Appendix 10 Laboratory Data Packages and Data Usability … · 2016. 10. 7. · Laboratory Review...

CES Griggs Road VCP Site APAR March 2016 119

Appendix 10 Laboratory Data Packages and Data Usability Summary – Volume 2

September 30, 2015

Brenda BasilePBW Houston11231 Richmond AvenueSuite D104Houston, TX 77082

The analytical data provided relates directly to the samples received by ALS Environmental and for only the analyses requested. Results are expressed as "as received" unless otherwise noted.

QC sample results for this data met EPA or laboratory specifications except as noted in the Case Narrative or as noted with qualifiers in the QC batch information. Should this laboratory report need to be reproduced, it should be reproduced in full unless written approval has been obtained by ALS Environmental. Samples will be disposed in 30 days unless storage arrangements are made.

If you have any questions regarding this report, please feel free to call me.

Sincerely,

ALS Environmental received 17 sample(s) on Sep 23, 2015 for the analysis presented in the following report.

Laboratory Results for: CES Griggs Rd VCP

Dear Brenda,

Work Order: HS15091001

Generated By: Dayna.Fisher

Dane J. Wacasey

10450 Stancliff Rd. Suite 210 Houston, TX 77099 T: +1 281 530 5656 F: +1 281 530 5887 www.alsglobal.com

Page 1 of 155

Client:TRRP Laboratory Data Package Cover PageProject:

WorkOrder:

PBW HoustonCES Griggs Rd VCPHS15091001

This data package consists of all or some of the following as applicable:

This signature page, the laboratory review checklist, and the following reportable data:

R1 Field chain-of-custody documentation;

R2 Sample identification cross-reference;

R3 Test reports (analytical data sheets) for each environmental sample that includes:a) Items consistent with NELAC Chapter 5, b) dilution factors, c) preparation methods, d) cleanup methods, and e) if required for the project, tentatively identified compounds (TICs).

R4 Surrogate recovery data including:a) Calculated recovery (%R), and b) The laboratory’s surrogate QC limits.

R5 Test reports/summary forms for blank samples;

R6 Test reports/summary forms for laboratory control samples (LCSs) including:a) LCS spiking amounts, b) Calculated %R for each analyte, and c)The laboratory’s LCS QC limits.

R7 Test reports for project matrix spike/matrix spike duplicates (MS/MSDs) including:a) Samples associated with the MS/MSD clearly identified, b) MS/MSD spiking amounts, c) Concentration of each MS/MSD analyte measured in the parent and spiked samples, d) Calculated %Rs and relative percent differences (RPDs), and e) The laboratory’s MS/MSD QC limits.

R8 Laboratory analytical duplicate (if applicable) recovery and precision:a) the amount of analyte measured in the duplicate, b) the calculated RPD, and c) the laboratory’s QC limits for analytical duplicates.

R9 List of method quantitation limits (MQLs) and detectability check sample results for eachanalyte for each method and matrix.

R10 Other problems or anomalies. The Exception Report for each “No” or “Not Reviewed (NR)” item in Laboratory Review Checklist andfor each analyte, matrix, and method for which the laboratory does not hold NELAC accreditation underthe Texas Laboratory Accreditation Program.

ALS Group USA, Corp Date: 30-Sep-15

Page 2 of 155


WorkOrder:


Dane J. Wacasey

Release Statement: I am responsible for the release of this laboratory data package. This laboratory isNELAC accredited under the Texas Laboratory Accreditation Program for all the methods, analytes andmatrices reported in this data package except as noted in the Exception Reports. The data have beenreviewed and are technically compliant with the requirements of the methods used, except where noted bythe laboratory in the attached exception reports. By my signature below, I affirm to the best of myknowledge, all problems/anomalies, observed by the laboratory have been identified by the laboratory inthe Laboratory Review Checklist, and no information affecting the quality of the data has been knowinglywithheld.

Check, if applicable: [NA] This laboratory meets an exception under 30 TAC §25.6 and was last inspectedby [ ] TCEQ or [ ] ______________ on (enter date of last inspection). Any findings affecting the data inthis laboratory data package are noted in the Exception Reports herein. The official signing the cover pageof the report in which these data are used is responsible for releasing this data package and is by signatureaffirming the above release statement is true.


Page 3 of 155

Laboratory Review Checklist: Reportable Data

Laboratory Name: ALS Laboratory Group LRC Date: 09/30/2015 Project Name: CES Griggs Rd VCP Laboratory Job Number: HS15091001

Reviewer Name: Dane Wacasey Prep Batch Number(s): 97408, 97448, 97451, 97509, R261899, R262070, R262131, R262143, R262231

#1 A2 Description Yes No NA3 NR4 ER#5

R1 OI Chain-of-custody (C-O-C)

Did samples meet the laboratory’s standard conditions of sample acceptability upon receipt? X

Were all departures from standard conditions described in an exception report? X R2 OI Sample and quality control (QC) identification Are all field sample ID numbers cross-referenced to the laboratory ID numbers? X Are all laboratory ID numbers cross-referenced to the corresponding QC data? X R3 OI Test reports Were all samples prepared and analyzed within holding times? X

Other than those results < MQL, were all other raw values bracketed by calibration standards? X

Were calculations checked by a peer or supervisor? X Were all analyte identifications checked by a peer or supervisor? X Were sample detection limits reported for all analytes not detected? X Were all results for soil and sediment samples reported on a dry weight basis? X Were % moisture (or solids) reported for all soil and sediment samples? X

Were bulk soils/solids samples for volatile analysis extracted with methanol per SW-846 Method 5035? X

If required for the project, TICs reported? X R4 O Surrogate recovery data Were surrogates added prior to extraction? X

Were surrogate percent recoveries in all samples within the laboratory QC limits? X

R5 OI Test reports/summary forms for blank samples Were appropriate type(s) of blanks analyzed? X Were blanks analyzed at the appropriate frequency? X

Were method blanks taken through the entire analytical process, including preparation and, if applicable, cleanup procedures? X

Were blank concentrations < MQL? X R6 OI Laboratory control samples (LCS): Were all COCs included in the LCS? X

Was each LCS taken through the entire analytical procedure, including prep and cleanup steps? X

Were LCSs analyzed at the required frequency? X Were LCS (and LCSD, if applicable) %Rs within the laboratory QC limits? X

Does the detectability data document the laboratory’s capability to detect the COCs at the MDL used to calculate the SDLs? X

Was the LCSD RPD within QC limits? X R7 OI Matrix spike (MS) and matrix spike duplicate (MSD) data Were the project/method specified analytes included in the MS and MSD? X Were MS/MSD analyzed at the appropriate frequency? X Were MS (and MSD, if applicable) %Rs within the laboratory QC limits? X 1 Were MS/MSD RPDs within laboratory QC limits? X 2 R8 OI Analytical duplicate data Were appropriate analytical duplicates analyzed for each matrix? X Were analytical duplicates analyzed at the appropriate frequency? X Were RPDs or relative standard deviations within the laboratory QC limits? X R9 OI Method quantitation limits (MQLs): Are the MQLs for each method analyte included in the laboratory data package? X

Do the MQLs correspond to the concentration of the lowest non-zero calibration standard? X

Are unadjusted MQLs and DCSs included in the laboratory data package? X R10 OI Other problems/anomalies

Are all known problems/anomalies/special conditions noted in this LRC and ER? X

Were all necessary corrective actions performed for the reported data? X

Was applicable and available technology used to lower the SDL and minimize the matrix interference affects on the sample results? X

Is the laboratory NELAC-accredited under the Texas Laboratory Program for the analytes, matrices and methods associated with this laboratory data package? X 3

Page 4 of 155

Laboratory Review Checklist: Reportable Data Laboratory Name: ALS Laboratory Group LRC Date: 09/30/2015 Project Name: CES Griggs Rd VCP Laboratory Job Number: HS15091001



S1 OI Initial calibration (ICAL)

Were response factors and/or relative response factors for each analyte within QC limits? X

Were percent RSDs or correlation coefficient criteria met? X Was the number of standards recommended in the method used for all analytes? X

Were all points generated between the lowest and highest standard used to calculate the curve? X

Are ICAL data available for all instruments used? X

Has the initial calibration curve been verified using an appropriate second source standard? X

S2 OI Initial and continuing calibration verification (ICCV and CCV) and

continuing calibration blank (CCB) Was the CCV analyzed at the method-required frequency? X Were percent differences for each analyte within the method-required QC limits? X 4 Was the ICAL curve verified for each analyte? X Was the absolute value of the analyte concentration in the inorganic CCB < MDL? X 5 S3 O Mass spectral tuning: Was the appropriate compound for the method used for tuning? X Were ion abundance data within the method-required QC limits? X S4 O Internal standards (IS): Were IS area counts and retention times within the method-required QC limits? X

S5 OI Raw data (NELAC section 1 appendix A glossary, and section 5.12 or ISO/IEC 17025 section

Were the raw data (for example, chromatograms, spectral data) reviewed by an analyst? X

Were data associated with manual integrations flagged on the raw data? X S6 O Dual column confirmation Did dual column confirmation results meet the method-required QC? X S7 O Tentatively identified compounds (TICs):

If TICs were requested, were the mass spectra and TIC data subject to appropriate checks? X

S8 I Interference Check Sample (ICS) results: Were percent recoveries within method QC limits? X S9 I Serial dilutions, post digestion spikes, and method of standard additions

Were percent differences, recoveries, and the linearity within the QC limits specified in the method? X 6

S10 OI Method detection limit (MDL) studies Was a MDL study performed for each reported analyte? X Is the MDL either adjusted or supported by the analysis of DCSs? X S11 OI Proficiency test reports:

Was the laboratory's performance acceptable on the applicable proficiency tests or evaluation studies? X

S12 OI Standards documentation

Are all standards used in the analyses NIST-traceable or obtained from other appropriate sources? X

S13 OI Compound/analyte identification procedures Are the procedures for compound/analyte identification documented? X S14 OI Demonstration of analyst competency (DOC) Was DOC conducted consistent with NELAC Chapter 5C or ISO/IEC 4? X Is documentation of the analyst’s competency up-to-date and on file? X

S15 OI Verification/validation documentation for methods (NELAC Chap 5 or ISO/IEC 17025 Section 5)

Are all the methods used to generate the data documented, verified, and validated, where applicable? X

S16 OI Laboratory standard operating procedures (SOPs): Are laboratory SOPs current and on file for each method performed? X Items identified by the letter “R” must be included in the laboratory data package submitted in the TRRP-required report(s). Items identified by the letter “S” should be retained and made available upon request for the appropriate retention period. O = Organic Analyses; I = Inorganic Analyses (and general chemistry, when applicable); NA = Not Applicable; NR = Not Reviewed; R# = Exception Report identification number (an Exception Report should be completed for an item if “NR” or “No” is checked).

Page 5 of 155




ER#5 Description

1

Batch 97448, Metals Method SW6020, sample 4904-SB21-16.5, MS and or MSD recovered outside the control limits for Antimony, Barium, Lead and Manganese; however, the results in the parent sample is greater than 4x the spike amount for Manganese. Batch 97408, Semivolatile Organics Method SW8270, sample 4904-SB21-16.5, MSD recovered outside the control limits for Di-n-octyl phthalate and Hexachlorocyclopentadiene Batch R262131, Volatile Organics Method SW8260, sample 4904-SB21-16.5, MS recovered outside the control limits for Tetrachloroethene.

2 Batch R261899, Volatile Organics Method SW8260, sample HS15091033-01, MSD RPD is for anf unrelated sample.

3

With the exception of Volatile Organics Method SW8260 Cyclohexane and Semivolatile Organics Method SW8270 1-Methylnaphthalene and Benzaldehyde, ALS is NELAC-accredited under the Texas Laboratory Program for the analytes, matrices and methods associated with this laboratory data package. Because TCEQ does not offer accreditation for these compounds, the results are flagged with n.

4

Batch R262131, Volatile Organics Method SW8260: Bromomethane exceeded %D (122%) exceeded control limits (80-120) in the CCV; Bromomethane was not detected in any of the associated samples.

5

See Run Log and CCB Exceptions Report.

6

Batch 97448, Metals Method SW6020, sample 4904-SB21-16.5, Bench Spike (PDS) recovered outside the control limits for Manganese, however, the results in the parent sample is greater than 4x the spike.

Items identified by the letter “R” must be included in the laboratory data package submitted in the TRRP-required report(s). Items identified by the letter “S” should be retained and made available upon request for the appropriate retention period. O = Organic Analyses; I = Inorganic Analyses (and general chemistry, when applicable); NA = Not Applicable; NR = Not Reviewed; R# = Exception Report identification number (an Exception Report should be completed for an item if “NR” or “No” is checked).

Page 6 of 155

ICPMS04_262044Run ID:

FORM 13 - ANALYSIS RUN LOG

SW6020Method: Instrument:

Sample No. D/F Time Analytes

HS15091001CES Griggs Rd VCPPBW Houston

WorkOrder:Project:Client:

ICPMS04

Start Date: End Date:28-Sep-2015 29-Sep-2015

FileIDICV 1 28-Sep-2015

12:11AG AS BA BE CD CO CR CU MN NI PB SB SE TL V ZN009SMPL.D

LLICV5 1 28-Sep-2015 12:15

AG AS BA BE CD CO CR CU MN NI PB SB SE TL V ZN010SMPL.D

LLICV2 1 28-Sep-2015 12:20


ICB 1 28-Sep-2015 12:24

AG AS BA BE CD CO CR CU MN NI PB SB SE TL V ZN012CCB.D

ICSA 1 28-Sep-2015 12:29


ICSAB 1 28-Sep-2015 12:34


CCB 1 1 28-Sep-2015 13:23


CCV 1 1 28-Sep-2015 13:28


CCV 2 1 28-Sep-2015 14:16


CCB 2 1 28-Sep-2015 14:20


MBLK-97448 1 28-Sep-2015 14:29

AG AS BA CD CO CR CU MN NI PB SB SE TL V ZN040SMPL.D

MLCS-97448 1 28-Sep-2015 14:34

AG AS BA CD CO CR CU MN NI PB SB SE TL V ZN041SMPL.D

4904-SB21-16.5 1 28-Sep-2015 14:42

AG AS BA CD CO CR CU MN NI PB SB SE TL V043SMPL.D

4904-SB21-16.5SD 5 28-Sep-2015 14:47


4904-SB21-16.5MS 1 28-Sep-2015 14:51


4904-SB21-16.5MSD 1 28-Sep-2015 14:55


4904-SB21-16.5PDS 1 28-Sep-2015 15:00


CCV 3 1 28-Sep-2015 15:04


CCB 3 1 28-Sep-2015 15:08


ICCV 4 1 28-Sep-2015 15:48


LLCCV5 1 28-Sep-2015 15:52


LLCCV2 1 28-Sep-2015 15:57


ICCB 4 1 28-Sep-2015 16:01


CCV 5 1 28-Sep-2015 16:36


CCB 5 1 28-Sep-2015 16:41


MBLK-97448 1 28-Sep-2015 16:45

BE071SMPL.D

MLCS-97448 1 28-Sep-2015 16:50

BE072SMPL.D

4904-SB21-16.5 1 28-Sep-2015 16:54

BE ZN073SMPL.D

4904-SB21-16.5SD 5 28-Sep-2015 16:58

BE ZN074SMPL.D

4904-SB21-16.5MS 1 28-Sep-2015 17:03

BE ZN075SMPL.D

4904-SB21-16.5MSD 1 28-Sep-2015 17:07

BE ZN076SMPL.D

4904-SB21-16.5PDS 1 28-Sep-2015 17:12

BE ZN077SMPL.D

CCV 6 1 28-Sep-2015 17:16

AG AS BA BE CD CO CR CU MN NI PB SB SE TL V ZN078CCV.D

30-Sep-15Date: ALS Group USA, Corp

Page 7 of 155







ICPMS04


FileIDCCB 6 1 28-Sep-2015

17:20AG AS BA BE CD CO CR CU MN NI PB SB SE TL V ZN079CCB.D

CCV 7 1 28-Sep-2015 17:51


CCB 7 1 28-Sep-2015 17:55


CCV 8 1 28-Sep-2015 18:21


CCB 8 1 28-Sep-2015 18:25


4904-SB19-03 1 28-Sep-2015 18:30


4904-SB19-14 1 28-Sep-2015 18:34


4904-SB19-16.5 1 28-Sep-2015 18:39


4904-SB20-02 1 28-Sep-2015 18:43

AG AS BE CD CO CR CU MN NI PB SB SE TL V ZN098SMPL.D

4904-SB20-07 1 28-Sep-2015 18:47


4904-SB20-19 1 28-Sep-2015 18:52


4904-SB21-04 1 28-Sep-2015 18:56


4904-SB21-10 1 28-Sep-2015 19:01


4904-SB22-03 1 28-Sep-2015 19:05


CCV 9 1 28-Sep-2015 19:09


CCB 9 1 28-Sep-2015 19:14


4904-SB22-05 1 28-Sep-2015 19:18


4904-SB22-20 1 28-Sep-2015 19:23


4904-SB23-04 1 28-Sep-2015 19:27


4904-SB23-10 1 28-Sep-2015 19:31


4904-SB23-19 1 28-Sep-2015 19:36


CCV 10 1 28-Sep-2015 19:57


CCB 10 1 28-Sep-2015 20:02


CCV 11 1 28-Sep-2015 20:37


CCB 11 1 28-Sep-2015 20:41


CCV 12 1 28-Sep-2015 21:20


CCB 12 1 28-Sep-2015 21:24


CCV 13 1 28-Sep-2015 22:03


CCB 13 1 28-Sep-2015 22:07


CCV 14 1 28-Sep-2015 22:47


CCB 14 1 28-Sep-2015 22:51


CCV 15 1 28-Sep-2015 23:38


CCB 15 1 28-Sep-2015 23:43



Page 8 of 155







ICPMS04


FileIDLLCCV2 1 28-Sep-2015


LLCCV5 1 28-Sep-2015 23:52


ICSA 1 28-Sep-2015 23:56


ICSAB 1 29-Sep-2015 00:01



Page 9 of 155


CCB EXCEPTIONS REPORT




ICPMS04

Seq: 3440317CCB 3 128-Sep-2015 15:08 D/F:Date:Analyte Result MDL Report Limit

Units: ug/L

1.426 1.1 5Selenium-1.037 0.6 5Vanadium


Units: ug/L

0.728 0.6 5Vanadium


Units: ug/L

1.29 1.1 5Selenium


Units: ug/L

0.243 0.2 2Thallium0.611 0.6 5Vanadium


Units: ug/L

1.481 1.1 5Selenium


Units: ug/L

2.748 1 5Copper1.657 1.1 5Selenium


Units: ug/L

1.766 1.1 5Selenium0.891 0.6 5Vanadium


Units: ug/L



Units: ug/L



Units: ug/L

2.603 1.1 5Selenium


Units: ug/L

2.453 1.1 5Selenium0.206 0.2 2Thallium


Page 10 of 155

Client: PBW Houston

Work Order: HS15091001Project: CES Griggs Rd VCP SAMPLE SUMMARY

Lab Samp ID Client Sample ID Collection DateMatrix TagNo Date Received Hold

HS15091001-01 23-Sep-2015 15:20 23-Sep-2015 12:294904-SB19-03 Soil

HS15091001-02 22-Sep-2015 15:25 23-Sep-2015 12:294904-SB19-14 Soil

HS15091001-03 22-Sep-2015 15:25 23-Sep-2015 12:294904-SB19-16.5 Soil

HS15091001-04 22-Sep-2015 10:35 23-Sep-2015 12:294904-SB20-02 Soil

HS15091001-05 22-Sep-2015 10:35 23-Sep-2015 12:294904-SB20-07 Soil

HS15091001-06 22-Sep-2015 10:40 23-Sep-2015 12:294904-SB20-19 Soil

HS15091001-07 22-Sep-2015 14:10 23-Sep-2015 12:294904-SB21-04 Soil

HS15091001-08 22-Sep-2015 14:20 23-Sep-2015 12:294904-SB21-10 Soil

HS15091001-09 22-Sep-2015 14:25 23-Sep-2015 12:294904-SB21-16.5 Soil

HS15091001-10 22-Sep-2015 16:35 23-Sep-2015 12:294904-SB22-03 Soil

HS15091001-11 22-Sep-2015 16:45 23-Sep-2015 12:294904-SB22-05 Soil

HS15091001-12 22-Sep-2015 16:50 23-Sep-2015 12:294904-SB22-20 Soil

HS15091001-13 22-Sep-2015 12:15 23-Sep-2015 12:294904-SB23-04 Soil

HS15091001-14 22-Sep-2015 12:20 23-Sep-2015 12:294904-SB23-10 Soil

HS15091001-15 22-Sep-2015 12:15 23-Sep-2015 12:294904-SB23-19 Soil

HS15091001-16 22-Sep-2015 17:00 23-Sep-2015 12:29TB01 092215 Water


ALS Group USA, Corp 30-Sep-15Date:

Page 11 of 155

Client:Project:Sample ID:

PBW HoustonCES Griggs Rd VCP4904-SB19-03

WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-01

23-Sep-2015 15:20 Matrix:Soil

ANALYTICAL REPORT

ANALYSES RESULT MQLDILUTION FACTORUNITS

DATE ANALYZEDQUAL SDL

VOLATILES BY SW8260C Method:SW8260 Analyst: WLR1mg/Kg-dry 29-Sep-2015 09:490.000641,1,1,2-Tetrachloroethane 0.0053U

1mg/Kg-dry 29-Sep-2015 09:490.000531,1,1-Trichloroethane 0.0053U

1mg/Kg-dry 29-Sep-2015 09:490.000851,1,2,2-Tetrachloroethane 0.0053U

1mg/Kg-dry 29-Sep-2015 09:490.000751,1,2-Trichlor-1,2,2-trifluoroethane 0.0053U


1mg/Kg-dry 29-Sep-2015 09:490.000531,1-Dichloroethane 0.0053U

1mg/Kg-dry 29-Sep-2015 09:490.000531,1-Dichloroethene 0.0053U

1mg/Kg-dry 29-Sep-2015 09:490.00121,2,3-Trichlorobenzene 0.0053U


1mg/Kg-dry 29-Sep-2015 09:490.00121,2,4-Trimethylbenzene 0.0053U

1mg/Kg-dry 29-Sep-2015 09:490.000531,2-Dibromoethane 0.0053U

1mg/Kg-dry 29-Sep-2015 09:490.00111,2-Dichlorobenzene 0.0053U


1mg/Kg-dry 29-Sep-2015 09:490.000851,2-Dichloropropane 0.0053U




1mg/Kg-dry 29-Sep-2015 09:49J 0.00142-Butanone 0.0110.0074

1mg/Kg-dry 29-Sep-2015 09:490.00152-Hexanone 0.011U

1mg/Kg-dry 29-Sep-2015 09:490.00124-Isopropyltoluene 0.0053U

1mg/Kg-dry 29-Sep-2015 09:490.00214-Methyl-2-pentanone 0.011U

1mg/Kg-dry 29-Sep-2015 09:490.0033Acetone 0.0210.055

1mg/Kg-dry 29-Sep-2015 09:490.00053Benzene 0.0053U

1mg/Kg-dry 29-Sep-2015 09:490.00053Bromodichloromethane 0.0053U

1mg/Kg-dry 29-Sep-2015 09:490.00064Bromoform 0.0053U

1mg/Kg-dry 29-Sep-2015 09:490.0011Bromomethane 0.011U

1mg/Kg-dry 29-Sep-2015 09:490.00064Carbon disulfide 0.011U

1mg/Kg-dry 29-Sep-2015 09:490.00064Carbon tetrachloride 0.0053U

1mg/Kg-dry 29-Sep-2015 09:490.00064Chlorobenzene 0.0053U

1mg/Kg-dry 29-Sep-2015 09:490.00085Chloroethane 0.011U

1mg/Kg-dry 29-Sep-2015 09:490.00053Chloroform 0.0053U

1mg/Kg-dry 29-Sep-2015 09:490.00053Chloromethane 0.011U

1mg/Kg-dry 29-Sep-2015 09:490.00085cis-1,2-Dichloroethene 0.0053U

1mg/Kg-dry 29-Sep-2015 09:490.00053cis-1,3-Dichloropropene 0.0053U

1mg/Kg-dry 29-Sep-2015 09:49n 0.0011Cyclohexane 0.0053U

1mg/Kg-dry 29-Sep-2015 09:490.00053Dibromochloromethane 0.0053U

1mg/Kg-dry 29-Sep-2015 09:490.00075Dichlorodifluoromethane 0.0053U

1mg/Kg-dry 29-Sep-2015 09:490.00075Ethylbenzene 0.0053U

1mg/Kg-dry 29-Sep-2015 09:490.00096Isopropylbenzene 0.0053U


Note: See Qualifiers Page for a list of qualifiers and their explanation.

Page 12 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-01


ANALYTICAL REPORT



VOLATILES BY SW8260C Method:SW8260 Analyst: WLR1mg/Kg-dry 29-Sep-2015 09:490.00053Methyl tert-butyl ether 0.0053U

1mg/Kg-dry 29-Sep-2015 09:490.0013Methylcyclohexane 0.0053U

1mg/Kg-dry 29-Sep-2015 09:490.0011Methylene chloride 0.011U

1mg/Kg-dry 29-Sep-2015 09:49J 0.00085Naphthalene 0.00530.0024

1mg/Kg-dry 29-Sep-2015 09:490.00064n-Butylbenzene 0.0053U

1mg/Kg-dry 29-Sep-2015 09:490.00096n-Propylbenzene 0.0053U

1mg/Kg-dry 29-Sep-2015 09:490.0011sec-Butylbenzene 0.0053U

1mg/Kg-dry 29-Sep-2015 09:490.00075Styrene 0.0053U

1mg/Kg-dry 29-Sep-2015 09:490.0011tert-Butylbenzene 0.0053U

1mg/Kg-dry 29-Sep-2015 09:490.00075Tetrachloroethene 0.0053U

1mg/Kg-dry 29-Sep-2015 09:490.00064Toluene 0.0053U

1mg/Kg-dry 29-Sep-2015 09:490.00053trans-1,2-Dichloroethene 0.0053U

1mg/Kg-dry 29-Sep-2015 09:490.00064trans-1,3-Dichloropropene 0.0053U

1mg/Kg-dry 29-Sep-2015 09:490.00064Trichloroethene 0.0053U

1mg/Kg-dry 29-Sep-2015 09:490.00053Trichlorofluoromethane 0.0053U

1mg/Kg-dry 29-Sep-2015 09:490.00085Vinyl chloride 0.0021U

1mg/Kg-dry 29-Sep-2015 09:490.0026Xylenes, Total 0.011U

Surr: 1,2-Dichloroethane-d4 1%REC 29-Sep-2015 09:4989.5 70-128

Surr: 4-Bromofluorobenzene 1%REC 29-Sep-2015 09:4999.2 73-126

Surr: Dibromofluoromethane 1%REC 29-Sep-2015 09:4994.8 71-128

Surr: Toluene-d8 1%REC 29-Sep-2015 09:49104 73-127



Page 13 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-01


ANALYTICAL REPORT



LOW-LEVEL SEMIVOLATILES Method:SW8270 Analyst: LGPrep:SW3541 / 24-Sep-2015

1mg/Kg-dry 25-Sep-2015 18:590.00221,1´-Biphenyl 0.0085U

1mg/Kg-dry 25-Sep-2015 18:590.00131,2,4,5-Tetrachlorobenzene 0.0085U

1mg/Kg-dry 25-Sep-2015 18:59Jn 0.00191-Methylnaphthalene 0.00420.0025

1mg/Kg-dry 25-Sep-2015 18:590.00372,3,4,6-Tetrachlorophenol 0.0085U

1mg/Kg-dry 25-Sep-2015 18:590.00322,4,5-Trichlorophenol 0.0085U


1mg/Kg-dry 25-Sep-2015 18:590.00172,4-Dichlorophenol 0.0085U

1mg/Kg-dry 25-Sep-2015 18:590.00422,4-Dimethylphenol 0.0085U

1mg/Kg-dry 25-Sep-2015 18:590.00582,4-Dinitrophenol 0.017U

1mg/Kg-dry 25-Sep-2015 18:590.00122,4-Dinitrotoluene 0.0085U


1mg/Kg-dry 25-Sep-2015 18:590.00172-Chloronaphthalene 0.0085U

1mg/Kg-dry 25-Sep-2015 18:590.00172-Chlorophenol 0.0085U

1mg/Kg-dry 25-Sep-2015 18:59J 0.000642-Methylnaphthalene 0.00420.0022

1mg/Kg-dry 25-Sep-2015 18:590.00142-Methylphenol 0.0085U

1mg/Kg-dry 25-Sep-2015 18:590.00242-Nitroaniline 0.0085U

1mg/Kg-dry 25-Sep-2015 18:590.00322-Nitrophenol 0.0085U

1mg/Kg-dry 25-Sep-2015 18:590.00133&4-Methylphenol 0.0085U

1mg/Kg-dry 25-Sep-2015 18:590.00323,3´-Dichlorobenzidine 0.0085U


1mg/Kg-dry 25-Sep-2015 18:590.00274,6-Dinitro-2-methylphenol 0.0085U

1mg/Kg-dry 25-Sep-2015 18:590.00214-Bromophenyl phenyl ether 0.0085U

1mg/Kg-dry 25-Sep-2015 18:590.000904-Chloro-3-methylphenol 0.0085U

1mg/Kg-dry 25-Sep-2015 18:590.00194-Chlorophenyl phenyl ether 0.0085U



1mg/Kg-dry 25-Sep-2015 18:590.00064Acenaphthene 0.0042U

1mg/Kg-dry 25-Sep-2015 18:590.0013Acenaphthylene 0.0042U

1mg/Kg-dry 25-Sep-2015 18:590.0010Acetophenone 0.0085U

1mg/Kg-dry 25-Sep-2015 18:590.0018Aniline 0.0085U

1mg/Kg-dry 25-Sep-2015 18:590.00064Anthracene 0.0042U

1mg/Kg-dry 25-Sep-2015 18:590.0021Benz(a)anthracene 0.0042U

1mg/Kg-dry 25-Sep-2015 18:59n 0.0015Benzaldehyde 0.0085U

1mg/Kg-dry 25-Sep-2015 18:590.0013Benzo(a)pyrene 0.0042U

1mg/Kg-dry 25-Sep-2015 18:590.0015Benzo(b)fluoranthene 0.0042U

1mg/Kg-dry 25-Sep-2015 18:590.00090Benzo(g,h,i)perylene 0.0042U

1mg/Kg-dry 25-Sep-2015 18:590.0012Benzo(k)fluoranthene 0.0042U

1mg/Kg-dry 25-Sep-2015 18:590.0012Bis(2-chloroethoxy)methane 0.0085U

1mg/Kg-dry 25-Sep-2015 18:590.0014Bis(2-chloroethyl)ether 0.0085U



Page 14 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-01


ANALYTICAL REPORT




1mg/Kg-dry 25-Sep-2015 18:590.0018Bis(2-chloroisopropyl)ether 0.0085U

1mg/Kg-dry 25-Sep-2015 18:590.0022Bis(2-ethylhexyl)phthalate 0.0085U

1mg/Kg-dry 25-Sep-2015 18:590.0017Butyl benzyl phthalate 0.0085U

1mg/Kg-dry 25-Sep-2015 18:590.0015Caprolactam 0.0085U

1mg/Kg-dry 25-Sep-2015 18:590.0015Carbazole 0.0085U

1mg/Kg-dry 25-Sep-2015 18:590.0010Chrysene 0.0042U

1mg/Kg-dry 25-Sep-2015 18:590.0021Dibenz(a,h)anthracene 0.0042U

1mg/Kg-dry 25-Sep-2015 18:590.00090Dibenzofuran 0.0042U

1mg/Kg-dry 25-Sep-2015 18:590.0013Diethyl phthalate 0.0085U

1mg/Kg-dry 25-Sep-2015 18:590.0010Dimethyl phthalate 0.0085U

1mg/Kg-dry 25-Sep-2015 18:590.0015Di-n-butyl phthalate 0.0085U

1mg/Kg-dry 25-Sep-2015 18:590.0012Di-n-octyl phthalate 0.0085U

1mg/Kg-dry 25-Sep-2015 18:590.0014Fluoranthene 0.0042U

1mg/Kg-dry 25-Sep-2015 18:590.0014Fluorene 0.0042U

1mg/Kg-dry 25-Sep-2015 18:590.0012Hexachlorobenzene 0.0085U

1mg/Kg-dry 25-Sep-2015 18:590.0015Hexachlorobutadiene 0.0085U

1mg/Kg-dry 25-Sep-2015 18:590.0010Hexachlorocyclopentadiene 0.0085U

1mg/Kg-dry 25-Sep-2015 18:590.0019Hexachloroethane 0.0085U

1mg/Kg-dry 25-Sep-2015 18:590.0010Indeno(1,2,3-cd)pyrene 0.0042U

1mg/Kg-dry 25-Sep-2015 18:590.0010Isophorone 0.0085U

1mg/Kg-dry 25-Sep-2015 18:590.00077Naphthalene 0.0042U

1mg/Kg-dry 25-Sep-2015 18:590.0012Nitrobenzene 0.0085U

1mg/Kg-dry 25-Sep-2015 18:590.0014N-Nitrosodi-n-propylamine 0.0085U

1mg/Kg-dry 25-Sep-2015 18:590.00090N-Nitrosodiphenylamine 0.0085U

1mg/Kg-dry 25-Sep-2015 18:590.0042Pentachlorophenol 0.0085U

1mg/Kg-dry 25-Sep-2015 18:590.0019Phenanthrene 0.0042U

1mg/Kg-dry 25-Sep-2015 18:590.0014Phenol 0.0085U

1mg/Kg-dry 25-Sep-2015 18:590.00077Pyrene 0.0042U

1mg/Kg-dry 25-Sep-2015 18:590.0012Pyridine 0.0085U

Surr: 2,4,6-Tribromophenol 1%REC 25-Sep-2015 18:5999.5 36-126

Surr: 2-Fluorobiphenyl 1%REC 25-Sep-2015 18:5977.8 43-125

Surr: 2-Fluorophenol 1%REC 25-Sep-2015 18:5985.6 37-125

Surr: 4-Terphenyl-d14 1%REC 25-Sep-2015 18:5982.2 32-125

Surr: Nitrobenzene-d5 1%REC 25-Sep-2015 18:59106 37-125

Surr: Phenol-d6 1%REC 25-Sep-2015 18:5987.3 40-125



Page 15 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-01


ANALYTICAL REPORT



METALS BY SW6020A Method:SW6020 Analyst: JDEPrep:SW3050A / 25-Sep-2015

1mg/Kg-dry 28-Sep-2015 18:300.243Antimony 0.609U

1mg/Kg-dry 28-Sep-2015 18:300.122Arsenic 0.6092.86

1mg/Kg-dry 28-Sep-2015 18:300.0974Barium 0.609141

1mg/Kg-dry 28-Sep-2015 18:300.0609Beryllium 0.6091.21

1mg/Kg-dry 28-Sep-2015 18:300.0609Cadmium 0.609U

1mg/Kg-dry 28-Sep-2015 18:300.110Chromium 0.60913.2

1mg/Kg-dry 28-Sep-2015 18:300.0852Cobalt 0.6099.30

1mg/Kg-dry 28-Sep-2015 18:300.122Copper 0.6097.59

1mg/Kg-dry 28-Sep-2015 18:300.0609Lead 0.60913.0

1mg/Kg-dry 28-Sep-2015 18:300.122Manganese 0.60980.4

1mg/Kg-dry 28-Sep-2015 18:300.110Nickel 0.6097.35

1mg/Kg-dry 28-Sep-2015 18:300.219Selenium 0.6090.742

1mg/Kg-dry 28-Sep-2015 18:300.0974Silver 0.609U

1mg/Kg-dry 28-Sep-2015 18:30J 0.0852Thallium 0.6090.125

1mg/Kg-dry 28-Sep-2015 18:300.280Vanadium 0.60940.7

1mg/Kg-dry 28-Sep-2015 18:300.304Zinc 0.60917.8

MERCURY BY SW7471B Method:SW7471A Analyst: OFOPrep:SW7471A / 28-Sep-2015

1mg/Kg-dry 28-Sep-2015 14:430.000623Mercury 0.004410.00460

TEXAS TPH BY TX1005 Method:TX1005 Analyst: JKPPrep:TX1005PR / 25-Sep-2015

1mg/Kg-dry 28-Sep-2015 10:1011nC6 to nC12 54U

1mg/Kg-dry 28-Sep-2015 10:1011>nC12 to nC28 54U


1mg/Kg-dry 28-Sep-2015 10:1011Total Petroleum Hydrocarbon 54U


Surr: Trifluoromethyl benzene 1%REC 28-Sep-2015 10:1096.3 70-130

MOISTURE Method:SW3550 Analyst: AP1wt% 25-Sep-2015 14:380.0100Percent Moisture 0.010022.3



Page 16 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-02


ANALYTICAL REPORT




















1mg/Kg-dry 29-Sep-2015 10:130.00122-Butanone 0.0090U




1mg/Kg-dry 29-Sep-2015 10:130.0028Acetone 0.018U




















Page 17 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-02


ANALYTICAL REPORT





















Surr: 4-Bromofluorobenzene 1%REC 29-Sep-2015 10:13100 73-126





Page 18 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-02


ANALYTICAL REPORT






1mg/Kg-dry 25-Sep-2015 19:19n 0.00171-Methylnaphthalene 0.0037U











1mg/Kg-dry 25-Sep-2015 19:190.000562-Methylnaphthalene 0.0037U




























Page 19 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-02


ANALYTICAL REPORT





1mg/Kg-dry 25-Sep-2015 19:190.0019Bis(2-ethylhexyl)phthalate 0.0074U




































Page 20 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-02


ANALYTICAL REPORT






1mg/Kg-dry 28-Sep-2015 18:340.0802Barium 0.50130.2






1mg/Kg-dry 28-Sep-2015 18:340.0501Lead 0.5015.09



1mg/Kg-dry 28-Sep-2015 18:34J 0.180Selenium 0.5010.349




1mg/Kg-dry 28-Sep-2015 18:340.251Zinc 0.50115.3


1mg/Kg-dry 28-Sep-2015 14:450.000542Mercury 0.00383U


1mg/Kg-dry 28-Sep-2015 10:398.2nC6 to nC12 41U

1mg/Kg-dry 28-Sep-2015 10:398.2>nC12 to nC28 41U


1mg/Kg-dry 28-Sep-2015 10:398.2Total Petroleum Hydrocarbon 41U






Page 21 of 155


PBW HoustonCES Griggs Rd VCP4904-SB19-16.5

WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-03


ANALYTICAL REPORT












































Page 22 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-03


ANALYTICAL REPORT


























Page 23 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-03


ANALYTICAL REPORT




































1mg/Kg-dry 25-Sep-2015 19:38Jn 0.0013Benzaldehyde 0.00690.0018









Page 24 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-03


ANALYTICAL REPORT





1mg/Kg-dry 25-Sep-2015 19:38J 0.0018Bis(2-ethylhexyl)phthalate 0.00690.0028


1mg/Kg-dry 25-Sep-2015 19:380.0013Caprolactam 0.00690.014


1mg/Kg-dry 25-Sep-2015 19:38J 0.00084Chrysene 0.00350.0011





1mg/Kg-dry 25-Sep-2015 19:38J 0.0013Di-n-butyl phthalate 0.00690.0014


1mg/Kg-dry 25-Sep-2015 19:380.0012Fluoranthene 0.00350.0052













1mg/Kg-dry 25-Sep-2015 19:380.0016Phenanthrene 0.00350.0063


1mg/Kg-dry 25-Sep-2015 19:38J 0.00063Pyrene 0.00350.0021










Page 25 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-03


ANALYTICAL REPORT







1mg/Kg-dry 28-Sep-2015 18:39J 0.0482Beryllium 0.4820.275





1mg/Kg-dry 28-Sep-2015 18:390.0482Lead 0.4822.76





1mg/Kg-dry 28-Sep-2015 18:390.0674Thallium 0.482U


1mg/Kg-dry 28-Sep-2015 18:390.241Zinc 0.4827.77













Page 26 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-04


ANALYTICAL REPORT

























1mg/Kg-dry 29-Sep-2015 12:33J 0.00050Benzene 0.00500.0020



















Page 27 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-04


ANALYTICAL REPORT













1mg/Kg-dry 29-Sep-2015 12:33J 0.00060Toluene 0.00500.0019













Page 28 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-04


ANALYTICAL REPORT
































1mg/Kg-dry 25-Sep-2015 19:57J 0.0010Acetophenone 0.00830.0011






1mg/Kg-dry 25-Sep-2015 19:57J 0.0015Benzo(b)fluoranthene 0.00410.0016







Page 29 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-04


ANALYTICAL REPORT












1mg/Kg-dry 25-Sep-2015 19:57J 0.0013Diethyl phthalate 0.00830.0019


















1mg/Kg-dry 25-Sep-2015 19:57J 0.0014Phenol 0.00830.0015



Surr: 2,4,6-Tribromophenol 1%REC 25-Sep-2015 19:57102 36-126




Surr: Nitrobenzene-d5 1%REC 25-Sep-2015 19:5794.1 37-125

Surr: Phenol-d6 1%REC 25-Sep-2015 19:57113 40-125



Page 30 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-04


ANALYTICAL REPORT








1mg/Kg-dry 28-Sep-2015 18:43J 0.0583Cadmium 0.5830.0954




1mg/Kg-dry 28-Sep-2015 18:430.0583Lead 0.58318.6

1mg/Kg-dry 28-Sep-2015 18:430.117Manganese 0.583180



1mg/Kg-dry 28-Sep-2015 18:43J 0.0932Silver 0.5830.138



1mg/Kg-dry 28-Sep-2015 18:430.291Zinc 0.58326.6









Surr: Trifluoromethyl benzene 1%REC 28-Sep-2015 11:38100 70-130




Page 31 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-05


ANALYTICAL REPORT












































Page 32 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-05


ANALYTICAL REPORT


























Page 33 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-05


ANALYTICAL REPORT













































Page 34 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-05


ANALYTICAL REPORT









































Page 35 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-05


ANALYTICAL REPORT












1mg/Kg-dry 28-Sep-2015 18:470.0590Lead 0.5908.87







1mg/Kg-dry 28-Sep-2015 18:470.295Zinc 0.59023.9


1mg/Kg-dry 28-Sep-2015 14:51J 0.000615Mercury 0.004350.00174











Page 36 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-06


ANALYTICAL REPORT












































Page 37 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-06


ANALYTICAL REPORT


























Page 38 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-06


ANALYTICAL REPORT













































Page 39 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-06


ANALYTICAL REPORT





1mg/Kg-dry 25-Sep-2015 20:350.0018Bis(2-ethylhexyl)phthalate 0.00720.012





























Surr: 2-Fluorobiphenyl 1%REC 25-Sep-2015 20:35103 43-125

Surr: 2-Fluorophenol 1%REC 25-Sep-2015 20:35112 37-125






Page 40 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-06


ANALYTICAL REPORT












1mg/Kg-dry 28-Sep-2015 18:520.0522Lead 0.5223.91







1mg/Kg-dry 28-Sep-2015 18:520.261Zinc 0.52212.8













Page 41 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-07


ANALYTICAL REPORT












1mg/Kg-dry 29-Sep-2015 13:44J 0.00111,2,4-Trimethylbenzene 0.00510.0050













1mg/Kg-dry 29-Sep-2015 13:440.00051Benzene 0.00510.012















1mg/Kg-dry 29-Sep-2015 13:44J 0.00071Ethylbenzene 0.00510.0013




Page 42 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-07


ANALYTICAL REPORT



VOLATILES BY SW8260C Method:SW8260 Analyst: WLR1mg/Kg-dry 29-Sep-2015 13:440.00051Methyl tert-butyl ether 0.00510.0070





1mg/Kg-dry 29-Sep-2015 13:44J 0.00092n-Propylbenzene 0.00510.0043











1mg/Kg-dry 29-Sep-2015 13:44J 0.0024Xylenes, Total 0.0100.0039







Page 43 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-07


ANALYTICAL REPORT













































Page 44 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-07


ANALYTICAL REPORT




































Surr: 4-Terphenyl-d14 1%REC 25-Sep-2015 22:31103 32-125





Page 45 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-07


ANALYTICAL REPORT












1mg/Kg-dry 28-Sep-2015 18:560.0604Lead 0.6048.77







1mg/Kg-dry 28-Sep-2015 18:560.302Zinc 0.60420.8













Page 46 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-08


ANALYTICAL REPORT












































Page 47 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-08


ANALYTICAL REPORT


























Page 48 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-08


ANALYTICAL REPORT













































Page 49 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-08


ANALYTICAL REPORT









































Page 50 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-08


ANALYTICAL REPORT












1mg/Kg-dry 28-Sep-2015 19:010.0619Lead 0.6199.18







1mg/Kg-dry 28-Sep-2015 19:010.310Zinc 0.61919.6










MOISTURE Method:SW3550 Analyst: JHD1wt% 30-Sep-2015 10:270.0100Percent Moisture 0.010023.9



Page 51 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-09


ANALYTICAL REPORT












































Page 52 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-09


ANALYTICAL REPORT


























Page 53 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-09


ANALYTICAL REPORT













































Page 54 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-09


ANALYTICAL REPORT









































Page 55 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-09


ANALYTICAL REPORT












1mg/Kg-dry 28-Sep-2015 14:420.0510Lead 0.5106.38







1mg/Kg-dry 28-Sep-2015 16:540.255Zinc 0.51011.1













Page 56 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-10


ANALYTICAL REPORT












































Page 57 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-10


ANALYTICAL REPORT


























Page 58 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-10


ANALYTICAL REPORT













































Page 59 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-10


ANALYTICAL REPORT



































Surr: 2-Fluorophenol 1%REC 25-Sep-2015 23:09100 37-125






Page 60 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-10


ANALYTICAL REPORT




1mg/Kg-dry 28-Sep-2015 19:05J 0.252Antimony 0.6300.324








1mg/Kg-dry 28-Sep-2015 19:050.0630Lead 0.63023.1







1mg/Kg-dry 28-Sep-2015 19:050.315Zinc 0.630151













Page 61 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-11


ANALYTICAL REPORT












































Page 62 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-11


ANALYTICAL REPORT


























Page 63 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-11


ANALYTICAL REPORT













































Page 64 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-11


ANALYTICAL REPORT









































Page 65 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-11


ANALYTICAL REPORT












1mg/Kg-dry 28-Sep-2015 19:180.0591Lead 0.59115.5







1mg/Kg-dry 28-Sep-2015 19:180.295Zinc 0.59115.8













Page 66 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-12


ANALYTICAL REPORT












































Page 67 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-12


ANALYTICAL REPORT


























Page 68 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-12


ANALYTICAL REPORT













































Page 69 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-12


ANALYTICAL REPORT









































Page 70 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-12


ANALYTICAL REPORT












1mg/Kg-dry 28-Sep-2015 19:230.0524Lead 0.5244.32







1mg/Kg-dry 28-Sep-2015 19:230.262Zinc 0.52412.5













Page 71 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-13


ANALYTICAL REPORT












































Page 72 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-13


ANALYTICAL REPORT


























Page 73 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-13


ANALYTICAL REPORT













































Page 74 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-13


ANALYTICAL REPORT









































Page 75 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-13


ANALYTICAL REPORT












1mg/Kg-dry 28-Sep-2015 19:270.0618Lead 0.61812.1







1mg/Kg-dry 28-Sep-2015 19:270.309Zinc 0.61818.5













Page 76 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-14


ANALYTICAL REPORT












































Page 77 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-14


ANALYTICAL REPORT


























Page 78 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-14


ANALYTICAL REPORT













































Page 79 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-14


ANALYTICAL REPORT









































Page 80 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-14


ANALYTICAL REPORT












1mg/Kg-dry 28-Sep-2015 19:310.0520Lead 0.5205.13







1mg/Kg-dry 28-Sep-2015 19:310.260Zinc 0.52012.1













Page 81 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-15


ANALYTICAL REPORT












































Page 82 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-15


ANALYTICAL REPORT


























Page 83 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-15


ANALYTICAL REPORT













































Page 84 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-15


ANALYTICAL REPORT









































Page 85 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-15


ANALYTICAL REPORT












1mg/Kg-dry 28-Sep-2015 19:360.0559Lead 0.5594.24







1mg/Kg-dry 28-Sep-2015 19:360.279Zinc 0.55911.4













Page 86 of 155


PBW HoustonCES Griggs Rd VCPTB01 092215

WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-16

22-Sep-2015 17:00 Matrix:Water

ANALYTICAL REPORT



LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: AKP1mg/L 25-Sep-2015 01:420.000301,1,1,2-Tetrachloroethane 0.0010U

1mg/L 25-Sep-2015 01:420.000201,1,1-Trichloroethane 0.0010U

1mg/L 25-Sep-2015 01:420.000501,1,2,2-Tetrachloroethane 0.0010U

1mg/L 25-Sep-2015 01:420.00101,1,2-Trichlor-1,2,2-trifluoroethane 0.0010U


1mg/L 25-Sep-2015 01:420.000201,1-Dichloroethane 0.0010U

1mg/L 25-Sep-2015 01:420.000201,1-Dichloroethene 0.0010U

1mg/L 25-Sep-2015 01:420.000401,2,3-Trichlorobenzene 0.0010U


1mg/L 25-Sep-2015 01:420.000301,2,4-Trimethylbenzene 0.0010U

1mg/L 25-Sep-2015 01:420.000201,2-Dibromoethane 0.0010U

1mg/L 25-Sep-2015 01:420.000501,2-Dichlorobenzene 0.0010U


1mg/L 25-Sep-2015 01:420.000501,2-Dichloropropane 0.0010U




1mg/L 25-Sep-2015 01:420.000502-Butanone 0.0020U

1mg/L 25-Sep-2015 01:420.00102-Hexanone 0.0020U

1mg/L 25-Sep-2015 01:420.000304-Isopropyltoluene 0.0010U

1mg/L 25-Sep-2015 01:420.000704-Methyl-2-pentanone 0.0020U

1mg/L 25-Sep-2015 01:420.0020Acetone 0.0020U

1mg/L 25-Sep-2015 01:420.00020Benzene 0.0010U

1mg/L 25-Sep-2015 01:420.00020Bromodichloromethane 0.0010U

1mg/L 25-Sep-2015 01:420.00040Bromoform 0.0010U

1mg/L 25-Sep-2015 01:420.00040Bromomethane 0.0010U

1mg/L 25-Sep-2015 01:420.00060Carbon disulfide 0.0020U

1mg/L 25-Sep-2015 01:420.00050Carbon tetrachloride 0.0010U

1mg/L 25-Sep-2015 01:420.00030Chlorobenzene 0.0010U

1mg/L 25-Sep-2015 01:420.00030Chloroethane 0.0010U

1mg/L 25-Sep-2015 01:420.00020Chloroform 0.0010U

1mg/L 25-Sep-2015 01:420.00020Chloromethane 0.0010U

1mg/L 25-Sep-2015 01:420.00020cis-1,2-Dichloroethene 0.0010U

1mg/L 25-Sep-2015 01:420.00010cis-1,3-Dichloropropene 0.0010U

1mg/L 25-Sep-2015 01:42n 0.00030Cyclohexane 0.0010U

1mg/L 25-Sep-2015 01:420.00030Dibromochloromethane 0.0010U

1mg/L 25-Sep-2015 01:420.00030Dichlorodifluoromethane 0.0010U

1mg/L 25-Sep-2015 01:420.00030Ethylbenzene 0.0010U

1mg/L 25-Sep-2015 01:420.00030Isopropylbenzene 0.0010U



Page 87 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-16


ANALYTICAL REPORT



LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: AKP1mg/L 25-Sep-2015 01:420.00020Methyl tert-butyl ether 0.0010U

1mg/L 25-Sep-2015 01:420.00030Methylcyclohexane 0.0010U

1mg/L 25-Sep-2015 01:420.0010Methylene chloride 0.0020U

1mg/L 25-Sep-2015 01:420.00030Naphthalene 0.0010U

1mg/L 25-Sep-2015 01:420.00040n-Butylbenzene 0.0010U

1mg/L 25-Sep-2015 01:420.00030n-Propylbenzene 0.0010U

1mg/L 25-Sep-2015 01:420.00030sec-Butylbenzene 0.0010U

1mg/L 25-Sep-2015 01:420.00030Styrene 0.0010U

1mg/L 25-Sep-2015 01:420.00030tert-Butylbenzene 0.0010U

1mg/L 25-Sep-2015 01:420.00030Tetrachloroethene 0.0010U

1mg/L 25-Sep-2015 01:420.00020Toluene 0.0010U

1mg/L 25-Sep-2015 01:420.00020trans-1,2-Dichloroethene 0.0010U

1mg/L 25-Sep-2015 01:420.00020trans-1,3-Dichloropropene 0.0010U

1mg/L 25-Sep-2015 01:420.00020Trichloroethene 0.0010U

1mg/L 25-Sep-2015 01:420.00030Trichlorofluoromethane 0.0010U

1mg/L 25-Sep-2015 01:420.00020Vinyl chloride 0.0010U

1mg/L 25-Sep-2015 01:420.00050Xylenes, Total 0.0030U

Surr: 1,2-Dichloroethane-d4 1%REC 25-Sep-2015 01:42100 71-125


Surr: Dibromofluoromethane 1%REC 25-Sep-2015 01:42102 74-125

Surr: Toluene-d8 1%REC 25-Sep-2015 01:4299.3 75-125



Page 88 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-17


ANALYTICAL REPORT
























1mg/L 25-Sep-2015 02:070.0020Acetone 0.0020U

1mg/L 25-Sep-2015 02:070.00020Benzene 0.0010U



















Page 89 of 155



WorkOrder:Lab ID:

Collection Date:

HS15091001HS15091001-17


ANALYTICAL REPORT










1mg/L 25-Sep-2015 02:070.00030Styrene 0.0010U



1mg/L 25-Sep-2015 02:070.00020Toluene 0.0010U













Page 90 of 155

WEIGHT LOG



Batch ID: 547 Method: VOLATILES BY SW8260C

ContainerSampIDContainer Type

Sample Wt/Vol

Final Volume

Weight Factor

HS15091001-01 2 6.015 (g) TerraCore (5035A)5 (mL) 0.83HS15091001-02 2 6.262 (g) TerraCore (5035A)5 (mL) 0.8HS15091001-03 2 5.793 (g) TerraCore (5035A)5 (mL) 0.86HS15091001-04 2 6.249 (g) TerraCore (5035A)5 (mL) 0.8HS15091001-05 2 6.204 (g) TerraCore (5035A)5 (mL) 0.81HS15091001-06 2 5.294 (g) TerraCore (5035A)5 (mL) 0.94HS15091001-07 2 6.231 (g) TerraCore (5035A)5 (mL) 0.8HS15091001-08 2 6.119 (g) TerraCore (5035A)5 (mL) 0.82HS15091001-09 4 5.341 (g) TerraCore (5035A)5 (mL) 0.94HS15091001-10 2 6.659 (g) TerraCore (5035A)5 (mL) 0.75HS15091001-11 2 6.412 (g) TerraCore (5035A)5 (mL) 0.78HS15091001-12 2 5.267 (g) TerraCore (5035A)5 (mL) 0.95HS15091001-13 2 5.534 (g) TerraCore (5035A)5 (mL) 0.9HS15091001-14 2 6.853 (g) TerraCore (5035A)5 (mL) 0.73HS15091001-15 2 5.17 (g) TerraCore (5035A)5 (mL) 0.97

Batch ID: 97408 Method: LOW-LEVEL SEMIVOLATILES 3541_B_LOWPrep:

ContainerSampIDSample Wt/Vol

Final Volume

Prep Factor

HS15091001-01 1 30.04 1 (mL) 0.03329HS15091001-02 1 30.02 1 (mL) 0.03331HS15091001-03 1 30.07 1 (mL) 0.03326HS15091001-04 1 30.01 1 (mL) 0.03332HS15091001-05 1 30.04 1 (mL) 0.03329HS15091001-06 1 30.08 1 (mL) 0.03324HS15091001-07 1 30.03 1 (mL) 0.0333HS15091001-08 1 30.02 1 (mL) 0.03331HS15091001-09 1 30.08 1 (mL) 0.03324HS15091001-10 1 30.03 1 (mL) 0.0333HS15091001-11 1 30.09 1 (mL) 0.03323HS15091001-12 1 30.01 1 (mL) 0.03332HS15091001-13 1 30.04 1 (mL) 0.03329HS15091001-14 1 30.06 1 (mL) 0.03327HS15091001-15 1 30.03 1 (mL) 0.0333


Page 91 of 155

WEIGHT LOG



Batch ID: 97448 Method: METALS BY SW6020A 3050_I_LOWPrep:


Final Volume

Prep Factor


Batch ID: 97451 Method: TEXAS TPH BY TX1005 TX 1005_S PRPrep:


Final Volume

Prep Factor



Page 92 of 155

WEIGHT LOG



Batch ID: 97509 Method: MERCURY BY SW7471B HG_S_LOWPRPrep:


Final Volume

Prep Factor



Page 93 of 155

Client:CES Griggs Rd VCPPBW Houston

WorkOrder:Project:

HS15091001DATES REPORT

Collection Date Prep Date Analysis DateClient Samp IDSample ID TCLP Date DF

Batch ID 97408 Test Name : LOW-LEVEL SEMIVOLATILES Matrix: Soil

24 Sep 2015 14:02 25 Sep 2015 18:59HS15091001-01 23 Sep 2015 15:20 14904-SB19-03

24 Sep 2015 14:02 25 Sep 2015 19:19HS15091001-02 22 Sep 2015 15:25 14904-SB19-14

24 Sep 2015 14:02 25 Sep 2015 19:38HS15091001-03 22 Sep 2015 15:25 14904-SB19-16.5

24 Sep 2015 14:02 25 Sep 2015 19:57HS15091001-04 22 Sep 2015 10:35 14904-SB20-02

24 Sep 2015 14:02 28 Sep 2015 21:06HS15091001-05 22 Sep 2015 10:35 14904-SB20-07

24 Sep 2015 14:02 25 Sep 2015 20:35HS15091001-06 22 Sep 2015 10:40 14904-SB20-19

24 Sep 2015 14:02 25 Sep 2015 22:31HS15091001-07 22 Sep 2015 14:10 14904-SB21-04

24 Sep 2015 14:02 25 Sep 2015 22:50HS15091001-08 22 Sep 2015 14:20 14904-SB21-10

24 Sep 2015 14:02 24 Sep 2015 17:13HS15091001-09 22 Sep 2015 14:25 14904-SB21-16.5

24 Sep 2015 14:02 25 Sep 2015 23:09HS15091001-10 22 Sep 2015 16:35 14904-SB22-03

24 Sep 2015 14:02 25 Sep 2015 20:55HS15091001-11 22 Sep 2015 16:45 14904-SB22-05

24 Sep 2015 14:02 25 Sep 2015 21:14HS15091001-12 22 Sep 2015 16:50 14904-SB22-20

24 Sep 2015 14:02 25 Sep 2015 21:33HS15091001-13 22 Sep 2015 12:15 14904-SB23-04

24 Sep 2015 14:02 25 Sep 2015 21:52HS15091001-14 22 Sep 2015 12:20 14904-SB23-10

24 Sep 2015 14:02 25 Sep 2015 22:11HS15091001-15 22 Sep 2015 12:15 14904-SB23-19

Batch ID 97448 Test Name : METALS BY SW6020A Matrix: Soil

25 Sep 2015 08:19 28 Sep 2015 18:30HS15091001-01 23 Sep 2015 15:20 14904-SB19-03

25 Sep 2015 08:19 28 Sep 2015 18:34HS15091001-02 22 Sep 2015 15:25 14904-SB19-14

25 Sep 2015 08:19 28 Sep 2015 18:39HS15091001-03 22 Sep 2015 15:25 14904-SB19-16.5

25 Sep 2015 08:19 29 Sep 2015 11:27HS15091001-04 22 Sep 2015 10:35 24904-SB20-02

25 Sep 2015 08:19 28 Sep 2015 18:43HS15091001-04 22 Sep 2015 10:35 14904-SB20-02

25 Sep 2015 08:19 28 Sep 2015 18:47HS15091001-05 22 Sep 2015 10:35 14904-SB20-07

25 Sep 2015 08:19 28 Sep 2015 18:52HS15091001-06 22 Sep 2015 10:40 14904-SB20-19

25 Sep 2015 08:19 28 Sep 2015 18:56HS15091001-07 22 Sep 2015 14:10 14904-SB21-04

25 Sep 2015 08:19 28 Sep 2015 19:01HS15091001-08 22 Sep 2015 14:20 14904-SB21-10

25 Sep 2015 08:19 28 Sep 2015 16:54HS15091001-09 22 Sep 2015 14:25 14904-SB21-16.5

25 Sep 2015 08:19 28 Sep 2015 14:42HS15091001-09 22 Sep 2015 14:25 14904-SB21-16.5

25 Sep 2015 08:19 28 Sep 2015 19:05HS15091001-10 22 Sep 2015 16:35 14904-SB22-03

25 Sep 2015 08:19 28 Sep 2015 19:18HS15091001-11 22 Sep 2015 16:45 14904-SB22-05

25 Sep 2015 08:19 28 Sep 2015 19:23HS15091001-12 22 Sep 2015 16:50 14904-SB22-20

25 Sep 2015 08:19 28 Sep 2015 19:27HS15091001-13 22 Sep 2015 12:15 14904-SB23-04

25 Sep 2015 08:19 28 Sep 2015 19:31HS15091001-14 22 Sep 2015 12:20 14904-SB23-10

25 Sep 2015 08:19 28 Sep 2015 19:36HS15091001-15 22 Sep 2015 12:15 14904-SB23-19


Page 94 of 155


WorkOrder:Project:



Batch ID 97451 Test Name : TEXAS TPH BY TX1005 Matrix: Soil

25 Sep 2015 10:30 28 Sep 2015 10:10HS15091001-01 23 Sep 2015 15:20 14904-SB19-03

25 Sep 2015 10:30 28 Sep 2015 10:39HS15091001-02 22 Sep 2015 15:25 14904-SB19-14

25 Sep 2015 10:30 28 Sep 2015 11:09HS15091001-03 22 Sep 2015 15:25 14904-SB19-16.5

25 Sep 2015 10:30 28 Sep 2015 11:38HS15091001-04 22 Sep 2015 10:35 14904-SB20-02

25 Sep 2015 10:30 28 Sep 2015 12:07HS15091001-05 22 Sep 2015 10:35 14904-SB20-07

25 Sep 2015 10:30 28 Sep 2015 12:36HS15091001-06 22 Sep 2015 10:40 14904-SB20-19

25 Sep 2015 10:30 28 Sep 2015 14:28HS15091001-07 22 Sep 2015 14:10 14904-SB21-04

25 Sep 2015 10:30 28 Sep 2015 14:57HS15091001-08 22 Sep 2015 14:20 14904-SB21-10

25 Sep 2015 10:30 28 Sep 2015 15:26HS15091001-09 22 Sep 2015 14:25 14904-SB21-16.5

25 Sep 2015 10:30 28 Sep 2015 18:50HS15091001-10 22 Sep 2015 16:35 14904-SB22-03

25 Sep 2015 10:30 28 Sep 2015 19:20HS15091001-11 22 Sep 2015 16:45 14904-SB22-05

25 Sep 2015 10:30 28 Sep 2015 19:49HS15091001-12 22 Sep 2015 16:50 14904-SB22-20

25 Sep 2015 10:30 28 Sep 2015 20:18HS15091001-13 22 Sep 2015 12:15 14904-SB23-04

25 Sep 2015 10:30 28 Sep 2015 20:47HS15091001-14 22 Sep 2015 12:20 14904-SB23-10

25 Sep 2015 10:30 28 Sep 2015 21:17HS15091001-15 22 Sep 2015 12:15 14904-SB23-19

Batch ID 97509 Test Name : MERCURY BY SW7471B Matrix: Soil

28 Sep 2015 10:15 28 Sep 2015 14:43HS15091001-01 23 Sep 2015 15:20 14904-SB19-03

28 Sep 2015 10:15 28 Sep 2015 14:45HS15091001-02 22 Sep 2015 15:25 14904-SB19-14

28 Sep 2015 10:15 28 Sep 2015 14:47HS15091001-03 22 Sep 2015 15:25 14904-SB19-16.5

28 Sep 2015 10:15 28 Sep 2015 14:49HS15091001-04 22 Sep 2015 10:35 14904-SB20-02

28 Sep 2015 10:15 28 Sep 2015 14:51HS15091001-05 22 Sep 2015 10:35 14904-SB20-07

28 Sep 2015 10:15 28 Sep 2015 14:53HS15091001-06 22 Sep 2015 10:40 14904-SB20-19

28 Sep 2015 10:15 28 Sep 2015 14:55HS15091001-07 22 Sep 2015 14:10 14904-SB21-04

28 Sep 2015 10:15 28 Sep 2015 15:01HS15091001-08 22 Sep 2015 14:20 14904-SB21-10

28 Sep 2015 10:15 28 Sep 2015 14:25HS15091001-09 22 Sep 2015 14:25 14904-SB21-16.5

28 Sep 2015 10:15 28 Sep 2015 15:03HS15091001-10 22 Sep 2015 16:35 14904-SB22-03

28 Sep 2015 10:15 28 Sep 2015 15:05HS15091001-11 22 Sep 2015 16:45 14904-SB22-05

28 Sep 2015 10:15 28 Sep 2015 15:07HS15091001-12 22 Sep 2015 16:50 14904-SB22-20

28 Sep 2015 10:15 28 Sep 2015 15:08HS15091001-13 22 Sep 2015 12:15 14904-SB23-04

28 Sep 2015 10:15 28 Sep 2015 15:10HS15091001-14 22 Sep 2015 12:20 14904-SB23-10

28 Sep 2015 10:15 28 Sep 2015 15:12HS15091001-15 22 Sep 2015 12:15 14904-SB23-19

Batch ID R261899 Test Name : LOW LEVEL VOLATILES BY SW8260C Matrix: Water

25 Sep 2015 01:42HS15091001-16 22 Sep 2015 17:00 1TB01 092215

25 Sep 2015 02:07HS15091001-17 22 Sep 2015 17:05 1TB02 092215


Page 95 of 155


WorkOrder:Project:



Batch ID R262070 Test Name : MOISTURE Matrix: Soil

25 Sep 2015 14:38HS15091001-01 23 Sep 2015 15:20 14904-SB19-03

25 Sep 2015 14:38HS15091001-02 22 Sep 2015 15:25 14904-SB19-14

25 Sep 2015 14:38HS15091001-03 22 Sep 2015 15:25 14904-SB19-16.5

25 Sep 2015 14:38HS15091001-04 22 Sep 2015 10:35 14904-SB20-02

25 Sep 2015 14:38HS15091001-05 22 Sep 2015 10:35 14904-SB20-07

25 Sep 2015 14:38HS15091001-06 22 Sep 2015 10:40 14904-SB20-19

25 Sep 2015 14:38HS15091001-07 22 Sep 2015 14:10 14904-SB21-04

Batch ID R262131 Test Name : VOLATILES BY SW8260C Matrix: Soil

29 Sep 2015 09:49HS15091001-01 23 Sep 2015 15:20 14904-SB19-03

29 Sep 2015 10:13HS15091001-02 22 Sep 2015 15:25 14904-SB19-14

29 Sep 2015 10:36HS15091001-03 22 Sep 2015 15:25 14904-SB19-16.5

29 Sep 2015 12:33HS15091001-04 22 Sep 2015 10:35 14904-SB20-02

29 Sep 2015 12:57HS15091001-05 22 Sep 2015 10:35 14904-SB20-07

29 Sep 2015 13:20HS15091001-06 22 Sep 2015 10:40 14904-SB20-19

29 Sep 2015 13:44HS15091001-07 22 Sep 2015 14:10 14904-SB21-04

29 Sep 2015 14:08HS15091001-08 22 Sep 2015 14:20 14904-SB21-10

29 Sep 2015 11:00HS15091001-09 22 Sep 2015 14:25 14904-SB21-16.5

29 Sep 2015 14:31HS15091001-10 22 Sep 2015 16:35 14904-SB22-03

29 Sep 2015 14:54HS15091001-11 22 Sep 2015 16:45 14904-SB22-05

29 Sep 2015 15:18HS15091001-12 22 Sep 2015 16:50 14904-SB22-20

29 Sep 2015 15:42HS15091001-13 22 Sep 2015 12:15 14904-SB23-04

29 Sep 2015 16:05HS15091001-14 22 Sep 2015 12:20 14904-SB23-10

29 Sep 2015 16:29HS15091001-15 22 Sep 2015 12:15 14904-SB23-19


29 Sep 2015 12:22HS15091001-10 22 Sep 2015 16:35 14904-SB22-03

29 Sep 2015 12:22HS15091001-11 22 Sep 2015 16:45 14904-SB22-05

29 Sep 2015 12:22HS15091001-12 22 Sep 2015 16:50 14904-SB22-20

29 Sep 2015 12:22HS15091001-13 22 Sep 2015 12:15 14904-SB23-04

29 Sep 2015 12:22HS15091001-14 22 Sep 2015 12:20 14904-SB23-10

29 Sep 2015 12:22HS15091001-15 22 Sep 2015 12:15 14904-SB23-19


30 Sep 2015 10:27HS15091001-08 22 Sep 2015 14:20 14904-SB21-10

30 Sep 2015 10:27HS15091001-09 22 Sep 2015 14:25 14904-SB21-16.5


Page 96 of 155


WorkOrder: HS15091001

Test Code: TX1005_S_REV3InstrumentID: FID-10

METHOD DETECTION / REPORTING LIMITS

SolidMatrix:Test Number: TX1005Test Name: Texas TPH by TX1005

Units: mg/Kg

Type Analyte DCSCAS MDL PQLDCS SpikeA 22TPHGRO 10nC6 to nC12 5025

A 22TPHDRO 10>nC12 to nC28 5025

A 4910W40MOTOROIL 10>nC28 to nC35 5025

A 71TPH 10Total Petroleum Hydrocarbon 5050

S 0321-60-8 02-Fluorobiphenyl 00

S 098-08-8 0Trifluoromethyl benzene 00

Page 97 of 155



Test Code: HG_S_LOWInstrumentID: HG02


SolidMatrix:Test Number: SW7471ATest Name: Mercury by SW7471B

Units: mg/Kg

Type Analyte DCSCAS MDL PQLDCS SpikeA 0.0007337439-97-6 0.000470Mercury 0.003320.000833

Page 98 of 155



Test Code: ICP_S_LowInstrumentID: ICPMS04


SolidMatrix:Test Number: SW6020Test Name: Metals by SW6020A

Units: mg/Kg

Type Analyte DCSCAS MDL PQLDCS SpikeA 0.2297440-36-0 0.200Antimony 0.5000.250

A 0.2627440-38-2 0.100Arsenic 0.5000.250

A 0.2447440-39-3 0.0800Barium 0.5000.250

A 0.2017440-41-7 0.0500Beryllium 0.5000.250

A 0.2597440-43-9 0.0500Cadmium 0.5000.250

A 0.2917440-47-3 0.0900Chromium 0.5000.250

A 0.2637440-48-4 0.0700Cobalt 0.5000.250

A 0.2027440-50-8 0.100Copper 0.5000.250

A 0.2447439-92-1 0.0500Lead 0.5000.250

A 0.2707439-96-5 0.100Manganese 0.5000.250

A 0.2637440-02-0 0.0900Nickel 0.5000.250

A 0.3147782-49-2 0.180Selenium 0.5000.250

A 0.2437440-22-4 0.0800Silver 0.5000.250

A 0.2397440-28-0 0.0700Thallium 0.5000.250

A 0.3277440-62-2 0.230Vanadium 0.5000.250

A 0.3267440-66-6 0.250Zinc 0.5000.250

Page 99 of 155



Test Code: 8270_LOW_SInstrumentID: SV-6


SolidMatrix:Test Number: SW8270Test Name: Low-Level Semivolatiles

Units: mg/Kg

Type Analyte DCSCAS MDL PQLDCS SpikeA 0.003592-52-4 0.00171,1´-Biphenyl 0.00660.0033

A 0.001995-94-3 0.00101,2,4,5-Tetrachlorobenzene 0.00660.0033

A 0.001890-12-0 0.00151-Methylnaphthalene 0.00330.0017

A 0.002958-90-2 0.00292,3,4,6-Tetrachlorophenol 0.00660.0033

A 0.003195-95-4 0.00252,4,5-Trichlorophenol 0.00660.0033


A 0.0027120-83-2 0.00132,4-Dichlorophenol 0.00660.0033

A 0.0025105-67-9 0.00332,4-Dimethylphenol 0.00660.0033

A 0.004051-28-5 0.00452,4-Dinitrophenol 0.0130.0033

A 0.0030121-14-2 0.000902,4-Dinitrotoluene 0.00660.0033


A 0.003391-58-7 0.00132-Chloronaphthalene 0.00660.0033

A 0.003095-57-8 0.00132-Chlorophenol 0.00660.0033


A 0.002895-48-7 0.00112-Methylphenol 0.00660.0033

A 0.003688-74-4 0.00192-Nitroaniline 0.00660.0033

A 0.003288-75-5 0.00252-Nitrophenol 0.00660.0033

A 0.00253/4-CRESOL 0.00103&4-Methylphenol 0.00660.0033

A 0.003091-94-1 0.00253,3´-Dichlorobenzidine 0.00660.0033

A 0.003199-09-2 0.00193-Nitroaniline 0.00660.0033

A 0.0040534-52-1 0.00214,6-Dinitro-2-methylphenol 0.00660.0033

A 0.0029101-55-3 0.00164-Bromophenyl phenyl ether 0.00660.0033

A 0.003359-50-7 0.000704-Chloro-3-methylphenol 0.00660.0033

A 0.00337005-72-3 0.00154-Chlorophenyl phenyl ether 0.00660.0033

A 0.0034100-01-6 0.00224-Nitroaniline 0.00660.0033

A 0.0022100-02-7 0.00194-Nitrophenol 0.0130.0033

A 0.002083-32-9 0.00050Acenaphthene 0.00330.0017

A 0.0020208-96-8 0.0010Acenaphthylene 0.00330.0017

A 0.003398-86-2 0.00080Acetophenone 0.00660.0033

A 0.002662-53-3 0.0014Aniline 0.00660.0033

A 0.0017120-12-7 0.00050Anthracene 0.00330.0017

A 0.001956-55-3 0.0016Benz(a)anthracene 0.00330.0017

A 0.0036100-52-7 0.0012Benzaldehyde 0.00660.0033

A 0.001650-32-8 0.0010Benzo(a)pyrene 0.00330.0017

A 0.0016205-99-2 0.0012Benzo(b)fluoranthene 0.00330.0017

A 0.0017191-24-2 0.00070Benzo(g,h,i)perylene 0.00330.0017

A 0.0016207-08-9 0.00090Benzo(k)fluoranthene 0.00330.0017

A 0.0032111-91-1 0.00090Bis(2-chloroethoxy)methane 0.00660.0033

A 0.0035111-44-4 0.0011Bis(2-chloroethyl)ether 0.00660.0033

A 0.0034108-60-1 0.0014Bis(2-chloroisopropyl)ether 0.00660.0033

A 0.0033117-81-7 0.0017Bis(2-ethylhexyl)phthalate 0.00660.0033

Page 100 of 155






Units: mg/Kg

Type Analyte DCSCAS MDL PQLDCS SpikeA 0.003785-68-7 0.0013Butyl benzyl phthalate 0.00660.0033

A 0.0016105-60-2 0.0012Caprolactam 0.00660.0033

A 0.003286-74-8 0.0012Carbazole 0.00660.0033

A 0.0019218-01-9 0.00080Chrysene 0.00330.0017

A 0.001653-70-3 0.0016Dibenz(a,h)anthracene 0.00330.0017

A 0.0034132-64-9 0.00070Dibenzofuran 0.00330.0033

A 0.003484-66-2 0.0010Diethyl phthalate 0.00660.0033

A 0.0033131-11-3 0.00080Dimethyl phthalate 0.00660.0033

A 0.003184-74-2 0.0012Di-n-butyl phthalate 0.00660.0033

A 0.0031117-84-0 0.00090Di-n-octyl phthalate 0.00660.0033

A 0.0017206-44-0 0.0011Fluoranthene 0.00330.0017

A 0.001986-73-7 0.0011Fluorene 0.00330.0017

A 0.0029118-74-1 0.00090Hexachlorobenzene 0.00660.0033

A 0.002887-68-3 0.0012Hexachlorobutadiene 0.00660.0033

A 0.003477-47-4 0.00080Hexachlorocyclopentadiene 0.00660.0033

A 0.003467-72-1 0.0015Hexachloroethane 0.00660.0033

A 0.0014193-39-5 0.00080Indeno(1,2,3-cd)pyrene 0.00330.0017

A 0.003778-59-1 0.00080Isophorone 0.00660.0033

A 0.001991-20-3 0.00060Naphthalene 0.00330.0017

A 0.003998-95-3 0.00090Nitrobenzene 0.00660.0033

A 0.0031621-64-7 0.0011N-Nitrosodi-n-propylamine 0.00660.0033

A 0.002886-30-6 0.00070N-Nitrosodiphenylamine 0.00660.0033

A 0.002187-86-5 0.0033Pentachlorophenol 0.00660.0033

A 0.001885-01-8 0.0015Phenanthrene 0.00330.0017

A 0.0031108-95-2 0.0011Phenol 0.00660.0033

A 0.0018129-00-0 0.00060Pyrene 0.00330.0017

A 0.0028110-86-1 0.00090Pyridine 0.00660.0033

S 0118-79-6 02,4,6-Tribromophenol 00


S 0367-12-4 02-Fluorophenol 00

S 01718-51-0 04-Terphenyl-d14 00

S 04165-60-0 0Nitrobenzene-d5 00

S 013127-88-3 0Phenol-d6 00

Page 101 of 155



Test Code: 8260_LL_WInstrumentID: VOA2


AqueousMatrix:Test Number: SW8260Test Name: Low Level Volatiles by SW8260C

Units: mg/L

Type Analyte DCSCAS MDL PQLDCS SpikeA 0.00063630-20-6 0.000301,1,1,2-Tetrachloroethane 0.00100.00050

A 0.0009771-55-6 0.000201,1,1-Trichloroethane 0.00100.00050

A 0.0005879-34-5 0.000501,1,2,2-Tetrachloroethane 0.00100.00050

A 0.0009276-13-1 0.00101,1,2-Trichlor-1,2,2-trifluoroethane 0.00100.00050


A 0.0004975-34-3 0.000201,1-Dichloroethane 0.00100.00050

A 0.0004675-35-4 0.000201,1-Dichloroethene 0.00100.00050

A 0.002487-61-6 0.000401,2,3-Trichlorobenzene 0.00100.00050


A 0.0006095-63-6 0.000301,2,4-Trimethylbenzene 0.00100.00050

A 0.00060106-93-4 0.000201,2-Dibromoethane 0.00100.00050

A 0.0005595-50-1 0.000501,2-Dichlorobenzene 0.00100.00050


A 0.0004978-87-5 0.000501,2-Dichloropropane 0.00100.00050




A 0.001078-93-3 0.000502-Butanone 0.00200.0010

A 0.0044591-78-6 0.00102-Hexanone 0.00200.0010

A 0.0007899-87-6 0.000304-Isopropyltoluene 0.00100.00050

A 0.0026108-10-1 0.000704-Methyl-2-pentanone 0.00200.0010

A 0.001767-64-1 0.0020Acetone 0.00200.0010

A 0.0005871-43-2 0.00020Benzene 0.00100.00050

A 0.0005375-27-4 0.00020Bromodichloromethane 0.00100.00050

A 0.0006175-25-2 0.00040Bromoform 0.00100.00050

A 0.0002774-83-9 0.00040Bromomethane 0.00100.00050

A 0.001675-15-0 0.00060Carbon disulfide 0.00200.0010

A 0.0005856-23-5 0.00050Carbon tetrachloride 0.00100.00050

A 0.00063108-90-7 0.00030Chlorobenzene 0.00100.00050

A 0.001175-00-3 0.00030Chloroethane 0.00100.00050

A 0.0005867-66-3 0.00020Chloroform 0.00100.00050

A 0.0007874-87-3 0.00020Chloromethane 0.00100.00050

A 0.00058156-59-2 0.00020cis-1,2-Dichloroethene 0.00100.00050

A 0.0005410061-01-5 0.00010cis-1,3-Dichloropropene 0.00100.00050

A 0.00049110-82-7 0.00030Cyclohexane 0.00100.00050

A 0.00075124-48-1 0.00030Dibromochloromethane 0.00100.00050

A 0.0005675-71-8 0.00030Dichlorodifluoromethane 0.00100.00050

A 0.00066100-41-4 0.00030Ethylbenzene 0.00100.00050

A 0.0005898-82-8 0.00030Isopropylbenzene 0.00100.00050

A 0.000531634-04-4 0.00020Methyl tert-butyl ether 0.00100.00050

A 0.00068108-87-2 0.00030Methylcyclohexane 0.00100.00050

Page 102 of 155






Units: mg/L

Type Analyte DCSCAS MDL PQLDCS SpikeA 0.0005375-09-2 0.0010Methylene chloride 0.00200.00050

A 0.001691-20-3 0.00030Naphthalene 0.00100.00050

A 0.00085104-51-8 0.00040n-Butylbenzene 0.00100.00050

A 0.00064103-65-1 0.00030n-Propylbenzene 0.00100.00050

A 0.00075135-98-8 0.00030sec-Butylbenzene 0.00100.00050

A 0.00067100-42-5 0.00030Styrene 0.00100.00050

A 0.0006098-06-6 0.00030tert-Butylbenzene 0.00100.00050

A 0.00077127-18-4 0.00030Tetrachloroethene 0.00100.00050

A 0.00085108-88-3 0.00020Toluene 0.00100.00050

A 0.00063156-60-5 0.00020trans-1,2-Dichloroethene 0.00100.00050

A 0.0005410061-02-6 0.00020trans-1,3-Dichloropropene 0.00100.00050

A 0.0006679-01-6 0.00020Trichloroethene 0.00100.00050

A 0.0007075-69-4 0.00030Trichlorofluoromethane 0.00100.00050

A 0.0005675-01-4 0.00020Vinyl chloride 0.00100.00050

A 0.00231330-20-7 0.00050Xylenes, Total 0.00300.0015

S 017060-07-0 01,2-Dichloroethane-d4 0.00100

S 0460-00-4 04-Bromofluorobenzene 0.00100

S 01868-53-7 0Dibromofluoromethane 0.00100

S 02037-26-5 0Toluene-d8 0.00100

Page 103 of 155



Test Code: 8260_SInstrumentID: VOA5


SolidMatrix:Test Number: SW8260Test Name: Volatiles by SW8260C

Units: mg/Kg











A 0.0012106-93-4 0.000501,2-Dibromoethane 0.00500.0012







A 0.002978-93-3 0.00132-Butanone 0.0100.0025

A 0.0024591-78-6 0.00142-Hexanone 0.0100.0025



A 0.01467-64-1 0.0031Acetone 0.0200.010

A 0.001371-43-2 0.00050Benzene 0.00500.0012


A 0.003375-25-2 0.00060Bromoform 0.00500.0012

A 0.001774-83-9 0.0010Bromomethane 0.0100.0012



A 0.0012108-90-7 0.00060Chlorobenzene 0.00500.0012

A 0.001375-00-3 0.00080Chloroethane 0.0100.0012

A 0.002367-66-3 0.00050Chloroform 0.00500.0012

A 0.001474-87-3 0.00050Chloromethane 0.0100.0012



A 0.0011110-82-7 0.0010Cyclohexane 0.00500.0012



A 0.0012100-41-4 0.00070Ethylbenzene 0.00500.0012




Page 104 of 155






Units: mg/Kg


A 0.001691-20-3 0.00080Naphthalene 0.00500.0012

A 0.0013104-51-8 0.00060n-Butylbenzene 0.00500.0012



A 0.0016100-42-5 0.00070Styrene 0.00500.0012



A 0.0014108-88-3 0.00060Toluene 0.00500.0012





A 0.001175-01-4 0.00080Vinyl chloride 0.00200.0012

A 0.00381330-20-7 0.0024Xylenes, Total 0.0100.0038

S 017060-07-0 01,2-Dichloroethane-d4 00

S 0460-00-4 04-Bromofluorobenzene 00

S 01868-53-7 0Dibromofluoromethane 00

S 02037-26-5 0Toluene-d8 00

Page 105 of 155



Test Code: MOIST_SW3550InstrumentID: Balance1


SolidMatrix:Test Number: SW3550Test Name: Moisture

Units: wt%

Type Analyte DCSCAS MDL PQLDCS SpikeA 0MOIST 0.0100Percent Moisture 0.01000

Page 106 of 155

Client:Project:

PBW HoustonCES Griggs Rd VCP


QC BATCH REPORT

Batch ID: 97451 Instrument: FID-10 Method: TX1005

Sample ID: MBLK-97451 Units: mg/Kg Analysis Date: 28-Sep-2015 08:42

Run ID: FID-10_262159 SeqNo: 3442500 PrepDate: 25-Sep-2015 DF: 1

Analyte SPK ValMQLResultSPK Ref

Value %RECControl

LimitRPD Ref

Value %RPDRPD Limit Qual

MBLK

Client ID:

nC6 to nC12 U 50

>nC12 to nC28 U 50

>nC28 to nC35 U 50

Total Petroleum Hydrocarbon U 50

22.21 25 0 88.9 70 - 1300Surr: 2-Fluorobiphenyl

24.05 25 0 96.2 70 - 1300Surr: Trifluoromethyl benzene

Sample ID: LCS-97451 Units: mg/Kg Analysis Date: 28-Sep-2015 09:12



Value %RECControl

LimitRPD Ref


LCS

Client ID:

nC6 to nC12 255.3 250 0 102 75 - 12550

>nC12 to nC28 240.8 250 0 96.3 75 - 12550

26.79 25 0 107 70 - 1300Surr: 2-Fluorobiphenyl


Sample ID: LCSD-97451 Units: mg/Kg Analysis Date: 28-Sep-2015 09:41



Value %RECControl

LimitRPD Ref


LCSD

Client ID:

nC6 to nC12 269.8 250 0 108 75 - 125 255.3 5.54 2050

>nC12 to nC28 263.1 250 0 105 75 - 125 240.8 8.86 2050

29.02 25 0 116 70 - 130 26.79 8.01 200Surr: 2-Fluorobiphenyl

26.14 25 0 105 70 - 130 24.65 5.84 200Surr: Trifluoromethyl benzene

Sample ID: HS15091001-09MS Units: mg/Kg Analysis Date: 28-Sep-2015 15:55



Value %RECControl

LimitRPD Ref


MS

Client ID: 4904-SB21-16.5

nC6 to nC12 219.9 233 0 94.4 75 - 12547

>nC12 to nC28 192.6 233 0 82.6 75 - 12547

27.89 23.3 0 120 70 - 1300Surr: 2-Fluorobiphenyl

20.58 23.3 0 88.3 70 - 1300Surr: Trifluoromethyl benzene



Page 107 of 155

Client:Project:



QC BATCH REPORT


Sample ID: HS15091001-09MSD Units: mg/Kg Analysis Date: 28-Sep-2015 16:24



Value %RECControl

LimitRPD Ref


MSD


nC6 to nC12 204.8 228.1 0 89.8 75 - 125 219.9 7.15 2046

>nC12 to nC28 194.3 228.1 0 85.2 75 - 125 192.6 0.89 2046

25.63 22.81 0 112 70 - 130 27.89 8.44 200Surr: 2-Fluorobiphenyl

19.34 22.81 0 84.8 70 - 130 20.58 6.24 200Surr: Trifluoromethyl benzene

The following samples were anayzed in this batch: HS15091001-01 HS15091001-02 HS15091001-03 HS15091001-04 HS15091001-05 HS15091001-06 HS15091001-07 HS15091001-08 HS15091001-09 HS15091001-10 HS15091001-11 HS15091001-12 HS15091001-13 HS15091001-14 HS15091001-15



Page 108 of 155

Client:Project:



QC BATCH REPORT

Batch ID: 97448 Instrument: ICPMS04 Method: SW6020


Run ID: ICPMS04_262044 SeqNo: 3440300 PrepDate: 25-Sep-2015 DF: 1


Value %RECControl

LimitRPD Ref


MBLK

Client ID:

Antimony U 0.500

Arsenic U 0.500

Barium U 0.500

Cadmium U 0.500

Chromium U 0.500

Cobalt U 0.500

Copper U 0.500

Lead U 0.500

Manganese U 0.500

Nickel U 0.500

Selenium U 0.500

Silver U 0.500

Thallium U 0.500

Vanadium U 0.500

Zinc U 0.500




Value %RECControl

LimitRPD Ref


MBLK

Client ID:

Beryllium U 0.500



Page 109 of 155

Client:Project:



QC BATCH REPORT


Sample ID: MLCS-97448 Units: mg/Kg Analysis Date: 28-Sep-2015 14:34



Value %RECControl

LimitRPD Ref


LCS

Client ID:

Antimony 9.547 10 0 95.5 80 - 1200.500

Arsenic 9.718 10 0 97.2 80 - 1200.500

Barium 9.758 10 0 97.6 80 - 1200.500

Cadmium 9.902 10 0 99.0 80 - 1200.500

Chromium 10.12 10 0 101 80 - 1200.500

Cobalt 10.04 10 0 100 80 - 1200.500

Copper 9.86 10 0 98.6 80 - 1200.500

Lead 9.344 10 0 93.4 80 - 1200.500

Manganese 10.2 10 0 102 80 - 1200.500

Nickel 9.978 10 0 99.8 80 - 1200.500

Selenium 9.623 10 0 96.2 80 - 1200.500

Silver 10.01 10 0 100 80 - 1200.500

Thallium 9.318 10 0 93.2 80 - 1200.500

Vanadium 10.28 10 0 103 80 - 1200.500

Zinc 10.03 10 0 100 80 - 1200.500




Value %RECControl

LimitRPD Ref


LCS

Client ID:

Beryllium 10.16 10 0 102 80 - 1200.500



Page 110 of 155

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MS


Antimony 5.526 9.429 0.04517 58.1 75 - 125 S 0.471

Arsenic 9.946 9.429 1.404 90.6 75 - 1250.471

Barium 23.95 9.429 26.45 -26.5 75 - 125 S 0.471

Cadmium 9.417 9.429 0.01515 99.7 75 - 1250.471

Chromium 15.26 9.429 4.717 112 75 - 1250.471

Cobalt 12 9.429 3.219 93.2 75 - 1250.471

Copper 12.84 9.429 4.058 93.2 75 - 1250.471

Lead 12.7 9.429 5.922 71.9 75 - 125 S 0.471

Manganese 64.44 9.429 109.9 -482 75 - 125 SO 0.471

Nickel 15.42 9.429 5.432 106 75 - 1250.471

Selenium 8.757 9.429 0.371 88.9 75 - 1250.471

Silver 9.38 9.429 0.0303 99.2 75 - 1250.471

Thallium 8.69 9.429 0.05312 91.6 75 - 1250.471

Vanadium 20.03 9.429 8.521 122 75 - 1250.471




Value %RECControl

LimitRPD Ref


MS


Beryllium 10.26 9.429 0.4143 104 75 - 1250.471

Zinc 21.11 9.429 10.32 114 75 - 1250.471



Page 111 of 155

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MSD


Antimony 5.761 9.677 0.04517 59.1 75 - 125 5.526 4.16 20 S 0.484

Arsenic 10.15 9.677 1.404 90.3 75 - 125 9.946 1.99 200.484

Barium 22.64 9.677 26.45 -39.4 75 - 125 23.95 5.63 20 S 0.484

Cadmium 9.665 9.677 0.01515 99.7 75 - 125 9.417 2.6 200.484

Chromium 15.35 9.677 4.717 110 75 - 125 15.26 0.574 200.484

Cobalt 11.91 9.677 3.219 89.8 75 - 125 12 0.814 200.484

Copper 13.1 9.677 4.058 93.4 75 - 125 12.84 1.95 200.484

Lead 12.94 9.677 5.922 72.5 75 - 125 12.7 1.88 20 S 0.484

Manganese 52.72 9.677 109.9 -590 75 - 125 64.44 20 20 SO 0.484

Nickel 15.35 9.677 5.432 103 75 - 125 15.42 0.419 200.484

Selenium 9.067 9.677 0.371 89.9 75 - 125 8.757 3.49 200.484

Silver 9.546 9.677 0.0303 98.3 75 - 125 9.38 1.76 200.484

Thallium 8.976 9.677 0.05312 92.2 75 - 125 8.69 3.24 200.484

Vanadium 20.07 9.677 8.521 119 75 - 125 20.03 0.184 200.484




Value %RECControl

LimitRPD Ref


MSD


Beryllium 10.5 9.677 0.4143 104 75 - 125 10.26 2.29 200.484

Zinc 21.36 9.677 10.32 114 75 - 125 21.11 1.15 200.484



Page 112 of 155

Client:Project:



QC BATCH REPORT


Sample ID: HS15091001-09BS Units: mg/Kg Analysis Date: 28-Sep-2015 15:00



Value %RECControl

LimitRPD Ref


PDS


Antimony 8.336 9.47 0.04517 87.6 75 - 1250.473

Arsenic 9.971 9.47 1.404 90.5 75 - 1250.473

Barium 34.89 9.47 26.45 89.2 75 - 1250.473

Cadmium 8.862 9.47 0.01515 93.4 75 - 1250.473

Chromium 13.58 9.47 4.717 93.5 75 - 1250.473

Cobalt 11.78 9.47 3.219 90.4 75 - 1250.473

Copper 12.36 9.47 4.058 87.7 75 - 1250.473

Lead 14.64 9.47 5.922 92.0 75 - 1250.473

Manganese 115.7 9.47 109.9 61.6 75 - 125 SO 0.473

Nickel 13.76 9.47 5.432 88.0 75 - 1250.473

Selenium 9.103 9.47 0.371 92.2 75 - 1250.473

Silver 8.911 9.47 0.0303 93.8 75 - 1250.473

Thallium 8.463 9.47 0.05312 88.8 75 - 1250.473

Vanadium 17.57 9.47 8.521 95.5 75 - 1250.473




Value %RECControl

LimitRPD Ref


PDS


Beryllium 8.511 9.47 0.4143 85.5 75 - 1250.473

Zinc 17.91 9.47 10.32 80.1 75 - 1250.473



Page 113 of 155

Client:Project:



QC BATCH REPORT


Sample ID: HS15091001-09 DIL SX Units: mg/Kg Analysis Date: 28-Sep-2015 14:47



Value %RECControl

LimitRPD Ref

Value %D%D Limit Qual

SD


Antimony U 0.04517 0 102.37

Arsenic 1.439 1.404 0 10 J 2.37

Barium 27.21 26.45 2.86 102.37

Cadmium U 0.01515 0 102.37

Chromium 4.839 4.717 2.58 102.37

Cobalt 3.396 3.219 5.48 102.37

Copper 4.176 4.058 2.92 102.37

Lead 6.099 5.922 2.98 102.37

Manganese 109.7 109.9 0.121 102.37

Nickel 5.776 5.432 6.33 102.37

Selenium 0.9144 0.371 0 10 J 2.37

Silver U 0.0303 0 102.37

Thallium U 0.05312 0 102.37

Vanadium 8.266 8.521 2.99 102.37




Value %RECControl

LimitRPD Ref


SD


Beryllium 0.4178 0.4143 0 10 J 2.37

Zinc 10.02 10.32 2.89 102.37




Page 114 of 155

Client:Project:



QC BATCH REPORT

Batch ID: 97509 Instrument: HG02 Method: SW7471A

Sample ID: MBLK-97509 Units: ug/Kg Analysis Date: 28-Sep-2015 14:21

Run ID: HG02_262082 SeqNo: 3440462 PrepDate: 28-Sep-2015 DF: 1


Value %RECControl

LimitRPD Ref


MBLK

Client ID:

Mercury U 3.32

Sample ID: LCS-97509 Units: ug/Kg Analysis Date: 28-Sep-2015 14:23



Value %RECControl

LimitRPD Ref


LCS

Client ID:

Mercury 343.3 333.3 0 103 85 - 1153.32

Sample ID: HS15091001-09MS Units: ug/Kg Analysis Date: 28-Sep-2015 14:27



Value %RECControl

LimitRPD Ref


MS


Mercury 375.5 345.7 -0.0693 109 85 - 1153.45

Sample ID: HS15091001-09MSD Units: ug/Kg Analysis Date: 28-Sep-2015 14:29



Value %RECControl

LimitRPD Ref


MSD


Mercury 375.9 344.9 -0.0693 109 85 - 115 375.5 0.126 203.44




Page 115 of 155

Client:Project:



QC BATCH REPORT

Batch ID: 97408 Instrument: SV-6 Method: SW8270


Run ID: SV-6_262020 SeqNo: 3439326 PrepDate: 24-Sep-2015 DF: 1


Value %RECControl

LimitRPD Ref


MBLK

Client ID:

1,1´-Biphenyl U 6.6

1,2,4,5-Tetrachlorobenzene U 6.6

1-Methylnaphthalene U 3.3

2,3,4,6-Tetrachlorophenol U 6.6

2,4,5-Trichlorophenol U 6.6


2,4-Dichlorophenol U 6.6

2,4-Dimethylphenol U 6.6

2,4-Dinitrophenol U 13

2,4-Dinitrotoluene U 6.6


2-Chloronaphthalene U 6.6

2-Chlorophenol U 6.6


2-Methylphenol U 6.6

2-Nitroaniline U 6.6

2-Nitrophenol U 6.6

3&4-Methylphenol U 6.6

3,3´-Dichlorobenzidine U 6.6


4,6-Dinitro-2-methylphenol U 6.6

4-Bromophenyl phenyl ether U 6.6

4-Chloro-3-methylphenol U 6.6

4-Chlorophenyl phenyl ether U 6.6


4-Nitrophenol U 13

Acenaphthene U 3.3

Acenaphthylene U 3.3

Acetophenone U 6.6

Aniline U 6.6

Anthracene U 3.3

Benz(a)anthracene U 3.3

Benzaldehyde U 6.6

Benzo(a)pyrene U 3.3



Page 116 of 155

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MBLK

Client ID:

Benzo(b)fluoranthene U 3.3

Benzo(g,h,i)perylene U 3.3

Benzo(k)fluoranthene U 3.3

Bis(2-chloroethoxy)methane U 6.6

Bis(2-chloroethyl)ether U 6.6

Bis(2-chloroisopropyl)ether U 6.6

Bis(2-ethylhexyl)phthalate U 6.6

Butyl benzyl phthalate U 6.6

Caprolactam U 6.6

Carbazole U 6.6

Chrysene U 3.3

Dibenz(a,h)anthracene U 3.3

Dibenzofuran U 3.3

Diethyl phthalate U 6.6

Dimethyl phthalate U 6.6

Di-n-butyl phthalate U 6.6

Di-n-octyl phthalate U 6.6

Fluoranthene U 3.3

Fluorene U 3.3

Hexachlorobenzene U 6.6

Hexachlorobutadiene U 6.6

Hexachlorocyclopentadiene U 6.6

Hexachloroethane U 6.6

Indeno(1,2,3-cd)pyrene U 3.3

Isophorone U 6.6

Naphthalene U 3.3

Nitrobenzene U 6.6

N-Nitrosodi-n-propylamine U 6.6

N-Nitrosodiphenylamine U 6.6

Pentachlorophenol U 6.6

Phenanthrene U 3.3

Phenol U 6.6

Pyrene U 3.3

Pyridine U 6.6



Page 117 of 155

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MBLK

Client ID:

109.2 167 0 65.4 36 - 1260Surr: 2,4,6-Tribromophenol


111.1 167 0 66.6 37 - 1250Surr: 2-Fluorophenol

129.8 167 0 77.7 32 - 1250Surr: 4-Terphenyl-d14

124.9 167 0 74.8 37 - 1250Surr: Nitrobenzene-d5

123.5 167 0 74.0 40 - 1250Surr: Phenol-d6



Page 118 of 155

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


LCS

Client ID:

1,1´-Biphenyl 114.7 167 0 68.7 50 - 1206.6

1,2,4,5-Tetrachlorobenzene 128.8 167 0 77.2 40 - 1406.6

1-Methylnaphthalene 118.6 167 0 71.0 50 - 1203.3

2,3,4,6-Tetrachlorophenol 110.6 167 0 66.2 40 - 1406.6

2,4,5-Trichlorophenol 108.9 167 0 65.2 45 - 1276.6


2,4-Dichlorophenol 112.4 167 0 67.3 45 - 1256.6

2,4-Dimethylphenol 116.1 167 0 69.5 45 - 1206.6

2,4-Dinitrophenol 64.11 167 0 38.4 10 - 12613

2,4-Dinitrotoluene 117.6 167 0 70.4 50 - 1306.6

2,6-Dinitrotoluene 122 167 0 73.1 50 - 1256.6

2-Chloronaphthalene 115 167 0 68.9 50 - 1456.6

2-Chlorophenol 123.1 167 0 73.7 45 - 1206.6


2-Methylphenol 134.1 167 0 80.3 45 - 1206.6

2-Nitroaniline 158 167 0 94.6 45 - 1386.6

2-Nitrophenol 110.1 167 0 66.0 45 - 1256.6

3&4-Methylphenol 137.6 167 0 82.4 45 - 1206.6

3,3´-Dichlorobenzidine 129.4 167 0 77.5 15 - 1206.6

3-Nitroaniline 109.6 167 0 65.6 40 - 1206.6

4,6-Dinitro-2-methylphenol 81.97 167 0 49.1 15 - 1356.6

4-Bromophenyl phenyl ether 117.2 167 0 70.2 50 - 1256.6

4-Chloro-3-methylphenol 121.4 167 0 72.7 45 - 1306.6

4-Chlorophenyl phenyl ether 113.9 167 0 68.2 50 - 1206.6

4-Nitroaniline 103.5 167 0 62.0 50 - 1276.6

4-Nitrophenol 113.6 167 0 68.0 40 - 14713

Acenaphthene 108.8 167 0 65.2 50 - 1203.3

Acenaphthylene 113.7 167 0 68.1 50 - 1203.3

Acetophenone 115.5 167 0 69.1 50 - 1206.6

Aniline 99.28 167 0 59.4 10 - 1356.6

Anthracene 120.6 167 0 72.2 50 - 1233.3

Benz(a)anthracene 129.1 167 0 77.3 50 - 1313.3

Benzaldehyde 37.38 167 0 22.4 22 - 1296.6

Benzo(a)pyrene 124.8 167 0 74.7 50 - 1303.3



Page 119 of 155

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


LCS

Client ID:

Benzo(b)fluoranthene 135.3 167 0 81.0 50 - 1373.3

Benzo(g,h,i)perylene 120.2 167 0 72.0 50 - 1303.3

Benzo(k)fluoranthene 115.4 167 0 69.1 50 - 1433.3

Bis(2-chloroethoxy)methane 126.4 167 0 75.7 50 - 1206.6

Bis(2-chloroethyl)ether 133.8 167 0 80.1 45 - 1276.6

Bis(2-chloroisopropyl)ether 129.5 167 0 77.5 50 - 1206.6

Bis(2-ethylhexyl)phthalate 161.9 167 0 96.9 21 - 1486.6

Butyl benzyl phthalate 162.1 167 0 97.1 50 - 1366.6

Caprolactam 122.3 167 0 73.3 50 - 1356.6

Carbazole 117.9 167 0 70.6 50 - 1436.6

Chrysene 122.6 167 0 73.4 50 - 1303.3

Dibenz(a,h)anthracene 111.2 167 0 66.6 50 - 1303.3

Dibenzofuran 114.1 167 0 68.3 50 - 1253.3

Diethyl phthalate 126.4 167 0 75.7 50 - 1256.6

Dimethyl phthalate 116.6 167 0 69.8 50 - 1256.6

Di-n-butyl phthalate 143 167 0 85.6 50 - 1406.6

Di-n-octyl phthalate 178.4 167 0 107 50 - 1406.6

Fluoranthene 122.2 167 0 73.2 50 - 1313.3

Fluorene 114.2 167 0 68.4 50 - 1253.3

Hexachlorobenzene 113.9 167 0 68.2 50 - 1246.6

Hexachlorobutadiene 105.2 167 0 63.0 50 - 1256.6

Hexachlorocyclopentadiene 87.66 167 0 52.5 45 - 1356.6

Hexachloroethane 128.5 167 0 76.9 45 - 1256.6

Indeno(1,2,3-cd)pyrene 121.7 167 0 72.9 45 - 1393.3

Isophorone 126.7 167 0 75.9 45 - 1306.6

Naphthalene 119.9 167 0 71.8 50 - 1253.3

Nitrobenzene 124.1 167 0 74.3 50 - 1256.6

N-Nitrosodi-n-propylamine 141.5 167 0 84.7 45 - 1206.6

N-Nitrosodiphenylamine 123.9 167 0 74.2 50 - 1306.6

Pentachlorophenol 67.54 167 0 40.4 23 - 1366.6

Phenanthrene 120.8 167 0 72.3 50 - 1253.3

Phenol 127.9 167 0 76.6 45 - 1306.6

Pyrene 130.8 167 0 78.3 45 - 1303.3

Pyridine 98.8 167 0 59.2 15 - 1206.6



Page 120 of 155

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


LCS

Client ID:




130 167 0 77.8 32 - 1250Surr: 4-Terphenyl-d14


120.5 167 0 72.2 40 - 1250Surr: Phenol-d6



Page 121 of 155

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MS


1,1´-Biphenyl 145.8 166.7 0 87.4 50 - 1206.6

1,2,4,5-Tetrachlorobenzene 162.4 166.7 0 97.4 40 - 1406.6

1-Methylnaphthalene 142.6 166.7 0 85.5 50 - 1203.3

2,3,4,6-Tetrachlorophenol 149.5 166.7 0 89.7 40 - 1406.6

2,4,5-Trichlorophenol 142.1 166.7 0 85.2 45 - 1276.6


2,4-Dichlorophenol 137 166.7 0 82.2 45 - 1256.6

2,4-Dimethylphenol 141.3 166.7 0 84.8 45 - 1206.6

2,4-Dinitrophenol 52.3 166.7 0 31.4 10 - 12613

2,4-Dinitrotoluene 156.9 166.7 0 94.1 50 - 1306.6

2,6-Dinitrotoluene 150.9 166.7 0 90.5 50 - 1256.6

2-Chloronaphthalene 156 166.7 0 93.6 50 - 1456.6

2-Chlorophenol 151.3 166.7 0 90.7 45 - 1206.6


2-Methylphenol 165.3 166.7 0 99.2 45 - 1206.6

2-Nitroaniline 198.8 166.7 0 119 45 - 1386.6

2-Nitrophenol 138.7 166.7 0 83.2 45 - 1256.6

3&4-Methylphenol 165.8 166.7 0 99.4 45 - 1206.6

3,3´-Dichlorobenzidine 144.7 166.7 0 86.8 15 - 1206.6

3-Nitroaniline 122.3 166.7 0 73.4 40 - 1206.6

4,6-Dinitro-2-methylphenol 97.08 166.7 0 58.2 15 - 1356.6

4-Bromophenyl phenyl ether 152.4 166.7 0 91.4 50 - 1256.6

4-Chloro-3-methylphenol 151.8 166.7 0 91.0 45 - 1306.6

4-Chlorophenyl phenyl ether 142.2 166.7 0 85.3 50 - 1206.6

4-Nitroaniline 122.1 166.7 0 73.2 50 - 1276.6

4-Nitrophenol 167.2 166.7 0 100 40 - 14713

Acenaphthene 138.6 166.7 0 83.1 50 - 1203.3

Acenaphthylene 147 166.7 0 88.2 50 - 1203.3

Acetophenone 136.5 166.7 0 81.9 50 - 1206.6

Aniline 120.9 166.7 0 72.5 10 - 1356.6

Anthracene 154.2 166.7 0 92.5 50 - 1233.3

Benz(a)anthracene 159.5 166.7 0 95.7 50 - 1313.3

Benzaldehyde 37.04 166.7 0 22.2 22 - 1296.6

Benzo(a)pyrene 156.8 166.7 0 94.1 50 - 1303.3



Page 122 of 155

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MS


Benzo(b)fluoranthene 188.9 166.7 0 113 50 - 1373.3

Benzo(g,h,i)perylene 115.6 166.7 0 69.3 50 - 1303.3

Benzo(k)fluoranthene 150.2 166.7 0 90.1 50 - 1433.3

Bis(2-chloroethoxy)methane 151.8 166.7 0 91.0 50 - 1206.6

Bis(2-chloroethyl)ether 159.8 166.7 0 95.9 45 - 1276.6

Bis(2-chloroisopropyl)ether 162 166.7 0 97.2 50 - 1206.6

Bis(2-ethylhexyl)phthalate 199.8 166.7 7.878 115 21 - 1486.6

Butyl benzyl phthalate 199.9 166.7 0 120 50 - 1366.6

Caprolactam 158.6 166.7 19.51 83.4 50 - 1356.6

Carbazole 142.2 166.7 0 85.3 50 - 1436.6

Chrysene 148.5 166.7 0 89.1 50 - 1303.3

Dibenz(a,h)anthracene 119.4 166.7 0 71.6 50 - 1303.3

Dibenzofuran 145.7 166.7 0 87.4 50 - 1253.3

Diethyl phthalate 157.3 166.7 0 94.4 50 - 1256.6

Dimethyl phthalate 143.6 166.7 0 86.1 50 - 1256.6

Di-n-butyl phthalate 174.9 166.7 0 105 50 - 1406.6

Di-n-octyl phthalate 231 166.7 0 139 50 - 1406.6

Fluoranthene 147.2 166.7 0 88.3 50 - 1313.3

Fluorene 146.7 166.7 0 88.0 50 - 1253.3

Hexachlorobenzene 152 166.7 0 91.2 50 - 1246.6

Hexachlorobutadiene 128.1 166.7 0 76.8 50 - 1256.6

Hexachlorocyclopentadiene 88.25 166.7 0 52.9 45 - 1356.6

Hexachloroethane 151.3 166.7 0 90.8 45 - 1256.6

Indeno(1,2,3-cd)pyrene 131 166.7 0 78.6 45 - 1393.3

Isophorone 153.7 166.7 0 92.2 45 - 1306.6

Naphthalene 143.9 166.7 0 86.3 50 - 1253.3

Nitrobenzene 156.1 166.7 0 93.6 50 - 1256.6

N-Nitrosodi-n-propylamine 174.2 166.7 0 104 45 - 1206.6

N-Nitrosodiphenylamine 156.1 166.7 0 93.7 50 - 1306.6

Pentachlorophenol 101.5 166.7 0 60.9 23 - 1366.6

Phenanthrene 153.7 166.7 0 92.2 50 - 1253.3

Phenol 155.4 166.7 0 93.2 45 - 1306.6

Pyrene 167.5 166.7 0 100 45 - 1303.3

Pyridine 144.4 166.7 0 86.6 15 - 1206.6



Page 123 of 155

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MS


123.1 166.7 0 73.8 36 - 1260Surr: 2,4,6-Tribromophenol

136.5 166.7 0 81.9 43 - 1250Surr: 2-Fluorobiphenyl

138 166.7 0 82.8 37 - 1250Surr: 2-Fluorophenol

155.6 166.7 0 93.4 32 - 1250Surr: 4-Terphenyl-d14

141.6 166.7 0 84.9 37 - 1250Surr: Nitrobenzene-d5

142.8 166.7 0 85.6 40 - 1250Surr: Phenol-d6



Page 124 of 155

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MSD


1,1´-Biphenyl 137 166.6 0 82.2 50 - 120 145.8 6.22 306.6

1,2,4,5-Tetrachlorobenzene 156.4 166.6 0 93.9 40 - 140 162.4 3.77 306.6

1-Methylnaphthalene 139.3 166.6 0 83.6 50 - 120 142.6 2.33 303.3

2,3,4,6-Tetrachlorophenol 136.8 166.6 0 82.1 40 - 140 149.5 8.86 306.6

2,4,5-Trichlorophenol 143.5 166.6 0 86.1 45 - 127 142.1 0.994 306.6


2,4-Dichlorophenol 138 166.6 0 82.8 45 - 125 137 0.756 306.6

2,4-Dimethylphenol 135.4 166.6 0 81.2 45 - 120 141.3 4.32 306.6

2,4-Dinitrophenol 60.09 166.6 0 36.1 10 - 126 52.3 13.9 3013

2,4-Dinitrotoluene 150.3 166.6 0 90.2 50 - 130 156.9 4.26 306.6

2,6-Dinitrotoluene 144.2 166.6 0 86.5 50 - 125 150.9 4.56 306.6

2-Chloronaphthalene 148.5 166.6 0 89.1 50 - 145 156 4.96 306.6

2-Chlorophenol 145.4 166.6 0 87.3 45 - 120 151.3 3.98 306.6


2-Methylphenol 165.2 166.6 0 99.2 45 - 120 165.3 0.0715 306.6

2-Nitroaniline 187 166.6 0 112 45 - 138 198.8 6.07 306.6

2-Nitrophenol 132.8 166.6 0 79.7 45 - 125 138.7 4.35 306.6

3&4-Methylphenol 166.5 166.6 0 99.9 45 - 120 165.8 0.442 306.6

3,3´-Dichlorobenzidine 125.4 166.6 0 75.3 15 - 120 144.7 14.3 306.6

3-Nitroaniline 111.7 166.6 0 67.1 40 - 120 122.3 9.03 306.6

4,6-Dinitro-2-methylphenol 93.02 166.6 0 55.8 15 - 135 97.08 4.27 306.6

4-Bromophenyl phenyl ether 139.6 166.6 0 83.8 50 - 125 152.4 8.76 306.6

4-Chloro-3-methylphenol 149.3 166.6 0 89.6 45 - 130 151.8 1.65 306.6

4-Chlorophenyl phenyl ether 137.6 166.6 0 82.6 50 - 120 142.2 3.31 306.6

4-Nitroaniline 119.2 166.6 0 71.6 50 - 127 122.1 2.36 306.6

4-Nitrophenol 165.9 166.6 0 99.6 40 - 147 167.2 0.757 3013

Acenaphthene 132.6 166.6 0 79.6 50 - 120 138.6 4.37 303.3

Acenaphthylene 136.8 166.6 0 82.1 50 - 120 147 7.24 303.3

Acetophenone 132.6 166.6 0 79.6 50 - 120 136.5 2.87 306.6

Aniline 107.7 166.6 0 64.6 10 - 135 120.9 11.6 306.6

Anthracene 143.7 166.6 0 86.3 50 - 123 154.2 7.05 303.3

Benz(a)anthracene 152.6 166.6 0 91.6 50 - 131 159.5 4.4 303.3

Benzaldehyde 42.73 166.6 0 25.6 22 - 129 37.04 14.3 306.6

Benzo(a)pyrene 153 166.6 0 91.8 50 - 130 156.8 2.46 303.3



Page 125 of 155

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MSD


Benzo(b)fluoranthene 177.4 166.6 0 107 50 - 137 188.9 6.25 303.3

Benzo(g,h,i)perylene 119.5 166.6 0 71.7 50 - 130 115.6 3.3 303.3

Benzo(k)fluoranthene 155.3 166.6 0 93.2 50 - 143 150.2 3.37 303.3

Bis(2-chloroethoxy)methane 143.9 166.6 0 86.4 50 - 120 151.8 5.31 306.6

Bis(2-chloroethyl)ether 161.2 166.6 0 96.7 45 - 127 159.8 0.837 306.6

Bis(2-chloroisopropyl)ether 157.8 166.6 0 94.7 50 - 120 162 2.67 306.6

Bis(2-ethylhexyl)phthalate 188.6 166.6 7.878 108 21 - 148 199.8 5.77 306.6

Butyl benzyl phthalate 191.7 166.6 0 115 50 - 136 199.9 4.19 306.6

Caprolactam 164.4 166.6 19.51 86.9 50 - 135 158.6 3.59 306.6

Carbazole 136.6 166.6 0 82.0 50 - 143 142.2 3.97 306.6

Chrysene 142.7 166.6 0 85.6 50 - 130 148.5 4.02 303.3

Dibenz(a,h)anthracene 114.1 166.6 0 68.5 50 - 130 119.4 4.51 303.3

Dibenzofuran 140.4 166.6 0 84.2 50 - 125 145.7 3.76 303.3

Diethyl phthalate 152.2 166.6 0 91.4 50 - 125 157.3 3.3 306.6

Dimethyl phthalate 135.3 166.6 0 81.2 50 - 125 143.6 5.94 306.6

Di-n-butyl phthalate 158.8 166.6 0 95.3 50 - 140 174.9 9.66 306.6

Di-n-octyl phthalate 253 166.6 0 152 50 - 140 231 9.08 30 S 6.6

Fluoranthene 139 166.6 0 83.4 50 - 131 147.2 5.78 303.3

Fluorene 139.2 166.6 0 83.6 50 - 125 146.7 5.24 303.3

Hexachlorobenzene 138.2 166.6 0 83.0 50 - 124 152 9.48 306.6

Hexachlorobutadiene 123.7 166.6 0 74.3 50 - 125 128.1 3.43 306.6

Hexachlorocyclopentadiene 67.06 166.6 0 40.3 45 - 135 88.25 27.3 30 S 6.6

Hexachloroethane 147.8 166.6 0 88.7 45 - 125 151.3 2.35 306.6

Indeno(1,2,3-cd)pyrene 116.9 166.6 0 70.1 45 - 139 131 11.4 303.3

Isophorone 150.4 166.6 0 90.3 45 - 130 153.7 2.15 306.6

Naphthalene 138.3 166.6 0 83.0 50 - 125 143.9 4.02 303.3

Nitrobenzene 149 166.6 0 89.5 50 - 125 156.1 4.63 306.6

N-Nitrosodi-n-propylamine 173.6 166.6 0 104 45 - 120 174.2 0.351 306.6

N-Nitrosodiphenylamine 145.8 166.6 0 87.5 50 - 130 156.1 6.82 306.6

Pentachlorophenol 98.48 166.6 0 59.1 23 - 136 101.5 3 306.6

Phenanthrene 144.2 166.6 0 86.6 50 - 125 153.7 6.38 303.3

Phenol 156.8 166.6 0 94.1 45 - 130 155.4 0.91 306.6

Pyrene 155 166.6 0 93.0 45 - 130 167.5 7.73 303.3

Pyridine 114.3 166.6 0 68.6 15 - 120 144.4 23.2 306.6



Page 126 of 155

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MSD


127.4 166.6 0 76.5 36 - 126 123.1 3.48 300Surr: 2,4,6-Tribromophenol

130.6 166.6 0 78.4 43 - 125 136.5 4.46 300Surr: 2-Fluorobiphenyl

135.1 166.6 0 81.1 37 - 125 138 2.07 300Surr: 2-Fluorophenol

147.7 166.6 0 88.6 32 - 125 155.6 5.26 300Surr: 4-Terphenyl-d14

132.4 166.6 0 79.5 37 - 125 141.6 6.68 300Surr: Nitrobenzene-d5

147.3 166.6 0 88.4 40 - 125 142.8 3.13 300Surr: Phenol-d6




Page 127 of 155

Client:Project:



QC BATCH REPORT

Batch ID: R261899 Instrument: VOA2 Method: SW8260

Sample ID: VBLKW-150924 Units: ug/L Analysis Date: 25-Sep-2015 01:16

Run ID: VOA2_261899 SeqNo: 3436606 PrepDate: DF: 1


Value %RECControl

LimitRPD Ref


MBLK

Client ID:

1,1,1,2-Tetrachloroethane U 1.0

1,1,1-Trichloroethane U 1.0


1,1,2-Trichlor-1,2,2-trifluoroethane U 1.0


1,1-Dichloroethane U 1.0

1,1-Dichloroethene U 1.0

1,2,3-Trichlorobenzene U 1.0


1,2,4-Trimethylbenzene U 1.0

1,2-Dibromoethane U 1.0

1,2-Dichlorobenzene U 1.0


1,2-Dichloropropane U 1.0




2-Butanone U 2.0

2-Hexanone U 2.0

4-Isopropyltoluene U 1.0

4-Methyl-2-pentanone U 2.0

Acetone U 2.0

Benzene U 1.0

Bromodichloromethane U 1.0

Bromoform U 1.0

Bromomethane U 1.0

Carbon disulfide U 2.0

Carbon tetrachloride U 1.0

Chlorobenzene U 1.0

Chloroethane U 1.0

Chloroform U 1.0

Chloromethane U 1.0

cis-1,2-Dichloroethene U 1.0

cis-1,3-Dichloropropene U 1.0



Page 128 of 155

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MBLK

Client ID:

Cyclohexane U 1.0

Dibromochloromethane U 1.0

Dichlorodifluoromethane U 1.0

Ethylbenzene U 1.0

Isopropylbenzene U 1.0

Methyl tert-butyl ether U 1.0

Methylcyclohexane U 1.0

Methylene chloride U 2.0

Naphthalene U 1.0

n-Butylbenzene U 1.0

n-Propylbenzene U 1.0

sec-Butylbenzene U 1.0

Styrene U 1.0

tert-Butylbenzene U 1.0

Tetrachloroethene U 1.0

Toluene U 1.0

trans-1,2-Dichloroethene U 1.0

trans-1,3-Dichloropropene U 1.0

Trichloroethene U 1.0

Trichlorofluoromethane U 1.0

Vinyl chloride U 1.0

Xylenes, Total U 3.0

50.04 50 0 100 71 - 1251.0Surr: 1,2-Dichloroethane-d4

49.59 50 0 99.2 70 - 1251.0Surr: 4-Bromofluorobenzene

51.26 50 0 103 74 - 1251.0Surr: Dibromofluoromethane

49.1 50 0 98.2 75 - 1251.0Surr: Toluene-d8



Page 129 of 155

Client:Project:



QC BATCH REPORT


Sample ID: VLCSW-150924 Units: ug/L Analysis Date: 25-Sep-2015 00:26



Value %RECControl

LimitRPD Ref


LCS

Client ID:

1,1,1,2-Tetrachloroethane 49.78 50 0 99.6 80 - 1201.0

1,1,1-Trichloroethane 49.84 50 0 99.7 75 - 1301.0


1,1,2-Trichlor-1,2,2-trifluoroethane 46.05 50 0 92.1 70 - 1301.0


1,1-Dichloroethane 48.63 50 0 97.3 76 - 1201.0

1,1-Dichloroethene 48.12 50 0 96.2 75 - 1301.0

1,2,3-Trichlorobenzene 52.81 50 0 106 70 - 1311.0


1,2,4-Trimethylbenzene 47.22 50 0 94.4 70 - 1251.0

1,2-Dibromoethane 50.32 50 0 101 80 - 1211.0

1,2-Dichlorobenzene 48.47 50 0 96.9 80 - 1201.0

1,2-Dichloroethane 47.04 50 0 94.1 76 - 1201.0

1,2-Dichloropropane 47.95 50 0 95.9 80 - 1201.0




2-Butanone 107.1 100 0 107 60 - 1402.0

2-Hexanone 95.35 100 0 95.3 60 - 1312.0

4-Isopropyltoluene 48.12 50 0 96.2 79 - 1271.0

4-Methyl-2-pentanone 100.4 100 0 100 60 - 1352.0

Acetone 103.9 100 0 104 60 - 1402.0

Benzene 44.85 50 0 89.7 80 - 1201.0

Bromodichloromethane 49.66 50 0 99.3 75 - 1251.0

Bromoform 48.19 50 0 96.4 70 - 1301.0

Bromomethane 50.4 50 0 101 60 - 1401.0

Carbon disulfide 93.53 100 0 93.5 70 - 1302.0

Carbon tetrachloride 46.52 50 0 93.0 75 - 1251.0

Chlorobenzene 48.77 50 0 97.5 80 - 1201.0

Chloroethane 45.26 50 0 90.5 70 - 1301.0

Chloroform 46.73 50 0 93.5 70 - 1301.0

Chloromethane 41.88 50 0 83.8 65 - 1301.0

cis-1,2-Dichloroethene 46.84 50 0 93.7 75 - 1251.0

cis-1,3-Dichloropropene 47.94 50 0 95.9 79 - 1251.0



Page 130 of 155

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


LCS

Client ID:

Cyclohexane 47.77 50 0 95.5 70 - 1301.0

Dibromochloromethane 49.66 50 0 99.3 70 - 1301.0

Dichlorodifluoromethane 40.24 50 0 80.5 60 - 1401.0

Ethylbenzene 46.3 50 0 92.6 80 - 1201.0

Isopropylbenzene 49.27 50 0 98.5 75 - 1301.0

Methyl tert-butyl ether 47.99 50 0 96.0 70 - 1301.0

Methylcyclohexane 46.24 50 0 92.5 70 - 1261.0

Methylene chloride 42.61 50 0 85.2 65 - 1332.0

Naphthalene 49.72 50 0 99.4 65 - 1351.0

n-Butylbenzene 48.3 50 0 96.6 75 - 1281.0

n-Propylbenzene 47.63 50 0 95.3 75 - 1301.0

sec-Butylbenzene 48.14 50 0 96.3 70 - 1251.0

Styrene 48.19 50 0 96.4 78 - 1221.0

tert-Butylbenzene 48.63 50 0 97.3 70 - 1301.0

Tetrachloroethene 46.97 50 0 93.9 75 - 1301.0

Toluene 51.29 50 0 103 75 - 1211.0

trans-1,2-Dichloroethene 46.75 50 0 93.5 75 - 1251.0

trans-1,3-Dichloropropene 47.94 50 0 95.9 76 - 1251.0

Trichloroethene 47.23 50 0 94.5 71 - 1251.0

Trichlorofluoromethane 51.72 50 0 103 67 - 1321.0

Vinyl chloride 44.08 50 0 88.2 70 - 1351.0

Xylenes, Total 134.1 150 0 89.4 79 - 1243.0

49.05 50 0 98.1 71 - 1251.0Surr: 1,2-Dichloroethane-d4

50.32 50 0 101 70 - 1251.0Surr: 4-Bromofluorobenzene


48.8 50 0 97.6 75 - 1251.0Surr: Toluene-d8



Page 131 of 155

Client:Project:



QC BATCH REPORT


Sample ID: HS15091033-01MS Units: ug/L Analysis Date: 25-Sep-2015 03:47



Value %RECControl

LimitRPD Ref


MS

Client ID:

1,1,1,2-Tetrachloroethane 50.67 50 0 101 80 - 1201.0

1,1,1-Trichloroethane 58.58 50 0 117 75 - 1301.0


1,1,2-Trichlor-1,2,2-trifluoroethane 59.45 50 0 119 70 - 1301.0


1,1-Dichloroethane 51.91 50 0 104 76 - 1201.0

1,1-Dichloroethene 55.91 50 0 112 75 - 1301.0




1,2-Dibromoethane 48.99 50 0 98.0 80 - 1211.0


1,2-Dichloroethane 48.12 50 0 96.2 76 - 1201.0


1,3,5-Trimethylbenzene 51.12 50 0 102 80 - 1231.0

1,3-Dichlorobenzene 50.87 50 0 102 80 - 1201.0


2-Butanone 100.2 100 0 100 60 - 1402.0

2-Hexanone 89.83 100 0 89.8 60 - 1312.0

4-Isopropyltoluene 53.53 50 0 107 79 - 1271.0

4-Methyl-2-pentanone 96.25 100 0 96.3 60 - 1352.0

Acetone 93.08 100 0 93.1 60 - 1402.0

Benzene 48.6 50 0 97.2 80 - 1201.0


Bromoform 48.1 50 0 96.2 70 - 1301.0

Bromomethane 55.2 50 0 110 60 - 1401.0

Carbon disulfide 110.4 100 0 110 70 - 1302.0

Carbon tetrachloride 57.66 50 0 115 79 - 1201.0

Chlorobenzene 50.59 50 0 101 80 - 1201.0

Chloroethane 53.94 50 0 108 70 - 1301.0

Chloroform 50.23 50 0 100 70 - 1301.0

Chloromethane 42.99 50 0 86.0 65 - 1301.0





Page 132 of 155

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MS

Client ID:

Cyclohexane 61.65 50 0 123 70 - 1301.0



Ethylbenzene 50.73 50 0 101 80 - 1201.0

Isopropylbenzene 54.63 50 0 109 75 - 1301.0


Methylcyclohexane 60.9 50 0 122 70 - 1261.0


Naphthalene 47.87 50 0 95.7 65 - 1351.0

n-Butylbenzene 54.76 50 0 110 75 - 1281.0

n-Propylbenzene 53.49 50 0 107 75 - 1301.0

sec-Butylbenzene 55.8 50 0 112 70 - 1251.0

Styrene 49.57 50 0 99.1 78 - 1221.0

tert-Butylbenzene 54.62 50 0 109 70 - 1301.0

Tetrachloroethene 54.17 50 0 108 75 - 1301.0

Toluene 55.71 50 0 111 75 - 1211.0

trans-1,2-Dichloroethene 53.2 50 0 106 75 - 1251.0




Vinyl chloride 53.7 50 0 107 70 - 1351.0

Xylenes, Total 143 150 0 95.3 80 - 1243.0



49.84 50 0 99.7 74 - 1251.0Surr: Dibromofluoromethane

48.52 50 0 97.0 75 - 1251.0Surr: Toluene-d8



Page 133 of 155

Client:Project:



QC BATCH REPORT


Sample ID: HS15091033-01MSD Units: ug/L Analysis Date: 25-Sep-2015 04:13



Value %RECControl

LimitRPD Ref


MSD

Client ID:

1,1,1,2-Tetrachloroethane 49.68 50 0 99.4 80 - 120 50.67 1.97 201.0

1,1,1-Trichloroethane 55.09 50 0 110 75 - 130 58.58 6.13 201.0


1,1,2-Trichlor-1,2,2-trifluoroethane 56.39 50 0 113 70 - 130 59.45 5.29 201.0

1,1,2-Trichloroethane 48.06 50 0 96.1 80 - 120 49.33 2.61 201.0

1,1-Dichloroethane 49.92 50 0 99.8 76 - 120 51.91 3.91 201.0

1,1-Dichloroethene 53.75 50 0 108 75 - 130 55.91 3.94 201.0

1,2,3-Trichlorobenzene 53.58 50 0 107 70 - 131 52.37 2.28 201.0

1,2,4-Trichlorobenzene 53.74 50 0 107 75 - 126 53.46 0.528 201.0

1,2,4-Trimethylbenzene 49.06 50 0 98.1 70 - 125 49.13 0.157 201.0

1,2-Dibromoethane 48.14 50 0 96.3 80 - 121 48.99 1.76 201.0

1,2-Dichlorobenzene 48.35 50 0 96.7 80 - 120 49.37 2.09 201.0

1,2-Dichloroethane 45.31 50 0 90.6 76 - 120 48.12 6 201.0

1,2-Dichloropropane 47.27 50 0 94.5 80 - 120 48.2 1.94 201.0

1,3,5-Trimethylbenzene 50.27 50 0 101 80 - 123 51.12 1.69 201.0



2-Butanone 100 100 0 100 60 - 140 100.2 0.163 202.0

2-Hexanone 90.9 100 0 90.9 60 - 131 89.83 1.18 202.0

4-Isopropyltoluene 52.57 50 0 105 79 - 127 53.53 1.8 201.0

4-Methyl-2-pentanone 96.27 100 0 96.3 60 - 135 96.25 0.0142 202.0

Acetone 96.49 100 0 96.5 60 - 140 93.08 3.6 202.0

Benzene 46.7 50 0 93.4 80 - 120 48.6 3.98 201.0

Bromodichloromethane 48.28 50 0 96.6 75 - 125 49.86 3.22 201.0

Bromoform 47.18 50 0 94.4 70 - 130 48.1 1.93 201.0

Bromomethane 49.55 50 0 99.1 60 - 140 55.2 10.8 201.0

Carbon disulfide 104.7 100 0 105 70 - 130 110.4 5.29 202.0

Carbon tetrachloride 53.73 50 0 107 75 - 125 57.66 7.06 201.0

Chlorobenzene 49.03 50 0 98.1 80 - 120 50.59 3.13 201.0

Chloroethane 49.86 50 0 99.7 70 - 130 53.94 7.88 201.0

Chloroform 47.5 50 0 95.0 70 - 130 50.23 5.59 201.0

Chloromethane 41.75 50 0 83.5 65 - 130 42.99 2.93 201.0

cis-1,2-Dichloroethene 47.98 50 0 96.0 75 - 125 49.08 2.25 201.0

cis-1,3-Dichloropropene 46.01 50 0 92.0 79 - 125 46.99 2.11 201.0



Page 134 of 155

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MSD

Client ID:

Cyclohexane 59.14 50 0 118 70 - 130 61.65 4.16 201.0

Dibromochloromethane 48.95 50 0 97.9 70 - 130 49.96 2.05 201.0

Dichlorodifluoromethane 38.05 50 0 76.1 60 - 140 44.93 16.6 201.0

Ethylbenzene 48.59 50 0 97.2 80 - 120 50.73 4.31 201.0

Isopropylbenzene 53.2 50 0 106 75 - 130 54.63 2.65 201.0

Methyl tert-butyl ether 45.7 50 0 91.4 70 - 130 46.72 2.21 201.0

Methylcyclohexane 57.29 50 0 115 70 - 126 60.9 6.11 201.0

Methylene chloride 44.16 50 0 88.3 65 - 133 46.86 5.92 202.0

Naphthalene 47.91 50 0 95.8 65 - 135 47.87 0.0888 201.0

n-Butylbenzene 53.52 50 0 107 75 - 128 54.76 2.3 201.0

n-Propylbenzene 52.34 50 0 105 75 - 130 53.49 2.17 201.0

sec-Butylbenzene 54.44 50 0 109 70 - 125 55.8 2.46 201.0

Styrene 48.42 50 0 96.8 78 - 122 49.57 2.35 201.0

tert-Butylbenzene 54.14 50 0 108 70 - 130 54.62 0.885 201.0

Tetrachloroethene 52.38 50 0 105 75 - 130 54.17 3.35 201.0

Toluene 53.59 50 0 107 75 - 121 55.71 3.88 201.0

trans-1,2-Dichloroethene 51.2 50 0 102 75 - 125 53.2 3.84 201.0

trans-1,3-Dichloropropene 46.01 50 0 92.0 76 - 125 46.99 2.11 201.0

Trichloroethene 45.41 50 0 90.8 71 - 125 49.16 7.94 201.0

Trichlorofluoromethane 60.93 50 0 122 67 - 132 63.13 3.54 201.0

Vinyl chloride 43.59 50 0 87.2 70 - 135 53.7 20.8 20 R 1.0

Xylenes, Total 140 150 0 93.4 80 - 124 143 2.11 203.0

50.81 50 0 102 71 - 125 49.81 1.98 201.0Surr: 1,2-Dichloroethane-d4

51.17 50 0 102 70 - 125 49.24 3.84 201.0Surr: 4-Bromofluorobenzene

48.85 50 0 97.7 74 - 125 49.84 2 201.0Surr: Dibromofluoromethane

49.04 50 0 98.1 75 - 125 48.52 1.07 201.0Surr: Toluene-d8

The following samples were anayzed in this batch: HS15091001-16 HS15091001-17



Page 135 of 155

Client:Project:



QC BATCH REPORT


Sample ID: VBLKS1-092915 Units: ug/Kg Analysis Date: 29-Sep-2015 09:26



Value %RECControl

LimitRPD Ref


MBLK

Client ID:


















2-Butanone U 10

2-Hexanone U 10


4-Methyl-2-pentanone U 10

Acetone U 20

Benzene U 5.0


Bromoform U 5.0

Bromomethane U 10

Carbon disulfide U 10


Chlorobenzene U 5.0

Chloroethane U 10

Chloroform U 5.0

Chloromethane U 10





Page 136 of 155

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MBLK

Client ID:

Cyclohexane U 5.0



Ethylbenzene U 5.0




Methylene chloride U 10

Naphthalene U 5.0




Styrene U 5.0



Toluene U 5.0






Xylenes, Total U 10

45.1 50 0 90.2 70 - 1280Surr: 1,2-Dichloroethane-d4

49.23 50 0 98.5 73 - 1260Surr: 4-Bromofluorobenzene

48.63 50 0 97.3 71 - 1280Surr: Dibromofluoromethane

51.84 50 0 104 73 - 1270Surr: Toluene-d8



Page 137 of 155

Client:Project:



QC BATCH REPORT


Sample ID: VLCSS1-092915 Units: ug/Kg Analysis Date: 29-Sep-2015 08:39



Value %RECControl

LimitRPD Ref


LCS

Client ID:






1,1-Dichloroethane 53.16 50 0 106 75 - 1245.0

1,1-Dichloroethene 55.2 50 0 110 76 - 1285.0




1,2-Dibromoethane 52.46 50 0 105 70 - 1205.0


1,2-Dichloroethane 51.3 50 0 103 73 - 1215.0

1,2-Dichloropropane 53.49 50 0 107 75 - 1245.0




2-Butanone 108.2 100 0 108 65 - 13010

2-Hexanone 115.1 100 0 115 65 - 13310


4-Methyl-2-pentanone 115.9 100 0 116 69 - 13010

Acetone 112.2 100 0 112 53 - 14220

Benzene 53.45 50 0 107 79 - 1225.0

Bromodichloromethane 51.85 50 0 104 79 - 1215.0

Bromoform 52.23 50 0 104 74 - 1255.0

Bromomethane 63.74 50 0 127 68 - 13110

Carbon disulfide 111.7 100 0 112 78 - 13110


Chlorobenzene 52.11 50 0 104 79 - 1205.0

Chloroethane 50.71 50 0 101 74 - 12610

Chloroform 49.16 50 0 98.3 78 - 1225.0

Chloromethane 50.14 50 0 100 69 - 12910

cis-1,2-Dichloroethene 50.82 50 0 102 78 - 1225.0

cis-1,3-Dichloropropene 54.14 50 0 108 77 - 1235.0



Page 138 of 155

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


LCS

Client ID:

Cyclohexane 52.97 50 0 106 74 - 1265.0

Dibromochloromethane 52.91 50 0 106 78 - 1225.0


Ethylbenzene 54.54 50 0 109 80 - 1225.0


Methyl tert-butyl ether 53.49 50 0 107 76 - 1245.0


Methylene chloride 48.02 50 0 96.0 65 - 13010

Naphthalene 53.66 50 0 107 71 - 1285.0

n-Butylbenzene 51.65 50 0 103 77 - 1265.0

n-Propylbenzene 50.84 50 0 102 79 - 1235.0


Styrene 54.39 50 0 109 78 - 1245.0



Toluene 53.34 50 0 107 79 - 1205.0


trans-1,3-Dichloropropene 55.32 50 0 111 77 - 1205.0

Trichloroethene 54.49 50 0 109 75 - 1235.0


Vinyl chloride 52.83 50 0 106 76 - 1262.0

Xylenes, Total 163.9 150 0 109 80 - 12010


51.51 50 0 103 73 - 1260Surr: 4-Bromofluorobenzene


50.8 50 0 102 73 - 1270Surr: Toluene-d8



Page 139 of 155

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MS


1,1,1,2-Tetrachloroethane 48.14 48.5 0 99.3 79 - 1214.8

1,1,1-Trichloroethane 51.09 48.5 0 105 79 - 1284.8


1,1,2-Trichlor-1,2,2-trifluoroethane 49.37 48.5 0 102 76 - 1274.8


1,1-Dichloroethane 49.43 48.5 0 102 75 - 1244.8

1,1-Dichloroethene 52.62 48.5 0 108 76 - 1284.8

1,2,3-Trichlorobenzene 45.13 48.5 0 93.1 73 - 1264.8


1,2,4-Trimethylbenzene 45.32 48.5 0 93.5 79 - 1234.8

1,2-Dibromoethane 50.44 48.5 0 104 70 - 1204.8

1,2-Dichlorobenzene 46.78 48.5 0 96.4 75 - 1204.8

1,2-Dichloroethane 47.96 48.5 0 98.9 73 - 1214.8

1,2-Dichloropropane 49.71 48.5 0 102 75 - 1244.8




2-Butanone 110.8 97 0 114 65 - 1309.7

2-Hexanone 119.2 97 0 123 65 - 1339.7

4-Isopropyltoluene 46.29 48.5 0 95.4 80 - 1254.8


Acetone 110.7 97 0 114 53 - 14219

Benzene 51.26 48.5 0 106 79 - 1224.8

Bromodichloromethane 48.49 48.5 0 100.0 79 - 1214.8

Bromoform 51.53 48.5 0 106 74 - 1254.8

Bromomethane 59.94 48.5 0 124 68 - 1319.7


Carbon tetrachloride 49.3 48.5 0 102 74 - 1264.8

Chlorobenzene 49.43 48.5 0 102 79 - 1204.8

Chloroethane 49 48.5 0 101 74 - 1269.7

Chloroform 45.2 48.5 0 93.2 78 - 1224.8

Chloromethane 49.28 48.5 0 102 69 - 1299.7

cis-1,2-Dichloroethene 48.31 48.5 0 99.6 78 - 1224.8

cis-1,3-Dichloropropene 49.86 48.5 0 103 77 - 1234.8



Page 140 of 155

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MS


Cyclohexane 51.15 48.5 0 105 74 - 1264.8

Dibromochloromethane 50.11 48.5 0 103 78 - 1224.8

Dichlorodifluoromethane 49.93 48.5 0 103 57 - 1404.8

Ethylbenzene 51.57 48.5 0 106 80 - 1224.8

Isopropylbenzene 53.88 48.5 0 111 72 - 1274.8

Methyl tert-butyl ether 48.67 48.5 0 100 76 - 1244.8

Methylcyclohexane 51.88 48.5 0 107 77 - 1274.8

Methylene chloride 45.13 48.5 0 93.0 65 - 1309.7

Naphthalene 47.36 48.5 0 97.6 71 - 1284.8

n-Butylbenzene 45.27 48.5 0 93.3 77 - 1264.8

n-Propylbenzene 46.32 48.5 0 95.5 79 - 1234.8

sec-Butylbenzene 46.65 48.5 0 96.2 80 - 1234.8

Styrene 50.65 48.5 0 104 78 - 1244.8

tert-Butylbenzene 49.28 48.5 0 102 79 - 1244.8

Tetrachloroethene 64.4 48.5 0 133 70 - 130 S 4.8

Toluene 51.8 48.5 0.7132 105 79 - 1204.8

trans-1,2-Dichloroethene 50.42 48.5 0 104 79 - 1224.8

trans-1,3-Dichloropropene 50.37 48.5 0 104 77 - 1204.8

Trichloroethene 53.81 48.5 0 111 75 - 1234.8

Trichlorofluoromethane 51.16 48.5 0 105 75 - 1264.8

Vinyl chloride 52.36 48.5 0 108 76 - 1261.9

Xylenes, Total 154.4 145.5 0 106 80 - 1209.7

45.61 48.5 0 94.0 70 - 1280Surr: 1,2-Dichloroethane-d4

48.97 48.5 0 101 73 - 1260Surr: 4-Bromofluorobenzene

45.06 48.5 0 92.9 71 - 1280Surr: Dibromofluoromethane

48.32 48.5 0 99.6 73 - 1270Surr: Toluene-d8



Page 141 of 155

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MSD


1,1,1,2-Tetrachloroethane 46.15 48.5 0 95.2 79 - 121 48.14 4.22 304.8

1,1,1-Trichloroethane 47.44 48.5 0 97.8 79 - 128 51.09 7.4 304.8


1,1,2-Trichlor-1,2,2-trifluoroethane 48.03 48.5 0 99.0 76 - 127 49.37 2.75 304.8


1,1-Dichloroethane 46.45 48.5 0 95.8 75 - 124 49.43 6.21 304.8

1,1-Dichloroethene 50.97 48.5 0 105 76 - 128 52.62 3.19 304.8

1,2,3-Trichlorobenzene 43.93 48.5 0 90.6 73 - 126 45.13 2.7 304.8


1,2,4-Trimethylbenzene 43.44 48.5 0 89.6 79 - 123 45.32 4.24 304.8

1,2-Dibromoethane 49.19 48.5 0 101 70 - 120 50.44 2.51 304.8

1,2-Dichlorobenzene 45.06 48.5 0 92.9 75 - 120 46.78 3.74 304.8

1,2-Dichloroethane 43.63 48.5 0 90.0 73 - 121 47.96 9.46 304.8

1,2-Dichloropropane 47.13 48.5 0 97.2 75 - 124 49.71 5.33 304.8




2-Butanone 109 97 0 112 65 - 130 110.8 1.7 309.7

2-Hexanone 117.6 97 0 121 65 - 133 119.2 1.34 309.7

4-Isopropyltoluene 43.96 48.5 0 90.6 80 - 125 46.29 5.17 304.8

4-Methyl-2-pentanone 113.1 97 0 117 69 - 130 118.2 4.39 309.7

Acetone 114.3 97 0 118 53 - 142 110.7 3.28 3019

Benzene 48.48 48.5 0 100.0 79 - 122 51.26 5.57 304.8

Bromodichloromethane 44.59 48.5 0 91.9 79 - 121 48.49 8.38 304.8

Bromoform 48.31 48.5 0 99.6 74 - 125 51.53 6.44 304.8

Bromomethane 57.24 48.5 0 118 68 - 131 59.94 4.61 309.7


Carbon tetrachloride 47.28 48.5 0 97.5 74 - 126 49.3 4.18 304.8

Chlorobenzene 46.58 48.5 0 96.0 79 - 120 49.43 5.93 304.8

Chloroethane 46.12 48.5 0 95.1 74 - 126 49 6.06 309.7

Chloroform 41.9 48.5 0 86.4 78 - 122 45.2 7.59 304.8

Chloromethane 46.06 48.5 0 95.0 69 - 129 49.28 6.75 309.7

cis-1,2-Dichloroethene 45.18 48.5 0 93.2 78 - 122 48.31 6.69 304.8

cis-1,3-Dichloropropene 46.63 48.5 0 96.1 77 - 123 49.86 6.7 304.8



Page 142 of 155

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MSD


Cyclohexane 48.98 48.5 0 101 74 - 126 51.15 4.33 304.8

Dibromochloromethane 47.78 48.5 0 98.5 78 - 122 50.11 4.76 304.8

Dichlorodifluoromethane 47.53 48.5 0 98.0 57 - 140 49.93 4.91 304.8

Ethylbenzene 49.94 48.5 0 103 80 - 122 51.57 3.21 304.8

Isopropylbenzene 50.43 48.5 0 104 72 - 127 53.88 6.61 304.8

Methyl tert-butyl ether 45.85 48.5 0 94.5 76 - 124 48.67 5.96 304.8

Methylcyclohexane 49.19 48.5 0 101 77 - 127 51.88 5.31 304.8

Methylene chloride 41.47 48.5 0 85.5 65 - 130 45.13 8.46 309.7

Naphthalene 48.87 48.5 0 101 71 - 128 47.36 3.15 304.8

n-Butylbenzene 43.04 48.5 0 88.7 77 - 126 45.27 5.06 304.8

n-Propylbenzene 44.47 48.5 0 91.7 79 - 123 46.32 4.07 304.8

sec-Butylbenzene 44.44 48.5 0 91.6 80 - 123 46.65 4.84 304.8

Styrene 47.83 48.5 0 98.6 78 - 124 50.65 5.72 304.8

tert-Butylbenzene 46.94 48.5 0 96.8 79 - 124 49.28 4.86 304.8

Tetrachloroethene 61.17 48.5 0 126 70 - 130 64.4 5.14 304.8

Toluene 49.38 48.5 0.7132 100 79 - 120 51.8 4.76 304.8

trans-1,2-Dichloroethene 47.31 48.5 0 97.5 79 - 122 50.42 6.37 304.8

trans-1,3-Dichloropropene 47.58 48.5 0 98.1 77 - 120 50.37 5.7 304.8

Trichloroethene 50.93 48.5 0 105 75 - 123 53.81 5.5 304.8

Trichlorofluoromethane 49.15 48.5 0 101 75 - 126 51.16 4.01 304.8

Vinyl chloride 49.95 48.5 0 103 76 - 126 52.36 4.72 301.9

Xylenes, Total 146.8 145.5 0 101 80 - 120 154.4 5.08 309.7

46 48.5 0 94.8 70 - 128 45.61 0.848 300Surr: 1,2-Dichloroethane-d4

49.32 48.5 0 102 73 - 126 48.97 0.706 300Surr: 4-Bromofluorobenzene

44.62 48.5 0 92.0 71 - 128 45.06 0.979 300Surr: Dibromofluoromethane

49.25 48.5 0 102 73 - 127 48.32 1.91 300Surr: Toluene-d8




Page 143 of 155

Client:Project:



QC BATCH REPORT

Batch ID: R262070 Instrument: Balance1 Method: SW3550

Sample ID: HS15091001-09DUP Units: wt% Analysis Date: 25-Sep-2015 14:38

Run ID: Balance1_262070 SeqNo: 3440254 PrepDate: DF: 1


Value %RECControl

LimitRPD Ref


DUP


Percent Moisture 6.67 6.23 6.82 200.0100

The following samples were anayzed in this batch: HS15091001-01 HS15091001-02 HS15091001-03 HS15091001-04 HS15091001-05 HS15091001-06 HS15091001-07



Page 144 of 155

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


DUP

Client ID:


The following samples were anayzed in this batch: HS15091001-10 HS15091001-11 HS15091001-12 HS15091001-13 HS15091001-14 HS15091001-15



Page 145 of 155

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


DUP

Client ID:





Value %RECControl

LimitRPD Ref


DUP






Page 146 of 155

QUALIFIERS, ACRONYMS, UNITS

Client:Project:WorkOrder:


Qualifier Description* Value exceeds Regulatory Limit

a Not accredited

B Analyte detected in the associated Method Blank above the Reporting Limit

E Value above quantitation range

H Analyzed outside of Holding Time

J Analyte detected below quantitation limit

M Manually integrated, see raw data for justification

n Not offered for accreditation

ND Not Detected at the Reporting Limit

O Sample amount is > 4 times amount spiked

P Dual Column results percent difference > 40%

R RPD above laboratory control limit

S Spike Recovery outside laboratory control limits

U Analyzed but not detected above the MDL/SDL

Acronym DescriptionDCS Detectability Check Study

DUP Method Duplicate

LCS Laboratory Control Sample

LCSD Laboratory Control Sample Duplicate

MBLK Method Blank

MDL Method Detection Limit

MQL Method Quantitation Limit

MS Matrix Spike

MSD Matrix Spike Duplicate

PDS Post Digestion Spike

PQL Practical Quantitaion Limit

SD Serial Dilution

SDL Sample Detection Limit

TRRP Texas Risk Reduction Program

Unit Reported Descriptionmg/Kg-dry Milligrams per Kilogram- Dry weight corrected

mg/L Milligrams per Liter


Page 147 of 155

CERTIFICATIONS,ACCREDITATIONS & LICENSES

Agency Number Expire Date

Arkansas 15-024-0 27-Mar-2016

California 2919 31-Jul-2016

Dept of Defense L2231 Rev 3-20-2014 22-Dec-2015

Illinois 003622 09-May-2016

Kentucky KY 2015-2016 30-Apr-2016

Louisiana 03087 2015/2016 30-Jun-2016

North Carolina 624 - 2015 31-Dec-2015

Oklahoma 2015-047 31-Aug-2016

Texas T104704231-15-15 30-Apr-2016


Page 148 of 155

Client: PBW Houston

Work Order: HS15091001Project: CES Griggs Rd VCP SAMPLE TRACKING

Lab Samp ID Client Sample ID Action Date Person New Location

HS15091001-01 4904-SB19-03 Login 9/23/2015 3:13:32 PM PMG 7C

HS15091001-01 4904-SB19-03 Login 9/23/2015 3:13:32 PM PMG LF-13

HS15091001-01 4904-SB19-03 Login 9/23/2015 3:13:32 PM PMG 5035



HS15091001-02 4904-SB19-14 Login 9/23/2015 3:19:51 PM PMG 5035

HS15091001-03 4904-SB19-16.5 Login 9/23/2015 3:19:51 PM PMG 7C

HS15091001-03 4904-SB19-16.5 Login 9/23/2015 3:19:51 PM PMG LF-13

HS15091001-03 4904-SB19-16.5 Login 9/23/2015 3:19:51 PM PMG 5035



HS15091001-04 4904-SB20-02 Login 9/23/2015 3:19:51 PM PMG 5035



HS15091001-05 4904-SB20-07 Login 9/23/2015 3:19:51 PM PMG 5035



HS15091001-06 4904-SB20-19 Login 9/23/2015 3:19:51 PM PMG 5035



HS15091001-07 4904-SB21-04 Login 9/23/2015 3:19:51 PM PMG 5035



HS15091001-08 4904-SB21-10 Login 9/23/2015 3:19:51 PM PMG 5035

HS15091001-09 4904-SB21-16.5 Login 9/23/2015 3:19:51 PM PMG 7C


HS15091001-09 4904-SB21-16.5 Login 9/23/2015 3:19:51 PM PMG 5035



HS15091001-10 4904-SB22-03 Login 9/23/2015 3:19:51 PM PMG 5035



HS15091001-11 4904-SB22-05 Login 9/23/2015 3:24:38 PM PMG 5035



HS15091001-12 4904-SB22-20 Login 9/23/2015 3:24:38 PM PMG 5035



HS15091001-13 4904-SB23-04 Login 9/23/2015 3:24:38 PM PMG 5035



Page 149 of 155

Client: PBW Houston



HS15091001-14 4904-SB23-10 Login 9/23/2015 3:24:39 PM PMG 5035



HS15091001-15 4904-SB23-19 Login 9/23/2015 3:24:39 PM PMG 5035

HS15091001-16 TB01 092215 Login 9/23/2015 3:25:37 PM PMG VW-3


HS15091001-01 4904-SB19-03 Out 9/25/2015 8:22:52 AM AAP METPREP


HS15091001-03 4904-SB19-16.5 Out 9/25/2015 8:22:52 AM AAP METPREP













HS15091001-01 4904-SB19-03 Return 9/25/2015 2:49:15 PM AAP 7C


HS15091001-03 4904-SB19-16.5 Return 9/25/2015 2:49:15 PM AAP 7C






HS15091001-09 4904-SB21-16.5 Return 9/25/2015 2:49:15 PM AAP 7C







HS15091001-01 4904-SB19-03 Out 9/28/2015 11:46:50 AM OFO METPREP


HS15091001-03 4904-SB19-16.5 Out 9/28/2015 11:46:50 AM OFO METPREP




Page 150 of 155

Client: PBW Houston












HS15091001-01 4904-SB19-03 Return 9/28/2015 11:53:41 AM OFO 7C


HS15091001-03 4904-SB19-16.5 Return 9/28/2015 11:53:41 AM OFO 7C






HS15091001-09 4904-SB21-16.5 Return 9/28/2015 11:53:41 AM OFO 7C








Page 151 of 155

PS

23-Sep-2015 12:29Date/Time Received:

HS15091001

PBW - Houston

Work Order:

Client Name:

Sample Receipt Checklist

Received by:

Shipping container/cooler in good condition?

Custody seals intact on shipping container/cooler?

Custody seals intact on sample bottles?

Chain of custody present?

Chain of custody signed when relinquished and received?

Chain of custody agrees with sample labels?

Samples in proper container/bottle?

Sample containers intact?

Sufficient sample volume for indicated test?

All samples received within holding time?

Container/Temp Blank temperature in compliance?

Temperature(s)/Thermometer(s):

Cooler(s)/Kit(s):

Date/Time sample(s) sent to storage:

Water - VOA vials have zero headspace?

Water - pH acceptable upon receipt?

pH adjusted?

pH adjusted by:

Login Notes:

No Not Present

Yes No Not Present

Yes No Not Present

Yes No

Yes No

Yes No

Yes No

Yes No

Yes No

Yes No

Yes No

0.7c/0.6c,0.4c/0.3c,0.8c/0.7c U/C IR15613,4295, Red9/23/15 16:40

Yes No No VOA vials submitted

Yes No N/A

Yes No N/A

Terracore vials not labeled. 4904-SB21-10:COC time=14:20 & labels=14:15.Logged per COC; 4904-SB21-16.5:1x4oz jar label has no depth. 4904SB-2-16.5 & 4904-SB22-20-5035 Bulk jars no sample. 4904-SB19-03:1xTPH vial 5g only. Sufficient volume remains.

Checklist completed by: Paresh M. GigaDateeSignatureDateeSignature

25-Sep-201523-Sep-2015

ALS CourierSoil/Water Carrier name:Matrices:

Reviewed by: Dane J. Wacasey

Client Contacted: Date Contacted: Person Contacted:

Contacted By: Regarding:

Comments:

Corrective Action:

0

Yes

NoYesTX1005 solids received in hermetically sealed vials? N/A


Page 152 of 155

Page 153 of 155

Page 154 of 155

Page 155 of 155

October 02, 2015





Sincerely,

ALS Environmental received 24 sample(s) on Sep 24, 2015 for the analysis presented in the following report.


Dear Brenda,



Dane J. Wacasey


Page 1 of 261


WorkOrder:














ALS Group USA, Corp Date: 02-Oct-15

Page 2 of 261


WorkOrder:


Dane J. Wacasey




Page 3 of 261



Reviewer Name: Dane Wacasey

Prep Batch Number(s): 97447, 97456, 97466, 97468, 97500, 97510, 97516, 97519, 97544, 97547, 97632, R261940, R262045, R262131, R262143, R262216, R262267, R262409




Were all departures from standard conditions described in an exception report? X R2 OI Sample and quality control (QC) identification Are all field sample ID numbers cross-referenced to the laboratory ID numbers? X Are all laboratory ID numbers cross-referenced to the corresponding QC data? X R3 OI Test reports Were all samples prepared and analyzed within holding times? X 1





Were surrogate percent recoveries in all samples within the laboratory QC limits? X 2





Were LCSs analyzed at the required frequency? X Were LCS (and LCSD, if applicable) %Rs within the laboratory QC limits? X 3


Was the LCSD RPD within QC limits? X R7 OI Matrix spike (MS) and matrix spike duplicate (MSD) data Were the project/method specified analytes included in the MS and MSD? X Were MS/MSD analyzed at the appropriate frequency? X 4 Were MS (and MSD, if applicable) %Rs within the laboratory QC limits? X 5 Were MS/MSD RPDs within laboratory QC limits? X 6 R8 OI Analytical duplicate data Were appropriate analytical duplicates analyzed for each matrix? X Were analytical duplicates analyzed at the appropriate frequency? X Were RPDs or relative standard deviations within the laboratory QC limits? X R9 OI Method quantitation limits (MQLs): Are the MQLs for each method analyte included in the laboratory data package? X






Is the laboratory NELAC-accredited under the Texas Laboratory Program for the analytes, matrices and methods associated with this laboratory data package? X 7

Page 4 of 261

Laboratory Review Checklist: Reportable Data Laboratory Name: ALS Laboratory Group LRC Date: 10/02/2015 Project Name: CES Griggs Rd VCP Laboratory Job Number: HS15091078











continuing calibration blank (CCB) Was the CCV analyzed at the method-required frequency? X Were percent differences for each analyte within the method-required QC limits? X 8 Was the ICAL curve verified for each analyte? X Was the absolute value of the analyte concentration in the inorganic CCB < MDL? X 9 S3 O Mass spectral tuning: Was the appropriate compound for the method used for tuning? X Were ion abundance data within the method-required QC limits? X S4 O Internal standards (IS): Were IS area counts and retention times within the method-required QC limits? X






Were percent differences, recoveries, and the linearity within the QC limits specified in the method? X 10









Page 5 of 261





ER#5 Description

1

Sample received outside method holding time for pH. pH is an immediate test. Sample results are flagged with an "H" qualifier. The temperature at the time of pH is reported. Please note that all pH results are already normalized to a temperature of 25 degrees C.

2 Semivolatile Organics Method SW8270, sample 4904-SB11-00, surrogate 2,4,6-Tribromophenol recovered above the upper control limits due to suspect matrix effect.

3 Batch 97500, Semivolatile Organics, LCSD RPD was above the control limits for Pentachlorophenol. The individual recoveries were in control.

4 Batch 97500, Semivolatile Organics, Insufficient sample to perform MS/MSD. LCS/LCSD provided as batch quality control.

5

Batch 97447, Metals Method SW6020, sample HS15091053-16, MS and MSD were performed on unrelated sample. Batch 97519, Metals Method SW6020, sample 4904-SB10-08, MS and or MSD recovered outside the control limits for antimony, barium, manganese and vanadium, however, the results in the parent sample is greater than 4x the spike amount. Batch 97544, Metals Method SW6020, sample 4904-SB16-21.5, MS and or MSD recovered outside the control limits for multiple compounds, however the results in the parent sample is greater than 4x the spike amount for Barium and Manganese. Batch R262131, Volatile Organics Method SW8260, sample HS15091001-09, MS and MSD were performed on unrelated sample. Batch R262216, Volatile Organics Method SW8260, sample 4904-SB10-08, MS recovered outside the control limits for some few compounds.

6

Batch 97466; Texas TPH by TX1005 sample EB 092315,MS/MSD RPD recovered above the RPD limits for nC6 to nC12 and 2-Fluorobiphenyl. Individual recoveries were within criteria. Batch 97544, Metals Method SW6020, sample 4904-SB16-21.5, MSD RPD recovered above the RPD limits for Barium, Lead and Manganese. Batch R262409, Volatile Organics Method SW8260, sample 4904-SB16-21.5, MSD RPD recovered above the RPD limits for Bromoform.

7

With the exception of Volatile Organics Method SW8260 Cyclohexane and Semivolatile Organics Method SW8270 1-Methylnaphthalene and Benzaldehyde, ALS is NELAC-accredited under the Texas Laboratory Program for the analytes, matrices and methods associated with this laboratory data package. Because TCEQ does not offer accreditation for these compounds, the results are flagged with n.

8

Batch R261970, Volatile Organics Method SW8260: 2,2-Dichloropropane exceeded %D (125%) exceeded control limits (80-120) in the CCV and cis-1,3-Dichloropropene exceeded %D (122%) exceeded control limits (80-120) in the CCV. The analytes were not detected in the associated samples. Batch R262131, Volatile Organics Method SW8260: Bromomethane exceeded %D (122%) exceeded control limits (80-120) in the CCV; Bromomethane was not detected in any of the associated samples. Batch R262216, Volatile Organics Method SW8260: Bromomethane exceeded %D (122%) exceeded control limits (80-120) in the CCV; Bromomethane was not detected in any of the associated samples.

9 See Run Log and CCB Exceptions Report.

10

Batch 97447, Metals Method SW6020, sample HS15091053-16 Bench Spike (PDS) was performed on unrelated sample. Batch 97519, Metals Method SW6020, sample 4904-SB10-08, Bench Spike (PDS) recovered above the control limits for Barium, however, the parent sample is greater than 4x the spike amount.


Page 6 of 261







ICPMS03



13:24AG AS BA BE CD CO CR CU MN NI PB SB SE TL V ZN010ICV1.D#

LLICV5 1 29-Sep-2015 13:28

AG AS BA CD CO CR CU MN NI PB SB SE V ZN011SMPL.D#

LLICV2 1 29-Sep-2015 13:32


ICB 1 29-Sep-2015 13:37

AG AS BA BE CD CO CR CU MN NI PB SB SE TL V ZN013_ICB.D#

ICSA 1 29-Sep-2015 13:41


ICSAB 1 29-Sep-2015 13:45


CCV 1 1 29-Sep-2015 14:25

AG AS BA BE CD CO CR CU MN NI PB SB SE TL V ZN024SMPL.D#

CCB 1 1 29-Sep-2015 14:29

AG AS BA BE CD CO CR CU MN NI PB SB SE TL V ZN025_CCB.D#

CCV 2 1 29-Sep-2015 15:08


CCB 2 1 29-Sep-2015 15:12


CCV 3 1 29-Sep-2015 15:44


CCB 3 1 29-Sep-2015 15:48


CCV 4 1 29-Sep-2015 16:18


CCB 4 1 29-Sep-2015 16:23


ICCV 5 1 29-Sep-2015 17:50


LLCCV5 1 29-Sep-2015 17:54


ICCB 5 1 29-Sep-2015 18:02


LLCCV2 1 29-Sep-2015 18:11


CCV 6 1 29-Sep-2015 18:24

AG AS BA BE CD CO CR CU MN NI PB SB SE TL V ZN078CCV1.D#

CCB 6 1 29-Sep-2015 18:28


CCV 7 1 29-Sep-2015 18:50


CCB 7 1 29-Sep-2015 18:54


CCV 8 1 29-Sep-2015 19:20


CCB 8 1 29-Sep-2015 19:25


CCV 9 1 29-Sep-2015 19:46


CCB 9 1 29-Sep-2015 19:51


MBLK-97544 1 29-Sep-2015 19:55


MLCS-97544 1 29-Sep-2015 19:59


CCV 10 1 29-Sep-2015 20:03


CCB 10 1 29-Sep-2015 20:08


4904-SB16-09 1 29-Sep-2015 20:12

AG AS CD CO CR CU NI PB SB SE V ZN103SMPL.D#

4904-SB16-21.5 1 29-Sep-2015 20:16


4904-SB16-21.5SD 5 29-Sep-2015 20:21


02-Oct-15Date: ALS Group USA, Corp

Page 7 of 261







ICPMS03


FileID4904-SB16-21.5MS 1 29-Sep-2015

20:25AG AS BA CD CO CR CU MN NI PB SB SE V ZN106SMPL.D#

4904-SB16-21.5MSD 1 29-Sep-2015 20:29


4904-SB16-21.5PDS 1 29-Sep-2015 20:34

AG AS CD CO CR CU NI PB SB SE V108SMPL.D#

4904-SB17-00 1 29-Sep-2015 20:38


4904-SB17-09 1 29-Sep-2015 20:42


CCV 11 1 29-Sep-2015 20:46


CCB 11 1 29-Sep-2015 20:51


4904-SB17-22 1 29-Sep-2015 20:55

AG AS BA CD CO CR CU NI PB SB SE V ZN113SMPL.D#

CCV 12 1 29-Sep-2015 21:30


CCB 12 1 29-Sep-2015 21:34


CCV 13 1 29-Sep-2015 22:13


CCB 13 1 29-Sep-2015 22:17


LLICV2 1 29-Sep-2015 22:21


LLICV5 1 29-Sep-2015 22:26


ICSA 1 29-Sep-2015 22:30


ICSAB 1 29-Sep-2015 22:34



Page 8 of 261







ICPMS03



12:51AG AS BA BE CD CO CR CU MN NI PB SB SE TL V ZN010ICV1.D#

LLICV2 1 30-Sep-2015 12:59

BA BE MN TL012SMPL.D#

ICB 1 30-Sep-2015 13:04

AG AS BA BE CD CO CR CU MN NI PB SB SE TL V ZN013_ICB.D#

LLICV5 1 30-Sep-2015 13:09


ICSA 1 30-Sep-2015 13:18


ICSAB 1 30-Sep-2015 13:22


CCV 1 1 30-Sep-2015 13:45


CCB 1 1 30-Sep-2015 13:49


CCV 2 1 30-Sep-2015 14:28


CCB 2 1 30-Sep-2015 14:33


MBLK-97544 1 30-Sep-2015 14:37

BE TL034SMPL.D#

MLCS-97544 1 30-Sep-2015 14:41

BE TL035SMPL.D#

4904-SB16-09 10 30-Sep-2015 14:46

BA MN036SMPL.D#

4904-SB16-21.5 5 30-Sep-2015 14:50

BA MN037SMPL.D#

4904-SB16-21.5SD 25 30-Sep-2015 14:54

BA MN038SMPL.D#

4904-SB16-21.5PDS 5 30-Sep-2015 14:58

BA MN039SMPL.D#

4904-SB17-09 10 30-Sep-2015 15:03

BA MN040SMPL.D#

4904-SB17-22 10 30-Sep-2015 15:07

MN041SMPL.D#

CCV 3 1 30-Sep-2015 15:11


CCB 3 1 30-Sep-2015 15:16


4904-SB16-09 1 30-Sep-2015 15:20

BE TL044SMPL.D#

4904-SB16-21.5 1 30-Sep-2015 15:24

BE TL045SMPL.D#

4904-SB16-21.5SD 5 30-Sep-2015 15:29

BE TL046SMPL.D#

4904-SB16-21.5MS 1 30-Sep-2015 15:33

BE TL047SMPL.D#

4904-SB16-21.5MSD 1 30-Sep-2015 15:37

BE TL048SMPL.D#

4904-SB16-21.5PDS 1 30-Sep-2015 15:42

BE TL ZN049SMPL.D#

4904-SB17-00 1 30-Sep-2015 15:47

BE TL050SMPL.D#

4904-SB17-09 1 30-Sep-2015 15:51

BE TL051SMPL.D#

CCV 4 1 30-Sep-2015 15:55


CCB 4 1 30-Sep-2015 15:59


4904-SB17-22 1 30-Sep-2015 16:04

BE TL054SMPL.D#

CCV 5 1 30-Sep-2015 16:21


CCB 5 1 30-Sep-2015 16:25



Page 9 of 261







ICPMS03


FileIDCCV 6 1 30-Sep-2015

16:51AG AS BA BE CD CO CR CU MN NI PB SB SE TL V ZN065SMPL.D#

CCB 6 1 30-Sep-2015 16:55


CCV 7 1 30-Sep-2015 17:08


CCB 7 1 30-Sep-2015 17:13


CCV 8 1 30-Sep-2015 17:51


CCB 8 1 30-Sep-2015 17:56


CCV 9 1 30-Sep-2015 18:39


CCB 9 1 30-Sep-2015 18:43


CCV 10 1 30-Sep-2015 19:14


CCB 10 1 30-Sep-2015 19:18


LLICV2 1 30-Sep-2015 19:22


LLICV5 1 30-Sep-2015 19:27


ICSA 1 30-Sep-2015 19:31


ICSAB 1 30-Sep-2015 19:35



Page 10 of 261







ICPMS04




LLICV5 1 29-Sep-2015 11:00


LLICV2 1 29-Sep-2015 11:05


ICB 1 29-Sep-2015 11:09


ICSA 1 29-Sep-2015 11:14


ICSAB 1 29-Sep-2015 11:18


CCV 1 1 29-Sep-2015 11:58


CCB 1 1 29-Sep-2015 12:02


CCV 2 1 29-Sep-2015 12:41


CCB 2 1 29-Sep-2015 12:45


CCV 3 1 29-Sep-2015 13:29


CCB 3 1 29-Sep-2015 13:34


CCV 4 1 29-Sep-2015 14:13


CCB 4 1 29-Sep-2015 14:17


CCV 5 1 29-Sep-2015 15:05


CCB 5 1 29-Sep-2015 15:09


CCV 6 1 29-Sep-2015 15:29


CCB 6 1 29-Sep-2015 15:34


LLCCV5 1 29-Sep-2015 16:18


LLCCV2 1 29-Sep-2015 16:23


ICCB 7 1 29-Sep-2015 16:27


ICCV 7 1 29-Sep-2015 16:32


CCV 8 1 29-Sep-2015 17:15


CCB 8 1 29-Sep-2015 17:20


CCV 9 1 29-Sep-2015 18:03


CCB 9 1 29-Sep-2015 18:08


ICSA 1 29-Sep-2015 18:43


ICSAB 1 29-Sep-2015 18:47


CCV 10 1 29-Sep-2015 18:56


CCB 10 1 29-Sep-2015 19:00


MBLK-97519 1 29-Sep-2015 19:05

AG AS BA BE CD CO CR CU MN NI PB SB SE TL V ZN120SMPL_15I29k00.D

MLCS-97519 1 29-Sep-2015 19:10


4904-SB03-01 1 29-Sep-2015 19:14

AG AS BE CD CO CR CU NI PB SB SE TL V ZN122SMPL_15I29k00.D


Page 11 of 261







ICPMS04


FileID4904-SB03-01 Dup 1 29-Sep-2015

19:18AG AS BA BE CD CO CR CU NI PB SB SE TL V ZN123SMPL_15I29k00.D

4904-SB03-02 1 29-Sep-2015 19:22


4904-SB03-12 1 29-Sep-2015 19:27


4904-SB10-01 1 29-Sep-2015 19:31

AG AS BE CD CO CR CU MN NI PB SB SE TL V ZN126SMPL_15I29k00.D

4904-SB10-05 1 29-Sep-2015 19:36


CCV 11 1 29-Sep-2015 19:40

AG AS BA BE CD CO CR CU MN NI PB SB SE TL V ZN128CCV_15I29k00.D

CCB 11 1 29-Sep-2015 19:44

AG AS BA BE CD CO CR CU MN NI PB SB SE TL V ZN129CCB_15I29k00.D

4904-SB10-08 1 29-Sep-2015 19:49

AG AS BA BE CD CO CR CU NI PB SB SE TL V ZN130SMPL_15I29k00.D

4904-SB10-08SD 5 29-Sep-2015 19:53


4904-SB10-08MS 1 29-Sep-2015 19:58


4904-SB10-08MSD 1 29-Sep-2015 20:02


4904-SB10-08PDS 1 29-Sep-2015 20:07


4904-SB11-00 1 29-Sep-2015 20:11


4904-SB11-04 1 29-Sep-2015 20:15


CCV 12 1 29-Sep-2015 20:20


CCB 12 1 29-Sep-2015 20:24


4904-SB11-09 1 29-Sep-2015 20:28


4904-SB11-09 Dup 1 29-Sep-2015 20:33


4904-SB13-02 1 29-Sep-2015 20:37


4904-SB13-10 1 29-Sep-2015 20:42

AG AS BE CD CO CR CU NI PB SB SE TL V ZN142SMPL_15I29k00.D

4904-SB13-25 1 29-Sep-2015 20:46


4904-SB16-04 1 29-Sep-2015 20:51


CCV 13 1 29-Sep-2015 21:08


CCB 13 1 29-Sep-2015 21:13


CCV 14 1 29-Sep-2015 21:52


CCB 14 1 29-Sep-2015 21:57


CCV 15 1 29-Sep-2015 22:36


CCB 15 1 29-Sep-2015 22:40


LLCCV2 1 29-Sep-2015 22:45


LLCCV5 1 29-Sep-2015 22:49


ICSA 1 29-Sep-2015 22:54


ICSAB 1 29-Sep-2015 22:58



Page 12 of 261







ICPMS05



11:15AG AS BA BE CD CO CR CU MN NI PB SB SE TL V ZN010_ICV.d

LLICV5 1 28-Sep-2015 11:18

AG AS BA BE CD CO CR CU MN NI PB SB SE TL V ZN011LICV.d

LLICV2 1 28-Sep-2015 11:20

AG AS BA BE CD CO CR CU MN NI PB SB SE TL V ZN012SMPL.d

ICB 1 28-Sep-2015 11:23

AG AS BA BE CD CO CR CU MN NI PB SB SE TL V ZN013_ICB.d

ICSA 1 28-Sep-2015 11:26

AG AS BA BE CD CO CR CU MN NI PB SB SE TL V ZN014ICSA.d

ICSAB 1 28-Sep-2015 11:28

AG AS BA BE CD CO CR CU MN NI PB SB SE TL V ZN015ICSB.d

CCV 1 1 28-Sep-2015 11:47

AG AS BA BE CD CO CR CU MN NI PB SB SE TL V ZN022_CCV.d

CCB 1 1 28-Sep-2015 11:49

AG AS BA BE CD CO CR CU MN NI PB SB SE TL V ZN023_CCB.d

CCV 2 1 28-Sep-2015 12:18


CCB 2 1 28-Sep-2015 12:21


CCV 3 1 28-Sep-2015 12:49


CCB 3 1 28-Sep-2015 12:52


CCV 4 1 28-Sep-2015 13:21


CCB 4 1 28-Sep-2015 13:24


CCV 5 1 28-Sep-2015 13:26


ICCV 6 1 28-Sep-2015 13:55

AG AS BA BE CD CO CR CU MN NI PB SB SE TL V ZN071_ICV.d

LLCCV5 1 28-Sep-2015 13:58


LLCCV2 1 28-Sep-2015 14:01


ICCB 5 1 28-Sep-2015 14:03


CCV 7 1 28-Sep-2015 14:19


CCB 6 1 28-Sep-2015 14:21


CCV 8 1 28-Sep-2015 14:47


CCB 7 1 28-Sep-2015 14:50


MBLK-97447 1 28-Sep-2015 14:53


MLCS-97447 1 28-Sep-2015 14:55


ZZZZZZSD 5 28-Sep-2015 15:06


ZZZZZZMS 1 28-Sep-2015 15:09


ZZZZZZMSD 1 28-Sep-2015 15:11


ZZZZZZPDS 1 28-Sep-2015 15:14


CCV 9 1 28-Sep-2015 15:19


CCB 8 1 28-Sep-2015 15:22


CCV 10 1 28-Sep-2015 15:24


EB 092315 1 28-Sep-2015 15:46



Page 13 of 261







ICPMS05


FileIDCCV 11 1 28-Sep-2015

15:51AG AS BA BE CD CO CR CU MN NI PB SB SE TL V ZN115_CCV.d

CCB 9 1 28-Sep-2015 15:56


ICCV 12 1 28-Sep-2015 16:25

AG AS BA BE CD CO CR CU MN NI PB SB SE TL V ZN127_ICV.d

LLCCV5 1 28-Sep-2015 16:27


LLCCV2 1 28-Sep-2015 16:30


ICCB 10 1 28-Sep-2015 16:32


CCV 13 1 28-Sep-2015 16:50


CCB 11 1 28-Sep-2015 16:53


CCV 14 1 28-Sep-2015 17:22


CCB 12 1 28-Sep-2015 17:24


CCV 15 1 28-Sep-2015 17:53


CCB 13 1 28-Sep-2015 17:56


CCV 16 1 28-Sep-2015 18:06


CCB 14 1 28-Sep-2015 18:09


LLCCV5 1 28-Sep-2015 18:11


LLCCV2 1 28-Sep-2015 18:14


ICSA 1 28-Sep-2015 18:16

AG AS BA BE CD CO CR CU MN NI PB SB SE TL V ZN170ICSA.d

ICSAB 1 28-Sep-2015 18:19

AG AS BA BE CD CO CR CU MN NI PB SB SE TL V ZN171ICSB.d


Page 14 of 261






ICPMS03


Units: ug/L

0.4717 0.4 5Antimony


Units: ug/L

0.5916 0.4 5Antimony1.392 1.1 5Selenium


Units: ug/L

0.4236 0.4 5Antimony1.164 1.1 5Selenium


Units: ug/L

0.5991 0.4 5Antimony0.4348 0.4 5Arsenic

1.616 1.1 5Selenium

Seq: 3443501ICCB 5 129-Sep-2015 18:02 D/F:Date:Analyte Result MDL Report Limit

Units: ug/L

-0.3333 0.2 2Cadmium-0.4559 0.2 5Silver


Units: ug/L


-0.2661 0.2 5Silver


Units: ug/L

-0.3194 0.2 5Silver


Units: ug/L


-0.3033 0.2 5Silver


Units: ug/L

0.4011 0.4 5Arsenic-0.2792 0.2 5Silver

3.11 2 5Zinc


Units: ug/L

0.4708 0.4 5Arsenic-0.2903 0.2 5Silver


Units: ug/L

0.4994 0.4 5Arsenic-0.2821 0.2 5Silver


Page 15 of 261






ICPMS03


Units: ug/L

0.4787 0.4 5Arsenic1.177 1.1 5Selenium

-0.275 0.2 5Silver


Units: ug/L

0.4924 0.4 5Arsenic-0.2921 0.2 5Silver


Page 16 of 261






ICPMS03

Seq: 3444966ICB 130-Sep-2015 13:04 D/F:Date:Analyte Result MDL Report Limit

Units: ug/L

0.2843 0.2 2Beryllium0.353 0.2 2Thallium


Units: ug/L



Units: ug/L



Units: ug/L



Units: ug/L



Units: ug/L



Units: ug/L



Units: ug/L



Units: ug/L



Units: ug/L



Units: ug/L



Page 17 of 261






ICPMS04


Units: ug/L

0.944 0.6 5Vanadium


Units: ug/L


1.05 0.6 5Vanadium


Units: ug/L



Units: ug/L



Units: ug/L

0.82 0.7 5Manganese1.453 1.1 5Selenium0.205 0.2 2Thallium


Units: ug/L



Units: ug/L

0.25 0.2 2Thallium


Units: ug/L

0.878 0.7 5Manganese0.267 0.2 2Thallium


Units: ug/L

0.288 0.2 2Thallium


Units: ug/L

0.269 0.2 2Thallium


Units: ug/L

0.306 0.2 2Thallium


Units: ug/L

0.342 0.2 2Thallium


Page 18 of 261






ICPMS04


Units: ug/L

0.292 0.2 2Thallium


Units: ug/L

0.307 0.2 2Thallium


Page 19 of 261






ICPMS05


Units: ug/L

0.364 0.2 2Thallium


Units: ug/L

0.374 0.2 2Thallium


Units: ug/L

0.451 0.4 5Chromium0.339 0.2 2Thallium0.709 0.6 5Vanadium


Units: ug/L

0.498 0.4 5Chromium0.352 0.2 2Thallium


Units: ug/L

0.32 0.2 2Thallium


Units: ug/L

0.343 0.2 2Thallium


Units: ug/L

0.319 0.2 2Thallium


Units: ug/L

0.233 0.2 2Thallium-0.603 0.6 5Vanadium


Units: ug/L

0.314 0.2 2Thallium


Units: ug/L

0.331 0.2 2Thallium


Units: ug/L

0.925 0.7 5Manganese0.34 0.2 2Thallium


Units: ug/L

0.31 0.2 2Thallium


Page 20 of 261

Client: PBW Houston



HS15091078-01 23-Sep-2015 09:10 24-Sep-2015 12:574904-SB03-01 Soil

HS15091078-02 23-Sep-2015 09:10 24-Sep-2015 12:574904-SB03-01 Dup Soil

HS15091078-03 23-Sep-2015 09:10 24-Sep-2015 12:574904-SB03-02 Soil

HS15091078-04 23-Sep-2015 09:20 24-Sep-2015 12:574904-SB03-12 Soil

HS15091078-05 23-Sep-2015 17:50 24-Sep-2015 12:574904-SB10-01 Soil

HS15091078-06 23-Sep-2015 17:55 24-Sep-2015 12:574904-SB10-05 Soil

HS15091078-07 23-Sep-2015 18:00 24-Sep-2015 12:574904-SB10-08 Soil

HS15091078-08 23-Sep-2015 16:40 24-Sep-2015 12:574904-SB11-00 Soil

HS15091078-09 23-Sep-2015 16:40 24-Sep-2015 12:574904-SB11-04 Soil

HS15091078-10 23-Sep-2015 16:45 24-Sep-2015 12:574904-SB11-09 Soil

HS15091078-11 23-Sep-2015 16:45 24-Sep-2015 12:574904-SB11-09 Dup Soil

HS15091078-12 23-Sep-2015 15:20 24-Sep-2015 12:574904-SB13-02 Soil

HS15091078-13 23-Sep-2015 15:25 24-Sep-2015 12:574904-SB13-10 Soil

HS15091078-14 23-Sep-2015 15:25 24-Sep-2015 12:574904-SB13-25 Soil

HS15091078-15 23-Sep-2015 13:25 24-Sep-2015 12:574904-SB16-04 Soil

HS15091078-16 23-Sep-2015 13:30 24-Sep-2015 12:574904-SB16-09 Soil

HS15091078-17 23-Sep-2015 13:35 24-Sep-2015 12:574904-SB16-21.5 Soil

HS15091078-18 23-Sep-2015 11:15 24-Sep-2015 12:574904-SB17-00 Soil

HS15091078-19 23-Sep-2015 11:10 24-Sep-2015 12:574904-SB17-09 Soil

HS15091078-20 23-Sep-2015 11:15 24-Sep-2015 12:574904-SB17-22 Soil

HS15091078-21 23-Sep-2015 18:15 24-Sep-2015 12:57EB 092315 Water




ALS Group USA, Corp 02-Oct-15Date:

Page 21 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-01


ANALYTICAL REPORT




















1mg/Kg-dry 29-Sep-2015 16:520.00142-Butanone 0.0110.015
























Page 22 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-01


ANALYTICAL REPORT


























Page 23 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-01


ANALYTICAL REPORT






























1mg/Kg-dry 30-Sep-2015 18:33J 0.00061Acenaphthene 0.00400.00090

1mg/Kg-dry 30-Sep-2015 18:33J 0.0012Acenaphthylene 0.00400.0018



1mg/Kg-dry 30-Sep-2015 18:33J 0.00061Anthracene 0.00400.0031

1mg/Kg-dry 30-Sep-2015 18:330.0019Benz(a)anthracene 0.00400.0059


1mg/Kg-dry 30-Sep-2015 18:330.0012Benzo(a)pyrene 0.00400.0064

1mg/Kg-dry 30-Sep-2015 18:330.0015Benzo(b)fluoranthene 0.00400.010

1mg/Kg-dry 30-Sep-2015 18:330.00085Benzo(g,h,i)perylene 0.00400.0093

1mg/Kg-dry 30-Sep-2015 18:33J 0.0011Benzo(k)fluoranthene 0.00400.0038





Page 24 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-01


ANALYTICAL REPORT








1mg/Kg-dry 30-Sep-2015 18:33J 0.0015Carbazole 0.00800.0025

1mg/Kg-dry 30-Sep-2015 18:330.00097Chrysene 0.00400.0077








1mg/Kg-dry 30-Sep-2015 18:33J 0.0013Fluorene 0.00400.0015





1mg/Kg-dry 30-Sep-2015 18:330.00097Indeno(1,2,3-cd)pyrene 0.00400.011









1mg/Kg-dry 30-Sep-2015 18:330.00073Pyrene 0.00400.011










Page 25 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-01


ANALYTICAL REPORT












1mg/Kg-dry 29-Sep-2015 19:140.0574Lead 0.57451.6







1mg/Kg-dry 29-Sep-2015 19:140.287Zinc 0.574116













Page 26 of 261


PBW HoustonCES Griggs Rd VCP4904-SB03-01 Dup

WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-02


ANALYTICAL REPORT












1mg/Kg-dry 29-Sep-2015 17:160.00111,2,4-Trimethylbenzene 0.00490.0049
































Page 27 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-02


ANALYTICAL REPORT


























Page 28 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-02


ANALYTICAL REPORT




1mg/Kg-dry 01-Oct-2015 15:220.00211,1´-Biphenyl 0.0082U

1mg/Kg-dry 01-Oct-2015 15:220.00121,2,4,5-Tetrachlorobenzene 0.0082U

1mg/Kg-dry 01-Oct-2015 15:22n 0.00191-Methylnaphthalene 0.0041U

1mg/Kg-dry 01-Oct-2015 15:220.00362,3,4,6-Tetrachlorophenol 0.0082U

1mg/Kg-dry 01-Oct-2015 15:220.00312,4,5-Trichlorophenol 0.0082U

1mg/Kg-dry 01-Oct-2015 15:220.00212,4,6-Trichlorophenol 0.0082U

1mg/Kg-dry 01-Oct-2015 15:220.00162,4-Dichlorophenol 0.0082U

1mg/Kg-dry 01-Oct-2015 15:220.00412,4-Dimethylphenol 0.0082U

1mg/Kg-dry 01-Oct-2015 15:220.00562,4-Dinitrophenol 0.016U

1mg/Kg-dry 01-Oct-2015 15:220.00112,4-Dinitrotoluene 0.0082U

1mg/Kg-dry 01-Oct-2015 15:220.00412,6-Dinitrotoluene 0.0082U

1mg/Kg-dry 01-Oct-2015 15:220.00162-Chloronaphthalene 0.0082U

1mg/Kg-dry 01-Oct-2015 15:220.00162-Chlorophenol 0.0082U

1mg/Kg-dry 01-Oct-2015 15:220.000622-Methylnaphthalene 0.0041U

1mg/Kg-dry 01-Oct-2015 15:220.00142-Methylphenol 0.0082U

1mg/Kg-dry 01-Oct-2015 15:220.00242-Nitroaniline 0.0082U

1mg/Kg-dry 01-Oct-2015 15:220.00312-Nitrophenol 0.0082U

1mg/Kg-dry 01-Oct-2015 15:22J 0.00123&4-Methylphenol 0.00820.0022

1mg/Kg-dry 01-Oct-2015 15:220.00313,3´-Dichlorobenzidine 0.0082U


1mg/Kg-dry 01-Oct-2015 15:220.00264,6-Dinitro-2-methylphenol 0.0082U

1mg/Kg-dry 01-Oct-2015 15:220.00204-Bromophenyl phenyl ether 0.0082U

1mg/Kg-dry 01-Oct-2015 15:220.000874-Chloro-3-methylphenol 0.0082U

1mg/Kg-dry 01-Oct-2015 15:220.00194-Chlorophenyl phenyl ether 0.0082U


1mg/Kg-dry 01-Oct-2015 15:220.00244-Nitrophenol 0.016U

1mg/Kg-dry 01-Oct-2015 15:220.00062Acenaphthene 0.0041U

1mg/Kg-dry 01-Oct-2015 15:220.0012Acenaphthylene 0.0041U

1mg/Kg-dry 01-Oct-2015 15:22J 0.00099Acetophenone 0.00820.0032

1mg/Kg-dry 01-Oct-2015 15:220.0017Aniline 0.0082U

1mg/Kg-dry 01-Oct-2015 15:22J 0.00062Anthracene 0.00410.0011

1mg/Kg-dry 01-Oct-2015 15:22J 0.0020Benz(a)anthracene 0.00410.0024

1mg/Kg-dry 01-Oct-2015 15:22Jn 0.0015Benzaldehyde 0.00820.0034

1mg/Kg-dry 01-Oct-2015 15:22J 0.0012Benzo(a)pyrene 0.00410.0038

1mg/Kg-dry 01-Oct-2015 15:220.0015Benzo(b)fluoranthene 0.00410.0059

1mg/Kg-dry 01-Oct-2015 15:220.00087Benzo(g,h,i)perylene 0.00410.0042

1mg/Kg-dry 01-Oct-2015 15:22J 0.0011Benzo(k)fluoranthene 0.00410.0030

1mg/Kg-dry 01-Oct-2015 15:220.0011Bis(2-chloroethoxy)methane 0.0082U

1mg/Kg-dry 01-Oct-2015 15:220.0014Bis(2-chloroethyl)ether 0.0082U



Page 29 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-02


ANALYTICAL REPORT




1mg/Kg-dry 01-Oct-2015 15:220.0017Bis(2-chloroisopropyl)ether 0.0082U

1mg/Kg-dry 01-Oct-2015 15:22J 0.0021Bis(2-ethylhexyl)phthalate 0.00820.0078

1mg/Kg-dry 01-Oct-2015 15:22J 0.0016Butyl benzyl phthalate 0.00820.0023

1mg/Kg-dry 01-Oct-2015 15:220.0015Caprolactam 0.00820.013

1mg/Kg-dry 01-Oct-2015 15:220.0015Carbazole 0.0082U

1mg/Kg-dry 01-Oct-2015 15:22J 0.00099Chrysene 0.00410.0036

1mg/Kg-dry 01-Oct-2015 15:22J 0.0020Dibenz(a,h)anthracene 0.00410.0026

1mg/Kg-dry 01-Oct-2015 15:220.00087Dibenzofuran 0.0041U

1mg/Kg-dry 01-Oct-2015 15:220.0012Diethyl phthalate 0.0082U

1mg/Kg-dry 01-Oct-2015 15:220.00099Dimethyl phthalate 0.0082U

1mg/Kg-dry 01-Oct-2015 15:22J 0.0015Di-n-butyl phthalate 0.00820.0020

1mg/Kg-dry 01-Oct-2015 15:220.0011Di-n-octyl phthalate 0.0082U

1mg/Kg-dry 01-Oct-2015 15:220.0014Fluoranthene 0.00410.0063

1mg/Kg-dry 01-Oct-2015 15:220.0014Fluorene 0.0041U

1mg/Kg-dry 01-Oct-2015 15:220.0011Hexachlorobenzene 0.0082U

1mg/Kg-dry 01-Oct-2015 15:220.0015Hexachlorobutadiene 0.0082U

1mg/Kg-dry 01-Oct-2015 15:220.00099Hexachlorocyclopentadiene 0.0082U

1mg/Kg-dry 01-Oct-2015 15:220.0019Hexachloroethane 0.0082U

1mg/Kg-dry 01-Oct-2015 15:220.00099Indeno(1,2,3-cd)pyrene 0.00410.0053

1mg/Kg-dry 01-Oct-2015 15:220.00099Isophorone 0.0082U

1mg/Kg-dry 01-Oct-2015 15:22J 0.00075Naphthalene 0.00410.0013

1mg/Kg-dry 01-Oct-2015 15:220.0011Nitrobenzene 0.0082U

1mg/Kg-dry 01-Oct-2015 15:220.0014N-Nitrosodi-n-propylamine 0.0082U

1mg/Kg-dry 01-Oct-2015 15:220.00087N-Nitrosodiphenylamine 0.0082U

1mg/Kg-dry 01-Oct-2015 15:220.0041Pentachlorophenol 0.0082U

1mg/Kg-dry 01-Oct-2015 15:22J 0.0019Phenanthrene 0.00410.0019

1mg/Kg-dry 01-Oct-2015 15:22J 0.0014Phenol 0.00820.0023

1mg/Kg-dry 01-Oct-2015 15:220.00075Pyrene 0.00410.0054

1mg/Kg-dry 01-Oct-2015 15:220.0011Pyridine 0.0082U

Surr: 2,4,6-Tribromophenol 1%REC 01-Oct-2015 15:22103 36-126

Surr: 2-Fluorobiphenyl 1%REC 01-Oct-2015 15:2275.0 43-125

Surr: 2-Fluorophenol 1%REC 01-Oct-2015 15:2265.3 37-125

Surr: 4-Terphenyl-d14 1%REC 01-Oct-2015 15:2278.1 32-125

Surr: Nitrobenzene-d5 1%REC 01-Oct-2015 15:2280.4 37-125

Surr: Phenol-d6 1%REC 01-Oct-2015 15:2288.4 40-125



Page 30 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-02


ANALYTICAL REPORT












1mg/Kg-dry 29-Sep-2015 19:180.0578Lead 0.57836.5







1mg/Kg-dry 29-Sep-2015 19:180.289Zinc 0.57881.7













Page 31 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-03


ANALYTICAL REPORT












































Page 32 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-03


ANALYTICAL REPORT



VOLATILES BY SW8260C Method:SW8260 Analyst: WLR1mg/Kg-dry 29-Sep-2015 17:39J 0.00046Methyl tert-butyl ether 0.00460.0019























Page 33 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-03


ANALYTICAL REPORT






























1mg/Kg-dry 30-Sep-2015 19:12J 0.00059Acenaphthene 0.00390.0012





1mg/Kg-dry 30-Sep-2015 19:12J 0.0019Benz(a)anthracene 0.00390.0034


1mg/Kg-dry 30-Sep-2015 19:12J 0.0012Benzo(a)pyrene 0.00390.0039


1mg/Kg-dry 30-Sep-2015 19:120.00082Benzo(g,h,i)perylene 0.00390.0049






Page 34 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-03


ANALYTICAL REPORT






1mg/Kg-dry 30-Sep-2015 19:12J 0.0015Butyl benzyl phthalate 0.00770.0015



1mg/Kg-dry 30-Sep-2015 19:120.00094Chrysene 0.00390.0049


1mg/Kg-dry 30-Sep-2015 19:12J 0.00082Dibenzofuran 0.00390.0012






1mg/Kg-dry 30-Sep-2015 19:12J 0.0013Fluorene 0.00390.0021





1mg/Kg-dry 30-Sep-2015 19:120.00094Indeno(1,2,3-cd)pyrene 0.00390.0047









1mg/Kg-dry 30-Sep-2015 19:120.00070Pyrene 0.00390.0074










Page 35 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-03


ANALYTICAL REPORT












1mg/Kg-dry 29-Sep-2015 19:220.0546Lead 0.54615.9







1mg/Kg-dry 29-Sep-2015 19:220.273Zinc 0.54629.1













Page 36 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-04


ANALYTICAL REPORT












































Page 37 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-04


ANALYTICAL REPORT


























Page 38 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-04


ANALYTICAL REPORT













































Page 39 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-04


ANALYTICAL REPORT







1mg/Kg-dry 30-Sep-2015 13:02J 0.0014Caprolactam 0.00780.0067















1mg/Kg-dry 30-Sep-2015 13:02J 0.00095Indeno(1,2,3-cd)pyrene 0.00390.0011



















Page 40 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-04


ANALYTICAL REPORT












1mg/Kg-dry 29-Sep-2015 19:270.0541Lead 0.5415.47







1mg/Kg-dry 29-Sep-2015 19:270.270Zinc 0.54114.1











PH SOIL BY SW9045D Method:SW9045B Analyst: TDW1pH Units 28-Sep-2015 12:00H 0.100pH 0.1008.82

1°C 28-Sep-2015 12:00H 0Temp Deg C @pH 021.4



Page 41 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-05


ANALYTICAL REPORT












































Page 42 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-05


ANALYTICAL REPORT


























Page 43 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-05


ANALYTICAL REPORT



































1mg/Kg-dry 30-Sep-2015 13:21J 0.0020Benz(a)anthracene 0.00420.0025




1mg/Kg-dry 30-Sep-2015 13:21J 0.00089Benzo(g,h,i)perylene 0.00420.0025






Page 44 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-05


ANALYTICAL REPORT









































Page 45 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-05


ANALYTICAL REPORT












1mg/Kg-dry 29-Sep-2015 19:310.0589Lead 0.58912.6







1mg/Kg-dry 29-Sep-2015 19:310.294Zinc 0.58925.1











PH SOIL BY SW9045D Method:SW9045B Analyst: TDW1pH Units 28-Sep-2015 12:00H 0.100pH 0.1007.96

1°C 28-Sep-2015 12:00H 0Temp Deg C @pH 021.1



Page 46 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-06


ANALYTICAL REPORT












































Page 47 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-06


ANALYTICAL REPORT


























Page 48 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-06


ANALYTICAL REPORT













































Page 49 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-06


ANALYTICAL REPORT









































Page 50 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-06


ANALYTICAL REPORT












1mg/Kg-dry 29-Sep-2015 19:360.0606Lead 0.60611.2







1mg/Kg-dry 29-Sep-2015 19:360.303Zinc 0.60618.3













Page 51 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-07


ANALYTICAL REPORT












































Page 52 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-07


ANALYTICAL REPORT


























Page 53 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-07


ANALYTICAL REPORT













































Page 54 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-07


ANALYTICAL REPORT







1mg/Kg-dry 29-Sep-2015 11:49J 0.0016Caprolactam 0.00860.0080








1mg/Kg-dry 29-Sep-2015 11:49J 0.0012Di-n-octyl phthalate 0.00860.0057


























Page 55 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-07


ANALYTICAL REPORT












1mg/Kg-dry 29-Sep-2015 19:490.0609Lead 0.6099.48







1mg/Kg-dry 29-Sep-2015 19:490.304Zinc 0.60922.8













Page 56 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-08


ANALYTICAL REPORT
























1mg/Kg-dry 30-Sep-2015 12:03J 0.0031Acetone 0.0200.015




















Page 57 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-08


ANALYTICAL REPORT


























Page 58 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-08


ANALYTICAL REPORT













































Page 59 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-08


ANALYTICAL REPORT
















1mg/Kg-dry 30-Sep-2015 14:00J 0.0014Fluoranthene 0.00410.0028

















Surr: 2,4,6-Tribromophenol 1%REC 30-Sep-2015 14:00S128 36-126








Page 60 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-08


ANALYTICAL REPORT












1mg/Kg-dry 29-Sep-2015 20:110.0567Lead 0.56714.6







1mg/Kg-dry 29-Sep-2015 20:110.283Zinc 0.56721.8













Page 61 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-09


ANALYTICAL REPORT












































Page 62 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-09


ANALYTICAL REPORT


























Page 63 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-09


ANALYTICAL REPORT













































Page 64 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-09


ANALYTICAL REPORT









































Page 65 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-09


ANALYTICAL REPORT












1mg/Kg-dry 29-Sep-2015 20:150.0539Lead 0.53911.6







1mg/Kg-dry 29-Sep-2015 20:150.269Zinc 0.53914.5













Page 66 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-10


ANALYTICAL REPORT












































Page 67 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-10


ANALYTICAL REPORT


























Page 68 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-10


ANALYTICAL REPORT













































Page 69 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-10


ANALYTICAL REPORT









































Page 70 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-10


ANALYTICAL REPORT












1mg/Kg-dry 29-Sep-2015 20:280.0556Lead 0.5567.71



1mg/Kg-dry 29-Sep-2015 20:280.200Selenium 0.556U




1mg/Kg-dry 29-Sep-2015 20:280.278Zinc 0.55619.1













Page 71 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-11


ANALYTICAL REPORT












































Page 72 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-11


ANALYTICAL REPORT


























Page 73 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-11


ANALYTICAL REPORT













































Page 74 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-11


ANALYTICAL REPORT









































Page 75 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-11


ANALYTICAL REPORT












1mg/Kg-dry 29-Sep-2015 20:330.0550Lead 0.5505.97







1mg/Kg-dry 29-Sep-2015 20:330.275Zinc 0.55013.7













Page 76 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-12


ANALYTICAL REPORT












































Page 77 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-12


ANALYTICAL REPORT


























Page 78 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-12


ANALYTICAL REPORT






1mg/Kg-dry 30-Sep-2015 15:18Jn 0.00191-Methylnaphthalene 0.00410.0019







































Page 79 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-12


ANALYTICAL REPORT









































Page 80 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-12


ANALYTICAL REPORT












1mg/Kg-dry 29-Sep-2015 20:370.0574Lead 0.57413.2







1mg/Kg-dry 29-Sep-2015 20:370.287Zinc 0.57413.8













Page 81 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-13


ANALYTICAL REPORT












































Page 82 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-13


ANALYTICAL REPORT


























Page 83 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-13


ANALYTICAL REPORT













































Page 84 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-13


ANALYTICAL REPORT









































Page 85 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-13


ANALYTICAL REPORT












1mg/Kg-dry 29-Sep-2015 20:420.0546Lead 0.54617.6

10mg/Kg-dry 30-Sep-2015 12:581.09Manganese 5.461,950






1mg/Kg-dry 29-Sep-2015 20:420.273Zinc 0.54614.3













Page 86 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-14


ANALYTICAL REPORT












































Page 87 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-14


ANALYTICAL REPORT


























Page 88 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-14


ANALYTICAL REPORT













































Page 89 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-14


ANALYTICAL REPORT









































Page 90 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-14


ANALYTICAL REPORT












1mg/Kg-dry 29-Sep-2015 20:460.0493Lead 0.4934.95







1mg/Kg-dry 29-Sep-2015 20:460.246Zinc 0.4933.23













Page 91 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-15


ANALYTICAL REPORT












































Page 92 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-15


ANALYTICAL REPORT


























Page 93 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-15


ANALYTICAL REPORT













































Page 94 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-15


ANALYTICAL REPORT





























1mg/Kg-dry 30-Sep-2015 16:17J 0.0019Phenanthrene 0.00430.0022












Page 95 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-15


ANALYTICAL REPORT












1mg/Kg-dry 29-Sep-2015 20:510.0568Lead 0.56817.2







1mg/Kg-dry 29-Sep-2015 20:510.284Zinc 0.56823.3













Page 96 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-16


ANALYTICAL REPORT












































Page 97 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-16


ANALYTICAL REPORT


























Page 98 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-16


ANALYTICAL REPORT













































Page 99 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-16


ANALYTICAL REPORT
















1mg/Kg-dry 30-Sep-2015 16:36J 0.0013Fluoranthene 0.00390.0017

























Page 100 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-16


ANALYTICAL REPORT



METALS BY SW6020A Method:SW6020 Analyst: JCJPrep:SW3050A / 29-Sep-2015









1mg/Kg-dry 29-Sep-2015 20:120.0584Lead 0.58418.7







1mg/Kg-dry 29-Sep-2015 20:120.292Zinc 0.58415.2













Page 101 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-17


ANALYTICAL REPORT



VOLATILES BY SW8260C Method:SW8260 Analyst: WLR1mg/Kg-dry 02-Oct-2015 13:340.000561,1,1,2-Tetrachloroethane 0.0046U

1mg/Kg-dry 02-Oct-2015 13:340.000461,1,1-Trichloroethane 0.0046U

1mg/Kg-dry 02-Oct-2015 13:340.000741,1,2,2-Tetrachloroethane 0.0046U

1mg/Kg-dry 02-Oct-2015 13:340.000651,1,2-Trichlor-1,2,2-trifluoroethane 0.0046U

1mg/Kg-dry 02-Oct-2015 13:340.000461,1,2-Trichloroethane 0.0046U

1mg/Kg-dry 02-Oct-2015 13:340.000461,1-Dichloroethane 0.0046U

1mg/Kg-dry 02-Oct-2015 13:340.000461,1-Dichloroethene 0.0046U

1mg/Kg-dry 02-Oct-2015 13:340.00101,2,3-Trichlorobenzene 0.0046U

1mg/Kg-dry 02-Oct-2015 13:340.00101,2,4-Trichlorobenzene 0.0046U

1mg/Kg-dry 02-Oct-2015 13:340.00101,2,4-Trimethylbenzene 0.0046U

1mg/Kg-dry 02-Oct-2015 13:340.000461,2-Dibromoethane 0.0046U

1mg/Kg-dry 02-Oct-2015 13:340.000931,2-Dichlorobenzene 0.0046U

1mg/Kg-dry 02-Oct-2015 13:340.000561,2-Dichloroethane 0.0046U

1mg/Kg-dry 02-Oct-2015 13:340.000741,2-Dichloropropane 0.0046U

1mg/Kg-dry 02-Oct-2015 13:340.000741,3,5-Trimethylbenzene 0.0046U



1mg/Kg-dry 02-Oct-2015 13:340.00122-Butanone 0.0093U

1mg/Kg-dry 02-Oct-2015 13:340.00132-Hexanone 0.0093U

1mg/Kg-dry 02-Oct-2015 13:340.00104-Isopropyltoluene 0.0046U

1mg/Kg-dry 02-Oct-2015 13:340.00194-Methyl-2-pentanone 0.0093U

1mg/Kg-dry 02-Oct-2015 13:340.0029Acetone 0.019U

1mg/Kg-dry 02-Oct-2015 13:340.00046Benzene 0.0046U

1mg/Kg-dry 02-Oct-2015 13:340.00046Bromodichloromethane 0.0046U

1mg/Kg-dry 02-Oct-2015 13:340.00056Bromoform 0.0046U

1mg/Kg-dry 02-Oct-2015 13:340.00093Bromomethane 0.0093U

1mg/Kg-dry 02-Oct-2015 13:340.00056Carbon disulfide 0.0093U

1mg/Kg-dry 02-Oct-2015 13:340.00056Carbon tetrachloride 0.0046U

1mg/Kg-dry 02-Oct-2015 13:340.00056Chlorobenzene 0.0046U

1mg/Kg-dry 02-Oct-2015 13:340.00074Chloroethane 0.0093U

1mg/Kg-dry 02-Oct-2015 13:340.00046Chloroform 0.0046U

1mg/Kg-dry 02-Oct-2015 13:340.00046Chloromethane 0.0093U

1mg/Kg-dry 02-Oct-2015 13:340.00074cis-1,2-Dichloroethene 0.0046U

1mg/Kg-dry 02-Oct-2015 13:340.00046cis-1,3-Dichloropropene 0.0046U

1mg/Kg-dry 02-Oct-2015 13:34n 0.00093Cyclohexane 0.0046U

1mg/Kg-dry 02-Oct-2015 13:340.00046Dibromochloromethane 0.0046U

1mg/Kg-dry 02-Oct-2015 13:340.00065Dichlorodifluoromethane 0.0046U

1mg/Kg-dry 02-Oct-2015 13:340.00065Ethylbenzene 0.0046U

1mg/Kg-dry 02-Oct-2015 13:340.00084Isopropylbenzene 0.0046U



Page 102 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-17


ANALYTICAL REPORT



VOLATILES BY SW8260C Method:SW8260 Analyst: WLR1mg/Kg-dry 02-Oct-2015 13:340.00046Methyl tert-butyl ether 0.0046U

1mg/Kg-dry 02-Oct-2015 13:340.0011Methylcyclohexane 0.0046U

1mg/Kg-dry 02-Oct-2015 13:340.00093Methylene chloride 0.0093U

1mg/Kg-dry 02-Oct-2015 13:34J 0.00074Naphthalene 0.00460.0022

1mg/Kg-dry 02-Oct-2015 13:340.00056n-Butylbenzene 0.0046U

1mg/Kg-dry 02-Oct-2015 13:340.00084n-Propylbenzene 0.0046U

1mg/Kg-dry 02-Oct-2015 13:340.00093sec-Butylbenzene 0.0046U

1mg/Kg-dry 02-Oct-2015 13:340.00065Styrene 0.0046U

1mg/Kg-dry 02-Oct-2015 13:340.00093tert-Butylbenzene 0.0046U

1mg/Kg-dry 02-Oct-2015 13:340.00065Tetrachloroethene 0.0046U

1mg/Kg-dry 02-Oct-2015 13:340.00056Toluene 0.0046U

1mg/Kg-dry 02-Oct-2015 13:340.00046trans-1,2-Dichloroethene 0.0046U

1mg/Kg-dry 02-Oct-2015 13:340.00056trans-1,3-Dichloropropene 0.0046U

1mg/Kg-dry 02-Oct-2015 13:340.00056Trichloroethene 0.0046U

1mg/Kg-dry 02-Oct-2015 13:340.00046Trichlorofluoromethane 0.0046U

1mg/Kg-dry 02-Oct-2015 13:340.00074Vinyl chloride 0.0019U

1mg/Kg-dry 02-Oct-2015 13:340.0022Xylenes, Total 0.0093U

Surr: 1,2-Dichloroethane-d4 1%REC 02-Oct-2015 13:3491.5 70-128

Surr: 4-Bromofluorobenzene 1%REC 02-Oct-2015 13:3498.6 73-126

Surr: Dibromofluoromethane 1%REC 02-Oct-2015 13:3499.6 71-128

Surr: Toluene-d8 1%REC 02-Oct-2015 13:34101 73-127



Page 103 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-17


ANALYTICAL REPORT













































Page 104 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-17


ANALYTICAL REPORT









































Page 105 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-17


ANALYTICAL REPORT












1mg/Kg-dry 29-Sep-2015 20:160.0605Lead 0.6056.29







1mg/Kg-dry 29-Sep-2015 20:160.303Zinc 0.60522.1

MERCURY BY SW7471B Method:SW7471A Analyst: OFOPrep:SW7471A / 01-Oct-2015

1mg/Kg-dry 01-Oct-2015 15:310.000582Mercury 0.00411U











Page 106 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-18


ANALYTICAL REPORT












































Page 107 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-18


ANALYTICAL REPORT



VOLATILES BY SW8260C Method:SW8260 Analyst: WLR1mg/Kg-dry 30-Sep-2015 15:37J 0.00050Methyl tert-butyl ether 0.00500.0029























Page 108 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-18


ANALYTICAL REPORT













































Page 109 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-18


ANALYTICAL REPORT









































Page 110 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-18


ANALYTICAL REPORT












1mg/Kg-dry 29-Sep-2015 20:380.0626Lead 0.62615.8







1mg/Kg-dry 29-Sep-2015 20:380.313Zinc 0.62616.8













Page 111 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-19


ANALYTICAL REPORT












































Page 112 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-19


ANALYTICAL REPORT


























Page 113 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-19


ANALYTICAL REPORT













































Page 114 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-19


ANALYTICAL REPORT









































Page 115 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-19


ANALYTICAL REPORT












1mg/Kg-dry 29-Sep-2015 20:420.0550Lead 0.55011.3







1mg/Kg-dry 29-Sep-2015 20:420.275Zinc 0.55017.1













Page 116 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-20


ANALYTICAL REPORT












































Page 117 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-20


ANALYTICAL REPORT


























Page 118 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-20


ANALYTICAL REPORT













































Page 119 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-20


ANALYTICAL REPORT









































Page 120 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-20


ANALYTICAL REPORT












1mg/Kg-dry 29-Sep-2015 20:550.0632Lead 0.63223.5







1mg/Kg-dry 29-Sep-2015 20:550.316Zinc 0.63242.1













Page 121 of 261


PBW HoustonCES Griggs Rd VCPEB 092315

WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-21


ANALYTICAL REPORT
























1mg/L 25-Sep-2015 10:350.0020Acetone 0.00200.036

1mg/L 25-Sep-2015 10:350.00020Benzene 0.0010U









1mg/L 25-Sep-2015 10:350.00020Chloromethane 0.00100.0030










Page 122 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-21


ANALYTICAL REPORT










1mg/L 25-Sep-2015 10:350.00030Styrene 0.0010U



1mg/L 25-Sep-2015 10:350.00020Toluene 0.0010U













Page 123 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-21


ANALYTICAL REPORT




1mg/L 28-Sep-2015 16:350.0000241,1´-Biphenyl 0.00020U

1mg/L 28-Sep-2015 16:350.0000391,2,4,5-Tetrachlorobenzene 0.00020U

1mg/L 28-Sep-2015 16:35n 0.0000101-Methylnaphthalene 0.00010U

1mg/L 28-Sep-2015 16:350.0000552,3,4,6-Tetrachlorophenol 0.00020U

1mg/L 28-Sep-2015 16:350.0000572,4,5-Trichlorophenol 0.00020U

1mg/L 28-Sep-2015 16:350.0000482,4,6-Trichlorophenol 0.00020U

1mg/L 28-Sep-2015 16:350.0000432,4-Dichlorophenol 0.00020U

1mg/L 28-Sep-2015 16:350.0000402,4-Dimethylphenol 0.00020U

1mg/L 28-Sep-2015 16:350.000102,4-Dinitrophenol 0.0010U

1mg/L 28-Sep-2015 16:350.0000582,4-Dinitrotoluene 0.00020U

1mg/L 28-Sep-2015 16:350.0000422,6-Dinitrotoluene 0.00020U

1mg/L 28-Sep-2015 16:350.0000212-Chloronaphthalene 0.00020U

1mg/L 28-Sep-2015 16:350.0000362-Chlorophenol 0.00020U

1mg/L 28-Sep-2015 16:350.0000192-Methylnaphthalene 0.00010U

1mg/L 28-Sep-2015 16:350.0000452-Methylphenol 0.00020U

1mg/L 28-Sep-2015 16:350.0000412-Nitroaniline 0.00020U

1mg/L 28-Sep-2015 16:350.0000342-Nitrophenol 0.00020U

1mg/L 28-Sep-2015 16:350.0000363&4-Methylphenol 0.00020U

1mg/L 28-Sep-2015 16:350.0000443,3´-Dichlorobenzidine 0.00020U


1mg/L 28-Sep-2015 16:350.0000204,6-Dinitro-2-methylphenol 0.00020U

1mg/L 28-Sep-2015 16:350.0000514-Bromophenyl phenyl ether 0.00020U

1mg/L 28-Sep-2015 16:350.0000324-Chloro-3-methylphenol 0.00020U

1mg/L 28-Sep-2015 16:350.0000444-Chlorophenyl phenyl ether 0.00020U


1mg/L 28-Sep-2015 16:350.0000474-Nitrophenol 0.0010U

1mg/L 28-Sep-2015 16:350.000027Acenaphthene 0.00010U

1mg/L 28-Sep-2015 16:350.000015Acenaphthylene 0.00010U

1mg/L 28-Sep-2015 16:350.000024Acetophenone 0.00020U

1mg/L 28-Sep-2015 16:350.000020Aniline 0.00020U

1mg/L 28-Sep-2015 16:350.000014Anthracene 0.00010U

1mg/L 28-Sep-2015 16:350.000050Benz(a)anthracene 0.00010U

1mg/L 28-Sep-2015 16:35Jn 0.000030Benzaldehyde 0.000200.00013

1mg/L 28-Sep-2015 16:350.000020Benzo(a)pyrene 0.00010U

1mg/L 28-Sep-2015 16:350.000023Benzo(b)fluoranthene 0.00010U

1mg/L 28-Sep-2015 16:350.000014Benzo(g,h,i)perylene 0.00010U

1mg/L 28-Sep-2015 16:350.000019Benzo(k)fluoranthene 0.00010U

1mg/L 28-Sep-2015 16:350.000030Bis(2-chloroethoxy)methane 0.00020U

1mg/L 28-Sep-2015 16:350.000026Bis(2-chloroethyl)ether 0.00020U



Page 124 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-21


ANALYTICAL REPORT




1mg/L 28-Sep-2015 16:350.000070Bis(2-chloroisopropyl)ether 0.00020U

1mg/L 28-Sep-2015 16:35J 0.000037Bis(2-ethylhexyl)phthalate 0.000200.00011

1mg/L 28-Sep-2015 16:350.000019Butyl benzyl phthalate 0.00020U

1mg/L 28-Sep-2015 16:350.000045Caprolactam 0.00020U

1mg/L 28-Sep-2015 16:350.000025Carbazole 0.00020U

1mg/L 28-Sep-2015 16:350.000021Chrysene 0.00010U

1mg/L 28-Sep-2015 16:350.000024Dibenz(a,h)anthracene 0.00010U

1mg/L 28-Sep-2015 16:350.000020Dibenzofuran 0.00010U

1mg/L 28-Sep-2015 16:350.000030Diethyl phthalate 0.00020U

1mg/L 28-Sep-2015 16:350.000041Dimethyl phthalate 0.00020U

1mg/L 28-Sep-2015 16:35J 0.000020Di-n-butyl phthalate 0.000200.000041

1mg/L 28-Sep-2015 16:35J 0.000020Di-n-octyl phthalate 0.000200.000025

1mg/L 28-Sep-2015 16:350.000010Fluoranthene 0.00010U

1mg/L 28-Sep-2015 16:350.000030Fluorene 0.00010U

1mg/L 28-Sep-2015 16:350.000044Hexachlorobenzene 0.00020U

1mg/L 28-Sep-2015 16:350.000030Hexachlorobutadiene 0.00020U

1mg/L 28-Sep-2015 16:350.000030Hexachlorocyclopentadiene 0.00020U

1mg/L 28-Sep-2015 16:350.000059Hexachloroethane 0.00020U

1mg/L 28-Sep-2015 16:350.000022Indeno(1,2,3-cd)pyrene 0.00010U

1mg/L 28-Sep-2015 16:350.000025Isophorone 0.00020U


1mg/L 28-Sep-2015 16:350.000024Nitrobenzene 0.00020U

1mg/L 28-Sep-2015 16:350.000032N-Nitrosodi-n-propylamine 0.00020U

1mg/L 28-Sep-2015 16:350.000025N-Nitrosodiphenylamine 0.00020U

1mg/L 28-Sep-2015 16:350.000079Pentachlorophenol 0.00020U

1mg/L 28-Sep-2015 16:350.000021Phenanthrene 0.00010U

1mg/L 28-Sep-2015 16:350.000035Phenol 0.00020U

1mg/L 28-Sep-2015 16:350.000019Pyrene 0.00010U

1mg/L 28-Sep-2015 16:350.000030Pyridine 0.0010U









Page 125 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-21


ANALYTICAL REPORT



ICP-MS METALS BY SW6020A Method:SW6020 Analyst: RPMPrep:SW3010A / 25-Sep-2015

1mg/L 28-Sep-2015 15:460.000400Antimony 0.00500U

1mg/L 28-Sep-2015 15:460.000400Arsenic 0.00500U

1mg/L 28-Sep-2015 15:460.00190Barium 0.00500U

1mg/L 28-Sep-2015 15:460.000200Beryllium 0.00200U

1mg/L 28-Sep-2015 15:460.000200Cadmium 0.00200U

1mg/L 28-Sep-2015 15:460.000400Chromium 0.00500U

1mg/L 28-Sep-2015 15:460.000200Cobalt 0.00500U

1mg/L 28-Sep-2015 15:460.00100Copper 0.00500U

1mg/L 28-Sep-2015 15:460.000600Lead 0.00500U

1mg/L 28-Sep-2015 15:46J 0.000700Manganese 0.005000.000739

1mg/L 28-Sep-2015 15:460.000600Nickel 0.00500U

1mg/L 28-Sep-2015 15:460.00110Selenium 0.00500U

1mg/L 28-Sep-2015 15:460.000200Silver 0.00500U

1mg/L 28-Sep-2015 15:460.000200Thallium 0.00200U

1mg/L 28-Sep-2015 15:460.000600Vanadium 0.00500U

1mg/L 28-Sep-2015 15:460.00200Zinc 0.00500U

MERCURY BY SW7470A Method:SW7470 Analyst: OFOPrep:SW7470 / 25-Sep-2015

1mg/L 25-Sep-2015 15:040.0000400Mercury 0.000200U

LOW-LEVEL TEXAS TPH BY TX1005 Method:TX1005 Analyst: JKPPrep:TX1005PR / 25-Sep-2015

1mg/L 26-Sep-2015 06:090.19nC6 to nC12 0.48U

1mg/L 26-Sep-2015 06:090.19>nC12 to nC28 0.48U

1mg/L 26-Sep-2015 06:090.19>nC28 to nC35 0.48U

1mg/L 26-Sep-2015 06:090.19Total Petroleum Hydrocarbon 0.48U





Page 126 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-22


ANALYTICAL REPORT
























1mg/L 25-Sep-2015 11:010.0020Acetone 0.0020U

1mg/L 25-Sep-2015 11:010.00020Benzene 0.0010U



















Page 127 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-22


ANALYTICAL REPORT










1mg/L 25-Sep-2015 11:010.00030Styrene 0.0010U



1mg/L 25-Sep-2015 11:010.00020Toluene 0.0010U













Page 128 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-23


ANALYTICAL REPORT
























1mg/L 25-Sep-2015 11:510.0020Acetone 0.0020U

1mg/L 25-Sep-2015 11:510.00020Benzene 0.0010U



















Page 129 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-23


ANALYTICAL REPORT










1mg/L 25-Sep-2015 11:510.00030Styrene 0.0010U



1mg/L 25-Sep-2015 11:510.00020Toluene 0.0010U













Page 130 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-24


ANALYTICAL REPORT
























1mg/L 25-Sep-2015 12:170.0020Acetone 0.0020U

1mg/L 25-Sep-2015 12:170.00020Benzene 0.0010U



















Page 131 of 261



WorkOrder:Lab ID:

Collection Date:

HS15091078HS15091078-24


ANALYTICAL REPORT










1mg/L 25-Sep-2015 12:170.00030Styrene 0.0010U



1mg/L 25-Sep-2015 12:170.00020Toluene 0.0010U













Page 132 of 261

WEIGHT LOG





Sample Wt/Vol

Final Volume

Weight Factor

HS15091078-01 2 5.632 (g) TerraCore (5035A)5 (mL) 0.89HS15091078-02 2 6.311 (g) TerraCore (5035A)5 (mL) 0.79HS15091078-03 2 6.385 (g) TerraCore (5035A)5 (mL) 0.78HS15091078-04 2 5.77 (g) TerraCore (5035A)5 (mL) 0.87HS15091078-05 2 6.137 (g) TerraCore (5035A)5 (mL) 0.81HS15091078-06 2 6.118 (g) TerraCore (5035A)5 (mL) 0.82HS15091078-07 4 6.069 (g) TerraCore (5035A)5 (mL) 0.82HS15091078-08 2 6.259 (g) TerraCore (5035A)5 (mL) 0.8HS15091078-09 2 6.591 (g) TerraCore (5035A)5 (mL) 0.76HS15091078-10 2 6.592 (g) TerraCore (5035A)5 (mL) 0.76HS15091078-11 2 6.604 (g) TerraCore (5035A)5 (mL) 0.76HS15091078-12 2 5.651 (g) TerraCore (5035A)5 (mL) 0.88HS15091078-13 2 7.195 (g) TerraCore (5035A)5 (mL) 0.69HS15091078-14 2 6.614 (g) TerraCore (5035A)5 (mL) 0.76HS15091078-15 2 11.276 (g) TerraCore (5035A)5 (mL) 0.44HS15091078-16 2 6.464 (g) TerraCore (5035A)5 (mL) 0.77HS15091078-17 4 6.498 (g) TerraCore (5035A)5 (mL) 0.77HS15091078-18 2 6.26 (g) TerraCore (5035A)5 (mL) 0.8HS15091078-19 2 6.812 (g) TerraCore (5035A)5 (mL) 0.73HS15091078-20 2 6.207 (g) TerraCore (5035A)5 (mL) 0.81

Batch ID: 97447 Method: ICP-MS METALS BY SW6020A 3010APrep:


Final Volume

Prep Factor

HS15091078-21 1 50 50 (mL) 1

Batch ID: 97456 Method: MERCURY BY SW7470A HG_WPRPrep:


Final Volume

Prep Factor

HS15091078-21 1 40 40 (mL) 1

Batch ID: 97466 Method: LOW-LEVEL TEXAS TPH BY TX1005 TX 1005_W PRPrep:


Final Volume

Prep Factor

HS15091078-21 1 31.38 3 (mL) 0.0956


Page 133 of 261

WEIGHT LOG





Final Volume

Prep Factor

HS15091078-01 1 13.02 10 (mL) 0.768HS15091078-02 1 13.16 10 (mL) 0.7599HS15091078-03 1 13.57 10 (mL) 0.7369HS15091078-04 1 12.71 10 (mL) 0.7868HS15091078-05 1 12.54 10 (mL) 0.7974HS15091078-06 1 12.75 10 (mL) 0.7843HS15091078-07 1 13.24 10 (mL) 0.7553HS15091078-08 1 12.28 10 (mL) 0.8143HS15091078-09 1 13.42 10 (mL) 0.7452HS15091078-10 1 12.28 10 (mL) 0.8143HS15091078-11 1 13.3 10 (mL) 0.7519HS15091078-12 1 12.32 10 (mL) 0.8117HS15091078-13 1 14.06 10 (mL) 0.7112HS15091078-14 1 13.89 10 (mL) 0.7199HS15091078-15 1 5.01 10 (mL) 1.996HS15091078-16 1 13.84 10 (mL) 0.7225HS15091078-17 1 13.23 10 (mL) 0.7559HS15091078-18 1 12.88 10 (mL) 0.7764HS15091078-19 1 13.22 10 (mL) 0.7564HS15091078-20 1 12.73 10 (mL) 0.7855



Final Volume

Prep Factor

HS15091078-21 1 1000 1 (mL) 0.001



Final Volume

Prep Factor

HS15091078-01 1 0.5924 40 (mL) 67.52HS15091078-02 1 0.5824 40 (mL) 68.68HS15091078-03 1 0.5621 40 (mL) 71.16HS15091078-04 1 0.5879 40 (mL) 68.04HS15091078-05 1 0.5906 40 (mL) 67.73HS15091078-06 1 0.5863 40 (mL) 68.22HS15091078-07 1 0.5825 40 (mL) 68.67HS15091078-08 1 0.5847 40 (mL) 68.41HS15091078-09 1 0.5774 40 (mL) 69.28HS15091078-10 1 0.5828 40 (mL) 68.63HS15091078-11 1 0.5627 40 (mL) 71.09HS15091078-12 1 0.5599 40 (mL) 71.44HS15091078-13 1 0.5748 40 (mL) 69.59HS15091078-14 1 0.5821 40 (mL) 68.72HS15091078-15 1 0.5649 40 (mL) 70.81HS15091078-16 1 0.5824 40 (mL) 68.68HS15091078-18 1 0.5778 40 (mL) 69.23HS15091078-19 1 0.5744 40 (mL) 69.64HS15091078-20 1 0.5781 40 (mL) 69.19


Page 134 of 261

WEIGHT LOG





Final Volume

Prep Factor

HS15091078-01 1 30.02 1 (mL) 0.03331HS15091078-02 1 30.06 1 (mL) 0.03327HS15091078-03 1 30.01 1 (mL) 0.03332HS15091078-07 1 30.03 1 (mL) 0.0333



Final Volume

Prep Factor




Final Volume

Prep Factor

HS15091078-16 1 0.5113 50 (mL) 97.79HS15091078-17 1 0.4984 50 (mL) 100.3HS15091078-18 1 0.5033 50 (mL) 99.34HS15091078-19 1 0.5378 50 (mL) 92.97HS15091078-20 1 0.492 50 (mL) 101.6


Page 135 of 261

WEIGHT LOG





Final Volume

Prep Factor

HS15091078-04 1 30.02 1 (mL) 0.03331HS15091078-05 1 30.05 1 (mL) 0.03328HS15091078-06 1 30.03 1 (mL) 0.0333HS15091078-08 1 30.09 1 (mL) 0.03323HS15091078-09 1 30.04 1 (mL) 0.03329HS15091078-10 1 30.01 1 (mL) 0.03332HS15091078-11 1 30.06 1 (mL) 0.03327HS15091078-12 1 30.09 1 (mL) 0.03323HS15091078-13 1 30.07 1 (mL) 0.03326HS15091078-14 1 30.02 1 (mL) 0.03331HS15091078-15 1 30.05 1 (mL) 0.03328HS15091078-16 1 30.08 1 (mL) 0.03324HS15091078-17 1 30.03 1 (mL) 0.0333HS15091078-18 1 30.01 1 (mL) 0.03332HS15091078-19 1 30.09 1 (mL) 0.03323HS15091078-20 1 30.02 1 (mL) 0.03331



Final Volume

Prep Factor

HS15091078-17 1 0.5849 40 (mL) 68.39


Page 136 of 261


WorkOrder:Project:



Batch ID 97447 Test Name : ICP-MS METALS BY SW6020A Matrix: Water

25 Sep 2015 08:16 28 Sep 2015 15:46HS15091078-21 23 Sep 2015 18:15 1EB 092315

Batch ID 97456 Test Name : MERCURY BY SW7470A Matrix: Water

25 Sep 2015 10:32 25 Sep 2015 15:04HS15091078-21 23 Sep 2015 18:15 1EB 092315

Batch ID 97466 Test Name : LOW-LEVEL TEXAS TPH BY TX1005 Matrix: Water

25 Sep 2015 13:35 26 Sep 2015 06:09HS15091078-21 23 Sep 2015 18:15 1EB 092315


25 Sep 2015 13:50 27 Sep 2015 23:58HS15091078-01 23 Sep 2015 09:10 14904-SB03-01

25 Sep 2015 13:50 28 Sep 2015 00:27HS15091078-02 23 Sep 2015 09:10 14904-SB03-01 Dup

25 Sep 2015 13:50 28 Sep 2015 00:56HS15091078-03 23 Sep 2015 09:10 14904-SB03-02

25 Sep 2015 13:50 28 Sep 2015 01:25HS15091078-04 23 Sep 2015 09:20 14904-SB03-12

25 Sep 2015 13:50 28 Sep 2015 01:55HS15091078-05 23 Sep 2015 17:50 14904-SB10-01

25 Sep 2015 13:50 28 Sep 2015 02:23HS15091078-06 23 Sep 2015 17:55 14904-SB10-05

25 Sep 2015 13:50 28 Sep 2015 02:53HS15091078-07 23 Sep 2015 18:00 14904-SB10-08

25 Sep 2015 13:50 28 Sep 2015 04:20HS15091078-08 23 Sep 2015 16:40 14904-SB11-00

25 Sep 2015 13:50 28 Sep 2015 04:49HS15091078-09 23 Sep 2015 16:40 14904-SB11-04

25 Sep 2015 13:50 28 Sep 2015 05:18HS15091078-10 23 Sep 2015 16:45 14904-SB11-09


25 Sep 2015 13:50 28 Sep 2015 07:44HS15091078-12 23 Sep 2015 15:20 14904-SB13-02

25 Sep 2015 13:50 28 Sep 2015 08:13HS15091078-13 23 Sep 2015 15:25 14904-SB13-10

25 Sep 2015 13:50 28 Sep 2015 08:42HS15091078-14 23 Sep 2015 15:25 14904-SB13-25

25 Sep 2015 13:50 28 Sep 2015 09:12HS15091078-15 23 Sep 2015 13:25 14904-SB16-04

25 Sep 2015 13:50 28 Sep 2015 09:41HS15091078-16 23 Sep 2015 13:30 14904-SB16-09

25 Sep 2015 13:50 28 Sep 2015 10:10HS15091078-17 23 Sep 2015 13:35 14904-SB16-21.5

25 Sep 2015 13:50 28 Sep 2015 11:38HS15091078-18 23 Sep 2015 11:15 14904-SB17-00

25 Sep 2015 13:50 28 Sep 2015 12:07HS15091078-19 23 Sep 2015 11:10 14904-SB17-09

25 Sep 2015 13:50 28 Sep 2015 12:36HS15091078-20 23 Sep 2015 11:15 14904-SB17-22

Batch ID 97500 Test Name : LOW-LEVEL SEMIVOLATILES Matrix: Water

28 Sep 2015 08:33 28 Sep 2015 16:35HS15091078-21 23 Sep 2015 18:15 1EB 092315


Page 137 of 261


WorkOrder:Project:




28 Sep 2015 10:27 28 Sep 2015 15:32HS15091078-01 23 Sep 2015 09:10 14904-SB03-01


28 Sep 2015 10:27 28 Sep 2015 15:36HS15091078-03 23 Sep 2015 09:10 14904-SB03-02

28 Sep 2015 10:27 28 Sep 2015 15:38HS15091078-04 23 Sep 2015 09:20 14904-SB03-12

28 Sep 2015 10:27 28 Sep 2015 15:44HS15091078-05 23 Sep 2015 17:50 14904-SB10-01

28 Sep 2015 10:27 28 Sep 2015 15:46HS15091078-06 23 Sep 2015 17:55 14904-SB10-05

28 Sep 2015 10:27 28 Sep 2015 15:24HS15091078-07 23 Sep 2015 18:00 14904-SB10-08

28 Sep 2015 10:27 28 Sep 2015 15:48HS15091078-08 23 Sep 2015 16:40 14904-SB11-00

28 Sep 2015 10:27 28 Sep 2015 15:50HS15091078-09 23 Sep 2015 16:40 14904-SB11-04

28 Sep 2015 10:27 28 Sep 2015 15:52HS15091078-10 23 Sep 2015 16:45 14904-SB11-09


28 Sep 2015 10:27 28 Sep 2015 15:56HS15091078-12 23 Sep 2015 15:20 14904-SB13-02

28 Sep 2015 10:27 28 Sep 2015 15:58HS15091078-13 23 Sep 2015 15:25 14904-SB13-10

28 Sep 2015 10:27 28 Sep 2015 16:00HS15091078-14 23 Sep 2015 15:25 14904-SB13-25

28 Sep 2015 10:27 28 Sep 2015 16:02HS15091078-15 23 Sep 2015 13:25 14904-SB16-04

28 Sep 2015 10:27 28 Sep 2015 16:08HS15091078-16 23 Sep 2015 13:30 14904-SB16-09

28 Sep 2015 10:27 28 Sep 2015 16:10HS15091078-18 23 Sep 2015 11:15 14904-SB17-00

28 Sep 2015 10:27 28 Sep 2015 16:12HS15091078-19 23 Sep 2015 11:10 14904-SB17-09

28 Sep 2015 10:27 28 Sep 2015 16:14HS15091078-20 23 Sep 2015 11:15 14904-SB17-22


28 Sep 2015 13:18 30 Sep 2015 18:33HS15091078-01 23 Sep 2015 09:10 14904-SB03-01

28 Sep 2015 13:18 01 Oct 2015 15:22HS15091078-02 23 Sep 2015 09:10 14904-SB03-01 Dup

28 Sep 2015 13:18 30 Sep 2015 19:12HS15091078-03 23 Sep 2015 09:10 14904-SB03-02

28 Sep 2015 13:18 29 Sep 2015 11:49HS15091078-07 23 Sep 2015 18:00 14904-SB10-08


Page 138 of 261


WorkOrder:Project:




28 Sep 2015 13:39 30 Sep 2015 12:18HS15091078-01 23 Sep 2015 09:10 24904-SB03-01

28 Sep 2015 13:39 29 Sep 2015 19:14HS15091078-01 23 Sep 2015 09:10 14904-SB03-01



28 Sep 2015 13:39 29 Sep 2015 19:22HS15091078-03 23 Sep 2015 09:10 14904-SB03-02

28 Sep 2015 13:39 29 Sep 2015 19:27HS15091078-04 23 Sep 2015 09:20 14904-SB03-12

28 Sep 2015 13:39 30 Sep 2015 12:27HS15091078-05 23 Sep 2015 17:50 24904-SB10-01

28 Sep 2015 13:39 29 Sep 2015 19:31HS15091078-05 23 Sep 2015 17:50 14904-SB10-01

28 Sep 2015 13:39 29 Sep 2015 19:36HS15091078-06 23 Sep 2015 17:55 14904-SB10-05

28 Sep 2015 13:39 30 Sep 2015 12:40HS15091078-07 23 Sep 2015 18:00 54904-SB10-08

28 Sep 2015 13:39 29 Sep 2015 19:49HS15091078-07 23 Sep 2015 18:00 14904-SB10-08

28 Sep 2015 13:39 29 Sep 2015 20:11HS15091078-08 23 Sep 2015 16:40 14904-SB11-00

28 Sep 2015 13:39 29 Sep 2015 20:15HS15091078-09 23 Sep 2015 16:40 14904-SB11-04

28 Sep 2015 13:39 30 Sep 2015 12:53HS15091078-10 23 Sep 2015 16:45 24904-SB11-09

28 Sep 2015 13:39 29 Sep 2015 20:28HS15091078-10 23 Sep 2015 16:45 14904-SB11-09


28 Sep 2015 13:39 29 Sep 2015 20:37HS15091078-12 23 Sep 2015 15:20 14904-SB13-02

28 Sep 2015 13:39 30 Sep 2015 12:58HS15091078-13 23 Sep 2015 15:25 104904-SB13-10

28 Sep 2015 13:39 29 Sep 2015 20:42HS15091078-13 23 Sep 2015 15:25 14904-SB13-10

28 Sep 2015 13:39 29 Sep 2015 20:46HS15091078-14 23 Sep 2015 15:25 14904-SB13-25

28 Sep 2015 13:39 29 Sep 2015 20:51HS15091078-15 23 Sep 2015 13:25 14904-SB16-04


29 Sep 2015 09:34 30 Sep 2015 15:20HS15091078-16 23 Sep 2015 13:30 14904-SB16-09

29 Sep 2015 09:34 30 Sep 2015 14:46HS15091078-16 23 Sep 2015 13:30 104904-SB16-09

29 Sep 2015 09:34 29 Sep 2015 20:12HS15091078-16 23 Sep 2015 13:30 14904-SB16-09

29 Sep 2015 09:34 30 Sep 2015 15:24HS15091078-17 23 Sep 2015 13:35 14904-SB16-21.5

29 Sep 2015 09:34 30 Sep 2015 14:50HS15091078-17 23 Sep 2015 13:35 54904-SB16-21.5

29 Sep 2015 09:34 29 Sep 2015 20:16HS15091078-17 23 Sep 2015 13:35 14904-SB16-21.5

29 Sep 2015 09:34 30 Sep 2015 15:47HS15091078-18 23 Sep 2015 11:15 14904-SB17-00

29 Sep 2015 09:34 29 Sep 2015 20:38HS15091078-18 23 Sep 2015 11:15 14904-SB17-00

29 Sep 2015 09:34 30 Sep 2015 15:51HS15091078-19 23 Sep 2015 11:10 14904-SB17-09

29 Sep 2015 09:34 30 Sep 2015 15:03HS15091078-19 23 Sep 2015 11:10 104904-SB17-09

29 Sep 2015 09:34 29 Sep 2015 20:42HS15091078-19 23 Sep 2015 11:10 14904-SB17-09

29 Sep 2015 09:34 30 Sep 2015 16:04HS15091078-20 23 Sep 2015 11:15 14904-SB17-22

29 Sep 2015 09:34 30 Sep 2015 15:07HS15091078-20 23 Sep 2015 11:15 104904-SB17-22

29 Sep 2015 09:34 29 Sep 2015 20:55HS15091078-20 23 Sep 2015 11:15 14904-SB17-22


Page 139 of 261


WorkOrder:Project:




29 Sep 2015 09:49 30 Sep 2015 13:02HS15091078-04 23 Sep 2015 09:20 14904-SB03-12

29 Sep 2015 09:49 30 Sep 2015 13:21HS15091078-05 23 Sep 2015 17:50 14904-SB10-01

29 Sep 2015 09:49 30 Sep 2015 13:41HS15091078-06 23 Sep 2015 17:55 14904-SB10-05

29 Sep 2015 09:49 30 Sep 2015 14:00HS15091078-08 23 Sep 2015 16:40 14904-SB11-00

29 Sep 2015 09:49 30 Sep 2015 14:20HS15091078-09 23 Sep 2015 16:40 14904-SB11-04

29 Sep 2015 09:49 30 Sep 2015 14:39HS15091078-10 23 Sep 2015 16:45 14904-SB11-09


29 Sep 2015 09:49 30 Sep 2015 15:18HS15091078-12 23 Sep 2015 15:20 14904-SB13-02

29 Sep 2015 09:49 30 Sep 2015 19:32HS15091078-13 23 Sep 2015 15:25 14904-SB13-10

29 Sep 2015 09:49 30 Sep 2015 15:57HS15091078-14 23 Sep 2015 15:25 14904-SB13-25

29 Sep 2015 09:49 30 Sep 2015 16:17HS15091078-15 23 Sep 2015 13:25 14904-SB16-04

29 Sep 2015 09:49 30 Sep 2015 16:36HS15091078-16 23 Sep 2015 13:30 14904-SB16-09

29 Sep 2015 09:49 30 Sep 2015 11:58HS15091078-17 23 Sep 2015 13:35 14904-SB16-21.5

29 Sep 2015 09:49 30 Sep 2015 16:56HS15091078-18 23 Sep 2015 11:15 14904-SB17-00

29 Sep 2015 09:49 30 Sep 2015 17:15HS15091078-19 23 Sep 2015 11:10 14904-SB17-09

29 Sep 2015 09:49 30 Sep 2015 17:35HS15091078-20 23 Sep 2015 11:15 14904-SB17-22


01 Oct 2015 10:17 01 Oct 2015 15:31HS15091078-17 23 Sep 2015 13:35 14904-SB16-21.5


25 Sep 2015 10:35HS15091078-21 23 Sep 2015 18:15 1EB 092315

25 Sep 2015 11:01HS15091078-22 23 Sep 2015 18:20 1TB01 092315

25 Sep 2015 11:51HS15091078-23 23 Sep 2015 18:25 1TB02 092315

25 Sep 2015 12:17HS15091078-24 23 Sep 2015 18:30 1TB03 092315

Batch ID R262045 Test Name : PH SOIL BY SW9045D Matrix: Soil

28 Sep 2015 12:00HS15091078-04 23 Sep 2015 09:20 14904-SB03-12

28 Sep 2015 12:00HS15091078-05 23 Sep 2015 17:50 14904-SB10-01


29 Sep 2015 16:52HS15091078-01 23 Sep 2015 09:10 14904-SB03-01

29 Sep 2015 17:16HS15091078-02 23 Sep 2015 09:10 14904-SB03-01 Dup

29 Sep 2015 17:39HS15091078-03 23 Sep 2015 09:10 14904-SB03-02

29 Sep 2015 18:03HS15091078-04 23 Sep 2015 09:20 14904-SB03-12

29 Sep 2015 18:27HS15091078-05 23 Sep 2015 17:50 14904-SB10-01


Page 140 of 261


WorkOrder:Project:




29 Sep 2015 12:22HS15091078-01 23 Sep 2015 09:10 14904-SB03-01

29 Sep 2015 12:22HS15091078-02 23 Sep 2015 09:10 14904-SB03-01 Dup

29 Sep 2015 12:22HS15091078-03 23 Sep 2015 09:10 14904-SB03-02

29 Sep 2015 12:22HS15091078-04 23 Sep 2015 09:20 14904-SB03-12

29 Sep 2015 12:22HS15091078-05 23 Sep 2015 17:50 14904-SB10-01

29 Sep 2015 12:22HS15091078-06 23 Sep 2015 17:55 14904-SB10-05

29 Sep 2015 12:22HS15091078-07 23 Sep 2015 18:00 14904-SB10-08

29 Sep 2015 12:22HS15091078-08 23 Sep 2015 16:40 14904-SB11-00

29 Sep 2015 12:22HS15091078-09 23 Sep 2015 16:40 14904-SB11-04

29 Sep 2015 12:22HS15091078-10 23 Sep 2015 16:45 14904-SB11-09

29 Sep 2015 12:22HS15091078-11 23 Sep 2015 16:45 14904-SB11-09 Dup


30 Sep 2015 10:04HS15091078-06 23 Sep 2015 17:55 14904-SB10-05

30 Sep 2015 10:28HS15091078-07 23 Sep 2015 18:00 14904-SB10-08

30 Sep 2015 12:03HS15091078-08 23 Sep 2015 16:40 14904-SB11-00

30 Sep 2015 12:27HS15091078-09 23 Sep 2015 16:40 14904-SB11-04

30 Sep 2015 12:50HS15091078-10 23 Sep 2015 16:45 14904-SB11-09

30 Sep 2015 13:14HS15091078-11 23 Sep 2015 16:45 14904-SB11-09 Dup

30 Sep 2015 13:38HS15091078-12 23 Sep 2015 15:20 14904-SB13-02

30 Sep 2015 14:02HS15091078-13 23 Sep 2015 15:25 14904-SB13-10

30 Sep 2015 14:25HS15091078-14 23 Sep 2015 15:25 14904-SB13-25

30 Sep 2015 14:49HS15091078-15 23 Sep 2015 13:25 14904-SB16-04

30 Sep 2015 15:14HS15091078-16 23 Sep 2015 13:30 14904-SB16-09

30 Sep 2015 15:37HS15091078-18 23 Sep 2015 11:15 14904-SB17-00

30 Sep 2015 16:01HS15091078-19 23 Sep 2015 11:10 14904-SB17-09

30 Sep 2015 16:25HS15091078-20 23 Sep 2015 11:15 14904-SB17-22


30 Sep 2015 14:32HS15091078-12 23 Sep 2015 15:20 14904-SB13-02

30 Sep 2015 14:32HS15091078-13 23 Sep 2015 15:25 14904-SB13-10

30 Sep 2015 14:32HS15091078-14 23 Sep 2015 15:25 14904-SB13-25

30 Sep 2015 14:32HS15091078-15 23 Sep 2015 13:25 14904-SB16-04

30 Sep 2015 14:32HS15091078-16 23 Sep 2015 13:30 14904-SB16-09

30 Sep 2015 14:32HS15091078-17 23 Sep 2015 13:35 14904-SB16-21.5

30 Sep 2015 14:32HS15091078-18 23 Sep 2015 11:15 14904-SB17-00

30 Sep 2015 14:32HS15091078-19 23 Sep 2015 11:10 14904-SB17-09

30 Sep 2015 14:32HS15091078-20 23 Sep 2015 11:15 14904-SB17-22


02 Oct 2015 13:34HS15091078-17 23 Sep 2015 13:35 14904-SB16-21.5


Page 141 of 261






Units: mg/Kg

Type Analyte DCSCAS MDL PQLDCS SpikeA 53TPHGRO 10nC6 to nC12 5025

A 23TPHDRO 10>nC12 to nC28 5025

A 2310W40MOTOROIL 10>nC28 to nC35 5025




Page 142 of 261



Test Code: TX1005_W_LowInstrumentID: FID-13


AqueousMatrix:Test Number: TX1005Test Name: Low-level Texas TPH by TX1005

Units: mg/L

Type Analyte DCSCAS MDL PQLDCS SpikeA 0.53TPHGRO 0.20nC6 to nC12 0.500.50

A 0.57TPHDRO 0.20>nC12 to nC28 0.500.50

A 0.5710W40MOTOROIL 0.20>nC28 to nC35 0.500.50

A 1.1TPH 0.20Total Petroleum Hydrocarbon 0.501.0



Page 143 of 261



Test Code: HG_S_LOWInstrumentID: HG02


SolidMatrix:Test Number: SW7471ATest Name: Mercury by SW7471B

Units: mg/Kg


Page 144 of 261



Test Code: HG_WInstrumentID: HG03


AqueousMatrix:Test Number: SW7470Test Name: Mercury by SW7470A

Units: mg/L


Page 145 of 261






Units: mg/Kg


A 0.2627440-38-2 0.100Arsenic 0.5000.250

A 0.2447440-39-3 0.0800Barium 0.5000.250

A 0.2017440-41-7 0.0500Beryllium 0.5000.250

A 0.2597440-43-9 0.0500Cadmium 0.5000.250

A 0.2917440-47-3 0.0900Chromium 0.5000.250

A 0.2637440-48-4 0.0700Cobalt 0.5000.250

A 0.2027440-50-8 0.100Copper 0.5000.250

A 0.2447439-92-1 0.0500Lead 0.5000.250

A 0.2707439-96-5 0.100Manganese 0.5000.250

A 0.2637440-02-0 0.0900Nickel 0.5000.250

A 0.3147782-49-2 0.180Selenium 0.5000.250

A 0.2437440-22-4 0.0800Silver 0.5000.250

A 0.2397440-28-0 0.0700Thallium 0.5000.250

A 0.3277440-62-2 0.230Vanadium 0.5000.250

A 0.3267440-66-6 0.250Zinc 0.5000.250

Page 146 of 261






Units: mg/Kg


A 0.1347440-38-2 0.100Arsenic 0.5000.100

A 0.05897440-39-3 0.0800Barium 0.5000.100

A 0.1097440-41-7 0.0500Beryllium 0.5000.100

A 0.07507440-43-9 0.0500Cadmium 0.5000.100

A 0.1497440-47-3 0.0900Chromium 0.5000.100

A 0.09887440-48-4 0.0700Cobalt 0.5000.100

A 0.09157440-50-8 0.100Copper 0.5000.100

A 0.1017439-92-1 0.0500Lead 0.5000.100

A 0.1247439-96-5 0.100Manganese 0.5000.100

A 0.08187440-02-0 0.0900Nickel 0.5000.100

A 0.1597782-49-2 0.180Selenium 0.5000.100

A 0.06617440-22-4 0.0800Silver 0.5000.100

A 0.09237440-28-0 0.0700Thallium 0.5000.100

A 0.1727440-62-2 0.230Vanadium 0.5000.100

A 0.1657440-66-6 0.250Zinc 0.5000.100

Page 147 of 261



Test Code: ICP_TWInstrumentID: ICPMS05


AqueousMatrix:Test Number: SW6020Test Name: ICP-MS Metals by SW6020A

Units: mg/L


A 0.0009347440-38-2 0.000400Arsenic 0.005000.00100

A 0.001047440-39-3 0.00190Barium 0.005000.00100

A 0.0007937440-41-7 0.000200Beryllium 0.002000.00100

A 0.001017440-43-9 0.000200Cadmium 0.002000.00100

A 0.0008547440-47-3 0.000400Chromium 0.005000.00100

A 0.001017440-48-4 0.000200Cobalt 0.005000.00100

A 0.0007787440-50-8 0.00100Copper 0.005000.00100

A 0.001047439-92-1 0.000600Lead 0.005000.00100

A 0.0008757439-96-5 0.000700Manganese 0.005000.00100

A 0.0006887440-02-0 0.000600Nickel 0.005000.00100

A 0.0007487782-49-2 0.00110Selenium 0.005000.00100

A 0.001017440-22-4 0.000200Silver 0.005000.00100

A 0.0008887440-28-0 0.000200Thallium 0.002000.00100

A 0.0007707440-62-2 0.000600Vanadium 0.005000.00100

A 0.007487440-66-6 0.00200Zinc 0.005000.00100

Page 148 of 261






Units: mg/Kg









A 0.009151-28-5 0.00452,4-Dinitrophenol 0.0130.0033




A 0.003095-57-8 0.00132-Chlorophenol 0.00660.0033


A 0.003295-48-7 0.00112-Methylphenol 0.00660.0033

A 0.003688-74-4 0.00192-Nitroaniline 0.00660.0033

A 0.002788-75-5 0.00252-Nitrophenol 0.00660.0033



A 0.002899-09-2 0.00193-Nitroaniline 0.00660.0033





A 0.0024100-01-6 0.00224-Nitroaniline 0.00660.0033

A 0.0024100-02-7 0.00194-Nitrophenol 0.0130.0033

A 0.001783-32-9 0.00050Acenaphthene 0.00330.0017


A 0.003698-86-2 0.00080Acetophenone 0.00660.0033

A 0.003462-53-3 0.0014Aniline 0.00660.0033

A 0.0016120-12-7 0.00050Anthracene 0.00330.0017


A 0.0045100-52-7 0.0012Benzaldehyde 0.00660.0033

A 0.001350-32-8 0.0010Benzo(a)pyrene 0.00330.0017








Page 149 of 261






Units: mg/Kg


A 0.0037105-60-2 0.0012Caprolactam 0.00660.0033

A 0.003086-74-8 0.0012Carbazole 0.00660.0033

A 0.0019218-01-9 0.00080Chrysene 0.00330.0017


A 0.0017132-64-9 0.00070Dibenzofuran 0.00330.0017





A 0.0018206-44-0 0.0011Fluoranthene 0.00330.0017

A 0.001786-73-7 0.0011Fluorene 0.00330.0017






A 0.003778-59-1 0.00080Isophorone 0.00660.0033

A 0.001791-20-3 0.00060Naphthalene 0.00330.0017

A 0.004398-95-3 0.00090Nitrobenzene 0.00660.0033




A 0.001885-01-8 0.0015Phenanthrene 0.00330.0017

A 0.0038108-95-2 0.0011Phenol 0.00660.0033

A 0.0016129-00-0 0.00060Pyrene 0.00330.0017

A 0.0029110-86-1 0.00090Pyridine 0.00660.0033




S 01718-51-0 04-Terphenyl-d14 00


S 013127-88-3 0Phenol-d6 00

Page 150 of 261



Test Code: 8270_LOW_WInstrumentID: SV-6


AqueousMatrix:Test Number: SW8270Test Name: Low-Level Semivolatiles

Units: mg/L









A 0.00008351-28-5 0.000102,4-Dinitrophenol 0.00100.00010




A 0.00008995-57-8 0.0000362-Chlorophenol 0.000200.00010


A 0.00007895-48-7 0.0000452-Methylphenol 0.000200.00010

A 0.00009588-74-4 0.0000412-Nitroaniline 0.000200.00010

A 0.00008388-75-5 0.0000342-Nitrophenol 0.000200.00010



A 0.00007799-09-2 0.0000493-Nitroaniline 0.000200.00010





A 0.00010100-01-6 0.0000354-Nitroaniline 0.000200.00010

A 0.000081100-02-7 0.0000474-Nitrophenol 0.00100.00010

A 0.00005783-32-9 0.000027Acenaphthene 0.000100.000050


A 0.00008898-86-2 0.000024Acetophenone 0.000200.00010

A 0.00007862-53-3 0.000020Aniline 0.000200.00010

A 0.000045120-12-7 0.000014Anthracene 0.000100.000050


A 0.00012100-52-7 0.000030Benzaldehyde 0.000200.00010

A 0.00005150-32-8 0.000020Benzo(a)pyrene 0.000100.000050








Page 151 of 261






Units: mg/L


A 0.000056105-60-2 0.000045Caprolactam 0.000200.00010

A 0.00008486-74-8 0.000025Carbazole 0.000200.00010

A 0.000057218-01-9 0.000021Chrysene 0.000100.000050


A 0.000098132-64-9 0.000020Dibenzofuran 0.000100.00010





A 0.000048206-44-0 0.000010Fluoranthene 0.000100.000050

A 0.00005186-73-7 0.000030Fluorene 0.000100.000050






A 0.00009678-59-1 0.000025Isophorone 0.000200.00010

A 0.00005291-20-3 0.000020Naphthalene 0.000100.000050

A 0.0001298-95-3 0.000024Nitrobenzene 0.000200.00010




A 0.00005185-01-8 0.000021Phenanthrene 0.000100.000050

A 0.000096108-95-2 0.000035Phenol 0.000200.00010

A 0.000049129-00-0 0.000019Pyrene 0.000100.000050

A 0.000082110-86-1 0.000030Pyridine 0.00100.00010

S 0118-79-6 02,4,6-Tribromophenol 0.000200

S 0321-60-8 02-Fluorobiphenyl 0.000200

S 0367-12-4 02-Fluorophenol 0.000200

S 01718-51-0 04-Terphenyl-d14 0.000200

S 04165-60-0 0Nitrobenzene-d5 0.000200

S 013127-88-3 0Phenol-d6 0.000200

Page 152 of 261






Units: mg/L











A 0.00055106-93-4 0.000201,2-Dibromoethane 0.00100.00050







A 0.001278-93-3 0.000502-Butanone 0.00200.0010

A 0.00083591-78-6 0.00102-Hexanone 0.00200.0010



A 0.001667-64-1 0.0020Acetone 0.00200.0010

A 0.0006271-43-2 0.00020Benzene 0.00100.00050


A 0.0006275-25-2 0.00040Bromoform 0.00100.00050

A 0.002674-83-9 0.00040Bromomethane 0.00100.00050



A 0.00071108-90-7 0.00030Chlorobenzene 0.00100.00050

A 0.0007775-00-3 0.00030Chloroethane 0.00100.00050

A 0.0007467-66-3 0.00020Chloroform 0.00100.00050

A 0.0007274-87-3 0.00020Chloromethane 0.00100.00050



A 0.0012110-82-7 0.00030Cyclohexane 0.00100.00050



A 0.00068100-41-4 0.00030Ethylbenzene 0.00100.00050




Page 153 of 261






Units: mg/L


A 0.00003591-20-3 0.00030Naphthalene 0.00100.0010

A 0.00045104-51-8 0.00040n-Butylbenzene 0.00100.00050



A 0.00058100-42-5 0.00030Styrene 0.00100.00050



A 0.00066108-88-3 0.00020Toluene 0.00100.00050





A 0.0005575-01-4 0.00020Vinyl chloride 0.00100.00050

A 0.00181330-20-7 0.00050Xylenes, Total 0.00300.0015




S 02037-26-5 0Toluene-d8 0.00100

Page 154 of 261






Units: mg/Kg











A 0.0012106-93-4 0.000501,2-Dibromoethane 0.00500.0012







A 0.002978-93-3 0.00132-Butanone 0.0100.0025

A 0.0024591-78-6 0.00142-Hexanone 0.0100.0025



A 0.01467-64-1 0.0031Acetone 0.0200.010

A 0.001371-43-2 0.00050Benzene 0.00500.0012


A 0.003375-25-2 0.00060Bromoform 0.00500.0012

A 0.001774-83-9 0.0010Bromomethane 0.0100.0012



A 0.0012108-90-7 0.00060Chlorobenzene 0.00500.0012

A 0.001375-00-3 0.00080Chloroethane 0.0100.0012

A 0.002367-66-3 0.00050Chloroform 0.00500.0012

A 0.001474-87-3 0.00050Chloromethane 0.0100.0012



A 0.0011110-82-7 0.0010Cyclohexane 0.00500.0012



A 0.0012100-41-4 0.00070Ethylbenzene 0.00500.0012




Page 155 of 261






Units: mg/Kg


A 0.001691-20-3 0.00080Naphthalene 0.00500.0012

A 0.0013104-51-8 0.00060n-Butylbenzene 0.00500.0012



A 0.0016100-42-5 0.00070Styrene 0.00500.0012



A 0.0014108-88-3 0.00060Toluene 0.00500.0012





A 0.001175-01-4 0.00080Vinyl chloride 0.00200.0012

A 0.00381330-20-7 0.0024Xylenes, Total 0.0100.0038




S 02037-26-5 0Toluene-d8 00

Page 156 of 261






Units: wt%


Page 157 of 261



Test Code: PH_SInstrumentID: WetChem_HS


SolidMatrix:Test Number: SW9045BTest Name: pH Soil by SW9045D

Units: pH Units

Type Analyte DCSCAS MDL PQLDCS SpikeA 0PH 0.100pH 0.1000

A 0TEMP 0Temp Deg C @pH 00

Page 158 of 261

Client:Project:



QC BATCH REPORT


Sample ID: MBLK-97466 Units: mg/L Analysis Date: 26-Sep-2015 02:30



Value %RECControl

LimitRPD Ref


MBLK

Client ID:

nC6 to nC12 U 0.50

>nC12 to nC28 U 0.50

>nC28 to nC35 U 0.50

Total Petroleum Hydrocarbon U 0.50


2.952 2.5 0 118 70 - 1300Surr: Trifluoromethyl benzene

Sample ID: LCS-97466 Units: mg/L Analysis Date: 26-Sep-2015 03:01



Value %RECControl

LimitRPD Ref


LCS

Client ID:

nC6 to nC12 28.52 25 0 114 75 - 1250.50

>nC12 to nC28 29.13 25 0 117 75 - 1250.50



Sample ID: LCSD-97466 Units: mg/L Analysis Date: 26-Sep-2015 03:32



Value %RECControl

LimitRPD Ref


LCSD

Client ID:

nC6 to nC12 26.83 25 0 107 75 - 125 28.52 6.09 200.50

>nC12 to nC28 28.95 25 0 116 75 - 125 29.13 0.638 200.50


2.847 2.5 0 114 70 - 130 3.024 6.05 200Surr: Trifluoromethyl benzene

Sample ID: HS15091078-21MS Units: mg/L Analysis Date: 29-Sep-2015 13:29



Value %RECControl

LimitRPD Ref


MS

Client ID: EB 092315

nC6 to nC12 19.57 23.47 0 83.4 75 - 1250.47

>nC12 to nC28 20.45 23.47 0 87.1 75 - 1250.47





Page 159 of 261

Client:Project:



QC BATCH REPORT


Sample ID: HS15091078-21MSD Units: mg/L Analysis Date: 29-Sep-2015 13:58



Value %RECControl

LimitRPD Ref


MSD


nC6 to nC12 25 23.13 0 108 75 - 125 19.57 24.4 20 R 0.46

>nC12 to nC28 23.78 23.13 0 103 75 - 125 20.45 15.1 200.46

2.707 2.313 0 117 70 - 130 2.205 20.4 20 R 0Surr: 2-Fluorobiphenyl


The following samples were anayzed in this batch: HS15091078-21



Page 160 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MBLK

Client ID:

nC6 to nC12 U 50

>nC12 to nC28 U 50

>nC28 to nC35 U 50




Sample ID: LCS-97468 Units: mg/Kg Analysis Date: 27-Sep-2015 23:00



Value %RECControl

LimitRPD Ref


LCS

Client ID:

nC6 to nC12 275.5 250 0 110 75 - 12550

>nC12 to nC28 286.1 250 0 114 75 - 12550


26.23 25 0 105 70 - 1300Surr: Trifluoromethyl benzene

Sample ID: LCSD-97468 Units: mg/Kg Analysis Date: 27-Sep-2015 23:29



Value %RECControl

LimitRPD Ref


LCSD

Client ID:

nC6 to nC12 236.7 250 0 94.7 75 - 125 275.5 15.2 2050

>nC12 to nC28 252 250 0 101 75 - 125 286.1 12.7 2050


22.05 25 0 88.2 70 - 130 26.23 17.3 200Surr: Trifluoromethyl benzene




Value %RECControl

LimitRPD Ref


MS


nC6 to nC12 198.3 182.7 0 109 75 - 12537

>nC12 to nC28 172.8 182.7 0 94.5 75 - 12537





Page 161 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MS

Client ID: 4904-SB10-08

nC6 to nC12 228.3 190.3 0 120 75 - 12538

>nC12 to nC28 193.6 190.3 0 102 75 - 12538






Value %RECControl

LimitRPD Ref


MSD


nC6 to nC12 174.1 187.1 0 93.0 75 - 125 198.3 13 2037

>nC12 to nC28 177.3 187.1 0 94.8 75 - 125 172.8 2.61 2037






Value %RECControl

LimitRPD Ref


MSD


nC6 to nC12 230.8 200.5 0 115 75 - 125 228.3 1.09 2040

>nC12 to nC28 214.7 200.5 0 107 75 - 125 193.6 10.3 2040



The following samples were anayzed in this batch: HS15091078-01 HS15091078-02 HS15091078-03 HS15091078-04 HS15091078-05 HS15091078-06 HS15091078-07 HS15091078-08 HS15091078-09 HS15091078-10 HS15091078-11 HS15091078-12 HS15091078-13 HS15091078-14 HS15091078-15 HS15091078-16 HS15091078-17 HS15091078-18 HS15091078-19 HS15091078-20



Page 162 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MBLK

Client ID:

Antimony U 0.00500

Arsenic U 0.00500

Barium U 0.00500

Beryllium U 0.00200

Cadmium U 0.00200

Chromium U 0.00500

Cobalt U 0.00500

Copper U 0.00500

Lead U 0.00500

Manganese U 0.00500

Nickel U 0.00500

Selenium U 0.00500

Silver U 0.00500

Thallium U 0.00200

Vanadium U 0.00500

Zinc 0.002802 J 0.00500



Page 163 of 261

Client:Project:



QC BATCH REPORT


Sample ID: MLCS-97447 Units: mg/L Analysis Date: 28-Sep-2015 14:55



Value %RECControl

LimitRPD Ref


LCS

Client ID:

Antimony 0.04788 0.05 0 95.8 80 - 1200.00500

Arsenic 0.04732 0.05 0 94.6 80 - 1200.00500

Barium 0.04667 0.05 0 93.3 80 - 1200.00500

Beryllium 0.04756 0.05 0 95.1 80 - 1200.00200

Cadmium 0.04713 0.05 0 94.3 80 - 1200.00200

Chromium 0.04756 0.05 0 95.1 80 - 1200.00500

Cobalt 0.0477 0.05 0 95.4 80 - 1200.00500

Copper 0.04724 0.05 0 94.5 80 - 1200.00500

Lead 0.04632 0.05 0 92.6 80 - 1200.00500

Manganese 0.04778 0.05 0 95.6 80 - 1200.00500

Nickel 0.04689 0.05 0 93.8 80 - 1200.00500

Selenium 0.04624 0.05 0 92.5 80 - 1200.00500

Silver 0.04747 0.05 0 94.9 80 - 1200.00500

Thallium 0.04501 0.05 0 90.0 80 - 1200.00200

Vanadium 0.04642 0.05 0 92.8 80 - 1200.00500

Zinc 0.05251 0.05 0 105 80 - 1200.00500



Page 164 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MS

Client ID:

Antimony 0.04902 0.05 0.000088 97.9 80 - 1200.00500

Arsenic 0.05176 0.05 0.002384 98.8 80 - 1200.00500

Barium 0.1505 0.05 0.1017 97.5 80 - 1200.00500

Beryllium 0.07322 0.05 0.000099 146 80 - 120 S 0.00200

Cadmium 0.04575 0.05 0.000311 90.9 80 - 1200.00200

Chromium 0.04784 0.05 0.000951 93.8 80 - 1200.00500

Cobalt 0.04864 0.05 0.00377 89.7 80 - 1200.00500

Copper 0.04696 0.05 0.003695 86.5 80 - 1200.00500

Lead 0.0475 0.05 0.000454 94.1 80 - 1200.00500

Manganese 2.258 0.05 2.212 92.8 80 - 120 EO 0.00500

Nickel 0.2038 0.05 0.1604 86.6 80 - 1200.00500

Selenium 0.05034 0.05 0.000596 99.5 80 - 1200.00500

Silver 0.04506 0.05 0.000031 90.1 80 - 1200.00500

Thallium 0.04589 0.05 0.000675 90.4 80 - 1200.00200

Vanadium 0.06307 0.05 0.01464 96.9 80 - 1200.00500

Zinc 0.0495 0.05 0.004209 90.6 80 - 1200.00500



Page 165 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MSD

Client ID:

Antimony 0.0479 0.05 0.000088 95.6 80 - 120 0.04902 2.3 200.00500

Arsenic 0.05049 0.05 0.002384 96.2 80 - 120 0.05176 2.49 200.00500

Barium 0.1473 0.05 0.1017 91.1 80 - 120 0.1505 2.15 200.00500

Beryllium 0.07283 0.05 0.000099 145 80 - 120 0.07322 0.534 20 S 0.00200

Cadmium 0.046 0.05 0.000311 91.4 80 - 120 0.04575 0.538 200.00200

Chromium 0.04711 0.05 0.000951 92.3 80 - 120 0.04784 1.53 200.00500

Cobalt 0.04787 0.05 0.00377 88.2 80 - 120 0.04864 1.6 200.00500

Copper 0.04676 0.05 0.003695 86.1 80 - 120 0.04696 0.427 200.00500

Lead 0.04668 0.05 0.000454 92.4 80 - 120 0.0475 1.75 200.00500

Manganese 2.262 0.05 2.212 99.6 80 - 120 2.258 0.15 20 EO 0.00500

Nickel 0.2032 0.05 0.1604 85.5 80 - 120 0.2038 0.275 200.00500

Selenium 0.04914 0.05 0.000596 97.1 80 - 120 0.05034 2.41 200.00500

Silver 0.04482 0.05 0.000031 89.6 80 - 120 0.04506 0.523 200.00500

Thallium 0.04478 0.05 0.000675 88.2 80 - 120 0.04589 2.45 200.00200

Vanadium 0.06273 0.05 0.01464 96.2 80 - 120 0.06307 0.545 200.00500

Zinc 0.04948 0.05 0.004209 90.5 80 - 120 0.0495 0.0384 200.00500



Page 166 of 261

Client:Project:



QC BATCH REPORT


Sample ID: HS15091053-16BS Units: mg/L Analysis Date: 28-Sep-2015 15:14



Value %RECControl

LimitRPD Ref


PDS

Client ID:

Antimony 0.09189 0.1 0.000088 91.8 75 - 1250.00500

Arsenic 0.09242 0.1 0.002384 90.0 75 - 1250.00500

Barium 0.188 0.1 0.1017 86.3 75 - 1250.00500

Beryllium 0.1122 0.1 0.000099 112 75 - 1250.00200

Cadmium 0.08783 0.1 0.000311 87.5 75 - 1250.00200

Chromium 0.08558 0.1 0.000951 84.6 75 - 1250.00500

Cobalt 0.08664 0.1 0.00377 82.9 75 - 1250.00500

Copper 0.08425 0.1 0.003695 80.6 75 - 1250.00500

Lead 0.09117 0.1 0.000454 90.7 75 - 1250.00500

Manganese 2.215 0.1 2.212 3.44 75 - 125 SEO 0.00500

Nickel 0.2341 0.1 0.1604 73.7 75 - 125 S 0.00500

Selenium 0.09072 0.1 0.000596 90.1 75 - 1250.00500

Silver 0.08402 0.1 0.000031 84.0 75 - 1250.00500

Thallium 0.0899 0.1 0.000675 89.2 75 - 1250.00200

Vanadium 0.1016 0.1 0.01464 87.0 75 - 1250.00500

Zinc 0.08991 0.1 0.004209 85.7 75 - 1250.00500



Page 167 of 261

Client:Project:



QC BATCH REPORT


Sample ID: HS15091053-16 DIL SX Units: mg/L Analysis Date: 28-Sep-2015 15:06



Value %RECControl

LimitRPD Ref


SD

Client ID:

Antimony U 0.000088 0 100.0250

Arsenic 0.00249 0.002384 0 10 J 0.0250

Barium 0.1015 0.1017 0.17 100.0250

Beryllium U 0.000099 0 100.0100

Cadmium U 0.000311 0 100.0100

Chromium U 0.000951 0 100.0250

Cobalt 0.003981 0.00377 0 10 J 0.0250

Copper U 0.003695 0 100.0250

Lead U 0.000454 0 100.0250

Manganese 2.161 2.212 2.3 100.0250

Nickel 0.1673 0.1604 4.29 100.0250

Selenium U 0.000596 0 100.0250

Silver U 0.000031 0 100.0250

Thallium U 0.000675 0 100.0100

Vanadium 0.01235 0.01464 0 10 J 0.0250

Zinc U 0.004209 0 100.0250




Page 168 of 261

Client:Project:



QC BATCH REPORT

Batch ID: 97456 Instrument: HG03 Method: SW7470




Value %RECControl

LimitRPD Ref


MBLK

Client ID:

Mercury U 0.000200

Sample ID: LCS-97456 Units: mg/L Analysis Date: 25-Sep-2015 15:02



Value %RECControl

LimitRPD Ref


LCS

Client ID:

Mercury 0.00499 0.005 0 99.8 80 - 1240.000200




Value %RECControl

LimitRPD Ref


MS


Mercury 0.00493 0.005 0.000016 98.3 80 - 1240.000200




Value %RECControl

LimitRPD Ref


MSD


Mercury 0.00491 0.005 0.000016 97.9 80 - 124 0.00493 0.407 200.000200




Page 169 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MBLK

Client ID:

Mercury U 3.32




Value %RECControl

LimitRPD Ref


LCS

Client ID:

Mercury 344 333.3 0 103 85 - 1153.32




Value %RECControl

LimitRPD Ref


MS


Mercury 337.2 342.6 -0.1373 98.4 85 - 1153.42




Value %RECControl

LimitRPD Ref


MSD


Mercury 333 341.9 -0.1373 97.4 85 - 115 337.2 1.23 203.41

The following samples were anayzed in this batch: HS15091078-01 HS15091078-02 HS15091078-03 HS15091078-04 HS15091078-05 HS15091078-06 HS15091078-07 HS15091078-08 HS15091078-09 HS15091078-10 HS15091078-11 HS15091078-12 HS15091078-13 HS15091078-14 HS15091078-15 HS15091078-16 HS15091078-18 HS15091078-19 HS15091078-20



Page 170 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MBLK

Client ID:

Antimony U 0.500

Arsenic U 0.500

Barium U 0.500

Beryllium U 0.500

Cadmium U 0.500

Chromium U 0.500

Cobalt U 0.500

Copper U 0.500

Lead U 0.500

Manganese U 0.500

Nickel U 0.500

Selenium U 0.500

Silver U 0.500

Thallium U 0.500

Vanadium U 0.500

Zinc U 0.500



Page 171 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


LCS

Client ID:

Antimony 9.864 10 0 98.6 80 - 1200.500

Arsenic 9.627 10 0 96.3 80 - 1200.500

Barium 9.798 10 0 98.0 80 - 1200.500

Beryllium 10.29 10 0 103 80 - 1200.500

Cadmium 9.646 10 0 96.5 80 - 1200.500

Chromium 9.879 10 0 98.8 80 - 1200.500

Cobalt 10.02 10 0 100 80 - 1200.500

Copper 10.16 10 0 102 80 - 1200.500

Lead 9.528 10 0 95.3 80 - 1200.500

Manganese 9.612 10 0 96.1 80 - 1200.500

Nickel 10.09 10 0 101 80 - 1200.500

Selenium 9.37 10 0 93.7 80 - 1200.500

Silver 9.847 10 0 98.5 80 - 1200.500

Thallium 9.444 10 0 94.4 80 - 1200.500

Vanadium 9.757 10 0 97.6 80 - 1200.500

Zinc 10.03 10 0 100 80 - 1200.500



Page 172 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MS


Antimony 5.769 9.101 0.01775 63.2 75 - 125 S 0.455

Arsenic 9.741 9.101 1.442 91.2 75 - 1250.455

Barium 154.6 9.101 124.1 335 75 - 125 SO 0.455

Beryllium 10.8 9.101 0.808 110 75 - 1250.455

Cadmium 8.611 9.101 0.0262 94.3 75 - 1250.455

Chromium 20.07 9.101 8.92 122 75 - 1250.455

Cobalt 12.83 9.101 3.858 98.6 75 - 1250.455

Copper 14 9.101 5.023 98.7 75 - 1250.455

Lead 16.62 9.101 7.308 102 75 - 1250.455

Manganese 262.2 9.101 224.8 411 75 - 125 SEO 0.455

Nickel 19.24 9.101 9.775 104 75 - 1250.455

Selenium 8.31 9.101 0.1771 89.4 75 - 1250.455

Silver 8.561 9.101 0.006948 94.0 75 - 1250.455

Thallium 8.252 9.101 0.08451 89.7 75 - 1250.455

Vanadium 27.54 9.101 14.86 139 75 - 125 S 0.455

Zinc 28.9 9.101 17.57 124 75 - 1250.455



Page 173 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MSD


Antimony 6.714 9.266 0.01775 72.3 75 - 125 5.769 15.1 20 S 0.463

Arsenic 9.954 9.266 1.442 91.9 75 - 125 9.741 2.16 200.463

Barium 141 9.266 124.1 183 75 - 125 154.6 9.18 20 SO 0.463

Beryllium 11.12 9.266 0.808 111 75 - 125 10.8 2.94 200.463

Cadmium 8.845 9.266 0.0262 95.2 75 - 125 8.611 2.68 200.463

Chromium 18.67 9.266 8.92 105 75 - 125 20.07 7.22 200.463

Cobalt 12.8 9.266 3.858 96.5 75 - 125 12.83 0.244 200.463

Copper 13.71 9.266 5.023 93.7 75 - 125 14 2.14 200.463

Lead 16.37 9.266 7.308 97.8 75 - 125 16.62 1.52 200.463

Manganese 260.2 9.266 224.8 382 75 - 125 262.2 0.775 20 SEO 0.463

Nickel 18.92 9.266 9.775 98.7 75 - 125 19.24 1.68 200.463

Selenium 8.578 9.266 0.1771 90.7 75 - 125 8.31 3.18 200.463

Silver 8.81 9.266 0.006948 95.0 75 - 125 8.561 2.86 200.463

Thallium 8.537 9.266 0.08451 91.2 75 - 125 8.252 3.4 200.463

Vanadium 25.21 9.266 14.86 112 75 - 125 27.54 8.82 200.463

Zinc 26.93 9.266 17.57 101 75 - 125 28.9 7.06 200.463



Page 174 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


PDS


Antimony 8.92 9.39 0.01775 94.8 75 - 1250.469

Arsenic 10.28 9.39 1.442 94.1 75 - 1250.469

Barium 139.4 9.39 124.1 163 75 - 125 SO 0.469

Beryllium 9.873 9.39 0.808 96.5 75 - 1250.469

Cadmium 8.973 9.39 0.0262 95.3 75 - 1250.469

Chromium 18.07 9.39 8.92 97.5 75 - 1250.469

Cobalt 12.81 9.39 3.858 95.3 75 - 1250.469

Copper 14.16 9.39 5.023 97.3 75 - 1250.469

Lead 16.54 9.39 7.308 98.3 75 - 1250.469

Nickel 18.75 9.39 9.775 95.6 75 - 1250.469

Selenium 8.868 9.39 0.1771 92.6 75 - 1250.469

Silver 9.018 9.39 0.006948 96.0 75 - 1250.469

Thallium 8.649 9.39 0.08451 91.2 75 - 1250.469

Vanadium 24.46 9.39 14.86 102 75 - 1250.469

Zinc 26.74 9.39 17.57 97.7 75 - 1250.469




Value %RECControl

LimitRPD Ref


PDS


Manganese 273.2 46.95 240.8 69.0 75 - 125 SO 2.35



Page 175 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


SD


Antimony U 0.01775 0 102.35

Arsenic 1.503 1.442 0 10 J 2.35

Barium 123.2 124.1 0.707 102.35

Beryllium 0.7546 0.808 0 10 J 2.35

Cadmium U 0.0262 0 102.35

Chromium 9.233 8.92 3.51 102.35

Cobalt 4.016 3.858 4.1 102.35

Copper 5.164 5.023 2.8 102.35

Lead 7.638 7.308 4.51 102.35

Manganese 238.7 224.8 6.17 102.35

Nickel 10.31 9.775 5.51 102.35

Selenium U 0.1771 0 102.35

Silver U 0.006948 0 102.35

Thallium U 0.08451 0 102.35

Vanadium 15.45 14.86 3.92 102.35

Zinc 18.25 17.57 3.82 102.35




Value %RECControl

LimitRPD Ref


SD


Manganese 225.8 240.8 6.23 1011.7




Page 176 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MBLK

Client ID:

Antimony U 0.500

Arsenic U 0.500

Barium U 0.500

Cadmium U 0.500

Chromium U 0.500

Cobalt U 0.500

Copper U 0.500

Lead U 0.500

Manganese U 0.500

Nickel U 0.500

Selenium U 0.500

Silver U 0.500

Vanadium U 0.500

Zinc U 0.500




Value %RECControl

LimitRPD Ref


MBLK

Client ID:

Beryllium U 0.500

Thallium U 0.500



Page 177 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


LCS

Client ID:

Antimony 10.49 10 0 105 80 - 1200.500

Arsenic 9.708 10 0 97.1 80 - 1200.500

Barium 10.16 10 0 102 80 - 1200.500

Cadmium 10.12 10 0 101 80 - 1200.500

Chromium 9.86 10 0 98.6 80 - 1200.500

Cobalt 9.829 10 0 98.3 80 - 1200.500

Copper 9.921 10 0 99.2 80 - 1200.500

Lead 10.16 10 0 102 80 - 1200.500

Manganese 9.842 10 0 98.4 80 - 1200.500

Nickel 9.806 10 0 98.1 80 - 1200.500

Selenium 9.813 10 0 98.1 80 - 1200.500

Silver 10.03 10 0 100 80 - 1200.500

Vanadium 9.876 10 0 98.8 80 - 1200.500

Zinc 10.04 10 0 100 80 - 1200.500




Value %RECControl

LimitRPD Ref


LCS

Client ID:

Beryllium 9.981 10 0 99.8 80 - 1200.500

Thallium 9.764 10 0 97.6 80 - 1200.500



Page 178 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MS


Antimony 2.971 8.962 0.0944 32.1 75 - 125 S 0.448

Arsenic 14.9 8.962 2.814 135 75 - 125 S 0.448

Barium 98.58 8.962 321.9 -2490 75 - 125 SO 0.448

Cadmium 8.864 8.962 0.1475 97.3 75 - 1250.448

Chromium 22.21 8.962 8.859 149 75 - 125 S 0.448

Cobalt 15.68 8.962 3.072 141 75 - 125 S 0.448

Copper 16.28 8.962 4.711 129 75 - 125 S 0.448

Lead 20.49 8.962 5.212 170 75 - 125 S 0.448

Manganese 463.3 8.962 337.7 1400 75 - 125 SEO 0.448

Nickel 20.55 8.962 9.318 125 75 - 125 S 0.448

Selenium 8.906 8.962 0.7864 90.6 75 - 1250.448

Silver 8.441 8.962 -0.0353 94.6 75 - 1250.448

Vanadium 35.69 8.962 12.19 262 75 - 125 S 0.448

Zinc 32.55 8.962 18.36 158 75 - 125 S 0.448




Value %RECControl

LimitRPD Ref


MS


Beryllium 10.14 8.962 0.5222 107 75 - 1250.448

Thallium 8.7 8.962 0.1281 95.7 75 - 1250.448



Page 179 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MSD


Antimony 3.052 9.604 0.0944 30.8 75 - 125 2.971 2.7 20 S 0.480

Arsenic 16.56 9.604 2.814 143 75 - 125 14.9 10.5 20 S 0.480

Barium 1239 9.604 321.9 9550 75 - 125 98.58 171 20 SREO 0.480

Cadmium 9.115 9.604 0.1475 93.4 75 - 125 8.864 2.79 200.480

Chromium 25.27 9.604 8.859 171 75 - 125 22.21 12.9 20 S 0.480

Cobalt 14.52 9.604 3.072 119 75 - 125 15.68 7.69 200.480

Copper 18.6 9.604 4.711 145 75 - 125 16.28 13.3 20 S 0.480

Lead 16.01 9.604 5.212 112 75 - 125 20.49 24.5 20 R 0.480

Manganese 344.3 9.604 337.7 69.1 75 - 125 463.3 29.5 20 SREO 0.480

Nickel 23.35 9.604 9.318 146 75 - 125 20.55 12.7 20 S 0.480

Selenium 9.523 9.604 0.7864 91.0 75 - 125 8.906 6.7 200.480

Silver 8.802 9.604 -0.0353 92.0 75 - 125 8.441 4.2 200.480

Vanadium 38.67 9.604 12.19 276 75 - 125 35.69 8.01 20 S 0.480

Zinc 39.13 9.604 18.36 216 75 - 125 32.55 18.4 20 S 0.480




Value %RECControl

LimitRPD Ref


MSD


Beryllium 10.75 9.604 0.5222 106 75 - 125 10.14 5.85 200.480

Thallium 9.169 9.604 0.1281 94.1 75 - 125 8.7 5.25 200.480



Page 180 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


PDS


Antimony 9.835 10.03 0.0944 97.1 75 - 1250.502

Arsenic 12.11 10.03 2.814 92.6 75 - 1250.502

Cadmium 9.576 10.03 0.1475 94.0 75 - 1250.502

Chromium 17.64 10.03 8.859 87.5 75 - 1250.502

Cobalt 12.02 10.03 3.072 89.2 75 - 1250.502

Copper 13.14 10.03 4.711 84.0 75 - 1250.502

Lead 14.85 10.03 5.212 96.0 75 - 1250.502

Nickel 17.69 10.03 9.318 83.4 75 - 1250.502

Selenium 10.22 10.03 0.7864 94.1 75 - 1250.502

Silver 9.117 10.03 -0.0353 91.2 75 - 1250.502

Vanadium 20.8 10.03 12.19 85.8 75 - 1250.502




Value %RECControl

LimitRPD Ref


PDS


Barium 323.6 50.16 282.6 81.8 75 - 125 O 2.51

Manganese 361.6 50.16 317.3 88.2 75 - 125 O 2.51




Value %RECControl

LimitRPD Ref


PDS


Beryllium 10.02 10.03 0.5222 94.6 75 - 1250.502

Thallium 9.577 10.03 0.1281 94.2 75 - 1250.502

Zinc 25.53 10.03 17.12 83.8 75 - 1250.502



Page 181 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


SD


Antimony U 0.0944 0 102.51

Arsenic 2.738 2.814 2.69 102.51

Cadmium U 0.1475 0 102.51

Chromium 8.658 8.859 2.28 102.51

Cobalt 2.983 3.072 2.91 102.51

Copper 4.804 4.711 1.97 102.51

Lead 5.227 5.212 0.289 102.51

Nickel 9.295 9.318 0.248 102.51

Selenium U 0.7864 0 102.51

Silver U -0.0353 0 102.51

Vanadium 11.87 12.19 2.59 102.51

Zinc 19.03 18.36 3.63 102.51




Value %RECControl

LimitRPD Ref


SD


Barium 286.9 282.6 1.54 1012.5

Manganese 306.7 317.3 3.34 1012.5




Value %RECControl

LimitRPD Ref


SD


Beryllium 0.6074 0.5222 0 10 J 2.51

Thallium U 0.1281 0 102.51

The following samples were anayzed in this batch: HS15091078-16 HS15091078-17 HS15091078-18 HS15091078-19 HS15091078-20



Page 182 of 261

Client:Project:



QC BATCH REPORT


Sample ID: MBLK-97632 Units: ug/Kg Analysis Date: 01-Oct-2015 15:27

Run ID: HG02_262370 SeqNo: 3447225 PrepDate: 01-Oct-2015 DF: 1


Value %RECControl

LimitRPD Ref


MBLK

Client ID:

Mercury U 3.32

Sample ID: LCS-97632 Units: ug/Kg Analysis Date: 01-Oct-2015 15:29



Value %RECControl

LimitRPD Ref


LCS

Client ID:

Mercury 336.7 333.3 0 101 85 - 1153.32

Sample ID: HS15091078-17MS Units: ug/Kg Analysis Date: 01-Oct-2015 15:33



Value %RECControl

LimitRPD Ref


MS


Mercury 382.7 341.7 -0.1368 112 85 - 1153.41

Sample ID: HS15091078-17MSD Units: ug/Kg Analysis Date: 01-Oct-2015 15:35



Value %RECControl

LimitRPD Ref


MSD


Mercury 386.3 341.2 -0.1368 113 85 - 115 382.7 0.929 203.40




Page 183 of 261

Client:Project:



QC BATCH REPORT


Sample ID: MBLK-97500 Units: ug/L Analysis Date: 28-Sep-2015 14:55



Value %RECControl

LimitRPD Ref


MBLK

Client ID:









2,4-Dinitrophenol U 1.0








2-Nitrophenol U 0.20









4-Nitrophenol U 1.0

Acenaphthene U 0.10


Acetophenone U 0.20

Aniline U 0.20

Anthracene U 0.10


Benzaldehyde U 0.20




Page 184 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MBLK

Client ID:









Caprolactam U 0.20

Carbazole U 0.20

Chrysene U 0.10


Dibenzofuran U 0.10





Fluoranthene U 0.10

Fluorene U 0.10






Isophorone U 0.20

Naphthalene U 0.10

Nitrobenzene U 0.20




Phenanthrene U 0.10

Phenol U 0.20

Pyrene U 0.10

Pyridine U 1.0



Page 185 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MBLK

Client ID:

1.841 5 0 36.8 34 - 1290.20Surr: 2,4,6-Tribromophenol

3.007 5 0 60.1 40 - 1250.20Surr: 2-Fluorobiphenyl

1.988 5 0 39.8 20 - 1200.20Surr: 2-Fluorophenol

3.14 5 0 62.8 40 - 1350.20Surr: 4-Terphenyl-d14

3.58 5 0 71.6 41 - 1200.20Surr: Nitrobenzene-d5

2.521 5 0 50.4 20 - 1200.20Surr: Phenol-d6



Page 186 of 261

Client:Project:



QC BATCH REPORT


Sample ID: LCS-97500 Units: ug/L Analysis Date: 28-Sep-2015 15:14



Value %RECControl

LimitRPD Ref


LCS

Client ID:

1,1´-Biphenyl 3.114 5 0 62.3 45 - 1250.20






2,4-Dichlorophenol 2.951 5 0 59.0 49 - 1200.20

2,4-Dimethylphenol 2.046 5 0 40.9 35 - 1200.20

2,4-Dinitrophenol 2.197 5 0 43.9 15 - 1201.0

2,4-Dinitrotoluene 3.137 5 0 62.7 50 - 1220.20

2,6-Dinitrotoluene 3.121 5 0 62.4 50 - 1200.20

2-Chloronaphthalene 3.602 5 0 72.0 50 - 1200.20

2-Chlorophenol 3.441 5 0 68.8 40 - 1200.20


2-Methylphenol 2.894 5 0 57.9 45 - 1200.20

2-Nitroaniline 4.918 5 0 98.4 28 - 1390.20

2-Nitrophenol 3.037 5 0 60.7 40 - 1200.20

3&4-Methylphenol 3.034 5 0 60.7 35 - 1200.20


3-Nitroaniline 3.165 5 0 63.3 30 - 1200.20





4-Nitroaniline 3.276 5 0 65.5 30 - 1330.20

4-Nitrophenol 2.896 5 0 57.9 30 - 1301.0

Acenaphthene 3.162 5 0 63.2 45 - 1200.10

Acenaphthylene 3.193 5 0 63.9 47 - 1200.10

Acetophenone 3.239 5 0 64.8 40 - 1200.20

Aniline 2.062 5 0 41.2 10 - 1200.20

Anthracene 2.951 5 0 59.0 45 - 1200.10


Benzaldehyde 1.423 5 0 28.5 15 - 1200.20

Benzo(a)pyrene 3.292 5 0 65.8 45 - 1200.10



Page 187 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


LCS

Client ID:









Caprolactam 2.996 5 0 59.9 35 - 1340.20

Carbazole 3.261 5 0 65.2 42 - 1280.20

Chrysene 3.2 5 0 64.0 43 - 1200.10


Dibenzofuran 3.157 5 0 63.1 50 - 1200.10



Di-n-butyl phthalate 3.565 5 0 71.3 45 - 1230.20

Di-n-octyl phthalate 4.721 5 0 94.4 45 - 1290.20

Fluoranthene 2.959 5 0 59.2 45 - 1250.10

Fluorene 3.078 5 0 61.6 49 - 1200.10





Indeno(1,2,3-cd)pyrene 3.296 5 0 65.9 41 - 1280.10

Isophorone 3.644 5 0 72.9 40 - 1210.20

Naphthalene 3.332 5 0 66.6 45 - 1200.10

Nitrobenzene 3.772 5 0 75.4 44 - 1200.20




Phenanthrene 3.109 5 0 62.2 45 - 1210.10

Phenol 3.52 5 0 70.4 20 - 1240.20

Pyrene 3.558 5 0 71.2 40 - 1300.10

Pyridine 3.611 5 0 72.2 15 - 1201.0



Page 188 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


LCS

Client ID:




3.24 5 0 64.8 40 - 1350.20Surr: 4-Terphenyl-d14


3.515 5 0 70.3 20 - 1200.20Surr: Phenol-d6



Page 189 of 261

Client:Project:



QC BATCH REPORT


Sample ID: LCSD-97500 Units: ug/L Analysis Date: 28-Sep-2015 15:34



Value %RECControl

LimitRPD Ref


LCSD

Client ID:

1,1´-Biphenyl 2.928 5 0 58.6 45 - 125 3.114 6.17 200.20

1,2,4,5-Tetrachlorobenzene 3.137 5 0 62.7 40 - 140 3.336 6.15 200.20

1-Methylnaphthalene 2.889 5 0 57.8 45 - 120 3.089 6.67 200.10

2,3,4,6-Tetrachlorophenol 2.576 5 0 51.5 30 - 140 2.69 4.31 200.20

2,4,5-Trichlorophenol 2.994 5 0 59.9 46 - 120 3.102 3.53 200.20

2,4,6-Trichlorophenol 2.718 5 0 54.4 42 - 120 2.796 2.85 200.20

2,4-Dichlorophenol 2.718 5 0 54.4 49 - 120 2.951 8.23 200.20

2,4-Dimethylphenol 1.82 5 0 36.4 35 - 120 2.046 11.7 200.20

2,4-Dinitrophenol 2.221 5 0 44.4 15 - 120 2.197 1.09 501.0

2,4-Dinitrotoluene 3.036 5 0 60.7 50 - 122 3.137 3.26 200.20

2,6-Dinitrotoluene 2.838 5 0 56.8 50 - 120 3.121 9.49 200.20

2-Chloronaphthalene 3.317 5 0 66.3 50 - 120 3.602 8.24 200.20

2-Chlorophenol 3.207 5 0 64.1 40 - 120 3.441 7.05 200.20

2-Methylnaphthalene 2.858 5 0 57.2 50 - 120 3.07 7.14 200.10

2-Methylphenol 3.11 5 0 62.2 45 - 120 2.894 7.17 200.20

2-Nitroaniline 4.681 5 0 93.6 28 - 139 4.918 4.94 200.20

2-Nitrophenol 2.922 5 0 58.4 40 - 120 3.037 3.87 200.20

3&4-Methylphenol 3.309 5 0 66.2 35 - 120 3.034 8.68 200.20

3,3´-Dichlorobenzidine 2.818 5 0 56.4 15 - 120 3.141 10.8 200.20

3-Nitroaniline 3.061 5 0 61.2 30 - 120 3.165 3.33 200.20

4,6-Dinitro-2-methylphenol 2.606 5 0 52.1 25 - 121 2.36 9.87 300.20

4-Bromophenyl phenyl ether 2.664 5 0 53.3 45 - 120 2.664 0.0135 200.20

4-Chloro-3-methylphenol 3.019 5 0 60.4 47 - 120 2.974 1.5 200.20

4-Chlorophenyl phenyl ether 2.697 5 0 53.9 50 - 120 2.873 6.33 200.20

4-Nitroaniline 3.075 5 0 61.5 30 - 133 3.276 6.32 200.20

4-Nitrophenol 2.808 5 0 56.2 30 - 130 2.896 3.11 201.0

Acenaphthene 2.944 5 0 58.9 45 - 120 3.162 7.12 200.10

Acenaphthylene 3.001 5 0 60.0 47 - 120 3.193 6.22 200.10

Acetophenone 3.031 5 0 60.6 40 - 120 3.239 6.64 200.20

Aniline 2.435 5 0 48.7 10 - 120 2.062 16.5 500.20

Anthracene 2.792 5 0 55.8 45 - 120 2.951 5.55 200.10

Benz(a)anthracene 3.22 5 0 64.4 40 - 120 3.432 6.38 200.10

Benzaldehyde 1.758 5 0 35.2 15 - 120 1.423 21.1 300.20

Benzo(a)pyrene 3.065 5 0 61.3 45 - 120 3.292 7.14 200.10



Page 190 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


LCSD

Client ID:

Benzo(b)fluoranthene 3.275 5 0 65.5 50 - 120 3.427 4.55 200.10

Benzo(g,h,i)perylene 3.223 5 0 64.5 42 - 127 3.403 5.44 200.10

Benzo(k)fluoranthene 3.053 5 0 61.1 45 - 127 3.31 8.07 200.10

Bis(2-chloroethoxy)methane 3.367 5 0 67.3 45 - 120 3.636 7.7 200.20

Bis(2-chloroethyl)ether 3.473 5 0 69.5 37 - 121 3.701 6.36 200.20

Bis(2-chloroisopropyl)ether 3.429 5 0 68.6 40 - 120 3.565 3.9 200.20

Bis(2-ethylhexyl)phthalate 4.163 5 0 83.3 40 - 139 4.412 5.81 200.20

Butyl benzyl phthalate 4.187 5 0 83.7 47 - 123 4.463 6.36 200.20

Caprolactam 2.98 5 0 59.6 35 - 134 2.996 0.554 200.20

Carbazole 3.308 5 0 66.2 42 - 128 3.261 1.45 200.20

Chrysene 3.267 5 0 65.3 43 - 120 3.2 2.07 200.10

Dibenz(a,h)anthracene 3.198 5 0 64.0 45 - 125 3.364 5.07 200.10

Dibenzofuran 2.95 5 0 59.0 50 - 120 3.157 6.77 200.10

Diethyl phthalate 3.176 5 0 63.5 41 - 120 3.392 6.58 200.20

Dimethyl phthalate 2.882 5 0 57.6 40 - 122 3.106 7.49 200.20

Di-n-butyl phthalate 3.542 5 0 70.8 45 - 123 3.565 0.652 200.20

Di-n-octyl phthalate 4.381 5 0 87.6 45 - 129 4.721 7.49 200.20

Fluoranthene 2.943 5 0 58.9 45 - 125 2.959 0.557 200.10

Fluorene 2.881 5 0 57.6 49 - 120 3.078 6.61 200.10

Hexachlorobenzene 2.545 5 0 50.9 48 - 120 2.625 3.09 200.20

Hexachlorobutadiene 2.508 5 0 50.2 40 - 120 2.59 3.22 200.20

Hexachlorocyclopentadiene 2.346 5 0 46.9 34 - 136 2.387 1.72 200.20

Hexachloroethane 3.518 5 0 70.4 40 - 120 3.622 2.91 200.20

Indeno(1,2,3-cd)pyrene 3.197 5 0 63.9 41 - 128 3.296 3.05 200.10

Isophorone 3.412 5 0 68.2 40 - 121 3.644 6.56 200.20

Naphthalene 3.103 5 0 62.1 45 - 120 3.332 7.11 200.10

Nitrobenzene 3.561 5 0 71.2 44 - 120 3.772 5.74 200.20

N-Nitrosodi-n-propylamine 3.844 5 0 76.9 40 - 120 3.954 2.83 200.20

N-Nitrosodiphenylamine 2.971 5 0 59.4 40 - 125 3.015 1.47 200.20

Pentachlorophenol 2.343 5 0 46.9 19 - 121 1.916 20.1 20 R 0.20

Phenanthrene 3.026 5 0 60.5 45 - 121 3.109 2.7 200.10

Phenol 3.511 5 0 70.2 20 - 124 3.52 0.249 200.20

Pyrene 3.386 5 0 67.7 40 - 130 3.558 4.95 200.10

Pyridine 3.332 5 0 66.6 15 - 120 3.611 8.03 201.0



Page 191 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


LCSD

Client ID:

2.114 5 0 42.3 34 - 129 2.058 2.69 200.20Surr: 2,4,6-Tribromophenol

2.775 5 0 55.5 40 - 125 3.05 9.44 200.20Surr: 2-Fluorobiphenyl

2.983 5 0 59.7 20 - 120 3.021 1.27 200.20Surr: 2-Fluorophenol

3.014 5 0 60.3 40 - 135 3.24 7.24 200.20Surr: 4-Terphenyl-d14

3.34 5 0 66.8 41 - 120 3.577 6.86 200.20Surr: Nitrobenzene-d5

3.33 5 0 66.6 20 - 120 3.515 5.42 200.20Surr: Phenol-d6




Page 192 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MBLK

Client ID:

















2-Nitrophenol U 6.6









4-Nitrophenol U 13

Acenaphthene U 3.3


Acetophenone U 6.6

Aniline U 6.6

Anthracene U 3.3


Benzaldehyde U 6.6




Page 193 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MBLK

Client ID:









Caprolactam U 6.6

Carbazole U 6.6

Chrysene U 3.3


Dibenzofuran U 3.3





Fluoranthene U 3.3

Fluorene U 3.3






Isophorone U 6.6

Naphthalene U 3.3

Nitrobenzene U 6.6




Phenanthrene U 3.3

Phenol U 6.6

Pyrene U 3.3

Pyridine U 6.6



Page 194 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MBLK

Client ID:




141.7 167 0 84.8 32 - 1250Surr: 4-Terphenyl-d14


144.7 167 0 86.6 40 - 1250Surr: Phenol-d6



Page 195 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


LCS

Client ID:

1,1´-Biphenyl 129.6 167 0 77.6 50 - 1206.6






2,4-Dichlorophenol 138.5 167 0 83.0 45 - 1256.6

2,4-Dimethylphenol 130.1 167 0 77.9 45 - 1206.6

2,4-Dinitrophenol 138.7 167 0 83.1 10 - 12613

2,4-Dinitrotoluene 143.7 167 0 86.0 50 - 1306.6

2,6-Dinitrotoluene 150 167 0 89.8 50 - 1256.6


2-Chlorophenol 130.6 167 0 78.2 45 - 1206.6


2-Methylphenol 142.3 167 0 85.2 45 - 1206.6

2-Nitroaniline 147.5 167 0 88.3 45 - 1386.6

2-Nitrophenol 136.4 167 0 81.7 45 - 1256.6

3&4-Methylphenol 144.8 167 0 86.7 45 - 1206.6


3-Nitroaniline 141.1 167 0 84.5 40 - 1206.6





4-Nitroaniline 142.6 167 0 85.4 50 - 1276.6

4-Nitrophenol 176.2 167 0 106 40 - 14713

Acenaphthene 137.6 167 0 82.4 50 - 1203.3

Acenaphthylene 131.7 167 0 78.9 50 - 1203.3

Acetophenone 133.8 167 0 80.1 50 - 1206.6

Aniline 139.6 167 0 83.6 10 - 1356.6

Anthracene 148.4 167 0 88.9 50 - 1233.3


Benzaldehyde 39.38 167 0 23.6 22 - 1296.6

Benzo(a)pyrene 153.4 167 0 91.8 50 - 1303.3



Page 196 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


LCS

Client ID:

Benzo(b)fluoranthene 169.2 167 0 101 50 - 1373.3








Caprolactam 155.2 167 0 93.0 50 - 1356.6

Carbazole 145.1 167 0 86.9 50 - 1436.6

Chrysene 141 167 0 84.4 50 - 1303.3

Dibenz(a,h)anthracene 171.1 167 0 102 50 - 1303.3

Dibenzofuran 134.2 167 0 80.4 50 - 1253.3



Di-n-butyl phthalate 158 167 0 94.6 50 - 1406.6


Fluoranthene 160.9 167 0 96.4 50 - 1313.3

Fluorene 139.8 167 0 83.7 50 - 1253.3





Indeno(1,2,3-cd)pyrene 194.8 167 0 117 45 - 1393.3

Isophorone 151.5 167 0 90.7 45 - 1306.6

Naphthalene 129 167 0 77.2 50 - 1253.3

Nitrobenzene 151.3 167 0 90.6 50 - 1256.6




Phenanthrene 141.8 167 0 84.9 50 - 1253.3

Phenol 143.2 167 0 85.8 45 - 1306.6

Pyrene 143.1 167 0 85.7 45 - 1303.3

Pyridine 143.8 167 0 86.1 15 - 1206.6



Page 197 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


LCS

Client ID:

178.4 167 0 107 36 - 1260Surr: 2,4,6-Tribromophenol


140 167 0 83.8 37 - 1250Surr: 2-Fluorophenol

145 167 0 86.8 32 - 1250Surr: 4-Terphenyl-d14


153 167 0 91.6 40 - 1250Surr: Phenol-d6



Page 198 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MS


1,1´-Biphenyl 120.5 166.9 0 72.2 50 - 1206.6



2,3,4,6-Tetrachlorophenol 140.9 166.9 0 84.4 40 - 1406.6



2,4-Dichlorophenol 121 166.9 0 72.5 45 - 1256.6

2,4-Dimethylphenol 108.1 166.9 0 64.7 45 - 1206.6

2,4-Dinitrophenol 94.53 166.9 0 56.6 10 - 12613

2,4-Dinitrotoluene 125.7 166.9 0 75.3 50 - 1306.6

2,6-Dinitrotoluene 129.3 166.9 0 77.5 50 - 1256.6

2-Chloronaphthalene 132.7 166.9 0 79.5 50 - 1456.6

2-Chlorophenol 117.7 166.9 0 70.5 45 - 1206.6

2-Methylnaphthalene 121 166.9 0 72.5 50 - 1203.3

2-Methylphenol 144.4 166.9 0 86.5 45 - 1206.6

2-Nitroaniline 130 166.9 0 77.9 45 - 1386.6

2-Nitrophenol 123.5 166.9 0 73.9 45 - 1256.6

3&4-Methylphenol 143.5 166.9 0 86.0 45 - 1206.6


3-Nitroaniline 127.4 166.9 0 76.3 40 - 1206.6



4-Chloro-3-methylphenol 134.8 166.9 0 80.8 45 - 1306.6


4-Nitroaniline 128.8 166.9 0 77.2 50 - 1276.6

4-Nitrophenol 156.1 166.9 0 93.5 40 - 14713

Acenaphthene 126 166.9 0 75.5 50 - 1203.3

Acenaphthylene 120.8 166.9 0 72.4 50 - 1203.3

Acetophenone 121 166.9 0 72.5 50 - 1206.6

Aniline 121.9 166.9 0 73.0 10 - 1356.6

Anthracene 132 166.9 0 79.1 50 - 1233.3


Benzaldehyde 51.54 166.9 2.282 29.5 22 - 1296.6

Benzo(a)pyrene 135 166.9 0 80.8 50 - 1303.3



Page 199 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MS


Benzo(b)fluoranthene 153.1 166.9 0 91.7 50 - 1373.3




Bis(2-chloroethyl)ether 165.1 166.9 0 98.9 45 - 1276.6

Bis(2-chloroisopropyl)ether 138.9 166.9 0 83.2 50 - 1206.6

Bis(2-ethylhexyl)phthalate 147.2 166.9 2.077 86.9 21 - 1486.6

Butyl benzyl phthalate 149.3 166.9 0.9201 88.9 50 - 1366.6

Caprolactam 142.1 166.9 6.18 81.4 50 - 1356.6

Carbazole 129.1 166.9 0 77.3 50 - 1436.6

Chrysene 124.3 166.9 0 74.4 50 - 1303.3

Dibenz(a,h)anthracene 142.4 166.9 0 85.3 50 - 1303.3

Dibenzofuran 124.8 166.9 0 74.8 50 - 1253.3

Diethyl phthalate 129.9 166.9 0 77.8 50 - 1256.6


Di-n-butyl phthalate 138.7 166.9 0.8621 82.6 50 - 1406.6

Di-n-octyl phthalate 139.6 166.9 4.432 81.0 50 - 1406.6

Fluoranthene 139.3 166.9 0 83.4 50 - 1313.3

Fluorene 128.7 166.9 0 77.1 50 - 1253.3

Hexachlorobenzene 130.1 166.9 0 77.9 50 - 1246.6

Hexachlorobutadiene 132.9 166.9 0 79.6 50 - 1256.6



Indeno(1,2,3-cd)pyrene 148 166.9 0 88.7 45 - 1393.3

Isophorone 132.2 166.9 0 79.2 45 - 1306.6

Naphthalene 116.2 166.9 0 69.6 50 - 1253.3

Nitrobenzene 136.7 166.9 0 81.9 50 - 1256.6

N-Nitrosodi-n-propylamine 159.5 166.9 0 95.5 45 - 1206.6



Phenanthrene 126 166.9 0 75.5 50 - 1253.3

Phenol 135 166.9 0 80.9 45 - 1306.6

Pyrene 131.6 166.9 0 78.9 45 - 1303.3

Pyridine 130.4 166.9 0 78.1 15 - 1206.6



Page 200 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MS




131.6 166.9 0 78.8 37 - 1250Surr: 2-Fluorophenol

129.6 166.9 0 77.6 32 - 1250Surr: 4-Terphenyl-d14


155 166.9 0 92.8 40 - 1250Surr: Phenol-d6



Page 201 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MSD


1,1´-Biphenyl 120.9 166.7 0 72.5 50 - 120 120.5 0.376 306.6

1,2,4,5-Tetrachlorobenzene 115.4 166.7 0 69.2 40 - 140 119.3 3.39 306.6



2,4,5-Trichlorophenol 129 166.7 0 77.4 45 - 127 126.8 1.69 306.6


2,4-Dichlorophenol 126.8 166.7 0 76.1 45 - 125 121 4.69 306.6

2,4-Dimethylphenol 103.8 166.7 0 62.3 45 - 120 108.1 3.99 306.6

2,4-Dinitrophenol 110.4 166.7 0 66.2 10 - 126 94.53 15.5 3013

2,4-Dinitrotoluene 130.8 166.7 0 78.5 50 - 130 125.7 4.01 306.6

2,6-Dinitrotoluene 138.1 166.7 0 82.8 50 - 125 129.3 6.55 306.6

2-Chloronaphthalene 130.3 166.7 0 78.2 50 - 145 132.7 1.81 306.6

2-Chlorophenol 121.7 166.7 0 73.0 45 - 120 117.7 3.38 306.6

2-Methylnaphthalene 124.1 166.7 0 74.4 50 - 120 121 2.54 303.3

2-Methylphenol 130.7 166.7 0 78.4 45 - 120 144.4 9.98 306.6

2-Nitroaniline 136.2 166.7 0 81.7 45 - 138 130 4.7 306.6

2-Nitrophenol 129 166.7 0 77.4 45 - 125 123.5 4.37 306.6

3&4-Methylphenol 132.5 166.7 0 79.5 45 - 120 143.5 7.99 306.6


3-Nitroaniline 126.1 166.7 0 75.6 40 - 120 127.4 1.03 306.6



4-Chloro-3-methylphenol 143.8 166.7 0 86.2 45 - 130 134.8 6.4 306.6


4-Nitroaniline 134.6 166.7 0 80.7 50 - 127 128.8 4.37 306.6

4-Nitrophenol 156 166.7 0 93.5 40 - 147 156.1 0.0824 3013

Acenaphthene 128.6 166.7 0 77.2 50 - 120 126 2.1 303.3

Acenaphthylene 124.1 166.7 0 74.4 50 - 120 120.8 2.66 303.3

Acetophenone 125 166.7 0 75.0 50 - 120 121 3.25 306.6

Aniline 111.2 166.7 0 66.7 10 - 135 121.9 9.25 306.6

Anthracene 136.4 166.7 0 81.8 50 - 123 132 3.26 303.3

Benz(a)anthracene 134 166.7 0 80.4 50 - 131 133.9 0.0534 303.3

Benzaldehyde 43.48 166.7 2.282 24.7 22 - 129 51.54 17 306.6

Benzo(a)pyrene 139.2 166.7 0 83.5 50 - 130 135 3.12 303.3



Page 202 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MSD


Benzo(b)fluoranthene 144.9 166.7 0 86.9 50 - 137 153.1 5.5 303.3

Benzo(g,h,i)perylene 139 166.7 0 83.4 50 - 130 138.4 0.42 303.3

Benzo(k)fluoranthene 135 166.7 0 81.0 50 - 143 119.8 11.9 303.3


Bis(2-chloroethyl)ether 150.2 166.7 0 90.1 45 - 127 165.1 9.43 306.6

Bis(2-chloroisopropyl)ether 124.6 166.7 0 74.7 50 - 120 138.9 10.9 306.6

Bis(2-ethylhexyl)phthalate 145.9 166.7 2.077 86.3 21 - 148 147.2 0.858 306.6

Butyl benzyl phthalate 149.6 166.7 0.9201 89.2 50 - 136 149.3 0.216 306.6

Caprolactam 143.2 166.7 6.18 82.2 50 - 135 142.1 0.772 306.6

Carbazole 136.6 166.7 0 81.9 50 - 143 129.1 5.6 306.6

Chrysene 121.6 166.7 0 73.0 50 - 130 124.3 2.13 303.3

Dibenz(a,h)anthracene 146.6 166.7 0 87.9 50 - 130 142.4 2.95 303.3

Dibenzofuran 124.7 166.7 0 74.8 50 - 125 124.8 0.0785 303.3

Diethyl phthalate 131.8 166.7 0 79.0 50 - 125 129.9 1.44 306.6


Di-n-butyl phthalate 146.4 166.7 0.8621 87.3 50 - 140 138.7 5.34 306.6

Di-n-octyl phthalate 146.1 166.7 4.432 85.0 50 - 140 139.6 4.53 306.6

Fluoranthene 146.6 166.7 0 87.9 50 - 131 139.3 5.11 303.3

Fluorene 128.5 166.7 0 77.1 50 - 125 128.7 0.212 303.3

Hexachlorobenzene 136.8 166.7 0 82.1 50 - 124 130.1 5.05 306.6


Hexachlorocyclopentadiene 136.2 166.7 0 81.7 45 - 135 128.3 6.02 306.6


Indeno(1,2,3-cd)pyrene 173.1 166.7 0 104 45 - 139 148 15.6 303.3

Isophorone 137.6 166.7 0 82.6 45 - 130 132.2 4.04 306.6

Naphthalene 118.6 166.7 0 71.2 50 - 125 116.2 2.06 303.3

Nitrobenzene 140.7 166.7 0 84.4 50 - 125 136.7 2.91 306.6

N-Nitrosodi-n-propylamine 151.3 166.7 0 90.7 45 - 120 159.5 5.27 306.6


Pentachlorophenol 116.5 166.7 0 69.9 23 - 136 114.9 1.38 306.6

Phenanthrene 130.9 166.7 0 78.5 50 - 125 126 3.84 303.3

Phenol 129.3 166.7 0 77.6 45 - 130 135 4.28 306.6

Pyrene 126.2 166.7 0 75.7 45 - 130 131.6 4.2 303.3

Pyridine 119 166.7 0 71.4 15 - 120 130.4 9.14 306.6



Page 203 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MSD




126.3 166.7 0 75.7 37 - 125 131.6 4.13 300Surr: 2-Fluorophenol

125.2 166.7 0 75.1 32 - 125 129.6 3.42 300Surr: 4-Terphenyl-d14


138.3 166.7 0 83.0 40 - 125 155 11.4 300Surr: Phenol-d6

The following samples were anayzed in this batch: HS15091078-01 HS15091078-02 HS15091078-03 HS15091078-07



Page 204 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MBLK

Client ID:

















2-Nitrophenol U 6.6









4-Nitrophenol U 13

Acenaphthene U 3.3


Acetophenone U 6.6

Aniline U 6.6

Anthracene U 3.3


Benzaldehyde U 6.6




Page 205 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MBLK

Client ID:









Caprolactam U 6.6

Carbazole U 6.6

Chrysene U 3.3


Dibenzofuran U 3.3





Fluoranthene U 3.3

Fluorene U 3.3






Isophorone U 6.6

Naphthalene U 3.3

Nitrobenzene U 6.6




Phenanthrene U 3.3

Phenol U 6.6

Pyrene U 3.3

Pyridine U 6.6



Page 206 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MBLK

Client ID:




130.6 167 0 78.2 32 - 1250Surr: 4-Terphenyl-d14


134.4 167 0 80.5 40 - 1250Surr: Phenol-d6



Page 207 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


LCS

Client ID:

1,1´-Biphenyl 119.9 167 0 71.8 50 - 1206.6



2,3,4,6-Tetrachlorophenol 143 167 0 85.7 40 - 1406.6



2,4-Dichlorophenol 130.2 167 0 78.0 45 - 1256.6

2,4-Dimethylphenol 117.4 167 0 70.3 45 - 1206.6

2,4-Dinitrophenol 162.8 167 0 97.5 10 - 12613

2,4-Dinitrotoluene 136.2 167 0 81.5 50 - 1306.6

2,6-Dinitrotoluene 134 167 0 80.2 50 - 1256.6


2-Chlorophenol 118.8 167 0 71.1 45 - 1206.6


2-Methylphenol 128.5 167 0 77.0 45 - 1206.6

2-Nitroaniline 148.1 167 0 88.7 45 - 1386.6

2-Nitrophenol 141.8 167 0 84.9 45 - 1256.6

3&4-Methylphenol 125.2 167 0 75.0 45 - 1206.6


3-Nitroaniline 128.7 167 0 77.1 40 - 1206.6





4-Nitroaniline 126.5 167 0 75.7 50 - 1276.6

4-Nitrophenol 154.8 167 0 92.7 40 - 14713

Acenaphthene 119.8 167 0 71.8 50 - 1203.3

Acenaphthylene 123.4 167 0 73.9 50 - 1203.3

Acetophenone 124.3 167 0 74.4 50 - 1206.6

Aniline 128.5 167 0 77.0 10 - 1356.6

Anthracene 136.9 167 0 82.0 50 - 1233.3


Benzaldehyde 37.17 167 0 22.3 22 - 1296.6

Benzo(a)pyrene 132.6 167 0 79.4 50 - 1303.3



Page 208 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


LCS

Client ID:









Caprolactam 146.2 167 0 87.6 50 - 1356.6

Carbazole 135.9 167 0 81.4 50 - 1436.6

Chrysene 118.9 167 0 71.2 50 - 1303.3


Dibenzofuran 125.8 167 0 75.3 50 - 1253.3



Di-n-butyl phthalate 143.8 167 0 86.1 50 - 1406.6


Fluoranthene 144.2 167 0 86.4 50 - 1313.3

Fluorene 130.4 167 0 78.1 50 - 1253.3





Indeno(1,2,3-cd)pyrene 180.3 167 0 108 45 - 1393.3

Isophorone 137.2 167 0 82.1 45 - 1306.6

Naphthalene 118.4 167 0 70.9 50 - 1253.3

Nitrobenzene 139.3 167 0 83.4 50 - 1256.6




Phenanthrene 131.8 167 0 78.9 50 - 1253.3

Phenol 127.8 167 0 76.6 45 - 1306.6

Pyrene 126.8 167 0 75.9 45 - 1303.3

Pyridine 127.4 167 0 76.3 15 - 1206.6



Page 209 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


LCS

Client ID:




125.2 167 0 75.0 32 - 1250Surr: 4-Terphenyl-d14


130.4 167 0 78.1 40 - 1250Surr: Phenol-d6



Page 210 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MS


1,1´-Biphenyl 137 166.6 0 82.2 50 - 1206.6



2,3,4,6-Tetrachlorophenol 170.3 166.6 0 102 40 - 1406.6

2,4,5-Trichlorophenol 148 166.6 0 88.8 45 - 1276.6


2,4-Dichlorophenol 150.6 166.6 0 90.4 45 - 1256.6

2,4-Dimethylphenol 133.2 166.6 0 80.0 45 - 1206.6

2,4-Dinitrophenol 150.3 166.6 0 90.2 10 - 12613

2,4-Dinitrotoluene 153.3 166.6 0 92.0 50 - 1306.6

2,6-Dinitrotoluene 149.5 166.6 0 89.7 50 - 1256.6

2-Chloronaphthalene 150.6 166.6 0 90.4 50 - 1456.6

2-Chlorophenol 131.8 166.6 0 79.1 45 - 1206.6


2-Methylphenol 154.2 166.6 0 92.5 45 - 1206.6

2-Nitroaniline 167.7 166.6 0 101 45 - 1386.6

2-Nitrophenol 162.2 166.6 0 97.4 45 - 1256.6

3&4-Methylphenol 150.6 166.6 0 90.4 45 - 1206.6


3-Nitroaniline 146.9 166.6 0 88.1 40 - 1206.6



4-Chloro-3-methylphenol 165 166.6 0 99.0 45 - 1306.6


4-Nitroaniline 152 166.6 0 91.2 50 - 1276.6

4-Nitrophenol 182.9 166.6 0 110 40 - 14713

Acenaphthene 138.5 166.6 0 83.1 50 - 1203.3

Acenaphthylene 140.6 166.6 0 84.4 50 - 1203.3

Acetophenone 146 166.6 0 87.6 50 - 1206.6

Aniline 126.9 166.6 0 76.2 10 - 1356.6

Anthracene 157.9 166.6 0 94.8 50 - 1233.3


Benzaldehyde 52.52 166.6 4.498 28.8 22 - 1296.6

Benzo(a)pyrene 155.6 166.6 0 93.4 50 - 1303.3



Page 211 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MS


Benzo(b)fluoranthene 180.9 166.6 0 109 50 - 1373.3




Bis(2-chloroethyl)ether 180 166.6 0 108 45 - 1276.6

Bis(2-chloroisopropyl)ether 149.8 166.6 0 89.9 50 - 1206.6

Bis(2-ethylhexyl)phthalate 178.6 166.6 5.59 104 21 - 1486.6

Butyl benzyl phthalate 184.9 166.6 3.077 109 50 - 1366.6

Caprolactam 187 166.6 20.79 99.7 50 - 1356.6

Carbazole 159.9 166.6 0 96.0 50 - 1436.6

Chrysene 148.2 166.6 0 88.9 50 - 1303.3

Dibenz(a,h)anthracene 171.8 166.6 0 103 50 - 1303.3

Dibenzofuran 144.5 166.6 0 86.7 50 - 1253.3

Diethyl phthalate 153.1 166.6 0.7965 91.4 50 - 1256.6


Di-n-butyl phthalate 166.5 166.6 2.004 98.8 50 - 1406.6

Di-n-octyl phthalate 168.7 166.6 0 101 50 - 1406.6

Fluoranthene 163.6 166.6 0 98.2 50 - 1313.3

Fluorene 149.6 166.6 0 89.8 50 - 1253.3

Hexachlorobenzene 170.5 166.6 0 102 50 - 1246.6

Hexachlorobutadiene 167.8 166.6 0 101 50 - 1256.6



Indeno(1,2,3-cd)pyrene 207.5 166.6 0 125 45 - 1393.3

Isophorone 159.2 166.6 0 95.6 45 - 1306.6

Naphthalene 137.3 166.6 0 82.4 50 - 1253.3

Nitrobenzene 162.7 166.6 0 97.7 50 - 1256.6

N-Nitrosodi-n-propylamine 163.8 166.6 0 98.3 45 - 1206.6



Phenanthrene 151.6 166.6 0 91.0 50 - 1253.3

Phenol 136.7 166.6 0.8876 81.5 45 - 1306.6

Pyrene 151.9 166.6 0 91.2 45 - 1303.3

Pyridine 128.6 166.6 0 77.2 15 - 1206.6



Page 212 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MS


204.8 166.6 0 123 36 - 1260Surr: 2,4,6-Tribromophenol



154.2 166.6 0 92.5 32 - 1250Surr: 4-Terphenyl-d14


156.7 166.6 0 94.0 40 - 1250Surr: Phenol-d6



Page 213 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MSD


1,1´-Biphenyl 134.8 166.8 0 80.8 50 - 120 137 1.65 306.6

1,2,4,5-Tetrachlorobenzene 134 166.8 0 80.4 40 - 140 135.8 1.35 306.6



2,4,5-Trichlorophenol 152.8 166.8 0 91.6 45 - 127 148 3.2 306.6

2,4,6-Trichlorophenol 155.6 166.8 0 93.3 45 - 130 160.3 3 306.6

2,4-Dichlorophenol 147.9 166.8 0 88.7 45 - 125 150.6 1.78 306.6

2,4-Dimethylphenol 131.5 166.8 0 78.9 45 - 120 133.2 1.29 306.6

2,4-Dinitrophenol 150.8 166.8 0 90.4 10 - 126 150.3 0.308 3013

2,4-Dinitrotoluene 155.5 166.8 0 93.2 50 - 130 153.3 1.4 306.6

2,6-Dinitrotoluene 152.3 166.8 0 91.3 50 - 125 149.5 1.86 306.6

2-Chloronaphthalene 149.8 166.8 0 89.8 50 - 145 150.6 0.482 306.6

2-Chlorophenol 137.5 166.8 0 82.5 45 - 120 131.8 4.22 306.6


2-Methylphenol 145 166.8 0 86.9 45 - 120 154.2 6.14 306.6

2-Nitroaniline 165.3 166.8 0 99.1 45 - 138 167.7 1.45 306.6

2-Nitrophenol 159.4 166.8 0 95.6 45 - 125 162.2 1.76 306.6

3&4-Methylphenol 141.1 166.8 0 84.6 45 - 120 150.6 6.47 306.6


3-Nitroaniline 149.8 166.8 0 89.8 40 - 120 146.9 1.95 306.6



4-Chloro-3-methylphenol 159.8 166.8 0 95.8 45 - 130 165 3.22 306.6


4-Nitroaniline 150.7 166.8 0 90.3 50 - 127 152 0.863 306.6

4-Nitrophenol 187.1 166.8 0 112 40 - 147 182.9 2.27 3013

Acenaphthene 139.9 166.8 0 83.9 50 - 120 138.5 0.992 303.3

Acenaphthylene 139.4 166.8 0 83.6 50 - 120 140.6 0.895 303.3

Acetophenone 143.3 166.8 0 85.9 50 - 120 146 1.82 306.6

Aniline 124.4 166.8 0 74.6 10 - 135 126.9 2.01 306.6

Anthracene 157.2 166.8 0 94.3 50 - 123 157.9 0.403 303.3

Benz(a)anthracene 155.8 166.8 0 93.4 50 - 131 158.9 1.99 303.3

Benzaldehyde 47.24 166.8 4.498 25.6 22 - 129 52.52 10.6 306.6

Benzo(a)pyrene 157.5 166.8 0 94.4 50 - 130 155.6 1.19 303.3



Page 214 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MSD


Benzo(b)fluoranthene 170.1 166.8 0 102 50 - 137 180.9 6.13 303.3

Benzo(g,h,i)perylene 165.3 166.8 0 99.1 50 - 130 160.9 2.72 303.3

Benzo(k)fluoranthene 134.9 166.8 0 80.9 50 - 143 133.1 1.33 303.3


Bis(2-chloroethyl)ether 161.4 166.8 0 96.8 45 - 127 180 10.9 306.6

Bis(2-chloroisopropyl)ether 134 166.8 0 80.4 50 - 120 149.8 11.1 306.6

Bis(2-ethylhexyl)phthalate 178.8 166.8 5.59 104 21 - 148 178.6 0.119 306.6

Butyl benzyl phthalate 180.8 166.8 3.077 107 50 - 136 184.9 2.27 306.6

Caprolactam 188.5 166.8 20.79 101 50 - 135 187 0.835 306.6

Carbazole 163 166.8 0 97.7 50 - 143 159.9 1.91 306.6

Chrysene 145 166.8 0 87.0 50 - 130 148.2 2.13 303.3

Dibenz(a,h)anthracene 174 166.8 0 104 50 - 130 171.8 1.28 303.3

Dibenzofuran 141 166.8 0 84.5 50 - 125 144.5 2.46 303.3

Diethyl phthalate 150 166.8 0.7965 89.5 50 - 125 153.1 2.03 306.6


Di-n-butyl phthalate 163.6 166.8 2.004 96.9 50 - 140 166.5 1.8 306.6

Di-n-octyl phthalate 171.3 166.8 0 103 50 - 140 168.7 1.52 306.6

Fluoranthene 163.2 166.8 0 97.8 50 - 131 163.6 0.24 303.3

Fluorene 149.5 166.8 0 89.6 50 - 125 149.6 0.0745 303.3

Hexachlorobenzene 167.1 166.8 0 100 50 - 124 170.5 1.96 306.6


Hexachlorocyclopentadiene 155.2 166.8 0 93.1 45 - 135 159.4 2.66 306.6


Indeno(1,2,3-cd)pyrene 210.2 166.8 0 126 45 - 139 207.5 1.31 303.3

Isophorone 154.3 166.8 0 92.5 45 - 130 159.2 3.16 306.6

Naphthalene 134.9 166.8 0 80.9 50 - 125 137.3 1.82 303.3

Nitrobenzene 159.3 166.8 0 95.5 50 - 125 162.7 2.13 306.6

N-Nitrosodi-n-propylamine 162.4 166.8 0 97.4 45 - 120 163.8 0.889 306.6


Pentachlorophenol 140.4 166.8 0 84.2 23 - 136 140.5 0.0727 306.6

Phenanthrene 151.2 166.8 0 90.7 50 - 125 151.6 0.26 303.3

Phenol 132 166.8 0.8876 78.6 45 - 130 136.7 3.46 306.6

Pyrene 150.5 166.8 0 90.3 45 - 130 151.9 0.879 303.3

Pyridine 114.2 166.8 0 68.5 15 - 120 128.6 11.9 306.6



Page 215 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MSD


209.6 166.8 0 126 36 - 126 204.8 2.3 300Surr: 2,4,6-Tribromophenol



155.3 166.8 0 93.1 32 - 125 154.2 0.734 300Surr: 4-Terphenyl-d14


149.5 166.8 0 89.7 40 - 125 156.7 4.67 300Surr: Phenol-d6

The following samples were anayzed in this batch: HS15091078-04 HS15091078-05 HS15091078-06 HS15091078-08 HS15091078-09 HS15091078-10 HS15091078-11 HS15091078-12 HS15091078-13 HS15091078-14 HS15091078-15 HS15091078-16 HS15091078-17 HS15091078-18 HS15091078-19 HS15091078-20



Page 216 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MBLK

Client ID:


















2-Butanone U 2.0

2-Hexanone U 2.0


4-Methyl-2-pentanone U 2.0

Acetone U 2.0

Benzene U 1.0


Bromoform U 1.0

Bromomethane U 1.0

Carbon disulfide U 2.0


Chlorobenzene U 1.0

Chloroethane U 1.0

Chloroform U 1.0

Chloromethane U 1.0





Page 217 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MBLK

Client ID:

Cyclohexane U 1.0



Ethylbenzene U 1.0




Methylene chloride U 2.0

Naphthalene U 1.0




Styrene U 1.0



Toluene U 1.0






Xylenes, Total U 3.0




53.43 50 0 107 75 - 1251.0Surr: Toluene-d8



Page 218 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


LCS

Client ID:



1,1,2,2-Tetrachloroethane 44 50 0 88.0 74 - 1231.0



1,1-Dichloroethane 55.46 50 0 111 76 - 1201.0

1,1-Dichloroethene 53.8 50 0 108 75 - 1301.0

1,2,3-Trichlorobenzene 46.26 50 0 92.5 70 - 1311.0



1,2-Dibromoethane 50.33 50 0 101 80 - 1211.0


1,2-Dichloroethane 57.39 50 0 115 76 - 1201.0





2-Butanone 106.5 100 0 107 60 - 1402.0

2-Hexanone 102.7 100 0 103 60 - 1312.0



Acetone 109.8 100 0 110 60 - 1402.0

Benzene 52.55 50 0 105 80 - 1201.0


Bromoform 52.32 50 0 105 70 - 1301.0

Bromomethane 61.46 50 0 123 60 - 1401.0



Chlorobenzene 48.58 50 0 97.2 80 - 1201.0

Chloroethane 53.06 50 0 106 70 - 1301.0

Chloroform 57.75 50 0 116 70 - 1301.0

Chloromethane 52.51 50 0 105 65 - 1301.0





Page 219 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


LCS

Client ID:

Cyclohexane 54.97 50 0 110 70 - 1301.0



Ethylbenzene 48.52 50 0 97.0 80 - 1201.0




Methylene chloride 54.66 50 0 109 65 - 1332.0

Naphthalene 45.92 50 0 91.8 65 - 1351.0

n-Butylbenzene 51.64 50 0 103 75 - 1281.0

n-Propylbenzene 48.78 50 0 97.6 75 - 1301.0


Styrene 51.64 50 0 103 78 - 1221.0



Toluene 48.2 50 0 96.4 75 - 1211.0





Vinyl chloride 52.48 50 0 105 70 - 1351.0

Xylenes, Total 144.4 150 0 96.3 79 - 1243.0




50.71 50 0 101 75 - 1251.0Surr: Toluene-d8



Page 220 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MS

Client ID:

1,1,1,2-Tetrachloroethane 528.8 500 0 106 80 - 12010

1,1,1-Trichloroethane 612.5 500 0 122 75 - 13010

1,1,2,2-Tetrachloroethane 448.1 500 0 89.6 74 - 12310

1,1,2-Trichlor-1,2,2-trifluoroethane 1653 500 1060 119 70 - 13010

1,1,2-Trichloroethane 477.2 500 0 95.4 80 - 12010

1,1-Dichloroethane 571 500 0 114 76 - 12010

1,1-Dichloroethene 564.4 500 15.72 110 75 - 13010

1,2,3-Trichlorobenzene 454.7 500 41.02 82.7 70 - 13110

1,2,4-Trichlorobenzene 470.2 500 26.66 88.7 75 - 12610

1,2,4-Trimethylbenzene 507.8 500 3.985 101 70 - 12510

1,2-Dibromoethane 511.2 500 0 102 80 - 12110

1,2-Dichlorobenzene 483.4 500 7.996 95.1 80 - 12010

1,2-Dichloroethane 557.1 500 0 111 76 - 12010

1,2-Dichloropropane 531.6 500 0 106 80 - 12010

1,3,5-Trimethylbenzene 504.4 500 0 101 80 - 12310

1,3-Dichlorobenzene 472.7 500 5.135 93.5 80 - 12010

1,4-Dichlorobenzene 510.2 500 0 102 80 - 12010

2-Butanone 1083 1000 0 108 60 - 14020

2-Hexanone 1070 1000 0 107 60 - 13120

4-Isopropyltoluene 514.1 500 5.584 102 79 - 12710

4-Methyl-2-pentanone 981.4 1000 0 98.1 60 - 13520

Acetone 1104 1000 0 110 60 - 14020

Benzene 530.4 500 0 106 80 - 12010

Bromodichloromethane 550.2 500 0 110 75 - 12510

Bromoform 518.8 500 0 104 70 - 13010

Bromomethane 577.2 500 0 115 60 - 14010

Carbon disulfide 1131 1000 0 113 70 - 13020

Carbon tetrachloride 553.4 500 0 111 79 - 12010

Chlorobenzene 497 500 0 99.4 80 - 12010

Chloroethane 542.9 500 0 109 70 - 13010

Chloroform 579.1 500 0 116 70 - 13010

Chloromethane 541.1 500 0 108 65 - 13010

cis-1,2-Dichloroethene 541.4 500 0 108 75 - 12510

cis-1,3-Dichloropropene 609.3 500 0 122 79 - 12510



Page 221 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MS

Client ID:

Cyclohexane 578.6 500 11.59 113 70 - 13010

Dibromochloromethane 526.5 500 0 105 70 - 13010

Dichlorodifluoromethane 431.5 500 28.25 80.7 60 - 14010

Ethylbenzene 501.5 500 0 100 80 - 12010

Isopropylbenzene 509.2 500 0 102 75 - 13010

Methyl tert-butyl ether 539.6 500 0 108 70 - 13010

Methylcyclohexane 521.8 500 0 104 70 - 12610

Methylene chloride 536.6 500 0 107 65 - 13320

Naphthalene 448.3 500 34.95 82.7 65 - 13510

n-Butylbenzene 541.7 500 0 108 75 - 12810

n-Propylbenzene 497 500 0 99.4 75 - 13010

sec-Butylbenzene 506.2 500 5.135 100 70 - 12510

Styrene 526.7 500 0 105 78 - 12210

tert-Butylbenzene 490.3 500 5.268 97.0 70 - 13010

Tetrachloroethene 496.8 500 12.12 96.9 75 - 13010

Toluene 496.6 500 0 99.3 75 - 12110

trans-1,2-Dichloroethene 565.7 500 0 113 75 - 12510

trans-1,3-Dichloropropene 504.6 500 0 101 76 - 12510

Trichloroethene 517.2 500 12.91 101 71 - 12510

Trichlorofluoromethane 630.1 500 24.72 121 67 - 13210

Vinyl chloride 545.9 500 0 109 70 - 13510

Xylenes, Total 1495 1500 0 99.6 80 - 12430

557 500 0 111 71 - 12510Surr: 1,2-Dichloroethane-d4


551.5 500 0 110 74 - 12510Surr: Dibromofluoromethane

497.2 500 0 99.4 75 - 12510Surr: Toluene-d8



Page 222 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MSD

Client ID:

1,1,1,2-Tetrachloroethane 524.1 500 0 105 80 - 120 528.8 0.886 2010

1,1,1-Trichloroethane 580.3 500 0 116 75 - 130 612.5 5.39 2010

1,1,2,2-Tetrachloroethane 467.7 500 0 93.5 74 - 123 448.1 4.29 2010

1,1,2-Trichlor-1,2,2-trifluoroethane 1553 500 1060 98.7 70 - 130 1653 6.21 2010

1,1,2-Trichloroethane 486.2 500 0 97.2 80 - 120 477.2 1.88 2010

1,1-Dichloroethane 538.3 500 0 108 76 - 120 571 5.89 2010

1,1-Dichloroethene 541.4 500 15.72 105 75 - 130 564.4 4.16 2010

1,2,3-Trichlorobenzene 511.1 500 41.02 94.0 70 - 131 454.7 11.7 2010

1,2,4-Trichlorobenzene 508.5 500 26.66 96.4 75 - 126 470.2 7.81 2010

1,2,4-Trimethylbenzene 499.2 500 3.985 99.0 70 - 125 507.8 1.7 2010

1,2-Dibromoethane 497 500 0 99.4 80 - 121 511.2 2.82 2010

1,2-Dichlorobenzene 489.2 500 7.996 96.2 80 - 120 483.4 1.18 2010

1,2-Dichloroethane 557.5 500 0 112 76 - 120 557.1 0.0792 2010

1,2-Dichloropropane 533.8 500 0 107 80 - 120 531.6 0.426 2010

1,3,5-Trimethylbenzene 499.6 500 0 99.9 80 - 123 504.4 0.956 2010

1,3-Dichlorobenzene 497.8 500 5.135 98.5 80 - 120 472.7 5.18 2010

1,4-Dichlorobenzene 522.8 500 0 105 80 - 120 510.2 2.45 2010

2-Butanone 1092 1000 0 109 60 - 140 1083 0.893 2020

2-Hexanone 1089 1000 0 109 60 - 131 1070 1.73 2020

4-Isopropyltoluene 512.8 500 5.584 101 79 - 127 514.1 0.258 2010

4-Methyl-2-pentanone 1024 1000 0 102 60 - 135 981.4 4.26 2020

Acetone 1104 1000 0 110 60 - 140 1104 0.0285 2020

Benzene 512.3 500 0 102 80 - 120 530.4 3.47 2010

Bromodichloromethane 529.7 500 0 106 75 - 125 550.2 3.79 2010

Bromoform 540 500 0 108 70 - 130 518.8 4.01 2010

Bromomethane 576.5 500 0 115 60 - 140 577.2 0.133 2010

Carbon disulfide 1067 1000 0 107 70 - 130 1131 5.81 2020

Carbon tetrachloride 545.8 500 0 109 75 - 125 553.4 1.39 2010

Chlorobenzene 486.4 500 0 97.3 80 - 120 497 2.15 2010

Chloroethane 516.1 500 0 103 70 - 130 542.9 5.07 2010

Chloroform 534.5 500 0 107 70 - 130 579.1 8.02 2010

Chloromethane 521.5 500 0 104 65 - 130 541.1 3.69 2010

cis-1,2-Dichloroethene 523.8 500 0 105 75 - 125 541.4 3.32 2010

cis-1,3-Dichloropropene 606.1 500 0 121 79 - 125 609.3 0.512 2010



Page 223 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MSD

Client ID:

Cyclohexane 553.9 500 11.59 108 70 - 130 578.6 4.36 2010

Dibromochloromethane 522.8 500 0 105 70 - 130 526.5 0.713 2010

Dichlorodifluoromethane 389.1 500 28.25 72.2 60 - 140 431.5 10.3 2010

Ethylbenzene 489.2 500 0 97.8 80 - 120 501.5 2.48 2010

Isopropylbenzene 505 500 0 101 75 - 130 509.2 0.839 2010

Methyl tert-butyl ether 533.7 500 0 107 70 - 130 539.6 1.1 2010

Methylcyclohexane 505.1 500 0 101 70 - 126 521.8 3.24 2010

Methylene chloride 513.3 500 0 103 65 - 133 536.6 4.43 2020

Naphthalene 501.7 500 34.95 93.3 65 - 135 448.3 11.2 2010

n-Butylbenzene 547.5 500 0 109 75 - 128 541.7 1.06 2010

n-Propylbenzene 508.4 500 0 102 75 - 130 497 2.28 2010

sec-Butylbenzene 518.8 500 5.135 103 70 - 125 506.2 2.45 2010

Styrene 505.7 500 0 101 78 - 122 526.7 4.08 2010

tert-Butylbenzene 507.3 500 5.268 100 70 - 130 490.3 3.41 2010

Tetrachloroethene 491.7 500 12.12 95.9 75 - 130 496.8 1.02 2010

Toluene 482.7 500 0 96.5 75 - 121 496.6 2.84 2010

trans-1,2-Dichloroethene 510.9 500 0 102 75 - 125 565.7 10.2 2010

trans-1,3-Dichloropropene 512.9 500 0 103 76 - 125 504.6 1.64 2010

Trichloroethene 508.4 500 12.91 99.1 71 - 125 517.2 1.7 2010

Trichlorofluoromethane 600.2 500 24.72 115 67 - 132 630.1 4.86 2010

Vinyl chloride 518.9 500 0 104 70 - 135 545.9 5.07 2010

Xylenes, Total 1450 1500 0 96.7 80 - 124 1495 3.04 2030

541.2 500 0 108 71 - 125 557 2.88 2010Surr: 1,2-Dichloroethane-d4

475.5 500 0 95.1 70 - 125 490.2 3.04 2010Surr: 4-Bromofluorobenzene

523.9 500 0 105 74 - 125 551.5 5.14 2010Surr: Dibromofluoromethane

493.3 500 0 98.7 75 - 125 497.2 0.785 2010Surr: Toluene-d8




Page 224 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MBLK

Client ID:


















2-Butanone U 10

2-Hexanone U 10



Acetone U 20

Benzene U 5.0


Bromoform U 5.0

Bromomethane U 10



Chlorobenzene U 5.0

Chloroethane U 10

Chloroform U 5.0

Chloromethane U 10





Page 225 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MBLK

Client ID:

Cyclohexane U 5.0



Ethylbenzene U 5.0





Naphthalene U 5.0




Styrene U 5.0



Toluene U 5.0






Xylenes, Total U 10




51.84 50 0 104 73 - 1270Surr: Toluene-d8



Page 226 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


LCS

Client ID:






1,1-Dichloroethane 53.16 50 0 106 75 - 1245.0

1,1-Dichloroethene 55.2 50 0 110 76 - 1285.0




1,2-Dibromoethane 52.46 50 0 105 70 - 1205.0


1,2-Dichloroethane 51.3 50 0 103 73 - 1215.0





2-Butanone 108.2 100 0 108 65 - 13010

2-Hexanone 115.1 100 0 115 65 - 13310



Acetone 112.2 100 0 112 53 - 14220

Benzene 53.45 50 0 107 79 - 1225.0


Bromoform 52.23 50 0 104 74 - 1255.0

Bromomethane 63.74 50 0 127 68 - 13110



Chlorobenzene 52.11 50 0 104 79 - 1205.0

Chloroethane 50.71 50 0 101 74 - 12610

Chloroform 49.16 50 0 98.3 78 - 1225.0

Chloromethane 50.14 50 0 100 69 - 12910





Page 227 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


LCS

Client ID:

Cyclohexane 52.97 50 0 106 74 - 1265.0



Ethylbenzene 54.54 50 0 109 80 - 1225.0





Naphthalene 53.66 50 0 107 71 - 1285.0

n-Butylbenzene 51.65 50 0 103 77 - 1265.0

n-Propylbenzene 50.84 50 0 102 79 - 1235.0


Styrene 54.39 50 0 109 78 - 1245.0



Toluene 53.34 50 0 107 79 - 1205.0





Vinyl chloride 52.83 50 0 106 76 - 1262.0

Xylenes, Total 163.9 150 0 109 80 - 12010




50.8 50 0 102 73 - 1270Surr: Toluene-d8



Page 228 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MS

Client ID:




1,1,2-Trichlor-1,2,2-trifluoroethane 49.37 48.5 0 102 76 - 1274.8


1,1-Dichloroethane 49.43 48.5 0 102 75 - 1244.8

1,1-Dichloroethene 52.62 48.5 0 108 76 - 1284.8




1,2-Dibromoethane 50.44 48.5 0 104 70 - 1204.8


1,2-Dichloroethane 47.96 48.5 0 98.9 73 - 1214.8

1,2-Dichloropropane 49.71 48.5 0 102 75 - 1244.8




2-Butanone 110.8 97 0 114 65 - 1309.7

2-Hexanone 119.2 97 0 123 65 - 1339.7

4-Isopropyltoluene 46.29 48.5 0 95.4 80 - 1254.8


Acetone 110.7 97 0 114 53 - 14219

Benzene 51.26 48.5 0 106 79 - 1224.8

Bromodichloromethane 48.49 48.5 0 100.0 79 - 1214.8

Bromoform 51.53 48.5 0 106 74 - 1254.8

Bromomethane 59.94 48.5 0 124 68 - 1319.7


Carbon tetrachloride 49.3 48.5 0 102 74 - 1264.8

Chlorobenzene 49.43 48.5 0 102 79 - 1204.8

Chloroethane 49 48.5 0 101 74 - 1269.7

Chloroform 45.2 48.5 0 93.2 78 - 1224.8

Chloromethane 49.28 48.5 0 102 69 - 1299.7


cis-1,3-Dichloropropene 49.86 48.5 0 103 77 - 1234.8



Page 229 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MS

Client ID:

Cyclohexane 51.15 48.5 0 105 74 - 1264.8

Dibromochloromethane 50.11 48.5 0 103 78 - 1224.8

Dichlorodifluoromethane 49.93 48.5 0 103 57 - 1404.8

Ethylbenzene 51.57 48.5 0 106 80 - 1224.8

Isopropylbenzene 53.88 48.5 0 111 72 - 1274.8

Methyl tert-butyl ether 48.67 48.5 0 100 76 - 1244.8

Methylcyclohexane 51.88 48.5 0 107 77 - 1274.8

Methylene chloride 45.13 48.5 0 93.0 65 - 1309.7

Naphthalene 47.36 48.5 0 97.6 71 - 1284.8

n-Butylbenzene 45.27 48.5 0 93.3 77 - 1264.8

n-Propylbenzene 46.32 48.5 0 95.5 79 - 1234.8

sec-Butylbenzene 46.65 48.5 0 96.2 80 - 1234.8

Styrene 50.65 48.5 0 104 78 - 1244.8

tert-Butylbenzene 49.28 48.5 0 102 79 - 1244.8

Tetrachloroethene 64.4 48.5 0 133 70 - 130 S 4.8

Toluene 51.8 48.5 0.7132 105 79 - 1204.8

trans-1,2-Dichloroethene 50.42 48.5 0 104 79 - 1224.8

trans-1,3-Dichloropropene 50.37 48.5 0 104 77 - 1204.8

Trichloroethene 53.81 48.5 0 111 75 - 1234.8

Trichlorofluoromethane 51.16 48.5 0 105 75 - 1264.8

Vinyl chloride 52.36 48.5 0 108 76 - 1261.9

Xylenes, Total 154.4 145.5 0 106 80 - 1209.7


48.97 48.5 0 101 73 - 1260Surr: 4-Bromofluorobenzene


48.32 48.5 0 99.6 73 - 1270Surr: Toluene-d8



Page 230 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MSD

Client ID:






1,1-Dichloroethane 46.45 48.5 0 95.8 75 - 124 49.43 6.21 304.8

1,1-Dichloroethene 50.97 48.5 0 105 76 - 128 52.62 3.19 304.8




1,2-Dibromoethane 49.19 48.5 0 101 70 - 120 50.44 2.51 304.8


1,2-Dichloroethane 43.63 48.5 0 90.0 73 - 121 47.96 9.46 304.8





2-Butanone 109 97 0 112 65 - 130 110.8 1.7 309.7

2-Hexanone 117.6 97 0 121 65 - 133 119.2 1.34 309.7



Acetone 114.3 97 0 118 53 - 142 110.7 3.28 3019

Benzene 48.48 48.5 0 100.0 79 - 122 51.26 5.57 304.8


Bromoform 48.31 48.5 0 99.6 74 - 125 51.53 6.44 304.8

Bromomethane 57.24 48.5 0 118 68 - 131 59.94 4.61 309.7



Chlorobenzene 46.58 48.5 0 96.0 79 - 120 49.43 5.93 304.8

Chloroethane 46.12 48.5 0 95.1 74 - 126 49 6.06 309.7

Chloroform 41.9 48.5 0 86.4 78 - 122 45.2 7.59 304.8

Chloromethane 46.06 48.5 0 95.0 69 - 129 49.28 6.75 309.7





Page 231 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MSD

Client ID:

Cyclohexane 48.98 48.5 0 101 74 - 126 51.15 4.33 304.8



Ethylbenzene 49.94 48.5 0 103 80 - 122 51.57 3.21 304.8



Methylcyclohexane 49.19 48.5 0 101 77 - 127 51.88 5.31 304.8


Naphthalene 48.87 48.5 0 101 71 - 128 47.36 3.15 304.8

n-Butylbenzene 43.04 48.5 0 88.7 77 - 126 45.27 5.06 304.8

n-Propylbenzene 44.47 48.5 0 91.7 79 - 123 46.32 4.07 304.8


Styrene 47.83 48.5 0 98.6 78 - 124 50.65 5.72 304.8

tert-Butylbenzene 46.94 48.5 0 96.8 79 - 124 49.28 4.86 304.8

Tetrachloroethene 61.17 48.5 0 126 70 - 130 64.4 5.14 304.8

Toluene 49.38 48.5 0.7132 100 79 - 120 51.8 4.76 304.8


trans-1,3-Dichloropropene 47.58 48.5 0 98.1 77 - 120 50.37 5.7 304.8


Trichlorofluoromethane 49.15 48.5 0 101 75 - 126 51.16 4.01 304.8

Vinyl chloride 49.95 48.5 0 103 76 - 126 52.36 4.72 301.9

Xylenes, Total 146.8 145.5 0 101 80 - 120 154.4 5.08 309.7

46 48.5 0 94.8 70 - 128 45.61 0.848 300Surr: 1,2-Dichloroethane-d4



49.25 48.5 0 102 73 - 127 48.32 1.91 300Surr: Toluene-d8




Page 232 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MBLK

Client ID:


















2-Butanone U 10

2-Hexanone U 10



Acetone U 20

Benzene U 5.0


Bromoform U 5.0

Bromomethane U 10



Chlorobenzene U 5.0

Chloroethane U 10

Chloroform U 5.0

Chloromethane U 10





Page 233 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MBLK

Client ID:

Cyclohexane U 5.0



Ethylbenzene U 5.0





Naphthalene U 5.0




Styrene U 5.0



Toluene U 5.0






Xylenes, Total U 10




50.86 50 0 102 73 - 1270Surr: Toluene-d8



Page 234 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


LCS

Client ID:


1,1,1-Trichloroethane 52 50 0 104 79 - 1285.0


1,1,2-Trichlor-1,2,2-trifluoroethane 50 50 0 100.0 76 - 1275.0


1,1-Dichloroethane 50.8 50 0 102 75 - 1245.0

1,1-Dichloroethene 54.98 50 0 110 76 - 1285.0




1,2-Dibromoethane 52.48 50 0 105 70 - 1205.0


1,2-Dichloroethane 51 50 0 102 73 - 1215.0





2-Butanone 98.1 100 0 98.1 65 - 13010

2-Hexanone 108.3 100 0 108 65 - 13310



Acetone 110.1 100 0 110 53 - 14220

Benzene 53.05 50 0 106 79 - 1225.0


Bromoform 52.7 50 0 105 74 - 1255.0

Bromomethane 61.87 50 0 124 68 - 13110



Chlorobenzene 52.32 50 0 105 79 - 1205.0

Chloroethane 49.4 50 0 98.8 74 - 12610

Chloroform 47.88 50 0 95.8 78 - 1225.0

Chloromethane 47.58 50 0 95.2 69 - 12910





Page 235 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


LCS

Client ID:

Cyclohexane 49.26 50 0 98.5 74 - 1265.0



Ethylbenzene 54.68 50 0 109 80 - 1225.0





Naphthalene 51.77 50 0 104 71 - 1285.0

n-Butylbenzene 48.11 50 0 96.2 77 - 1265.0

n-Propylbenzene 49.11 50 0 98.2 79 - 1235.0


Styrene 54.05 50 0 108 78 - 1245.0



Toluene 53.54 50 0 107 79 - 1205.0





Vinyl chloride 51.27 50 0 103 76 - 1262.0

Xylenes, Total 162.2 150 0 108 80 - 12010




50.34 50 0 101 73 - 1270Surr: Toluene-d8



Page 236 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MS







1,1-Dichloroethane 32.4 40 0 81.0 75 - 1244.0

1,1-Dichloroethene 33.8 40 0 84.5 76 - 1284.0


1,2,4-Trichlorobenzene 31 40 0 77.5 74 - 1284.0

1,2,4-Trimethylbenzene 30.47 40 0 76.2 79 - 123 S 4.0

1,2-Dibromoethane 31.29 40 0 78.2 70 - 1204.0


1,2-Dichloroethane 31.44 40 0 78.6 73 - 1214.0





2-Butanone 55.94 80 0 69.9 65 - 1308.0

2-Hexanone 61.93 80 0 77.4 65 - 1338.0

4-Isopropyltoluene 31.15 40 0 77.9 80 - 125 S 4.0


Acetone 55.94 80 0 69.9 53 - 14216

Benzene 34.09 40 0 85.2 79 - 1224.0


Bromoform 31.78 40 0 79.4 74 - 1254.0

Bromomethane 36.45 40 0 91.1 68 - 1318.0

Carbon disulfide 67.64 80 0 84.5 78 - 1318.0


Chlorobenzene 32.41 40 0 81.0 79 - 1204.0

Chloroethane 30.52 40 0 76.3 74 - 1268.0

Chloroform 30.12 40 0 75.3 78 - 122 S 4.0

Chloromethane 30.64 40 0 76.6 69 - 1298.0





Page 237 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MS


Cyclohexane 32.69 40 0 81.7 74 - 1264.0



Ethylbenzene 34.17 40 0 85.4 80 - 1224.0





Naphthalene 29.39 40 0 73.5 71 - 1284.0

n-Butylbenzene 29.83 40 0 74.6 77 - 126 S 4.0

n-Propylbenzene 30.66 40 0 76.6 79 - 123 S 4.0

sec-Butylbenzene 31.61 40 0 79.0 80 - 123 S 4.0

Styrene 33.28 40 0 83.2 78 - 1244.0



Toluene 33.39 40 0.7195 81.7 79 - 1204.0


trans-1,3-Dichloropropene 33 40 0 82.5 77 - 1204.0


Trichlorofluoromethane 33.17 40 0 82.9 75 - 1264.0

Vinyl chloride 32.66 40 0 81.7 76 - 1261.6

Xylenes, Total 100.9 120 0 84.1 80 - 1208.0




40.24 40 0 101 73 - 1270Surr: Toluene-d8



Page 238 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MSD



1,1,1-Trichloroethane 37.72 37.5 0 101 79 - 128 33.07 13.2 303.8




1,1-Dichloroethane 35.24 37.5 0 94.0 75 - 124 32.4 8.4 303.8

1,1-Dichloroethene 38.06 37.5 0 101 76 - 128 33.8 11.8 303.8


1,2,4-Trichlorobenzene 35.05 37.5 0 93.5 74 - 128 31 12.3 303.8


1,2-Dibromoethane 34.55 37.5 0 92.1 70 - 120 31.29 9.93 303.8


1,2-Dichloroethane 34.53 37.5 0 92.1 73 - 121 31.44 9.37 303.8





2-Butanone 61.32 75 0 81.8 65 - 130 55.94 9.19 307.5

2-Hexanone 67.85 75 0 90.5 65 - 133 61.93 9.13 307.5


4-Methyl-2-pentanone 69.04 75 0 92.1 69 - 130 62.83 9.43 307.5

Acetone 61.26 75 0 81.7 53 - 142 55.94 9.08 3015

Benzene 37.69 37.5 0 100 79 - 122 34.09 10 303.8


Bromoform 34.97 37.5 0 93.3 74 - 125 31.78 9.57 303.8

Bromomethane 43.46 37.5 0 116 68 - 131 36.45 17.6 307.5



Chlorobenzene 36.35 37.5 0 96.9 79 - 120 32.41 11.5 303.8

Chloroethane 33.87 37.5 0 90.3 74 - 126 30.52 10.4 307.5

Chloroform 33.29 37.5 0 88.8 78 - 122 30.12 10 303.8

Chloromethane 33.11 37.5 0 88.3 69 - 129 30.64 7.75 307.5





Page 239 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MSD


Cyclohexane 35.9 37.5 0 95.7 74 - 126 32.69 9.38 303.8



Ethylbenzene 37.98 37.5 0 101 80 - 122 34.17 10.6 303.8



Methylcyclohexane 37.18 37.5 0 99.1 77 - 127 33.27 11.1 303.8


Naphthalene 33.89 37.5 0 90.4 71 - 128 29.39 14.2 303.8

n-Butylbenzene 33.12 37.5 0 88.3 77 - 126 29.83 10.4 303.8

n-Propylbenzene 33.53 37.5 0 89.4 79 - 123 30.66 8.97 303.8


Styrene 37.58 37.5 0 100 78 - 124 33.28 12.1 303.8

tert-Butylbenzene 39.36 37.5 0 105 79 - 124 34.96 11.8 303.8

Tetrachloroethene 34.86 37.5 0 93.0 70 - 130 30.99 11.7 303.8

Toluene 37.39 37.5 0.7195 97.8 79 - 120 33.39 11.3 303.8


trans-1,3-Dichloropropene 37.03 37.5 0 98.8 77 - 120 33 11.5 303.8


Trichlorofluoromethane 37.11 37.5 0 99.0 75 - 126 33.17 11.2 303.8

Vinyl chloride 35.28 37.5 0 94.1 76 - 126 32.66 7.69 301.5

Xylenes, Total 114.1 112.5 0 101 80 - 120 100.9 12.3 307.5

34.88 37.5 0 93.0 70 - 128 36.69 5.06 300Surr: 1,2-Dichloroethane-d4



37.75 37.5 0 101 73 - 127 40.24 6.39 300Surr: Toluene-d8

The following samples were anayzed in this batch: HS15091078-06 HS15091078-07 HS15091078-08 HS15091078-09 HS15091078-10 HS15091078-11 HS15091078-12 HS15091078-13 HS15091078-14 HS15091078-15 HS15091078-16 HS15091078-18 HS15091078-19 HS15091078-20



Page 240 of 261

Client:Project:



QC BATCH REPORT


Sample ID: VBLKS1-100215 Units: ug/Kg Analysis Date: 02-Oct-2015 13:11



Value %RECControl

LimitRPD Ref


MBLK

Client ID:


















2-Butanone U 10

2-Hexanone U 10



Acetone U 20

Benzene U 5.0


Bromoform U 5.0

Bromomethane U 10



Chlorobenzene U 5.0

Chloroethane U 10

Chloroform U 5.0

Chloromethane U 10





Page 241 of 261

Client:Project:



QC BATCH REPORT


Sample ID: VBLKS1-100215 Units: ug/Kg Analysis Date: 02-Oct-2015 13:11



Value %RECControl

LimitRPD Ref


MBLK

Client ID:

Cyclohexane U 5.0



Ethylbenzene U 5.0





Naphthalene U 5.0




Styrene U 5.0



Toluene U 5.0






Xylenes, Total U 10




50.67 50 0 101 73 - 1270Surr: Toluene-d8



Page 242 of 261

Client:Project:



QC BATCH REPORT


Sample ID: VLCSS1-100215 Units: ug/Kg Analysis Date: 02-Oct-2015 12:24



Value %RECControl

LimitRPD Ref


LCS

Client ID:






1,1-Dichloroethane 50.45 50 0 101 75 - 1245.0

1,1-Dichloroethene 47.63 50 0 95.3 76 - 1285.0




1,2-Dibromoethane 50.21 50 0 100 70 - 1205.0


1,2-Dichloroethane 50.13 50 0 100 73 - 1215.0





2-Butanone 93.62 100 0 93.6 65 - 13010

2-Hexanone 94.12 100 0 94.1 65 - 13310



Acetone 86.21 100 0 86.2 53 - 14220

Benzene 51.31 50 0 103 79 - 1225.0


Bromoform 45.14 50 0 90.3 74 - 1255.0

Bromomethane 49.65 50 0 99.3 68 - 13110

Carbon disulfide 93.99 100 0 94.0 78 - 13110


Chlorobenzene 51.24 50 0 102 79 - 1205.0

Chloroethane 50.37 50 0 101 74 - 12610

Chloroform 47.26 50 0 94.5 78 - 1225.0

Chloromethane 50.55 50 0 101 69 - 12910





Page 243 of 261

Client:Project:



QC BATCH REPORT


Sample ID: VLCSS1-100215 Units: ug/Kg Analysis Date: 02-Oct-2015 12:24



Value %RECControl

LimitRPD Ref


LCS

Client ID:

Cyclohexane 47.68 50 0 95.4 74 - 1265.0



Ethylbenzene 52.45 50 0 105 80 - 1225.0





Naphthalene 48.64 50 0 97.3 71 - 1285.0

n-Butylbenzene 47.96 50 0 95.9 77 - 1265.0

n-Propylbenzene 48.05 50 0 96.1 79 - 1235.0


Styrene 52.83 50 0 106 78 - 1245.0



Toluene 51.61 50 0 103 79 - 1205.0




Trichlorofluoromethane 53 50 0 106 75 - 1265.0

Vinyl chloride 48.49 50 0 97.0 76 - 1262.0

Xylenes, Total 159.2 150 0 106 80 - 12010




50.73 50 0 101 73 - 1270Surr: Toluene-d8



Page 244 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MS







1,1-Dichloroethane 42.1 37 0 114 75 - 1243.7

1,1-Dichloroethene 39.56 37 0 107 76 - 1283.7




1,2-Dibromoethane 40.6 37 0 110 70 - 1203.7


1,2-Dichloroethane 39.62 37 0 107 73 - 1213.7





2-Butanone 76 74 0 103 65 - 1307.4

2-Hexanone 74.66 74 0 101 65 - 1337.4



Acetone 68.34 74 0 92.3 53 - 14215

Benzene 42.7 37 0 115 79 - 1223.7


Bromoform 36.87 37 0 99.6 74 - 1253.7

Bromomethane 41.8 37 0 113 68 - 1317.4



Chlorobenzene 41.31 37 0 112 79 - 1203.7

Chloroethane 42.57 37 0 115 74 - 1267.4

Chloroform 38.91 37 0 105 78 - 1223.7

Chloromethane 41.17 37 0 111 69 - 1297.4





Page 245 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MS


Cyclohexane 39 37 0 105 74 - 1263.7


Dichlorodifluoromethane 39.46 37 0 107 57 - 1403.7

Ethylbenzene 42.67 37 0 115 80 - 1223.7




Methylene chloride 39.99 37 0 108 65 - 1307.4

Naphthalene 35.14 37 1.815 90.1 71 - 1283.7

n-Butylbenzene 37.29 37 0 101 77 - 1263.7

n-Propylbenzene 37.83 37 0 102 79 - 1233.7


Styrene 41.97 37 0 113 78 - 1243.7



Toluene 42.79 37 0 116 79 - 1203.7





Vinyl chloride 40.09 37 0 108 76 - 1261.5

Xylenes, Total 127.7 111 0 115 80 - 1207.4


38 37 0 103 73 - 1260Surr: 4-Bromofluorobenzene

37.11 37 0 100 71 - 1280Surr: Dibromofluoromethane

37.85 37 0 102 73 - 1270Surr: Toluene-d8



Page 246 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MSD


1,1,1,2-Tetrachloroethane 41.42 38 0 109 79 - 121 41.76 0.813 303.8

1,1,1-Trichloroethane 36.52 38 0 96.1 79 - 128 38.74 5.9 303.8


1,1,2-Trichlor-1,2,2-trifluoroethane 35.16 38 0 92.5 76 - 127 38.11 8.04 303.8

1,1,2-Trichloroethane 40.38 38 0 106 77 - 120 40.27 0.278 303.8

1,1-Dichloroethane 40.64 38 0 107 75 - 124 42.1 3.54 303.8

1,1-Dichloroethene 37.4 38 0 98.4 76 - 128 39.56 5.61 303.8

1,2,3-Trichlorobenzene 36.45 38 0 95.9 73 - 126 34.74 4.78 303.8

1,2,4-Trichlorobenzene 35.5 38 0 93.4 74 - 128 34.97 1.51 303.8


1,2-Dibromoethane 40 38 0 105 70 - 120 40.6 1.49 303.8

1,2-Dichlorobenzene 40.61 38 0 107 75 - 120 40.07 1.32 303.8

1,2-Dichloroethane 40.15 38 0 106 73 - 121 39.62 1.33 303.8

1,2-Dichloropropane 41.22 38 0 108 75 - 124 40.68 1.33 303.8




2-Butanone 79.68 76 0 105 65 - 130 76 4.73 307.6

2-Hexanone 76.82 76 0 101 65 - 133 74.66 2.85 307.6

4-Isopropyltoluene 36.58 38 0 96.3 80 - 125 37.88 3.48 303.8


Acetone 77.14 76 0 102 53 - 142 68.34 12.1 3015

Benzene 41.48 38 0 109 79 - 122 42.7 2.9 303.8

Bromodichloromethane 40.75 38 0 107 79 - 121 40.93 0.447 303.8

Bromoform 37.1 38 0 97.6 74 - 125 36.87 0.621 303.8

Bromomethane 30.37 38 0 79.9 68 - 131 41.8 31.7 30 R 7.6

Carbon disulfide 73.35 76 0 96.5 78 - 131 78.26 6.48 307.6

Carbon tetrachloride 34.87 38 0 91.8 74 - 126 37.56 7.42 303.8

Chlorobenzene 40.36 38 0 106 79 - 120 41.31 2.33 303.8

Chloroethane 39.8 38 0 105 74 - 126 42.57 6.71 307.6

Chloroform 38.01 38 0 100 78 - 122 38.91 2.36 303.8

Chloromethane 40.01 38 0 105 69 - 129 41.17 2.85 307.6

cis-1,2-Dichloroethene 40.83 38 0 107 78 - 122 41.96 2.73 303.8

cis-1,3-Dichloropropene 37.02 38 0 97.4 77 - 123 37.01 0.034 303.8



Page 247 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MSD


Cyclohexane 35.61 38 0 93.7 74 - 126 39 9.07 303.8

Dibromochloromethane 41.13 38 0 108 78 - 122 41.31 0.43 303.8

Dichlorodifluoromethane 36.29 38 0 95.5 57 - 140 39.46 8.38 303.8

Ethylbenzene 41.54 38 0 109 80 - 122 42.67 2.7 303.8

Isopropylbenzene 37.15 38 0 97.8 72 - 127 38.88 4.56 303.8

Methyl tert-butyl ether 40.15 38 0 106 76 - 124 39.73 1.05 303.8

Methylcyclohexane 36.3 38 0 95.5 77 - 127 38.97 7.09 303.8

Methylene chloride 38.63 38 0 102 65 - 130 39.99 3.46 307.6

Naphthalene 38.05 38 1.815 95.4 71 - 128 35.14 7.96 303.8

n-Butylbenzene 36.26 38 0 95.4 77 - 126 37.29 2.78 303.8

n-Propylbenzene 36.99 38 0 97.3 79 - 123 37.83 2.24 303.8

sec-Butylbenzene 37.22 38 0 98.0 80 - 123 38.53 3.44 303.8

Styrene 41.83 38 0 110 78 - 124 41.97 0.337 303.8

tert-Butylbenzene 35.99 38 0 94.7 79 - 124 37.19 3.28 303.8


Toluene 41.66 38 0 110 79 - 120 42.79 2.67 303.8


trans-1,3-Dichloropropene 36.4 38 0 95.8 77 - 120 35.57 2.3 303.8

Trichloroethene 42.8 38 0 113 75 - 123 43.13 0.781 303.8

Trichlorofluoromethane 39.35 38 0 104 75 - 126 42.96 8.76 303.8

Vinyl chloride 37.49 38 0 98.7 76 - 126 40.09 6.7 301.5

Xylenes, Total 123.7 114 0 108 80 - 120 127.7 3.21 307.6

37.2 38 0 97.9 70 - 128 36.28 2.49 300Surr: 1,2-Dichloroethane-d4

38.34 38 0 101 73 - 126 38 0.87 300Surr: 4-Bromofluorobenzene

37.97 38 0 99.9 71 - 128 37.11 2.3 300Surr: Dibromofluoromethane

38.62 38 0 102 73 - 127 37.85 2.01 300Surr: Toluene-d8




Page 248 of 261

Client:Project:



QC BATCH REPORT

Batch ID: R262045 Instrument: WetChem_HS Method: SW9045B

Sample ID: LCS-262045 Units: pH Units Analysis Date: 28-Sep-2015 12:00

Run ID: WetChem_HS_262045 SeqNo: 3439850 PrepDate: DF: 1


Value %RECControl

LimitRPD Ref


LCS

Client ID:

pH 6.01 6 0 100 97 - 1030.100

Sample ID: HS15091139-01DUP Units: pH Units Analysis Date: 28-Sep-2015 12:00

Run ID: WetChem_HS_262045 SeqNo: 3439851 PrepDate: DF: 1


Value %RECControl

LimitRPD Ref


DUP

Client ID:

pH 9.14 9.11 0.329 100.100

Temp Deg C @pH 21.8 21.7 0.46 100




Page 249 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


DUP



The following samples were anayzed in this batch: HS15091078-01 HS15091078-02 HS15091078-03 HS15091078-04 HS15091078-05 HS15091078-06 HS15091078-07 HS15091078-08 HS15091078-09 HS15091078-10 HS15091078-11



Page 250 of 261

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


DUP



The following samples were anayzed in this batch: HS15091078-12 HS15091078-13 HS15091078-14 HS15091078-15 HS15091078-16 HS15091078-17 HS15091078-18 HS15091078-19 HS15091078-20



Page 251 of 261





a Not accredited

















MBLK Method Blank



MS Matrix Spike




SD Serial Dilution






Page 252 of 261



Arkansas 15-024-0 27-Mar-2016




Kentucky KY 2015-2016 30-Apr-2016

Louisiana 03087 2015/2016 30-Jun-2016


Oklahoma 2015-047 31-Aug-2016

Texas T104704231-15-15 30-Apr-2016


Page 253 of 261

Client: PBW Houston



HS15091078-01 4904-SB03-01 Login 9/24/2015 7:00:40 PM PMG 8B


HS15091078-01 4904-SB03-01 Login 9/24/2015 7:00:40 PM PMG 5035

HS15091078-02 4904-SB03-01 Dup Login 9/24/2015 7:11:50 PM PMG 8B

HS15091078-02 4904-SB03-01 Dup Login 9/24/2015 7:11:50 PM PMG LF-13

HS15091078-02 4904-SB03-01 Dup Login 9/24/2015 7:11:50 PM PMG 5035



HS15091078-03 4904-SB03-02 Login 9/24/2015 7:11:50 PM PMG 5035



HS15091078-04 4904-SB03-12 Login 9/24/2015 7:11:50 PM PMG 5035



HS15091078-05 4904-SB10-01 Login 9/24/2015 7:11:50 PM PMG 5035



HS15091078-06 4904-SB10-05 Login 9/24/2015 7:11:50 PM PMG 5035



HS15091078-07 4904-SB10-08 Login 9/24/2015 7:11:50 PM PMG 5035



HS15091078-08 4904-SB11-00 Login 9/24/2015 7:11:50 PM PMG 5035



HS15091078-09 4904-SB11-04 Login 9/24/2015 7:11:50 PM PMG 5035



HS15091078-10 4904-SB11-09 Login 9/24/2015 7:11:50 PM PMG 5035

HS15091078-11 4904-SB11-09 Dup Login 9/24/2015 7:14:12 PM PMG 8B

HS15091078-11 4904-SB11-09 Dup Login 9/24/2015 7:14:12 PM PMG LF-13

HS15091078-11 4904-SB11-09 Dup Login 9/24/2015 7:14:12 PM PMG 5035



HS15091078-12 4904-SB13-02 Login 9/24/2015 7:14:12 PM PMG 5035



HS15091078-13 4904-SB13-10 Login 9/24/2015 7:14:12 PM PMG 5035



Page 254 of 261

Client: PBW Houston



HS15091078-14 4904-SB13-25 Login 9/24/2015 7:14:12 PM PMG 5035



HS15091078-15 4904-SB16-04 Login 9/24/2015 7:14:12 PM PMG 5035



HS15091078-16 4904-SB16-09 Login 9/24/2015 7:14:12 PM PMG 5035

HS15091078-17 4904-SB16-21.5 Login 9/24/2015 7:14:12 PM PMG 8B


HS15091078-17 4904-SB16-21.5 Login 9/24/2015 7:14:12 PM PMG 5035



HS15091078-18 4904-SB17-00 Login 9/24/2015 7:14:12 PM PMG 5035



HS15091078-19 4904-SB17-09 Login 9/24/2015 7:14:12 PM PMG 5035



HS15091078-20 4904-SB17-22 Login 9/24/2015 7:14:12 PM PMG 5035

HS15091078-21 EB 092315 Login 9/24/2015 7:18:15 PM PMG 8B

HS15091078-21 EB 092315 Login 9/24/2015 7:18:15 PM PMG 8B

HS15091078-21 EB 092315 Login 9/24/2015 7:18:15 PM PMG VW-3

HS15091078-21 EB 092315 Login 9/24/2015 7:18:15 PM PMG TPH C1




HS15091078-21 EB 092315 Out 9/25/2015 8:18:42 AM AAP METPREP

HS15091078-21 EB 092315 Out 9/25/2015 1:58:25 PM OFO METPREP

HS15091078-21 EB 092315 Return 9/25/2015 2:03:38 PM OFO 8B

HS15091078-21 EB 092315 Return 9/25/2015 2:48:27 PM AAP 8B


HS15091078-02 4904-SB03-01 Dup Out 9/28/2015 11:50:45 AM OFO METPREP









HS15091078-11 4904-SB11-09 Dup Out 9/28/2015 11:50:45 AM OFO METPREP


Page 255 of 261

Client: PBW Houston










HS15091078-01 4904-SB03-01 Return 9/28/2015 11:51:24 AM OFO 8B

HS15091078-02 4904-SB03-01 Dup Return 9/28/2015 11:51:24 AM OFO 8B









HS15091078-11 4904-SB11-09 Dup Return 9/28/2015 11:51:24 AM OFO 8B









HS15091078-01 4904-SB03-01 Out 9/28/2015 1:42:46 PM AAP METPREP

HS15091078-02 4904-SB03-01 Dup Out 9/28/2015 1:42:46 PM AAP METPREP









HS15091078-11 4904-SB11-09 Dup Out 9/28/2015 1:42:46 PM AAP METPREP






Page 256 of 261

Client: PBW Houston


HS15091078-01 4904-SB03-01 Return 9/28/2015 3:30:04 PM AAP 8B

HS15091078-02 4904-SB03-01 Dup Return 9/28/2015 3:30:04 PM AAP 8B









HS15091078-11 4904-SB11-09 Dup Return 9/28/2015 3:30:04 PM AAP 8B






HS15091078-17 4904-SB16-21.5 Out 9/29/2015 12:45:06 PM AAP METPREP






HS15091078-17 4904-SB16-21.5 Return 9/29/2015 5:31:16 PM AAP 8B

HS15091078-17 4904-SB16-21.5 Return 9/29/2015 5:31:16 PM AAP 8B








HS15091078-17 4904-SB16-21.5 Return 10/1/2015 4:27:45 PM OFO 8B


Page 257 of 261

PS

24-Sep-2015 12:57Date/Time Received:

HS15091078

PBW - Houston

Work Order:

Client Name:


Received by:













Cooler(s)/Kit(s):




pH adjusted?

pH adjusted by:

Login Notes:

No Not Present

Yes No Not Present

Yes No Not Present

Yes No

Yes No

Yes No

Yes No

Yes No

Yes No

Yes No

Yes No

0.4c/0.3c,5.0c/4.9c,1.9c/1.8c,1.4c/1.3c U/C IR123657,24771,24499,18649/24/15 20:15


Yes No N/A

Yes No N/A


25-Sep-201524-Sep-2015


Reviewed by: Bernadette A. Fini



Comments:

Corrective Action:

0

Yes



Page 258 of 261

Page 259 of 261

Page 260 of 261

Page 261 of 261

November 13, 2015





Sincerely,

ALS Environmental received 8 sample(s) on Nov 09, 2015 for the analysis presented in the following report.


Dear Brenda,



Dane J. Wacasey


Page 1 of 36


WorkOrder:














ALS Group USA, Corp Date: 13-Nov-15

Page 2 of 36


WorkOrder:


Dane J. Wacasey




Page 3 of 36


Laboratory Name: ALS Laboratory Group LRC Date: 11/13/2015 Project Name: CES Griggs Rd VCP Laboratory Job Number: HS15110343 Reviewer Name: Dane Wacasey Prep Batch Number(s): 98833, R264592, R264594, R264597 #1 A2 Description Yes No NA3 NR4 ER#5















Was the LCSD RPD within QC limits? X R7 OI Matrix spike (MS) and matrix spike duplicate (MSD) data Were the project/method specified analytes included in the MS and MSD? X Were MS/MSD analyzed at the appropriate frequency? X Were MS (and MSD, if applicable) %Rs within the laboratory QC limits? X 1 Were MS/MSD RPDs within laboratory QC limits? X R8 OI Analytical duplicate data Were appropriate analytical duplicates analyzed for each matrix? X Were analytical duplicates analyzed at the appropriate frequency? X Were RPDs or relative standard deviations within the laboratory QC limits? X R9 OI Method quantitation limits (MQLs): Are the MQLs for each method analyte included in the laboratory data package? X






Is the laboratory NELAC-accredited under the Texas Laboratory Program for the analytes, matrices and methods associated with this laboratory data package? X

Page 4 of 36

Laboratory Review Checklist: Reportable Data Laboratory Name: ALS Laboratory Group LRC Date: 11/13/2015 Project Name: CES Griggs Rd VCP Laboratory Job Number: HS15110343 Reviewer Name: Dane Wacasey Prep Batch Number(s): 98833, R264592, R264594, R264597 #1 A2 Description Yes No NA3 NR4 ER#5








continuing calibration blank (CCB) Was the CCV analyzed at the method-required frequency? X Were percent differences for each analyte within the method-required QC limits? X Was the ICAL curve verified for each analyte? X Was the absolute value of the analyte concentration in the inorganic CCB < MDL? X 2 S3 O Mass spectral tuning: Was the appropriate compound for the method used for tuning? X Were ion abundance data within the method-required QC limits? X S4 O Internal standards (IS): Were IS area counts and retention times within the method-required QC limits? X






Were percent differences, recoveries, and the linearity within the QC limits specified in the method? X









Page 5 of 36


Laboratory Name: ALS Laboratory Group LRC Date: 11/13/2015 Project Name: CES Griggs Rd VCP Laboratory Job Number: HS15110343 Reviewer Name: Dane Wacasey Prep Batch Number(s): 98833, R264592, R264594, R264597 ER#5 Description

1 Batch 98833, Metals by Method SW6020, Sample HS15110353-06 MS and MSD were performed on an unrelated sample.

2 See Run Log and CCB Exception Reports.


Page 6 of 36







ICPMS04

Start Date: End Date:11-Nov-2015 12-Nov-2015

FileIDICV 1 11-Nov-2015

10:50AS MN V009SMPL.D

LLICV5 1 11-Nov-2015 10:54

AS MN V010SMPL.D

LLICV2 1 11-Nov-2015 10:59

AS MN V011SMPL.D

ICB 1 11-Nov-2015 11:03

AS MN V012CCB.D

ICSA 1 11-Nov-2015 11:09

AS MN V013SMPL.D

ICSAB 1 11-Nov-2015 11:14

AS MN V014SMPL.D

CCV 1 1 11-Nov-2015 12:04

AS MN V025SMPL.D

CCB 1 1 11-Nov-2015 12:08

AS MN V026CCB.D

CCV 2 1 11-Nov-2015 12:57

AS MN V037SMPL.D

CCB 2 1 11-Nov-2015 13:05

AS MN V038CCB.D

CCV 3 1 11-Nov-2015 13:54

AS MN V049SMPL.D

CCB 3 1 11-Nov-2015 13:58

AS MN V050CCB.D

CCV 4 1 11-Nov-2015 14:31

AS MN V057SMPL.D

CCB 4 1 11-Nov-2015 14:38

AS MN V058CCB.D

CCV 5 1 11-Nov-2015 15:28

AS MN V068SMPL.D

CCB 5 1 11-Nov-2015 15:33

AS MN V069CCB.D

CCV 6 1 11-Nov-2015 16:17

AS MN V079SMPL.D

CCB 6 1 11-Nov-2015 16:33

AS MN V082CCB.D

CCV 7 1 11-Nov-2015 17:12

AS MN V091SMPL.D

CCB 7 1 11-Nov-2015 17:18

AS MN V092CCB.D

CCV 8 1 11-Nov-2015 18:02

AS MN V102CCV.D

CCB 8 1 11-Nov-2015 18:19

AS MN V106CCB.D

ICCV 9 1 11-Nov-2015 18:54

AS MN V114SMPL.D

LLCCV5 1 11-Nov-2015 18:58

AS MN V115SMPL.D

LLCCV2 1 11-Nov-2015 19:03

AS MN V116SMPL.D

ICCB 9 1 11-Nov-2015 19:07

AS MN V117SMPL.D

CCV 10 1 11-Nov-2015 19:12

AS MN V118CCV.D

CCB 10 1 11-Nov-2015 19:16

AS MN V119CCB.D

CCV 11 1 11-Nov-2015 20:04

AS MN V130CCV.D

CCB 11 1 11-Nov-2015 20:09

AS MN V131CCB.D

MBLK-98833 1 11-Nov-2015 20:13

AS MN V132SMPL.D

MLCS-98833 1 11-Nov-2015 20:18

AS MN V133SMPL.D

CCV 12 1 11-Nov-2015 20:22

AS MN V134CCV.D

13-Nov-15Date: ALS Group USA, Corp

Page 7 of 36







ICPMS04


FileIDCCB 12 1 11-Nov-2015

20:26AS MN V135CCB.D

5910-SB01-00 1 11-Nov-2015 20:31

V136SMPL.D

5910-SB04-12 1 11-Nov-2015 20:39

AS138SMPL.D

4904-SB09-14 1 11-Nov-2015 20:52

AS141SMPL.D

4904-SB17-09 1 11-Nov-2015 20:57

MN142SMPL.D

4904-SB17-22 1 11-Nov-2015 21:01

AS143SMPL.D

CCV 13 1 11-Nov-2015 21:05

AS MN V144CCV.D

CCB 13 1 11-Nov-2015 21:14

AS MN V146CCB.D

ICCV 14 1 11-Nov-2015 21:50

AS MN V154SMPL.D

LLCCV5 1 11-Nov-2015 21:54

AS MN V155SMPL.D

LLCCV2 1 11-Nov-2015 21:59

AS MN V156SMPL.D

ICCB 14 1 11-Nov-2015 22:04

AS MN V157SMPL.D

CCV 15 1 11-Nov-2015 22:08

AS MN V158CCV.D

CCB 15 1 11-Nov-2015 22:13

AS MN V159CCB.D

ICSA 1 11-Nov-2015 22:17

AS MN V160SMPL.D

ICSAB 1 11-Nov-2015 22:22

AS MN V161SMPL.D

CCV 16 1 11-Nov-2015 22:54

AS MN V168CCV.D

CCB 16 1 11-Nov-2015 22:59

AS MN V169CCB.D

ZZZZZZSD 5 11-Nov-2015 23:08

AS MN V171SMPL.D

ZZZZZZMS 1 11-Nov-2015 23:13

AS MN V172SMPL.D

ZZZZZZMSD 1 11-Nov-2015 23:17

AS MN V173SMPL.D

ZZZZZZPDS 1 11-Nov-2015 23:21

AS MN V174SMPL.D

CCV 17 1 11-Nov-2015 23:30

AS MN V176CCV.D

CCB 17 1 11-Nov-2015 23:35

AS MN V177CCB.D

CCV 18 1 12-Nov-2015 00:07

AS MN V184CCV.D

CCB 18 1 12-Nov-2015 00:11

AS MN V185CCB.D

CCV 19 1 12-Nov-2015 00:25

AS MN V188CCV.D

CCB 19 1 12-Nov-2015 00:29

AS MN V189CCB.D

CCV 20 1 12-Nov-2015 01:05

AS MN V197CCV.D

CCB 20 1 12-Nov-2015 01:10

AS MN V198CCB.D

CCV 21 1 12-Nov-2015 01:55

AS MN V208CCV.D

CCB 21 1 12-Nov-2015 02:00

AS MN V209CCB.D

CCV 22 1 12-Nov-2015 02:18

AS MN V213CCV.D


Page 8 of 36







ICPMS04



02:27AS MN V215CCB.D

ICCV 23 1 12-Nov-2015 03:06

AS MN V223SMPL.D

LLCCV5 1 12-Nov-2015 03:11

AS MN V224SMPL.D

LLCCV2 1 12-Nov-2015 03:16

AS MN V225SMPL.D

ICCB 23 1 12-Nov-2015 03:21

AS MN V226SMPL.D

CCV 24 1 12-Nov-2015 03:26

AS MN V227CCV.D

CCB 24 1 12-Nov-2015 03:31

AS MN V228CCB.D

LLCCV2 1 12-Nov-2015 03:36

AS MN V229SMPL.D

LLCCV5 1 12-Nov-2015 03:41

AS MN V230SMPL.D

ICSA 1 12-Nov-2015 03:46

AS MN V231SMPL.D

ICSAB 1 12-Nov-2015 03:51

AS MN V232SMPL.D


Page 9 of 36






ICPMS04

Seq: 3491792CCB 7 111-Nov-2015 17:18 D/F:Date:Analyte Result MDL Report Limit

Units: ug/L

0.728 0.4 5Arsenic


Units: ug/L

0.621 0.6 5Vanadium


Units: ug/L

0.642 0.6 5Vanadium


Units: ug/L

1.579 0.7 5Manganese0.625 0.6 5Vanadium

Seq: 3491857ICCB 14 111-Nov-2015 22:04 D/F:Date:Analyte Result MDL Report Limit

Units: ug/L

0.69 0.6 5Vanadium


Units: ug/L

0.717 0.6 5Vanadium


Units: ug/L

0.764 0.6 5Vanadium


Units: ug/L

1.063 0.6 5Vanadium


Units: ug/L

0.698 0.6 5Vanadium


Units: ug/L

0.691 0.6 5Vanadium


Units: ug/L

0.679 0.6 5Vanadium


Units: ug/L

0.693 0.6 5Vanadium


Units: ug/L

0.659 0.6 5Vanadium

Seq: 3491926ICCB 23 112-Nov-2015 03:21 D/F:Date:Analyte Result MDL Report Limit

Units: ug/L

0.787 0.6 5Vanadium


Page 10 of 36






ICPMS04


Units: ug/L

0.862 0.6 5Vanadium


Page 11 of 36

Client: PBW Houston



HS15110343-01 16-Sep-2015 17:30HS15090757-01

17-Sep-2015 13:095910-SB01-00 Soil

HS15110343-02 16-Sep-2015 15:35HS15090757-011

17-Sep-2015 13:095910-SB04-01.5 Soil

HS15110343-03 16-Sep-2015 15:40HS15090757-13

17-Sep-2015 13:095910-SB04-12 Soil

HS15110343-04 16-Sep-2015 12:45HS15090757-14

17-Sep-2015 13:095910-SB05-01 Soil

HS15110343-05 16-Sep-2015 11:10HS15090757-17

17-Sep-2015 13:095910-SB06-01 Soil

HS15110343-06 18-Sep-2015 14:45HS15090825-36

18-Sep-2015 17:084904-SB09-14 Soil

HS15110343-07 23-Sep-2015 11:10HS15091078-19

24-Sep-2015 12:574904-SB17-09 Soil

HS15110343-08 23-Sep-2015 11:15HS15091078-20

24-Sep-2015 12:574904-SB17-22 Soil

ALS Group USA, Corp 13-Nov-15Date:

Page 12 of 36



WorkOrder:Lab ID:

Collection Date:

HS15110343HS15110343-01


ANALYTICAL REPORT



METALS BY SW6020A Method:SW6020 Analyst: JCJPrep:SW3050A / 10-Nov-2015

10mg/Kg-dry 12-Nov-2015 13:021.04Manganese 5.181,050

1mg/Kg-dry 11-Nov-2015 20:310.238Vanadium 0.51860.9




Page 13 of 36



WorkOrder:Lab ID:

Collection Date:

HS15110343HS15110343-02


ANALYTICAL REPORT




10mg/Kg-dry 12-Nov-2015 13:061.21Manganese 6.05557




Page 14 of 36



WorkOrder:Lab ID:

Collection Date:

HS15110343HS15110343-03


ANALYTICAL REPORT



METALS BY SW6020A Method:SW6020 Analyst: JDEPrep:SW3050A / 10-Nov-2015

1mg/Kg-dry 11-Nov-2015 20:390.107Arsenic 0.5352.98




Page 15 of 36



WorkOrder:Lab ID:

Collection Date:

HS15110343HS15110343-04


ANALYTICAL REPORT




200mg/Kg-dry 12-Nov-2015 13:1121.4Manganese 10722,500

200mg/Kg-dry 12-Nov-2015 13:1149.2Vanadium 1071,030




Page 16 of 36



WorkOrder:Lab ID:

Collection Date:

HS15110343HS15110343-05


ANALYTICAL REPORT





10mg/Kg-dry 12-Nov-2015 13:152.72Vanadium 5.91584



Page 17 of 36



WorkOrder:Lab ID:

Collection Date:

HS15110343HS15110343-06


ANALYTICAL REPORT








Page 18 of 36



WorkOrder:Lab ID:

Collection Date:

HS15110343HS15110343-07


ANALYTICAL REPORT




1mg/Kg-dry 11-Nov-2015 20:570.116Manganese 0.57867.8




Page 19 of 36



WorkOrder:Lab ID:

Collection Date:

HS15110343HS15110343-08


ANALYTICAL REPORT








Page 20 of 36

WEIGHT LOG





Final Volume

Prep Factor

HS15110343-01 1 0.5446 50 (mL) 91.81HS15110343-02 1 0.5314 50 (mL) 94.09HS15110343-03 1 0.5338 50 (mL) 93.67HS15110343-04 1 0.5195 50 (mL) 96.25HS15110343-05 1 0.5245 50 (mL) 95.33HS15110343-06 1 0.5211 50 (mL) 95.95HS15110343-07 1 0.5123 50 (mL) 97.6HS15110343-08 1 0.5588 50 (mL) 89.48


Page 21 of 36


WorkOrder:Project:




10 Nov 2015 08:07 12 Nov 2015 13:02HS15110343-01 16 Sep 2015 17:30 105910-SB01-00

10 Nov 2015 08:07 11 Nov 2015 20:31HS15110343-01 16 Sep 2015 17:30 15910-SB01-00

10 Nov 2015 08:07 12 Nov 2015 13:06HS15110343-02 16 Sep 2015 15:35 105910-SB04-01.5

10 Nov 2015 08:07 11 Nov 2015 20:39HS15110343-03 16 Sep 2015 15:40 15910-SB04-12

10 Nov 2015 08:07 12 Nov 2015 13:11HS15110343-04 16 Sep 2015 12:45 2005910-SB05-01

10 Nov 2015 08:07 12 Nov 2015 13:15HS15110343-05 16 Sep 2015 11:10 105910-SB06-01

10 Nov 2015 08:07 11 Nov 2015 20:52HS15110343-06 18 Sep 2015 14:45 14904-SB09-14

10 Nov 2015 08:07 11 Nov 2015 20:57HS15110343-07 23 Sep 2015 11:10 14904-SB17-09

10 Nov 2015 08:07 11 Nov 2015 21:01HS15110343-08 23 Sep 2015 11:15 14904-SB17-22


23 Sep 2015 16:09HS15110343-01 16 Sep 2015 17:30 15910-SB01-00

23 Sep 2015 16:09HS15110343-02 16 Sep 2015 15:35 15910-SB04-01.5

23 Sep 2015 16:09HS15110343-03 16 Sep 2015 15:40 15910-SB04-12

23 Sep 2015 16:09HS15110343-04 16 Sep 2015 12:45 15910-SB05-01

23 Sep 2015 16:09HS15110343-05 16 Sep 2015 11:10 15910-SB06-01


24 Sep 2015 16:37HS15110343-06 18 Sep 2015 14:45 14904-SB09-14


30 Sep 2015 14:32HS15110343-07 23 Sep 2015 11:10 14904-SB17-09

30 Sep 2015 14:32HS15110343-08 23 Sep 2015 11:15 14904-SB17-22


Page 22 of 36






Units: mg/Kg

Type Analyte DCSCAS MDL PQLDCS SpikeA 0.2627440-38-2 0.100Arsenic 0.5000.250

A 0.2707439-96-5 0.100Manganese 0.5000.250

A 0.3277440-62-2 0.230Vanadium 0.5000.250

Page 23 of 36






Units: wt%


Page 24 of 36

Client:Project:



QC BATCH REPORT


Sample ID: MBLK-98833 Units: mg/Kg Analysis Date: 11-Nov-2015 20:13

Run ID: ICPMS04_264602 SeqNo: 3491832 PrepDate: 10-Nov-2015 DF: 1


Value %RECControl

LimitRPD Ref


MBLK

Client ID:

Arsenic U 0.500

Manganese U 0.500

Vanadium U 0.500

Sample ID: MLCS-98833 Units: mg/Kg Analysis Date: 11-Nov-2015 20:18



Value %RECControl

LimitRPD Ref


LCS

Client ID:

Arsenic 9.878 10 0 98.8 80 - 1200.500

Manganese 9.729 10 0 97.3 80 - 1200.500

Vanadium 9.702 10 0 97.0 80 - 1200.500

Sample ID: HS15110353-06MS Units: mg/Kg Analysis Date: 11-Nov-2015 23:13



Value %RECControl

LimitRPD Ref


MS

Client ID:

Arsenic 9.332 9.418 1.001 88.5 75 - 1250.471

Manganese 17.71 9.418 23.62 -62.7 75 - 125 S 0.471

Vanadium 16.02 9.418 7.892 86.3 75 - 1250.471

Sample ID: HS15110353-06MSD Units: mg/Kg Analysis Date: 11-Nov-2015 23:17



Value %RECControl

LimitRPD Ref


MSD

Client ID:

Arsenic 9.55 9.666 1.001 88.4 75 - 125 9.332 2.3 200.483

Manganese 18.09 9.666 23.62 -57.2 75 - 125 17.71 2.11 20 S 0.483

Vanadium 15.98 9.666 7.892 83.7 75 - 125 16.02 0.2 200.483



Page 25 of 36

Client:Project:



QC BATCH REPORT


Sample ID: HS15110353-06BS Units: mg/Kg Analysis Date: 11-Nov-2015 23:21



Value %RECControl

LimitRPD Ref


PDS

Client ID:

Arsenic 9.086 8.856 1.001 91.3 75 - 1250.443

Manganese 31.06 8.856 23.62 84.1 75 - 1250.443

Vanadium 16.08 8.856 7.892 92.5 75 - 1250.443

Sample ID: HS15110353-06 DIL SX Units: mg/Kg Analysis Date: 11-Nov-2015 23:08



Value %RECControl

LimitRPD Ref


SD

Client ID:

Arsenic 1.05 1.001 0 10 J 2.21

Manganese 22.85 23.62 3.28 102.21

Vanadium 8.517 7.892 7.91 102.21

The following samples were anayzed in this batch: HS15110343-01 HS15110343-02 HS15110343-03 HS15110343-04 HS15110343-05 HS15110343-06 HS15110343-07 HS15110343-08



Page 26 of 36





a Not accredited

















MBLK Method Blank



MS Matrix Spike




SD Serial Dilution




Page 27 of 36



Arkansas 15-024-0 27-Mar-2016




Kansas E-10352 2014-2015 30-Nov-2015

Kentucky KY 2015-2016 30-Apr-2016

Louisiana 03087 2015/2016 30-Jun-2016


North Dakota R-193 2015-2016 30-Apr-2016

Oklahoma 2015-047 31-Aug-2016

Texas T104704231-15-15 30-Apr-2016


Page 28 of 36

Client: PBW Houston



HS15110343-01 5910-SB01-00 Login 11/9/2015 2:07:39 PM RPG 4C

HS15110343-02 5910-SB04-01.5 Login 11/9/2015 2:20:10 PM RPG 4C















HS15110343-01 5910-SB01-00 Return 11/11/2015 8:22:46 AM AAP 4C

HS15110343-02 5910-SB04-01.5 Return 11/11/2015 8:22:46 AM AAP 4C








Page 29 of 36

PS

09-Nov-2015 14:07Date/Time Received:

HS15110343

PBW - Houston

Work Order:

Client Name:


Received by:













Cooler(s)/Kit(s):




pH adjusted?

pH adjusted by:

Login Notes:

No Not Present

Yes No Not Present

Yes No Not Present

Yes No

Yes No

Yes No

Yes No

Yes No

Yes No

Yes No

Yes No

1.0c/0.7c/1.7c/1.4c/2.3c/2.0c u/c 64709/24537/303009/17/2015 18:29


Yes No N/A

Yes No N/A

COC: 5910-SB03-05 (txtcore4) of 4 is emptyCOC: 5910-SB03-05 DUP (txtcore4)of 4 is emptyCOC:TB-01 091615 Sample: TB-01 090915-52COC:TB-02 091615 Sample: TB-02 090915-59

Checklist completed by: ADMINDateeSignatureDateeSignature

9-Nov-201517-Sep-2015

ALS CourierSoils Carrier name:Matrices:




Comments:

Corrective Action:

0

Yes



Page 30 of 36

PS


HS15110343

PBW - Houston

Work Order:

Client Name:


Received by:













Cooler(s)/Kit(s):




pH adjusted?

pH adjusted by:

Login Notes:

No Not Present

Yes No Not Present

Yes No Not Present

Yes No

Yes No

Yes No

Yes No

Yes No

Yes No

Yes No

Yes No

0.6c/0.5c,2.3c/2.2c,0.5c/0.4c,3.7c/3.6c,1.4c/1.3c,3.1c/3.0c U/C

IR1

5161,3074,2773,3210,24517,237099/18/15 20:40


Yes No N/A

Yes No N/A

4904-SB06-10 - received 17 containers. Logged in as MS/MSD. 4900-SB01-05 - 1 x VOC vial has 10grams of sample.. Following sample bulk jars received empty - 4900SB01-16 & Dup. 4904-SB06-01 & Dup


23-Sep-201518-Sep-2015





Comments:

Corrective Action:

0

Yes



Page 31 of 36

PS


HS15110343

PBW - Houston

Work Order:

Client Name:


Received by:













Cooler(s)/Kit(s):




pH adjusted?

pH adjusted by:

Login Notes:

No Not Present

Yes No Not Present

Yes No Not Present

Yes No

Yes No

Yes No

Yes No

Yes No

Yes No

Yes No

Yes No

0.4c/0.3c,5.0c/4.9c,1.9c/1.8c,1.4c/1.3c U/C IR123657,24771,24499,18649/24/15 20:15


Yes No N/A

Yes No N/A


25-Sep-201524-Sep-2015





Comments:

Corrective Action:

0

Yes



Page 32 of 36

Page 33 of 36

Page 34 of 36

Page 35 of 36

Page 36 of 36

February 22, 2016

Brenda BasilePastor, Behling & Wheeler, LLC11231 Richmond AvenueSuite D104Houston, TX 77082




Sincerely,

ALS Environmental received 20 sample(s) on Jan 06, 2016 for the analysis presented in the following report.

Laboratory Results for: CES Griggs Road Phase II

Dear Brenda,


Generated By: Jumoke.Lawal

Dane J. Wacasey


Page 1 of 71


WorkOrder:

Pastor, Behling & Wheeler, LLCCES Griggs Road Phase IIHS16010118













ALS Group USA, Corp Date: 22-Feb-16

Page 2 of 71


WorkOrder:


Dane J. Wacasey




Page 3 of 71


Laboratory Name: ALS Laboratory Group LRC Date: 02/22/2016 Project Name: CES Griggs Road Phase II Laboratory Job Number: HS16010118


Prep Batch Number(s): 100366,100371,100374,100404,100405,100438,R267325,R267338,R267382, R267449,R267607














Were LCSs analyzed at the required frequency? X Were LCS (and LCSD, if applicable) %Rs within the laboratory QC limits? X 1









Page 4 of 71

Laboratory Review Checklist: Reportable Data Laboratory Name: ALS Laboratory Group LRC Date:02/22/2016 Project Name: CES Griggs Road Phase II Laboratory Job Number: HS16010118


Prep Batch Number(s): 100366,100371,100374,100404,100405,100438,R267325,R267338,R267382,R267449, R267607
























Page 5 of 71


Laboratory Name: ALS Laboratory Group LRC Date: 02/22/2016 Project Name: CES Griggs Road Phase II Laboratory Job Number: HS16010118


Prep Batch Number(s): 100366,100371,100374,100404,100405,100438,R267325,R267338,R267382,R267449,R267607

ER#5 Description

1

Batch 100366, Semivolatile Organics Method SW8270, LCSD RPD recovered above the RPD limit for surrogate 2-Fluorophenol. The individual recoveries were in control.

2

Batch 100371, Metals Method SW6020, sample 4904-SB26-23, MS and or MSD recovered outside the control limits for Manganese, Vanadium and Zinc due to probable matrix interference in the sample.

3 Batch 100366, Semivolatile Organics Method SW8270, sample HS16010117-03, MS and MSD were performed on unrelated sample.



Page 6 of 71





HS16010118CES Griggs Road Phase IIPastor, Behling & Wheeler, LLC


ICPMS04

Start Date: End Date:08-Jan-2016 08-Jan-2016

FileIDICV 1 08-Jan-2016

13:02AS BA CO CU MN NI PB SE V ZN009SMPL.D

LLICV5 1 08-Jan-2016 13:06

AS BA CO CU MN NI PB SE V ZN010SMPL.D

LLICV2 1 08-Jan-2016 13:10


ICB 1 08-Jan-2016 13:15

AS BA CO CU MN NI PB SE V ZN012CCB.D

ICSA 1 08-Jan-2016 13:21


ICSAB 1 08-Jan-2016 13:26


CCV 1 1 08-Jan-2016 14:06


CCB 1 1 08-Jan-2016 14:10


CCV 2 1 08-Jan-2016 14:58


CCB 2 1 08-Jan-2016 15:03


CCV 3 1 08-Jan-2016 15:47


CCB 3 1 08-Jan-2016 15:51


MBLK-100371 1 08-Jan-2016 16:01


MLCS-100371 1 08-Jan-2016 16:05


4904-SB26-23 1 08-Jan-2016 16:09

CO NI SE ZN051SMPL.D

4904-SB26-23SD 5 08-Jan-2016 16:14


4904-SB26-23MS 1 08-Jan-2016 16:18


4904-SB26-23MSD 1 08-Jan-2016 16:22


4904-SB26-23PDS 1 08-Jan-2016 16:27


4904-SB27-14 1 08-Jan-2016 16:31

AS056SMPL.D

4904-SB28-16 1 08-Jan-2016 16:35

AS BA MN NI SE057SMPL.D

CCV 4 1 08-Jan-2016 16:40

AS BA CO CU MN NI PB SE V ZN058CCV.D

CCB 4 1 08-Jan-2016 16:44


5910-SB16-01 1 08-Jan-2016 16:48

V060SMPL.D

5910-SB15-01 1 08-Jan-2016 16:53

V061SMPL.D

4904-SB29-24 1 08-Jan-2016 16:57

AS CO CU MN NI PB SE062SMPL.D

5910-SB07-01 1 08-Jan-2016 17:01

MN063SMPL.D

5910-SB10-02.5 1 08-Jan-2016 17:06

MN V064SMPL.D

5910-SB11-02.5 1 08-Jan-2016 17:10

V065SMPL.D

5910-SB12-01 1 08-Jan-2016 17:14

MN V066SMPL.D

5910-SB12-01 DUP 1 08-Jan-2016 17:19

MN V067SMPL.D

5910-SB13-01 1 08-Jan-2016 17:23

MN V068SMPL.D

CCV 5 1 08-Jan-2016 17:28

AS BA CO CU MN NI PB SE V ZN069CCV.D

22-Feb-16Date: ALS Group USA, Corp

Page 7 of 71







ICPMS04


FileIDCCB 5 1 08-Jan-2016

17:32AS BA CO CU MN NI PB SE V ZN070CCB.D

LLCCV2 1 08-Jan-2016 17:36


LLCCV5 1 08-Jan-2016 17:41


ICSA 1 08-Jan-2016 17:45


ICSAB 1 08-Jan-2016 17:50



Page 8 of 71






ICPMS04

Seq: 3547845CCB 4 108-Jan-2016 16:44 D/F:Date:Analyte Result MDL Report Limit

Units: ug/L

0.653 0.6 5Vanadium


Units: ug/L

0.718 0.7 5Manganese0.722 0.6 5Vanadium


Page 9 of 71

Client: Pastor, Behling & Wheeler, LLC

Work Order: HS16010118Project: CES Griggs Road Phase II SAMPLE SUMMARY


HS16010118-01 05-Jan-2016 09:15 06-Jan-2016 18:104904-SB02A-02 Soil

HS16010118-02 05-Jan-2016 09:45 06-Jan-2016 18:104904-SB25-01.5 Soil

HS16010118-03 05-Jan-2016 09:45 06-Jan-2016 18:104904-SB25-04 Soil

HS16010118-04 05-Jan-2016 11:20 06-Jan-2016 18:104904-SB26-23 Soil

HS16010118-05 05-Jan-2016 16:00 06-Jan-2016 18:104904-SB27-14 Soil

HS16010118-06 05-Jan-2016 14:15 06-Jan-2016 18:104904-SB28-16 Soil

HS16010118-07 05-Jan-2016 16:40 06-Jan-2016 18:105910-SB16-01 Soil

HS16010118-08 05-Jan-2016 16:55 06-Jan-2016 18:105910-SB15-01 Soil

HS16010118-09 05-Jan-2016 17:25 06-Jan-2016 18:10EB 010516 Wastewater

HS16010118-10 06-Jan-2016 09:20 06-Jan-2016 18:104904-SB29-24 Soil

HS16010118-11 06-Jan-2016 16:10 06-Jan-2016 18:105910-SB07-01 Soil

HS16010118-12 06-Jan-2016 15:55 06-Jan-2016 18:105910-SB08-01 Soil

HS16010118-13 06-Jan-2016 15:35 06-Jan-2016 18:105910-SB09-02 Soil

HS16010118-14 06-Jan-2016 14:50 06-Jan-2016 18:105910-SB10-02.5 Soil

HS16010118-15 06-Jan-2016 14:25 06-Jan-2016 18:105910-SB11-02.5 Soil

HS16010118-16 06-Jan-2016 13:50 06-Jan-2016 18:105910-SB12-01 Soil

HS16010118-17 06-Jan-2016 13:50 06-Jan-2016 18:105910-SB12-01 DUP Soil

HS16010118-18 06-Jan-2016 16:30 06-Jan-2016 18:105910-SB13-01 Soil

HS16010118-19 06-Jan-2016 16:45 06-Jan-2016 18:10EB 010616 Water

HS16010118-20 06-Jan-2016 16:50 06-Jan-2016 18:10TB 010616 Water

ALS Group USA, Corp 22-Feb-16Date:

Page 10 of 71


Pastor, Behling & Wheeler, LLCCES Griggs Road Phase II4904-SB02A-02

WorkOrder:Lab ID:

Collection Date:

HS16010118HS16010118-01

05-Jan-2016 09:15 Matrix:Soil

ANALYTICAL REPORT



MOISTURE Method:SW3550 Analyst: DFF1wt% 13-Jan-2016 09:440.0100Percent Moisture 0.010015.5

TEXAS TPH BY TX1005 Method:TX1005 Analyst: KHTPrep:TX1005PR / 08-Jan-2016

1mg/Kg-dry 08-Jan-2016 21:31J 9.2>nC12 to nC28 4636

1mg/Kg-dry 08-Jan-2016 21:319.2>nC28 to nC35 4664

1mg/Kg-dry 08-Jan-2016 21:319.2Total Petroleum Hydrocarbon 46100

Surr: 2-Fluorobiphenyl 1%REC 08-Jan-2016 21:31113 70-130

Surr: Trifluoromethyl benzene 1%REC 08-Jan-2016 21:31103 70-130



Page 11 of 71


Pastor, Behling & Wheeler, LLCCES Griggs Road Phase II4904-SB25-01.5

WorkOrder:Lab ID:

Collection Date:

HS16010118HS16010118-02


ANALYTICAL REPORT





1mg/Kg-dry 08-Jan-2016 22:009.5>nC12 to nC28 48U

1mg/Kg-dry 08-Jan-2016 22:00J 9.5>nC28 to nC35 4817

1mg/Kg-dry 08-Jan-2016 22:00J 9.5Total Petroleum Hydrocarbon 4817.0





Page 12 of 71


Pastor, Behling & Wheeler, LLCCES Griggs Road Phase II4904-SB25-04

WorkOrder:Lab ID:

Collection Date:

HS16010118HS16010118-03


ANALYTICAL REPORT







1mg/Kg-dry 08-Jan-2016 22:296.8Total Petroleum Hydrocarbon 34U





Page 13 of 71



WorkOrder:Lab ID:

Collection Date:

HS16010118HS16010118-04


ANALYTICAL REPORT



VOLATILES BY SW8260C Method:SW8260 Analyst: WLR1mg/Kg-dry 07-Jan-2016 12:190.000421,1-Dichloroethane 0.0042U

1mg/Kg-dry 07-Jan-2016 12:190.00068cis-1,2-Dichloroethene 0.00420.0090

Surr: 1,2-Dichloroethane-d4 1%REC 07-Jan-2016 12:1984.4 70-128

Surr: 4-Bromofluorobenzene 1%REC 07-Jan-2016 12:1992.7 73-126

Surr: Dibromofluoromethane 1%REC 07-Jan-2016 12:1993.4 71-128

Surr: Toluene-d8 1%REC 07-Jan-2016 12:19100 73-127

METALS BY SW6020A Method:SW6020 Analyst: JDEPrep:SW3050A / 07-Jan-2016

1mg/Kg-dry 08-Jan-2016 16:090.0758Cobalt 0.5420.552

1mg/Kg-dry 08-Jan-2016 16:090.0975Nickel 0.5421.78

1mg/Kg-dry 08-Jan-2016 16:09J 0.195Selenium 0.5420.314

1mg/Kg-dry 08-Jan-2016 16:090.271Zinc 0.5423.73




Page 14 of 71



WorkOrder:Lab ID:

Collection Date:

HS16010118HS16010118-05


ANALYTICAL REPORT




1mg/Kg-dry 08-Jan-2016 16:310.133Arsenic 0.6671.71




Page 15 of 71



WorkOrder:Lab ID:

Collection Date:

HS16010118HS16010118-06


ANALYTICAL REPORT




1mg/Kg-dry 08-Jan-2016 16:35J 0.124Arsenic 0.6180.487

1mg/Kg-dry 08-Jan-2016 16:350.0989Barium 0.6186.77

1mg/Kg-dry 08-Jan-2016 16:350.124Manganese 0.61815.0






Page 16 of 71



WorkOrder:Lab ID:

Collection Date:

HS16010118HS16010118-07


ANALYTICAL REPORT





1mg/Kg-dry 08-Jan-2016 16:480.291Vanadium 0.63230.1



Page 17 of 71



WorkOrder:Lab ID:

Collection Date:

HS16010118HS16010118-08


ANALYTICAL REPORT








Page 18 of 71


Pastor, Behling & Wheeler, LLCCES Griggs Road Phase IIEB 010516

WorkOrder:Lab ID:

Collection Date:

HS16010118HS16010118-09

05-Jan-2016 17:25 Matrix:Wastewater

ANALYTICAL REPORT



LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: AKP1mg/L 07-Jan-2016 16:300.000201,1-Dichloroethane 0.0010U

1mg/L 07-Jan-2016 16:300.00020cis-1,2-Dichloroethene 0.0010U


Surr: 4-Bromofluorobenzene 1%REC 07-Jan-2016 16:30109 70-125

Surr: Dibromofluoromethane 1%REC 07-Jan-2016 16:30101 74-125


ICP-MS METALS BY SW6020A Method:SW6020 Analyst: RPMPrep:SW3010A / 11-Jan-2016

1mg/L 12-Jan-2016 11:570.000400Arsenic 0.00500U

1mg/L 12-Jan-2016 11:570.00190Barium 0.00500U

1mg/L 12-Jan-2016 11:570.000200Cobalt 0.00500U

1mg/L 12-Jan-2016 11:570.00100Copper 0.00200U

1mg/L 12-Jan-2016 11:570.000600Lead 0.00500U

1mg/L 12-Jan-2016 11:57J 0.000700Manganese 0.005000.00136

1mg/L 12-Jan-2016 11:570.000600Nickel 0.00500U

1mg/L 12-Jan-2016 11:570.00110Selenium 0.00500U

1mg/L 12-Jan-2016 11:570.000600Vanadium 0.00500U

1mg/L 12-Jan-2016 11:570.00200Zinc 0.00500U

LOW-LEVEL TEXAS TPH BY TX1005 Method:TX1005 Analyst: KHTPrep:TX1005PR / 08-Jan-2016

1mg/L 08-Jan-2016 22:000.20>nC12 to nC28 0.49U

1mg/L 08-Jan-2016 22:000.20>nC28 to nC35 0.49U

1mg/L 08-Jan-2016 22:000.20Total Petroleum Hydrocarbon 0.49U





Page 19 of 71



WorkOrder:Lab ID:

Collection Date:

HS16010118HS16010118-10


ANALYTICAL REPORT




1mg/Kg-dry 08-Jan-2016 16:570.109Arsenic 0.5471.09


1mg/Kg-dry 08-Jan-2016 16:570.109Copper 0.2192.12

1mg/Kg-dry 08-Jan-2016 16:570.0547Lead 0.5475.39







Page 20 of 71



WorkOrder:Lab ID:

Collection Date:

HS16010118HS16010118-11


ANALYTICAL REPORT




1mg/Kg-dry 08-Jan-2016 17:010.122Manganese 0.611127




Page 21 of 71



WorkOrder:Lab ID:

Collection Date:

HS16010118HS16010118-12


ANALYTICAL REPORT



LOW-LEVEL SEMIVOLATILES Method:SW8270 Analyst: ACNPrep:SW3541 / 07-Jan-2016

1mg/Kg-dry 07-Jan-2016 22:160.0013Benzo(a)pyrene 0.00420.021

Surr: 2,4,6-Tribromophenol 1%REC 07-Jan-2016 22:1696.1 36-126

Surr: 2-Fluorobiphenyl 1%REC 07-Jan-2016 22:1667.1 43-125

Surr: 2-Fluorophenol 1%REC 07-Jan-2016 22:1649.1 37-125

Surr: 4-Terphenyl-d14 1%REC 07-Jan-2016 22:1678.2 32-125

Surr: Nitrobenzene-d5 1%REC 07-Jan-2016 22:1679.2 37-125

Surr: Phenol-d6 1%REC 07-Jan-2016 22:1658.5 40-125




Page 22 of 71



WorkOrder:Lab ID:

Collection Date:

HS16010118HS16010118-13


ANALYTICAL REPORT




1mg/Kg-dry 07-Jan-2016 22:36J 0.0012Benzo(a)pyrene 0.00400.0022










Page 23 of 71



WorkOrder:Lab ID:

Collection Date:

HS16010118HS16010118-14


ANALYTICAL REPORT





Surr: 2,4,6-Tribromophenol 1%REC 07-Jan-2016 22:55106 36-126












Page 24 of 71



WorkOrder:Lab ID:

Collection Date:

HS16010118HS16010118-15


ANALYTICAL REPORT





Surr: 2,4,6-Tribromophenol 1%REC 07-Jan-2016 17:41104 36-126







500mg/Kg-dry 11-Jan-2016 11:4659.3Manganese 29624,800





Page 25 of 71



WorkOrder:Lab ID:

Collection Date:

HS16010118HS16010118-16


ANALYTICAL REPORT









Page 26 of 71


Pastor, Behling & Wheeler, LLCCES Griggs Road Phase II5910-SB12-01 DUP

WorkOrder:Lab ID:

Collection Date:

HS16010118HS16010118-17


ANALYTICAL REPORT









Page 27 of 71



WorkOrder:Lab ID:

Collection Date:

HS16010118HS16010118-18


ANALYTICAL REPORT









Page 28 of 71


Pastor, Behling & Wheeler, LLCCES Griggs Road Phase IIEB 010616

WorkOrder:Lab ID:

Collection Date:

HS16010118HS16010118-19

06-Jan-2016 16:45 Matrix:Water

ANALYTICAL REPORT




1mg/L 07-Jan-2016 21:57J 0.000020Benzo(a)pyrene 0.000100.000025








1mg/L 12-Jan-2016 12:000.000700Manganese 0.005000.00607

1mg/L 12-Jan-2016 12:000.000600Vanadium 0.00500U



Page 29 of 71


Pastor, Behling & Wheeler, LLCCES Griggs Road Phase IITB 010616

WorkOrder:Lab ID:

Collection Date:

HS16010118HS16010118-20


ANALYTICAL REPORT



LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: AKP1mg/L 07-Jan-2016 16:550.000201,1-Dichloroethane 0.0010U

1mg/L 07-Jan-2016 16:550.00020cis-1,2-Dichloroethene 0.0010U


Surr: 4-Bromofluorobenzene 1%REC 07-Jan-2016 16:55111 70-125

Surr: Dibromofluoromethane 1%REC 07-Jan-2016 16:5598.0 74-125




Page 30 of 71

WEIGHT LOG





Sample Wt/Vol

Final Volume

Weight Factor

HS16010118-04 2 6.917 (g) TerraCore (5035A)5 (mL) 0.72



Final Volume

Prep Factor

HS16010118-19 1 1000 1 (mL) 0.001



Final Volume

Prep Factor

HS16010118-04 1 0.5442 50 (mL) 91.88HS16010118-05 1 0.5009 50 (mL) 99.82HS16010118-06 1 0.5391 50 (mL) 92.75HS16010118-07 1 0.5182 50 (mL) 96.49HS16010118-08 1 0.5203 50 (mL) 96.1HS16010118-10 1 0.5407 50 (mL) 92.47HS16010118-11 1 0.5324 50 (mL) 93.91HS16010118-14 1 0.5438 50 (mL) 91.95HS16010118-15 1 0.5214 50 (mL) 95.9HS16010118-16 1 0.5258 50 (mL) 95.09HS16010118-17 1 0.5435 50 (mL) 92HS16010118-18 1 0.5294 50 (mL) 94.45



Final Volume

Prep Factor

HS16010118-12 1 30.09 1 (mL) 0.03323HS16010118-13 1 30.16 1 (mL) 0.03316HS16010118-14 1 30.08 1 (mL) 0.03324HS16010118-15 1 30.05 1 (mL) 0.03328



Final Volume

Prep Factor

HS16010118-09 1 30.57 3 (mL) 0.09814



Final Volume

Prep Factor

HS16010118-01 1 12.92 10 (mL) 0.774HS16010118-02 1 12.29 10 (mL) 0.8137HS16010118-03 1 17.61 10 (mL) 0.5679


Page 31 of 71

WEIGHT LOG





Final Volume

Prep Factor

HS16010118-09 1 50 50 (mL) 1HS16010118-19 1 50 50 (mL) 1


Page 32 of 71

Client:CES Griggs Road Phase IIPastor, Behling & Wheeler, LLC

WorkOrder:Project:




07 Jan 2016 06:58 07 Jan 2016 21:57HS16010118-19 06 Jan 2016 16:45 1EB 010616


07 Jan 2016 10:33 08 Jan 2016 16:09HS16010118-04 05 Jan 2016 11:20 14904-SB26-23

07 Jan 2016 10:33 08 Jan 2016 16:31HS16010118-05 05 Jan 2016 16:00 14904-SB27-14

07 Jan 2016 10:33 08 Jan 2016 16:35HS16010118-06 05 Jan 2016 14:15 14904-SB28-16

07 Jan 2016 10:33 08 Jan 2016 16:48HS16010118-07 05 Jan 2016 16:40 15910-SB16-01

07 Jan 2016 10:33 08 Jan 2016 16:53HS16010118-08 05 Jan 2016 16:55 15910-SB15-01

07 Jan 2016 10:33 08 Jan 2016 16:57HS16010118-10 06 Jan 2016 09:20 14904-SB29-24

07 Jan 2016 10:33 08 Jan 2016 17:01HS16010118-11 06 Jan 2016 16:10 15910-SB07-01

07 Jan 2016 10:33 08 Jan 2016 17:06HS16010118-14 06 Jan 2016 14:50 15910-SB10-02.5

07 Jan 2016 10:33 11 Jan 2016 11:46HS16010118-15 06 Jan 2016 14:25 5005910-SB11-02.5

07 Jan 2016 10:33 08 Jan 2016 17:10HS16010118-15 06 Jan 2016 14:25 15910-SB11-02.5

07 Jan 2016 10:33 08 Jan 2016 17:14HS16010118-16 06 Jan 2016 13:50 15910-SB12-01

07 Jan 2016 10:33 08 Jan 2016 17:19HS16010118-17 06 Jan 2016 13:50 15910-SB12-01 DUP

07 Jan 2016 10:33 08 Jan 2016 17:23HS16010118-18 06 Jan 2016 16:30 15910-SB13-01


07 Jan 2016 09:05 07 Jan 2016 22:16HS16010118-12 06 Jan 2016 15:55 15910-SB08-01

07 Jan 2016 09:05 07 Jan 2016 22:36HS16010118-13 06 Jan 2016 15:35 15910-SB09-02

07 Jan 2016 09:05 07 Jan 2016 22:55HS16010118-14 06 Jan 2016 14:50 15910-SB10-02.5

07 Jan 2016 09:05 07 Jan 2016 17:41HS16010118-15 06 Jan 2016 14:25 15910-SB11-02.5

Batch ID 100404 Test Name : LOW-LEVEL TEXAS TPH BY TX1005 Matrix: Wastewater

08 Jan 2016 11:31 08 Jan 2016 22:00HS16010118-09 05 Jan 2016 17:25 1EB 010516


08 Jan 2016 11:38 08 Jan 2016 21:31HS16010118-01 05 Jan 2016 09:15 14904-SB02A-02

08 Jan 2016 11:38 08 Jan 2016 22:00HS16010118-02 05 Jan 2016 09:45 14904-SB25-01.5

08 Jan 2016 11:38 08 Jan 2016 22:29HS16010118-03 05 Jan 2016 09:45 14904-SB25-04


11 Jan 2016 14:08 12 Jan 2016 12:00HS16010118-19 06 Jan 2016 16:45 1EB 010616

Batch ID 100438 Test Name : ICP-MS METALS BY SW6020A Matrix: Wastewater

11 Jan 2016 14:08 12 Jan 2016 11:57HS16010118-09 05 Jan 2016 17:25 1EB 010516


07 Jan 2016 12:19HS16010118-04 05 Jan 2016 11:20 14904-SB26-23


07 Jan 2016 16:55HS16010118-20 06 Jan 2016 16:50 1TB 010616

Batch ID R267338 Test Name : LOW LEVEL VOLATILES BY SW8260C Matrix: Wastewater

07 Jan 2016 16:30HS16010118-09 05 Jan 2016 17:25 1EB 010516


Page 33 of 71

Client:CES Griggs Road Phase IIPastor, Behling & Wheeler, LLC

WorkOrder:Project:




07 Jan 2016 15:29HS16010118-04 05 Jan 2016 11:20 14904-SB26-23

07 Jan 2016 15:29HS16010118-05 05 Jan 2016 16:00 14904-SB27-14

07 Jan 2016 15:29HS16010118-06 05 Jan 2016 14:15 14904-SB28-16

07 Jan 2016 15:29HS16010118-07 05 Jan 2016 16:40 15910-SB16-01


08 Jan 2016 11:00HS16010118-08 05 Jan 2016 16:55 15910-SB15-01

08 Jan 2016 11:00HS16010118-10 06 Jan 2016 09:20 14904-SB29-24

08 Jan 2016 11:00HS16010118-11 06 Jan 2016 16:10 15910-SB07-01

08 Jan 2016 11:00HS16010118-12 06 Jan 2016 15:55 15910-SB08-01

08 Jan 2016 11:00HS16010118-13 06 Jan 2016 15:35 15910-SB09-02

08 Jan 2016 11:00HS16010118-14 06 Jan 2016 14:50 15910-SB10-02.5

08 Jan 2016 11:00HS16010118-15 06 Jan 2016 14:25 15910-SB11-02.5

08 Jan 2016 11:00HS16010118-16 06 Jan 2016 13:50 15910-SB12-01

08 Jan 2016 11:00HS16010118-17 06 Jan 2016 13:50 15910-SB12-01 DUP

08 Jan 2016 11:00HS16010118-18 06 Jan 2016 16:30 15910-SB13-01


13 Jan 2016 09:44HS16010118-01 05 Jan 2016 09:15 14904-SB02A-02

13 Jan 2016 09:44HS16010118-02 05 Jan 2016 09:45 14904-SB25-01.5

13 Jan 2016 09:44HS16010118-03 05 Jan 2016 09:45 14904-SB25-04


Page 34 of 71






Units: mg/Kg

Type Analyte DCSCAS MDL PQLDCS SpikeA 22TPH-1005-2 10>nC12 to nC28 5025

A 22TPH-1005-4 10>nC28 to nC35 5025




Page 35 of 71






Units: mg/L

Type Analyte DCSCAS MDL PQLDCS SpikeA 0.98TPH-1005-2 0.20>nC12 to nC28 0.500.50

A 0.98TPH-1005-4 0.20>nC28 to nC35 0.500.50




Page 36 of 71






Units: mg/Kg


A 0.1077440-39-3 0.0800Barium 0.5000.100

A 0.1067440-48-4 0.0700Cobalt 0.5000.100

A 0.04837440-50-8 0.100Copper 0.2000.100

A 0.09497439-92-1 0.0500Lead 0.5000.100

A 0.1107439-96-5 0.100Manganese 0.5000.100

A 0.09357440-02-0 0.0900Nickel 0.5000.100

A 0.3147782-49-2 0.180Selenium 0.5000.250

A 0.3277440-62-2 0.230Vanadium 0.5000.250

A 0.3267440-66-6 0.250Zinc 0.5000.250

Page 37 of 71






Units: mg/L


A 0.002347440-39-3 0.00190Barium 0.005000.00250

A 0.001017440-48-4 0.000200Cobalt 0.005000.00100

A 0.0007787440-50-8 0.00100Copper 0.002000.00100

A 0.001047439-92-1 0.000600Lead 0.005000.00100

A 0.0008757439-96-5 0.000700Manganese 0.005000.00100

A 0.0006887440-02-0 0.000600Nickel 0.005000.00100

A 0.002587782-49-2 0.00110Selenium 0.005000.00250

A 0.0007707440-62-2 0.000600Vanadium 0.005000.00100

A 0.003147440-66-6 0.00200Zinc 0.005000.00250

Page 38 of 71






Units: mg/Kg

Type Analyte DCSCAS MDL PQLDCS SpikeA 0.001450-32-8 0.0010Benzo(a)pyrene 0.00330.0017




S 01718-51-0 04-Terphenyl-d14 00


S 013127-88-3 0Phenol-d6 00

Page 39 of 71






Units: mg/L

Type Analyte DCSCAS MDL PQLDCS SpikeA 0.00004450-32-8 0.000020Benzo(a)pyrene 0.000100.000050



S 0367-12-4 02-Fluorophenol 0.000200

S 01718-51-0 04-Terphenyl-d14 0.000200

S 04165-60-0 0Nitrobenzene-d5 0.000200

S 013127-88-3 0Phenol-d6 0.000200

Page 40 of 71






Units: mg/L

Type Analyte DCSCAS MDL PQLDCS SpikeA 0.0006375-34-3 0.000201,1-Dichloroethane 0.00100.00050





S 02037-26-5 0Toluene-d8 0.00100

Page 41 of 71






Units: mg/Kg

Type Analyte DCSCAS MDL PQLDCS SpikeA 0.001175-34-3 0.000501,1-Dichloroethane 0.00500.0012





S 02037-26-5 0Toluene-d8 00

Page 42 of 71






Units: wt%

Type Analyte DCSCAS MDL PQLDCS SpikeA 0.0100MOIST 0.0100Percent Moisture 0.01000.0100

Page 43 of 71

Client:Project:

Pastor, Behling & Wheeler, LLCCES Griggs Road Phase II


QC BATCH REPORT


Sample ID: MBLK-100404 Units: mg/L Analysis Date: 08-Jan-2016 18:07

Run ID: FID-11_267528 SeqNo: 3549413 PrepDate: 08-Jan-2016 DF: 1


Value %RECControl

LimitRPD Ref


MBLK

Client ID:

>nC12 to nC28 U 0.50

>nC28 to nC35 U 0.50




Sample ID: LCS-100404 Units: mg/L Analysis Date: 08-Jan-2016 18:36



Value %RECControl

LimitRPD Ref


LCS

Client ID:

>nC12 to nC28 24.39 25 0 97.6 75 - 1250.50



Sample ID: LCSD-100404 Units: mg/L Analysis Date: 08-Jan-2016 19:06



Value %RECControl

LimitRPD Ref


LCSD

Client ID:

>nC12 to nC28 23.34 25 0 93.3 75 - 125 24.39 4.42 200.50



Sample ID: HS16010183-02MS Units: mg/L Analysis Date: 08-Jan-2016 20:04



Value %RECControl

LimitRPD Ref


MS

Client ID:

>nC12 to nC28 23.07 24.95 0 92.5 75 - 1250.50





Page 44 of 71

Client:Project:



QC BATCH REPORT


Sample ID: HS16010183-02MSD Units: mg/L Analysis Date: 08-Jan-2016 20:33



Value %RECControl

LimitRPD Ref


MSD

Client ID:

>nC12 to nC28 24.53 24.45 0 100 75 - 125 23.07 6.13 200.49






Page 45 of 71

Client:Project:



QC BATCH REPORT


Sample ID: MBLK-100405 Units: mg/Kg Analysis Date: 08-Jan-2016 18:07



Value %RECControl

LimitRPD Ref


MBLK

Client ID:

>nC12 to nC28 U 50

>nC28 to nC35 U 50




Sample ID: LCS-100405 Units: mg/Kg Analysis Date: 08-Jan-2016 18:36



Value %RECControl

LimitRPD Ref


LCS

Client ID:

>nC12 to nC28 245.6 250 0 98.2 75 - 12550



Sample ID: LCSD-100405 Units: mg/Kg Analysis Date: 08-Jan-2016 19:06



Value %RECControl

LimitRPD Ref


LCSD

Client ID:

>nC12 to nC28 237.8 250 0 95.1 75 - 125 245.6 3.23 2050



Sample ID: HS16010148-02MS Units: mg/Kg Analysis Date: 08-Jan-2016 20:04



Value %RECControl

LimitRPD Ref


MS

Client ID:

>nC12 to nC28 284.7 248.5 0 115 75 - 12550





Page 46 of 71

Client:Project:



QC BATCH REPORT


Sample ID: HS16010148-02MSD Units: mg/Kg Analysis Date: 08-Jan-2016 20:33



Value %RECControl

LimitRPD Ref


MSD

Client ID:

>nC12 to nC28 236.8 247.8 0 95.6 75 - 125 284.7 18.4 2050



The following samples were anayzed in this batch: HS16010118-01 HS16010118-02 HS16010118-03



Page 47 of 71

Client:Project:



QC BATCH REPORT



Run ID: ICPMS04_267378 SeqNo: 3547835 PrepDate: 07-Jan-2016 DF: 1


Value %RECControl

LimitRPD Ref


MBLK

Client ID:

Arsenic U 0.500

Barium U 0.500

Cobalt U 0.500

Copper U 0.200

Lead U 0.500

Manganese U 0.500

Nickel U 0.500

Selenium U 0.500

Vanadium U 0.500

Zinc U 0.500

Sample ID: MLCS-100371 Units: mg/Kg Analysis Date: 08-Jan-2016 16:05



Value %RECControl

LimitRPD Ref


LCS

Client ID:

Arsenic 8.853 10 0 88.5 80 - 1200.500

Barium 9.162 10 0 91.6 80 - 1200.500

Cobalt 8.762 10 0 87.6 80 - 1200.500

Copper 8.759 10 0 87.6 80 - 1200.200

Lead 9.028 10 0 90.3 80 - 1200.500

Manganese 8.864 10 0 88.6 80 - 1200.500

Nickel 9.069 10 0 90.7 80 - 1200.500

Selenium 8.705 10 0 87.0 80 - 1200.500

Vanadium 8.714 10 0 87.1 80 - 1200.500

Zinc 8.946 10 0 89.5 80 - 1200.500



Page 48 of 71

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MS


Arsenic 9.353 9.413 0.8961 89.8 75 - 1250.471

Barium 16.1 9.413 5.595 112 75 - 1250.471

Cobalt 9.004 9.413 0.4683 90.7 75 - 1250.471

Copper 11.21 9.413 2.222 95.5 75 - 1250.188

Lead 13.39 9.413 3.728 103 75 - 1250.471

Manganese 21.38 9.413 7.592 147 75 - 125 S 0.471

Nickel 11.17 9.413 1.511 103 75 - 1250.471

Selenium 7.997 9.413 0.2664 82.1 75 - 1250.471

Vanadium 21.61 9.413 6.981 155 75 - 125 S 0.471

Zinc 14.61 9.413 3.165 122 75 - 1250.471




Value %RECControl

LimitRPD Ref


MSD


Arsenic 9.194 9.363 0.8961 88.6 75 - 125 9.353 1.71 200.468

Barium 16.15 9.363 5.595 113 75 - 125 16.1 0.284 200.468

Cobalt 9.009 9.363 0.4683 91.2 75 - 125 9.004 0.0611 200.468

Copper 11.08 9.363 2.222 94.6 75 - 125 11.21 1.14 200.187

Lead 13.39 9.363 3.728 103 75 - 125 13.39 0.0223 200.468

Manganese 20.72 9.363 7.592 140 75 - 125 21.38 3.17 20 S 0.468

Nickel 11.02 9.363 1.511 102 75 - 125 11.17 1.37 200.468

Selenium 8.076 9.363 0.2664 83.4 75 - 125 7.997 0.984 200.468

Vanadium 19.56 9.363 6.981 134 75 - 125 21.61 9.96 20 S 0.468

Zinc 15.44 9.363 3.165 131 75 - 125 14.61 5.51 20 S 0.468



Page 49 of 71

Client:Project:



QC BATCH REPORT


Sample ID: HS16010118-04BS Units: mg/Kg Analysis Date: 08-Jan-2016 16:27



Value %RECControl

LimitRPD Ref


PDS


Arsenic 9.38 9.188 0.8961 92.3 75 - 1250.459

Barium 14.22 9.188 5.595 93.9 75 - 1250.459

Cobalt 8.483 9.188 0.4683 87.2 75 - 1250.459

Copper 10.3 9.188 2.222 87.9 75 - 1250.184

Lead 12.43 9.188 3.728 94.8 75 - 1250.459

Manganese 15.66 9.188 7.592 87.9 75 - 1250.459

Nickel 9.881 9.188 1.511 91.1 75 - 1250.459

Selenium 8.683 9.188 0.2664 91.6 75 - 1250.459

Vanadium 15.01 9.188 6.981 87.4 75 - 1250.459

Zinc 11.44 9.188 3.165 90.1 75 - 1250.459

Sample ID: HS16010118-04 DIL SX Units: mg/Kg Analysis Date: 08-Jan-2016 16:14



Value %RECControl

LimitRPD Ref


SD


Arsenic 0.9685 0.8961 0 10 J 2.30

Barium 5.812 5.595 3.89 102.30

Cobalt 0.4948 0.4683 0 10 J 2.30

Copper 2.419 2.222 8.85 100.919

Lead 3.961 3.728 6.24 102.30

Manganese 7.871 7.592 3.67 102.30

Nickel 1.568 1.511 0 10 J 2.30

Selenium U 0.2664 0 102.30

Vanadium 7.442 6.981 6.62 102.30

Zinc 3.169 3.165 0.136 102.30

The following samples were anayzed in this batch: HS16010118-04 HS16010118-05 HS16010118-06 HS16010118-07 HS16010118-08 HS16010118-10 HS16010118-11 HS16010118-14 HS16010118-15 HS16010118-16 HS16010118-17 HS16010118-18



Page 50 of 71

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MBLK

Client ID:

Arsenic U 0.00500

Barium U 0.00500

Cobalt U 0.00500

Copper U 0.00200

Lead U 0.00500

Manganese U 0.00500

Nickel U 0.00500

Selenium U 0.00500

Vanadium U 0.00500

Zinc U 0.00500

Sample ID: MLCS-100438 Units: mg/L Analysis Date: 12-Jan-2016 11:33



Value %RECControl

LimitRPD Ref


LCS

Client ID:

Arsenic 0.04454 0.05 0 89.1 80 - 1200.00500

Barium 0.04918 0.05 0 98.4 80 - 1200.00500

Cobalt 0.04663 0.05 0 93.3 80 - 1200.00500

Copper 0.0466 0.05 0 93.2 80 - 1200.00200

Lead 0.04799 0.05 0 96.0 80 - 1200.00500

Manganese 0.04594 0.05 0 91.9 80 - 1200.00500

Nickel 0.04753 0.05 0 95.1 80 - 1200.00500

Selenium 0.04409 0.05 0 88.2 80 - 1200.00500

Vanadium 0.04559 0.05 0 91.2 80 - 1200.00500

Zinc 0.05021 0.05 0 100 80 - 1200.00500



Page 51 of 71

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MS

Client ID:

Arsenic 0.04928 0.05 0.001746 95.1 80 - 1200.00500

Barium 0.1014 0.05 0.05248 97.9 80 - 1200.00500

Cobalt 0.04665 0.05 0.000083 93.1 80 - 1200.00500

Copper 0.04574 0.05 -0.000065 91.6 80 - 1200.00200

Lead 0.05001 0.05 0.000009 100.0 80 - 1200.00500

Manganese 0.1501 0.05 0.105 90.1 80 - 1200.00500

Nickel 0.04588 0.05 0.000661 90.4 80 - 1200.00500

Selenium 0.04684 0.05 0.000457 92.8 80 - 1200.00500

Vanadium 0.04827 0.05 0.001164 94.2 80 - 1200.00500

Zinc 0.04771 0.05 0.002046 91.3 80 - 1200.00500




Value %RECControl

LimitRPD Ref


MSD

Client ID:

Arsenic 0.04906 0.05 0.001746 94.6 80 - 120 0.04928 0.445 200.00500

Barium 0.1027 0.05 0.05248 100 80 - 120 0.1014 1.22 200.00500

Cobalt 0.04633 0.05 0.000083 92.5 80 - 120 0.04665 0.678 200.00500

Copper 0.04618 0.05 -0.000065 92.5 80 - 120 0.04574 0.949 200.00200

Lead 0.0493 0.05 0.000009 98.6 80 - 120 0.05001 1.43 200.00500

Manganese 0.1547 0.05 0.105 99.4 80 - 120 0.1501 3.05 200.00500

Nickel 0.04618 0.05 0.000661 91.0 80 - 120 0.04588 0.643 200.00500

Selenium 0.04816 0.05 0.000457 95.4 80 - 120 0.04684 2.79 200.00500

Vanadium 0.04905 0.05 0.001164 95.8 80 - 120 0.04827 1.6 200.00500

Zinc 0.0504 0.05 0.002046 96.7 80 - 120 0.04771 5.48 200.00500



Page 52 of 71

Client:Project:



QC BATCH REPORT


Sample ID: HS16010117-07BS Units: mg/L Analysis Date: 12-Jan-2016 11:54



Value %RECControl

LimitRPD Ref


PDS

Client ID:

Arsenic 0.1005 0.1 0.001746 98.7 75 - 1250.00500

Barium 0.1556 0.1 0.05248 103 75 - 1250.00500

Cobalt 0.09472 0.1 0.000083 94.6 75 - 1250.00500

Copper 0.09461 0.1 -0.000065 94.7 75 - 1250.00200

Lead 0.1022 0.1 0.000009 102 75 - 1250.00500

Manganese 0.2 0.1 0.105 94.9 75 - 1250.00500

Nickel 0.09309 0.1 0.000661 92.4 75 - 1250.00500

Selenium 0.09694 0.1 0.000457 96.5 75 - 1250.00500

Vanadium 0.09911 0.1 0.001164 97.9 75 - 1250.00500

Zinc 0.1012 0.1 0.002046 99.1 75 - 1250.00500

Sample ID: HS16010117-07 DIL SX Units: mg/L Analysis Date: 12-Jan-2016 11:45



Value %RECControl

LimitRPD Ref


SD

Client ID:

Arsenic U 0.001746 0 100.0250

Barium 0.05184 0.05248 1.2 100.0250

Cobalt U 0.000083 0 100.0250

Copper U -0.000065 0 100.0100

Lead U 0.000009 0 100.0250

Manganese 0.1093 0.105 4.02 100.0250

Nickel U 0.000661 0 100.0250

Selenium U 0.000457 0 100.0250

Vanadium U 0.001164 0 100.0250

Zinc U 0.002046 0 100.0250




Page 53 of 71

Client:Project:



QC BATCH REPORT


Sample ID: MBLK-100366 Units: ug/L Analysis Date: 07-Jan-2016 14:41

Run ID: SV-7_267386 SeqNo: 3546943 PrepDate: 07-Jan-2016 DF: 1


Value %RECControl

LimitRPD Ref


MBLK

Client ID:





4.399 5 0 88.0 40 - 1350.20Surr: 4-Terphenyl-d14


3.783 5 0 75.7 20 - 1200.20Surr: Phenol-d6

Sample ID: LCS-100366 Units: ug/L Analysis Date: 07-Jan-2016 13:24



Value %RECControl

LimitRPD Ref


LCS

Client ID:

Benzo(a)pyrene 4.379 5 0 87.6 45 - 1200.10

5.531 5 0 111 34 - 1290.20Surr: 2,4,6-Tribromophenol



3.917 5 0 78.3 40 - 1350.20Surr: 4-Terphenyl-d14


3.625 5 0 72.5 20 - 1200.20Surr: Phenol-d6

Sample ID: LCSD-100366 Units: ug/L Analysis Date: 07-Jan-2016 13:43



Value %RECControl

LimitRPD Ref


LCSD

Client ID:

Benzo(a)pyrene 4.481 5 0 89.6 45 - 120 4.379 2.29 200.10

5.555 5 0 111 34 - 129 5.531 0.428 200.20Surr: 2,4,6-Tribromophenol


4.503 5 0 90.1 20 - 120 3.273 31.6 20 R 0.20Surr: 2-Fluorophenol

4.094 5 0 81.9 40 - 135 3.917 4.44 200.20Surr: 4-Terphenyl-d14


4.322 5 0 86.4 20 - 120 3.625 17.5 200.20Surr: Phenol-d6



Page 54 of 71

Client:Project:



QC BATCH REPORT


Sample ID: HS16010117-07MS Units: ug/L Analysis Date: 07-Jan-2016 16:40



Value %RECControl

LimitRPD Ref


MS

Client ID:

Benzo(a)pyrene 4.399 5 0 88.0 45 - 1200.10




3.783 5 0 75.7 40 - 1350.20Surr: 4-Terphenyl-d14


3.085 5 0 61.7 20 - 1200.20Surr: Phenol-d6




Value %RECControl

LimitRPD Ref


MS

Client ID:

Benzo(a)pyrene 4.233 5 0 84.7 45 - 1200.10




3.686 5 0 73.7 40 - 1350.20Surr: 4-Terphenyl-d14


3.535 5 0 70.7 20 - 1200.20Surr: Phenol-d6

Sample ID: HS16010117-07MSD Units: ug/L Analysis Date: 07-Jan-2016 16:59



Value %RECControl

LimitRPD Ref


MSD

Client ID:

Benzo(a)pyrene 4.377 5 0 87.5 45 - 120 4.399 0.507 200.10




3.637 5 0 72.7 40 - 135 3.783 3.94 200.20Surr: 4-Terphenyl-d14


2.943 5 0 58.9 20 - 120 3.085 4.72 200.20Surr: Phenol-d6



Page 55 of 71

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MSD

Client ID:

Benzo(a)pyrene 4.344 5 0 86.9 45 - 120 4.233 2.57 200.10



2.133 5 0 42.7 20 - 120 2.888 30.1 20 R 0.20Surr: 2-Fluorophenol

3.648 5 0 73.0 40 - 135 3.686 1.02 200.20Surr: 4-Terphenyl-d14


3.422 5 0 68.4 20 - 120 3.535 3.25 200.20Surr: Phenol-d6




Page 56 of 71

Client:Project:



QC BATCH REPORT


Sample ID: MBLK-100374 Units: ug/Kg Analysis Date: 07-Jan-2016 14:03



Value %RECControl

LimitRPD Ref


MBLK

Client ID:





144.7 167 0 86.6 32 - 1250Surr: 4-Terphenyl-d14


159.2 167 0 95.3 40 - 1250Surr: Phenol-d6

Sample ID: LCS-100374 Units: ug/Kg Analysis Date: 07-Jan-2016 15:01



Value %RECControl

LimitRPD Ref


LCS

Client ID:

Benzo(a)pyrene 158.1 167 0 94.6 50 - 1303.3




134.2 167 0 80.4 32 - 1250Surr: 4-Terphenyl-d14


125.1 167 0 74.9 40 - 1250Surr: Phenol-d6

Sample ID: HS16010118-15MS Units: ug/Kg Analysis Date: 07-Jan-2016 18:00



Value %RECControl

LimitRPD Ref


MS


Benzo(a)pyrene 178.7 166.7 3.788 105 50 - 1303.3

180.1 166.7 0 108 36 - 1260Surr: 2,4,6-Tribromophenol

112 166.7 0 67.2 43 - 1250Surr: 2-Fluorobiphenyl


139.3 166.7 0 83.6 32 - 1250Surr: 4-Terphenyl-d14


104.6 166.7 0 62.7 40 - 1250Surr: Phenol-d6



Page 57 of 71

Client:Project:



QC BATCH REPORT


Sample ID: HS16010118-15MSD Units: ug/Kg Analysis Date: 07-Jan-2016 18:20



Value %RECControl

LimitRPD Ref


MSD


Benzo(a)pyrene 192.9 166.8 3.788 113 50 - 130 178.7 7.67 303.3

183.8 166.8 0 110 36 - 126 180.1 2.05 300Surr: 2,4,6-Tribromophenol

119.3 166.8 0 71.5 43 - 125 112 6.24 300Surr: 2-Fluorobiphenyl


137.9 166.8 0 82.7 32 - 125 139.3 1.05 300Surr: 4-Terphenyl-d14


122.2 166.8 0 73.2 40 - 125 104.6 15.5 300Surr: Phenol-d6




Page 58 of 71

Client:Project:



QC BATCH REPORT


Sample ID: VBLKS1-010716 Units: ug/Kg Analysis Date: 07-Jan-2016 09:36



Value %RECControl

LimitRPD Ref


MBLK

Client ID:






50.26 50 0 101 73 - 1270Surr: Toluene-d8

Sample ID: VLCSS1-010716 Units: ug/Kg Analysis Date: 07-Jan-2016 08:25



Value %RECControl

LimitRPD Ref


LCS

Client ID:

1,1-Dichloroethane 51 50 0 102 75 - 1245.0





49.14 50 0 98.3 73 - 1270Surr: Toluene-d8




Value %RECControl

LimitRPD Ref


MS

Client ID:

1,1-Dichloroethane 42.82 48.5 0 88.3 75 - 1244.8



45.46 48.5 0 93.7 73 - 1260Surr: 4-Bromofluorobenzene


47.04 48.5 0 97.0 73 - 1270Surr: Toluene-d8



Page 59 of 71

Client:Project:



QC BATCH REPORT


Sample ID: HS16010093-02MSD Units: ug/Kg Analysis Date: 07-Jan-2016 13:29



Value %RECControl

LimitRPD Ref


MSD

Client ID:

1,1-Dichloroethane 44.89 48.5 0 92.5 75 - 124 42.82 4.71 304.8


43.66 48.5 0 90.0 70 - 128 43.32 0.775 300Surr: 1,2-Dichloroethane-d4

45.76 48.5 0 94.4 73 - 126 45.46 0.676 300Surr: 4-Bromofluorobenzene


48 48.5 0 99.0 73 - 127 47.04 2.02 300Surr: Toluene-d8




Page 60 of 71

Client:Project:



QC BATCH REPORT


Sample ID: VBLKW-160107 Units: ug/L Analysis Date: 07-Jan-2016 11:04



Value %RECControl

LimitRPD Ref


MBLK

Client ID:






54.85 50 0 110 75 - 1251.0Surr: Toluene-d8

Sample ID: VLCSW-160107 Units: ug/L Analysis Date: 07-Jan-2016 10:14



Value %RECControl

LimitRPD Ref


LCS

Client ID:

1,1-Dichloroethane 46.97 50 0 93.9 76 - 1201.0





53.91 50 0 108 75 - 1251.0Surr: Toluene-d8




Value %RECControl

LimitRPD Ref


MS

Client ID:

1,1-Dichloroethane 44.8 50 0 89.6 76 - 1201.0





54.17 50 0 108 75 - 1251.0Surr: Toluene-d8



Page 61 of 71

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MSD

Client ID:

1,1-Dichloroethane 44.15 50 0 88.3 76 - 120 44.8 1.47 201.0


46.27 50 0 92.5 71 - 125 45.61 1.44 201.0Surr: 1,2-Dichloroethane-d4


48.17 50 0 96.3 74 - 125 48.26 0.191 201.0Surr: Dibromofluoromethane

53.63 50 0 107 75 - 125 54.17 1 201.0Surr: Toluene-d8




Page 62 of 71

Client:Project:



QC BATCH REPORT


Sample ID: HS16010118-07DUP Units: wt% Analysis Date: 07-Jan-2016 15:29



Value %RECControl

LimitRPD Ref


DUP






Page 63 of 71

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


DUP

Client ID:


The following samples were anayzed in this batch: HS16010118-08 HS16010118-10 HS16010118-11 HS16010118-12 HS16010118-13 HS16010118-14 HS16010118-15 HS16010118-16 HS16010118-17 HS16010118-18



Page 64 of 71

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


DUP

Client ID:





Page 65 of 71





a Not accredited

















MBLK Method Blank



MS Matrix Spike




SD Serial Dilution






Page 66 of 71



Arkansas 15-024-0 27-Mar-2016



Kentucky KY 2015-2016 30-Apr-2016

Louisiana 03087 2015/2016 30-Jun-2016



Oklahoma 2015-047 31-Aug-2016

Texas T104704231-15-15 30-Apr-2016


Page 67 of 71


Work Order: HS16010118Project: CES Griggs Road Phase II SAMPLE TRACKING


HS16010118-01 4904-SB02A-02 Login 1/6/2016 6:59:20 PM BHH LF-23

HS16010118-02 4904-SB25-01.5 Login 1/6/2016 6:59:20 PM BHH LF-23

HS16010118-03 4904-SB25-04 Login 1/6/2016 6:59:20 PM BHH LF-23

HS16010118-04 4904-SB26-23 Login 1/6/2016 6:59:20 PM BHH 2D

HS16010118-04 4904-SB26-23 Login 1/6/2016 6:59:20 PM BHH 5035





HS16010118-09 EB 010516 Login 1/6/2016 6:59:20 PM BHH 4B

HS16010118-09 EB 010516 Login 1/6/2016 6:59:20 PM BHH VW-3

HS16010118-09 EB 010516 Login 1/6/2016 6:59:20 PM BHH TPH C1





HS16010118-14 5910-SB10-02.5 Login 1/6/2016 6:59:20 PM BHH 2D





HS16010118-17 5910-SB12-01 DUP Login 1/6/2016 6:59:20 PM BHH 2D


HS16010118-19 EB 010616 Login 1/6/2016 6:59:20 PM BHH 17F

HS16010118-19 EB 010616 Login 1/6/2016 6:59:20 PM BHH 4B

HS16010118-20 TB 010616 Login 1/6/2016 6:59:20 PM BHH VW-3

HS16010118-04 4904-SB26-23 Return 1/7/2016 1:40:42 PM HAS 2D







HS16010118-14 5910-SB10-02.5 Return 1/7/2016 1:40:42 PM HAS 2D

HS16010118-15 5910-SB11-02.5 Return 1/7/2016 1:40:42 PM HAS 2D


HS16010118-17 5910-SB12-01 DUP Return 1/7/2016 1:40:42 PM HAS 2D



Page 68 of 71

CGG

06-Jan-2016 18:10Date/Time Received:

HS16010118

PBW - Houston

Work Order:

Client Name:


Received by:













Cooler(s)/Kit(s):




pH adjusted?

pH adjusted by:

Login Notes:

No Not Present

Yes No Not Present

Yes No Not Present

Yes No

Yes No

Yes No

Yes No

Yes No

Yes No

Yes No

Yes No

2.8c / 3.0c u/c IR#42467201/06/2016 19:20


Yes No N/A

Yes No N/A

Sample 4904-SB26-23 received an extra jar.

Checklist completed by: Baudelio HernandezDateeSignatureDateeSignature

8-Jan-20166-Jan-2016

ClientWater, Soil Carrier name:Matrices:




Comments:

Corrective Action:

0

Yes



Page 69 of 71

Page 70 of 71

Page 71 of 71

January 25, 2016





Sincerely,



Dear Brenda,


Generated By: Dane.Wacasey

Dane J. Wacasey


Page 1 of 42


WorkOrder:














ALS Group USA, Corp Date: 25-Jan-16

Page 2 of 42


WorkOrder:


Dane J. Wacasey




Page 3 of 42


Laboratory Name: ALS Laboratory Group LRC Date: 01/18/2016 Project Name: CES Griggs Rd VCP Laboratory Job Number: cccc

Reviewer Name: Dane Wacasey Prep Batch Number(s): 100404,100405,100410,100425,100456,100463,R267450









Were surrogate percent recoveries in all samples within the laboratory QC limits? X 1







Was the LCSD RPD within QC limits? X R7 OI Matrix spike (MS) and matrix spike duplicate (MSD) data Were the project/method specified analytes included in the MS and MSD? X Were MS/MSD analyzed at the appropriate frequency? X 2 Were MS (and MSD, if applicable) %Rs within the laboratory QC limits? X 3 Were MS/MSD RPDs within laboratory QC limits? X 4 R8 OI Analytical duplicate data Were appropriate analytical duplicates analyzed for each matrix? X Were analytical duplicates analyzed at the appropriate frequency? X Were RPDs or relative standard deviations within the laboratory QC limits? X R9 OI Method quantitation limits (MQLs): Are the MQLs for each method analyte included in the laboratory data package? X







Page 4 of 42

Laboratory Review Checklist: Reportable Data Laboratory Name: ALS Laboratory Group LRC Date: 01/18/2016 Project Name: CES Griggs Rd VCP Laboratory Job Number: cccc

























Page 5 of 42


Laboratory Name: ALS Laboratory Group LRC Date: 01/18/2016 Project Name: CES Griggs Rd VCP Laboratory Job Number: cccc


ER#5 Description

1

Texas TPH by TX1005, sample EB 010715, surrogates recovered above the upper control limits. No target analytes were detected in the sample. The high surrogate recoveries did not impact the non-detect results for target analytes.

2

Batch 100425, Semivolatile Organics Method SW8270, Insufficient sample to perform MS/MSD. LCS/LCSD provided as batch quality control.

3

Batch 100456, Metals Method SW6020, sample HS16010167-02, MS and MSD were performed on unrelated sample. Batch 100463, Metals Method SW6020, sample 5910-SB4A-15, MS and MSD recovered outside the control limits for Manganese, however, the result in the parent sample is greater than 4x the spike amount.

4

Batch 100463, Metals Method SW6020, sample 5910-SB4A-15, MSD RPD criterion was exceeded for Manganese. Batch 100410, Semivolatile Organics Method SW8270, sample 5910-SB4A-15, MSD RPD criterion was exceeded for Phenol. Individual recoveries were within criteria.

5

See Form 13 Run Log and CCB Exceptions report.


Page 6 of 42







ICPMS05


FileIDICV 1 13-Jan-2016

10:02CO MN NI V010_ICV.d

LLICV5 1 13-Jan-2016 10:05

CO MN NI V011LICV.d

LLICV2 1 13-Jan-2016 10:08

CO MN NI V012SMPL.d

ICB 1 13-Jan-2016 10:11

CO MN NI V013_ICB.d

ICV 1 13-Jan-2016 10:13

CO MN NI V014_ICV.d

ICSA 1 13-Jan-2016 10:17

CO MN NI V015ICSA.d

ICSAB 1 13-Jan-2016 10:20

CO MN NI V016ICSB.d

CCV 1 1 13-Jan-2016 10:40

CO MN NI V023_CCV.d

CCB 1 1 13-Jan-2016 10:43

CO MN NI V024_CCB.d

CCV 2 1 13-Jan-2016 11:16

CO MN NI V035_CCV.d

CCB 2 1 13-Jan-2016 11:19

CO MN NI V036_CCB.d

MBLK-100456 1 13-Jan-2016 11:49

CO MN NI V046SMPL.d

CCV 3 1 13-Jan-2016 11:52

CO MN NI V047_CCV.d

CCB 3 1 13-Jan-2016 11:55

CO MN NI V048_CCB.d

MLCS-100456 1 13-Jan-2016 11:58

CO MN NI V049SMPL.d

ZZZZZZSD 5 13-Jan-2016 12:10

CO MN NI V053SMPL.d

ZZZZZZMS 1 13-Jan-2016 12:13

CO MN NI V054SMPL.d

ZZZZZZMSD 1 13-Jan-2016 12:16

CO MN NI V055SMPL.d

ZZZZZZPDS 1 13-Jan-2016 12:19

CO MN NI V056SMPL.d

CCV 4 1 13-Jan-2016 12:28

CO MN NI V059_CCV.d

CCB 4 1 13-Jan-2016 12:31

CO MN NI V060_CCB.d

EB 010715 1 13-Jan-2016 12:55

CO MN NI V068SMPL.d

CCV 5 1 13-Jan-2016 13:04

CO MN NI V071_CCV.d

CCB 5 1 13-Jan-2016 13:08

CO MN NI V072_CCB.d

CCV 6 1 13-Jan-2016 13:48

CO MN NI V083_CCV.d

CCB 6 1 13-Jan-2016 13:51

CO MN NI V084_CCB.d

CCV 7 1 13-Jan-2016 13:54

CO MN NI V085_CCV.d

CCB 7 1 13-Jan-2016 13:57

CO MN NI V086_CCB.d

LLCCV5 1 13-Jan-2016 14:00

CO MN NI V087LICV.d

LLCCV2 1 13-Jan-2016 14:03

CO MN NI V088SMPL.d

ICSA 1 13-Jan-2016 14:06

CO MN NI V089ICSA.d

ICSAB 1 13-Jan-2016 14:09

CO MN NI V090ICSB.d

25-Jan-16Date: ALS Group USA, Corp

Page 7 of 42






ICPMS05


Units: ug/L

0.787 0.6 5Vanadium


Units: ug/L

1.05 0.6 5Vanadium


Units: ug/L

0.696 0.6 5Vanadium


Page 8 of 42

Client: PBW Houston



HS16010174-01 07-Jan-2016 09:35 07-Jan-2016 16:205910-SB4A-15 Soil

HS16010174-02 07-Jan-2016 10:50 07-Jan-2016 16:205910-SB14-01 Soil

HS16010174-03 07-Jan-2016 13:40 07-Jan-2016 16:204904-SB24-00 Soil

HS16010174-04 07-Jan-2016 13:50 07-Jan-2016 16:204904-SB24-04 Soil

HS16010174-05 07-Jan-2016 13:50 07-Jan-2016 16:204904-SB24-04 DUP Soil

HS16010174-06 07-Jan-2016 14:40 07-Jan-2016 16:20EB 010715 Water

ALS Group USA, Corp 25-Jan-16Date:

Page 9 of 42


PBW HoustonCES Griggs Rd VCP5910-SB4A-15

WorkOrder:Lab ID:

Collection Date:

HS16010174HS16010174-01


ANALYTICAL REPORT




1mg/Kg-dry 10-Jan-2016 14:130.0014Caprolactam 0.0077U

1mg/Kg-dry 10-Jan-2016 14:130.0013Phenol 0.0077U














Page 10 of 42



WorkOrder:Lab ID:

Collection Date:

HS16010174HS16010174-02


ANALYTICAL REPORT









Page 11 of 42



WorkOrder:Lab ID:

Collection Date:

HS16010174HS16010174-03


ANALYTICAL REPORT





1mg/Kg-dry 09-Jan-2016 06:14J 10>nC12 to nC28 5215

1mg/Kg-dry 09-Jan-2016 06:1410>nC28 to nC35 52U

1mg/Kg-dry 09-Jan-2016 06:14J 10Total Petroleum Hydrocarbon 5215.0





Page 12 of 42



WorkOrder:Lab ID:

Collection Date:

HS16010174HS16010174-04


ANALYTICAL REPORT












Page 13 of 42


PBW HoustonCES Griggs Rd VCP4904-SB24-04 DUP

WorkOrder:Lab ID:

Collection Date:

HS16010174HS16010174-05


ANALYTICAL REPORT












Page 14 of 42



WorkOrder:Lab ID:

Collection Date:

HS16010174HS16010174-06


ANALYTICAL REPORT




1mg/L 11-Jan-2016 23:220.000045Caprolactam 0.00020U

1mg/L 11-Jan-2016 23:220.000035Phenol 0.00020U








1mg/L 13-Jan-2016 12:550.000200Cobalt 0.00500U

1mg/L 13-Jan-2016 12:550.000700Manganese 0.00500U

1mg/L 13-Jan-2016 12:550.000600Nickel 0.00500U

1mg/L 13-Jan-2016 12:55J 0.000600Vanadium 0.005000.000906

LOW-LEVEL TEXAS TPH BY TX1005 Method:TX1005 Analyst: KHTPrep:TX1005PR / 08-Jan-2016

1mg/L 09-Jan-2016 05:160.20>nC12 to nC28 0.50U

1mg/L 09-Jan-2016 05:160.20>nC28 to nC35 0.50U

1mg/L 09-Jan-2016 05:160.20Total Petroleum Hydrocarbon 0.50U

Surr: 2-Fluorobiphenyl 1%REC 09-Jan-2016 05:16S148 70-130

Surr: Trifluoromethyl benzene 1%REC 09-Jan-2016 05:16S136 70-130



Page 15 of 42

WEIGHT LOG





Final Volume

Prep Factor

HS16010174-06 1 30.03 3 (mL) 0.0999



Final Volume

Prep Factor

HS16010174-03 1 12.03 10 (mL) 0.8313HS16010174-04 1 12.61 10 (mL) 0.793HS16010174-05 1 12.9 10 (mL) 0.7752



Final Volume

Prep Factor

HS16010174-01 1 30.05 1 (mL) 0.03328



Final Volume

Prep Factor

HS16010174-06 1 1000 1 (mL) 0.001



Final Volume

Prep Factor

HS16010174-06 1 50 50 (mL) 1



Final Volume

Prep Factor

HS16010174-01 1 0.5324 50 (mL) 93.91HS16010174-02 1 0.5122 50 (mL) 97.62


Page 16 of 42


WorkOrder:Project:



Batch ID 100404 Test Name : LOW-LEVEL TEXAS TPH BY TX1005 Matrix: Water

08 Jan 2016 11:31 09 Jan 2016 05:16HS16010174-06 07 Jan 2016 14:40 1EB 010715


08 Jan 2016 11:38 09 Jan 2016 06:14HS16010174-03 07 Jan 2016 13:40 14904-SB24-00

08 Jan 2016 11:38 09 Jan 2016 06:43HS16010174-04 07 Jan 2016 13:50 14904-SB24-04

08 Jan 2016 11:38 09 Jan 2016 07:11HS16010174-05 07 Jan 2016 13:50 14904-SB24-04 DUP


08 Jan 2016 09:57 10 Jan 2016 14:13HS16010174-01 07 Jan 2016 09:35 15910-SB4A-15


11 Jan 2016 07:37 11 Jan 2016 23:22HS16010174-06 07 Jan 2016 14:40 1EB 010715


12 Jan 2016 09:27 13 Jan 2016 12:55HS16010174-06 07 Jan 2016 14:40 1EB 010715


12 Jan 2016 12:21 13 Jan 2016 13:00HS16010174-01 07 Jan 2016 09:35 105910-SB4A-15

12 Jan 2016 12:21 13 Jan 2016 00:44HS16010174-01 07 Jan 2016 09:35 15910-SB4A-15

12 Jan 2016 12:21 13 Jan 2016 13:13HS16010174-02 07 Jan 2016 10:50 105910-SB14-01

12 Jan 2016 12:21 13 Jan 2016 01:06HS16010174-02 07 Jan 2016 10:50 15910-SB14-01


08 Jan 2016 11:08HS16010174-01 07 Jan 2016 09:35 15910-SB4A-15

08 Jan 2016 11:08HS16010174-02 07 Jan 2016 10:50 15910-SB14-01

08 Jan 2016 11:08HS16010174-03 07 Jan 2016 13:40 14904-SB24-00

08 Jan 2016 11:08HS16010174-04 07 Jan 2016 13:50 14904-SB24-04

08 Jan 2016 11:08HS16010174-05 07 Jan 2016 13:50 14904-SB24-04 DUP


Page 17 of 42






Units: mg/Kg


A 22TPH-1005-3 10>nC28 to nC35 5025




Page 18 of 42






Units: mg/L

Type Analyte DCSCAS MDL PQLDCS SpikeA 0.98TPH-1005-2 0.20>nC12 to nC28 0.500.50

A 0.98TPH-1005-3 0.20>nC28 to nC35 0.500.50




Page 19 of 42






Units: mg/Kg

Type Analyte DCSCAS MDL PQLDCS SpikeA 0.1067440-48-4 0.0700Cobalt 0.5000.100

A 0.1107439-96-5 0.100Manganese 0.5000.100

A 0.09357440-02-0 0.0900Nickel 0.5000.100

A 0.3277440-62-2 0.230Vanadium 0.5000.250

Page 20 of 42






Units: mg/L


A 0.0008757439-96-5 0.000700Manganese 0.005000.00100

A 0.0006887440-02-0 0.000600Nickel 0.005000.00100

A 0.0007707440-62-2 0.000600Vanadium 0.005000.00100

Page 21 of 42






Units: mg/Kg

Type Analyte DCSCAS MDL PQLDCS SpikeA 0.0031105-60-2 0.0012Caprolactam 0.00660.0033

A 0.0038108-95-2 0.0011Phenol 0.00660.0033




S 01718-51-0 04-Terphenyl-d14 00


S 013127-88-3 0Phenol-d6 00

Page 22 of 42






Units: mg/L

Type Analyte DCSCAS MDL PQLDCS SpikeA 0.000054105-60-2 0.000045Caprolactam 0.000200.00010

A 0.00011108-95-2 0.000035Phenol 0.000200.00010



S 0367-12-4 02-Fluorophenol 0.000200

S 01718-51-0 04-Terphenyl-d14 0.000200

S 04165-60-0 0Nitrobenzene-d5 0.000200

S 013127-88-3 0Phenol-d6 0.000200

Page 23 of 42






Units: wt%


Page 24 of 42

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MBLK

Client ID:

>nC12 to nC28 U 0.50

>nC28 to nC35 U 0.50




Sample ID: LCS-100404 Units: mg/L Analysis Date: 08-Jan-2016 18:36



Value %RECControl

LimitRPD Ref


LCS

Client ID:

>nC12 to nC28 24.39 25 0 97.6 75 - 1250.50



Sample ID: LCSD-100404 Units: mg/L Analysis Date: 08-Jan-2016 19:06



Value %RECControl

LimitRPD Ref


LCSD

Client ID:

>nC12 to nC28 23.34 25 0 93.3 75 - 125 24.39 4.42 200.50






Value %RECControl

LimitRPD Ref


MS

Client ID:

>nC12 to nC28 23.07 24.95 0 92.5 75 - 1250.50





Page 25 of 42

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MSD

Client ID:

>nC12 to nC28 24.53 24.45 0 100 75 - 125 23.07 6.13 200.49






Page 26 of 42

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MBLK

Client ID:

>nC12 to nC28 U 50

>nC28 to nC35 U 50




Sample ID: LCS-100405 Units: mg/Kg Analysis Date: 08-Jan-2016 18:36



Value %RECControl

LimitRPD Ref


LCS

Client ID:

>nC12 to nC28 245.6 250 0 98.2 75 - 12550



Sample ID: LCSD-100405 Units: mg/Kg Analysis Date: 08-Jan-2016 19:06



Value %RECControl

LimitRPD Ref


LCSD

Client ID:

>nC12 to nC28 237.8 250 0 95.1 75 - 125 245.6 3.23 2050






Value %RECControl

LimitRPD Ref


MS

Client ID:

>nC12 to nC28 284.7 248.5 0 115 75 - 12550





Page 27 of 42

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MSD

Client ID:

>nC12 to nC28 236.8 247.8 0 95.6 75 - 125 284.7 18.4 2050






Page 28 of 42

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MBLK

Client ID:

Cobalt U 0.00500

Manganese U 0.00500

Nickel U 0.00500

Vanadium U 0.00500

Sample ID: MLCS-100456 Units: mg/L Analysis Date: 13-Jan-2016 11:58



Value %RECControl

LimitRPD Ref


LCS

Client ID:

Cobalt 0.04701 0.05 0 94.0 80 - 1200.00500

Manganese 0.0464 0.05 0 92.8 80 - 1200.00500

Nickel 0.04603 0.05 0 92.1 80 - 1200.00500

Vanadium 0.04625 0.05 0 92.5 80 - 1200.00500




Value %RECControl

LimitRPD Ref


MS

Client ID:

Cobalt 0.04708 0.05 0.000929 92.3 80 - 1200.00500

Manganese 0.4134 0.05 0.372 82.8 80 - 120 O 0.00500

Nickel 0.04573 0.05 0.000525 90.4 80 - 1200.00500

Vanadium 0.05256 0.05 0.004418 96.3 80 - 1200.00500




Value %RECControl

LimitRPD Ref


MSD

Client ID:

Cobalt 0.04664 0.05 0.000929 91.4 80 - 120 0.04708 0.95 200.00500

Manganese 0.4068 0.05 0.372 69.7 80 - 120 0.4134 1.6 20 SO 0.00500

Nickel 0.0458 0.05 0.000525 90.6 80 - 120 0.04573 0.151 200.00500

Vanadium 0.05198 0.05 0.004418 95.1 80 - 120 0.05256 1.11 200.00500



Page 29 of 42

Client:Project:



QC BATCH REPORT


Sample ID: HS16010167-02BS Units: mg/L Analysis Date: 13-Jan-2016 12:19



Value %RECControl

LimitRPD Ref


PDS

Client ID:

Cobalt 0.08806 0.1 0.000929 87.1 75 - 1250.00500

Manganese 0.4569 0.1 0.372 85.0 75 - 1250.00500

Nickel 0.0852 0.1 0.000525 84.7 75 - 1250.00500

Vanadium 0.09571 0.1 0.004418 91.3 75 - 1250.00500

Sample ID: HS16010167-02 DIL SX Units: mg/L Analysis Date: 13-Jan-2016 12:10



Value %RECControl

LimitRPD Ref


SD

Client ID:

Cobalt U 0.000929 0 100.0250

Manganese 0.3803 0.372 2.23 100.0250

Nickel U 0.000525 0 100.0250

Vanadium 0.007442 0.004418 0 10 J 0.0250




Page 30 of 42

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MBLK

Client ID:

Cobalt U 0.500

Manganese U 0.500

Nickel U 0.500

Vanadium U 0.500




Value %RECControl

LimitRPD Ref


LCS

Client ID:

Cobalt 9.682 10 0 96.8 80 - 1200.500

Manganese 9.552 10 0 95.5 80 - 1200.500

Nickel 9.664 10 0 96.6 80 - 1200.500

Vanadium 9.507 10 0 95.1 80 - 1200.500




Value %RECControl

LimitRPD Ref


MS

Client ID: 5910-SB4A-15

Cobalt 11.41 9.569 2.579 92.3 75 - 1250.478

Manganese 460.6 9.569 666.2 -2150 75 - 125 SEO 0.478

Nickel 20.57 9.569 13.71 71.7 75 - 125 S 0.478

Vanadium 28.59 9.569 19.5 95.0 75 - 1250.478




Value %RECControl

LimitRPD Ref


MSD


Cobalt 11.42 9.527 2.579 92.8 75 - 125 11.41 0.144 200.476

Manganese 573.1 9.527 666.2 -977 75 - 125 460.6 21.8 20 SREO 0.476

Nickel 21.46 9.527 13.71 81.3 75 - 125 20.57 4.24 200.476

Vanadium 27.11 9.527 19.5 79.9 75 - 125 28.59 5.31 200.476



Page 31 of 42

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


PDS


Cobalt 10.84 9.391 2.579 88.0 75 - 1250.470

Nickel 21.3 9.391 13.71 80.8 75 - 1250.470

Vanadium 27.1 9.391 19.5 81.0 75 - 1250.470




Value %RECControl

LimitRPD Ref


PDS


Manganese 713.6 93.91 619.3 100 75 - 125 O 4.70




Value %RECControl

LimitRPD Ref


SD


Cobalt 2.72 2.579 5.45 102.35

Nickel 14.65 13.71 6.82 102.35

Vanadium 20.17 19.5 3.47 102.35




Value %RECControl

LimitRPD Ref


SD


Manganese 637.2 619.3 2.88 1023.5




Page 32 of 42

Client:Project:



QC BATCH REPORT


Sample ID: MBLK-100410 Units: ug/Kg Analysis Date: 10-Jan-2016 12:18



Value %RECControl

LimitRPD Ref


MBLK

Client ID:

Caprolactam U 6.6

Phenol U 6.6




146.5 167 0 87.8 32 - 1250Surr: 4-Terphenyl-d14


138.3 167 0 82.8 40 - 1250Surr: Phenol-d6

Sample ID: LCS-100410 Units: ug/Kg Analysis Date: 10-Jan-2016 12:37



Value %RECControl

LimitRPD Ref


LCS

Client ID:

Caprolactam 143.1 167 0 85.7 50 - 1356.6

Phenol 125.6 167 0 75.2 45 - 1306.6

175 167 0 105 36 - 1260Surr: 2,4,6-Tribromophenol


119 167 0 71.2 37 - 1250Surr: 2-Fluorophenol

136.9 167 0 82.0 32 - 1250Surr: 4-Terphenyl-d14


132.6 167 0 79.4 40 - 1250Surr: Phenol-d6




Value %RECControl

LimitRPD Ref


MS


Caprolactam 173.8 166.3 0 104 50 - 1356.6

Phenol 122.7 166.3 0 73.8 45 - 1306.6

193 166.3 0 116 36 - 1260Surr: 2,4,6-Tribromophenol



136.7 166.3 0 82.2 32 - 1250Surr: 4-Terphenyl-d14


115.3 166.3 0 69.3 40 - 1250Surr: Phenol-d6



Page 33 of 42

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MSD


Caprolactam 190.5 166.3 0 115 50 - 135 173.8 9.17 306.6

Phenol 86.91 166.3 0 52.3 45 - 130 122.7 34.1 30 R 6.6

198.9 166.3 0 120 36 - 126 193 3.02 300Surr: 2,4,6-Tribromophenol



152.8 166.3 0 91.9 32 - 125 136.7 11.1 300Surr: 4-Terphenyl-d14


135.1 166.3 0 81.2 40 - 125 115.3 15.8 300Surr: Phenol-d6




Page 34 of 42

Client:Project:



QC BATCH REPORT


Sample ID: MBLK-100425 Units: ug/L Analysis Date: 11-Jan-2016 16:58



Value %RECControl

LimitRPD Ref


MBLK

Client ID:

Caprolactam U 0.20

Phenol U 0.20




3.722 5 0 74.4 40 - 1350.20Surr: 4-Terphenyl-d14


3.58 5 0 71.6 20 - 1200.20Surr: Phenol-d6

Sample ID: LCS-100425 Units: ug/L Analysis Date: 11-Jan-2016 17:17



Value %RECControl

LimitRPD Ref


LCS

Client ID:

Caprolactam 4.001 5 0 80.0 35 - 1340.20

Phenol 3.418 5 0 68.4 20 - 1240.20




4.05 5 0 81.0 40 - 1350.20Surr: 4-Terphenyl-d14


5.142 5 0 103 20 - 1200.20Surr: Phenol-d6

Sample ID: LCSD-100425 Units: ug/L Analysis Date: 11-Jan-2016 17:37



Value %RECControl

LimitRPD Ref


LCSD

Client ID:

Caprolactam 4.27 5 0 85.4 35 - 134 4.001 6.49 200.20

Phenol 3.585 5 0 71.7 20 - 124 3.418 4.78 200.20

5.541 5 0 111 34 - 129 6.108 9.73 200.20Surr: 2,4,6-Tribromophenol



3.8 5 0 76.0 40 - 135 4.05 6.39 200.20Surr: 4-Terphenyl-d14


4.229 5 0 84.6 20 - 120 5.142 19.5 200.20Surr: Phenol-d6



Page 35 of 42

Client:Project:



QC BATCH REPORT





Page 36 of 42

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


DUP

Client ID:





Page 37 of 42





a Not accredited

















MBLK Method Blank



MS Matrix Spike




SD Serial Dilution






Page 38 of 42



Arkansas 15-024-0 27-Mar-2016



Kansas E-10352 2014-2015 31-Jan-2016

Kentucky KY 2015-2016 30-Apr-2016

Louisiana 03087 2015/2016 30-Jun-2016



Oklahoma 2015-047 31-Aug-2016

Texas T104704231-15-15 30-Apr-2016


Page 39 of 42

Client: PBW Houston



HS16010174-01 5910-SB4A-15 Login 1/7/2016 7:11:31 PM CGG 4D

HS16010174-01 5910-SB4A-15 Login 1/7/2016 7:11:31 PM CGG 4D

HS16010174-02 5910-SB14-01 Login 1/7/2016 7:11:31 PM CGG 4D

HS16010174-03 4904-SB24-00 Login 1/7/2016 7:11:31 PM CGG LF-23

HS16010174-04 4904-SB24-04 Login 1/7/2016 7:11:31 PM CGG LF-23

HS16010174-05 4904-SB24-04 DUP Login 1/7/2016 7:11:31 PM CGG LF-23

HS16010174-06 EB 010715 Login 1/7/2016 7:11:31 PM CGG 17F

HS16010174-06 EB 010715 Login 1/7/2016 7:11:31 PM CGG 4C

HS16010174-06 EB 010715 Login 1/7/2016 7:11:31 PM CGG TPH C1


Page 40 of 42

RPG


HS16010174

PBW - Houston

Work Order:

Client Name:


Received by:













Cooler(s)/Kit(s):




pH adjusted?

pH adjusted by:

Login Notes:

No Not Present

Yes No Not Present

Yes No Not Present

Yes No

Yes No

Yes No

Yes No

Yes No

Yes No

Yes No

Yes No

5.0c/5.2c uc/c IR#4419201/07/2016 19:45


Yes No N/A

Yes No N/A

Checklist completed by: Corey GranditsDateeSignatureDateeSignature

11-Jan-20167-Jan-2016

ClientSoil/Water Carrier name:Matrices:




Comments:

Corrective Action:

0

Yes



Page 41 of 42

Page 42 of 42

February 22, 2016





Sincerely,



Dear Brenda,



Dane J. Wacasey


Page 1 of 34


WorkOrder:

Pastor, Behling & Wheeler, LLCCES Griggs Rd VCPHS16010649














Page 2 of 34


WorkOrder:


Dane J. Wacasey




Page 3 of 34


Laboratory Name: ALS Laboratory Group LRC Date: 02/22/2016 Project Name: CES Griggs Rd VCP Laboratory Job Number: HS16020649 Reviewer Name: Dane Wacasey Prep Batch Number(s): 100805,98833,R268562,R269627 #1 A2 Description Yes No NA3 NR4 ER#5




Other than those results < MQL, were all other raw values bracketed by calibration standards? X 1











Was the LCSD RPD within QC limits? X R7 OI Matrix spike (MS) and matrix spike duplicate (MSD) data Were the project/method specified analytes included in the MS and MSD? X Were MS/MSD analyzed at the appropriate frequency? X Were MS (and MSD, if applicable) %Rs within the laboratory QC limits? X 2 Were MS/MSD RPDs within laboratory QC limits? X R8 OI Analytical duplicate data Were appropriate analytical duplicates analyzed for each matrix? X Were analytical duplicates analyzed at the appropriate frequency? X Were RPDs or relative standard deviations within the laboratory QC limits? X R9 OI Method quantitation limits (MQLs): Are the MQLs for each method analyte included in the laboratory data package? X







Page 4 of 34

Laboratory Review Checklist: Reportable Data Laboratory Name: ALS Laboratory Group LRC Date: 02/22/2016 Project Name: CES Griggs Rd VCP Laboratory Job Number: HS16020649 Reviewer Name: Dane Wacasey Prep Batch Number(s): 100805,98833,R268562,R269627 #1 A2 Description Yes No NA3 NR4 ER#5























Page 5 of 34


Laboratory Name: ALS Laboratory Group LRC Date: 02/22/2016 Project Name: CES Griggs Rd VCP Laboratory Job Number: HS16020649 Reviewer Name: Dane Wacasey Prep Batch Number(s): 100805,98833,R268562,R269627 ER#5 Description

1 Metals Method SW6020, sample 4904-SB17-22, Manganese value was above the calibration curve.

2

Batch 100805, Metals Method SW6020, sample HS16010716-24, MS and MSD were performed on unrelated sample. Batch 98833, Metals Method SW6020, sample HS15110353-06, MS and MSD were performed on unrelated sample.



Page 6 of 34





HS16010649CES Griggs Rd VCPPastor, Behling & Wheeler, LLC


ICPMS04


FileIDICV 1 11-Nov-2015

10:50CO CU MN NI PB SE009SMPL.D

LLICV5 1 11-Nov-2015 10:54

CO CU MN NI PB SE010SMPL.D

LLICV2 1 11-Nov-2015 10:59


ICB 1 11-Nov-2015 11:03

CO CU MN NI PB SE012CCB.D

ICSA 1 11-Nov-2015 11:09


ICSAB 1 11-Nov-2015 11:14


CCV 1 1 11-Nov-2015 12:04


CCB 1 1 11-Nov-2015 12:08


CCV 2 1 11-Nov-2015 12:57


CCB 2 1 11-Nov-2015 13:05


CCV 3 1 11-Nov-2015 13:54


CCB 3 1 11-Nov-2015 13:58


CCV 4 1 11-Nov-2015 14:31


CCB 4 1 11-Nov-2015 14:38


CCV 5 1 11-Nov-2015 15:28


CCB 5 1 11-Nov-2015 15:33


CCV 6 1 11-Nov-2015 16:17


CCB 6 1 11-Nov-2015 16:33


CCV 7 1 11-Nov-2015 17:12


CCB 7 1 11-Nov-2015 17:18


CCV 8 1 11-Nov-2015 18:02

CO CU MN NI PB SE102CCV.D

CCB 8 1 11-Nov-2015 18:19


ICCV 9 1 11-Nov-2015 18:54


LLCCV5 1 11-Nov-2015 18:58


LLCCV2 1 11-Nov-2015 19:03


ICCB 9 1 11-Nov-2015 19:07


CCV 10 1 11-Nov-2015 19:12


CCB 10 1 11-Nov-2015 19:16


CCV 11 1 11-Nov-2015 20:04


CCB 11 1 11-Nov-2015 20:09


MBLK-98833 1 11-Nov-2015 20:13

CO CU MN NI PB SE ZN132SMPL.D

MLCS-98833 1 11-Nov-2015 20:18

CO CU MN NI PB SE ZN133SMPL.D

CCV 12 1 11-Nov-2015 20:22



Page 7 of 34







ICPMS04



20:26CO CU MN NI PB SE135CCB.D

4904-SB17-22 1 11-Nov-2015 21:01


CCV 13 1 11-Nov-2015 21:05


CCB 13 1 11-Nov-2015 21:14


ICCV 14 1 11-Nov-2015 21:50


LLCCV5 1 11-Nov-2015 21:54


LLCCV2 1 11-Nov-2015 21:59


ICCB 14 1 11-Nov-2015 22:04


CCV 15 1 11-Nov-2015 22:08


CCB 15 1 11-Nov-2015 22:13


ICSA 1 11-Nov-2015 22:17


ICSAB 1 11-Nov-2015 22:22


CCV 16 1 11-Nov-2015 22:54


CCB 16 1 11-Nov-2015 22:59


ZZZZZZSD 5 11-Nov-2015 23:08

CU MN NI PB SE ZN171SMPL.D

ZZZZZZMS 1 11-Nov-2015 23:13


ZZZZZZMSD 1 11-Nov-2015 23:17


ZZZZZZPDS 1 11-Nov-2015 23:21


CCV 17 1 11-Nov-2015 23:30


CCB 17 1 11-Nov-2015 23:35


CCV 18 1 12-Nov-2015 00:07


CCB 18 1 12-Nov-2015 00:11


CCV 19 1 12-Nov-2015 00:25


CCB 19 1 12-Nov-2015 00:29


CCV 20 1 12-Nov-2015 01:05


CCB 20 1 12-Nov-2015 01:10


CCV 21 1 12-Nov-2015 01:55


CCB 21 1 12-Nov-2015 02:00


CCV 22 1 12-Nov-2015 02:18


CCB 22 1 12-Nov-2015 02:27


ICCV 23 1 12-Nov-2015 03:06


LLCCV5 1 12-Nov-2015 03:11


LLCCV2 1 12-Nov-2015 03:16



Page 8 of 34







ICPMS04


FileIDICCB 23 1 12-Nov-2015

03:21CO CU MN NI PB SE226SMPL.D

CCV 24 1 12-Nov-2015 03:26


CCB 24 1 12-Nov-2015 03:31


LLCCV2 1 12-Nov-2015 03:36


LLCCV5 1 12-Nov-2015 03:41


ICSA 1 12-Nov-2015 03:46


ICSAB 1 12-Nov-2015 03:51



Page 9 of 34






ICPMS04


Units: ug/L

1.579 0.7 5Manganese


Page 10 of 34






ICPMS04


Units: ug/L



Units: ug/L



Units: ug/L



Units: ug/L



Page 11 of 34




HS16010649-01 16-Sep-2015 14:25HS15090757-10

13-Jan-2016 14:005910-SB03-14 Soil

HS16010649-02 18-Sep-2015 09:15HS15090825-23

13-Jan-2016 14:004904-SB04-21 Soil

HS16010649-03 23-Sep-2015 13:35 13-Jan-2016 14:004904-SB16-21.5 Soil

HS16010649-04 23-Sep-2015 11:15 13-Jan-2016 14:004904-SB17-22 Soil


Page 12 of 34


Pastor, Behling & Wheeler, LLCCES Griggs Rd VCP5910-SB03-14

WorkOrder:Lab ID:

Collection Date:

HS16010649HS16010649-01


ANALYTICAL REPORT





100mg/Kg-dry 25-Jan-2016 13:0710.7Manganese 53.32,980


MOISTURE Method:SW3550 Analyst: JBA1wt% 23-Sep-2015 16:090.0100Percent Moisture 0.010014.2



Page 13 of 34



WorkOrder:Lab ID:

Collection Date:

HS16010649HS16010649-02


ANALYTICAL REPORT






1mg/Kg-dry 22-Jan-2016 16:060.221Selenium 0.6151.61

1mg/Kg-dry 22-Jan-2016 16:060.308Zinc 0.61535.5




Page 14 of 34



WorkOrder:Lab ID:

Collection Date:

HS16010649HS16010649-04


ANALYTICAL REPORT




1mg/Kg-dry 11-Nov-2015 21:010.0779Cobalt 0.55611.9

1mg/Kg-dry 11-Nov-2015 21:010.111Copper 0.22311.8

1mg/Kg-dry 11-Nov-2015 21:010.0556Lead 0.55615.4

1mg/Kg-dry 11-Nov-2015 21:01E 0.111Manganese 0.556622

1mg/Kg-dry 11-Nov-2015 21:010.100Nickel 0.55620.5

1mg/Kg-dry 11-Nov-2015 21:010.200Selenium 0.5560.591




Page 15 of 34

WEIGHT LOG





Final Volume

Prep Factor

HS16010649-04 1 0.5588 50 (mL) 89.48



Final Volume

Prep Factor

HS16010649-01 1 0.5464 50 (mL) 91.51HS16010649-02 1 0.5132 50 (mL) 97.43


Page 16 of 34

Client:CES Griggs Rd VCPPastor, Behling & Wheeler, LLC

WorkOrder:Project:




22 Jan 2016 10:47 25 Jan 2016 13:07HS16010649-01 16 Sep 2015 14:25 1005910-SB03-14

22 Jan 2016 10:47 22 Jan 2016 16:02HS16010649-01 16 Sep 2015 14:25 15910-SB03-14

22 Jan 2016 10:47 22 Jan 2016 16:06HS16010649-02 18 Sep 2015 09:15 14904-SB04-21


10 Nov 2015 08:07 11 Nov 2015 21:01HS16010649-04 23 Sep 2015 11:15 14904-SB17-22


24 Sep 2015 19:21HS16010649-02 18 Sep 2015 09:15 14904-SB04-21

30 Sep 2015 14:32HS16010649-04 23 Sep 2015 11:15 14904-SB17-22


23 Sep 2015 16:09HS16010649-01 16 Sep 2015 14:25 15910-SB03-14


Page 17 of 34






Units: mg/Kg


A 0.04837440-50-8 0.100Copper 0.2000.100

A 0.09497439-92-1 0.0500Lead 0.5000.100

A 0.1107439-96-5 0.100Manganese 0.5000.100

A 0.09357440-02-0 0.0900Nickel 0.5000.100

A 0.3147782-49-2 0.180Selenium 0.5000.250

A 0.3267440-66-6 0.250Zinc 0.5000.250

Page 18 of 34






Units: wt%


Page 19 of 34

Client:Project:

Pastor, Behling & Wheeler, LLCCES Griggs Rd VCP


QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MBLK

Client ID:

Cobalt U 0.500

Manganese U 0.500

Nickel U 0.500

Selenium U 0.500

Zinc U 0.500




Value %RECControl

LimitRPD Ref


LCS

Client ID:

Cobalt 9.164 10 0 91.6 80 - 1200.500

Manganese 8.962 10 0 89.6 80 - 1200.500

Nickel 9.383 10 0 93.8 80 - 1200.500

Selenium 8.298 10 0 83.0 80 - 1200.500

Zinc 8.817 10 0 88.2 80 - 1200.500




Value %RECControl

LimitRPD Ref


MS

Client ID:

Cobalt 13.93 9.234 6.322 82.4 75 - 1250.462

Manganese 333.8 9.234 354.4 -224 75 - 125 SEO 0.462

Nickel 17.6 9.234 8.302 101 75 - 1250.462

Selenium 8.96 9.234 1.421 81.6 75 - 1250.462

Zinc 59.1 9.234 39.33 214 75 - 125 SO 0.462



Page 20 of 34

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MSD

Client ID:

Cobalt 14.16 9.463 6.322 82.8 75 - 125 13.93 1.58 200.473

Manganese 312.4 9.463 354.4 -444 75 - 125 333.8 6.6 20 SEO 0.473

Nickel 17.8 9.463 8.302 100 75 - 125 17.6 1.12 200.473

Selenium 9.199 9.463 1.421 82.2 75 - 125 8.96 2.63 200.473

Zinc 61.44 9.463 39.33 234 75 - 125 59.1 3.88 20 SO 0.473




Value %RECControl

LimitRPD Ref


PDS

Client ID:

Cobalt 15.36 9.798 6.322 92.3 75 - 1250.490

Nickel 16.26 9.798 8.302 81.2 75 - 1250.490

Selenium 9.933 9.798 1.421 86.9 75 - 1250.490




Value %RECControl

LimitRPD Ref


PDS

Client ID:

Manganese 542.4 97.98 451.1 93.1 75 - 125 O 4.90

Zinc 152.1 97.98 48.95 105 75 - 1254.90




Value %RECControl

LimitRPD Ref


SD

Client ID:

Cobalt 6.683 6.322 5.71 102.45

Nickel 9.017 8.302 8.61 102.45

Selenium 1.625 1.421 0 10 J 2.45



Page 21 of 34

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


SD

Client ID:

Manganese 422.7 451.1 6.3 1024.5

Zinc 44.22 48.95 9.66 1024.5




Page 22 of 34

Client:Project:



QC BATCH REPORT


Sample ID: MBLK-98833 Units: mg/Kg Analysis Date: 11-Nov-2015 20:13



Value %RECControl

LimitRPD Ref


MBLK

Client ID:

Cobalt U 0.500

Copper U 0.500

Lead U 0.500

Manganese U 0.500

Nickel U 0.500

Selenium U 0.500

Sample ID: MLCS-98833 Units: mg/Kg Analysis Date: 11-Nov-2015 20:18



Value %RECControl

LimitRPD Ref


LCS

Client ID:

Cobalt 9.455 10 0 94.5 80 - 1200.500

Copper 9.856 10 0 98.6 80 - 1200.500

Lead 9.662 10 0 96.6 80 - 1200.500

Manganese 9.729 10 0 97.3 80 - 1200.500

Nickel 10.18 10 0 102 80 - 1200.500

Selenium 9.865 10 0 98.6 80 - 1200.500




Value %RECControl

LimitRPD Ref


MS

Client ID:

Cobalt 8.872 9.418 0.8565 85.1 75 - 1250.471




Value %RECControl

LimitRPD Ref


MS

Client ID:

Copper 10.29 9.418 1.358 94.9 75 - 1250.471

Lead 12.83 9.418 4.3 90.6 75 - 1250.471

Manganese 17.71 9.418 23.62 -62.7 75 - 125 S 0.471

Nickel 10.67 9.418 1.725 94.9 75 - 1250.471

Selenium 8.38 9.418 0.1518 87.4 75 - 1250.471



Page 23 of 34

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MSD

Client ID:

Cobalt 9.198 9.666 0.8565 86.3 75 - 125 8.872 3.6 200.483




Value %RECControl

LimitRPD Ref


MSD

Client ID:

Copper 10.78 9.666 1.358 97.5 75 - 125 10.29 4.6 200.483

Lead 13.15 9.666 4.3 91.6 75 - 125 12.83 2.47 200.483

Manganese 18.09 9.666 23.62 -57.2 75 - 125 17.71 2.11 20 S 0.483

Nickel 11.19 9.666 1.725 97.9 75 - 125 10.67 4.79 200.483

Selenium 8.822 9.666 0.1518 89.7 75 - 125 8.38 5.14 200.483




Value %RECControl

LimitRPD Ref


PDS

Client ID:

Cobalt 8.317 8.856 0.8565 84.2 75 - 1250.443




Value %RECControl

LimitRPD Ref


PDS

Client ID:

Copper 9.445 8.856 1.358 91.3 75 - 1250.443

Lead 12.47 8.856 4.3 92.3 75 - 1250.443

Manganese 31.06 8.856 23.62 84.1 75 - 1250.443

Nickel 9.741 8.856 1.725 90.5 75 - 1250.443

Selenium 8.355 8.856 0.1518 92.6 75 - 1250.443




Value %RECControl

LimitRPD Ref


SD

Client ID:

Cobalt 0.8983 0.8565 0 10 J 2.21



Page 24 of 34

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


SD

Client ID:

Copper 1.401 1.358 0 10 J 2.21

Lead 4.272 4.3 0.649 102.21

Manganese 22.85 23.62 3.28 102.21

Nickel 1.801 1.725 0 10 J 2.21

Selenium U 0.1518 0 102.21




Page 25 of 34





a Not accredited

















MBLK Method Blank



MS Matrix Spike




SD Serial Dilution




Page 26 of 34



Arkansas 15-024-0 27-Mar-2016



Kentucky KY 2015-2016 30-Apr-2016

Louisiana 03087 2015/2016 30-Jun-2016



Oklahoma 2015-047 31-Aug-2016

Texas T104704231-15-15 30-Apr-2016


Page 27 of 34




HS16010649-01 5910-SB03-14 Login 1/19/2016 5:39:52 PM RPG 8D

HS16010649-02 4904-SB04-21 Login 1/19/2016 5:39:52 PM RPG 8D


Page 28 of 34

PS


HS16010649

PBW - Houston

Work Order:

Client Name:


Received by:













Cooler(s)/Kit(s):




pH adjusted?

pH adjusted by:

Login Notes:

No Not Present

Yes No Not Present

Yes No Not Present

Yes No

Yes No

Yes No

Yes No

Yes No

Yes No

Yes No

Yes No

1.0c/0.7c/1.7c/1.4c/2.3c/2.0c u/c 64709/24537/303009/17/2015 18:29


Yes No N/A

Yes No N/A

COC: 5910-SB03-05 (txtcore4) of 4 is emptyCOC: 5910-SB03-05 DUP (txtcore4)of 4 is emptyCOC:TB-01 091615 Sample: TB-01 090915-52COC:TB-02 091615 Sample: TB-02 090915-59

Checklist completed by: Charity CarterDateeSignatureDateeSignature

17-Sep-2015

ALS CourierSoils Carrier name:Matrices:

Reviewed by:



Comments:

Corrective Action:

0

Yes



Page 29 of 34

Page 30 of 34

Page 31 of 34

Page 32 of 34

Page 33 of 34

Page 34 of 34

February 02, 2016





Sincerely,

ALS Environmental received 3 sample(s) on Feb 01, 2016 for the analysis presented in the following report.


Dear Brenda,



Dane J. Wacasey


Page 1 of 19


WorkOrder:















Page 2 of 19


WorkOrder:


Dane J. Wacasey




Page 3 of 19


Laboratory Name: ALS Laboratory Group LRC Date: 02/02/2016 Project Name: CES Griggs Rd VCP Laboratory Job Number: HS16020049 Reviewer Name: Dane Wacasey Prep Batch Number(s): R268672 #1 A2 Description Yes No NA3 NR4 ER#5















Was the LCSD RPD within QC limits? X R7 OI Matrix spike (MS) and matrix spike duplicate (MSD) data Were the project/method specified analytes included in the MS and MSD? X Were MS/MSD analyzed at the appropriate frequency? X Were MS (and MSD, if applicable) %Rs within the laboratory QC limits? X Were MS/MSD RPDs within laboratory QC limits? X R8 OI Analytical duplicate data Were appropriate analytical duplicates analyzed for each matrix? X Were analytical duplicates analyzed at the appropriate frequency? X Were RPDs or relative standard deviations within the laboratory QC limits? X R9 OI Method quantitation limits (MQLs): Are the MQLs for each method analyte included in the laboratory data package? X







Page 4 of 19

Laboratory Review Checklist: Reportable Data Laboratory Name: ALS Laboratory Group LRC Date: 02/02/2016 Project Name: CES Griggs Rd VCP Laboratory Job Number: HS16020049 Reviewer Name: Dane Wacasey Prep Batch Number(s): R268672 #1 A2 Description Yes No NA3 NR4 ER#5








continuing calibration blank (CCB) Was the CCV analyzed at the method-required frequency? X Were percent differences for each analyte within the method-required QC limits? X Was the ICAL curve verified for each analyte? X Was the absolute value of the analyte concentration in the inorganic CCB < MDL? X S3 O Mass spectral tuning: Was the appropriate compound for the method used for tuning? X Were ion abundance data within the method-required QC limits? X S4 O Internal standards (IS): Were IS area counts and retention times within the method-required QC limits? X















Page 5 of 19


Laboratory Name: ALS Laboratory Group LRC Date: 02/02/2016 Project Name: CES Griggs Rd VCP Laboratory Job Number: HS16020049 Reviewer Name: Dane Wacasey Prep Batch Number(s): R268672

ER#5 Description

No Exceptions


Page 6 of 19

Client: PBW Houston



HS16020049-01 01-Feb-2016 16:25 01-Feb-2016 17:374904-TMW01 Water

HS16020049-02 01-Feb-2016 16:25 01-Feb-2016 17:374904-TMW01 Dup Water

HS16020049-03 01-Feb-2016 16:45 01-Feb-2016 17:37TB01 020116 Water


Page 7 of 19


PBW HoustonCES Griggs Rd VCP4904-TMW01

WorkOrder:Lab ID:

Collection Date:

HS16020049HS16020049-01

01-Feb-2016 16:25 Matrix:Water

ANALYTICAL REPORT



LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: AKP1mg/L 02-Feb-2016 12:100.00020cis-1,2-Dichloroethene 0.00100.12

Surr: 1,2-Dichloroethane-d4 1%REC 02-Feb-2016 12:10103 71-125

Surr: 4-Bromofluorobenzene 1%REC 02-Feb-2016 12:10100 70-125

Surr: Dibromofluoromethane 1%REC 02-Feb-2016 12:10107 74-125

Surr: Toluene-d8 1%REC 02-Feb-2016 12:10101 75-125



Page 8 of 19


PBW HoustonCES Griggs Rd VCP4904-TMW01 Dup

WorkOrder:Lab ID:

Collection Date:

HS16020049HS16020049-02


ANALYTICAL REPORT










Page 9 of 19



WorkOrder:Lab ID:

Collection Date:

HS16020049HS16020049-03


ANALYTICAL REPORT



LOW LEVEL VOLATILES BY SW8260C Method:SW8260 Analyst: AKP1mg/L 02-Feb-2016 11:450.00020cis-1,2-Dichloroethene 0.0010U


Surr: 4-Bromofluorobenzene 1%REC 02-Feb-2016 11:4599.8 70-125





Page 10 of 19


WorkOrder:Project:




02 Feb 2016 12:10HS16020049-01 01 Feb 2016 16:25 14904-TMW01

02 Feb 2016 12:35HS16020049-02 01 Feb 2016 16:25 14904-TMW01 Dup

02 Feb 2016 11:45HS16020049-03 01 Feb 2016 16:45 1TB01 020116


Page 11 of 19






Units: mg/L

Type Analyte DCSCAS MDL PQLDCS SpikeA 0.00068156-59-2 0.00020cis-1,2-Dichloroethene 0.00100.00050




S 02037-26-5 0Toluene-d8 0.00100

Page 1 of 1

Page 12 of 19

Client:Project:



QC BATCH REPORT


Sample ID: VBLKW-160202 Units: ug/L Analysis Date: 02-Feb-2016 11:20



Value %RECControl

LimitRPD Ref


MBLK

Client ID:





50.03 50 0 100 75 - 1251.0Surr: Toluene-d8

Sample ID: VLCSW-160202 Units: ug/L Analysis Date: 02-Feb-2016 10:30



Value %RECControl

LimitRPD Ref


LCS

Client ID:





49.59 50 0 99.2 75 - 1251.0Surr: Toluene-d8

Sample ID: HS16011175-03MS Units: ug/L Analysis Date: 02-Feb-2016 13:25



Value %RECControl

LimitRPD Ref


MS

Client ID:





49.31 50 0 98.6 75 - 1251.0Surr: Toluene-d8



Page 13 of 19

Client:Project:



QC BATCH REPORT


Sample ID: HS16011175-03MSD Units: ug/L Analysis Date: 02-Feb-2016 13:50



Value %RECControl

LimitRPD Ref


MSD

Client ID:




50.66 50 0 101 74 - 125 50.29 0.738 201.0Surr: Dibromofluoromethane

49.5 50 0 99.0 75 - 125 49.31 0.387 201.0Surr: Toluene-d8




Page 14 of 19





a Not accredited

















MBLK Method Blank



MS Matrix Spike




SD Serial Dilution



Unit Reported Descriptionmg/L Milligrams per Liter


Page 15 of 19



Arkansas 15-024-0 27-Mar-2016



Kentucky KY 2015-2016 30-Apr-2016

Louisiana 03087 2015/2016 30-Jun-2016



Oklahoma 2015-047 31-Aug-2016

Texas T104704231-15-15 30-Apr-2016


Page 16 of 19

Client: PBW Houston



HS16020049-01 4904-TMW01 Login 2/1/2016 6:38:27 PM PMG VW-3

HS16020049-02 4904-TMW01 Dup Login 2/1/2016 6:38:27 PM PMG VW-3



Page 17 of 19

PMG

01-Feb-2016 17:37Date/Time Received:

HS16020049

PBW - Houston

Work Order:

Client Name:


Received by:













Cooler(s)/Kit(s):




pH adjusted?

pH adjusted by:

Login Notes:

No Not Present

Yes No Not Present

Yes No Not Present

Yes No

Yes No

Yes No

Yes No

Yes No

Yes No

Yes No

Yes No

3.5c/4.0c U/C IR5425782/1/16 18:50


Yes No N/A

Yes No N/A

Analyze Vial 1 of 3 for analysis. Screen using other 2 vials. Results due 2/3/16


1-Feb-20161-Feb-2016

ClientWater Carrier name:Matrices:




Comments:

Corrective Action:

0

Yes



Page 18 of 19

Page 19 of 19

February 09, 2016





Sincerely,



Dear Brenda,



Dane J. Wacasey


Page 1 of 34


WorkOrder:















Page 2 of 34


WorkOrder:


Dane J. Wacasey




Page 3 of 34


Laboratory Name: ALS Laboratory Group LRC Date: 02/09/2016 Project Name: CES Griggs Rd VCP Laboratory Job Number: HS16020120 Reviewer Name: Dane Wacasey Prep Batch Number(s): 101156, 101164, 101167,101173,R268820 #1 A2 Description Yes No NA3 NR4 ER#5






















Page 4 of 34

Laboratory Review Checklist: Reportable Data Laboratory Name: ALS Laboratory Group LRC Date: 02/09/2016 Project Name: CES Griggs Rd VCP Laboratory Job Number: HS16020120 Reviewer Name: Dane Wacasey Prep Batch Number(s): 101156, 101164, 101167,101173,R268820 #1 A2 Description Yes No NA3 NR4 ER#5























Page 5 of 34


Laboratory Name: ALS Laboratory Group LRC Date: 02/09/2016 Project Name: CES Griggs Rd VCP Laboratory Job Number: HS16020120 Reviewer Name: Dane Wacasey Prep Batch Number(s): 101156, 101164, 101167,101173,R268820

ER#5 Description

1

Batch 101156, Metals Method SW6020, sample HS16011178-45, MS and MSD were performed on unrelated sample. Batch 101167, Metals Method SW6020, sample HS16011169-03, MS and MSD were performed on unrelated sample. Batch 101173, Semivolatile Organics Method SW8270, sample HS16020149-03, MS and MSD were performed on unrelated sample.

2

Batch 101156, Metals Method SW6020, sample HS16011178-45, MSD RPD is for an unrelated sample. Batch 101167, Metals Method SW6020, sample HS16011169-03, MSD RPD is for an unrelated sample. Batch 101173, Semivolatile Organics Method SW8270, sample HS16020149-03, MSD RPD is for an unrelated sample.


Page 6 of 34

Client: PBW Houston



HS16020120-01 01-Feb-2016 13:15 02-Feb-2016 15:504904-SB02B-02 Soil

HS16020120-02 01-Feb-2016 14:45 02-Feb-2016 15:504904-SB29A-09 Soil

HS16020120-03 01-Feb-2016 13:49 02-Feb-2016 15:504904-SB30-00 Soil

HS16020120-04 01-Feb-2016 14:10 02-Feb-2016 15:504904-SB30-12 Soil

HS16020120-05 01-Feb-2016 15:40 02-Feb-2016 15:505910-SB03A-16 Soil

HS16020120-06 01-Feb-2016 15:40 02-Feb-2016 15:505910-SB03A-16 Dup Soil

HS16020120-07 01-Feb-2016 15:58 02-Feb-2016 15:505910-SB17-01 Soil

HS16020120-08 01-Feb-2016 16:30 02-Feb-2016 15:505910-SB18-01 Soil

HS16020120-09 01-Feb-2016 00:00080515-75 02-Feb-2016 15:50Trip Blank Water


Page 7 of 34


PBW HoustonCES Griggs Rd VCP4904-SB02B-02

WorkOrder:Lab ID:

Collection Date:

HS16020120HS16020120-01

01-Feb-2016 13:15 Matrix:Soil

ANALYTICAL REPORT



MOISTURE Method:SW3550 Analyst: DFF1wt% 04-Feb-2016 09:050.0100Percent Moisture 0.010017.4

TEXAS TPH BY TX1005 Method:TX1005 Analyst: KHTPrep:TX1005PR / 04-Feb-2016

1mg/Kg-dry 04-Feb-2016 22:599.5>nC12 to nC28 4852

1mg/Kg-dry 04-Feb-2016 22:599.5>nC28 to nC35 48170

1mg/Kg-dry 04-Feb-2016 22:599.5Total Petroleum Hydrocarbon 48232

Surr: 2-Fluorobiphenyl 1%REC 04-Feb-2016 22:5992.8 70-130

Surr: Trifluoromethyl benzene 1%REC 04-Feb-2016 22:5986.1 70-130



Page 8 of 34



WorkOrder:Lab ID:

Collection Date:

HS16020120HS16020120-02


ANALYTICAL REPORT



METALS BY SW6020A Method:SW6020 Analyst: JDEPrep:SW3050A / 04-Feb-2016

100mg/Kg-dry 05-Feb-2016 14:2912.3Manganese 61.620,900




Page 9 of 34



WorkOrder:Lab ID:

Collection Date:

HS16020120HS16020120-03


ANALYTICAL REPORT




10mg/Kg-dry 05-Feb-2016 14:331.03Manganese 5.17795




Page 10 of 34



WorkOrder:Lab ID:

Collection Date:

HS16020120HS16020120-04


ANALYTICAL REPORT




1mg/Kg-dry 04-Feb-2016 22:280.122Manganese 0.61053.9




Page 11 of 34



WorkOrder:Lab ID:

Collection Date:

HS16020120HS16020120-05


ANALYTICAL REPORT




1mg/Kg-dry 04-Feb-2016 22:320.0751Cobalt 0.5372.43


1mg/Kg-dry 04-Feb-2016 22:320.0966Nickel 0.5374.44


LOW-LEVEL SEMIVOLATILES Method:SW8270 Analyst: ACNPrep:SW3541 / 04-Feb-2016

1mg/Kg-dry 05-Feb-2016 17:120.0013Phenol 0.0076U

Surr: 2,4,6-Tribromophenol 1%REC 05-Feb-2016 17:12107 36-126

Surr: 2-Fluorophenol 1%REC 05-Feb-2016 17:1285.7 37-125

Surr: Phenol-d6 1%REC 05-Feb-2016 17:1295.7 40-125



Page 12 of 34


PBW HoustonCES Griggs Rd VCP5910-SB03A-16 Dup

WorkOrder:Lab ID:

Collection Date:

HS16020120HS16020120-06


ANALYTICAL REPORT




1mg/Kg-dry 04-Feb-2016 22:360.0747Cobalt 0.5334.37


1mg/Kg-dry 04-Feb-2016 22:360.0960Nickel 0.5336.91


LOW-LEVEL SEMIVOLATILES Method:SW8270 Analyst: ACNPrep:SW3541 / 04-Feb-2016

1mg/Kg-dry 05-Feb-2016 17:310.0013Phenol 0.0075U

Surr: 2,4,6-Tribromophenol 1%REC 05-Feb-2016 17:31124 36-126

Surr: 2-Fluorophenol 1%REC 05-Feb-2016 17:3183.1 37-125

Surr: Phenol-d6 1%REC 05-Feb-2016 17:31109 40-125



Page 13 of 34



WorkOrder:Lab ID:

Collection Date:

HS16020120HS16020120-07


ANALYTICAL REPORT




10mg/Kg-dry 05-Feb-2016 14:381.15Manganese 5.76553




Page 14 of 34



WorkOrder:Lab ID:

Collection Date:

HS16020120HS16020120-08


ANALYTICAL REPORT




100mg/Kg-dry 05-Feb-2016 14:1611.3Manganese 56.412,500

100mg/Kg-dry 05-Feb-2016 14:1625.9Vanadium 56.4688




Page 15 of 34

WEIGHT LOG





Final Volume

Prep Factor

HS16020120-08 1 0.5499 50 (mL) 90.93



Final Volume

Prep Factor

HS16020120-01 1 12.68 10 (mL) 0.7886



Final Volume

Prep Factor

HS16020120-02 1 0.535 50 (mL) 93.46HS16020120-03 1 0.5447 50 (mL) 91.79HS16020120-04 1 0.5494 50 (mL) 91.01HS16020120-05 1 0.5411 50 (mL) 92.4HS16020120-06 1 0.5357 50 (mL) 93.34HS16020120-07 1 0.5441 50 (mL) 91.89



Final Volume

Prep Factor

HS16020120-05 1 30.08 1 (mL) 0.03324HS16020120-06 1 30.09 1 (mL) 0.03323


Page 16 of 34


WorkOrder:Project:




04 Feb 2016 10:00 05 Feb 2016 14:16HS16020120-08 01 Feb 2016 16:30 1005910-SB18-01


04 Feb 2016 10:09 04 Feb 2016 22:59HS16020120-01 01 Feb 2016 13:15 14904-SB02B-02


04 Feb 2016 10:21 05 Feb 2016 14:29HS16020120-02 01 Feb 2016 14:45 1004904-SB29A-09

04 Feb 2016 10:21 05 Feb 2016 14:33HS16020120-03 01 Feb 2016 13:49 104904-SB30-00

04 Feb 2016 10:21 04 Feb 2016 22:28HS16020120-04 01 Feb 2016 14:10 14904-SB30-12

04 Feb 2016 10:21 04 Feb 2016 22:32HS16020120-05 01 Feb 2016 15:40 15910-SB03A-16

04 Feb 2016 10:21 04 Feb 2016 22:36HS16020120-06 01 Feb 2016 15:40 15910-SB03A-16 Dup

04 Feb 2016 10:21 05 Feb 2016 14:38HS16020120-07 01 Feb 2016 15:58 105910-SB17-01


04 Feb 2016 08:41 05 Feb 2016 17:12HS16020120-05 01 Feb 2016 15:40 15910-SB03A-16

04 Feb 2016 08:41 05 Feb 2016 17:31HS16020120-06 01 Feb 2016 15:40 15910-SB03A-16 Dup


04 Feb 2016 09:05HS16020120-01 01 Feb 2016 13:15 14904-SB02B-02

04 Feb 2016 09:05HS16020120-02 01 Feb 2016 14:45 14904-SB29A-09

04 Feb 2016 09:05HS16020120-03 01 Feb 2016 13:49 14904-SB30-00

04 Feb 2016 09:05HS16020120-04 01 Feb 2016 14:10 14904-SB30-12

04 Feb 2016 09:05HS16020120-05 01 Feb 2016 15:40 15910-SB03A-16

04 Feb 2016 09:05HS16020120-06 01 Feb 2016 15:40 15910-SB03A-16 Dup

04 Feb 2016 09:05HS16020120-07 01 Feb 2016 15:58 15910-SB17-01

04 Feb 2016 09:05HS16020120-08 01 Feb 2016 16:30 15910-SB18-01


Page 17 of 34






Units: mg/Kg


A 22TPH-1005-3 10>nC28 to nC35 5025




Page 18 of 34






Units: mg/Kg


A 0.1247439-96-5 0.100Manganese 0.5000.100

A 0.08187440-02-0 0.0900Nickel 0.5000.100

A 0.3337440-62-2 0.230Vanadium 0.5000.250

Page 19 of 34






Units: mg/Kg

Type Analyte DCSCAS MDL PQLDCS SpikeA 0.0038108-95-2 0.0011Phenol 0.00660.0033



S 013127-88-3 0Phenol-d6 00

Page 20 of 34






Units: wt%


Page 21 of 34

Client:Project:



QC BATCH REPORT


Sample ID: MBLK-101164 Units: mg/Kg Analysis Date: 04-Feb-2016 16:51

Run ID: FID-12_268830 SeqNo: 3576313 PrepDate: 04-Feb-2016 DF: 1


Value %RECControl

LimitRPD Ref


MBLK

Client ID:

>nC12 to nC28 U 50

>nC28 to nC35 U 50




Sample ID: LCS-101164 Units: mg/Kg Analysis Date: 04-Feb-2016 17:21



Value %RECControl

LimitRPD Ref


LCS

Client ID:

>nC12 to nC28 219.1 250 0 87.7 75 - 12550



Sample ID: LCSD-101164 Units: mg/Kg Analysis Date: 04-Feb-2016 17:52



Value %RECControl

LimitRPD Ref


LCSD

Client ID:

>nC12 to nC28 209 250 0 83.6 75 - 125 219.1 4.72 2050

22.86 25 0 91.4 70 - 130 22.99 0.586 200Surr: 2-Fluorobiphenyl

20.48 25 0 81.9 70 - 130 21.1 2.99 200Surr: Trifluoromethyl benzene

Sample ID: HS16020090-04MS Units: mg/Kg Analysis Date: 04-Feb-2016 20:25



Value %RECControl

LimitRPD Ref


MS

Client ID:

>nC12 to nC28 203.6 249.5 0 81.6 75 - 12550





Page 22 of 34

Client:Project:



QC BATCH REPORT


Sample ID: HS16020090-04MSD Units: mg/Kg Analysis Date: 04-Feb-2016 20:56



Value %RECControl

LimitRPD Ref


MSD

Client ID:

>nC12 to nC28 237.5 295.2 0 80.5 75 - 125 203.6 15.4 2059






Page 23 of 34

Client:Project:



QC BATCH REPORT


Sample ID: MBLKB-101156 Units: mg/Kg Analysis Date: 04-Feb-2016 16:13

Run ID: ICPMS03_268795 SeqNo: 3575971 PrepDate: 03-Feb-2016 DF: 1


Value %RECControl

LimitRPD Ref


MBLK

Client ID:

Manganese U 0.576

Vanadium U 0.576

Sample ID: MLCS-101156 Units: mg/Kg Analysis Date: 04-Feb-2016 16:17



Value %RECControl

LimitRPD Ref


LCS

Client ID:

Manganese 9.362 11.36 0 82.4 80 - 1200.568

Vanadium 9.523 11.36 0 83.8 80 - 1200.568




Value %RECControl

LimitRPD Ref


MS

Client ID:

Manganese 521.8 9.479 335.7 1960 75 - 125 SEO 0.474

Vanadium 53.64 9.479 23.04 323 75 - 125 S 0.474




Value %RECControl

LimitRPD Ref


MSD

Client ID:

Manganese 234.8 9.379 335.7 -1080 75 - 125 521.8 75.9 20 SREO 0.469

Vanadium 45 9.379 23.04 234 75 - 125 53.64 17.5 20 S 0.469

Sample ID: HS16011178-45BS Units: mg/Kg Analysis Date: 05-Feb-2016 13:54



Value %RECControl

LimitRPD Ref


PDS

Client ID:

Manganese 449.7 95.62 357.6 96.3 75 - 1254.78



Page 24 of 34

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


PDS

Client ID:

Vanadium 31.49 9.562 23.04 88.3 75 - 1250.478

Sample ID: HS16011178-45 DIL SX Units: mg/Kg Analysis Date: 05-Feb-2016 13:50



Value %RECControl

LimitRPD Ref


SD

Client ID:

Manganese 356.9 357.6 0.201 1023.9




Value %RECControl

LimitRPD Ref


SD

Client ID:

Vanadium 23.81 23.04 3.32 102.39




Page 25 of 34

Client:Project:



QC BATCH REPORT


Sample ID: MBLKB-101167 Units: mg/Kg Analysis Date: 04-Feb-2016 19:36



Value %RECControl

LimitRPD Ref


MBLK

Client ID:

Cobalt U 0.568

Manganese U 0.568

Nickel U 0.568

Sample ID: MLCSB-101167 Units: mg/Kg Analysis Date: 04-Feb-2016 19:40



Value %RECControl

LimitRPD Ref


LCS

Client ID:

Cobalt 10.07 11.31 0 89.0 80 - 1200.565

Manganese 9.681 11.31 0 85.6 80 - 1200.565

Nickel 10.02 11.31 0 88.6 80 - 1200.565




Value %RECControl

LimitRPD Ref


MS

Client ID:

Cobalt 10.34 9.263 2.234 87.5 75 - 1250.463

Manganese 1321 9.263 96.32 13200 75 - 125 SEO 0.463

Nickel 14.29 9.263 5.044 99.8 75 - 1250.463




Value %RECControl

LimitRPD Ref


MSD

Client ID:

Cobalt 10.83 9.295 2.234 92.5 75 - 125 10.34 4.65 200.465

Manganese 155.1 9.295 96.32 633 75 - 125 1321 158 20 SRO 0.465

Nickel 13.87 9.295 5.044 94.9 75 - 125 14.29 3.01 200.465



Page 26 of 34

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


PDS

Client ID:

Cobalt 10.22 9.443 2.234 84.5 75 - 1250.472

Manganese 106.1 9.443 96.32 104 75 - 125 O 0.472

Nickel 12.71 9.443 5.044 81.2 75 - 1250.472




Value %RECControl

LimitRPD Ref


SD

Client ID:

Cobalt 2.083 2.234 0 10 J 2.36

Manganese 94.05 96.32 2.35 102.36

Nickel 5.118 5.044 1.46 102.36

The following samples were anayzed in this batch: HS16020120-02 HS16020120-03 HS16020120-04 HS16020120-05 HS16020120-06 HS16020120-07



Page 27 of 34

Client:Project:



QC BATCH REPORT


Sample ID: MBLK-101173 Units: ug/Kg Analysis Date: 04-Feb-2016 15:47

Run ID: SV-7_268826 SeqNo: 3578108 PrepDate: 04-Feb-2016 DF: 1


Value %RECControl

LimitRPD Ref


MBLK

Client ID:

Phenol U 6.6



172.4 167 0 103 40 - 1250Surr: Phenol-d6

Sample ID: LCS-101173 Units: ug/Kg Analysis Date: 04-Feb-2016 16:06



Value %RECControl

LimitRPD Ref


LCS

Client ID:

Phenol 150.4 167 0 90.0 45 - 1306.6



138.9 167 0 83.2 40 - 1250Surr: Phenol-d6

Sample ID: HS16020149-03MS Units: ug/Kg Analysis Date: 05-Feb-2016 01:22



Value %RECControl

LimitRPD Ref


MS

Client ID:

Phenol 235.6 166.7 0 141 45 - 130 S 66



186 166.7 0 112 40 - 1250Surr: Phenol-d6

Sample ID: HS16020149-03MSD Units: ug/Kg Analysis Date: 05-Feb-2016 01:41



Value %RECControl

LimitRPD Ref


MSD

Client ID:

Phenol 289.9 166.8 0 174 45 - 130 235.6 20.7 30 S 66


133.4 166.8 0 80.0 37 - 125 69.22 63.4 30 R 0Surr: 2-Fluorophenol

218.1 166.8 0 131 40 - 125 186 15.9 30 S 0Surr: Phenol-d6




Page 28 of 34

Client:Project:



QC BATCH REPORT


Sample ID: HS16020142-12DUP Units: wt% Analysis Date: 04-Feb-2016 09:05



Value %RECControl

LimitRPD Ref


DUP

Client ID:

Percent Moisture 15.3 15 1.98 200.0100

The following samples were anayzed in this batch: HS16020120-01 HS16020120-02 HS16020120-03 HS16020120-04 HS16020120-05 HS16020120-06 HS16020120-07 HS16020120-08



Page 29 of 34





a Not accredited

















MBLK Method Blank



MS Matrix Spike




SD Serial Dilution





Page 30 of 34



Arkansas 15-024-0 27-Mar-2016



Kentucky KY 2015-2016 30-Apr-2016

Louisiana 03087 2015/2016 30-Jun-2016



Oklahoma 2015-047 31-Aug-2016

Texas T104704231-15-15 30-Apr-2016


Page 31 of 34

Client: PBW Houston



HS16020120-01 4904-SB02B-02 Login 2/3/2016 11:58:16 AM CGG 13D

HS16020120-01 4904-SB02B-02 Login 2/3/2016 11:58:16 AM CGG LF-02

HS16020120-02 4904-SB29A-09 Login 2/3/2016 11:58:16 AM CGG 13D

HS16020120-03 4904-SB30-00 Login 2/3/2016 11:58:16 AM CGG 13D


HS16020120-05 5910-SB03A-16 Login 2/3/2016 11:58:16 AM CGG 13D

HS16020120-06 5910-SB03A-16 Dup Login 2/3/2016 11:58:16 AM CGG 13D




Page 32 of 34

JJT


HS16020120

PBW - Houston

Work Order:

Client Name:


Received by:













Cooler(s)/Kit(s):




pH adjusted?

pH adjusted by:

Login Notes:

No Not Present

Yes No Not Present

Yes No Not Present

Yes No

Yes No

Yes No

Yes No

Yes No

Yes No

Yes No

Yes No

2.6c/2.8c , 2.0c/2.2c uc/c IR42486 , 2457302/03/2016 12:20


Yes No N/A

Yes No N/A

Trip blank received (one vial broken), not listed on Chain of Custody. Logged without analysis.

Checklist completed by: Corey GranditsDateeSignatureDateeSignature

5-Feb-20163-Feb-2016

ClientSoil/Water Carrier name:Matrices:




Comments:

Corrective Action:

0

Yes



Page 33 of 34

Page 34 of 34

February 29, 2016





Sincerely,



Dear Brenda,


Generated By: Dane.Wacasey

Dane J. Wacasey


Page 1 of 27


WorkOrder:















Page 2 of 27


WorkOrder:


Dane J. Wacasey




Page 3 of 27


Laboratory Name: ALS Laboratory Group LRC Date: 2/29/2016 Project Name: CES Griggs Rd VCP Laboratory Job Number: HS16021013 Reviewer Name: Dane J. Wacasey Prep Batch Number(s): R269919, R269937, R270051 #1 A2 Description Yes No NA3 NR4 ER#5















Was the LCSD RPD within QC limits? X R7 OI Matrix spike (MS) and matrix spike duplicate (MSD) data Were the project/method specified analytes included in the MS and MSD? X Were MS/MSD analyzed at the appropriate frequency? X Were MS (and MSD, if applicable) %Rs within the laboratory QC limits? X Were MS/MSD RPDs within laboratory QC limits? X R8 OI Analytical duplicate data Were appropriate analytical duplicates analyzed for each matrix? X Were analytical duplicates analyzed at the appropriate frequency? X Were RPDs or relative standard deviations within the laboratory QC limits? X R9 OI Method quantitation limits (MQLs): Are the MQLs for each method analyte included in the laboratory data package? X







Page 4 of 27

Laboratory Review Checklist: Reportable Data Laboratory Name: ALS Laboratory Group LRC Date: 2/29/2016 Project Name: CES Griggs Rd VCP Laboratory Job Number: HS16021013 Reviewer Name: Dane J. Wacasey Prep Batch Number(s): R269919, R269937, R270051 #1 A2 Description Yes No NA3 NR4 ER#5























Page 5 of 27


Laboratory Name: ALS Laboratory Group LRC Date: 2/29/2016 Project Name: CES Griggs Rd VCP Laboratory Job Number: HS16021013 Reviewer Name: Dane J. Wacasey Prep Batch Number(s): R269919, R269937, R270051 ER#5 Description

No Exceptions


Page 6 of 27




HS16021013-01 24-Feb-2016 08:40 24-Feb-2016 14:10MW-03 160224 Groundwater




HS16021013-05 24-Feb-2016 11:10 24-Feb-2016 14:10MW-01 Dup 160224 Groundwater


HS16021013-07 24-Feb-2016 08:00 24-Feb-2016 14:10Trip Blank 160224 Groundwater

HS16021013-08 24-Feb-2016 00:00 24-Feb-2016 14:10Trip Blank 021116-89 Groundwater


Page 7 of 27


Pastor, Behling & Wheeler, LLCCES Griggs Rd VCPMW-03 160224

WorkOrder:Lab ID:

Collection Date:

HS16021013HS16021013-01

24-Feb-2016 08:40 Matrix:Groundwater

ANALYTICAL REPORT




1mg/L 26-Feb-2016 01:160.00030Tetrachloroethene 0.0010U

1mg/L 26-Feb-2016 01:160.00020trans-1,2-Dichloroethene 0.0010U

1mg/L 26-Feb-2016 01:160.00020Trichloroethene 0.0010U

1mg/L 26-Feb-2016 01:160.00020Vinyl chloride 0.0010U







Page 8 of 27



WorkOrder:Lab ID:

Collection Date:

HS16021013HS16021013-02


ANALYTICAL REPORT




1mg/L 26-Feb-2016 08:490.00030Tetrachloroethene 0.00100.0020


1mg/L 26-Feb-2016 08:49J 0.00020Trichloroethene 0.00100.00064








Page 9 of 27



WorkOrder:Lab ID:

Collection Date:

HS16021013HS16021013-03


ANALYTICAL REPORT





1mg/L 26-Feb-2016 09:140.00020trans-1,2-Dichloroethene 0.00100.0024

1mg/L 26-Feb-2016 09:140.00020Trichloroethene 0.00100.0025

1mg/L 26-Feb-2016 09:140.00020Vinyl chloride 0.00100.0068







Page 10 of 27



WorkOrder:Lab ID:

Collection Date:

HS16021013HS16021013-04


ANALYTICAL REPORT








Surr: 1,2-Dichloroethane-d4 1%REC 29-Feb-2016 14:3199.8 71-125






Page 11 of 27


Pastor, Behling & Wheeler, LLCCES Griggs Rd VCPMW-01 Dup 160224

WorkOrder:Lab ID:

Collection Date:

HS16021013HS16021013-05


ANALYTICAL REPORT







1mg/L 26-Feb-2016 04:280.00020Vinyl chloride 0.00100.0044







Page 12 of 27



WorkOrder:Lab ID:

Collection Date:

HS16021013HS16021013-06


ANALYTICAL REPORT






1mg/L 26-Feb-2016 04:530.00020Trichloroethene 0.0010U


Surr: 1,2-Dichloroethane-d4 1%REC 26-Feb-2016 04:5398.0 71-125






Page 13 of 27

Client:CES Griggs Rd VCPPastor, Behling & Wheeler, LLC

WorkOrder:Project:



Batch ID R269919 Test Name : LOW LEVEL VOLATILES BY SW8260C Matrix: Groundwater

26 Feb 2016 01:16HS16021013-01 24 Feb 2016 08:40 1MW-03 160224

26 Feb 2016 08:49HS16021013-02 24 Feb 2016 09:45 1MW-04 160224

26 Feb 2016 09:14HS16021013-03 24 Feb 2016 10:30 1MW-05 160224


26 Feb 2016 04:28HS16021013-05 24 Feb 2016 11:10 1MW-01 Dup 160224

26 Feb 2016 04:53HS16021013-06 24 Feb 2016 11:55 1MW-02 160224


29 Feb 2016 14:31HS16021013-04 24 Feb 2016 11:05 1MW-01 160224


Page 14 of 27






Units: mg/L





A 0.0004575-01-4 0.00020Vinyl chloride 0.00100.00050




S 02037-26-5 0Toluene-d8 0.00100

Page 15 of 27






Units: mg/L





A 0.0004175-01-4 0.00020Vinyl chloride 0.00100.00050




S 02037-26-5 0Toluene-d8 0.00100

Page 16 of 27

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MBLK

Client ID:









54.64 50 0 109 75 - 1251.0Surr: Toluene-d8




Value %RECControl

LimitRPD Ref


LCS

Client ID:





Vinyl chloride 53.9 50 0 108 70 - 1351.0




52.74 50 0 105 75 - 1251.0Surr: Toluene-d8



Page 17 of 27

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MS

Client ID: MW-03 160224





Vinyl chloride 58.06 50 0 116 70 - 1351.0




49.86 50 0 99.7 75 - 1251.0Surr: Toluene-d8




Value %RECControl

LimitRPD Ref


MSD

Client ID: MW-03 160224

cis-1,2-Dichloroethene 57.12 50 0 114 75 - 125 57.49 0.65 201.0




Vinyl chloride 58.51 50 0 117 70 - 135 58.06 0.768 201.0



57.77 50 0 116 74 - 125 55.82 3.43 201.0Surr: Dibromofluoromethane

53.05 50 0 106 75 - 125 49.86 6.2 201.0Surr: Toluene-d8




Page 18 of 27

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MBLK

Client ID:









50.6 50 0 101 75 - 1251.0Surr: Toluene-d8




Value %RECControl

LimitRPD Ref


LCS

Client ID:





Vinyl chloride 52.03 50 0 104 70 - 1351.0




49.54 50 0 99.1 75 - 1251.0Surr: Toluene-d8



Page 19 of 27

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MS

Client ID:





Vinyl chloride 58.93 50 0 118 70 - 1351.0




49.5 50 0 99.0 75 - 1251.0Surr: Toluene-d8




Value %RECControl

LimitRPD Ref


MSD

Client ID:



trans-1,2-Dichloroethene 48.92 50 0 97.8 75 - 125 52.8 7.63 201.0


Vinyl chloride 50.07 50 0 100 70 - 135 58.93 16.3 201.0




49.97 50 0 99.9 75 - 125 49.5 0.939 201.0Surr: Toluene-d8




Page 20 of 27

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MBLK

Client ID:









51.91 50 0 104 75 - 1251.0Surr: Toluene-d8




Value %RECControl

LimitRPD Ref


LCS

Client ID:





Vinyl chloride 49.65 50 0 99.3 70 - 1351.0




49.03 50 0 98.1 75 - 1251.0Surr: Toluene-d8



Page 21 of 27

Client:Project:



QC BATCH REPORT





Value %RECControl

LimitRPD Ref


MS

Client ID:





Vinyl chloride 54.99 50 0 110 70 - 1351.0




49.99 50 0 100.0 75 - 1251.0Surr: Toluene-d8




Value %RECControl

LimitRPD Ref


MSD

Client ID:



trans-1,2-Dichloroethene 49.3 50 0 98.6 75 - 125 50.98 3.35 201.0

Trichloroethene 49.46 50 0 98.9 71 - 125 51.7 4.42 201.0

Vinyl chloride 50.63 50 0 101 70 - 135 54.99 8.25 201.0


49.86 50 0 99.7 70 - 125 50.12 0.511 201.0Surr: 4-Bromofluorobenzene


48.93 50 0 97.9 75 - 125 49.99 2.15 201.0Surr: Toluene-d8




Page 22 of 27





a Not accredited

















MBLK Method Blank



MS Matrix Spike




SD Serial Dilution



Unit Reported Descriptionmg/L Milligrams per Liter


Page 23 of 27



Arkansas 15-024-0 27-Mar-2016



Kentucky KY 2015-2016 30-Apr-2016

Louisiana 03087 2015/2016 30-Jun-2016



Oklahoma 2015-047 31-Aug-2016

Texas T104704231-15-15 30-Apr-2016


Page 24 of 27




HS16021013-01 MW-03 160224 Login 2/25/2016 8:16:13 AM RPG VW-3




HS16021013-05 MW-01 Dup 160224 Login 2/25/2016 8:16:13 AM RPG VW-3



Page 25 of 27

PMG


HS16021013

PBW - Houston

Work Order:

Client Name:


Received by:













Cooler(s)/Kit(s):




pH adjusted?

pH adjusted by:

Login Notes:

No Not Present

Yes No Not Present

Yes No Not Present

Yes No

Yes No

Yes No

Yes No

Yes No

Yes No

Yes No

Yes No

3.6c/4.2c uc/c IR 5484702/25/2016 08:24


Yes No N/A

Yes No N/A

Extra Volume vilas for MS/MSD times do not match. Logged in per COC information.Two sets Trip Blanks rec'd placed on Hold.

Checklist completed by: Raegen GigaDateeSignatureDateeSignature

29-Feb-201625-Feb-2016

ClientGW Carrier name:Matrices:




Comments:

Corrective Action:

0

Yes



Page 26 of 27

Page 27 of 27

Date post:	30-Oct-2020
Category:	Documents
Upload:	others
View:	3 times
Download:	0 times

Appendix 10 Laboratory Data Packages and Data Usability … · 2016. 10. 7. · Laboratory Review...

Documents