APPENDIX A SEDIMENT INVESTIGATION (GOLDER 2010) · Environmental Sample Disposal Fee 5 Elements by...

APPENDIX A SEDIMENT INVESTIGATION (GOLDER 2010)

(CONTINUED)

APPENDIX A CERTIFICATES OF ANALYSIS AND DATA QUALITY REVIEW CHECKLISTS

(CONTINUED)

Task Order#: 11062608Site#: P11605Site Location: Burrard Inlet Pipe Removal Port Moody BCProject #: SUPPLIMENTAL SEDIMENT CHARACTEYour C.O.C. #: f156639Attention: Blair MacDonald

GOLDER ASSOCIATES500-4260 STILL CREEK DRIVEBURNABY, BCCANADA V5C 6C6

Report Date: 2009/12/09

CERTIFICATE OF ANALYSIS

MAXXAM JOB #: A968904Received: 2009/12/01, 18:10

Sample Matrix: Sediment# Samples Received: 5

Analyses Quantity Laboratory Method Primary referenceSend Part to Archive 5Environmental Sample Disposal Fee 5Elements by ICPMS (total) 5 BRN SOP-00203 R5.0 Based on EPA 200.8Simultaneously Extractable Metals-ICPMS 5 BRN SOP-00203 5.0 Based on EPA 200.8Moisture 5 BRN SOP-00321 R5.0 Ont MOE -E 3139PAH in Soil by GC/MS (SIM) 5 BRN SOP-00332 R9.0 Based on EPA 8270DTotal LMW, HMW, Total PAH Calc 5pH (2:1 DI Water Extract) ( 2 ) 5 BRN SOP-00266 R6.0 Carter, SSMA 16.2Sulfide (AVS) (soil) - Calc for umole/g 5 BRN SOP-00229 R2.0 Based EPA821-R91-100Sulfide (AVS) (soil) 5 BRN SOP-00229 R2.0 Based EPA821-R91-100Total Organic Carbon LECO Method ( 1 ) 5 EENVSOP-00151 LECO# 203-821-170EPH less PAH in Soil By GC/FID ( 2 ) 5BC Hydrocarbons in Soil by GC/FID ( 2 ) 5 BRN SOP-00341 R14 Based BCCSR Method 3Texture by Hydrometer ( 1 ) 5 EENVSOP-00076 MMFSPA Ch9Texture Class ( 1 ) 5 EENVSOP-00076 MMFSPA Ch9

Remarks:

All Blank values are reported. Associated data are not blank corrected.Solids results are based on dry weight except Biota Analyses & Special Waste Oil & Grease.Organic analyses are not corrected for extraction recovery standards except for Isotope Dilution methods, (i.e. CARB 429PAH, all PCDD/F and DBD/DBF analyses).

Maxxam Analytics has performed all analytical testing herein in accordance with ISO 17025.

All CCME results met required criteria unless otherwise stated in the report. The CWS PHC methods employed byMaxxam conform to all prescribed elements of the reference method and performance based elements have beenvalidated. All modifications have been validated and proven equivalent following the 'Alberta Environment Draft Addenda tothe CWS-PHC, Appendix 6, Validation of Alternate Methods'. Documentation is available upon request. Deviations fromReference Method for the Canada-wide Standard for Petroleum Hydrocarbons in Soil-Tier 1 Method:F2/F3/F4 data reported using validated cold solvent extraction instead of Soxhlet extraction.

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Task Order#: 11062608Site#: P11605Site Location: Burrard Inlet Pipe Removal Port Moody BCProject #: SUPPLIMENTAL SEDIMENT CHARACTEYour C.O.C. #: f156639Attention: Blair MacDonald



CERTIFICATE OF ANALYSIS-2-

MAXXAM JOB #: A968904Received: 2009/12/01, 18:10All analysis data reported was generated when the analytical methods were in statistical control and criteria for spikerecoveries, reference material recoveries, method blanks data and duplicate precision were met unless otherwise stated.All samples were analysed within hold time unless otherwise flagged. All BTEX samples were methanol extracted within 24hours unless otherwise flagged.This report shall not be reproduced except in full, without the written approval of the laboratory.

Methods used by Maxxam are based upon those found in 'Standard Methods for the Examination of Water andWastewater', 21st Edition, published by the American Public Health Association, or on US EPA, protocols found in the 'Test Methods for Evaluating Solid Waste ', Physical/Chemical Methods, SW846, 3rd Edition. Other procedures are basedon the methodologies accepted by the appropriate regulatory agency. Methodology briefs are available by written request.

All work recorded herein has been done in accordance with normal professional standards using accepted testingmethodologies, quality assurance and quality control procedures except where otherwise agreed to by the client andtesting company in writing. Maxxam Analytics is limited in liability to the actual cost of analysis unless otherwise agreed inwriting. There is no other warranty expressed or implied. Your samples will be retained at Maxxam for a period of 45 daysfrom receipt of data or as per contract.

* RPDs calculated using raw data. The rounding of final results may result in the apparent difference.

(1) This test was performed by Maxxam Edmonton Environmental(2) SCC/CAEAL

Encryption Key

Please direct all questions regarding this Certificate of Analysis to your Project Manager.

SUE REYNOLDS, BBY Customer ServiceEmail: [email protected]# (604) 444-4808 Ext:235

====================================================================Maxxam has procedures in place to guard against improper use of the electronic signature and have the required "signatories", as per section5.10.2 of ISO/IEC 17025:2005(E), signing the reports. SCC and CALA have approved this reporting process and electronic report format.

Total cover pages: 2

Maxxam Analytics International Corporation o/a Maxxam Analytics Burnaby: 8577 Commerce Court V5A 4N5 Telephone(604) 444-4808 Fax(604) 444-4511

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Sue Reynolds

09 Dec 2009 16:20:41 -08:00

GOLDER ASSOCIATESMaxxam Job #: A968904 Task Order#: 11062608Report Date: 2009/12/09 Site#: P11605

Site Location: Burrard Inlet Pipe Removal Port Moody BCProject #: SUPPLIMENTAL SEDIMENT CHARACTE

RESULTS OF CHEMICAL ANALYSES OF SEDIMENT

Maxxam ID S 0 0 3 0 5 S 0 0 3 1 0 S 0 0 3 1 1Sampling Date 2009/12/01 2009/12/01 2009/12/01

11:29 14:19 12:10COC Number f156639 f156639 f156639

U n i t s IPS-SD09-20 IPS-SD09-21 R D L IPS-SD09-22 R D L QC Batch

Calculated Parameters

Sulphide umole/g 12.0 8.7 0.3 32.6 0.6 3601189

MISCELLANEOUS

Sulphide ug/g 384 279 10 1040 20 3609489

Physical Properties

% sand by hydrometer % 24 33 2 35 2 3609980

% silt by hydrometer % 56 49 2 48 2 3609980

Clay Content % 19 18 2 17 2 3609980

Texture N/A SILT LOAM LOAM N/A LOAM N/A 3601265

Moisture % 71 67 0.3 70 0.3 3602004

RDL = Reportable Detection Limit

Maxxam ID S 0 0 3 1 2 S 0 0 3 1 3Sampling Date 2009/12/01 2009/12/01

15:00 15:45COC Number f156639 f156639

U n i t s IPS-SD09-23 IPS-SD09-27 R D L QC Batch


Sulphide umole/g 6.0 5.4 0.3 3601189

MISCELLANEOUS

Sulphide ug/g 192 174 10 3609489

Physical Properties

% sand by hydrometer % 71 83 2 3609980

% silt by hydrometer % 20 13 2 3609980

Clay Content % 9 4 2 3609980

Texture N/A SANDY LOAM LOAMY SAND N/A 3601265

Moisture % 35 33 0.3 3602004


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ELEMENTS BY ATOMIC SPECTROSCOPY (SEDIMENT)


11:29 14:19 12:10COC Number f156639 f156639 f156639

U n i t s IPS-SD09-20 IPS-SD09-21 IPS-SD09-22 R D L QC Batch

SEM Metals by ICPMS

SEM Cadmium (Cd) umole/g 0.0215 0.0149 0.0127 0.0002 3612878

SEM Copper (Cu) umole/g 0.935 0.709 0.356 0.004 3612878

SEM Lead (Pb) umole/g 0.267 0.206 0.141 0.0002 3612878

SEM Mercury (Hg) umole/g <0.0003 <0.0003 <0.0003 0.0003 3612878

SEM Nickel (Ni) umole/g 0.402 0.311 0.222 0.004 3612878

SEM Zinc (Zn) umole/g 2.98 2.21 11.5 0.008 3612878



15:00 15:45COC Number f156639 f156639


SEM Metals by ICPMS

SEM Cadmium (Cd) umole/g 0.0051 0.0058 0.0002 3612878

SEM Copper (Cu) umole/g 0.256 0.301 0.004 3612878

SEM Lead (Pb) umole/g 0.0597 0.0731 0.0002 3612878

SEM Mercury (Hg) umole/g <0.0003 <0.0003 0.0003 3612878

SEM Nickel (Ni) umole/g 0.117 0.138 0.004 3612878

SEM Zinc (Zn) umole/g 0.823 0.975 0.008 3612878


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TOTAL PETROLEUM HYDROCARBONS (SEDIMENT)


11:29 14:19 12:10COC Number f156639 f156639 f156639



HEPH (C19-C32 less PAH) mg/kg 432 403 445 100 3601190

LEPH (C10-C19 less PAH) mg/kg <100 <100 <100 100 3601190

Hydrocarbons

EPH (C10-C19) mg/kg <100 <100 <100 100 3605852

EPH (C19-C32) mg/kg 439 408 452 100 3605852

ExtractionSurrogate Recovery (%)

O-TERPHENYL (sur.) % 92 92 93 N/A 3605852

N/A = Not ApplicableRDL = Reportable Detection Limit


15:00 15:45COC Number f156639 f156639



HEPH (C19-C32 less PAH) mg/kg 135 109 100 3601190

LEPH (C10-C19 less PAH) mg/kg <100 <100 100 3601190

Hydrocarbons

EPH (C10-C19) mg/kg <100 <100 100 3605852

EPH (C19-C32) mg/kg 137 113 100 3605852


O-TERPHENYL (sur.) % 90 90 N/A 3605852


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MISCELLANEOUS (SEDIMENT)


11:29 14:19 12:10COC Number f156639 f156639 f156639


Misc. Inorganics

Total Organic Carbon (C) % 4.7 ( 1 ) 5.4 ( 1 ) 4.7 ( 1 ) 0.1 3611643

RDL = Reportable Detection Limit( 1 ) Detection limits raised due to dilution to bring analyte within the calibrated range.


15:00 15:45COC Number f156639 f156639


Misc. Inorganics

Total Organic Carbon (C) % 1.6 0.98 0.02 3611643


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CSR/CCME METALS IN SOIL (SEDIMENT)


11:29 14:19 12:10COC Number f156639 f156639 f156639


Misc. Inorganics

Soluble (2:1) pH pH Units 7.76 7.75 7.66 0.01 3605960

Total Metals by ICPMS

Total Aluminum (Al) mg/kg 18000 15400 17500 100 3605544

Total Antimony (Sb) mg/kg 0.6 0.5 0.5 0.1 3605544

Total Arsenic (As) mg/kg 14.9 13.7 14.6 0.2 3605544

Total Barium (Ba) mg/kg 54.4 47.2 50.9 0.1 3605544

Total Beryllium (Be) mg/kg 0.5 0.3 0.3 0.1 3605544

Total Bismuth (Bi) mg/kg 0.5 0.4 0.4 0.1 3605544

Total Cadmium (Cd) mg/kg 2.14 1.66 2.14 0.05 3605544

Total Calcium (Ca) mg/kg 8670 11700 10600 100 3605544

Total Chromium (Cr) mg/kg 41 36 39 1 3605544

Total Cobalt (Co) mg/kg 8.8 7.7 8.6 0.3 3605544

Total Copper (Cu) mg/kg 112 91.3 112 0.5 3605544

Total Iron (Fe) mg/kg 31300 27400 29400 100 3605544

Total Lead (Pb) mg/kg 53.7 47.3 49.9 0.1 3605544

Total Magnesium (Mg) mg/kg 10400 9600 11000 100 3605544

Total Manganese (Mn) mg/kg 285 258 277 0.2 3605544

Total Mercury (Hg) mg/kg 0.20 0.17 0.20 0.05 3605544

Total Molybdenum (Mo) mg/kg 3.7 3.3 3.2 0.1 3605544

Total Nickel (Ni) mg/kg 28.4 23.9 26.9 0.8 3605544

Total Phosphorus (P) mg/kg 994 837 1000 10 3605544

Total Potassium (K) mg/kg 3420 3010 3390 100 3605544

Total Selenium (Se) mg/kg 2.2 1.1 1.7 0.5 3605544

Total Silver (Ag) mg/kg 0.53 0.48 0.49 0.05 3605544

Total Sodium (Na) mg/kg 21700 17900 21000 100 3605544

Total Strontium (Sr) mg/kg 73.8 90.9 79.9 0.1 3605544

Total Thallium (Tl) mg/kg 0.36 0.31 0.35 0.05 3605544

Total Tin (Sn) mg/kg 2.3 2.1 2.2 0.1 3605544

Total Titanium (Ti) mg/kg 710 626 663 1 3605544

Total Vanadium (V) mg/kg 54 48 52 2 3605544

Total Zinc (Zn) mg/kg 196 157 197 1 3605544


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11:29 14:19 12:10COC Number f156639 f156639 f156639


Total Zirconium (Zr) mg/kg 3.0 2.2 2.6 0.5 3605544


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15:00 15:45COC Number f156639 f156639


Misc. Inorganics

Soluble (2:1) pH pH Units 8.24 8.22 0.01 3605960


Total Aluminum (Al) mg/kg 7030 7000 100 3605544

Total Antimony (Sb) mg/kg 0.2 0.2 0.1 3605544

Total Arsenic (As) mg/kg 6.0 4.6 0.2 3605544

Total Barium (Ba) mg/kg 20.7 17.2 0.1 3605544

Total Beryllium (Be) mg/kg 0.1 0.1 0.1 3605544

Total Bismuth (Bi) mg/kg 0.1 0.1 0.1 3605544

Total Cadmium (Cd) mg/kg 0.68 0.53 0.05 3605544

Total Calcium (Ca) mg/kg 21700 9420 100 3605544

Total Chromium (Cr) mg/kg 13 11 1 3605544

Total Cobalt (Co) mg/kg 3.8 3.4 0.3 3605544

Total Copper (Cu) mg/kg 28.4 22.7 0.5 3605544

Total Iron (Fe) mg/kg 12700 11600 100 3605544

Total Lead (Pb) mg/kg 16.7 13.8 0.1 3605544

Total Magnesium (Mg) mg/kg 3970 3530 100 3605544

Total Manganese (Mn) mg/kg 137 122 0.2 3605544

Total Mercury (Hg) mg/kg <0.05 <0.05 0.05 3605544

Total Molybdenum (Mo) mg/kg 1.2 0.9 0.1 3605544

Total Nickel (Ni) mg/kg 9.3 7.8 0.8 3605544

Total Phosphorus (P) mg/kg 476 409 10 3605544

Total Potassium (K) mg/kg 1120 937 100 3605544

Total Selenium (Se) mg/kg 0.7 0.6 0.5 3605544

Total Silver (Ag) mg/kg 0.13 0.10 0.05 3605544

Total Sodium (Na) mg/kg 5260 3890 100 3605544

Total Strontium (Sr) mg/kg 140 60.4 0.1 3605544

Total Thallium (Tl) mg/kg 0.18 0.18 0.05 3605544

Total Tin (Sn) mg/kg 0.7 0.5 0.1 3605544

Total Titanium (Ti) mg/kg 284 282 1 3605544

Total Vanadium (V) mg/kg 24 24 2 3605544

Total Zinc (Zn) mg/kg 67 58 1 3605544


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15:00 15:45COC Number f156639 f156639


Total Zirconium (Zr) mg/kg 0.7 0.6 0.5 3605544


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PAH IN SOIL BY GC/MS (SEDIMENT)


11:29 14:19 12:10COC Number f156639 f156639 f156639


Polycyclic Aromatics

Low Molecular Weight PAH`s mg/kg 1.6 1.5 2.2 0.01 3601188

High Molecular Weight PAH`s mg/kg 10 6.6 11 0.02 3601188

Total PAH mg/kg 12 8.1 13 0.02 3601188

Naphthalene mg/kg 0.20 0.22 0.20 0.01 3603949

2-Methylnaphthalene mg/kg 0.16 0.18 0.17 0.01 3603949

Acenaphthylene mg/kg 0.13 0.11 0.14 0.01 3603949

Acenaphthene mg/kg 0.07 0.07 0.07 0.01 3603949

Fluorene mg/kg 0.12 0.12 0.19 0.01 3603949

Phenanthrene mg/kg 0.60 0.51 1.0 0.01 3603949

Anthracene mg/kg 0.34 0.26 0.44 0.01 3603949

Fluoranthene mg/kg 1.8 1.0 2.3 0.01 3603949

Pyrene mg/kg 2.9 1.8 2.6 0.01 3603949

Benzo(a)anthracene mg/kg 0.89 0.51 0.89 0.01 3603949

Chrysene mg/kg 1.4 0.90 2.0 0.01 3603949

Benzo(b&j)fluoranthene mg/kg 1.4 0.98 1.4 0.01 3603949

Benzo(k)fluoranthene mg/kg 0.52 0.37 0.53 0.01 3603949

Benzo(a)pyrene mg/kg 0.78 0.52 0.71 0.01 3603949

Indeno(1,2,3-cd)pyrene mg/kg 0.31 0.22 0.30 0.02 3603949

Dibenz(a,h)anthracene mg/kg 0.08 0.06 0.08 0.02 3603949

Benzo(g,h,i)perylene mg/kg 0.34 0.26 0.33 0.02 3603949


D10-ANTHRACENE (sur.) % 101 102 100 N/A 3603949

D12-BENZO(A)PYRENE (sur.) % 91 89 91 N/A 3603949

D8-ACENAPHTHYLENE (sur.) % 77 87 87 N/A 3603949

TERPHENYL-D14 (sur.) % 97 98 98 N/A 3603949


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15:00 15:45COC Number f156639 f156639



Low Molecular Weight PAH`s mg/kg 0.53 1.3 0.01 3601188

High Molecular Weight PAH`s mg/kg 2.3 5.4 0.02 3601188

Total PAH mg/kg 2.8 6.7 0.02 3601188

Naphthalene mg/kg 0.09 0.12 0.01 3603949

2-Methylnaphthalene mg/kg 0.05 0.07 0.01 3603949

Acenaphthylene mg/kg 0.04 0.07 0.01 3603949

Acenaphthene mg/kg 0.02 0.08 0.01 3603949

Fluorene mg/kg 0.03 0.10 0.01 3603949

Phenanthrene mg/kg 0.20 0.61 0.01 3603949

Anthracene mg/kg 0.08 0.20 0.01 3603949

Fluoranthene mg/kg 0.53 1.2 0.01 3603949

Pyrene mg/kg 0.62 1.6 0.01 3603949

Benzo(a)anthracene mg/kg 0.14 0.48 0.01 3603949

Chrysene mg/kg 0.34 0.70 0.01 3603949

Benzo(b&j)fluoranthene mg/kg 0.30 0.59 0.01 3603949

Benzo(k)fluoranthene mg/kg 0.10 0.23 0.01 3603949

Benzo(a)pyrene mg/kg 0.14 0.32 0.01 3603949

Indeno(1,2,3-cd)pyrene mg/kg 0.06 0.10 0.02 3603949

Dibenz(a,h)anthracene mg/kg <0.02 0.03 0.02 3603949

Benzo(g,h,i)perylene mg/kg 0.07 0.11 0.02 3603949


D10-ANTHRACENE (sur.) % 101 103 N/A 3603949

D12-BENZO(A)PYRENE (sur.) % 90 88 N/A 3603949

D8-ACENAPHTHYLENE (sur.) % 94 96 N/A 3603949

TERPHENYL-D14 (sur.) % 95 100 N/A 3603949


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Test Summary

Maxxam ID S00305 Collected 2009/12/01Sample ID IPS-SD09-20 Shipped 2009/12/01

Matrix Sediment Received 2009/12/01

Test Description Instrumentation Batch Extracted Analyzed AnalystElements by ICPMS (total) ICPM/MS 3605544 2009/12/03 2009/12/03 DJSimultaneously Extractable Metals-ICPMS ICPM/MS 3612878 2009/12/07 2009/12/08 DJMoisture BAL 3602004 N/A 2009/12/03 SW4PAH in Soil by GC/MS (SIM) GC/MSD 3603949 2009/12/02 2009/12/04 TG1Total LMW, HMW, Total PAH Calc GC/MSD 3601188 N/A 2009/12/04 ASCpH (2:1 DI Water Extract) /PH 3605960 2009/12/03 2009/12/03 CB9Sulfide (AVS) (soil) - Calc for umole/g SPEC/COL 3601189 2009/12/08 2009/12/08 ASCSulfide (AVS) (soil) SPEC/COL 3609489 2009/12/05 2009/12/07 DM9Total Organic Carbon LECO Method LECO 3611643 2009/12/07 2009/12/08 JLAEPH less PAH in Soil By GC/FID GC/FID 3601190 N/A 2009/12/04 ASCBC Hydrocarbons in Soil by GC/FID GC/FID 3605852 2009/12/02 2009/12/03 JP1Texture by Hydrometer HY 3609980 N/A 2009/12/07 JB9Texture Class CALC 3601265 N/A 2009/12/07 ASC

Maxxam ID S00305 D u p Collected 2009/12/01Sample ID IPS-SD09-20 Shipped 2009/12/01


Test Description Instrumentation Batch Extracted Analyzed AnalystTotal Organic Carbon LECO Method LECO 3611643 2009/12/07 2009/12/08 JLA




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Test Summary









Test Description Instrumentation Batch Extracted Analyzed AnalystSimultaneously Extractable Metals-ICPMS ICPM/MS 3612878 2009/12/07 2009/12/08 DJSulfide (AVS) (soil) SPEC/COL 3609489 2009/12/05 2009/12/07 DM9BC Hydrocarbons in Soil by GC/FID GC/FID 3605852 2009/12/03 2009/12/03 JP1

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Test Summary






Test Description Instrumentation Batch Extracted Analyzed AnalystElements by ICPMS (total) ICPM/MS 3605544 2009/12/03 2009/12/03 DJPAH in Soil by GC/MS (SIM) GC/MSD 3603949 2009/12/03 2009/12/04 TG1pH (2:1 DI Water Extract) /PH 3605960 2009/12/03 2009/12/03 CB9

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General Comments

Sample S00305-: ** SEM/AVS = 0.38 [SEM IS THE SUM OF CD CU HG NI PB AND ZN] **





Results relate only to the items tested.

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GOLDER ASSOCIATESTask Order#: 11062608Site#: P11605Site Location: Burrard Inlet Pipe Removal Port Moody BCProject #: SUPPLIMENTAL SEDIMENT CHARACTE

Quality Assurance ReportMaxxam Job Number: A968904

QA/QC DateBatch AnalyzedNum Init QC Type Parameter yyyy/mm/dd Value Recovery Units QC Limits

3602004 SW4 Method Blank Moisture 2009/12/03 <0.3 %3603949 TG1 Method Blank D10-ANTHRACENE (sur.) 2009/12/03 112 % 30 - 130

D12-BENZO(A)PYRENE (sur.) 2009/12/03 96 % 30 - 130D8-ACENAPHTHYLENE (sur.) 2009/12/03 98 % 30 - 130TERPHENYL-D14 (sur.) 2009/12/03 103 % 30 - 130Naphthalene 2009/12/03 <0.01 mg/kg2-Methylnaphthalene 2009/12/03 <0.01 mg/kgAcenaphthylene 2009/12/03 <0.01 mg/kgAcenaphthene 2009/12/03 <0.01 mg/kgFluorene 2009/12/03 <0.01 mg/kgPhenanthrene 2009/12/03 <0.01 mg/kgAnthracene 2009/12/03 <0.01 mg/kgFluoranthene 2009/12/03 <0.01 mg/kgPyrene 2009/12/03 <0.01 mg/kgBenzo(a)anthracene 2009/12/03 <0.01 mg/kgChrysene 2009/12/03 <0.01 mg/kgBenzo(b&j)fluoranthene 2009/12/03 <0.01 mg/kgBenzo(k)fluoranthene 2009/12/03 <0.01 mg/kgBenzo(a)pyrene 2009/12/03 <0.01 mg/kgIndeno(1,2,3-cd)pyrene 2009/12/03 <0.02 mg/kgDibenz(a,h)anthracene 2009/12/03 <0.02 mg/kgBenzo(g,h,i)perylene 2009/12/03 <0.02 mg/kg

3605544 DJ Method Blank Total Aluminum (Al) 2009/12/03 <100 mg/kgTotal Antimony (Sb) 2009/12/03 <0.1 mg/kgTotal Arsenic (As) 2009/12/03 <0.2 mg/kgTotal Barium (Ba) 2009/12/03 <0.1 mg/kgTotal Beryllium (Be) 2009/12/03 <0.1 mg/kgTotal Bismuth (Bi) 2009/12/03 <0.1 mg/kgTotal Cadmium (Cd) 2009/12/03 <0.05 mg/kgTotal Calcium (Ca) 2009/12/03 <100 mg/kgTotal Chromium (Cr) 2009/12/03 <1 mg/kgTotal Cobalt (Co) 2009/12/03 <0.3 mg/kgTotal Copper (Cu) 2009/12/03 <0.5 mg/kgTotal Iron (Fe) 2009/12/03 <100 mg/kgTotal Lead (Pb) 2009/12/03 <0.1 mg/kgTotal Magnesium (Mg) 2009/12/03 <100 mg/kgTotal Manganese (Mn) 2009/12/03 <0.2 mg/kgTotal Mercury (Hg) 2009/12/03 <0.05 mg/kgTotal Molybdenum (Mo) 2009/12/03 <0.1 mg/kgTotal Nickel (Ni) 2009/12/03 <0.8 mg/kgTotal Phosphorus (P) 2009/12/03 <10 mg/kgTotal Potassium (K) 2009/12/03 <100 mg/kgTotal Selenium (Se) 2009/12/03 <0.5 mg/kgTotal Silver (Ag) 2009/12/03 <0.05 mg/kgTotal Sodium (Na) 2009/12/03 <100 mg/kgTotal Strontium (Sr) 2009/12/03 <0.1 mg/kgTotal Thallium (Tl) 2009/12/03 <0.05 mg/kgTotal Tin (Sn) 2009/12/03 <0.1 mg/kgTotal Titanium (Ti) 2009/12/03 <1 mg/kgTotal Vanadium (V) 2009/12/03 <2 mg/kgTotal Zinc (Zn) 2009/12/03 <1 mg/kgTotal Zirconium (Zr) 2009/12/03 <0.5 mg/kg

3605852 JP1 Method Blank O-TERPHENYL (sur.) 2009/12/03 91 % 50 - 130EPH (C10-C19) 2009/12/03 <100 mg/kgEPH (C19-C32) 2009/12/03 <100 mg/kg


Page 17 of 28


Quality Assurance Report (Continued)Maxxam Job Number: A968904


3609489 DM9 Method Blank Sulphide 2009/12/07 <0.2 ug/g3609980 JB9 Method Blank % sand by hydrometer 2009/12/07 <2 %

% silt by hydrometer 2009/12/07 <2 %Clay Content 2009/12/07 <2 %

3611643 JLA Method Blank Total Organic Carbon (C) 2009/12/08 0.02, RDL=0.02 %3612878 DJ Method Blank SEM Cadmium (Cd) 2009/12/08 <0.0002 umole/g

SEM Copper (Cu) 2009/12/08 <0.004 umole/gSEM Lead (Pb) 2009/12/08 <0.0002 umole/gSEM Mercury (Hg) 2009/12/08 <0.0003 umole/gSEM Nickel (Ni) 2009/12/08 <0.004 umole/gSEM Zinc (Zn) 2009/12/08 <0.008 umole/g

3611643 JLA RPD [ S 0 0 3 0 5 - 0 2 ] Total Organic Carbon (C) 2009/12/08 2.4 ( 1 ) % 503605852 JP1 RPD [ S 0 0 3 1 2 - 0 1 ] EPH (C10-C19) 2009/12/03 NC % 50

EPH (C19-C32) 2009/12/03 NC % 503609489 DM9 RPD [ S 0 0 3 1 2 - 0 4 ] Sulphide 2009/12/07 25.1 % 303612878 DJ RPD [ S 0 0 3 1 2 - 0 4 ] SEM Cadmium (Cd) 2009/12/08 21.5 % 30

SEM Copper (Cu) 2009/12/08 18.8 % 30SEM Lead (Pb) 2009/12/08 18.2 % 30SEM Mercury (Hg) 2009/12/08 NC % 30SEM Nickel (Ni) 2009/12/08 24.8 % 30SEM Zinc (Zn) 2009/12/08 17.4 % 30

3603949 TG1 RPD [ S 0 0 3 1 3 - 0 1 ] Naphthalene 2009/12/04 13.8 % 502-Methylnaphthalene 2009/12/04 1.4 % 50Acenaphthylene 2009/12/04 6.8 % 50Acenaphthene 2009/12/04 10.8 % 50Fluorene 2009/12/04 7.0 % 50Phenanthrene 2009/12/04 33.3 % 50Anthracene 2009/12/04 5.1 % 50Fluoranthene 2009/12/04 18.9 % 50Pyrene 2009/12/04 11.5 % 50Benzo(a)anthracene 2009/12/04 29.1 % 50Chrysene 2009/12/04 2.8 % 50Benzo(b&j)fluoranthene 2009/12/04 3.6 % 50Benzo(k)fluoranthene 2009/12/04 7.5 % 50Benzo(a)pyrene 2009/12/04 3.4 % 50Indeno(1,2,3-cd)pyrene 2009/12/04 3.2 % 50Dibenz(a,h)anthracene 2009/12/04 NC % 50Benzo(g,h,i)perylene 2009/12/04 6.8 % 50

3605544 DJ RPD [ S 0 0 3 1 3 - 0 1 ] Total Aluminum (Al) 2009/12/03 3.9 % 35Total Antimony (Sb) 2009/12/03 NC % 30Total Arsenic (As) 2009/12/03 5.7 % 30Total Barium (Ba) 2009/12/03 0.9 % 35Total Beryllium (Be) 2009/12/03 NC % 30Total Bismuth (Bi) 2009/12/03 NC % 30Total Cadmium (Cd) 2009/12/03 4.6 % 30Total Calcium (Ca) 2009/12/03 1.0 % 30Total Chromium (Cr) 2009/12/03 4.6 % 30Total Cobalt (Co) 2009/12/03 2.0 % 30Total Copper (Cu) 2009/12/03 3.0 % 30Total Iron (Fe) 2009/12/03 3.5 % 30Total Lead (Pb) 2009/12/03 0.09 % 35Total Magnesium (Mg) 2009/12/03 4.3 % 30Total Manganese (Mn) 2009/12/03 0.3 % 30Total Mercury (Hg) 2009/12/03 NC % 35Total Molybdenum (Mo) 2009/12/03 5.7 % 35


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3605544 DJ RPD [ S 0 0 3 1 3 - 0 1 ] Total Nickel (Ni) 2009/12/03 2.7 % 30Total Phosphorus (P) 2009/12/03 0.6 % 30Total Potassium (K) 2009/12/03 3.9 % 35Total Selenium (Se) 2009/12/03 NC % 30Total Silver (Ag) 2009/12/03 NC % 35Total Sodium (Na) 2009/12/03 3.4 % 35Total Strontium (Sr) 2009/12/03 1.7 % 35Total Thallium (Tl) 2009/12/03 NC % 30Total Tin (Sn) 2009/12/03 NC % 35Total Titanium (Ti) 2009/12/03 3.0 % 35Total Vanadium (V) 2009/12/03 2.5 % 30Total Zinc (Zn) 2009/12/03 1.1 % 30Total Zirconium (Zr) 2009/12/03 NC % 30

3605960 CB9 RPD [ S 0 0 3 1 3 - 0 1 ] Soluble (2:1) pH 2009/12/03 0 % 203603949 TG1 Matrix Spike

[S00313-01] D10-ANTHRACENE (sur.) 2009/12/04 93 % 30 - 130D12-BENZO(A)PYRENE (sur.) 2009/12/04 89 % 30 - 130D8-ACENAPHTHYLENE (sur.) 2009/12/04 100 % 30 - 130TERPHENYL-D14 (sur.) 2009/12/04 97 % 30 - 130Naphthalene 2009/12/04 88 % 50 - 1302-Methylnaphthalene 2009/12/04 87 % 50 - 130Acenaphthylene 2009/12/04 86 % 50 - 130Acenaphthene 2009/12/04 92 % 50 - 130Fluorene 2009/12/04 90 % 50 - 130Phenanthrene 2009/12/04 87 % 60 - 130Anthracene 2009/12/04 82 % 60 - 130Fluoranthene 2009/12/04 82 % 60 - 130Pyrene 2009/12/04 83 % 60 - 130Benzo(a)anthracene 2009/12/04 83 % 60 - 130Chrysene 2009/12/04 81 % 60 - 130Benzo(b&j)fluoranthene 2009/12/04 83 % 60 - 130Benzo(k)fluoranthene 2009/12/04 80 % 60 - 130Benzo(a)pyrene 2009/12/04 84 % 60 - 130Indeno(1,2,3-cd)pyrene 2009/12/04 77 % 60 - 130Dibenz(a,h)anthracene 2009/12/04 78 % 60 - 130Benzo(g,h,i)perylene 2009/12/04 77 % 60 - 130

3605544 DJ Matrix Spike[S00313-01] Total Arsenic (As) 2009/12/03 107 % 75 - 125

Total Beryllium (Be) 2009/12/03 101 % 75 - 125Total Cadmium (Cd) 2009/12/03 105 % 75 - 125Total Chromium (Cr) 2009/12/03 102 % 75 - 125Total Cobalt (Co) 2009/12/03 104 % 75 - 125Total Copper (Cu) 2009/12/03 110 % 75 - 125Total Lead (Pb) 2009/12/03 102 % 75 - 125Total Mercury (Hg) 2009/12/03 107 % 75 - 125Total Nickel (Ni) 2009/12/03 103 % 75 - 125Total Selenium (Se) 2009/12/03 107 % 75 - 125Total Vanadium (V) 2009/12/03 102 % 75 - 125Total Zinc (Zn) 2009/12/03 NC % 75 - 125

3605852 JP1 Matrix Spike[S00312-01] O-TERPHENYL (sur.) 2009/12/03 93 % 50 - 130

EPH (C10-C19) 2009/12/03 110 % 50 - 130EPH (C19-C32) 2009/12/03 108 % 50 - 130

3609489 DM9 Matrix Spike[S00312-04] Sulphide 2009/12/07 NC % 75 - 125


Page 19 of 28




3603949 TG1 LCS D10-ANTHRACENE (sur.) 2009/12/04 99 % 30 - 130D12-BENZO(A)PYRENE (sur.) 2009/12/04 99 % 30 - 130D8-ACENAPHTHYLENE (sur.) 2009/12/04 98 % 30 - 130TERPHENYL-D14 (sur.) 2009/12/04 100 % 30 - 130Naphthalene 2009/12/04 96 % 50 - 1302-Methylnaphthalene 2009/12/04 96 % 50 - 130Acenaphthylene 2009/12/04 93 % 50 - 130Acenaphthene 2009/12/04 100 % 50 - 130Fluorene 2009/12/04 100 % 50 - 130Phenanthrene 2009/12/04 100 % 60 - 130Anthracene 2009/12/04 97 % 60 - 130Fluoranthene 2009/12/04 98 % 60 - 130Pyrene 2009/12/04 96 % 60 - 130Benzo(a)anthracene 2009/12/04 97 % 60 - 130Chrysene 2009/12/04 96 % 60 - 130Benzo(b&j)fluoranthene 2009/12/04 97 % 60 - 130Benzo(k)fluoranthene 2009/12/04 95 % 60 - 130Benzo(a)pyrene 2009/12/04 100 % 60 - 130Indeno(1,2,3-cd)pyrene 2009/12/04 91 % 60 - 130Dibenz(a,h)anthracene 2009/12/04 91 % 60 - 130Benzo(g,h,i)perylene 2009/12/04 90 % 60 - 130

3605544 DJ LCS Total Arsenic (As) 2009/12/03 98 % 75 - 125Total Beryllium (Be) 2009/12/03 90 % 75 - 125Total Cadmium (Cd) 2009/12/03 102 % 75 - 125Total Chromium (Cr) 2009/12/03 99 % 75 - 125Total Cobalt (Co) 2009/12/03 98 % 75 - 125Total Copper (Cu) 2009/12/03 102 % 75 - 125Total Lead (Pb) 2009/12/03 100 % 75 - 125Total Mercury (Hg) 2009/12/03 110 % 75 - 125Total Nickel (Ni) 2009/12/03 99 % 75 - 125Total Selenium (Se) 2009/12/03 102 % 75 - 125Total Vanadium (V) 2009/12/03 100 % 75 - 125Total Zinc (Zn) 2009/12/03 98 % 75 - 125

3605852 JP1 LCS O-TERPHENYL (sur.) 2009/12/03 94 % 50 - 130EPH (C10-C19) 2009/12/03 96 % 50 - 130EPH (C19-C32) 2009/12/03 95 % 50 - 130

3605960 CB9 LCS Soluble (2:1) pH 2009/12/03 100 % 96 - 1043609489 DM9 LCS Sulphide 2009/12/07 85 % 75 - 1253611643 JLA LCS Total Organic Carbon (C) 2009/12/08 108 % 75 - 1253605544 DJ SRM Total Aluminum (Al) 2009/12/03 92 % 70 - 130

Total Antimony (Sb) 2009/12/03 102 % 70 - 130Total Arsenic (As) 2009/12/03 91 % 70 - 130Total Barium (Ba) 2009/12/03 100 % 70 - 130Total Cadmium (Cd) 2009/12/03 91 % 70 - 130Total Calcium (Ca) 2009/12/03 91 % 70 - 130Total Chromium (Cr) 2009/12/03 88 % 70 - 130Total Cobalt (Co) 2009/12/03 92 % 70 - 130Total Copper (Cu) 2009/12/03 89 % 70 - 130Total Iron (Fe) 2009/12/03 92 % 70 - 130Total Lead (Pb) 2009/12/03 96 % 70 - 130Total Magnesium (Mg) 2009/12/03 96 % 70 - 130Total Manganese (Mn) 2009/12/03 95 % 70 - 130Total Molybdenum (Mo) 2009/12/03 86 % 70 - 130Total Nickel (Ni) 2009/12/03 93 % 70 - 130Total Phosphorus (P) 2009/12/03 97 % 70 - 130


Page 20 of 28




3605544 DJ SRM Total Silver (Ag) 2009/12/03 87 % 70 - 130Total Strontium (Sr) 2009/12/03 96 % 70 - 130Total Thallium (Tl) 2009/12/03 84 % 70 - 130Total Titanium (Ti) 2009/12/03 96 % 70 - 130Total Vanadium (V) 2009/12/03 94 % 70 - 130Total Zinc (Zn) 2009/12/03 85 % 70 - 130

3609980 JB9 SRM % sand by hydrometer 2009/12/07 94 % 75 - 125% silt by hydrometer 2009/12/07 112 % 75 - 125Clay Content 2009/12/07 91 % 75 - 125

3611643 JLA SRM Total Organic Carbon (C) 2009/12/08 113 % 75 - 125

Duplicate: Paired analysis of a separate portion of the same sample. Used to evaluate the variance in the measurement.Matrix Spike: A sample to which a known amount of the analyte of interest has been added. Used to evaluate sample matrix interference.SRM: A blank matrix sample to which a known amount of the analyte has been added. Used to evaluate analyte recovery.LCS: A blank matrix sample to which a known amount of the analyte has been added. Used to evaluate analyte recovery.Method Blank: A blank matrix containing all reagents used in the analytical procedure. Used to identify laboratory contamination.Surrogate: A pure or isotopically labeled compound whose behavior mirrors the analytes of interest. Used to evaluate extraction efficiency.NC (Matrix Spike): The recovery in the matrix spike was not calculated. The relative difference between the concentration in the parent sample and thespiked amount was not sufficiently significant to permit a reliable recovery calculation.NC (RPD): The RPD was not calculated. The level of analyte detected in the parent sample and its duplicate was not sufficiently significant to permit areliable calculation.( 1 ) Detection limits raised due to dilution to bring analyte within the calibrated range.


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GOLDER ASSOCIATESReport Date: 2009/12/09 Task Order#: 11062608Maxxam Job #: A968904 Site#: P11605

Site Location: Burrard Inlet Pipe Removal Port Moody BCMaxxam Sample: S00305 Client ID: IPS-SD09-20

BC Hydrocarbons in Soil by GC/FID Chromatogram

Note: This information is provided for reference purposes only. Should detailed chemist intrepretationor fingerprinting be required to please contact the laboratory.

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Task Order#: 11062608Site#: P11605Site Location: Burrard Inlet Pipe Removal Port Moody BCProject #: 08-1436-0046-6075Your C.O.C. #: f156650Attention: Blair MacDonald






Analyses Quantity Laboratory Method Primary referenceEnvironmental Sample Disposal Fee 9Elements by ICPMS (total) 9 BRN SOP-00203 R5.0 Based on EPA 200.8Simultaneously Extractable Metals-ICPMS 9 BRN SOP-00203 5.0 Based on EPA 200.8Moisture 9 BRN SOP-00321 R5.0 Ont MOE -E 3139PAH in Soil by GC/MS (SIM) 9 BRN SOP-00332 R9.0 Based on EPA 8270DTotal LMW, HMW, Total PAH Calc 9pH (2:1 DI Water Extract) ( 3 ) 9 BRN SOP-00266 R6.0 Carter, SSMA 16.2Sulfide (AVS) (soil) - Calc for umole/g 9 BRN SOP-00229 R2.0 Based EPA821-R91-100Sulfide (AVS) (soil) 9 BRN SOP-00229 R2.0 Based EPA821-R91-100EPH less PAH in Soil By GC/FID ( 3 ) 9BC Hydrocarbons in Soil by GC/FID ( 3 ) 9 BRN SOP-00341 R14 Based BCCSR Method 3Texture by Hydrometer ( 1 ) 9 EENVSOP-00076 MMFSPA Ch9Texture Class ( 1 ) 9 EENVSOP-00076 MMFSPA Ch9TOC Soil Subcontract ( 2 ) 9

Remarks:




All analysis data reported was generated when the analytical methods were in statistical control and criteria for spike

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Task Order#: 11062608Site#: P11605Site Location: Burrard Inlet Pipe Removal Port Moody BCProject #: 08-1436-0046-6075Your C.O.C. #: f156650Attention: Blair MacDonald




MAXXAM JOB #: A969147Received: 2009/12/02, 17:30recoveries, reference material recoveries, method blanks data and duplicate precision were met unless otherwise stated.All samples were analysed within hold time unless otherwise flagged. All BTEX samples were methanol extracted within 24hours unless otherwise flagged.This report shall not be reproduced except in full, without the written approval of the laboratory.




(1) This test was performed by Maxxam Edmonton Environmental(2) This test was performed by Maxxam Bedford(From Burnaby)(3) SCC/CAEAL

Encryption Key






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Sue Reynolds

11 Dec 2009 15:11:35 -08:00


Site Location: Burrard Inlet Pipe Removal Port Moody BCProject #: 08-1436-0046-6075



10:33 09:24 09:34COC Number f156650 f156650 f156650

U n i t s IPS-SD09-39 R D L IPS-SD09-29 IPS-SD09-38 R D L QC Batch

Parameter

Subcontract Parameter N/A ATTACHED N/A ATTACHED ATTACHED N/A 3620899


Sulphide umole/g 9.2 0.3 20.0 24.2 0.6 3604581

MISCELLANEOUS

Sulphide ug/g 294 10 643 777 20 3609489

Physical Properties



Clay Content % 21 2 28 22 2 3619011

Texture N/A LOAM N/A SILT LOAM LOAM N/A 3604572

Moisture % 70 0.3 72 74 0.3 3604691


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15:16 14:15 10:23COC Number f156650 f156650 f156650

U n i t s IPS-SD09-REF2 R D L IPS-SD09-REF1 IPS-SD09-28 R D L QC Batch

Parameter

Subcontract Parameter N/A ATTACHED N/A ATTACHED ATTACHED N/A 3620899


Sulphide umole/g 0.007 0.006 7.3 8.0 0.3 3604581

MISCELLANEOUS

Sulphide ug/g 0.2 0.2 234 256 10 3609489

Physical Properties



Clay Content % 30 2 30 25 2 3619248

Texture N/A SLTY CL LO N/A SLTY CL LO LOAM N/A 3604572

Moisture % 68 0.3 72 68 0.3 3604691


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11:04 12:12 12:47COC Number f156650 f156650 f156650

U n i t s IPS-SD09-30 IPS-SD09-31 R D L IPS-SD09-32 R D L QC Batch

Parameter

Subcontract Parameter N/A ATTACHED ATTACHED N/A ATTACHED N/A 3620899


Sulphide umole/g 13.6 4.8 0.3 0.69 0.01 3604581

MISCELLANEOUS

Sulphide ug/g 435 155 10 22.1 0.4 3609489

Physical Properties



Clay Content % 31 26 2 27 2 3619248

Texture N/A SLTY CL LO SILT LOAM N/A SILT LOAM N/A 3604572

Moisture % 72 69 0.3 69 0.3 3604691


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10:33 09:24 09:34COC Number f156650 f156650 f156650


SEM Metals by ICPMS









15:16 14:15 10:23COC Number f156650 f156650 f156650

U n i t s IPS-SD09-REF2 IPS-SD09-REF1 IPS-SD09-28 R D L QC Batch

SEM Metals by ICPMS








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11:04 12:12 12:47COC Number f156650 f156650 f156650


SEM Metals by ICPMS








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10:33 09:24 09:34COC Number f156650 f156650 f156650





Hydrocarbons

EPH (C10-C19) mg/kg <100 <100 <100 100 3605852

EPH (C19-C32) mg/kg 447 460 498 100 3605852





15:16 14:15 10:23COC Number f156650 f156650 f156650





Hydrocarbons

EPH (C10-C19) mg/kg <100 <100 <100 100 3606237

EPH (C19-C32) mg/kg 396 388 471 100 3606237




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11:04 12:12 12:47COC Number f156650 f156650 f156650





Hydrocarbons

EPH (C10-C19) mg/kg <100 <100 <100 100 3606237

EPH (C19-C32) mg/kg 493 373 492 100 3606237




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10:33 09:24 09:34COC Number f156650 f156650 f156650


Misc. Inorganics













Total Copper (Cu) mg/kg 83.9 96.3 97.4 0.5 3608381













Total Strontium (Sr) mg/kg 100 110 126 0.1 3608381


Total Tin (Sn) mg/kg 1.8 2.0 2.0 0.1 3608381





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10:33 09:24 09:34COC Number f156650 f156650 f156650




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15:16 14:15 10:23COC Number f156650 f156650 f156650


Misc. Inorganics


























Total Strontium (Sr) mg/kg 58.3 72.3 105 0.1 3608381


Total Tin (Sn) mg/kg 1.6 1.6 1.9 0.1 3608381





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15:16 14:15 10:23COC Number f156650 f156650 f156650




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11:04 12:12 12:47COC Number f156650 f156650 f156650


Misc. Inorganics













Total Copper (Cu) mg/kg 102 83.5 87.5 0.5 3608381















Total Tin (Sn) mg/kg 2.2 1.9 2.3 0.1 3608381





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11:04 12:12 12:47COC Number f156650 f156650 f156650




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10:33 09:24 09:34COC Number f156650 f156650 f156650




High Molecular Weight PAH`s mg/kg 26 29 25 0.02 3603756

Total PAH mg/kg 30 34 28 0.02 3603756





Fluorene mg/kg 0.28 0.46 0.37 0.01 3607122


Anthracene mg/kg 0.78 1.2 0.86 0.01 3607122


Pyrene mg/kg 8.0 9.1 8.0 0.01 3607122


Chrysene mg/kg 3.8 4.3 3.0 0.01 3607122













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15:16 14:15 10:23COC Number f156650 f156650 f156650




High Molecular Weight PAH`s mg/kg 1.8 3.9 21 0.02 3603756

Total PAH mg/kg 2.5 4.7 26 0.02 3603756





Fluorene mg/kg 0.07 0.07 0.28 0.01 3607122


Anthracene mg/kg 0.06 0.11 0.59 0.01 3607122


Pyrene mg/kg 0.39 0.77 6.8 0.01 3607122


Chrysene mg/kg 0.19 0.49 2.7 0.01 3607122













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11:04 12:12 12:47COC Number f156650 f156650 f156650




High Molecular Weight PAH`s mg/kg 14 2.9 2.6 0.02 3603756

Total PAH mg/kg 16 3.7 3.6 0.02 3603756





Fluorene mg/kg 0.19 0.06 0.08 0.01 3607122


Anthracene mg/kg 0.51 0.12 0.13 0.01 3607122


Pyrene mg/kg 4.5 0.83 0.74 0.01 3607122


Chrysene mg/kg 2.2 0.29 0.34 0.01 3607122













Page 18 of 38



Test Summary



Test Description Instrumentation Batch Extracted Analyzed AnalystElements by ICPMS (total) ICPM/MS 3608381 2009/12/04 2009/12/04 JC8Simultaneously Extractable Metals-ICPMS ICPM/MS 3612878 2009/12/07 2009/12/08 DJMoisture BAL 3604691 N/A 2009/12/03 SW4PAH in Soil by GC/MS (SIM) GC/MSD 3607122 2009/12/03 2009/12/04 TG1Total LMW, HMW, Total PAH Calc GC/MSD 3603756 N/A 2009/12/07 ASCpH (2:1 DI Water Extract) /PH 3608419 2009/12/04 2009/12/04 AL8Sulfide (AVS) (soil) - Calc for umole/g SPEC/COL 3604581 2009/12/08 2009/12/08 ASCSulfide (AVS) (soil) SPEC/COL 3609489 2009/12/05 2009/12/07 DM9EPH less PAH in Soil By GC/FID GC/FID 3603757 N/A 2009/12/07 ASCBC Hydrocarbons in Soil by GC/FID GC/FID 3605852 2009/12/03 2009/12/03 JP1Texture by Hydrometer HY 3619011 N/A 2009/12/10 JB9Texture Class CALC 3604572 N/A 2009/12/10 ASCTOC Soil Subcontract 3620899 2009/12/10 2009/12/10 SR6






Test Description Instrumentation Batch Extracted Analyzed AnalystElements by ICPMS (total) ICPM/MS 3608381 2009/12/04 2009/12/04 JC8Simultaneously Extractable Metals-ICPMS ICPM/MS 3612878 2009/12/07 2009/12/08 DJMoisture BAL 3604691 N/A 2009/12/03 SW4PAH in Soil by GC/MS (SIM) GC/MSD 3607122 2009/12/03 2009/12/04 TG1Total LMW, HMW, Total PAH Calc GC/MSD 3603756 N/A 2009/12/07 ASCpH (2:1 DI Water Extract) /PH 3608419 2009/12/04 2009/12/04 AL8Sulfide (AVS) (soil) - Calc for umole/g SPEC/COL 3604581 2009/12/08 2009/12/08 ASCSulfide (AVS) (soil) SPEC/COL 3609489 2009/12/05 2009/12/07 DM9EPH less PAH in Soil By GC/FID GC/FID 3603757 N/A 2009/12/07 ASCBC Hydrocarbons in Soil by GC/FID GC/FID 3605852 2009/12/03 2009/12/03 JP1Texture by Hydrometer HY 3619011 N/A 2009/12/10 JB9Texture Class CALC 3604572 N/A 2009/12/10 ASC

Page 19 of 38



Test Summary

TOC Soil Subcontract 3620899 2009/12/10 2009/12/10 SR6

Maxxam ID S01927 Collected 2009/12/02Sample ID IPS-SD09-REF2 Shipped 2009/12/02


Test Description Instrumentation Batch Extracted Analyzed AnalystElements by ICPMS (total) ICPM/MS 3608381 2009/12/04 2009/12/04 JC8Simultaneously Extractable Metals-ICPMS ICPM/MS 3612878 2009/12/07 2009/12/08 DJMoisture BAL 3604691 N/A 2009/12/03 SW4PAH in Soil by GC/MS (SIM) GC/MSD 3607122 2009/12/03 2009/12/04 TG1Total LMW, HMW, Total PAH Calc GC/MSD 3603756 N/A 2009/12/07 ASCpH (2:1 DI Water Extract) /PH 3608419 2009/12/04 2009/12/04 AL8Sulfide (AVS) (soil) - Calc for umole/g SPEC/COL 3604581 2009/12/08 2009/12/08 ASCSulfide (AVS) (soil) SPEC/COL 3609489 2009/12/05 2009/12/07 DM9EPH less PAH in Soil By GC/FID GC/FID 3603757 N/A 2009/12/07 ASCBC Hydrocarbons in Soil by GC/FID GC/FID 3606237 2009/12/03 2009/12/03 JP1Texture by Hydrometer HY 3619248 N/A 2009/12/11 JB9Texture Class CALC 3604572 N/A 2009/12/11 DT3TOC Soil Subcontract 3620899 2009/12/10 2009/12/10 SR6

Maxxam ID S01928 Collected 2009/12/02Sample ID IPS-SD09-REF1 Shipped 2009/12/02





Test Description Instrumentation Batch Extracted Analyzed AnalystElements by ICPMS (total) ICPM/MS 3608381 2009/12/04 2009/12/04 JC8Simultaneously Extractable Metals-ICPMS ICPM/MS 3612878 2009/12/07 2009/12/08 DJMoisture BAL 3604691 N/A 2009/12/03 SW4PAH in Soil by GC/MS (SIM) GC/MSD 3607122 2009/12/03 2009/12/04 TG1Total LMW, HMW, Total PAH Calc GC/MSD 3603756 N/A 2009/12/07 ASCpH (2:1 DI Water Extract) /PH 3608419 2009/12/04 2009/12/04 AL8Sulfide (AVS) (soil) - Calc for umole/g SPEC/COL 3604581 2009/12/08 2009/12/08 ASCSulfide (AVS) (soil) SPEC/COL 3609489 2009/12/05 2009/12/07 DM9EPH less PAH in Soil By GC/FID GC/FID 3603757 N/A 2009/12/07 ASC

Page 20 of 38



Test Summary

BC Hydrocarbons in Soil by GC/FID GC/FID 3606237 2009/12/03 2009/12/03 JP1Texture by Hydrometer HY 3619248 N/A 2009/12/11 JB9Texture Class CALC 3604572 N/A 2009/12/11 ASCTOC Soil Subcontract 3620899 2009/12/10 2009/12/10 SR6



Test Description Instrumentation Batch Extracted Analyzed AnalystMoisture BAL 3604691 N/A 2009/12/03 SW4







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Test Summary



Test Description Instrumentation Batch Extracted Analyzed AnalystBC Hydrocarbons in Soil by GC/FID GC/FID 3606237 2009/12/03 2009/12/03 JP1






Test Description Instrumentation Batch Extracted Analyzed AnalystPAH in Soil by GC/MS (SIM) GC/MSD 3607122 2009/12/04 2009/12/04 TG1

Page 22 of 38



General Comments




Sample S01927-: ** SEM/AVS = 364.87 [SEM IS THE SUM OF CD CU HG NI PB AND ZN] ** SLTY CL LO = SILTY CLAY LOAM







Page 23 of 38

GOLDER ASSOCIATESTask Order#: 11062608Site#: P11605Site Location: Burrard Inlet Pipe Removal Port Moody BCProject #: 08-1436-0046-6075



3604691 SW4 Method Blank Moisture 2009/12/03 <0.3 %3605852 JP1 Method Blank O-TERPHENYL (sur.) 2009/12/03 91 % 50 - 130

EPH (C10-C19) 2009/12/03 <100 mg/kgEPH (C19-C32) 2009/12/03 <100 mg/kg


3607122 TG1 Method Blank D10-ANTHRACENE (sur.) 2009/12/04 98 % 30 - 130D12-BENZO(A)PYRENE (sur.) 2009/12/04 94 % 30 - 130D8-ACENAPHTHYLENE (sur.) 2009/12/04 93 % 30 - 130TERPHENYL-D14 (sur.) 2009/12/04 96 % 30 - 130Naphthalene 2009/12/04 <0.01 mg/kg2-Methylnaphthalene 2009/12/04 <0.01 mg/kgAcenaphthylene 2009/12/04 <0.01 mg/kgAcenaphthene 2009/12/04 <0.01 mg/kgFluorene 2009/12/04 <0.01 mg/kgPhenanthrene 2009/12/04 <0.01 mg/kgAnthracene 2009/12/04 <0.01 mg/kgFluoranthene 2009/12/04 <0.01 mg/kgPyrene 2009/12/04 <0.01 mg/kgBenzo(a)anthracene 2009/12/04 <0.01 mg/kgChrysene 2009/12/04 <0.01 mg/kgBenzo(b&j)fluoranthene 2009/12/04 <0.01 mg/kgBenzo(k)fluoranthene 2009/12/04 <0.01 mg/kgBenzo(a)pyrene 2009/12/04 <0.01 mg/kgIndeno(1,2,3-cd)pyrene 2009/12/04 <0.02 mg/kgDibenz(a,h)anthracene 2009/12/04 <0.02 mg/kgBenzo(g,h,i)perylene 2009/12/04 <0.02 mg/kg

3608381 JC8 Method Blank Total Aluminum (Al) 2009/12/04 <100 mg/kgTotal Antimony (Sb) 2009/12/04 <0.1 mg/kgTotal Arsenic (As) 2009/12/04 <0.2 mg/kgTotal Barium (Ba) 2009/12/04 <0.1 mg/kgTotal Beryllium (Be) 2009/12/04 <0.1 mg/kgTotal Bismuth (Bi) 2009/12/04 <0.1 mg/kgTotal Cadmium (Cd) 2009/12/04 <0.05 mg/kgTotal Calcium (Ca) 2009/12/04 <100 mg/kgTotal Chromium (Cr) 2009/12/04 <1 mg/kgTotal Cobalt (Co) 2009/12/04 <0.3 mg/kgTotal Copper (Cu) 2009/12/04 <0.5 mg/kgTotal Iron (Fe) 2009/12/04 <100 mg/kgTotal Lead (Pb) 2009/12/04 <0.1 mg/kgTotal Magnesium (Mg) 2009/12/04 <100 mg/kgTotal Manganese (Mn) 2009/12/04 <0.2 mg/kgTotal Mercury (Hg) 2009/12/04 <0.05 mg/kgTotal Molybdenum (Mo) 2009/12/04 <0.1 mg/kgTotal Nickel (Ni) 2009/12/04 <0.8 mg/kgTotal Phosphorus (P) 2009/12/04 <10 mg/kgTotal Potassium (K) 2009/12/04 <100 mg/kgTotal Selenium (Se) 2009/12/04 <0.5 mg/kgTotal Silver (Ag) 2009/12/04 <0.05 mg/kgTotal Sodium (Na) 2009/12/04 <100 mg/kgTotal Strontium (Sr) 2009/12/04 <0.1 mg/kgTotal Thallium (Tl) 2009/12/04 <0.05 mg/kgTotal Tin (Sn) 2009/12/04 <0.1 mg/kgTotal Titanium (Ti) 2009/12/04 <1 mg/kg


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3608381 JC8 Method Blank Total Vanadium (V) 2009/12/04 <2 mg/kgTotal Zinc (Zn) 2009/12/04 <1 mg/kgTotal Zirconium (Zr) 2009/12/04 <0.5 mg/kg

3609489 DM9 Method Blank Sulphide 2009/12/07 <0.2 ug/g3612878 DJ Method Blank SEM Cadmium (Cd) 2009/12/08 <0.0002 umole/g

SEM Copper (Cu) 2009/12/08 <0.004 umole/gSEM Lead (Pb) 2009/12/08 <0.0002 umole/gSEM Mercury (Hg) 2009/12/08 <0.0003 umole/gSEM Nickel (Ni) 2009/12/08 <0.004 umole/gSEM Zinc (Zn) 2009/12/08 <0.008 umole/g

3619011 JB9 Method Blank % sand by hydrometer 2009/12/10 <2 %% silt by hydrometer 2009/12/10 <2 %Clay Content 2009/12/10 <2 %


3604691 SW4 RPD [ S 0 1 9 2 9 - 0 1 ] Moisture 2009/12/03 1.0 % 203606237 JP1 RPD [ S 0 1 9 3 1 - 0 1 ] EPH (C10-C19) 2009/12/03 NC % 50

EPH (C19-C32) 2009/12/03 NC % 503607122 TG1 RPD [ S 0 1 9 3 2 - 0 1 ] Naphthalene 2009/12/04 16.0 % 50

2-Methylnaphthalene 2009/12/04 13.4 % 50Acenaphthylene 2009/12/04 4.7 % 50Acenaphthene 2009/12/04 NC % 50Fluorene 2009/12/04 12.6 % 50Phenanthrene 2009/12/04 13.5 % 50Anthracene 2009/12/04 16.8 % 50Fluoranthene 2009/12/04 7.3 % 50Pyrene 2009/12/04 10.5 % 50Benzo(a)anthracene 2009/12/04 9.0 % 50Chrysene 2009/12/04 25.7 % 50Benzo(b&j)fluoranthene 2009/12/04 5.4 % 50Benzo(k)fluoranthene 2009/12/04 6.6 % 50Benzo(a)pyrene 2009/12/04 7.3 % 50Indeno(1,2,3-cd)pyrene 2009/12/04 NC % 50Dibenz(a,h)anthracene 2009/12/04 NC % 50Benzo(g,h,i)perylene 2009/12/04 7.5 % 50


EPH (C10-C19) 2009/12/03 97 % 50 - 130EPH (C19-C32) 2009/12/03 NC % 50 - 130

3607122 TG1 Matrix Spike[S01932-01] D10-ANTHRACENE (sur.) 2009/12/04 84 % 30 - 130

D12-BENZO(A)PYRENE (sur.) 2009/12/04 84 % 30 - 130D8-ACENAPHTHYLENE (sur.) 2009/12/04 80 % 30 - 130TERPHENYL-D14 (sur.) 2009/12/04 89 % 30 - 130Naphthalene 2009/12/04 86 % 50 - 1302-Methylnaphthalene 2009/12/04 86 % 50 - 130Acenaphthylene 2009/12/04 76 % 50 - 130Acenaphthene 2009/12/04 87 % 50 - 130Fluorene 2009/12/04 86 % 50 - 130Phenanthrene 2009/12/04 82 % 60 - 130Anthracene 2009/12/04 81 % 60 - 130Fluoranthene 2009/12/04 80 % 60 - 130Pyrene 2009/12/04 81 % 60 - 130Benzo(a)anthracene 2009/12/04 80 % 60 - 130


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3607122 TG1 Matrix Spike[S01932-01] Chrysene 2009/12/04 79 % 60 - 130

Benzo(b&j)fluoranthene 2009/12/04 83 % 60 - 130Benzo(k)fluoranthene 2009/12/04 79 % 60 - 130Benzo(a)pyrene 2009/12/04 81 % 60 - 130Indeno(1,2,3-cd)pyrene 2009/12/04 70 % 60 - 130Dibenz(a,h)anthracene 2009/12/04 72 % 60 - 130Benzo(g,h,i)perylene 2009/12/04 68 % 60 - 130



3607122 TG1 LCS D10-ANTHRACENE (sur.) 2009/12/04 91 % 30 - 130D12-BENZO(A)PYRENE (sur.) 2009/12/04 89 % 30 - 130D8-ACENAPHTHYLENE (sur.) 2009/12/04 87 % 30 - 130TERPHENYL-D14 (sur.) 2009/12/04 91 % 30 - 130Naphthalene 2009/12/04 91 % 50 - 1302-Methylnaphthalene 2009/12/04 96 % 50 - 130Acenaphthylene 2009/12/04 83 % 50 - 130Acenaphthene 2009/12/04 88 % 50 - 130Fluorene 2009/12/04 89 % 50 - 130Phenanthrene 2009/12/04 90 % 60 - 130Anthracene 2009/12/04 90 % 60 - 130Fluoranthene 2009/12/04 90 % 60 - 130Pyrene 2009/12/04 89 % 60 - 130Benzo(a)anthracene 2009/12/04 88 % 60 - 130Chrysene 2009/12/04 87 % 60 - 130Benzo(b&j)fluoranthene 2009/12/04 91 % 60 - 130Benzo(k)fluoranthene 2009/12/04 86 % 60 - 130Benzo(a)pyrene 2009/12/04 91 % 60 - 130Indeno(1,2,3-cd)pyrene 2009/12/04 84 % 60 - 130Dibenz(a,h)anthracene 2009/12/04 84 % 60 - 130Benzo(g,h,i)perylene 2009/12/04 83 % 60 - 130

3608381 JC8 LCS Total Arsenic (As) 2009/12/04 97 % 75 - 125Total Beryllium (Be) 2009/12/04 93 % 75 - 125Total Cadmium (Cd) 2009/12/04 96 % 75 - 125Total Chromium (Cr) 2009/12/04 97 % 75 - 125Total Cobalt (Co) 2009/12/04 94 % 75 - 125Total Copper (Cu) 2009/12/04 99 % 75 - 125Total Lead (Pb) 2009/12/04 96 % 75 - 125Total Mercury (Hg) 2009/12/04 99 % 75 - 125Total Nickel (Ni) 2009/12/04 97 % 75 - 125Total Selenium (Se) 2009/12/04 100 % 75 - 125Total Vanadium (V) 2009/12/04 98 % 75 - 125Total Zinc (Zn) 2009/12/04 102 % 75 - 125

3608419 AL8 LCS Soluble (2:1) pH 2009/12/04 100 % 96 - 1043609489 DM9 LCS Sulphide 2009/12/07 85 % 75 - 1253608381 JC8 SRM Total Aluminum (Al) 2009/12/04 87 % 70 - 130

Total Antimony (Sb) 2009/12/04 92 % 70 - 130Total Arsenic (As) 2009/12/04 88 % 70 - 130Total Barium (Ba) 2009/12/04 97 % 70 - 130Total Cadmium (Cd) 2009/12/04 86 % 70 - 130Total Calcium (Ca) 2009/12/04 92 % 70 - 130


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3608381 JC8 SRM Total Chromium (Cr) 2009/12/04 88 % 70 - 130Total Cobalt (Co) 2009/12/04 87 % 70 - 130Total Copper (Cu) 2009/12/04 85 % 70 - 130Total Iron (Fe) 2009/12/04 89 % 70 - 130Total Lead (Pb) 2009/12/04 88 % 70 - 130Total Magnesium (Mg) 2009/12/04 93 % 70 - 130Total Manganese (Mn) 2009/12/04 92 % 70 - 130Total Molybdenum (Mo) 2009/12/04 91 % 70 - 130Total Nickel (Ni) 2009/12/04 89 % 70 - 130Total Phosphorus (P) 2009/12/04 87 % 70 - 130Total Silver (Ag) 2009/12/04 86 % 70 - 130Total Strontium (Sr) 2009/12/04 90 % 70 - 130Total Thallium (Tl) 2009/12/04 76 % 70 - 130Total Titanium (Ti) 2009/12/04 93 % 70 - 130Total Vanadium (V) 2009/12/04 95 % 70 - 130Total Zinc (Zn) 2009/12/04 81 % 70 - 130



Duplicate: Paired analysis of a separate portion of the same sample. Used to evaluate the variance in the measurement.Matrix Spike: A sample to which a known amount of the analyte of interest has been added. Used to evaluate sample matrix interference.SRM: A blank matrix sample to which a known amount of the analyte has been added. Used to evaluate analyte recovery.LCS: A blank matrix sample to which a known amount of the analyte has been added. Used to evaluate analyte recovery.Method Blank: A blank matrix containing all reagents used in the analytical procedure. Used to identify laboratory contamination.Surrogate: A pure or isotopically labeled compound whose behavior mirrors the analytes of interest. Used to evaluate extraction efficiency.NC (Matrix Spike): The recovery in the matrix spike was not calculated. The relative difference between the concentration in the parent sample and thespiked amount was not sufficiently significant to permit a reliable recovery calculation.NC (RPD): The RPD was not calculated. The level of analyte detected in the parent sample and its duplicate was not sufficiently significant to permit areliable calculation.


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Site Location: Burrard Inlet Pipe Removal Port Moody BCMaxxam Sample: S01927 Client ID: IPS-SD09-REF2



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Site Location: Burrard Inlet Pipe Removal Port Moody BCMaxxam Sample: S01928 Client ID: IPS-SD09-REF1



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Task Order#: 11062608Site#: P11450Site Location: 2225 IOCO RD, PORT MOODY BC. / 88006226Project #: 08-1436-0046-6075(A969147)Your C.O.C. #: F156650Attention: Sue Reynolds

Maxxam - Burnaby (Esso Samples)8577 Commerce CrtBurnaby, BCV5A 4N5



MAXXAM JOB #: A9G6544Received: 2009/12/09, 12:15

Sample Matrix: SOLID# Samples Received: 9

MethodAnalyses Quantity Laboratory Method Primary referenceTotal Organic Carbon in Soil 9 CAM SOP-00468 LECO Combustion

Remarks:

Maxxam Analytics has performed all analytical testing herein in accordance with ISO 17025 and the Protocol for AnalyticalMethods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act. All methodologiescomply with this document and are validated for use in the laboratory. The methods and techniques employed in thisanalysis conform to the performance criteria (detection limits, accuracy and precision) as outlined in the Protocol forAnalytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act.

The CWS PHC methods employed by Maxxam conform to all prescribed elements of the reference method andperformance based elements have been validated. All modifications have been validated and proven equivalent followingthe 'Alberta Environment Draft Addenda to the CWS-PHC, Appendix 6, Validation of Alternate Methods'. Documentation isavailable upon request. Maxxam has made the following improvements to the CWS-PHC reference benchmark method:(i) Headspace for F1; and, (ii) Mechanical extraction for F2-F4. Note: F4G cannot be added to the C6 to C50hydrocarbons.

Maxxam Analytics is accredited by SCC (Lab ID 97) for all specific parameters as required by GUCSO and O'Reg 153/04.Maxxam Analytics is limited in liability to the actual cost of analysis unless otherwise agreed in writing. There is no otherwarranty expressed or implied. Samples will be retained at Maxxam Analytics for three weeks from receipt of data or asper contract.

All data is in statistical control and has met all QC and method performance criteria unless otherwise flagged. All sampleswere analysed within hold time unless otherwise flagged. All BTEX samples were methanol extracted within 24 hoursunless otherwise flagged.

Page 1 of 9

Task Order#: 11062608Site#: P11450Site Location: 2225 IOCO RD, PORT MOODY BC. / 88006226Project #: 08-1436-0046-6075(A969147)Your C.O.C. #: F156650Attention: Sue Reynolds






Encryption Key


EMA GITEJ, Project ManagerEmail: [email protected]# (905) 817-5700


For Service Group specific validation please refer to the Validation Signature Page


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Ema Gitej

10 Dec 2009 17:43:59 -05:00

Maxxam - Burnaby (Esso Samples)Maxxam Job #: A9G6544 Task Order#: 11062608Report Date: 2009/12/10 Site#: P11450

Site Location: 2225 IOCO RD, PORT MOODY BC. / 88006226Project #: 08-1436-0046-6075(A969147)

RESULTS OF ANALYSES OF SOLID

Maxxam ID E P 2 7 0 8 E P 2 7 0 8 E P 2 7 0 9 E P 2 7 1 0Sampling Date 2009/12/02 2009/12/02 2009/12/02 2009/12/02

10:33 10:33 09:24 09:34COC Number F156650 F156650 F156650 F156650

U n i t s S01924 S01924 S01925 S01926 R D L QC Batch\ IPS-SD09-39 \ IPS-SD09-39 \ IPS-SD09-29 \ IPS-SD09-38

Lab-Dup

Total Organic Carbon mg/kg 35000 35000 34000 35000 500 2032732

RDL = Reportable Detection LimitQC Batch = Quality Control Batch


15:16 14:15 10:23 11:04COC Number F156650 F156650 F156650 F156650

U n i t s S01927 S01928 S01929 S01930 R D L QC Batch\ IPS-SD09-REF2 \ IPS-SD09-REF1 \ IPS-SD09-28 \ IPS-SD09-30



Maxxam ID E P 2 7 1 5 E P 2 7 1 6Sampling Date 2009/12/02 2009/12/02

12:12 12:47COC Number F156650 F156650

U n i t s S01931 S01932 R D L QC Batch\ IPS-SD09-31 \ IPS-SD09-32

Total Organic Carbon mg/kg 32000 33000 500 2032732


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Test Summary

Maxxam ID EP2708 Collected 2009/12/02Sample ID S01924 \ IPS-SD09-39 Shipped 2009/12/02

Matrix SOLID Received 2009/12/09

Test Description Instrumentation Batch Extracted Analyzed AnalystTotal Organic Carbon in Soil LECO 2032732 N/A 2009/12/10 BMO

Maxxam ID EP2708 D u p Collected 2009/12/02Sample ID S01924 \ IPS-SD09-39 Shipped 2009/12/02









Maxxam ID EP2711 Collected 2009/12/02Sample ID S01927 \ IPS-SD09-REF2 Shipped 2009/12/02



Maxxam ID EP2712 Collected 2009/12/02Sample ID S01928 \ IPS-SD09-REF1 Shipped 2009/12/02



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Test Summary













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Package 1 3.0°CEach temperature is the average of up to three cooler temperatures taken at receipt

GENERAL COMMENTS


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Maxxam - Burnaby (Esso Samples)Task Order#: 11062608Site#: P11450Site Location: 2225 IOCO RD, PORT MOODY BC. / 88006226Project #: 08-1436-0046-6075(A969147)

Quality Assurance ReportMaxxam Job Number: A9G6544


2032732 BMO Method Blank Total Organic Carbon 2009/12/10 <500 mg/kgRPD [ E P 2 7 0 8 - 0 1 ] Total Organic Carbon 2009/12/10 1.2 % 35SRM Total Organic Carbon 2009/12/10 94 % 80 - 120

Duplicate: Paired analysis of a separate portion of the same sample. Used to evaluate the variance in the measurement.SRM: A blank matrix sample to which a known amount of the analyte has been added. Used to evaluate analyte recovery.Method Blank: A blank matrix containing all reagents used in the analytical procedure. Used to identify laboratory contamination.

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Validation Signature Page

Maxxam Job #: A9G6544

The analytical data and all QC contained in this report were reviewed and validated by the following individual(s).

EWA PRANJIC, M.Sc., C.Chem, Scientific Specialist

====================================================================Maxxam has procedures in place to guard against improper use of the electronic signature and have the required "signatories", as per section 5.10.2 ofISO/IEC 17025:2005(E), signing the reports. SCC and CALA have approved this reporting process and electronic report format.

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Task Order#: 11062608Site#: P11605Site Location: Burrard Inlet Pipe Removal Port Moody BCProject #: 08-1436-0046-6075Your C.O.C. #: F156645Attention: Blair MacDonald






Analyses Quantity Laboratory Method Primary referenceSend Part to Archive 4Environmental Sample Disposal Fee 4Elements by ICPMS (total) 4 BRN SOP-00203 R5.0 Based on EPA 200.8Simultaneously Extractable Metals-ICPMS 4 BRN SOP-00203 5.0 Based on EPA 200.8Moisture 4 BRN SOP-00321 R5.0 Ont MOE -E 3139PAH in Soil by GC/MS (SIM) 4 BRN SOP-00332 R9.0 Based on EPA 8270DTotal LMW, HMW, Total PAH Calc 4pH (2:1 DI Water Extract) ( 3 ) 4 BRN SOP-00266 R6.0 Carter, SSMA 16.2Sulfide (AVS) (soil) - Calc for umole/g 4 BRN SOP-00229 R2.0 Based EPA821-R91-100Sulfide (AVS) (soil) 4 BRN SOP-00229 R2.0 Based EPA821-R91-100EPH less PAH in Soil By GC/FID ( 3 ) 4BC Hydrocarbons in Soil by GC/FID ( 3 ) 4 BRN SOP-00341 R14 Based BCCSR Method 3Texture by Hydrometer ( 1 ) 4 EENVSOP-00076 MMFSPA Ch9Texture Class ( 1 ) 4 EENVSOP-00076 MMFSPA Ch9TOC Soil Subcontract ( 2 ) 4

Remarks:




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(1) This test was performed by Maxxam Edmonton Environmental(2) This test was performed by Maxxam Bedford(From Burnaby)(3) SCC/CAEAL

Encryption Key




Total cover pages: 2Maxxam Analytics International Corporation o/a Maxxam Analytics Burnaby: 8577 Commerce Court V5A 4N5 Telephone(604) 444-4808 Fax(604) 444-4511

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Sue Reynolds

11 Dec 2009 16:10:42 -08:00





09:32 10:33 14:42COC Number F156645 F156645 F156645

U n i t s IA-SD09-REF3 IA-SD09-REF4 IPS-SD09-25 R D L QC Batch

Parameter

Subcontract Parameter N/A ATTACHED ATTACHED ATTACHED N/A 3620899


Sulphide umole/g 0.010 0.010 0.079 0.006 3607652

MISCELLANEOUS

Sulphide ug/g 0.3 ( 1 ) 0.3 2.5 0.2 3619832

Physical Properties

% sand by hydrometer % 54 86 85 2 3619011

% silt by hydrometer % 34 10 10 2 3619011

Clay Content % 12 4 6 2 3619011

Texture N/A SANDY LOAM LOAMY SAND LOAMY SAND N/A 3607565

Moisture % 40 23 24 0.3 3607919

RDL = Reportable Detection Limit( 1 ) Matrix spike exceeds acceptance limits due to matrix interference. Re-analysis yields similar results.

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Maxxam ID S 0 3 7 2 1Sampling Date 2009/12/03

13:22COC Number F156645

U n i t s IPN-SD09-REF5 R D L QC Batch

Parameter

Subcontract Parameter N/A ATTACHED N/A 3620899


Sulphide umole/g 0.219 0.006 3607652

MISCELLANEOUS

Sulphide ug/g 7.0 0.2 3619832

Physical Properties

% sand by hydrometer % 12 2 3619011

% silt by hydrometer % 64 2 3619011

Clay Content % 24 2 3619011

Texture N/A SILT LOAM N/A 3607565

Moisture % 71 0.3 3607919


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09:32 10:33 14:42COC Number F156645 F156645 F156645


SEM Metals by ICPMS











SEM Metals by ICPMS

SEM Cadmium (Cd) umole/g 0.0199 0.0002 3612878

SEM Copper (Cu) umole/g 0.469 0.004 3612878

SEM Lead (Pb) umole/g 0.170 0.0002 3612878

SEM Mercury (Hg) umole/g <0.0003 0.0003 3612878

SEM Nickel (Ni) umole/g 0.347 0.004 3612878

SEM Zinc (Zn) umole/g 2.02 0.008 3612878


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09:32 10:33 14:42COC Number F156645 F156645 F156645



HEPH (C19-C32 less PAH) mg/kg 108 <100 <100 100 3607155


Hydrocarbons

EPH (C10-C19) mg/kg <100 <100 <100 100 3608887

EPH (C19-C32) mg/kg 108 <100 <100 100 3608887








HEPH (C19-C32 less PAH) mg/kg 1110 100 3607155

LEPH (C10-C19 less PAH) mg/kg <100 100 3607155

Hydrocarbons

EPH (C10-C19) mg/kg <100 100 3608887

EPH (C19-C32) mg/kg 1110 100 3608887


O-TERPHENYL (sur.) % 96 N/A 3608887


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09:32 10:33 14:42COC Number F156645 F156645 F156645


Misc. Inorganics







Total Beryllium (Be) mg/kg 0.1 <0.1 <0.1 0.1 3611459

Total Bismuth (Bi) mg/kg 0.2 <0.1 <0.1 0.1 3611459









Total Manganese (Mn) mg/kg 189 94.7 112 0.2 3611459

Total Mercury (Hg) mg/kg 0.11 <0.05 <0.05 0.05 3611459





Total Selenium (Se) mg/kg 1.0 <0.5 0.5 0.5 3611459

Total Silver (Ag) mg/kg 0.35 0.08 <0.05 0.05 3611459




Total Tin (Sn) mg/kg 1.0 0.3 0.4 0.1 3611459





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09:32 10:33 14:42COC Number F156645 F156645 F156645


Total Zirconium (Zr) mg/kg 0.9 <0.5 <0.5 0.5 3611459


Page 8 of 24







Misc. Inorganics

Soluble (2:1) pH pH Units 7.22 0.01 3611639


Total Aluminum (Al) mg/kg 18600 100 3611459

Total Antimony (Sb) mg/kg 0.5 0.1 3611459

Total Arsenic (As) mg/kg 14.5 0.2 3611459

Total Barium (Ba) mg/kg 49.3 0.1 3611459

Total Beryllium (Be) mg/kg 0.3 0.1 3611459

Total Bismuth (Bi) mg/kg 0.4 0.1 3611459

Total Cadmium (Cd) mg/kg 2.64 0.05 3611459

Total Calcium (Ca) mg/kg 6400 100 3611459

Total Chromium (Cr) mg/kg 42 1 3611459

Total Cobalt (Co) mg/kg 9.2 0.3 3611459

Total Copper (Cu) mg/kg 86.7 0.5 3611459

Total Iron (Fe) mg/kg 32800 100 3611459

Total Lead (Pb) mg/kg 47.2 0.1 3611459

Total Magnesium (Mg) mg/kg 12300 100 3611459

Total Manganese (Mn) mg/kg 313 0.2 3611459

Total Mercury (Hg) mg/kg 0.17 0.05 3611459

Total Molybdenum (Mo) mg/kg 4.9 0.1 3611459

Total Nickel (Ni) mg/kg 30.2 0.8 3611459

Total Phosphorus (P) mg/kg 947 10 3611459

Total Potassium (K) mg/kg 3910 100 3611459

Total Selenium (Se) mg/kg 1.7 0.5 3611459

Total Silver (Ag) mg/kg 0.47 0.05 3611459

Total Sodium (Na) mg/kg 24300 100 3611459

Total Strontium (Sr) mg/kg 67.3 0.1 3611459

Total Thallium (Tl) mg/kg 0.39 0.05 3611459

Total Tin (Sn) mg/kg 1.9 0.1 3611459

Total Titanium (Ti) mg/kg 627 1 3611459

Total Vanadium (V) mg/kg 52 2 3611459

Total Zinc (Zn) mg/kg 168 1 3611459


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Total Zirconium (Zr) mg/kg 2.1 0.5 3611459


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09:32 10:33 14:42COC Number F156645 F156645 F156645




High Molecular Weight PAH`s mg/kg 1.1 0.06 0.52 0.02 3607154

Total PAH mg/kg 1.5 0.08 0.65 0.02 3607154


2-Methylnaphthalene mg/kg 0.03 <0.01 0.02 0.01 3609130

Acenaphthylene mg/kg 0.03 <0.01 0.01 0.01 3609130

Acenaphthene mg/kg 0.01 <0.01 <0.01 0.01 3609130

Fluorene mg/kg 0.02 <0.01 <0.01 0.01 3609130

Phenanthrene mg/kg 0.11 <0.01 0.05 0.01 3609130

Anthracene mg/kg 0.04 <0.01 0.02 0.01 3609130


Pyrene mg/kg 0.23 0.02 0.13 0.01 3609130

Benzo(a)anthracene mg/kg 0.08 <0.01 0.04 0.01 3609130

Chrysene mg/kg 0.14 0.01 0.06 0.01 3609130


Benzo(k)fluoranthene mg/kg 0.09 <0.01 0.04 0.01 3609130

Benzo(a)pyrene mg/kg 0.10 <0.01 0.04 0.01 3609130

Indeno(1,2,3-cd)pyrene mg/kg 0.06 <0.02 0.02 0.02 3609130

Dibenz(a,h)anthracene mg/kg <0.02 <0.02 <0.02 0.02 3609130

Benzo(g,h,i)perylene mg/kg 0.08 <0.02 0.03 0.02 3609130







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Low Molecular Weight PAH`s mg/kg 0.84 0.01 3607154

High Molecular Weight PAH`s mg/kg 1.6 0.02 3607154

Total PAH mg/kg 2.4 0.02 3607154

Naphthalene mg/kg 0.20 0.01 3609130

2-Methylnaphthalene mg/kg 0.21 0.01 3609130

Acenaphthylene mg/kg 0.03 0.01 3609130

Acenaphthene mg/kg 0.03 0.01 3609130

Fluorene mg/kg 0.06 0.01 3609130

Phenanthrene mg/kg 0.24 0.01 3609130

Anthracene mg/kg 0.07 0.01 3609130

Fluoranthene mg/kg 0.26 0.01 3609130

Pyrene mg/kg 0.34 0.01 3609130

Benzo(a)anthracene mg/kg 0.13 0.01 3609130

Chrysene mg/kg 0.19 0.01 3609130

Benzo(b&j)fluoranthene mg/kg 0.18 0.01 3609130

Benzo(k)fluoranthene mg/kg 0.12 0.01 3609130

Benzo(a)pyrene mg/kg 0.13 0.01 3609130

Indeno(1,2,3-cd)pyrene mg/kg 0.09 0.02 3609130

Dibenz(a,h)anthracene mg/kg 0.04 0.02 3609130

Benzo(g,h,i)perylene mg/kg 0.13 0.02 3609130


D10-ANTHRACENE (sur.) % 90 N/A 3609130

D12-BENZO(A)PYRENE (sur.) % 85 N/A 3609130

D8-ACENAPHTHYLENE (sur.) % 78 N/A 3609130

TERPHENYL-D14 (sur.) % 89 N/A 3609130


Page 12 of 24



Test Summary

Maxxam ID S03718 Collected 2009/12/03Sample ID IA-SD09-REF3 Shipped 2009/12/03


Test Description Instrumentation Batch Extracted Analyzed AnalystElements by ICPMS (total) ICPM/MS 3611459 2009/12/07 2009/12/07 DJSimultaneously Extractable Metals-ICPMS ICPM/MS 3612878 2009/12/10 2009/12/10 DJMoisture BAL 3607919 N/A 2009/12/04 SW4PAH in Soil by GC/MS (SIM) GC/MSD 3609130 2009/12/04 2009/12/07 RW4Total LMW, HMW, Total PAH Calc GC/MSD 3607154 N/A 2009/12/08 ASCpH (2:1 DI Water Extract) /PH 3611639 2009/12/07 2009/12/07 CB9Sulfide (AVS) (soil) - Calc for umole/g SPEC/COL 3607652 2009/12/11 2009/12/11 ASCSulfide (AVS) (soil) SPEC/COL 3619832 2009/12/05 2009/12/10 KVEPH less PAH in Soil By GC/FID GC/FID 3607155 N/A 2009/12/08 ASCBC Hydrocarbons in Soil by GC/FID GC/FID 3608887 2009/12/04 2009/12/04 JP1Texture by Hydrometer HY 3619011 N/A 2009/12/10 JB9Texture Class CALC 3607565 N/A 2009/12/10 ASCTOC Soil Subcontract 3620899 2009/12/10 2009/12/10 SR6

Maxxam ID S03718 D u p Collected 2009/12/03Sample ID IA-SD09-REF3 Shipped 2009/12/03


Test Description Instrumentation Batch Extracted Analyzed AnalystSimultaneously Extractable Metals-ICPMS ICPM/MS 3612878 2009/12/10 2009/12/10 DJSulfide (AVS) (soil) SPEC/COL 3619832 2009/12/10 2009/12/10 KV

Maxxam ID S03719 Collected 2009/12/03Sample ID IA-SD09-REF4 Shipped 2009/12/03



Page 13 of 24



Test Summary

Maxxam ID S03719 D u p Collected 2009/12/03Sample ID IA-SD09-REF4 Shipped 2009/12/03


Test Description Instrumentation Batch Extracted Analyzed AnalystMoisture BAL 3607919 N/A 2009/12/04 SW4




Maxxam ID S03721 Collected 2009/12/03Sample ID IPN-SD09-REF5 Shipped 2009/12/03



Page 14 of 24



General Comments






Page 15 of 24




3607919 SW4 Method Blank Moisture 2009/12/04 <0.3 %3608887 JP1 Method Blank O-TERPHENYL (sur.) 2009/12/04 95 % 50 - 130

EPH (C10-C19) 2009/12/04 <100 mg/kgEPH (C19-C32) 2009/12/04 <100 mg/kg

3609130 RW4 Method Blank D10-ANTHRACENE (sur.) 2009/12/07 99 % 30 - 130D12-BENZO(A)PYRENE (sur.) 2009/12/07 93 % 30 - 130D8-ACENAPHTHYLENE (sur.) 2009/12/07 96 % 30 - 130TERPHENYL-D14 (sur.) 2009/12/07 99 % 30 - 130Naphthalene 2009/12/07 <0.01 mg/kg2-Methylnaphthalene 2009/12/07 <0.01 mg/kgAcenaphthylene 2009/12/07 <0.01 mg/kgAcenaphthene 2009/12/07 <0.01 mg/kgFluorene 2009/12/07 <0.01 mg/kgPhenanthrene 2009/12/07 <0.01 mg/kgAnthracene 2009/12/07 <0.01 mg/kgFluoranthene 2009/12/07 <0.01 mg/kgPyrene 2009/12/07 <0.01 mg/kgBenzo(a)anthracene 2009/12/07 <0.01 mg/kgChrysene 2009/12/07 <0.01 mg/kgBenzo(b&j)fluoranthene 2009/12/07 <0.01 mg/kgBenzo(k)fluoranthene 2009/12/07 <0.01 mg/kgBenzo(a)pyrene 2009/12/07 <0.01 mg/kgIndeno(1,2,3-cd)pyrene 2009/12/07 <0.02 mg/kgDibenz(a,h)anthracene 2009/12/07 <0.02 mg/kgBenzo(g,h,i)perylene 2009/12/07 <0.02 mg/kg

3611459 DJ Method Blank Total Aluminum (Al) 2009/12/07 <100 mg/kgTotal Antimony (Sb) 2009/12/07 <0.1 mg/kgTotal Arsenic (As) 2009/12/07 0.3, RDL=0.2 mg/kgTotal Barium (Ba) 2009/12/07 <0.1 mg/kgTotal Beryllium (Be) 2009/12/07 <0.1 mg/kgTotal Bismuth (Bi) 2009/12/07 <0.1 mg/kgTotal Cadmium (Cd) 2009/12/07 <0.05 mg/kgTotal Calcium (Ca) 2009/12/07 <100 mg/kgTotal Chromium (Cr) 2009/12/07 <1 mg/kgTotal Cobalt (Co) 2009/12/07 <0.3 mg/kgTotal Copper (Cu) 2009/12/07 <0.5 mg/kgTotal Iron (Fe) 2009/12/07 <100 mg/kgTotal Lead (Pb) 2009/12/07 <0.1 mg/kgTotal Magnesium (Mg) 2009/12/07 <100 mg/kgTotal Manganese (Mn) 2009/12/07 <0.2 mg/kgTotal Mercury (Hg) 2009/12/07 <0.05 mg/kgTotal Molybdenum (Mo) 2009/12/07 <0.1 mg/kgTotal Nickel (Ni) 2009/12/07 <0.8 mg/kgTotal Phosphorus (P) 2009/12/07 <10 mg/kgTotal Potassium (K) 2009/12/07 <100 mg/kgTotal Selenium (Se) 2009/12/07 <0.5 mg/kgTotal Silver (Ag) 2009/12/07 <0.05 mg/kgTotal Sodium (Na) 2009/12/07 <100 mg/kgTotal Strontium (Sr) 2009/12/07 <0.1 mg/kgTotal Thallium (Tl) 2009/12/07 <0.05 mg/kgTotal Tin (Sn) 2009/12/07 <0.1 mg/kgTotal Titanium (Ti) 2009/12/07 <1 mg/kgTotal Vanadium (V) 2009/12/07 <2 mg/kgTotal Zinc (Zn) 2009/12/07 <1 mg/kgTotal Zirconium (Zr) 2009/12/07 <0.5 mg/kg


Page 16 of 24




3612878 DJ Method Blank SEM Cadmium (Cd) 2009/12/08 <0.0002 umole/gSEM Copper (Cu) 2009/12/08 <0.004 umole/gSEM Lead (Pb) 2009/12/08 <0.0002 umole/gSEM Mercury (Hg) 2009/12/08 <0.0003 umole/gSEM Nickel (Ni) 2009/12/08 <0.004 umole/gSEM Zinc (Zn) 2009/12/08 <0.008 umole/g


3619832 KV Method Blank Sulphide 2009/12/10 0.2, RDL=0.2 ug/g3612878 DJ RPD [ S 0 3 7 1 8 - 0 4 ] SEM Cadmium (Cd) 2009/12/10 11.7 % 30

SEM Copper (Cu) 2009/12/10 11.8 % 30SEM Lead (Pb) 2009/12/10 11.2 % 30SEM Mercury (Hg) 2009/12/10 NC % 30SEM Nickel (Ni) 2009/12/10 7.8 % 30SEM Zinc (Zn) 2009/12/10 8.7 % 30

3619832 KV RPD [ S 0 3 7 1 8 - 0 4 ] Sulphide 2009/12/10 NC % 303607919 SW4 RPD [ S 0 3 7 1 9 - 0 1 ] Moisture 2009/12/04 2.2 % 203619832 KV Matrix Spike

[S03718-04] Sulphide 2009/12/10 71 ( 1 ) % 75 - 1253608887 JP1 LCS O-TERPHENYL (sur.) 2009/12/04 99 % 50 - 130

EPH (C10-C19) 2009/12/04 91 % 50 - 130EPH (C19-C32) 2009/12/04 88 % 50 - 130

3609130 RW4 LCS D10-ANTHRACENE (sur.) 2009/12/07 96 % 30 - 130D12-BENZO(A)PYRENE (sur.) 2009/12/07 94 % 30 - 130D8-ACENAPHTHYLENE (sur.) 2009/12/07 94 % 30 - 130TERPHENYL-D14 (sur.) 2009/12/07 93 % 30 - 130Naphthalene 2009/12/07 91 % 50 - 1302-Methylnaphthalene 2009/12/07 93 % 50 - 130Acenaphthylene 2009/12/07 86 % 50 - 130Acenaphthene 2009/12/07 91 % 50 - 130Fluorene 2009/12/07 92 % 50 - 130Phenanthrene 2009/12/07 93 % 60 - 130Anthracene 2009/12/07 89 % 60 - 130Fluoranthene 2009/12/07 91 % 60 - 130Pyrene 2009/12/07 87 % 60 - 130Benzo(a)anthracene 2009/12/07 85 % 60 - 130Chrysene 2009/12/07 86 % 60 - 130Benzo(b&j)fluoranthene 2009/12/07 88 % 60 - 130Benzo(k)fluoranthene 2009/12/07 94 % 60 - 130Benzo(a)pyrene 2009/12/07 93 % 60 - 130Indeno(1,2,3-cd)pyrene 2009/12/07 87 % 60 - 130Dibenz(a,h)anthracene 2009/12/07 88 % 60 - 130Benzo(g,h,i)perylene 2009/12/07 85 % 60 - 130

3611459 DJ LCS Total Arsenic (As) 2009/12/07 98 % 75 - 125Total Beryllium (Be) 2009/12/07 98 % 75 - 125Total Cadmium (Cd) 2009/12/07 101 % 75 - 125Total Chromium (Cr) 2009/12/07 99 % 75 - 125Total Cobalt (Co) 2009/12/07 100 % 75 - 125Total Copper (Cu) 2009/12/07 101 % 75 - 125Total Lead (Pb) 2009/12/07 103 % 75 - 125Total Mercury (Hg) 2009/12/07 99 % 75 - 125Total Nickel (Ni) 2009/12/07 102 % 75 - 125Total Selenium (Se) 2009/12/07 104 % 75 - 125Total Vanadium (V) 2009/12/07 101 % 75 - 125


Page 17 of 24




3611459 DJ LCS Total Zinc (Zn) 2009/12/07 100 % 75 - 1253611639 CB9 LCS Soluble (2:1) pH 2009/12/07 99 % 96 - 1043619832 KV LCS Sulphide 2009/12/10 88 % 75 - 1253611459 DJ SRM Total Aluminum (Al) 2009/12/07 81 % 70 - 130

Total Antimony (Sb) 2009/12/07 94 % 70 - 130Total Arsenic (As) 2009/12/07 88 % 70 - 130Total Barium (Ba) 2009/12/07 102 % 70 - 130Total Cadmium (Cd) 2009/12/07 89 % 70 - 130Total Calcium (Ca) 2009/12/07 95 % 70 - 130Total Chromium (Cr) 2009/12/07 84 % 70 - 130Total Cobalt (Co) 2009/12/07 90 % 70 - 130Total Copper (Cu) 2009/12/07 88 % 70 - 130Total Iron (Fe) 2009/12/07 89 % 70 - 130Total Lead (Pb) 2009/12/07 99 % 70 - 130Total Magnesium (Mg) 2009/12/07 96 % 70 - 130Total Manganese (Mn) 2009/12/07 93 % 70 - 130Total Molybdenum (Mo) 2009/12/07 91 % 70 - 130Total Nickel (Ni) 2009/12/07 92 % 70 - 130Total Phosphorus (P) 2009/12/07 98 % 70 - 130Total Silver (Ag) 2009/12/07 86 % 70 - 130Total Strontium (Sr) 2009/12/07 95 % 70 - 130Total Thallium (Tl) 2009/12/07 85 % 70 - 130Total Titanium (Ti) 2009/12/07 86 % 70 - 130Total Vanadium (V) 2009/12/07 89 % 70 - 130Total Zinc (Zn) 2009/12/07 86 % 70 - 130


Duplicate: Paired analysis of a separate portion of the same sample. Used to evaluate the variance in the measurement.Matrix Spike: A sample to which a known amount of the analyte of interest has been added. Used to evaluate sample matrix interference.SRM: A blank matrix sample to which a known amount of the analyte has been added. Used to evaluate analyte recovery.LCS: A blank matrix sample to which a known amount of the analyte has been added. Used to evaluate analyte recovery.Method Blank: A blank matrix containing all reagents used in the analytical procedure. Used to identify laboratory contamination.Surrogate: A pure or isotopically labeled compound whose behavior mirrors the analytes of interest. Used to evaluate extraction efficiency.NC (RPD): The RPD was not calculated. The level of analyte detected in the parent sample and its duplicate was not sufficiently significant to permit areliable calculation.( 1 ) Recovery or RPD for this parameter is outside control limits. The overall quality control for this analysis meets acceptability criteria.


Page 18 of 24

Page 20 of 24


Site Location: Burrard Inlet Pipe Removal Port Moody BCMaxxam Sample: S03718 Client ID: IA-SD09-REF3



Page 21 of 24


Site Location: Burrard Inlet Pipe Removal Port Moody BCMaxxam Sample: S03719 Client ID: IA-SD09-REF4



Page 22 of 24





Page 23 of 24


Site Location: Burrard Inlet Pipe Removal Port Moody BCMaxxam Sample: S03721 Client ID: IPN-SD09-REF5



Page 24 of 24

Task Order#: 11062608Site#: P11450Site Location: 2225 IOCO RD PORT MOODY, BC/ 88006226Project #: 08-1436-0046-6075(A969396)Your C.O.C. #: F156645Attention: Sue Reynolds





Sample Matrix: SOLID# Samples Received: 4

MethodAnalyses Quantity Laboratory Method Primary referenceTotal Organic Carbon in Soil 4 CAM SOP-00468 LECO Combustion

Remarks:

Maxxam Analytics has performed all analytical testing herein in accordance with ISO 17025 and the Protocol for AnalyticalMethods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act. All methodologiescomply with this document and are validated for use in the laboratory. The methods and techniques employed in thisanalysis conform to the performance criteria (detection limits, accuracy and precision) as outlined in the Protocol forAnalytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act.

The CWS PHC methods employed by Maxxam conform to all prescribed elements of the reference method andperformance based elements have been validated. All modifications have been validated and proven equivalent followingthe 'Alberta Environment Draft Addenda to the CWS-PHC, Appendix 6, Validation of Alternate Methods'. Documentation isavailable upon request. Maxxam has made the following improvements to the CWS-PHC reference benchmark method:(i) Headspace for F1; and, (ii) Mechanical extraction for F2-F4. Note: F4G cannot be added to the C6 to C50hydrocarbons.

Maxxam Analytics is accredited by SCC (Lab ID 97) for all specific parameters as required by GUCSO and O'Reg 153/04.Maxxam Analytics is limited in liability to the actual cost of analysis unless otherwise agreed in writing. There is no otherwarranty expressed or implied. Samples will be retained at Maxxam Analytics for three weeks from receipt of data or asper contract.

All data is in statistical control and has met all QC and method performance criteria unless otherwise flagged. All sampleswere analysed within hold time unless otherwise flagged. All BTEX samples were methanol extracted within 24 hoursunless otherwise flagged.

Page 1 of 8

Task Order#: 11062608Site#: P11450Site Location: 2225 IOCO RD PORT MOODY, BC/ 88006226Project #: 08-1436-0046-6075(A969396)Your C.O.C. #: F156645Attention: Sue Reynolds






Encryption Key


EMA GITEJ, Project ManagerEmail: [email protected]# (905) 817-5700


For Service Group specific validation please refer to the Validation Signature Page


Page 2 of 8

Ema Gitej

10 Dec 2009 17:40:52 -05:00


Site Location: 2225 IOCO RD PORT MOODY, BC/ 88006226Project #: 08-1436-0046-6075(A969396)

RESULTS OF ANALYSES OF SOLID


09:32 10:33 14:42 13:22COC Number F156645 F156645 F156645 F156645

U n i t s S03718 S03719 S03720 S03721 R D L QC Batch\ IA-SD09-REF3 \ IA-SD09-REF4 \ IPS-SD09-25 \ IPN-SD09-REF5



Page 3 of 8



Test Summary

Maxxam ID EP2725 Collected 2009/12/03Sample ID S03718 \ IA-SD09-REF3 Shipped 2009/12/03



Maxxam ID EP2726 Collected 2009/12/03Sample ID S03719 \ IA-SD09-REF4 Shipped 2009/12/03






Maxxam ID EP2728 Collected 2009/12/03Sample ID S03721 \ IPN-SD09-REF5 Shipped 2009/12/03



Page 4 of 8



Package 1 3.0°CEach temperature is the average of up to three cooler temperatures taken at receipt

GENERAL COMMENTS


Page 5 of 8

Maxxam - Burnaby (Esso Samples)Task Order#: 11062608Site#: P11450Site Location: 2225 IOCO RD PORT MOODY, BC/ 88006226Project #: 08-1436-0046-6075(A969396)

Quality Assurance ReportMaxxam Job Number: A9G6552


2032732 BMO Method Blank Total Organic Carbon 2009/12/10 <500 mg/kgSRM Total Organic Carbon 2009/12/10 94 % 80 - 120

SRM: A blank matrix sample to which a known amount of the analyte has been added. Used to evaluate analyte recovery.Method Blank: A blank matrix containing all reagents used in the analytical procedure. Used to identify laboratory contamination.

Page 6 of 8

Validation Signature Page

Maxxam Job #: A9G6552

The analytical data and all QC contained in this report were reviewed and validated by the following individual(s).

EWA PRANJIC, M.Sc., C.Chem, Scientific Specialist

====================================================================Maxxam has procedures in place to guard against improper use of the electronic signature and have the required "signatories", as per section 5.10.2 ofISO/IEC 17025:2005(E), signing the reports. SCC and CALA have approved this reporting process and electronic report format.

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Pag

e 8

of 8

Task Order#: 11062608Site#: P11605Site Location: Burrard Inlet Pipe Removal Port Moody BCProject #: 08-1436-0046/6075Your C.O.C. #: F96026Attention: Blair MacDonald






Analyses Quantity Laboratory Method Primary referenceSend Part to Archive 5Environmental Sample Disposal Fee 5Elements by ICPMS (total) 5 BRN SOP-00203 R5.0 Based on EPA 200.8Simultaneously Extractable Metals-ICPMS 5 BRN SOP-00203 5.0 Based on EPA 200.8Moisture 5 BRN SOP-00321 R5.0 Ont MOE -E 3139PAH in Soil by GC/MS (SIM) 5 BRN SOP-00332 R9.0 Based on EPA 8270DTotal LMW, HMW, Total PAH Calc 5pH (2:1 DI Water Extract) ( 2 ) 5 BRN SOP-00266 R6.0 Carter, SSMA 16.2Sulfide (AVS) (soil) - Calc for umole/g 5 BRN SOP-00229 R2.0 Based EPA821-R91-100Sulfide (AVS) (soil) 5 BRN SOP-00229 R2.0 Based EPA821-R91-100Total Organic Carbon LECO Method ( 1 ) 5 EENVSOP-00151 LECO# 203-821-170EPH less PAH in Soil By GC/FID ( 2 ) 5BC Hydrocarbons in Soil by GC/FID ( 2 ) 5 BRN SOP-00341 R14 Based BCCSR Method 3Texture by Hydrometer ( 1 ) 5 EENVSOP-00076 MMFSPA Ch9Texture Class ( 1 ) 5 EENVSOP-00076 MMFSPA Ch9

Remarks:




Page 1 of 29

Task Order#: 11062608Site#: P11605Site Location: Burrard Inlet Pipe Removal Port Moody BCProject #: 08-1436-0046/6075Your C.O.C. #: F96026Attention: Blair MacDonald








(1) This test was performed by Maxxam Edmonton Environmental(2) SCC/CAEAL

Encryption Key






Page 2 of 29

Sue Reynolds

14 Dec 2009 16:30:07 -08:00


Site Location: Burrard Inlet Pipe Removal Port Moody BCProject #: 08-1436-0046/6075



13:09 14:00COC Number F96026 F96026

U n i t s IPN-SD09-18 R D L IPN-SD09-19 R D L QC Batch


Sulphide umole/g 22.0 0.3 66 1 3611469

MISCELLANEOUS

Sulphide ug/g 705 10 2100 40 3619832

Physical Properties



Clay Content % 20 2 21 2 3619011

Texture N/A SANDY LOAM N/A LOAM N/A 3611454

Moisture % 55 0.3 70 0.3 3611645



15:00 09:49COC Number F96026 F96026

U n i t s IPN-SD09-20 R D L IPN-SD09-17 R D L QC Batch


Sulphide umole/g 0.067 0.006 43.6 0.6 3611469

MISCELLANEOUS

Sulphide ug/g 2.2 0.2 1400 20 3619832

Physical Properties



Clay Content % 6 2 23 2 3619011

Texture N/A SAND N/A LOAM N/A 3611454

Moisture % 19 0.3 69 0.3 3611645


Page 3 of 29






U n i t s IPN-SD09-16 R D L QC Batch


Sulphide umole/g 54 1 3611469

MISCELLANEOUS

Sulphide ug/g 1730 40 3619832

Physical Properties

% sand by hydrometer % 41 2 3619011

% silt by hydrometer % 40 2 3619011

Clay Content % 19 2 3619011

Texture N/A LOAM N/A 3611454

Moisture % 68 0.3 3611645


Page 4 of 29





13:09 14:00 15:00COC Number F96026 F96026 F96026

U n i t s IPN-SD09-18 IPN-SD09-19 IPN-SD09-20 R D L QC Batch

SEM Metals by ICPMS

SEM Cadmium (Cd) umole/g <0.0002 0.0166 0.0020 0.0002 3612878

SEM Copper (Cu) umole/g <0.004 0.017 0.106 0.004 3612878

SEM Lead (Pb) umole/g <0.0002 0.280 0.0477 0.0002 3612878






09:49 09:29COC Number F96026 F96026

U n i t s IPN-SD09-17 IPN-SD09-16 R D L QC Batch

SEM Metals by ICPMS

SEM Cadmium (Cd) umole/g 0.0148 0.0140 0.0002 3612878

SEM Copper (Cu) umole/g <0.004 0.012 0.004 3612878

SEM Lead (Pb) umole/g 0.189 0.229 0.0002 3612878

SEM Mercury (Hg) umole/g <0.0003 <0.0003 0.0003 3612878

SEM Nickel (Ni) umole/g 0.149 0.155 0.004 3612878

SEM Zinc (Zn) umole/g 2.70 2.24 0.008 3612878


Page 5 of 29





13:09 14:00 15:00COC Number F96026 F96026 F96026



HEPH (C19-C32 less PAH) mg/kg 230 523 <100 100 3611470


Hydrocarbons

EPH (C10-C19) mg/kg <100 <100 <100 100 3614340

EPH (C19-C32) mg/kg 231 526 <100 100 3614340





09:49 09:29COC Number F96026 F96026



HEPH (C19-C32 less PAH) mg/kg 642 589 100 3611470

LEPH (C10-C19 less PAH) mg/kg <100 <100 100 3611470

Hydrocarbons

EPH (C10-C19) mg/kg <100 <100 100 3614340

EPH (C19-C32) mg/kg 649 593 100 3614340


O-TERPHENYL (sur.) % 98 97 N/A 3614340


Page 6 of 29



MISCELLANEOUS (SEDIMENT)


13:09 14:00 15:00COC Number F96026 F96026 F96026

U n i t s IPN-SD09-18 IPN-SD09-19 R D L IPN-SD09-20 R D L QC Batch

Misc. Inorganics

Total Organic Carbon (C) % 3.8 ( 1 ) 5.0 ( 1 ) 0.1 0.80 0.02 3620753



09:49 09:29COC Number F96026 F96026


Misc. Inorganics

Total Organic Carbon (C) % 6.5 ( 1 ) 6.0 ( 1 ) 0.1 3620753


Page 7 of 29





13:09 14:00 15:00COC Number F96026 F96026 F96026


Misc. Inorganics







Total Beryllium (Be) mg/kg <0.1 0.2 <0.1 0.1 3622485

Total Bismuth (Bi) mg/kg <0.1 0.2 <0.1 0.1 3622485









Total Manganese (Mn) mg/kg 52.5 178 143 0.2 3622485

Total Mercury (Hg) mg/kg <0.05 0.12 <0.05 0.05 3622485





Total Selenium (Se) mg/kg <0.5 1.1 <0.5 0.5 3622485



Total Strontium (Sr) mg/kg 430 209 37.2 0.1 3622485


Total Tin (Sn) mg/kg 0.6 2.3 0.9 0.1 3622485





Page 8 of 29





13:09 14:00 15:00COC Number F96026 F96026 F96026




Page 9 of 29





09:49 09:29COC Number F96026 F96026


Misc. Inorganics

Soluble (2:1) pH pH Units 8.18 8.14 0.01 3622378


Total Aluminum (Al) mg/kg 14100 16400 100 3622485

Total Antimony (Sb) mg/kg 0.6 0.6 0.1 3622485

Total Arsenic (As) mg/kg 12.6 14.1 0.2 3622485

Total Barium (Ba) mg/kg 39.1 46.4 0.1 3622485

Total Beryllium (Be) mg/kg 0.2 0.2 0.1 3622485

Total Bismuth (Bi) mg/kg 0.3 0.3 0.1 3622485

Total Cadmium (Cd) mg/kg 2.10 2.40 0.05 3622485

Total Calcium (Ca) mg/kg 64200 68100 100 3622485

Total Chromium (Cr) mg/kg 43 48 1 3622485

Total Cobalt (Co) mg/kg 5.5 6.5 0.3 3622485

Total Copper (Cu) mg/kg 85.1 111 0.5 3622485

Total Iron (Fe) mg/kg 20900 23700 100 3622485

Total Lead (Pb) mg/kg 74.8 85.1 0.1 3622485

Total Magnesium (Mg) mg/kg 7500 8770 100 3622485

Total Manganese (Mn) mg/kg 187 213 0.2 3622485

Total Mercury (Hg) mg/kg 0.16 0.18 0.05 3622485

Total Molybdenum (Mo) mg/kg 5.5 6.2 0.1 3622485

Total Nickel (Ni) mg/kg 19.5 22.4 0.8 3622485

Total Phosphorus (P) mg/kg 729 894 10 3622485

Total Potassium (K) mg/kg 2620 2940 100 3622485

Total Selenium (Se) mg/kg 1.1 1.3 0.5 3622485

Total Silver (Ag) mg/kg 0.31 0.35 0.05 3622485

Total Sodium (Na) mg/kg 16100 18900 100 3622485

Total Strontium (Sr) mg/kg 276 298 0.1 3622485

Total Thallium (Tl) mg/kg 0.27 0.32 0.05 3622485

Total Tin (Sn) mg/kg 3.2 3.5 0.1 3622485

Total Titanium (Ti) mg/kg 577 658 1 3622485

Total Vanadium (V) mg/kg 43 49 2 3622485

Total Zinc (Zn) mg/kg 205 241 1 3622485


Page 10 of 29





09:49 09:29COC Number F96026 F96026


Total Zirconium (Zr) mg/kg 2.4 2.8 0.5 3622485


Page 11 of 29





13:09 14:00 15:00COC Number F96026 F96026 F96026





Total PAH mg/kg 2.0 6.9 1.8 0.02 3611468




Acenaphthene mg/kg <0.01 0.02 0.01 0.01 3612475

Fluorene mg/kg 0.02 0.05 0.02 0.01 3612475


Anthracene mg/kg 0.06 0.16 0.04 0.01 3612475


Pyrene mg/kg 0.45 1.3 0.36 0.01 3612475


Chrysene mg/kg 0.22 1.2 0.11 0.01 3612475





Dibenz(a,h)anthracene mg/kg 0.02 0.07 <0.02 0.02 3612475








Page 12 of 29





09:49 09:29COC Number F96026 F96026




High Molecular Weight PAH`s mg/kg 10 5.5 0.02 3611468

Total PAH mg/kg 12 6.4 0.02 3611468




Acenaphthene mg/kg 0.03 0.03 0.01 3612475

Fluorene mg/kg 0.09 0.06 0.01 3612475


Anthracene mg/kg 0.39 0.19 0.01 3612475


Pyrene mg/kg 1.9 1.8 0.01 3612475


Chrysene mg/kg 1.4 0.60 0.01 3612475





Dibenz(a,h)anthracene mg/kg 0.19 0.08 0.02 3612475








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Test Summary

Maxxam ID S07308 Collected 2009/12/04Sample ID IPN-SD09-18 Shipped 2009/12/04


Test Description Instrumentation Batch Extracted Analyzed AnalystElements by ICPMS (total) ICPM/MS 3622485 2009/12/11 2009/12/11 JC8Simultaneously Extractable Metals-ICPMS ICPM/MS 3612878 2009/12/10 2009/12/10 DJMoisture BAL 3611645 N/A 2009/12/08 WC4PAH in Soil by GC/MS (SIM) GC/MSD 3612475 2009/12/07 2009/12/09 RW4Total LMW, HMW, Total PAH Calc GC/MSD 3611468 N/A 2009/12/09 ASCpH (2:1 DI Water Extract) /PH 3622378 2009/12/11 2009/12/11 CB9Sulfide (AVS) (soil) - Calc for umole/g SPEC/COL 3611469 2009/12/11 2009/12/11 ASCSulfide (AVS) (soil) SPEC/COL 3619832 2009/12/10 2009/12/10 KVTotal Organic Carbon LECO Method LECO 3620753 2009/12/10 2009/12/14 JLAEPH less PAH in Soil By GC/FID GC/FID 3611470 N/A 2009/12/09 ASCBC Hydrocarbons in Soil by GC/FID GC/FID 3614340 2009/12/07 2009/12/08 JP1Texture by Hydrometer HY 3619011 N/A 2009/12/10 JB9Texture Class CALC 3611454 N/A 2009/12/10 ASC

Maxxam ID S07308 D u p Collected 2009/12/04Sample ID IPN-SD09-18 Shipped 2009/12/04


Test Description Instrumentation Batch Extracted Analyzed AnalystPAH in Soil by GC/MS (SIM) GC/MSD 3612475 2009/12/07 2009/12/09 RW4Total Organic Carbon LECO Method LECO 3620753 2009/12/10 2009/12/14 JLABC Hydrocarbons in Soil by GC/FID GC/FID 3614340 2009/12/08 2009/12/08 JP1




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Test Summary




Maxxam ID S07310 D u p Collected 2009/12/04Sample ID IPN-SD09-20 Shipped 2009/12/04


Test Description Instrumentation Batch Extracted Analyzed AnalystElements by ICPMS (total) ICPM/MS 3622485 2009/12/11 2009/12/11 JC8Moisture BAL 3611645 N/A 2009/12/08 WC4pH (2:1 DI Water Extract) /PH 3622378 2009/12/11 2009/12/11 CB9Texture by Hydrometer HY 3619011 N/A 2009/12/10 JB9




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Test Summary




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General Comments







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GOLDER ASSOCIATESTask Order#: 11062608Site#: P11605Site Location: Burrard Inlet Pipe Removal Port Moody BCProject #: 08-1436-0046/6075



3611645 WC4 Method Blank Moisture 2009/12/08 <0.3 %3612475 RW4 Method Blank D10-ANTHRACENE (sur.) 2009/12/09 94 % 30 - 130


3612878 DJ Method Blank SEM Cadmium (Cd) 2009/12/08 <0.0002 umole/gSEM Copper (Cu) 2009/12/08 <0.004 umole/gSEM Lead (Pb) 2009/12/08 <0.0002 umole/gSEM Mercury (Hg) 2009/12/08 <0.0003 umole/gSEM Nickel (Ni) 2009/12/08 <0.004 umole/gSEM Zinc (Zn) 2009/12/08 <0.008 umole/g



3619832 KV Method Blank Sulphide 2009/12/10 0.2, RDL=0.2 ug/g3620753 JLA Method Blank Total Organic Carbon (C) 2009/12/11 <0.02 %3622485 JC8 Method Blank Total Aluminum (Al) 2009/12/11 <100 mg/kg

Total Antimony (Sb) 2009/12/11 <0.1 mg/kgTotal Arsenic (As) 2009/12/11 <0.2 mg/kgTotal Barium (Ba) 2009/12/11 <0.1 mg/kgTotal Beryllium (Be) 2009/12/11 <0.1 mg/kgTotal Bismuth (Bi) 2009/12/11 <0.1 mg/kgTotal Cadmium (Cd) 2009/12/11 <0.05 mg/kgTotal Calcium (Ca) 2009/12/11 <100 mg/kgTotal Chromium (Cr) 2009/12/11 <1 mg/kgTotal Cobalt (Co) 2009/12/11 <0.3 mg/kgTotal Copper (Cu) 2009/12/11 <0.5 mg/kgTotal Iron (Fe) 2009/12/11 <100 mg/kgTotal Lead (Pb) 2009/12/11 <0.1 mg/kgTotal Magnesium (Mg) 2009/12/11 <100 mg/kgTotal Manganese (Mn) 2009/12/11 <0.2 mg/kgTotal Mercury (Hg) 2009/12/11 <0.05 mg/kgTotal Molybdenum (Mo) 2009/12/11 <0.1 mg/kgTotal Nickel (Ni) 2009/12/11 <0.8 mg/kgTotal Phosphorus (P) 2009/12/11 <10 mg/kg


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3622485 JC8 Method Blank Total Potassium (K) 2009/12/11 <100 mg/kgTotal Selenium (Se) 2009/12/11 <0.5 mg/kgTotal Silver (Ag) 2009/12/11 <0.05 mg/kgTotal Sodium (Na) 2009/12/11 <100 mg/kgTotal Strontium (Sr) 2009/12/11 <0.1 mg/kgTotal Thallium (Tl) 2009/12/11 <0.05 mg/kgTotal Tin (Sn) 2009/12/11 <0.1 mg/kgTotal Titanium (Ti) 2009/12/11 <1 mg/kgTotal Vanadium (V) 2009/12/11 <2 mg/kgTotal Zinc (Zn) 2009/12/11 <1 mg/kgTotal Zirconium (Zr) 2009/12/11 <0.5 mg/kg

3612475 RW4 RPD [ S 0 7 3 0 8 - 0 1 ] Naphthalene 2009/12/09 NC % 502-Methylnaphthalene 2009/12/09 NC % 50Acenaphthylene 2009/12/09 NC % 50Acenaphthene 2009/12/09 NC % 50Fluorene 2009/12/09 NC % 50Phenanthrene 2009/12/09 8.8 % 50Anthracene 2009/12/09 17.2 % 50Fluoranthene 2009/12/09 21.9 % 50Pyrene 2009/12/09 4.8 % 50Benzo(a)anthracene 2009/12/09 24.4 % 50Chrysene 2009/12/09 28.9 % 50Benzo(b&j)fluoranthene 2009/12/09 16.0 % 50Benzo(k)fluoranthene 2009/12/09 17.4 % 50Benzo(a)pyrene 2009/12/09 16.5 % 50Indeno(1,2,3-cd)pyrene 2009/12/09 NC % 50Dibenz(a,h)anthracene 2009/12/09 NC % 50Benzo(g,h,i)perylene 2009/12/09 NC % 50

3614340 JP1 RPD [ S 0 7 3 0 8 - 0 1 ] EPH (C10-C19) 2009/12/08 NC % 50EPH (C19-C32) 2009/12/08 NC % 50

3620753 JLA RPD [ S 0 7 3 0 8 - 0 2 ] Total Organic Carbon (C) 2009/12/14 0.2 ( 1 ) % 503611645 WC4 RPD [ S 0 7 3 1 0 - 0 1 ] Moisture 2009/12/08 6.7 % 203619011 JB9 RPD [ S 0 7 3 1 0 - 0 3 ] % sand by hydrometer 2009/12/10 0 % 35

% silt by hydrometer 2009/12/10 NC % 35Clay Content 2009/12/10 NC % 35

3622378 CB9 RPD [ S 0 7 3 1 0 - 0 1 ] Soluble (2:1) pH 2009/12/11 0.6 % 203622485 JC8 RPD [ S 0 7 3 1 0 - 0 1 ] Total Aluminum (Al) 2009/12/11 4.8 % 35

Total Antimony (Sb) 2009/12/11 NC % 30Total Arsenic (As) 2009/12/11 3.7 % 30Total Barium (Ba) 2009/12/11 1.9 % 35Total Beryllium (Be) 2009/12/11 NC % 30Total Bismuth (Bi) 2009/12/11 NC % 30Total Cadmium (Cd) 2009/12/11 1.7 % 30Total Calcium (Ca) 2009/12/11 4.4 % 30Total Chromium (Cr) 2009/12/11 1.8 % 30Total Cobalt (Co) 2009/12/11 0.4 % 30Total Copper (Cu) 2009/12/11 7.9 % 30Total Iron (Fe) 2009/12/11 11.2 % 30Total Lead (Pb) 2009/12/11 0.7 % 35Total Magnesium (Mg) 2009/12/11 1.9 % 30Total Manganese (Mn) 2009/12/11 1.8 % 30Total Mercury (Hg) 2009/12/11 NC % 35Total Molybdenum (Mo) 2009/12/11 2.8 % 35Total Nickel (Ni) 2009/12/11 4.7 % 30Total Phosphorus (P) 2009/12/11 0.2 % 30


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3622485 JC8 RPD [ S 0 7 3 1 0 - 0 1 ] Total Potassium (K) 2009/12/11 3.5 % 35Total Selenium (Se) 2009/12/11 NC % 30Total Silver (Ag) 2009/12/11 NC % 35Total Sodium (Na) 2009/12/11 6.7 % 35Total Strontium (Sr) 2009/12/11 5.8 % 35Total Thallium (Tl) 2009/12/11 NC % 30Total Tin (Sn) 2009/12/11 17.0 % 35Total Titanium (Ti) 2009/12/11 1.3 % 35Total Vanadium (V) 2009/12/11 4.1 % 30Total Zinc (Zn) 2009/12/11 1.5 % 30Total Zirconium (Zr) 2009/12/11 NC % 30

3612475 RW4 Matrix Spike[S07308-01] D10-ANTHRACENE (sur.) 2009/12/09 85 % 30 - 130

D12-BENZO(A)PYRENE (sur.) 2009/12/09 84 % 30 - 130D8-ACENAPHTHYLENE (sur.) 2009/12/09 79 % 30 - 130TERPHENYL-D14 (sur.) 2009/12/09 85 % 30 - 130Naphthalene 2009/12/09 82 % 50 - 1302-Methylnaphthalene 2009/12/09 84 % 50 - 130Acenaphthylene 2009/12/09 73 % 50 - 130Acenaphthene 2009/12/09 82 % 50 - 130Fluorene 2009/12/09 81 % 50 - 130Phenanthrene 2009/12/09 81 % 60 - 130Anthracene 2009/12/09 79 % 60 - 130Fluoranthene 2009/12/09 82 % 60 - 130Pyrene 2009/12/09 79 % 60 - 130Benzo(a)anthracene 2009/12/09 80 % 60 - 130Chrysene 2009/12/09 79 % 60 - 130Benzo(b&j)fluoranthene 2009/12/09 84 % 60 - 130Benzo(k)fluoranthene 2009/12/09 73 % 60 - 130Benzo(a)pyrene 2009/12/09 82 % 60 - 130Indeno(1,2,3-cd)pyrene 2009/12/09 80 % 60 - 130Dibenz(a,h)anthracene 2009/12/09 80 % 60 - 130Benzo(g,h,i)perylene 2009/12/09 80 % 60 - 130


EPH (C10-C19) 2009/12/08 110 % 50 - 130EPH (C19-C32) 2009/12/08 111 % 50 - 130

3622485 JC8 Matrix Spike[S07310-01] Total Arsenic (As) 2009/12/11 98 % 75 - 125

Total Beryllium (Be) 2009/12/11 100 % 75 - 125Total Cadmium (Cd) 2009/12/11 99 % 75 - 125Total Chromium (Cr) 2009/12/11 94 % 75 - 125Total Cobalt (Co) 2009/12/11 96 % 75 - 125Total Copper (Cu) 2009/12/11 96 % 75 - 125Total Lead (Pb) 2009/12/11 97 % 75 - 125Total Mercury (Hg) 2009/12/11 98 % 75 - 125Total Nickel (Ni) 2009/12/11 94 % 75 - 125Total Selenium (Se) 2009/12/11 101 % 75 - 125Total Vanadium (V) 2009/12/11 93 % 75 - 125Total Zinc (Zn) 2009/12/11 NC % 75 - 125

3612475 RW4 LCS D10-ANTHRACENE (sur.) 2009/12/09 90 % 30 - 130D12-BENZO(A)PYRENE (sur.) 2009/12/09 88 % 30 - 130D8-ACENAPHTHYLENE (sur.) 2009/12/09 88 % 30 - 130TERPHENYL-D14 (sur.) 2009/12/09 89 % 30 - 130Naphthalene 2009/12/09 88 % 50 - 130


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3612475 RW4 LCS 2-Methylnaphthalene 2009/12/09 90 % 50 - 130Acenaphthylene 2009/12/09 82 % 50 - 130Acenaphthene 2009/12/09 88 % 50 - 130Fluorene 2009/12/09 87 % 50 - 130Phenanthrene 2009/12/09 89 % 60 - 130Anthracene 2009/12/09 86 % 60 - 130Fluoranthene 2009/12/09 87 % 60 - 130Pyrene 2009/12/09 85 % 60 - 130Benzo(a)anthracene 2009/12/09 80 % 60 - 130Chrysene 2009/12/09 83 % 60 - 130Benzo(b&j)fluoranthene 2009/12/09 83 % 60 - 130Benzo(k)fluoranthene 2009/12/09 87 % 60 - 130Benzo(a)pyrene 2009/12/09 88 % 60 - 130Indeno(1,2,3-cd)pyrene 2009/12/09 82 % 60 - 130Dibenz(a,h)anthracene 2009/12/09 83 % 60 - 130Benzo(g,h,i)perylene 2009/12/09 81 % 60 - 130


3619832 KV LCS Sulphide 2009/12/10 88 % 75 - 1253620753 JLA LCS Total Organic Carbon (C) 2009/12/11 110 % 75 - 1253622378 CB9 LCS Soluble (2:1) pH 2009/12/11 100 % 96 - 1043622485 JC8 LCS Total Arsenic (As) 2009/12/11 97 % 75 - 125

Total Beryllium (Be) 2009/12/11 101 % 75 - 125Total Cadmium (Cd) 2009/12/11 98 % 75 - 125Total Chromium (Cr) 2009/12/11 96 % 75 - 125Total Cobalt (Co) 2009/12/11 97 % 75 - 125Total Copper (Cu) 2009/12/11 97 % 75 - 125Total Lead (Pb) 2009/12/11 95 % 75 - 125Total Mercury (Hg) 2009/12/11 96 % 75 - 125Total Nickel (Ni) 2009/12/11 97 % 75 - 125Total Selenium (Se) 2009/12/11 100 % 75 - 125Total Vanadium (V) 2009/12/11 94 % 75 - 125Total Zinc (Zn) 2009/12/11 98 % 75 - 125


3620753 JLA SRM Total Organic Carbon (C) 2009/12/11 106 % 75 - 1253622485 JC8 SRM Total Aluminum (Al) 2009/12/11 111 % 70 - 130

Total Antimony (Sb) 2009/12/11 101 % 70 - 130Total Arsenic (As) 2009/12/11 94 % 70 - 130Total Barium (Ba) 2009/12/11 108 % 70 - 130Total Cadmium (Cd) 2009/12/11 92 % 70 - 130Total Calcium (Ca) 2009/12/11 97 % 70 - 130Total Chromium (Cr) 2009/12/11 104 % 70 - 130Total Cobalt (Co) 2009/12/11 99 % 70 - 130Total Copper (Cu) 2009/12/11 90 % 70 - 130Total Iron (Fe) 2009/12/11 102 % 70 - 130Total Lead (Pb) 2009/12/11 94 % 70 - 130Total Magnesium (Mg) 2009/12/11 101 % 70 - 130Total Manganese (Mn) 2009/12/11 101 % 70 - 130Total Molybdenum (Mo) 2009/12/11 100 % 70 - 130Total Nickel (Ni) 2009/12/11 98 % 70 - 130Total Phosphorus (P) 2009/12/11 103 % 70 - 130Total Silver (Ag) 2009/12/11 97 % 70 - 130


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3622485 JC8 SRM Total Strontium (Sr) 2009/12/11 96 % 70 - 130Total Thallium (Tl) 2009/12/11 85 % 70 - 130Total Titanium (Ti) 2009/12/11 111 % 70 - 130Total Vanadium (V) 2009/12/11 107 % 70 - 130Total Zinc (Zn) 2009/12/11 87 % 70 - 130

Duplicate: Paired analysis of a separate portion of the same sample. Used to evaluate the variance in the measurement.Matrix Spike: A sample to which a known amount of the analyte of interest has been added. Used to evaluate sample matrix interference.SRM: A blank matrix sample to which a known amount of the analyte has been added. Used to evaluate analyte recovery.LCS: A blank matrix sample to which a known amount of the analyte has been added. Used to evaluate analyte recovery.Method Blank: A blank matrix containing all reagents used in the analytical procedure. Used to identify laboratory contamination.Surrogate: A pure or isotopically labeled compound whose behavior mirrors the analytes of interest. Used to evaluate extraction efficiency.NC (Matrix Spike): The recovery in the matrix spike was not calculated. The relative difference between the concentration in the parent sample and thespiked amount was not sufficiently significant to permit a reliable recovery calculation.NC (RPD): The RPD was not calculated. The level of analyte detected in the parent sample and its duplicate was not sufficiently significant to permit areliable calculation.( 1 ) Detection limits raised due to dilution to bring analyte within the calibrated range.


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Site Location: Burrard Inlet Pipe Removal Port Moody BCMaxxam Sample: S07308 Client ID: IPN-SD09-18



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Analyses Quantity Laboratory Method Primary referenceSend Part to Archive 5Environmental Sample Disposal Fee 5Moisture 5 BRN SOP-00321 R5.0 Ont MOE -E 3139PAH in Soil by GC/MS (SIM) 5 BRN SOP-00332 R9.0 Based on EPA 8270DTotal LMW, HMW, Total PAH Calc 5

Remarks:




All analysis data reported was generated when the analytical methods were in statistical control and criteria for spikerecoveries, reference material recoveries, method blanks data and duplicate precision were met unless otherwise stated.All samples were analysed within hold time unless otherwise flagged. All BTEX samples were methanol extracted within 24hours unless otherwise flagged.This report shall not be reproduced except in full, without the written approval of the laboratory.

Methods used by Maxxam are based upon those found in 'Standard Methods for the Examination of Water andWastewater', 21st Edition, published by the American Public Health Association, or on US EPA, protocols found in the '

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MAXXAM JOB #: A969867Received: 2009/12/04, 17:45Test Methods for Evaluating Solid Waste ', Physical/Chemical Methods, SW846, 3rd Edition. Other procedures are basedon the methodologies accepted by the appropriate regulatory agency. Methodology briefs are available by written request.



Encryption Key






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Sue Reynolds

11 Dec 2009 15:20:09 -08:00




Maxxam ID S 0 7 3 8 9 S 0 7 3 9 0 S 0 7 3 9 1 S 0 7 3 9 2Sampling Date 2009/11/30 2009/12/04 2009/12/04 2009/12/04

14:31 10:43 11:31 11:01COC Number F120172 F120172 F120172 F120172

U n i t s IPS-SD09-33B IPS-SD09-35B IPS-SD09-36B IPS-SD09-37B R D L QC Batch

Physical Properties

Moisture % 69 63 68 58 0.3 3611754




U n i t s IPS-SD09-40B R D L QC Batch

Physical Properties

Moisture % 70 0.3 3611754


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14:31 10:43 11:31COC Number F120172 F120172 F120172

U n i t s IPS-SD09-33B IPS-SD09-35B IPS-SD09-36B R D L QC Batch




Total PAH mg/kg 5.8 8.3 5.5 0.02 3611468





Fluorene mg/kg 0.07 0.12 0.08 0.01 3613171


Anthracene mg/kg 0.22 0.33 0.21 0.01 3613171


Pyrene mg/kg 1.1 2.2 0.94 0.01 3613171


Chrysene mg/kg 0.96 0.64 0.46 0.01 3613171













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11:01 11:58COC Number F120172 F120172

U n i t s IPS-SD09-37B IPS-SD09-40B R D L QC Batch



High Molecular Weight PAH`s mg/kg 0.93 10 0.02 3611468

Total PAH mg/kg 1.2 12 0.02 3611468




Acenaphthene mg/kg <0.01 0.06 0.01 3613171

Fluorene mg/kg 0.02 0.16 0.01 3613171


Anthracene mg/kg 0.07 0.51 0.01 3613171


Pyrene mg/kg 0.25 3.2 0.01 3613171


Chrysene mg/kg 0.17 1.5 0.01 3613171





Dibenz(a,h)anthracene mg/kg <0.02 0.10 0.02 3613171








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Test Summary

Maxxam ID S07389 Collected 2009/11/30Sample ID IPS-SD09-33B Shipped 2009/12/04


Test Description Instrumentation Batch Extracted Analyzed AnalystMoisture BAL 3611754 N/A 2009/12/08 WC4PAH in Soil by GC/MS (SIM) GC/MSD 3613171 2009/12/07 2009/12/08 SYTotal LMW, HMW, Total PAH Calc GC/MSD 3611468 N/A 2009/12/11 ASC

Maxxam ID S07389 D u p Collected 2009/11/30Sample ID IPS-SD09-33B Shipped 2009/12/04


Test Description Instrumentation Batch Extracted Analyzed AnalystMoisture BAL 3611754 N/A 2009/12/08 WC4










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Test Summary




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General Comments


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3611754 WC4 Method Blank Moisture 2009/12/08 <0.3 %3613171 SY Method Blank D10-ANTHRACENE (sur.) 2009/12/08 90 % 30 - 130


3611754 WC4 RPD [ S 0 7 3 8 9 - 0 1 ] Moisture 2009/12/08 0.3 % 203613171 SY LCS D10-ANTHRACENE (sur.) 2009/12/08 79 % 30 - 130

D12-BENZO(A)PYRENE (sur.) 2009/12/08 74 % 30 - 130D8-ACENAPHTHYLENE (sur.) 2009/12/08 76 % 30 - 130TERPHENYL-D14 (sur.) 2009/12/08 78 % 30 - 130Naphthalene 2009/12/08 84 % 50 - 1302-Methylnaphthalene 2009/12/08 89 % 50 - 130Acenaphthylene 2009/12/08 79 % 50 - 130Acenaphthene 2009/12/08 84 % 50 - 130Fluorene 2009/12/08 81 % 50 - 130Phenanthrene 2009/12/08 83 % 60 - 130Anthracene 2009/12/08 81 % 60 - 130Fluoranthene 2009/12/08 84 % 60 - 130Pyrene 2009/12/08 86 % 60 - 130Benzo(a)anthracene 2009/12/08 78 % 60 - 130Chrysene 2009/12/08 78 % 60 - 130Benzo(b&j)fluoranthene 2009/12/08 82 % 60 - 130Benzo(k)fluoranthene 2009/12/08 74 % 60 - 130Benzo(a)pyrene 2009/12/08 80 % 60 - 130Indeno(1,2,3-cd)pyrene 2009/12/08 69 % 60 - 130Dibenz(a,h)anthracene 2009/12/08 65 % 60 - 130Benzo(g,h,i)perylene 2009/12/08 68 % 60 - 130

Duplicate: Paired analysis of a separate portion of the same sample. Used to evaluate the variance in the measurement.LCS: A blank matrix sample to which a known amount of the analyte has been added. Used to evaluate analyte recovery.Method Blank: A blank matrix containing all reagents used in the analytical procedure. Used to identify laboratory contamination.Surrogate: A pure or isotopically labeled compound whose behavior mirrors the analytes of interest. Used to evaluate extraction efficiency.


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