 f'oill Stlttli,d .. flOII '"'

, ........ 91)"'31 ... IOMlhtodt N••-11•• ~·· , ... -,.111,l,u1,o· ..... h•" 1:0111,t~II bi GC MS &•"Sit to"I\Jl(l"'"t flfat,r•l5f'i? 1.:-,

fl& "' tf\ tilt'''"' lllfttl ~ .. COl\ft<~ 1h GC MS

.. ""l'l""'*ifC111l-" ltft\f1 lot ftlt M~ t1w•l"ti'lt Ult I 10UltMIM-d I

.,. ftkfflt•y u•1coi.110,...,, •frl,,11,0,,Kt,o,,, tfti,a II flOI A1ttt111•1lr tht ..... U-,lnO"I .. lftl,of'I "'11\,t t fhf ftot"411 Or-..wl!S ~ IJ· ~i.1'Wl' '"' 1..-1rteel',.....,. f'4I •umffl ,,_ ~• 11111V WMIMt!'lllfri llma•tiat>li *•ttuen MM ... ette- il1T'$11 Othef

Wotllel t" IH!l•~lef •1118 l'h!fi ..... 1,11!1H -~ _,,.., \)A1111'8l""t I ~l'ltrll_,. fcl ltf\181~~ lleA!lf$lll ~ _.., 8 I I ..... 'llf' • iH..,..,.,.. 0, llf!iai't lflit ffllllt e,,et11al e,i. W<atlCI tll.t .,,wi,ct ,J t Uf'l)9Y"4! ti\li ""411 ttw _,.._.ifotet11 t,t.111-' w thf t♦tuts e Ith""" 11'11 ~,tllfd litte~.-i WM 1k!! .,., .. , lf\4lfl ..,. ,rt . 1a.r, ff Wi'lfl tf lillllCI~ • tO 6Jit I e,\f t OtftU· '.Ufllot'I., I YI ., • Ultwblttl. ~ti..,

tn11 fllQ •• uUCI ....,,., ,,_ ~ • fo-.1'\d ""11'11 l>I•._. u ...,.1." 1

N"l/,)lt fl ltd•CIIH S>ot\llblit f1Wl>lt ftlll\i COfllol'"''"'''t'~ 10\d

.-,,u Nit Ill• IIM• ID'"'' _,..ltlt att•

Ot --""' 5oeclf1t ti.ea •~•-~u IVl.il)"" '"""'"° u, "'°""'' h .-, . ..,. tht tH!itll ff UINI , ... , °"11111 Ol:r 111111 ft1< ••Cle "Cl lllf" °""'!Och0" $(1.ttl'ltf:I Ml~ 8'111 ~li"Wlt- raipot1

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L1boratorv Narne SOUTHWEST Lr -ORY or OKLA. CISt No _______ 5'.........,SZ::_--_/. _______ _ Sample Numbet

Fe &,~ Contract# 68-01~7168/lA 68-0b'J~At?A tg!Me, Anervais Data Sheet

(Page 2}

Semivofatile Compound,

Col'\Cef'itrlff()h. ~ 0a1e Eirtracttd 'Prepared

Date ANtvled

Cor,t/O11 Factor

Medium (Circle One} '2. p 1.$- 8 k

I Percent Mo,stute (Oec:anted) ___ '"'2...._$.,. ___ -__ _

CAS Numbtt

108 95-2 111-44-4

95-57-8

541-73'. 1

10ti-46-7 100-51•6

95-50-1

95-48-7 ..... 8-32-9

'""" 10£-44-S 621-64-7 67.72., 98 9S-3 ,a 59., 88-?S-5 105-67•9

65_-es-o 111-91-1

120-83·2 120-8..2-1 91-20-3 106-47•8

8'?-68-3 59-50-7 91•5?-ts .,, ... , ... 86·06·2 IS-95•4 91-51-7 88 , •.• ,,,.11.3

' ~6-8 .. 9!:t·u9·2

..

Pl'\el"lol 330 U b•s1 -2-C"iloroet,-.,\IIJE ther 330 U 2-Ct:iloroptienol ~no u 1 3-0,chloroMf'l?f'l"le 330 U 1 ~-01cMo,ooo"tt'le ~no u Be rirvl Atco"o' 330 U 1 2-0,cliloroberite"lt 330 U 2 -Me1,-..vlp"ierio1 330 U . .

b•sl2•thloro1soo•opvllEtlitr 330 U 4-Mtt"lyfpheno 330 U N- N1troso•01•n-Propvfal'l'line ~1ft II Me dctiloroethll ne 1-".!.n II NrftObel"ill! 'if- 330 U lsop"iorone 330 U 2-N 1tt9_p!-ieno1 3J0 U 2 •·O,rne1hvlc,tienol 330 U 13tnto•c A.c1d lfinrl U b1s1 · 2-CM0,oetho1v1M,1"iane 330 U_ 2 41-0,tlilorop!-ienol 3JO U 1. 2. 4-Trielilorobel'lzene 330 U Naoll1h11ene 330 U 4 ·C"loro.an,hne ':l~n II

He• •c l'\lorobut•d•t ne_ ~:l.O ti •-Chloro,3-Methylpheriol 330 U 2-Methyln•ohth1lent 330 U He111chloroevcloprntad,ene 330 U 2. •· 6· Tuchloroo,henol JJO U 1 . .t. 6-Tt,chloroph~nol t,:;nn _11 2 •Ch_lorol'l&il)hth• ftt\f S:l.n ll 2 •N ,t ,ca "•hfW!t 11.nn 11 D•rntthvl ,hthelat• 330 II Ac tntr,hthvfol\~ 330 U _3•N11toanihnt 1,mn 11

GPC Cleanup OYes t!No

Separatorv funnel E~r•~iori CJV~s

Continuous LiQuid • liQurd E.:tract,ol"I OVes

CAS Numbtlr

83-32-9 51-28-5 t 00-02-7 1.32-64 g 121-14-2

606-20-2

iSA-66-2 ?005-?2-J 86_-13.1 100-01-6

534-52-1 86-30•6 101-55-3 118-74-1 87-86-5 85-01 ·B 120-12•? 84-74•2 296-44•0 129-00·0 85-68-? 91 •94-1 5,6-55-3 11,.s,.1

-

~18-01-9 111-84-0 205-99-2 207•08-9 :,0-32-8 ,93.39.5

·;:v,o-:i , 9t •24-2

ug 11o~ {Ci;~~

Ace: riap'ittient- ~30 II ~

2. 4-Dirutroptienol 1600 lJ 4-N,uoplitl'lOI l finn t1 D,bentofvr•n 330 U 2 4-01n1trotolue"e 330 U --

2 5-0,nitrb10fue"t 310 U D1elhyfplith•late 330 U 4-Chloroplieriyl-e>"iflriyle,.,er 330 U Fluor,ni! 330_ IJ 4-N•troa,.,il,ne 1600 U 4. 6-01l'11tro•2-Met.,v!c,tiel'lol 16UU U N-N1tro1od,p"ienyl&rn1f'lt! ft I ~1n IL 4 · 9ro,noplienyf .pht_riylethl'r -~30 I! Noa thlor obenze "e 330 U Pentaeliloroc,"e"o' 1600 U Ph1H'llr"ltlirtt'le 330 U Arithr■cent 11n 11 O,,n-8u1vlp'111-iara1P 330 U Fluoral'lthel'I~ _330 U __ Pyrene 1::ln II B utvlbel'l.tyll)l,f "·III e 330 11 3 3 ·•Oicl'llorobtl'IJ1d1rie 690 V Bef'IJO(IJAruh,acen• .'l1n If r:,,~2-E11tvlhe11vllPhttill8!('

. - 130 ti c,,,vuiit 330 U o,.n-Ocrv1 Phthtltre 330 U Ben1o(b)fluor&nt~l'l,f 130 II Bento(klf luDrlMhtl'lf 330 IJ 8tl\Joiai,Pvr•l'lrl 330 U lndtno(1. 2, l-cd~tllt ~1tl II 01t>.ni11 h~nthraeel'le 11n II Btl'llola h, ilJ'&ryl#,__ ~10 II

r---­c­r-­r-0 0

l•bo,11or)' t-.a""'t SOUJHh'EST leATORY ,,Or QKr AHOMA (9 5=.\{ l Cut "-o ----~-..2....i;....,.._..._ ... _ ------

Contract I 68~0l .. 716S/lA or 2Aorganic• Anafy1is Date Sheet

.J._

(

(Page 3J

Pesticide IPCBs l

Mtd•ul'fl (C,rcfe One)' low GPC Clea l"ILJP OYea JSNo

Otte £.a:v4cte-d 'P,epared - 2 - 9 - & l 0 "! .-_ 'L. - ,.. l:

111 AP\1 1yr~J ------..J------~------C.0"1c ro;rF•ctot 2 h,$ 1 'l

St;ia,atorv F' U!-11'\tl E11r•ct1on;QVe!>

Contin..ious LiQuid • Liqu•d £r1rac1,ori OVes

Pe·cent Mort!urt! (dec111'ted) .,.__ ....... 2 ....... ~ ___ . _c __ _

v, -------

.3,9 86 6 Alt)"iil 81•1(

Jl9 es., 6etll &1o1C 1319-Bt·B Ot•:, e~c 56 89 9 Ga..-.~,a 8"4C IL•ndb">!l

t?E-4.4-8 Hrp\lJChlor

~09 00-2 Alc,,,n

1024-S'·J Mtotll :"'10, £poK ,de 1959 98·8 £"-dos..ilf11n I

·-

~' S?-1 O,eld••l'I

172-SS-9 4 4 -ODE f72•20·8 El'ldril'I

332t3-tS 9 Er.dcS..itf1" II

12-$4-8 ,. • .poo ,03, •07•8 £"dos.il<a" S"'Ha~t 50 29 3 4 • -ODT '2-43-S M,,,-,o•vct-.lo• SJ49t-70-5 E~d•11'\ kt'.O"t

!,'1,74 9 Ct-ilorda..,t

8,01-35 2 T ou p"'e "e -·

12674-11-2 A•c,clor-1016 '110,4-282 A1oc10•-t221 11141,165 A•ocio,-12J2 53469 2,_.9 Aroclor•U•2 12672'-29·6 Aroclo•• 1248 l 109'7,69-1 A•oc lor-1254

1 \096 82-5 Aroclo•· 1260

ug'lo~ fC1rt~

fi nu 8.0 U R n u 8.0 11 8.0 U A n 11 8.0 U 8.0 U

16.0 U 16.0 U 16.0 lJ 16.0 U J6.0 U 16 0 1t 16.0 II 80.0 U 16 0 Ir 80.0 U

H,n O II BP.0 U 80.0 U ou.u u 80.0 U 80.0 U

lbu.o U 160. 0 U_

V1 8 Volu,ne of ,st,1c1 11\j•cu-d (u1)

\11 • Volumt of Wlttt e1tr1e1td Cl'l'lfl

W" • We1.ah1 of IO'nplt t1tr.e11d (gt

v, • Voh,tnt of toltl t1ttlC'I h.ilt

a: 0 r----1"'--'

0 0

Lebora1ory Na -ne ,SOUTHWEST LAB".BY OE OKLA. Cese No S"" '51:;J

cu .. ...,.,.. .. 1,:Z•1C·<"f

2. ,. 4. 'T~r- ·· i £' --".:r

'·-6. ,. ..

10. , , . ,2.

13

,s. '' Hi -···

'\7.

18.

19.

20 21.

22.

23 ' ..

2, 25.

26 J-7,

21

29. ..

JO

Organics Anarvsis Data Sheet (Page 41

Tonutivelv ldentifi&d Compounds

C01"npo1.1nd Ntl"l\t Ft1ittio,n

Ike he 0-c_.'d /me f.1,.,'i/ ~ s I-_~"' fb 1-J A l(,\,\k-,,.,_oii,'--V\ I•

~ " r;_,- c..,c.fch.c:)<.~'\,,. ~ I - C . ..,_, .:2____ 4

U.JVI k-"'V..◊[J•..-1 ~J -v,' [Y..,"' L-i"M 0

.

-.. - -i -·· - ~

-

-·-

-

. ' - '

... -

'.'

Sample Number

f( ~& 2?

RTo, $an f1tim,ted Hum~, Col"lttntrat~

(ugl~--

4-e,e, 41 -(( S-17 h-4 A,; GIi C.'2---fh

' &~~ "l-\ .. .-,)

·' 2.A,Vl l. .~1f.'

~

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··Transfer Ship To:

@Regional Office:~. @ Po.-~ sample collected specify number- @. ~?:: 7 SamplingPersonnel:';:•- (!:j.;:• · ofcontainersusedandmarkvolumelevel -·i'· Rec'd~----~---;

o~eachbo~e. . . _ .. : _ ,.~. 0 ~ /... b. t - ·- --! ' -- • ~-- - . - - · - SampleCo~S.gr a.

Number of · ApproXllllate on Receipt {e.g., broken, o Containers Total Volume ice, Chain-of-Custody,-etc.).:-C

~- @ Sample Description

_ Surlace Water

__ Ground Water

---· _Leachate -

Otha·

_ Mixed Media

-dSolids _ Other(specify)-~--

@) specW ~ Instructions: (e.g., safety precautions, hazardous nature)

bjJOlH' :~ ·:) ::· .. ' ~ ~- ~: ::,--;k' :· .:.2 ~- ~~ :: : :>:: X VJGXs;:;: ·g J_V~;;_·ic; ~~-'.--~,: ho· B--~ g J8 . ...,_ ,.... ... ,b.,.--- •~vr-qc-"·--.·-~.- ... - ....... -·,· G '!UJJ I l ~, ~J,..,,!. ... ~-t.. .~,,. .. ~""-(.\,.it! - .

H~1:pr12 /J°'lSr.f.;; il.il.:;,:.:::h"J.;x:i;.: -_ ::Jl~·-$MAI801'11"~21'1.ll;' U30JEClIOL1 \fGILABF.lLBCOPY'

f • ......__ .. ,..,.~

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boot?

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bl

Ill

li

• Sample Number

Organics Analysis Data Sheet (Page 1)

case No: S s· C, I Laboratory Name. t.aa~L lab Sample 10 No: _........-:cf_.9'-'.£""--9~.Z...------Sampl~ Matr,ic ~==·-----~------­Data Release Authorized By: iJ.aJ:(\M-t- (!. u.,)_ui.\..t--\.

QC Report No: _9.;._:.7 ___ ~-------

CAS Nurnoor 74-87-3

74-83-9 75-01--4

75-00-3 75-09-2 67-ti4-1 75-15-0 75~35--4 75-34-3 156-60-5 67-66-3 107-06-2 7_8-93-3 71-55-6 56-23-5 108-05--4 75-27--4

Chlorometha1,~

Contract No:

Date Sample Received:

Volatile Compounds

Concentration: e Medium {Circle One)

Date Extracted/Prepared: -------~--~-­

Date Analyzed: J/.,t) (.IC:, Cone/Oil Factor: I pH........:&~. -=O ___ _

Percent Moisture: (Not Decanted I I 2. 7 °/4.

ug/lo~ (Cir~~

lit/

CAS Number 78-87-5 1, 2-DichloroprO(Jane

Brom.omethane IJ rJ 10061-02·6 Trans• 1, J•Dichforopr0pene

Vinyl Chloride 11 tJ 79-01-6 Trichloroethene ·

-Chloroethane //I) 124-48• t Dibromochloromethane

Methylene Chloride .:t7~ 79•00·5 1, 1. 2-Trichl0<ostha_ne

Acetone 9.t A 71.43.2 Bentene

Carbon Disulfide -/,. ii 10061 ·01 ·5 cis• 1. 3-DichlorOf)rOpene

1. 1-0ichloroethane t. ,J 110-75-8 2-Chloroethylvinyfether -·

1, 1-Dw::hl_oroethane t. 1) 75-25·2 Bromoform

Trans-1. 2-0ichloroothene _ t, ,, 108-10-1 4-Methyl• 2·P~ntanone --

Chloroform L ,, 591-78-6 2•Hexanone

1, 2-0ichloroethane /,, , I 127-18-4 Tetrachloroethene

2-Butanona I /J A 79.34.5 1. 1. 2. 2-Tetrachloroethane

t, 1, 1-Trichloroethane /,, IJ 108-88-3 Toluene

carbon Tetrachloride /,. ii 108-90-7 Chlorobenze ne -

Vinyl Acetate /I iJ 100-41-4 Ethylbenzene

Bromodichloromethane ln 100-42-5 Styrene

Total Xvlenes - -

Oaia ff.ipo,1,ng Ou.ahliers

l'o, t<!Q<>ll""il results 10 EPA. 1he lollo<Ning results quahf~ .ife used. Add,uonat nags o, lootnotu ekOll,ining re$ults are .n('Otj(~. ~•. the (kl11>1110n ol each flag mu u be 11.rplk:it.

.. -

.. ,l

ug/lo~ (Cir~'f

6tl

I, (/ t, 1/

bo t,v 0.5 .:f'

~u //u !nu

//11 /lu t. 1/

&. ~j

.i :J"fl J:. d

/4 0

6tJ i/.:r

II 1he r<!SUU IS a 11alue g,.,.,,,, tha11 OI ~1 ,o lhe ~1«1,oh lln\11.

rltpOI\ lhe v.iloo

C Thi$ f~o .tW!<eS to pest,c;,de pararrteletl wnete Iha ldent,IIC.IIIIOO h.1s hffo e0t1hr.ned by GCIMS Single CO<nt)Oner.t peslw:tdes~tO

tiglul '" lhc Ito.al e•tfttt lhould b$ COC'lflfmed by GCIMS. u

J

ln-dicacu compound WU llnl1Vled lor but not IIGloctl!d. flepo,-1 lhe m, nunum detcCIIO<'I Jmm fo, the sa mpi. ...,lh lhe U {e o .. I OUI b.ased 011 netesurv c(lneen11a11Qn/dilu11on achoo. lfl111 ts Nn t>Kesur"v the tns1rumen1 del~IOf\ hm•I.I The foolttote ihould read U· Comoound was ,11~1rre1d for bul flQI dclecictd Yhe numb!lt n lt>e m,n,mum 11111,nable det~Cl"1A r.mu '°' t~ Sl•llple

lnd1ea1es a11 astrm.111ed \'zlue. fhis llag rt used e,11-H!• when e-s111n.a1,ng a conce<11ra11on for 111nt111~1y tdtnulllld COln!)OUl\(H wt.e,e a I :I rcsgll)nse 11 assu,~ or ...-hen ttM trl.l1ss toeCtral daui iridica!ed thfl P,eS.I\CQ ol • Cl)fflll;Wnd th.al "'"II the idenlrflClllaon entefla but the rHutt tS leas th.an th. t()e(ifted det-.rtKM'I hn\it !MIi greater th.t<I tero. {e.g .. I OJI. U l,m11 of deiM;tton is t O pg/I aftd a Concflnlrll'ton ol 3 µgit is c.alcul.ued, reo,o,t a, JJ.

8 Th,s 019 ,, Us.ed ~" lhe al\lllft.t ta ,ouni:11n 1h41 blank .U well U a wmo~. 11 11\d,cac.1 POhlbltlp.robab\,t blanlo. CO<llamtn.lllH:l<'I and

warn$ me. d.111,1 - 10 tale ~°"'.au·, l!C11Qt1

Othet" Ot"- soec,hc flags ;and lootno1es ni.tybe ,eq1111ed 10 ,.,_.1y,1-,11ne the fHUlls H used. they mustltt! fullydeactlbsd lf'Xl IAICh deSCtlpl((>tl

a11Khed 10 lhe data IU<nrn.ttV ,epo,t ·

form I 11/85

C <X. r---0 0

Laboratory tfame---'=-~✓ e ~ ■case No: S Sl 1 . e

• Organics Analysis Data Sheet

(Page 2)

Sample Number

FC lb Q

Semivolatile Compounds

.Concentration: 9 Medium (Circl0 One)

Oate Extracted 1Prepared: .2., I .l. f / Gt _

.Dste Anatyzed: __ .J_I_. l_l.,..1 ...... 1....,Ce ......... _____ _

Cone/Oil factor: 1 S' d ~ a · q ~ a:n-h • Percent Moisture (OecantedJ

.CAS NumlMr

• • • • • • •

108-95·2 111-44-4

ss.s1-s 54 t•73·J . 106-40-7 100·51·6

-;;."50.1

$-48-7 -3!1'638-32-9

106-44·5 621-64-7 67-72-1 98-95-3

78-59-1

88-15-5 10$-67•9

65-85-0

111-91-1

120-83-2 120-82-1 --9\-20-3

106-47-8

87-68·3 59-50-7 91-57-6 77.47.4

88-06-2 95.95.4

--

. ''1enol

bis(· 2 -Ch lotoethvl}E I her

2-Chlo,ophenol

1 3 •0tchlorobenzene

1. A-01chlorobenlene

Benzyl Alcohol

1. 2•O1chlorobenze'le 2-Mettiylpheno!

b1S12•chloro1sopropv1lcthe,

4- Methylpheno:

N-Nitroso-Or-n,Ptopyiamirw

Hei.:.achloroelhane

N11robenzer.c

lsophorone 2-N1Hophenol

2. 4•Dunethylphenol

8ento1c Acid -·

b1st-2-Chforoeth01Cy!Methane

2. 4-D•chloroohenol

1. 2. 4-Tnchloroberuene

NaphthJlene

4-Chloroaruhne

He1Cathlo,obu1ad•ene

4-C!\loro-3-MetovtoheMI

l•Melhylnaphthalene

Hel(achlorocvclopeniad1ene

2. 4. 6-Trichlorophenor

2. 4. 5-TrichlototJhenol

og/lor~ (Circf~

/ Ill .:f.P, 7b0u 7tiJ,J 71.?u ?t,,l)u

7/-1),1 ?/,.,/Ju ,, /,./),,

7/.,/),J '? C. Du 7 r.. /),, ? t. /'J,, /)L/l,,

?1,,i);J 71...n ,, 7&-t?,,

31- n/J,, 7(.n,,

. ? r,0,, ,, ~ -~ (.1../5':r

,r .., t,,n,1

?'6- /),I

71 .. "'1,1.

7t:...ll,, ? 1,.,./), J

'7(,,/),,

~1 L IJ .-i ••

GPC Cleanup tg{es □No Separatorv Funnel E,araction □Yes

Continuous Liquid - Liquid E~raction OYes

CAS Number

83-32·9

51-28-5 100.02.1

132-64-9 121-14-2

606-20-2

84-66-2 1005.72.3 86-73-7 100-0t-6 534-52-1

86-30-6

101-55•3 118-74·1

-·

87-86·5 85-01-8

120-12-7 84-74-2

200-44-0 129-00-0 85-68-7

91-94-1

56-55-3 117-81-7

218-01·9 117-84•0

205-99·2 207-08-9

-·

Acenaphthe!le

2. 4-0initrophenol

4-Nitfophenol

Oiberuofuran

2. 4-0initrotoluene

2. 6-Dinitrotoluene

Oiethylc,hthafite

4-Chlorophenvl•phen'(lether

Fluorene

4-Nit'°aniline

4, 6-0initro-2-Methvfphenol

N-Nitrosodiphenylarnine (1 J 4-Bromophenvl-phenvlether

Hel(achlorobenzene

Pentaehlorophenot

Phenanthrene

Anthracei,.e

0,~n-8utv!Phlhalate

Fluoranthene

Pvrene

ButylbenzylpMhalate

3. 3·.01chlorobenz,oine -

8enzO:a1Anthr acene t}ls{2-Ethvlhe llVI IPhth.a late

Chtysene

01-n-Octyi Phthalate

Bento(b)Ff uor an1hen,• - -Benzo<~WI uor anthene

tJ:g/1~ (Ci~~

79v-... ~

.3 ~ 00 u .1t.OC>o

g,.r - c---

7t,o,, 7/,,,0u

3:J.:r- -/I,/) ,J

?l:,t),1

~ (; 0/Jv

3. "ia '2 ·L., '] I,. ,,,,,,

?t;/Jo 7~/J,,

:~/,.(I /J,, f .30 v "." >--

'lf..O,, tJ.(; ;, A

L 11:r _,._.

I /OJ' _ .... 71,. /) tJ

l'-~cW v 7 /,. /){)

o1.J)IJ J'B 71,0u 71,,0,, ~l,O" ?t./Ju

91-58-7 2 ·Chloronaphthalene .., /,./'Ju 88-74•4 2 •N1ttoar11hne ~1L fl/J \111

50-32·8 Benzo(a)Pvrene '1k /J,1 193.39.s lndeno(1. 2. 3-cdlf>Vt4?ne ..., /,./'J,1 53-70•3 131-11.3 D1mc1hyl Phthalate ,., r..n .• -

208-96~8 Acenaphthvlene '?t../1,, 99-09·2 J-Nuroanil1ne .1 I. A(/") ,I

!

!■ I

Oibenr(a. hlAnihracene ""It. ,1,,

191-24·2 Benzo<a. h. i)Peryfooe 71,/1,J

I

• I 7 85

• !

~

C ex. r-­c C

• ■

•

8'

II II

111 I

i I !,!I I

!

!,I I

!U I !

!I I i

Organics Analysis Oata Sheet (Page 3~

Pesticide/ PC Bs

Concentration @ Medium (Circle One) GPC Cleanup ~s □No Oate Extracted 'Prepared ,il_-;I 1? - 8" Separatorv Funnel Extractron □ Yes

Date Analyzed J- 7- 8~ Continuous Liquid• liqutd Extraction □Yes Cone/Oil Factor

Percent Moisture (decanted) ----"-'-o-____ _

vs

CAS Numbe,

319-84-6

319-85-7

319-86-8

58-89-9

76-44-8

309-00-2 1024-57-3

959-98-8 60-51-1 72-55-9

72-20-8

33213-65-9

72-54•8

W31-07-8

50-29-3 72.43.5 53494-70-5 57.74.9

0001-35-2 12674-11-2

11104-28-2 11141-16-S

53469-21-9

12672-29-6

t\097-69-1

11096-82-5

Atpha-BHC

Beta-BHC

Delta-BHC

Gamma-BHC (Lmdanel

Heptachfot

Aldrin

t-!eptachlO( Ep0:r:1de

Er"ldosulfan I --

O,elddn

4. 4·.ooE Endrm

Endosulfan II

4. 4·.000

Endosulfan Sulfate 4. 4·.oor

M.ethOl'.'{Chlof ..

Endrin Ketone

Chlordane

louphene

Aroclm-1016

Aroclor-1221

Aroclor-1232

Aroclor-124:? ..

A.roclor-12(8

Aroclo, -t 2.54

A.roclor- t 250

ug/1 ot ug/Kg (Circl-e o~ei

fl,. b U /{,,. () lJ u.,n 11

/t,6 11 J(,,O 11.

IJ..O L(.

Jt,0 U /1,.D l(

.3:l-0 u. -~.o Q

..3.;J,D I.J.. ~-0 u J;;],O u .3,.'Z,Q l,l .3.J,O u

I t.l>.l> u. .3,2.0 U tt-t>,0 u

,:uo.(> L(

JbO,D _ U.. //,l>.t> u. Jl.a,IJ u JU).() u N,IJ.O tt .3;l0.6 u .3~t>.O ll

V 1 "Volume of ertract 1n1ected (oil

Vs _:: Volume of water ea:tracted (ml)

Ws ~ Weight of S3mple ektraC1ed (gl

• Vt : Volume of total ew:tfact (ulJ

forrn 1 7185

r. C (X_

r---0

C

• Organics Antalysis Data Sheet

(Page 4)

l" entativerv Identified Com90unds

• --------------,r---~-~---r CAS '8) ~r Scan Ht,J,mWt Compe,ond Name fract.an Number

1. l,LJ fll

2. ------1--------~----------,~--...J--~-➔------1

.r 20.

21.

22.

23.

24. - .

25.

26.

27.

\ -~a. a,29. :to.

fo,m I, Patt B 7 85

@Regional 9ffice:- ;ra_: Sampling Personnel: · ,r- ·, -:~:,-

r.. --

® For each sample collected specify nwnber· @ Anal~~ of containe:ts u.soo and mark volume level . Rec'd~----.--....._· on each bottle. · Oat~ Rec'd: ;;__? ai~ ~~

- ~' , ... /. / / -. Sam le Co di . /J //'•• , C/l,.,. <~ .-- p n tion ,.._ 11 H. (Name).-.:" . ·- , _. . Number of Approximate ~n Receipt (e.g., broken, 5 II: ~i?,~h!·?i-46• 51 ,___W._a-ter-------i----Co_n_~_-_e_rs-t-_To_tal_V._o __ l_um_e-t-1_ce_._Chain_·_-o_f_.C_us_;t_od_Y_, e_t_c.)___,

' ·1 GC· (Extr ctabl ) i I Sampllii~Da~e;7;~:. _. ,--- ._ 1-----a __ e_----f--___ ,-.,...-+-____ --t-_______ ---1

II 2·/7 )7/,7£.. WatP.r ~ l, (Begin) 2· • •. ;~•;"J (End) -~- (VOA)

Q ~Ship~inglnfonnation .. :. ~~!~-

0 .. r I - 0>:;--/', ·; - -- -. t-~-"----n-~Sedirn~)--e ..... n--t --+----7'--_ ------i--c-_"_

1_-;1---------.......

Name of Carrier·. , .. -. ...--------+---=t..--_______ _,._ _____ +-___..'--------.--i

t I Other

~I Date Shipped:

~I ---Air-.-!--~-~;-~-~-(,_:,,,_,._:-~'""". i __ ._Y:;._____~ ___ _.,_ _____ ..,_ ____ ~---------~

d===========::===~=~========¼ i I ® Sample Description ® Sample Location

✓YJ ·i ..51 'f,.) (I _ Surface Water ~ Mixed Media , .,

~ I - Ground Water ~~lids ~/J ~- JJ.S- / r; J

ll

II II II II II II Q

Q

q

1!1 i \Q I IQ I

!q I !

\q i

\

tn

• Sample Numbe,

~<:._ 17/J Organics Analysis Data Sheet

(Page 1)

Laboralorv Name: f-tru, MA,J.."F ~ ~ case No: ss, I ~::;;~•:t:::N_o_: _=_ . ....,.jlliaJ/..a:l:1::;.::_:i..'l~-=-· -~-~-· ~-~:-=_:_=-~--- :n~r:::o_: --_.C...a;;... ..... :_,_~ __ , ... l=t.-.::$".~·~..:: .. ;..__ ____ _

Data Release Authorized Bv: }Mox:~£UL\- C,. \l} U&¼ Date Sample Received: _ .a I .z.f I l(,

Volatile Compounds

Concentration: 9 M~dium {Circle One)

Oa1e Extracted/Prepared: ________ _

Date Analy2ed: .. J /,//it, Cone/Oil Factor: _..;../ ____ pH (,. ()

Perce.-.1 Mois1u,e: (Not Oecantedl _ __:/;.._;;f,_ .. ..;;.2-;-:;:;;.. __ _

CA$ Number

ug/10~ (Cir~

CAS Numbar

ug/lof~ (Ci~

74-87-3 Ctilorom~than~ LJ~1 78-87•5 1. 2-0ichlorOpropane ?._o 74-93.g Bromomethane I.~ •• , 10061-02·6 T ran$-1. 3-0ichloraprc,pene J.,u 75-0t-4 Vinyf Chloride /.1. J 79-01 ·6 T richfor-oethene •• ,J

75-00-3 Chloroethane 1.'1 .. 1.24-48•1 Oibromochlorom8thane __ 6v ..

15-09•2 Mcthyfene Chloride /. 3/J IJ 79-00-5 1, 1, 2-Trichforoethane _, •J

67•64-1 Acetone l/t:,, .II 71-43-2 Benzene L..~ --..

75-15-0 Carbon Disulfide I.. t/ .. 10061-01-5 cis• 1. 3-0ichloroprapene 1,,,/

75-35-4 1, 1 •Dichloroethone 6n 110-75-8 2-Chlotoethyfvinvlether /J..~ -·

75.34--3 1, 1-0ichloroethane t. ,. '15-25-2 Bromoform L. ·"' ...

156_-fiO.!:j Trans-1. 2-Dichloroethene _I,,, u 108-10·1 4-Methvt-2-Pentanone 1-'··J 67-66-3 Chloroform I, V 591•78•6 2-Hexanone j _, .•

-

107-00-2 1, 2-0ichloroethane .l. ,J 127-18-4 Tetrachlo1oethene I,,..,

78-93~3 2•8U1anone -·

I I .:f' IJ 79-34-5 1. 1. 2. 2-Tetrachloroethane /., ,/

71.55.5 1, 1. 1-Trichloroothane I,,. • , 108-88-3 Toluene Q I/ -

56-23-5 Carbon Tetrac~loride , ... ,J \08-90-7 Chlorober;zene L ., .. . .

108-05-4 Vinyl Acetate /~v t00-41-4 Ethylbenzene .)..J 75-_27-4 Bromodiehloramethane. t. ,J 100-42-5 StVfene t. -~ -·-

Total Xvlenes '1-~ Ou• ~ct>Q Qu&ldius

Vati.oe

u

J

F<>t •eoorl•"O •Hults 10 £PA.. the toUo,,,,ng tesurts 411.ahf~rs are u~. Add,1-,al flags c,, footl'IQIH eqilaollitlg ,esutH ••• encoo•11gcd. Ho•~•. the det,n11,on ot e'Klt II~ tnUfl be ,11q1l1Ctt.

II the ttsuh is ll w&lue o,ie11.e, lhan Qt equll lo the delkt'°'11 llfl'ld. C tt?r,o,t lhe walue

k>dcea1es cornoound was analy1ed IOI but •WM delCH:t4d Aef)Cl(I the t111n1tnum d.!lectlOft lnni1 I011he s,mi,14! ...,,h 1M U (e g . IOUlbtsad B

O<'-necflUC,~t&t10<,/d1l~tO<'I ldion. {thisil--ity lht! 1nsttumen1 detection l.,n.,I.J The fGOlnoce -should ,ead: U•

COt,\pound w~• .aqaly1td fo, but nor ckuaed. fM ~ is the mtnomum. iltll'-'table detectie.\ luml 1o, the nmpk Otf>e¥

1"1SK:&lcn .... tlsllfftaled Vlll,M!. This lta,g tt IIS<!d e,thcf ~ eu~c•ng .a CQl'leemtacoon fu l<fnUI~ identifted ~ ..,,,,.e I U •HOOftte tS Hsumed o, whan ~ mds IIO«ttM data iac:hc:.&t'lld 1M IW•sentill of~~ lhll _..flit ..,.,.dcat_, ctltf.tia tiuc 111• tnc.h IS lus titan the Wlt(:ified decau.on r.n1ic buC o,aatec- th.afl nto. (e.f .• 10./f. a, f,ffl<I ot OKOCflOn is 10 IJOII and a ~C\U&tllln (14 ) 51tll ti talculaled. repooi H 3J,

forml

ttws fuo aoc,loes 1ai:,e,1icic1e .,_,ame1.e,s whet• tht toMntd,cauo,, h.U bHn conllf-.1 by GCIMS. $11"1gle compo,,ent p,,-s1oetde~~tO ng,u1 on the foul e1t,.11ct V>OIAd be canhrmoed by GCIMS.

l"ht$ fl.tt os uu.:1 ~n tho ,..,..,vr• n1 foundtf'I ""blMlli as well as• ~- It tadocatU oou,ble/0(~ t,unlo. ~IIQCII and w,11,ns Iha QI& c,set lO tal.e ~op,c.!llt KtO'I

Ott>e• ~ofoefta,isend rooeno4esmavbetequMadioo,ropedy6tfHMt lheresu11s ffuwd.1heymtn1bofulfydffl;.,,-:'datldtcldldn0'-,...,,. Jilt~ 10 the data Sl,lffllna,y fllt)Of\ ,

.

..

-.c C oc t­o 0

-Laboratory Name d~◄ t4~ t' ~ I) Case No; _____ _..5.......,$._f, __ ._{ _______ _

Q

llconcentration: low ~

Organics Analysis Data Sheet (Page 2)

Semivolatile Compaunds

(Circle OM) GPC Cleanup □Yes Utf'io

Simple NUMbet

~C/10

_ Extracted 'Prepared: ~ ....... J ..... ..,.J.L.t .... f.,.,l.~------ilOate A!Uiilvzed

Cone/Oil Factor:

J / 1, / J t Separatory funnel Extraction QYes

Continuous Liquid - Liquid E,ctraction OYes

(j q Percent Mo,sture (Oecanted)

II CAS Nun1wr

ug /I or .<i'g/Kg". (Circ~

CAS ug/lo~g Number (Circ ~

II II

d d d II II

10B-95·2 l 11-44-4

95-B'7-8 541,7~-1 106-46,7

100-51-6 9_5-50-1 95·48-7 39638-32-9 106-44-5 621-64-7

..

67-72-1

98-95-3 78-59-1 88-75-S

105-61-9 65-85·0 111-91-1

120-83-2 ..

t 20-82·1 9\-20-3 106-47•8

-

87-68·3 59-50-7 91-57-6 77-47-4

88·06-2 9!>-95-4 91-58-7 88•74-4 q1-11-3 208-96-8 99-09-2

Phenol

b1s1-2 -Chli;>H>e1 hyl \Ethef

2-Chlorophenol

1 3-0 rChlorobe nzene

t. 4-0rchll')rob-em:tne

BentYI Alcohol

t. 2-0,chlutobenzene

2-Metnylphenol

b1st2 •chloro1sopropyl}E ther

4-Me1hylpheno1

N-Nmoso-0,-n-Propylamine

He x.achlotoet ha ne

N1ttobenzen~ --

lsophorone

2•N1oophenol ..

2. 4-0imethylphenol

Benzorc Acid

b,s( • 2 •Chloroe1how.y)Mf!1hane

2. 4-0ichlorophenol

, . 2. 4-TnchlofOben.t!'l'l'le

Naph1halene

4-Chloroaniline

He,cact\lorobu1ad,ene

G-Chloro-3-Methylphenol

2 -Met>iylnaphthalette

Hew.at.hlor?Cvc.lopentaoceoe

2. 4. 6-Tt1chlo1ophenol -

2. 4_ 5-Trrchl~rophcnol

2: ChloronaphthalenP.

2-Nnroanihne

01methyl Phlhahue

Acen~Ohlhylene -

3-N,uoal\lhne

-1.a/dOOfJ 83·32·9 _,, ,., ,J/./)IJ{! l} 51 ·28-5

.9. 1/-/) 0 /) t} 100·02·7 J tlnlJ/Ju 132-64-9

..1 IJ. () /JI) ll 121-14-2

,t Y IJ fJO d 606·20•2

.2.-1 '100 n 84-66-2

.J,t-/0/J/)u 7005-72•3

,:J.t.11JIJOt1 86-73-7

,_ c/-lJ/J /),,. 100-01-6

J., l,1./) I)(}" 534-52-1

~ 1/IJI){)., 86-30-6

.J.. "() /)/) ti 101·55-3

.;!. J./b/11? tJ 118-74. t

- _, ul'J/Jt? V 87 •86-5

~ _,U/)/),? I.I. 85·01 -8 • .. -~~ .... ,1 120-12-7

J ~ J' /1/)/) ,J 84-74-2

.:Jo..ll'JMo 206,44-0

.:l. 'I 0/JIJiJ ~ i,....,-- 129-00-0 . -

.1 9P tJl)d • l.....- i85•6B-7

c,.,' '"'"',1,; __ 191-94-1

..i ,f,-,,1,1) ".,_ 56-55-3

-2., ,j t) /)/)" 117-8 \ · 7

£/ Rooo ,..- ~18-01 ·9

J, I./ 0,JI),, t 17-84-0

:2 ';'-",.,u 205.99.2

l;/,IJIJ/X)o1 -'07-08-9

~"'-;'AAf'_ :,0-32-8 . -

/ ..1/) /)JJ/19_ 193 . .39.5 ,.j, ,1/}A/J

.. - . .,, ·u

_ 1,,10:ri ~ 53•70•3 191 ·_24-2

l,.U btJOu

form I

Acena ptuhe ne . "I 9 tJt1/) ,. L-,---"

Z. 4-0initrophen.ol /il..0()0011 4-t-.·:t,ophenol ,I . -, .n A f.'Jt' ti

D1benzofurari .!Jhntu, ,. v 2. 4-01n1trotoluRne .2., .,I l)tJOu

2. 6-0initrotoluene .l ildi'Jf',. Oi!lthvlphthalate .t~tJIJOv 4-Chlotophenvl·ohenylether J. ./l'IJOu V fluorene ..../.1/l/l/J

4•Nitroaniline / ,a1 l' /){) I.}

4. 6-0miuo-2-Me1hylphenol / .J.A "t't?,,, . N-Nitrosodrphenylamine 11 I .:tyMOv

4-Bromophenyf.phenvlether .,t 1/PtJtJv Hel(achloro~ntene .:l.,4.//Jt/()µ Pentachlornohenol /.k>t)~Ov Phenanthrene J' ¥/JA/Jd -

i..,.,

Attthracene .:M JJ /JO J" 01-n-8utylph1hala1e J./ '/d 3" 1J

l........-fluoranthene 7'-1:0()(J .,. Pvtene !?. <;'.' A¥\() •

,,..,-,--0utylbe1'\lylphthalate ,z ttOt>tJ tJ

3. J'-01chloroben21dine ;,;-J' /Jl)t) ti - V BeMCl(aJA.nlhracene / <tJOIJ.--r b,st2-Ethylhe~vljPhthal:ire ti 7 I)() :f /j

V Chrysene I :J.A/)/J < O••n-Octyl Phthalate ,,;tt./l)tJ/1 ,,

V Benzo{b\f'I u(>f a ntheJ ne .. 7/)tJt} :r Ben.to{lc }Fluor a nthene t. h/Jll.-r.

v ..... - . V Benzo(aJPvrene /,. ¼J/) :r

lndeno(1, 2. 3-cdlPv,ene .2<#J0t)n _ Otben:(a h)Anlhtacene _., . , ::/\1'1,,

_ Bcflzo<a. h. 11Pervlene o2 1/(JLJ(J J)

,-as

....... C CL

r--0 0

IJ IJ

II Q

q i

i,Q i

llq I I

II I I.

- ~ • f-

Labot aiorv NamrlAJJt,..4 J., Z.s~t

- -- . -~ - -

__ 49 ,oeecs, tu. , ~

. Organics A,rtalysis Oata-Stteet -(Page 3)

--Pesticide/PCB,

-Samp&. -Nu,nber -- ~

__ F-i!. ---:_'8:zo

Concentration low ~ (Circle Onet GPC Cleanup □Yes. mtfo Date Extracted 'Prepared· .3 - 3- F <;. Date Anafvzed . 3- Z- ~ <o _( .3- /z~s(.

Separatory Funnel Extractt0n O Yes·

Continuous Liquid - Liquid Extraction □Yes

- ------~•_'I.Q_k.. ~-t Conc/011 Factor: -~ b-- - -- -~

Percent Moisture (decanted) ~-----' ... i"------

CAS Numbm

319-84-6

319-05•7

319-86•8

58-89·9

76-44-8

309-00-2 1024-57-3

9S9-98-8 60-57-1

72.55.9 72-20-8 33213-65-9

72-54-8 1031-07-8

50·29-3 72.43.5

53494-70•5

57.74.9

8001-35-2

12674-11-2 ---·

11104-28-2

11141-16-5

53469-21-9

12672-29-6

11097-69-1

11O96-82-S

Alpha-BHC

Beta·BHC

OeUa-8HC

Gamma-8HC {lrndanel

Heptachlor

Aldt1n

Heptactilor Epox1de

Endosuffao I

D1eldrin

4. 4"-DOE

Endun

Endosulfan II

4. 4·.000

Endosulfan Sulfate

4. 4·.oor Methoxychlor

Endnn Ke1one

Chlordane

loxaphene

Arodor-1016

Arodor-1221

Aroclor-1232

Aroclor-124)

Aroclot • 1248

Aroclor • 1254

Aroclor-126O

ug/lo~ (Cir~~

,i.o, () u ,/ ... -I ~O. () Ji

l'J.O,D lJ J20 {'") l{

I 2(), 0 U )~O,fl lJ !~6.0 ll

;tl/0.0 lJ ::llJ /ll'I u

_.:Zl/u,D u ..:tito,o u .::tt/0,C __ 11 .Rt/0,0 11 2t./aD u

1:2(;(),0 u ~l/1),0 I)

/:l,00 0 11 ;il/iJO,D (J

J:)OD 0 /)

LlCD.O fl

l:JCJCJ,0 fl

/,;ltxJ, C 11

1..200.0 U ~(j_OO,t;J U ,;1lfob,D U

V, "' Volume of elCtract 1111ected {ulJ

Vs "' Volume of water e!(tracted (ml)

W 5 = Weight of sample e1ttracted (gl

V1 = Volume of to1al eictract Cull

. 11-f!tJ~ / & o. o /"' A ..,,, .. lt ~

~ ft} t.Af_

- V - .,l,_C) J .-

form 1 7185

ubora1orv Name. - (p ~ '- .,.,......:r,:Y · -

llaseNo· · 6"Sl,( ---- . Jrganics Analysis Data Sheet

• (Page 4)

T entfttively Identified Compounds

·-=--· --,---------,--~~·--I RT Sc:an CAS NUMMt ft•ction Numbet

E1tirnbtttd Cone.. (ug/1~

1.----½------------------+----+----JJ.------1 2-----f---------------------t-----t----Jl-------1 3. ------1---~-----~----------+----1------4,-----4

/¥OJ" 4 -=---==-----l--~.l.::!.~:&!.LJa~:::t'].,£,l:Jo:A,d"'6,:i~~..4,...j ..... k4d.L----J--6Z.£..J.~+-L....;z.u!(L_+-Sl....2~!:...---4

6. 9 .1.$.>. ,J. /4,00.f

6. --

7_..,..:--_,-b~~~¥.,{.._.~.,,µ.~:i.e:!!~~~~~-+~--f--~~~-.J-_!,,._~~--1 ,5' t> ,J

I ~Ot) ::r' .. _J :· .......,!;-===·;__· --1---·"_. ~--:-------r--~ ............... ~~--­• 10.Z,h.U~L-j~~o!Zli4-'~~~T.:&..an,,1,&~~~----¼-----r·.J.J~..!lo,:::;:.-J-....L.L.!:::..J....-,I

,. ,. •• , . ,.

.. ,, J 11.

12 •. ~ lu 1

1• .. ... "' H

.9:t, " .. " ..

1/tJll ... el 21.~J.£./.~r.l-~.f,,LJ~g.t..t:U.,;.-..L::.;.....d~:U.::fJd11.&L-=-~~---+-..:::.--f-..J..:U.....td~..J--J.~U-!=L---f .

22---•-----jf--~-...-:::.a:::i.=~...-:;;.__, _____ .......,,....... _______ -+-----4----~ •• _ .w 7~.7---_ -23. '.ii) 8

24,---~1---------------------t----+------J----......... 25·---~1-------------------t----1------+-----1 26·-----1---------------------it------1------+--------t 21--------1,.--------~-------------it----t------+-------1 28·----+-------------------t---;-----~-----i 29·---~1.--------------------ii-----t-----1------t 30-------ii-.-----------------ii..---......._ ___ __._ ____ .........,

\. I i

II■ ! l

I• ~ l ........... __ "'"""""'&-&•••H ............. , • .,._ • ··•-N ..... _ .. c1 ................... ~ .. ---··

i

fo,m I. Part 8

······· ... ~ ........................................ ······~- ·-··········· ........ .

7 85

O' C a: t-0 0

6-