Appendix D - deq.state.or.us Inlet (bottom side) 6”-12” RF weld neck 150# flange (refer to chart...

Appendix D

SVE System Component Literature

PROTECT VSCarbon Adsorber Canisters

DescriptionThe PROTECT VS vapor phase carbon adsorber canisters are airor vapor treatment units that can treat higher flow rates orcontain larger beds of activated carbon, but with theconvenience of an economical canister. PROTECT VS canisterscontain all of the operating elements required for utilization ofgranular activated carbon in air or vapor treatment, including aflat carbon bed support across the entire bed cross sectional areaand plenum area below this support for effective air introductionand distribution across the bed. The canisters are constructed ofunlined carbon steel with a stainless steel screen bed support foruse with activated carbon in air treatment.The PROTECT VS vapor phase carbon adsorber canisters areavailable in 3 sizes that can contain up to 8,000 pounds ofgranular activated carbon for treating air or vapor sourcestypically up to 4,500 cfm. The PROTECT VS canisters can be usedin operating pressures up to 1 psi and a moderate vacuum of upto 5 inches Mercury.The PROTECT VS vapor phase adsorbers can be provided withany of Calgon Carbon’s wide variety of vapor phase activatedcarbon products that can be selected for a specific air or vaportreatment application. Most commonly used are Type AP4-60grade virgin activated carbon, which is a 4mm pelletizedactivated carbon with a Carbon Tetrachloride Number of 60 forhigher purity air or vapor, or optimal usage for low levelsof organic contamination, or Type VPR quality controlledreactivated grade vapor phase carbon for a more economicalcarbon product for general air treatment.

FeaturesThe PROTECT VS vapor phase carbon adsorber canisters offerseveral important features that make it an effective value drivenoption for many air or vapor phase treatment applications:•Sturdy carbon steel construction

• Sturdy carbon steel construction• Capable of operating up to 1 psig which will manage most

vent or exhaust fan situations.• Exterior painted with a durable urethane finish• Operating temperature up to 200 degrees F• Top 16 inch diameter access port for activated carbon media

fill and removal• Carbon bed support across the full canister cross sectional

area, consisting of 20 mesh type 316 stainless steel screenplaced on steel grating for vapor distribution across theentire bed for maximum activated carbon utilization and lowpressure drop.

• Top lifting lugs and bottom fork guides for portability

Specifications

Canister Sturdy carbon steel canister with ¼”thick steel shell and ¼” steel flatbottom and top heads(3/8” thickness for Model VS-8)

Pressure Recommended 1 psig maximumoperating pressure (shop hydrotestedin excess of recommended pressure)

Vacuum Recommended maximum5” Hg vacuum operation

Temperature Recommended 200˚F (max)

Internal Coating None – unfinished steel

External Coating Direct-to-Metal polyurethane

Inlet (bottom side) 6”-12” RF weld neck 150# flange(refer to chart for sizes for each Model)

Inlet Distributor Stainless steel screen bed support ongalvanized steel grating

Outlet (top side) 6”-12” RF weld neck 150# flange(refer to chart for sizes for each Model)

Drain (2 on bottom) ¾” FPT coupling with ¾” threaded plug

Access Port 16” diameter access port with threadedclamp ring and BUNA-N gasket.

Dimensions Refer to Model Chart

Making Water and Air Safer and Cleaner


Copyright© 2009 Calgon Carbon Corporation, all rights reserved. ES-0027-1109 www.calgoncarbon.com

Safety ConsiderationsWhile complying with the recommended installation instruc-tions, plant operators should also be aware of these additionalheat-related safety considerations:

• When in contact with activated carbon, some types oforganic chemical compounds, such as those from the ketoneand aldehyde families and some organic acids or organicsulfur compounds, may react on the carbon surface causingsevere exotherms or temperature excursions. If you areunaware or unsure of the reaction of an organiccompound on activated carbon, appropriate tests shouldbe performed before placing a PROTECT VS canisterin service.

• Heat of adsorption can lead to severe temperatureexcursions at high concentrations of organic compounds inthe inlet air or vapor. Heating may be controlled by dilutingthe inlet air or adding water vapor as a heat sink, by timeweighting the inlet concentration to allow heat to dissipate,or by pre-wetting the carbon.

• Do not use PROTECT VS canisters with ST1-X carbon inpetrochemical or chemical industry applications.

• ST1-X carbon can liberate heat by reacting chemicallywith oxygen. To prevent heat buildup within a canister, thecarbon must not be confined without adequate air flow todissipate the heat. In situations where there is insufficient ordisrupted air flow through the vessel, the chemical reactioncan be prevented by sealing the inlet and outlet connectionsto the canister.

Safety MessageActivated carbon will preferentially remove oxygen from air. Inclosed or partially closed containers or vessels, oxygen depletionmay reach hazardous levels. If workers are to enter a containeror vessel containing activated carbon, appropriate air samplingand work procedures for potentially low oxygen content spacesshould be followed, including all applicable Federal and Staterequirements.

WarrantyCalgon Carbon Corporation warrants that the PROTECT VScanister will be free from defects in materials and workmanshipfor a period of 90 days following the date of purchase. In theevent of a breach of this warranty, Calgon Carbon Corporationwill, in its discretion, repair or replace any defective parts or thecomplete unit during the warranty period. This warranty does notapply to defects caused by (i) normal wear and tear, (ii) accident,disaster or event of force majeure, (iii) misuse, fault ornegligence of or by Buyer, (iv) use of the PROTECT VS canister ina manner for which it is not designed, (v) external causes suchas, but not limited to, power failure or electrical power surges, or(vi) improper storage and handling of the PROTECT VS canister.Except as expressly provided in this warranty statement,Calgon Carbon Corporation disclaims all other warranties,whether express or implied, oral or written, including withoutlimitations all implied warranties or merchantability orfitness for particular purpose. Calgon Carbon Corporationdoes not warrant that the PROTECT VS canisters are error-freeor will accomplish any particular result. Any advice orassistance furnished by Calgon Carbon Corporation inrelation to the PROTECT VS canister provided for hereundershall not give rise to any warranty or guarantee of any kind.This warranty will take precedence over any and all otherwarranties unless specifically disclaimed and referenced byCalgon Carbon Corporation.

Limitations of LiabilityCarbon Carbon Corporation’ liability and the Buyer’s exclusiveremedy for any cause of action arising out this transaction,including, but not limited to, breach of warranty, negligenceand/or indemnification, is expressly limited to a maximum of thepurchase price of the canister sold hereunder. All claims ofwhatsoever nature shall be deemed waived unless made inwriting within forty-five (45) days of the occurrence giving rise tothe claim. Under no circumstance shall Calgon CarbonCorporation be liable for any incidental, consequential, punitive,exemplary, or special damages of any kind arising as a result ofor in connection with the PROTECT VS canisters regardless of thecause giving rise to any claim. Nor shall Calgon CarbonCorporation be liable for loss of profits or fines imposed bygovernmental agencies. In no event shall Calgon CarbonCorporation’s liability exceed the purchase price paid bypurchaser, for any reason, whether by reason of breach ofcontract, tort, indemnification, warranty or otherwise. Thislimitation of liability statement will take precedence over any andall other liability provisions unless specifically disclaimed andreferenced by Calgon Carbon Corporation.

Calgon Carbon CorporationP.O. Box 717Pgh, PA USA 15230-07171-800-422-7266Tel: 1-412-787-6700Fx: 1-412-787-6713

Chemviron CarbonEuropean Operations ofCalgon Carbon CorporationZoning Industriel C de FeluyB-7181 Feluy, BelgiumTel: + 32 (0) 64 51 18 11Fx: + 32 (0) 64 54 15 91

Calgon Carbon Asia PTE LTD9 Temasek Boulevard#08-01A Suntec Tower TwoSingapore 038989Tel: + 65 6 221 3500Fx: + 65 6 221 3554

Your local representative




Installation

PROTECT VS canisters are shipped ready for installation with thedry activated carbon fill installed in the unit. The canisters are selfsupporting and should be set on a level accessible area as nearas possible to the emission source. Standard installation doesnot utilize any anchoring devices. Installation is simple requiringa flexible hose, duct or pipe to connect the vent or emissionsource to the flanged bottom inlet of the canister.

The PROTECT VS canister’s treated air discharge is a flanged con-nection on the upper side of the vessel and can be left open orequipped with flexible hose, duct or pipe to direct the treated airto a desired discharge point. If the canister is located outside andto be vented directly, then a U-shaped outlet pipe or rain hat(such as a pipe tee) is recommended to be installed to preventprecipitation from entering the unit.

The recommended air flow for the PROTECT VS canisters arelisted in the table. If higher flows are anticipated, then either alarger canister should be utilized or two or more PROTECT VScanisters should be placed in parallel operation.

The recommended maximum static pressure and vacuumcapabilities are also listed. These ratings should not be exceed-ed, as the canister could be irreparably damaged.

PROTECT VS canisters can be used to treat vents directly fromstorage tank or other process vessels. The motive force for the airor vapor can be produced by either a blower or by using the pos-itive pressure inside the tank or process vessel. In many cases,the pressure or surge of pressure within the tank or vessel is suf-ficient to overcome the pressure drop across the canister, thuseliminating the need for a blower. Please consult thepressure drop data in this bulletin for more information.

When PROTECT VS canisters are used to control vapors fromorganic solvent storage tanks, refer to the typical installationdrawing in the bulletin and the following recommendedprecautions:

• A safety relief valve must be provided on the storage tank.This protects the storage tank should the canister becomeplugged or blocked in any fashion. Such a vent would openin an emergency situation, thereby relieving pressure withinthe storage tank.

• Under appropriate conditions, a flame arrestor and/orbackflow preventer must be installed as shown in thetypical installation drawing. This prevents backflow ofair through the canister when the storage tank isbeing emptied.

• High organic compound concentration in the vented air orvapor – defined as being greater than 0.5 to 1.0 volume %- may cause an elevated heat of adsorption in the carbonbed. This effect can be dissipated by pre-wetting thecarbon to provide a heat sink, adding dilution air to thevented air or vapor to reduce the concentration, or byadding water spray to the vented air or vapor to providean ongoing heat sink.

Typical Protect VS Installation at Storage Tank

If PROTECT VS canisters are used to control organic compoundemissions from air-strippers, soil venting or other high moisturecontent air or vapor streams, then it is recommended that thehumidity in the air stream be reduced to under 50%. Highhumidity may cause water vapor to condense within the carbonpores, filling the pores with water and preventing the air or vaporwith organic contamination from accessing the internal surfaceof the activated carbon where adsorption takes place. Therefore,lower humidity will optimize the adsorptive capacity of theactivated carbon. Also, for applications that may carry condensedwater, it is recommended to install a drain or condensate trap onthe inlet duct or piping.

Carbon Exchange or ReplacementWhen the treated air or vapor exceeds the desired contaminantconcentration, the granular activated carbon in the PROTECT VScanister should be replaced with fresh activated carbon. Thecanister is to be isolated from the process by either closing andlocking the inlet and outlet valves, or physically disconnecting thecanister from the inlet and outlet pipe or hose. The carbonexchange procedure can either take place where the canister isinstalled, or the disconnected canister can be moved to anotherlocation for this activity.The spent granular activated carbon can be removed by using avacuum media removal procedure through the top access port.Fresh granular activated carbon can be filled using bags or“supersacks” by loading into the canister through the top accessport. Refer to the table for the recommended amount of carbonto be used. Once the fresh carbon is installed and the bedleveled, the access port securely closed, and the inlet and outletconnections are reestablished, follow the procedures under theInstallation section.Contact Calgon Carbon Corporation for resupply of the carbonproducts for effective air or vapor treatment. Calgon CarbonCorporation can also provide complete turnkey services,including removal and management of the spent carbon andrefilling the canister with the fresh carbon.

www.calgoncarbon.com

Pressure Drop CurvePressure drop through a PROTECT VS canister is a function ofthe process air flow as shown in the graph. If higher flows orlower pressure drop is needed, multiple canisters can beinstalled in parallel operation. The maximum pressure in thecanister should not exceed 1 psig, regardless of the pressuredrop across the unit.

Pressure Drop Curve

Calgon Carbon Air Purification SystemsThe PROTECT VS canister is designed for a variety of air or vaporapplications at air flows up to 4,500 cfm and pressures up to 1psi. Calgon Carbon Corporation offers a wide range of carbonadsorption systems and services for a range of air or vapor flowrates and pressures to meet specific applications. Contact CalgonCarbon for resupply of the carbon products for effective watertreatment. Calgon Carbon can also provide complete turnkeyservices, including removal and management of the spentcarbon and refilling the unit with the fresh carbon.

Manway

B

G

A

F

Drain

ED

VentOutlet

Inlet

Model Number VS 4 VS 6 VS 8

GAC or media volume (cu ft) 72 180 288

GAC amount (pounds) 2,000 5,000 8,000

Recommended max flow rate (cfm) 1,100 2,500 4,500

Weight, empty (pounds) 1,760 3,340 4,900

Approximate operating weight (pounds) 3,760 8,340 12,900

Cross sectional area; square feet 16 36 64

Overall Height (A) in. (approx) 78 103 103

Width of side (B) in. +/- ¼” 49 73 97

Inlet /Outlet (C) 150# RF flange 6 8 12

Height to inlet (D) in. (approx) 8 10 13

Height to outlet (E) in. (approx) 70 92.5 89

Length including inlet/outlet flanges (F) +/- 52 77 101

Width of Forkguides (G) in 36 48 48

Model Information

0

2.0

4.0

6.0

8.0

10.0

12.0

14.0

16.0

0 1,000 2,000 3,000 4,000 5,000

VS-4

VS-6 VS-8

Flowrate (cfm)Estimated pressure drop based on 4x10 mesh carbon

Pres

sure

Dro

p(i

nche

sH

20)

Safety Relief Flame Arrestor

4" PipeHose or Duct

Vacuum Relief

Vent Pipe

PROTECT VSBackflowPreventer

StorageTank




Installation

PROTECT VS canisters are shipped ready for installation with thedry activated carbon fill installed in the unit. The canisters are selfsupporting and should be set on a level accessible area as nearas possible to the emission source. Standard installation doesnot utilize any anchoring devices. Installation is simple requiringa flexible hose, duct or pipe to connect the vent or emissionsource to the flanged bottom inlet of the canister.

The PROTECT VS canister’s treated air discharge is a flanged con-nection on the upper side of the vessel and can be left open orequipped with flexible hose, duct or pipe to direct the treated airto a desired discharge point. If the canister is located outside andto be vented directly, then a U-shaped outlet pipe or rain hat(such as a pipe tee) is recommended to be installed to preventprecipitation from entering the unit.

The recommended air flow for the PROTECT VS canisters arelisted in the table. If higher flows are anticipated, then either alarger canister should be utilized or two or more PROTECT VScanisters should be placed in parallel operation.

The recommended maximum static pressure and vacuumcapabilities are also listed. These ratings should not be exceed-ed, as the canister could be irreparably damaged.

PROTECT VS canisters can be used to treat vents directly fromstorage tank or other process vessels. The motive force for the airor vapor can be produced by either a blower or by using the pos-itive pressure inside the tank or process vessel. In many cases,the pressure or surge of pressure within the tank or vessel is suf-ficient to overcome the pressure drop across the canister, thuseliminating the need for a blower. Please consult thepressure drop data in this bulletin for more information.

When PROTECT VS canisters are used to control vapors fromorganic solvent storage tanks, refer to the typical installationdrawing in the bulletin and the following recommendedprecautions:

• A safety relief valve must be provided on the storage tank.This protects the storage tank should the canister becomeplugged or blocked in any fashion. Such a vent would openin an emergency situation, thereby relieving pressure withinthe storage tank.

• Under appropriate conditions, a flame arrestor and/orbackflow preventer must be installed as shown in thetypical installation drawing. This prevents backflow ofair through the canister when the storage tank isbeing emptied.

• High organic compound concentration in the vented air orvapor – defined as being greater than 0.5 to 1.0 volume %- may cause an elevated heat of adsorption in the carbonbed. This effect can be dissipated by pre-wetting thecarbon to provide a heat sink, adding dilution air to thevented air or vapor to reduce the concentration, or byadding water spray to the vented air or vapor to providean ongoing heat sink.

Typical Protect VS Installation at Storage Tank

If PROTECT VS canisters are used to control organic compoundemissions from air-strippers, soil venting or other high moisturecontent air or vapor streams, then it is recommended that thehumidity in the air stream be reduced to under 50%. Highhumidity may cause water vapor to condense within the carbonpores, filling the pores with water and preventing the air or vaporwith organic contamination from accessing the internal surfaceof the activated carbon where adsorption takes place. Therefore,lower humidity will optimize the adsorptive capacity of theactivated carbon. Also, for applications that may carry condensedwater, it is recommended to install a drain or condensate trap onthe inlet duct or piping.

Carbon Exchange or ReplacementWhen the treated air or vapor exceeds the desired contaminantconcentration, the granular activated carbon in the PROTECT VScanister should be replaced with fresh activated carbon. Thecanister is to be isolated from the process by either closing andlocking the inlet and outlet valves, or physically disconnecting thecanister from the inlet and outlet pipe or hose. The carbonexchange procedure can either take place where the canister isinstalled, or the disconnected canister can be moved to anotherlocation for this activity.The spent granular activated carbon can be removed by using avacuum media removal procedure through the top access port.Fresh granular activated carbon can be filled using bags or“supersacks” by loading into the canister through the top accessport. Refer to the table for the recommended amount of carbonto be used. Once the fresh carbon is installed and the bedleveled, the access port securely closed, and the inlet and outletconnections are reestablished, follow the procedures under theInstallation section.Contact Calgon Carbon Corporation for resupply of the carbonproducts for effective air or vapor treatment. Calgon CarbonCorporation can also provide complete turnkey services,including removal and management of the spent carbon andrefilling the canister with the fresh carbon.

www.calgoncarbon.com

Pressure Drop CurvePressure drop through a PROTECT VS canister is a function ofthe process air flow as shown in the graph. If higher flows orlower pressure drop is needed, multiple canisters can beinstalled in parallel operation. The maximum pressure in thecanister should not exceed 1 psig, regardless of the pressuredrop across the unit.

Pressure Drop Curve

Calgon Carbon Air Purification SystemsThe PROTECT VS canister is designed for a variety of air or vaporapplications at air flows up to 4,500 cfm and pressures up to 1psi. Calgon Carbon Corporation offers a wide range of carbonadsorption systems and services for a range of air or vapor flowrates and pressures to meet specific applications. Contact CalgonCarbon for resupply of the carbon products for effective watertreatment. Calgon Carbon can also provide complete turnkeyservices, including removal and management of the spentcarbon and refilling the unit with the fresh carbon.

Manway

B

G

A

F

Drain

ED

VentOutlet

Inlet

Model Number VS 4 VS 6 VS 8

GAC or media volume (cu ft) 72 180 288

GAC amount (pounds) 2,000 5,000 8,000

Recommended max flow rate (cfm) 1,100 2,500 4,500

Weight, empty (pounds) 1,760 3,340 4,900

Approximate operating weight (pounds) 3,760 8,340 12,900

Cross sectional area; square feet 16 36 64

Overall Height (A) in. (approx) 78 103 103

Width of side (B) in. +/- ¼” 49 73 97

Inlet /Outlet (C) 150# RF flange 6 8 12

Height to inlet (D) in. (approx) 8 10 13

Height to outlet (E) in. (approx) 70 92.5 89

Length including inlet/outlet flanges (F) +/- 52 77 101

Width of Forkguides (G) in 36 48 48

Model Information

0

2.0

4.0

6.0

8.0

10.0

12.0

14.0

16.0

0 1,000 2,000 3,000 4,000 5,000

VS-4

VS-6 VS-8

Flowrate (cfm)Estimated pressure drop based on 4x10 mesh carbon

Pres

sure

Dro

p(i

nche

sH

20)

Safety Relief Flame Arrestor

4" PipeHose or Duct

Vacuum Relief

Vent Pipe

PROTECT VSBackflowPreventer

StorageTank



DescriptionThe PROTECT VS vapor phase carbon adsorber canisters are airor vapor treatment units that can treat higher flow rates orcontain larger beds of activated carbon, but with theconvenience of an economical canister. PROTECT VS canisterscontain all of the operating elements required for utilization ofgranular activated carbon in air or vapor treatment, including aflat carbon bed support across the entire bed cross sectional areaand plenum area below this support for effective air introductionand distribution across the bed. The canisters are constructed ofunlined carbon steel with a stainless steel screen bed support foruse with activated carbon in air treatment.The PROTECT VS vapor phase carbon adsorber canisters areavailable in 3 sizes that can contain up to 8,000 pounds ofgranular activated carbon for treating air or vapor sourcestypically up to 4,500 cfm. The PROTECT VS canisters can be usedin operating pressures up to 1 psi and a moderate vacuum of upto 5 inches Mercury.The PROTECT VS vapor phase adsorbers can be provided withany of Calgon Carbon’s wide variety of vapor phase activatedcarbon products that can be selected for a specific air or vaportreatment application. Most commonly used are Type AP4-60grade virgin activated carbon, which is a 4mm pelletizedactivated carbon with a Carbon Tetrachloride Number of 60 forhigher purity air or vapor, or optimal usage for low levelsof organic contamination, or Type VPR quality controlledreactivated grade vapor phase carbon for a more economicalcarbon product for general air treatment.

FeaturesThe PROTECT VS vapor phase carbon adsorber canisters offerseveral important features that make it an effective value drivenoption for many air or vapor phase treatment applications:•Sturdy carbon steel construction

• Sturdy carbon steel construction• Capable of operating up to 1 psig which will manage most

vent or exhaust fan situations.• Exterior painted with a durable urethane finish• Operating temperature up to 200 degrees F• Top 16 inch diameter access port for activated carbon media

fill and removal• Carbon bed support across the full canister cross sectional

area, consisting of 20 mesh type 316 stainless steel screenplaced on steel grating for vapor distribution across theentire bed for maximum activated carbon utilization and lowpressure drop.

• Top lifting lugs and bottom fork guides for portability

Specifications

Canister Sturdy carbon steel canister with ¼”thick steel shell and ¼” steel flatbottom and top heads(3/8” thickness for Model VS-8)

Pressure Recommended 1 psig maximumoperating pressure (shop hydrotestedin excess of recommended pressure)

Vacuum Recommended maximum5” Hg vacuum operation

Temperature Recommended 200˚F (max)

Internal Coating None – unfinished steel

External Coating Direct-to-Metal polyurethane

Inlet (bottom side) 6”-12” RF weld neck 150# flange(refer to chart for sizes for each Model)

Inlet Distributor Stainless steel screen bed support ongalvanized steel grating

Outlet (top side) 6”-12” RF weld neck 150# flange(refer to chart for sizes for each Model)

Drain (2 on bottom) ¾” FPT coupling with ¾” threaded plug

Access Port 16” diameter access port with threadedclamp ring and BUNA-N gasket.

Dimensions Refer to Model Chart



Copyright© 2009 Calgon Carbon Corporation, all rights reserved. ES-0027-1109 www.calgoncarbon.com

Safety ConsiderationsWhile complying with the recommended installation instruc-tions, plant operators should also be aware of these additionalheat-related safety considerations:

• When in contact with activated carbon, some types oforganic chemical compounds, such as those from the ketoneand aldehyde families and some organic acids or organicsulfur compounds, may react on the carbon surface causingsevere exotherms or temperature excursions. If you areunaware or unsure of the reaction of an organiccompound on activated carbon, appropriate tests shouldbe performed before placing a PROTECT VS canisterin service.

• Heat of adsorption can lead to severe temperatureexcursions at high concentrations of organic compounds inthe inlet air or vapor. Heating may be controlled by dilutingthe inlet air or adding water vapor as a heat sink, by timeweighting the inlet concentration to allow heat to dissipate,or by pre-wetting the carbon.

• Do not use PROTECT VS canisters with ST1-X carbon inpetrochemical or chemical industry applications.

• ST1-X carbon can liberate heat by reacting chemicallywith oxygen. To prevent heat buildup within a canister, thecarbon must not be confined without adequate air flow todissipate the heat. In situations where there is insufficient ordisrupted air flow through the vessel, the chemical reactioncan be prevented by sealing the inlet and outlet connectionsto the canister.

Safety MessageActivated carbon will preferentially remove oxygen from air. Inclosed or partially closed containers or vessels, oxygen depletionmay reach hazardous levels. If workers are to enter a containeror vessel containing activated carbon, appropriate air samplingand work procedures for potentially low oxygen content spacesshould be followed, including all applicable Federal and Staterequirements.

WarrantyCalgon Carbon Corporation warrants that the PROTECT VScanister will be free from defects in materials and workmanshipfor a period of 90 days following the date of purchase. In theevent of a breach of this warranty, Calgon Carbon Corporationwill, in its discretion, repair or replace any defective parts or thecomplete unit during the warranty period. This warranty does notapply to defects caused by (i) normal wear and tear, (ii) accident,disaster or event of force majeure, (iii) misuse, fault ornegligence of or by Buyer, (iv) use of the PROTECT VS canister ina manner for which it is not designed, (v) external causes suchas, but not limited to, power failure or electrical power surges, or(vi) improper storage and handling of the PROTECT VS canister.Except as expressly provided in this warranty statement,Calgon Carbon Corporation disclaims all other warranties,whether express or implied, oral or written, including withoutlimitations all implied warranties or merchantability orfitness for particular purpose. Calgon Carbon Corporationdoes not warrant that the PROTECT VS canisters are error-freeor will accomplish any particular result. Any advice orassistance furnished by Calgon Carbon Corporation inrelation to the PROTECT VS canister provided for hereundershall not give rise to any warranty or guarantee of any kind.This warranty will take precedence over any and all otherwarranties unless specifically disclaimed and referenced byCalgon Carbon Corporation.

Limitations of LiabilityCarbon Carbon Corporation’ liability and the Buyer’s exclusiveremedy for any cause of action arising out this transaction,including, but not limited to, breach of warranty, negligenceand/or indemnification, is expressly limited to a maximum of thepurchase price of the canister sold hereunder. All claims ofwhatsoever nature shall be deemed waived unless made inwriting within forty-five (45) days of the occurrence giving rise tothe claim. Under no circumstance shall Calgon CarbonCorporation be liable for any incidental, consequential, punitive,exemplary, or special damages of any kind arising as a result ofor in connection with the PROTECT VS canisters regardless of thecause giving rise to any claim. Nor shall Calgon CarbonCorporation be liable for loss of profits or fines imposed bygovernmental agencies. In no event shall Calgon CarbonCorporation’s liability exceed the purchase price paid bypurchaser, for any reason, whether by reason of breach ofcontract, tort, indemnification, warranty or otherwise. Thislimitation of liability statement will take precedence over any andall other liability provisions unless specifically disclaimed andreferenced by Calgon Carbon Corporation.

Calgon Carbon CorporationP.O. Box 717Pgh, PA USA 15230-07171-800-422-7266Tel: 1-412-787-6700Fx: 1-412-787-6713

Chemviron CarbonEuropean Operations ofCalgon Carbon CorporationZoning Industriel C de FeluyB-7181 Feluy, BelgiumTel: + 32 (0) 64 51 18 11Fx: + 32 (0) 64 54 15 91

Calgon Carbon Asia PTE LTD9 Temasek Boulevard#08-01A Suntec Tower TwoSingapore 038989Tel: + 65 6 221 3500Fx: + 65 6 221 3554

Your local representative


C-23

EN 858 & CP 858Sealed Regenerative Blower w/Explosion-Proof MotorFEATURES• Manufactured in the USA – ISO 9001 compliant• Maximum flow: 400 SCFM• Maximum pressure: 120 IWG• Maximum vacuum: 98 IWG• Standard motor: 10 HP, explosion-proof• Cast aluminum blower housing, cover, impeller &

manifold; cast iron flanges (threaded); teflon lip seal• UL & CSA approved motor with permanently

sealed ball bearings for explosive gas atmospheres Class I Group D minimum

• Sealed blower assembly• Quiet operation within OSHA standards

MOTOR OPTIONS• International voltage & frequency (Hz)• Chemical duty, high efficiency, inverter duty

or industry-specific designs• Various horsepowers for application-specific needs

BLOWER OPTIONS• Corrosion resistant surface treatments & sealing options• Remote drive (motorless) models• Slip-on or face flanges for application-specific needs

ACCESSORIES (See Catalog Accessory Section)• Flowmeters reading in SCFM• Filters & moisture separators• Pressure gauges, vacuum gauges & relief valves• Switches – air flow, pressure, vacuum or temperature• External mufflers for additional silencing• Air knives (used on blow-off applications)• Variable frequency drive package

BLOWER PERFORMANCE AT STANDARD CONDITIONSAIR FLOW RATE (M3/MIN)

INC

HE

S O

F W

AT

ER

PS

IG

mB

AR

PRESSURE▲-MAX PRESSURE

POINTA-10 HP B-7.5 HP

AIR FLOW RATE (SCFM)

MO

TO

RW

IND

ING

TE

MP

RIS

E °

C

PO

WE

RIN

PU

TW

AT

TS

BL

OW

ER

AIR

TE

MP

RIS

E °

C

AIR FLOW RATE (M3/MIN)

INC

HE

S O

F W

AT

ER

INC

HE

S O

F M

ER

CU

RY


MO

TO

RW

IND

ING

TE

MP

RIS

E °

C

PO

WE

RIN

PU

TW

AT

TS

BL

OW

ER

AIR

TE

MP

RIS

E °

C

0 100 200 300 400 500

12,000

9,000

6,000

3,000

150

100

50

0

120

80

40

0

5.0

4.0

1.0

2.0

3.0

140

120

100

80

60

40

20

100

200

300

0 100 200 300 400 500

12,000

9,000

6,000

3,000

150

100

50

0

120

80

40

0

10

8

2

4

6

-140

-120

-100

-80

-60

-40

-20

100

200

300

60 Hz

50 Hz

BA

A

▲

60 Hz

50 Hz

A, Bm

BA

R

250

150

50

250

150

50

SUCTION▲-MAX SUCTION

POINTA-10 HP B-7.5 HP

▲

▲

▲▲

6.0 10.02.0 4.0 8.0 14.012.0 6.0 10.02.0 4.0 8.0 14.012.0

▲B A, B

Rev. 2/01

Rev. 2/01

Scale CAD drawing available upon request.

1 Rotron motors are designed to handle a broad range of world voltages and power supply variations. Our dual voltage 3 phase motors arefactory tested and certified to operate on both: 208-230 /415-460 VAC-3 ph-60 Hz and 190-208/380-415 VAC-3 ph-50 Hz. Our dualvoltage 1 phase motors are factory tested and certified to operate on both: 104-115/208-230 VAC-1 ph-60 Hz and 100-110 /200-220VAC-1 ph-50 Hz. All voltages above can handle a ±10% voltage fluctuation. Special wound motors can be ordered for voltages outside ourcertified range.

2 Maximum operating temperature: Motor winding temperature (winding rise plus ambient) should not exceed 140°C for Class F rated motorsor 120°C for Class B rated motors. Blower outlet air temperature should not exceed 140°C (air temperature rise plus inlet temperature).Performance curve maximum pressure and suction points are based on a 40°C inlet and ambient temperature. Consult factory for inlet orambient temperatures above 40°C.

3 Maximum blower amps corresponds to the performance point at which the motor or blower temperature rise with a 40°C inlet and/orambient temperature reaches the maximum operating temperature.

Specifications subject to change without notice. Please consult your Local Field Sales Engineer for specification updates.

C-24

EN 858 & CP 858Sealed Regenerative Blower w/Explosion-Proof Motor

SPECIFICATIONS

MODEL EN858BD72WL EN858BD86WL EN858BA72WL CP858FZ72WLRPart No. 038744 038745 080070 038980Motor Enclosure – Shaft Material Explosion-proof – CS Explosion-proof – CS Explosion-proof – CS Chem XP – SSHorsepower 10.0 10.0 7.5Phase – Frequency 1 Three - 60 Hz Three - 60 Hz Three - 60 HzVoltage 1 230 460 575 230 460Motor Nameplate Amps 24 12 9.6 17 8.5Max. Blower Amps 3 29 14.5 11.6 26 13Inrush Amps 162 81 93 126 63Starter Size 2 1 1 1 1Service Factor 1.0 1.0 1.0Thermal Protection 2 Class B - Pilot Duty Class B - Pilot Duty Class B - Pilot DutyXP Motor Class – Group I-D, II-F&G I-D, II-F&G I-D, II-F&GShipping Weight 332 lb (151 kg) 332 lb (151 kg) 320 lb (145 kg)

A 0.75" NPT CONDUIT CONNECTION AT 12 O’CLOCK POSITION

Same asEN858BD72WL –

038744except add

Chemical Processing(CP)

features from

cataloginside front cover

DIMENSIONS: INMM

TOLERANCES: .XX ± .12.5

(UNLESS OTHERWISE NOTED)

C-25

EN 909 & CP 909Sealed Regenerative Blower w/Explosion-Proof MotorFEATURES• Manufactured in the USA – ISO 9001 compliant• Maximum flow: 600 SCFM• Maximum pressure: 120 IWG• Maximum vacuum: 100 IWG• Standard motor: 15 HP, explosion-proof• Cast aluminum blower housing, cover, impeller &

manifold; cast iron flanges (threaded); teflon lip seal• UL & CSA approved motor with permanently

sealed ball bearings for explosive gas atmospheres Class I Group D minimum

• Sealed blower assembly• Quiet operation within OSHA standards

MOTOR OPTIONS• International voltage & frequency (Hz)• Chemical duty, high efficiency, inverter duty

or industry-specific designs• Various horsepowers for application-specific needs

BLOWER OPTIONS• Corrosion resistant surface treatments & sealing options• Remote drive (motorless) models• Slip-on or face flanges for application-specific needs

ACCESSORIES (See Catalog Accessory Section)• Flowmeters reading in SCFM• Filters & moisture separators• Pressure gauges, vacuum gauges & relief valves• Switches – air flow, pressure, vacuum or temperature• External mufflers for additional silencing• Air knives (used on blow-off applications)• Variable frequency drive package

BLOWER PERFORMANCE AT STANDARD CONDITIONSAIR FLOW RATE (M3/MIN)

140

120

100

80

60

40

20

350

300

250

200

150

100

50

5.0

4.0

3.0

2.0

1.0

INC

HE

S O

F W

AT

ER

PS

IG

mB

AR

0 100 200 300 500400 600 700

AIR FLOW RATE (SCFM)100

50

0

17,500

12,500

7,500

2,500

100

50

0

MO

TO

RW

IND

ING

TE

MP

RIS

E °

C

PO

WE

RIN

PU

TW

AT

TS

BL

OW

ER

AIR

TE

MP

RIS

E °

C

AIR FLOW RATE (M3/MIN)

10

8

6

4

2

INC

HE

S O

F W

AT

ER

INC

HE

S O

F M

ER

CU

RY


MO

TO

RW

IND

ING

TE

MP

RIS

E °

C

PO

WE

RIN

PU

TW

AT

TS

BL

OW

ER

AIR

TE

MP

RIS

E °

C

PRESSURE▲-MAX PRESSURE

POINTA-15 HP B-10 HP

-140

-120

-100

-80

-60

-40

-20

350

300

250

200

150

100

50

mB

AR

0 100 200 300 500400 600 700

SUCTION▲-MAX SUCTION

POINTA-15 HP B-10 HP

100

50

0

17,500

12,500

7,500

2,500

100

50

0

60 Hz50 Hz

60 Hz

50 Hz

▲

▲A,B

▲▲

A,B

▲

A

B

▲

A

B

2 4 6 8 10 12 14 16 18 20 2 4 6 8 10 12 14 16 18 20

Rev. 2/01

Rev. 2/01

Scale CAD drawing available upon request.

1 Rotron motors are designed to handle a broad range of world voltages and power supply variations. Our dual voltage 3 phase motors arefactory tested and certified to operate on both: 208-230 /415-460 VAC-3 ph-60 Hz and 190-208/380-415 VAC-3 ph-50 Hz. Our dualvoltage 1 phase motors are factory tested and certified to operate on both: 104-115/208-230 VAC-1 ph-60 Hz and 100-110 /200-220VAC-1 ph-50 Hz. All voltages above can handle a ±10% voltage fluctuation. Special wound motors can be ordered for voltages outside ourcertified range.

2 Maximum operating temperature: Motor winding temperature (winding rise plus ambient) should not exceed 140°C for Class F rated motorsor 120°C for Class B rated motors. Blower outlet air temperature should not exceed 140°C (air temperature rise plus inlet temperature).Performance curve maximum pressure and suction points are based on a 40°C inlet and ambient temperature. Consult factory for inlet orambient temperatures above 40°C.

3 Maximum blower amps corresponds to the performance point at which the motor or blower temperature rise with a 40°C inlet and/orambient temperature reaches the maximum operating temperature.

Specifications subject to change without notice. Please consult your Local Field Sales Engineer for specification updates.

C-26

EN 909 & CP 909Sealed Regenerative Blower w/Explosion-Proof Motor

SPECIFICATIONS

MODEL EN909BG72WL EN909BG86WL EN909BD72WL CP909GA72WLRPart No. 038629 038634 080071 038982Motor Enclosure – Shaft Material Explosion-proof – CS Explosion-proof – CS Explosion-proof – CS Chem XP – SSHorsepower 15 15 10Phase – Frequency 1 Three - 60 Hz Three - 60 Hz Three - 60 HzVoltage 1 230 460 575 230 460Motor Nameplate Amps 36 18 14.4 24 12Max. Blower Amps 3 44 22 18 26 13Inrush Amps 240 120 100 162 81Starter Size 2 2 2 2 1Service Factor 1.0 1.0 1.0Thermal Protection 2 Class B - Pilot Duty Class B - Pilot Duty Class B - Pilot DutyXP Motor Class – Group I-D, II-F&G I-D, II-F&G I-D, II-F&GShipping Weight 584 lb (265 kg) 584 lb (265 kg) 564 lb (256 kg)

A 1.25" NPT CONDUIT CONNECTION AT 6 O’CLOCK POSITION

Same asEN909BG72WL –

038629except add

Chemical Processing(CP)

features from

cataloginside front cover

DIMENSIONS: INMM

TOLERANCES: .XX ± .12.5

(UNLESS OTHERWISE NOTED)

Appendix E

Disposal Records

Appendix F

Shallow and Deep SVE and VCP Vapor Stream Laboratory Reports

12/2/2009

Mr. John FoxwellAsh Creek Associates9615 SW Allen BoulevardSuite 106Beaverton OR 97005

Project Name: TARRSVE IRAMProject #: 1073-06

Dear Mr. John Foxwell

The following report includes the data for the above referenced project for sample(s) received on 11/12/2009 at Air Toxics Ltd.

The data and associated QC analyzed by Modified TO-15 are compliant with the project requirements or laboratory criteria with the exception of the deviations noted in the attached case narrative.

Thank you for choosing Air Toxics Ltd. for your air analysis needs. Air Toxics Ltd. is committed to providing accurate data of the highest quality. Please feel free to contactthe Project Manager: Kelly Buettner at 916-985-1000 if you have any questions regarding the data in this report.

Regards,

Kelly BuettnerProject Manager

Workorder #: 0911256A

180 BLUE RAVINE ROAD, SUITE B FOLSOM, CA - 95630(916) 985-1000 .FAX (916) 985-1020

Hours 6:30 A.M to 5:30 PSTPage 1 of 24

Mr. John FoxwellAsh Creek Associates9615 SW Allen BoulevardSuite 106Beaverton, OR 97005

WORK ORDER #: 0911256A

CLIENT: BILL TO:

PHONE:


503-924-4704x113

503-924-4707

11/12/2009DATE COMPLETED: 12/02/2009

P.O. #

PROJECT # 1073-06 TARRSVE IRAM

Work Order Summary

FAX:

DATE RECEIVED: CONTACT: Kelly Buettner

NAMEFRACTION # TEST VAC./PRES.RECEIPT

PRESSUREFINAL

03A DEEP POSTCARBON-111109 Modified TO-15 3.0 "Hg 5 psi03B DEEP POSTCARBON-111109 Modified TO-15 3.0 "Hg 5 psi06A SHALLOW POSTCARBON-111109 Modified TO-15 2.5 "Hg 5 psi06B SHALLOW POSTCARBON-111109 Modified TO-15 2.5 "Hg 5 psi07A VCP POSTCARBON-111109 Modified TO-15 0.5 "Hg 5 psi07B VCP POSTCARBON-111109 Modified TO-15 0.5 "Hg 5 psi08A Lab Blank Modified TO-15 NA NA08B Lab Blank Modified TO-15 NA NA09A CCV Modified TO-15 NA NA09B CCV Modified TO-15 NA NA10A LCS Modified TO-15 NA NA10B LCS Modified TO-15 NA NA

CERTIFIED BY:

Laboratory Director

DATE:

Name of Accrediting Agency: NELAP/Florida Department of Health, Scope of Application: Clean Air Act, Accreditation number: E87680, Effective date: 07/01/09, Expiration date: 06/30/10

180 BLUE RAVINE ROAD, SUITE B FOLSOM, CA - 95630(916) 985-1000 . (800) 985-5955 . FAX (916) 985-1020

12/02/09

Page 2 of 24

This report shall not be reproduced, except in full, without the written approval of Air Toxics Ltd.

Air Toxics Ltd. certifies that the test results contained in this report meet all requirements of the NELAC standards

Certfication numbers: CA NELAP - 02110CA, LA NELAP/LELAP- AI 30763, NJ NELAP - CA004NY NELAP - 11291, UT NELAP - 9166389892, AZ Licensure AZ0719

LABORATORY NARRATIVEModified TO-15 Full Scan/SIM

Ash Creek AssociatesWorkorder# 0911256A

Laboratory Services Since 1989

Three 6 Liter Summa Canister (SIM Certified) samples were received on November 12, 2009. Thelaboratory performed analysis via modified EPA Method TO-15 using GC/MS in the Full Scan and SIMacquisition modes. The method involves concentrating up to 1.0 liters of air. The concentrated aliquot is then flash vaporized and swept through a water management system to remove water vapor. Following dehumidification, the sample passes directly into the GC/MS for analysis.

This workorder was independently validated prior to submittal using 'USEPA National Functional Guidelines' as generally applied to the analysis of volatile organic compounds in air. A rules-based, logic driven,independent validation engine was employed to assess completeness, evaluate pass/fail of relevant project quality control requirements and verification of all quantified amounts.

Method modifications taken to run these samples are summarized in the table below. Specific projectrequirements may over-ride the ATL modifications.

Requirement ATL ModificationsTO-15ICAL %RSD acceptance criteria </=30% RSD with 2

compounds allowed out to < 40% RSD

For Full Scan: 30% RSD with 4 compounds allowed out to < 40% RSD

For SIM:Project specific; default criteria is </=30% RSD with 10% of compounds allowed out to < 40% RSD

Daily Calibration +- 30% Difference For Full Scan:</= 30% Difference with four allowed out up to </=40%.; flag and narrate outliers

For SIM:Project specific; default criteria is </= 30% Difference with 10% of compounds allowed out up to </=40%.; flag and narrate outliers

Blank and standards Zero air Nitrogen

Method Detection Limit Follow 40CFR Pt.136 App. B

The MDL met all relevant requirements in Method TO-15 (statistical MDL less than the LOQ). The concentration of the spiked replicate may have exceeded 10X the calculated MDL in some cases

Receiving Notes

There were no receiving discrepancies.

The results for each sample in this report were acquired from two separate data files originating from thesame analytical run. The two data files have the same base file name and are differentiated with a "sim" extension on the SIM data file.

Analytical Notes

Page 3 of 24


All Quality Control Limit exceedences and affected sample results are noted by flags. Each flag is defined at the bottom of this Case Narrative and on each Sample Result Summary page. Target compound non-detectsin the samples that are associated with high bias in QC analyses have not been flagged.

Dilution was performed on samples DEEP POSTCARBON-111109, SHALLOWPOSTCARBON-111109 and VCP POSTCARBON-111109 due to the presence of high level non-targetspecies.

Eight qualifiers may have been used on the data analysis sheets and indicates as follows: B - Compound present in laboratory blank greater than reporting limit (background subtraction notperformed). J - Estimated value. E - Exceeds instrument calibration range. S - Saturated peak. Q - Exceeds quality control limits. U - Compound analyzed for but not detected above the reporting limit. UJ- Non-detected compound associated with low bias in the CCV N - The identification is based on presumptive evidence.

File extensions may have been used on the data analysis sheets and indicates as follows: a-File was requantified b-File was quantified by a second column and detector r1-File was requantified for the purpose of reissue

Definition of Data Qualifying Flags

Page 4 of 24

MODIFIED EPA METHOD TO-15 GC/MS SIM/FULL SCANSummary of Detected Compounds

Client Sample ID: DEEP POSTCARBON-111109

Lab ID#: 0911256A-03A

(ug/m3)(ug/m3)(ppbv)(ppbv)CompoundAmountRpt. LimitAmountRpt. Limit

0.25 1.3 1.1 5.8m,p-Xylene0.25 0.54 1.1 2.4o-Xylene0.25 0.43 0.51 0.89Chloromethane1.2 19 2.3 36Ethanol1.2 4.6 2.9 11Acetone1.2 3.3 3.0 8.12-Propanol

0.25 0.53 0.73 1.62-Butanone (Methyl Ethyl Ketone)0.25 0.62 1.2 3.04-Ethyltoluene0.25 0.25 1.2 1.21,3,5-Trimethylbenzene0.25 0.86 J 1.2 4.2 J1,2,4-Trimethylbenzene


Lab ID#: 0911256A-03B


0.050 1.3 0.19 5.0Toluene0.050 0.38 0.34 2.6Tetrachloroethene0.050 0.43 0.22 1.8Ethyl Benzene

Client Sample ID: SHALLOW POSTCARBON-111109

Lab ID#: 0911256A-06A


0.29 3.9 1.3 17m,p-Xylene0.29 1.3 1.3 5.7o-Xylene1.5 7.6 2.8 14Ethanol1.5 4.7 3.5 11Acetone1.5 3.1 3.6 7.62-Propanol

0.29 1.0 1.4 5.04-Ethyltoluene0.29 0.42 1.4 2.11,3,5-Trimethylbenzene0.29 1.5 J 1.4 7.3 J1,2,4-Trimethylbenzene


Lab ID#: 0911256A-06B

Page 5 of 24



Lab ID#: 0911256A-06B



Client Sample ID: VCP POSTCARBON-111109

Lab ID#: 0911256A-07A


0.27 3.9 1.2 17m,p-Xylene0.27 0.92 1.2 4.0o-Xylene0.27 0.82 1.3 4.0Freon 120.27 0.39 0.56 0.80Chloromethane1.4 14 2.6 27Ethanol1.4 3.4 3.2 8.0Acetone1.4 3.3 3.3 8.12-Propanol

0.27 0.72 1.3 3.54-Ethyltoluene0.27 0.82 J 1.3 4.0 J1,2,4-Trimethylbenzene


Lab ID#: 0911256A-07B


0.027 0.75 0.070 1.9Vinyl Chloride0.054 0.11 0.30 0.581,1,1-Trichloroethane0.14 0.19 0.43 0.60Benzene0.054 0.056 0.29 0.30Trichloroethene0.054 1.8 0.20 6.8Toluene0.054 0.090 0.37 0.61Tetrachloroethene0.054 1.1 0.24 4.7Ethyl Benzene

Page 6 of 24


Lab ID#: 0911256A-03A

MODIFIED EPA METHOD TO-15 GC/MS SIM/FULL SCAN

z112011File Name:Dil. Factor: 2.48

Date of Collection: 11/11/09 10:39:00 AMDate of Analysis: 11/20/09 05:44 PM


0.25 1.3 1.1 5.8m,p-Xylene0.25 0.54 1.1 2.4o-Xylene0.25 Not Detected 1.2 Not DetectedFreon 120.25 Not Detected 1.7 Not DetectedFreon 1140.25 0.43 0.51 0.89Chloromethane0.25 Not Detected 0.55 Not Detected1,3-Butadiene0.25 Not Detected 0.96 Not DetectedBromomethane0.25 Not Detected 0.65 Not DetectedChloroethane0.25 Not Detected 1.4 Not DetectedFreon 111.2 19 2.3 36Ethanol

0.25 Not Detected 1.9 Not DetectedFreon 1131.2 4.6 2.9 11Acetone1.2 3.3 3.0 8.12-Propanol1.2 Not Detected 3.9 Not DetectedCarbon Disulfide1.2 Not Detected 3.9 Not Detected3-Chloropropene

0.50 Not Detected 1.7 Not DetectedMethylene Chloride0.25 Not Detected 0.87 Not DetectedHexane0.25 0.53 0.73 1.62-Butanone (Methyl Ethyl Ketone)1.2 Not Detected 3.6 Not DetectedTetrahydrofuran

0.25 Not Detected 1.2 Not DetectedChloroform0.25 Not Detected 0.85 Not DetectedCyclohexane0.25 Not Detected 1.6 Not DetectedCarbon Tetrachloride1.2 Not Detected 5.8 Not Detected2,2,4-Trimethylpentane

0.25 Not Detected 1.0 Not DetectedHeptane0.25 Not Detected 1.1 Not Detected1,2-Dichloropropane0.25 Not Detected 0.89 Not Detected1,4-Dioxane0.25 Not Detected 1.7 Not DetectedBromodichloromethane0.25 Not Detected 1.1 Not Detectedcis-1,3-Dichloropropene0.25 Not Detected 1.0 Not Detected4-Methyl-2-pentanone0.25 Not Detected 1.1 Not Detectedtrans-1,3-Dichloropropene1.2 Not Detected 5.1 Not Detected2-Hexanone

0.25 Not Detected 2.1 Not DetectedDibromochloromethane0.25 Not Detected 1.9 Not Detected1,2-Dibromoethane (EDB)0.25 Not Detected 1.1 Not DetectedChlorobenzene0.25 Not Detected 1.0 Not DetectedStyrene0.25 Not Detected 2.6 Not DetectedBromoform0.25 Not Detected 1.2 Not DetectedCumene0.25 Not Detected 1.2 Not DetectedPropylbenzene0.25 0.62 1.2 3.04-Ethyltoluene

Page 7 of 24


Lab ID#: 0911256A-03A





0.25 0.25 1.2 1.21,3,5-Trimethylbenzene0.25 0.86 J 1.2 4.2 J1,2,4-Trimethylbenzene0.25 Not Detected 1.5 Not Detected1,3-Dichlorobenzene0.25 Not Detected 1.5 Not Detected1,4-Dichlorobenzene0.25 Not Detected 1.3 Not Detectedalpha-Chlorotoluene0.25 Not Detected 1.5 Not Detected1,2-Dichlorobenzene1.2 Not Detected 9.2 Not Detected1,2,4-Trichlorobenzene1.2 Not Detected 13 Not DetectedHexachlorobutadiene

J = Estimated value due to bias in the CCV.Container Type: 6 Liter Summa Canister (SIM Certified)

Limits%RecoverySurrogatesMethod

105 70-1301,2-Dichloroethane-d493 70-130Toluene-d8114 70-1304-Bromofluorobenzene

Page 8 of 24


Lab ID#: 0911256A-03B


z112011simFile Name:Dil. Factor: 2.48



0.025 Not Detected 0.063 Not DetectedVinyl Chloride0.025 Not Detected 0.098 Not Detected1,1-Dichloroethene0.050 Not Detected 0.20 Not Detected1,1-Dichloroethane0.050 Not Detected 0.20 Not Detectedcis-1,2-Dichloroethene0.050 Not Detected 0.27 Not Detected1,1,1-Trichloroethane0.12 Not Detected 0.40 Not DetectedBenzene0.050 Not Detected 0.20 Not Detected1,2-Dichloroethane0.050 Not Detected 0.27 Not DetectedTrichloroethene0.050 1.3 0.19 5.0Toluene0.050 Not Detected 0.27 Not Detected1,1,2-Trichloroethane0.050 0.38 0.34 2.6Tetrachloroethene0.050 0.43 0.22 1.8Ethyl Benzene0.050 Not Detected 0.34 Not Detected1,1,2,2-Tetrachloroethane0.25 Not Detected 0.98 Not Detectedtrans-1,2-Dichloroethene0.25 Not Detected 0.89 Not DetectedMethyl tert-butyl ether

Container Type: 6 Liter Summa Canister (SIM Certified)



Page 9 of 24


Lab ID#: 0911256A-06A



Date of Collection: 11/11/09 2:15:00 PMDate of Analysis: 11/20/09 04:19 PM


0.29 3.9 1.3 17m,p-Xylene0.29 1.3 1.3 5.7o-Xylene0.29 Not Detected 1.4 Not DetectedFreon 120.29 Not Detected 2.0 Not DetectedFreon 1140.29 Not Detected 0.60 Not DetectedChloromethane0.29 Not Detected 0.64 Not Detected1,3-Butadiene0.29 Not Detected 1.1 Not DetectedBromomethane0.29 Not Detected 0.77 Not DetectedChloroethane0.29 Not Detected 1.6 Not DetectedFreon 111.5 7.6 2.8 14Ethanol

0.29 Not Detected 2.2 Not DetectedFreon 1131.5 4.7 3.5 11Acetone1.5 3.1 3.6 7.62-Propanol1.5 Not Detected 4.5 Not DetectedCarbon Disulfide1.5 Not Detected 4.6 Not Detected3-Chloropropene

0.58 Not Detected 2.0 Not DetectedMethylene Chloride0.29 Not Detected 1.0 Not DetectedHexane0.29 Not Detected 0.86 Not Detected2-Butanone (Methyl Ethyl Ketone)1.5 Not Detected 4.3 Not DetectedTetrahydrofuran




Page 10 of 24


Lab ID#: 0911256A-06A





0.29 0.42 1.4 2.11,3,5-Trimethylbenzene0.29 1.5 J 1.4 7.3 J1,2,4-Trimethylbenzene0.29 Not Detected 1.8 Not Detected1,3-Dichlorobenzene0.29 Not Detected 1.8 Not Detected1,4-Dichlorobenzene0.29 Not Detected 1.5 Not Detectedalpha-Chlorotoluene0.29 Not Detected 1.8 Not Detected1,2-Dichlorobenzene1.5 Not Detected 11 Not Detected1,2,4-Trichlorobenzene1.5 Not Detected 16 Not DetectedHexachlorobutadiene




Page 11 of 24


Lab ID#: 0911256A-06B





0.029 Not Detected 0.075 Not DetectedVinyl Chloride0.029 Not Detected 0.12 Not Detected1,1-Dichloroethene0.058 Not Detected 0.24 Not Detected1,1-Dichloroethane0.058 Not Detected 0.23 Not Detectedcis-1,2-Dichloroethene0.058 Not Detected 0.32 Not Detected1,1,1-Trichloroethane0.15 Not Detected 0.47 Not DetectedBenzene0.058 Not Detected 0.24 Not Detected1,2-Dichloroethane0.058 Not Detected 0.31 Not DetectedTrichloroethene0.058 1.5 0.22 5.6Toluene0.058 Not Detected 0.32 Not Detected1,1,2-Trichloroethane0.058 0.23 0.40 1.5Tetrachloroethene0.058 1.1 0.25 4.9Ethyl Benzene0.058 Not Detected 0.40 Not Detected1,1,2,2-Tetrachloroethane0.29 Not Detected 1.2 Not Detectedtrans-1,2-Dichloroethene0.29 Not Detected 1.0 Not DetectedMethyl tert-butyl ether




Page 12 of 24


Lab ID#: 0911256A-07A





0.27 3.9 1.2 17m,p-Xylene0.27 0.92 1.2 4.0o-Xylene0.27 0.82 1.3 4.0Freon 120.27 Not Detected 1.9 Not DetectedFreon 1140.27 0.39 0.56 0.80Chloromethane0.27 Not Detected 0.60 Not Detected1,3-Butadiene0.27 Not Detected 1.0 Not DetectedBromomethane0.27 Not Detected 0.72 Not DetectedChloroethane0.27 Not Detected 1.5 Not DetectedFreon 111.4 14 2.6 27Ethanol

0.27 Not Detected 2.1 Not DetectedFreon 1131.4 3.4 3.2 8.0Acetone1.4 3.3 3.3 8.12-Propanol1.4 Not Detected 4.2 Not DetectedCarbon Disulfide1.4 Not Detected 4.2 Not Detected3-Chloropropene

0.54 Not Detected 1.9 Not DetectedMethylene Chloride0.27 Not Detected 0.96 Not DetectedHexane0.27 Not Detected 0.80 Not Detected2-Butanone (Methyl Ethyl Ketone)1.4 Not Detected 4.0 Not DetectedTetrahydrofuran




Page 13 of 24


Lab ID#: 0911256A-07A





0.27 Not Detected 1.3 Not Detected1,3,5-Trimethylbenzene0.27 0.82 J 1.3 4.0 J1,2,4-Trimethylbenzene0.27 Not Detected 1.6 Not Detected1,3-Dichlorobenzene0.27 Not Detected 1.6 Not Detected1,4-Dichlorobenzene0.27 Not Detected 1.4 Not Detectedalpha-Chlorotoluene0.27 Not Detected 1.6 Not Detected1,2-Dichlorobenzene1.4 Not Detected 10 Not Detected1,2,4-Trichlorobenzene1.4 Not Detected 14 Not DetectedHexachlorobutadiene




Page 14 of 24


Lab ID#: 0911256A-07B





0.027 0.75 0.070 1.9Vinyl Chloride0.027 Not Detected 0.11 Not Detected1,1-Dichloroethene0.054 Not Detected 0.22 Not Detected1,1-Dichloroethane0.054 Not Detected 0.22 Not Detectedcis-1,2-Dichloroethene0.054 0.11 0.30 0.581,1,1-Trichloroethane0.14 0.19 0.43 0.60Benzene0.054 Not Detected 0.22 Not Detected1,2-Dichloroethane0.054 0.056 0.29 0.30Trichloroethene0.054 1.8 0.20 6.8Toluene0.054 Not Detected 0.30 Not Detected1,1,2-Trichloroethane0.054 0.090 0.37 0.61Tetrachloroethene0.054 1.1 0.24 4.7Ethyl Benzene0.054 Not Detected 0.37 Not Detected1,1,2,2-Tetrachloroethane0.27 Not Detected 1.1 Not Detectedtrans-1,2-Dichloroethene0.27 Not Detected 0.98 Not DetectedMethyl tert-butyl ether




Page 15 of 24

Client Sample ID: Lab Blank

Lab ID#: 0911256A-08A



Date of Collection: NA Date of Analysis: 11/20/09 02:35 PM


0.10 Not Detected 0.43 Not Detectedm,p-Xylene0.10 Not Detected 0.43 Not Detectedo-Xylene0.10 Not Detected 0.49 Not DetectedFreon 120.10 Not Detected 0.70 Not DetectedFreon 1140.10 Not Detected 0.21 Not DetectedChloromethane0.10 Not Detected 0.22 Not Detected1,3-Butadiene0.10 Not Detected 0.39 Not DetectedBromomethane0.10 Not Detected 0.26 Not DetectedChloroethane0.10 Not Detected 0.56 Not DetectedFreon 110.50 Not Detected 0.94 Not DetectedEthanol0.10 Not Detected 0.77 Not DetectedFreon 1130.50 Not Detected 1.2 Not DetectedAcetone0.50 Not Detected 1.2 Not Detected2-Propanol0.50 Not Detected 1.6 Not DetectedCarbon Disulfide0.50 Not Detected 1.6 Not Detected3-Chloropropene0.20 Not Detected 0.69 Not DetectedMethylene Chloride0.10 Not Detected 0.35 Not DetectedHexane0.10 Not Detected 0.29 Not Detected2-Butanone (Methyl Ethyl Ketone)0.50 Not Detected 1.5 Not DetectedTetrahydrofuran0.10 Not Detected 0.49 Not DetectedChloroform0.10 Not Detected 0.34 Not DetectedCyclohexane0.10 Not Detected 0.63 Not DetectedCarbon Tetrachloride0.50 Not Detected 2.3 Not Detected2,2,4-Trimethylpentane0.10 Not Detected 0.41 Not DetectedHeptane0.10 Not Detected 0.46 Not Detected1,2-Dichloropropane0.10 Not Detected 0.36 Not Detected1,4-Dioxane0.10 Not Detected 0.67 Not DetectedBromodichloromethane0.10 Not Detected 0.45 Not Detectedcis-1,3-Dichloropropene0.10 Not Detected 0.41 Not Detected4-Methyl-2-pentanone0.10 Not Detected 0.45 Not Detectedtrans-1,3-Dichloropropene0.50 Not Detected 2.0 Not Detected2-Hexanone0.10 Not Detected 0.85 Not DetectedDibromochloromethane0.10 Not Detected 0.77 Not Detected1,2-Dibromoethane (EDB)0.10 Not Detected 0.46 Not DetectedChlorobenzene0.10 Not Detected 0.42 Not DetectedStyrene0.10 Not Detected 1.0 Not DetectedBromoform0.10 Not Detected 0.49 Not DetectedCumene0.10 Not Detected 0.49 Not DetectedPropylbenzene0.10 Not Detected 0.49 Not Detected4-Ethyltoluene

Page 16 of 24


Lab ID#: 0911256A-08A





0.10 Not Detected 0.49 Not Detected1,3,5-Trimethylbenzene0.10 Not Detected 0.49 Not Detected1,2,4-Trimethylbenzene0.10 Not Detected 0.60 Not Detected1,3-Dichlorobenzene0.10 Not Detected 0.60 Not Detected1,4-Dichlorobenzene0.10 Not Detected 0.52 Not Detectedalpha-Chlorotoluene0.10 Not Detected 0.60 Not Detected1,2-Dichlorobenzene0.50 Not Detected 3.7 Not Detected1,2,4-Trichlorobenzene0.50 Not Detected 5.3 Not DetectedHexachlorobutadiene

Container Type: NA - Not Applicable



Page 17 of 24


Lab ID#: 0911256A-08B





0.010 Not Detected 0.026 Not DetectedVinyl Chloride0.010 Not Detected 0.040 Not Detected1,1-Dichloroethene0.020 Not Detected 0.081 Not Detected1,1-Dichloroethane0.020 Not Detected 0.079 Not Detectedcis-1,2-Dichloroethene0.020 Not Detected 0.11 Not Detected1,1,1-Trichloroethane0.050 Not Detected 0.16 Not DetectedBenzene0.020 Not Detected 0.081 Not Detected1,2-Dichloroethane0.020 Not Detected 0.11 Not DetectedTrichloroethene0.020 Not Detected 0.075 Not DetectedToluene0.020 Not Detected 0.11 Not Detected1,1,2-Trichloroethane0.020 Not Detected 0.14 Not DetectedTetrachloroethene0.020 Not Detected 0.087 Not DetectedEthyl Benzene0.020 Not Detected 0.14 Not Detected1,1,2,2-Tetrachloroethane0.10 Not Detected 0.40 Not Detectedtrans-1,2-Dichloroethene0.10 Not Detected 0.36 Not DetectedMethyl tert-butyl ether




Page 18 of 24

Client Sample ID: CCV

Lab ID#: 0911256A-09A



Date of Collection: NA Date of Analysis: 11/20/09 10:11 AM

%RecoveryCompound

120m,p-Xylene118o-Xylene101Freon 1298Freon 114106Chloromethane1011,3-Butadiene94Bromomethane102Chloroethane106Freon 1197Ethanol91Freon 113109Acetone1042-Propanol104Carbon Disulfide1093-Chloropropene95Methylene Chloride114Hexane1232-Butanone (Methyl Ethyl Ketone)112Tetrahydrofuran106Chloroform113Cyclohexane123Carbon Tetrachloride1102,2,4-Trimethylpentane122Heptane1051,2-Dichloropropane1141,4-Dioxane116Bromodichloromethane124cis-1,3-Dichloropropene

132 Q4-Methyl-2-pentanone116trans-1,3-Dichloropropene1172-Hexanone118Dibromochloromethane1121,2-Dibromoethane (EDB)101Chlorobenzene119Styrene126Bromoform123Cumene121Propylbenzene1234-Ethyltoluene

Page 19 of 24


Lab ID#: 0911256A-09A




%RecoveryCompound

1221,3,5-Trimethylbenzene134 Q1,2,4-Trimethylbenzene1161,3-Dichlorobenzene1211,4-Dichlorobenzene

138 Qalpha-Chlorotoluene1211,2-Dichlorobenzene1181,2,4-Trichlorobenzene122Hexachlorobutadiene

Q = Exceeds Quality Control limits.Container Type: NA - Not Applicable



Page 20 of 24


Lab ID#: 0911256A-09B




%RecoveryCompound

101Vinyl Chloride1041,1-Dichloroethene1071,1-Dichloroethane112cis-1,2-Dichloroethene1111,1,1-Trichloroethane103Benzene1191,2-Dichloroethane101Trichloroethene109Toluene1071,1,2-Trichloroethane103Tetrachloroethene118Ethyl Benzene1041,1,2,2-Tetrachloroethane111trans-1,2-Dichloroethene

142 QMethyl tert-butyl ether




Page 21 of 24

Client Sample ID: LCS

Lab ID#: 0911256A-10A




%RecoveryCompound

119m,p-Xylene118o-Xylene96Freon 1294Freon 11492Chloromethane1021,3-Butadiene92Bromomethane99Chloroethane98Freon 11119Ethanol82Freon 11384Acetone962-Propanol99Carbon Disulfide1063-Chloropropene84Methylene Chloride109Hexane1152-Butanone (Methyl Ethyl Ketone)104Tetrahydrofuran99Chloroform111Cyclohexane123Carbon Tetrachloride1072,2,4-Trimethylpentane114Heptane1031,2-Dichloropropane1031,4-Dioxane108Bromodichloromethane118cis-1,3-Dichloropropene1244-Methyl-2-pentanone118trans-1,3-Dichloropropene1192-Hexanone116Dibromochloromethane1151,2-Dibromoethane (EDB)100Chlorobenzene119Styrene122Bromoform118Cumene118Propylbenzene1224-Ethyltoluene

Page 22 of 24


Lab ID#: 0911256A-10A




%RecoveryCompound

1191,3,5-Trimethylbenzene1301,2,4-Trimethylbenzene1141,3-Dichlorobenzene1191,4-Dichlorobenzene129alpha-Chlorotoluene1191,2-Dichlorobenzene1121,2,4-Trichlorobenzene107Hexachlorobutadiene




Page 23 of 24


Lab ID#: 0911256A-10B




%RecoveryCompound

104Vinyl Chloride911,1-Dichloroethene991,1-Dichloroethane108cis-1,2-Dichloroethene1061,1,1-Trichloroethane96Benzene1071,2-Dichloroethane96Trichloroethene98Toluene1081,1,2-Trichloroethane104Tetrachloroethene120Ethyl Benzene1031,1,2,2-Tetrachloroethane107trans-1,2-Dichloroethene140Methyl tert-butyl ether




Page 24 of 24

12/2/2009Mr. John FoxwellAsh Creek Associates9615 SW Allen BoulevardSuite 106Beaverton OR 97005

Project Name: TARRSVE IRAMProject #: 1073-06





Regards,


Workorder #: 0911256B




WORK ORDER #: 0911256B

CLIENT: BILL TO:

PHONE:


503-924-4704x113

503-924-470711/12/2009

DATE COMPLETED: 12/02/2009

P.O. #

PROJECT # 1073-06 TARRSVE IRAM

Work Order Summary

FAX:

DATE RECEIVED:CONTACT: Kelly Buettner


PRESSUREFINAL

01A DEEP PRECARBON-111109 Modified TO-15 1.5 "Hg 5 psi02A DEEP MIDCARBON-111109 Modified TO-15 5.0 "Hg 5 psi02B DEEP MIDCARBON-111109 Modified TO-15 5.0 "Hg 5 psi04A SHALLOW PRECARBON-111109 Modified TO-15 3.0 "Hg 5 psi05A SHALLOW MIDCARBON-111109 Modified TO-15 2.5 "Hg 5 psi05B SHALLOW MIDCARBON-111109 Modified TO-15 2.5 "Hg 5 psi06A Lab Blank Modified TO-15 NA NA06B Lab Blank Modified TO-15 NA NA06C Lab Blank Modified TO-15 NA NA07A CCV Modified TO-15 NA NA07B CCV Modified TO-15 NA NA07C CCV Modified TO-15 NA NA08A LCS Modified TO-15 NA NA08B LCS Modified TO-15 NA NA08C LCS Modified TO-15 NA NA

CERTIFIED BY:

Laboratory Director

DATE:



12/02/09

Page 2 of 31





Ash Creek AssociatesWorkorder# 0911256B


Four 6 Liter Summa Canister (SIM Certified) samples were received on November 12, 2009. The laboratory performed analysis via modified EPA Method TO-15 using GC/MS in the Full Scan and SIM acquisition modes. The method involves concentrating up to 1.0 liters of air. The concentrated aliquot is then flash vaporized and swept through a water management system to remove water vapor. Following dehumidification, the sample passes directly into the GC/MS for analysis.

This workorder was independently validated prior to submittal using 'USEPA National Functional Guidelines' as generally applied to the analysis of volatile organic compounds in air. A rules-based,logic driven, independent validation engine was employed to assess completeness, evaluate pass/fail of relevant project quality control requirements and verification of all quantified amounts.

Method modifications taken to run these samples are summarized in the table below. Specific project requirements may over-ride the ATL modifications.










Receiving Notes

The Chain of Custody (COC) information for sample SHALLOW MIDCARBON-111109 did not match the information on the canister with regard to canister identification. The client was notified of the discrepancy and the information on the canister was used to process and report the sample.

The results for each sample in this report were acquired from two separate data files originating from the same analytical run. The two data files have the same base file name and are differentiated with a

Analytical Notes

Page 3 of 31


"sim" extension on the SIM data file.

All Quality Control Limit exceedences and affected sample results are noted by flags. Each flag is defined at the bottom of this Case Narrative and on each Sample Result Summary page. Target compound non-detects in the samples that are associated with high bias in QC analyses have not been flagged.

Dilution was performed on samples DEEP MIDCARBON-111109 and SHALLOWMIDCARBON-111109 due to the presence of high level non-target species.

Eight qualifiers may have been used on the data analysis sheets and indicates as follows: B - Compound present in laboratory blank greater than reporting limit (background subtractionnot performed). J - Estimated value. E - Exceeds instrument calibration range. S - Saturated peak. Q - Exceeds quality control limits. U - Compound analyzed for but not detected above the reporting limit. UJ- Non-detected compound associated with low bias in the CCV N - The identification is based on presumptive evidence.



Page 4 of 31

MODIFIED EPA METHOD TO-15 GC/MSSummary of Detected Compounds

Client Sample ID: DEEP PRECARBON-111109

Lab ID#: 0911256B-01A


700 860 2800 34001,1-Dichloroethene700 2600 2500 9100Hexane700 18000 2800 72000cis-1,2-Dichloroethene700 3000 3800 160001,1,1-Trichloroethane700 2400 2400 8100Cyclohexane700 860 3300 40002,2,4-Trimethylpentane700 4200 2900 17000Heptane700 46000 3800 250000Trichloroethene700 3000 2600 12000Toluene700 360000 4800 2500000Tetrachloroethene

Client Sample ID: DEEP MIDCARBON-111109

Lab ID#: 0911256B-02A


0.32 1.5 1.4 6.6m,p-Xylene0.32 0.56 1.4 2.4o-Xylene0.32 0.78 1.6 3.9Freon 120.32 0.38 0.66 0.78Chloromethane1.6 25 3.0 48Ethanol1.6 3.3 3.8 8.0Acetone1.6 4.5 4.0 112-Propanol

0.64 1.3 2.2 4.5Methylene Chloride0.32 0.74 1.6 3.64-Ethyltoluene0.32 1.0 J 1.6 5.2 J1,2,4-Trimethylbenzene


Lab ID#: 0911256B-02B


0.032 61 0.082 160Vinyl Chloride0.064 1.5 0.24 5.5Toluene0.064 0.19 0.44 1.3Tetrachloroethene0.064 0.52 0.28 2.3Ethyl Benzene

Page 5 of 31


Client Sample ID: SHALLOW PRECARBON-111109

Lab ID#: 0911256B-04A


53 930 210 3700cis-1,2-Dichloroethene53 730 160 2200Tetrahydrofuran53 91 290 5001,1,1-Trichloroethane53 91 220 370Heptane53 1400 280 7700Trichloroethene53 2700 200 10000Toluene53 25000 360 170000Tetrachloroethene53 190 230 820Ethyl Benzene53 570 230 2500m,p-Xylene53 190 230 820o-Xylene

Client Sample ID: SHALLOW MIDCARBON-111109

Lab ID#: 0911256B-05A


0.29 1.8 1.3 8.0m,p-Xylene0.29 0.73 1.3 3.2o-Xylene1.5 7.0 2.8 13Ethanol1.5 10 3.5 24Acetone1.5 2.7 3.6 6.62-Propanol

0.29 1.4 0.86 4.22-Butanone (Methyl Ethyl Ketone)0.29 0.81 1.4 4.04-Ethyltoluene0.29 0.37 1.4 1.81,3,5-Trimethylbenzene0.29 1.3 J 1.4 6.6 J1,2,4-Trimethylbenzene


Lab ID#: 0911256B-05B



Page 6 of 31

Client Sample ID: DEEP PRECARBON-111109Lab ID#: 0911256B-01A

MODIFIED EPA METHOD TO-15 GC/MS

b112211File Name:Dil. Factor: 141

Date of Collection: 11/11/09 10:28:00 ADate of Analysis: 11/22/09 11:58 AM


700 Not Detected 3500 Not DetectedFreon 12700 Not Detected 4900 Not DetectedFreon 114

2800 Not Detected 5800 Not DetectedChloromethane700 Not Detected 1800 Not DetectedVinyl Chloride700 Not Detected 1600 Not Detected1,3-Butadiene700 Not Detected 2700 Not DetectedBromomethane700 Not Detected 1900 Not DetectedChloroethane700 Not Detected 4000 Not DetectedFreon 11

2800 Not Detected 5300 Not DetectedEthanol700 Not Detected 5400 Not DetectedFreon 113700 860 2800 34001,1-Dichloroethene

2800 Not Detected 6700 Not DetectedAcetone2800 Not Detected 6900 Not Detected2-Propanol700 Not Detected 2200 Not DetectedCarbon Disulfide

2800 Not Detected 8800 Not Detected3-Chloropropene700 Not Detected 2400 Not DetectedMethylene Chloride700 Not Detected 2500 Not DetectedMethyl tert-butyl ether700 Not Detected 2800 Not Detectedtrans-1,2-Dichloroethene700 2600 2500 9100Hexane700 Not Detected 2800 Not Detected1,1-Dichloroethane700 Not Detected 2100 Not Detected2-Butanone (Methyl Ethyl Ketone)700 18000 2800 72000cis-1,2-Dichloroethene700 Not Detected 2100 Not DetectedTetrahydrofuran700 Not Detected 3400 Not DetectedChloroform700 3000 3800 160001,1,1-Trichloroethane700 2400 2400 8100Cyclohexane700 Not Detected 4400 Not DetectedCarbon Tetrachloride700 860 3300 40002,2,4-Trimethylpentane700 Not Detected 2200 Not DetectedBenzene700 Not Detected 2800 Not Detected1,2-Dichloroethane700 4200 2900 17000Heptane700 46000 3800 250000Trichloroethene700 Not Detected 3200 Not Detected1,2-Dichloropropane

2800 Not Detected 10000 Not Detected1,4-Dioxane700 Not Detected 4700 Not DetectedBromodichloromethane700 Not Detected 3200 Not Detectedcis-1,3-Dichloropropene700 Not Detected 2900 Not Detected4-Methyl-2-pentanone700 3000 2600 12000Toluene700 Not Detected 3200 Not Detectedtrans-1,3-Dichloropropene

Page 7 of 31

Client Sample ID: DEEP PRECARBON-111109Lab ID#: 0911256B-01A


b112211File Name:Dil. Factor: 141

Date of Collection: 11/11/09 10:28:00 ADate of Analysis: 11/22/09 11:58 AM


700 Not Detected 3800 Not Detected1,1,2-Trichloroethane700 360000 4800 2500000Tetrachloroethene

2800 Not Detected 12000 Not Detected2-Hexanone700 Not Detected 6000 Not DetectedDibromochloromethane700 Not Detected 5400 Not Detected1,2-Dibromoethane (EDB)700 Not Detected 3200 Not DetectedChlorobenzene700 Not Detected 3100 Not DetectedEthyl Benzene700 Not Detected 3100 Not Detectedm,p-Xylene700 Not Detected 3100 Not Detectedo-Xylene700 Not Detected 3000 Not DetectedStyrene700 Not Detected 7300 Not DetectedBromoform700 Not Detected 3500 Not DetectedCumene700 Not Detected 4800 Not Detected1,1,2,2-Tetrachloroethane700 Not Detected 3500 Not DetectedPropylbenzene700 Not Detected 3500 Not Detected4-Ethyltoluene700 Not Detected 3500 Not Detected1,3,5-Trimethylbenzene700 Not Detected 3500 Not Detected1,2,4-Trimethylbenzene700 Not Detected 4200 Not Detected1,3-Dichlorobenzene700 Not Detected 4200 Not Detected1,4-Dichlorobenzene700 Not Detected 3600 Not Detectedalpha-Chlorotoluene700 Not Detected 4200 Not Detected1,2-Dichlorobenzene

2800 Not Detected 21000 Not Detected1,2,4-Trichlorobenzene2800 Not Detected 30000 Not DetectedHexachlorobutadiene



96 70-1301,2-Dichloroethane-d499 70-130Toluene-d8

100 70-1304-Bromofluorobenzene

Page 8 of 31

Client Sample ID: DEEP MIDCARBON-111109Lab ID#: 0911256B-02A



Date of Collection: 11/11/09 10:35:00 ADate of Analysis: 11/20/09 06:39 PM


0.32 1.5 1.4 6.6m,p-Xylene0.32 0.56 1.4 2.4o-Xylene0.32 0.78 1.6 3.9Freon 120.32 Not Detected 2.2 Not DetectedFreon 1140.32 0.38 0.66 0.78Chloromethane0.32 Not Detected 0.71 Not Detected1,3-Butadiene0.32 Not Detected 1.2 Not DetectedBromomethane0.32 Not Detected 0.85 Not DetectedChloroethane0.32 Not Detected 1.8 Not DetectedFreon 111.6 25 3.0 48Ethanol

0.32 Not Detected 2.5 Not DetectedFreon 1131.6 3.3 3.8 8.0Acetone1.6 4.5 4.0 112-Propanol1.6 Not Detected 5.0 Not DetectedCarbon Disulfide1.6 Not Detected 5.0 Not Detected3-Chloropropene

0.64 1.3 2.2 4.5Methylene Chloride0.32 Not Detected 1.1 Not DetectedHexane0.32 Not Detected 0.95 Not Detected2-Butanone (Methyl Ethyl Ketone)1.6 Not Detected 4.7 Not DetectedTetrahydrofuran




Page 9 of 31

Client Sample ID: DEEP MIDCARBON-111109Lab ID#: 0911256B-02A





0.32 Not Detected 1.6 Not Detected1,3,5-Trimethylbenzene0.32 1.0 J 1.6 5.2 J1,2,4-Trimethylbenzene0.32 Not Detected 1.9 Not Detected1,3-Dichlorobenzene0.32 Not Detected 1.9 Not Detected1,4-Dichlorobenzene0.32 Not Detected 1.7 Not Detectedalpha-Chlorotoluene0.32 Not Detected 1.9 Not Detected1,2-Dichlorobenzene1.6 Not Detected 12 Not Detected1,2,4-Trichlorobenzene1.6 Not Detected 17 Not DetectedHexachlorobutadiene





Page 10 of 31

Client Sample ID: DEEP MIDCARBON-111109Lab ID#: 0911256B-02B





0.032 61 0.082 160Vinyl Chloride0.032 Not Detected 0.13 Not Detected1,1-Dichloroethene0.064 Not Detected 0.26 Not Detected1,1-Dichloroethane0.064 Not Detected 0.26 Not Detectedcis-1,2-Dichloroethene0.064 Not Detected 0.35 Not Detected1,1,1-Trichloroethane0.16 Not Detected 0.51 Not DetectedBenzene

0.064 Not Detected 0.26 Not Detected1,2-Dichloroethane0.064 Not Detected 0.35 Not DetectedTrichloroethene0.064 1.5 0.24 5.5Toluene0.064 Not Detected 0.35 Not Detected1,1,2-Trichloroethane0.064 0.19 0.44 1.3Tetrachloroethene0.064 0.52 0.28 2.3Ethyl Benzene0.064 Not Detected 0.44 Not Detected1,1,2,2-Tetrachloroethane0.32 Not Detected 1.3 Not Detectedtrans-1,2-Dichloroethene0.32 Not Detected 1.2 Not DetectedMethyl tert-butyl ether




Page 11 of 31

Client Sample ID: SHALLOW PRECARBON-111109Lab ID#: 0911256B-04A


b112212File Name:Dil. Factor: 10.6




210 Not Detected 440 Not DetectedChloromethane53 Not Detected 140 Not DetectedVinyl Chloride53 Not Detected 120 Not Detected1,3-Butadiene53 Not Detected 200 Not DetectedBromomethane53 Not Detected 140 Not DetectedChloroethane53 Not Detected 300 Not DetectedFreon 11

210 Not Detected 400 Not DetectedEthanol53 Not Detected 410 Not DetectedFreon 11353 Not Detected 210 Not Detected1,1-Dichloroethene


210 Not Detected 660 Not Detected3-Chloropropene53 Not Detected 180 Not DetectedMethylene Chloride53 Not Detected 190 Not DetectedMethyl tert-butyl ether53 Not Detected 210 Not Detectedtrans-1,2-Dichloroethene53 Not Detected 190 Not DetectedHexane53 Not Detected 210 Not Detected1,1-Dichloroethane53 Not Detected 160 Not Detected2-Butanone (Methyl Ethyl Ketone)53 930 210 3700cis-1,2-Dichloroethene53 730 160 2200Tetrahydrofuran53 Not Detected 260 Not DetectedChloroform53 91 290 5001,1,1-Trichloroethane53 Not Detected 180 Not DetectedCyclohexane53 Not Detected 330 Not DetectedCarbon Tetrachloride53 Not Detected 250 Not Detected2,2,4-Trimethylpentane53 Not Detected 170 Not DetectedBenzene53 Not Detected 210 Not Detected1,2-Dichloroethane53 91 220 370Heptane53 1400 280 7700Trichloroethene53 Not Detected 240 Not Detected1,2-Dichloropropane


Page 12 of 31

Client Sample ID: SHALLOW PRECARBON-111109Lab ID#: 0911256B-04A






210 Not Detected 870 Not Detected2-Hexanone53 Not Detected 450 Not DetectedDibromochloromethane53 Not Detected 410 Not Detected1,2-Dibromoethane (EDB)53 Not Detected 240 Not DetectedChlorobenzene53 190 230 820Ethyl Benzene53 570 230 2500m,p-Xylene53 190 230 820o-Xylene53 Not Detected 220 Not DetectedStyrene53 Not Detected 550 Not DetectedBromoform53 Not Detected 260 Not DetectedCumene53 Not Detected 360 Not Detected1,1,2,2-Tetrachloroethane53 Not Detected 260 Not DetectedPropylbenzene53 Not Detected 260 Not Detected4-Ethyltoluene53 Not Detected 260 Not Detected1,3,5-Trimethylbenzene53 Not Detected 260 Not Detected1,2,4-Trimethylbenzene53 Not Detected 320 Not Detected1,3-Dichlorobenzene53 Not Detected 320 Not Detected1,4-Dichlorobenzene53 Not Detected 270 Not Detectedalpha-Chlorotoluene53 Not Detected 320 Not Detected1,2-Dichlorobenzene






Page 13 of 31

Client Sample ID: SHALLOW MIDCARBON-111109Lab ID#: 0911256B-05A





0.29 1.8 1.3 8.0m,p-Xylene0.29 0.73 1.3 3.2o-Xylene0.29 Not Detected 1.4 Not DetectedFreon 120.29 Not Detected 2.0 Not DetectedFreon 1140.29 Not Detected 0.60 Not DetectedChloromethane0.29 Not Detected 0.64 Not Detected1,3-Butadiene0.29 Not Detected 1.1 Not DetectedBromomethane0.29 Not Detected 0.77 Not DetectedChloroethane0.29 Not Detected 1.6 Not DetectedFreon 111.5 7.0 2.8 13Ethanol

0.29 Not Detected 2.2 Not DetectedFreon 1131.5 10 3.5 24Acetone1.5 2.7 3.6 6.62-Propanol1.5 Not Detected 4.5 Not DetectedCarbon Disulfide1.5 Not Detected 4.6 Not Detected3-Chloropropene

0.58 Not Detected 2.0 Not DetectedMethylene Chloride0.29 Not Detected 1.0 Not DetectedHexane0.29 1.4 0.86 4.22-Butanone (Methyl Ethyl Ketone)1.5 Not Detected 4.3 Not DetectedTetrahydrofuran




Page 14 of 31

Client Sample ID: SHALLOW MIDCARBON-111109Lab ID#: 0911256B-05A





0.29 0.37 1.4 1.81,3,5-Trimethylbenzene0.29 1.3 J 1.4 6.6 J1,2,4-Trimethylbenzene0.29 Not Detected 1.8 Not Detected1,3-Dichlorobenzene0.29 Not Detected 1.8 Not Detected1,4-Dichlorobenzene0.29 Not Detected 1.5 Not Detectedalpha-Chlorotoluene0.29 Not Detected 1.8 Not Detected1,2-Dichlorobenzene1.5 Not Detected 11 Not Detected1,2,4-Trichlorobenzene1.5 Not Detected 16 Not DetectedHexachlorobutadiene





Page 15 of 31

Client Sample ID: SHALLOW MIDCARBON-111109Lab ID#: 0911256B-05B





0.029 Not Detected 0.075 Not DetectedVinyl Chloride0.029 Not Detected 0.12 Not Detected1,1-Dichloroethene0.058 Not Detected 0.24 Not Detected1,1-Dichloroethane0.058 Not Detected 0.23 Not Detectedcis-1,2-Dichloroethene0.058 Not Detected 0.32 Not Detected1,1,1-Trichloroethane0.15 Not Detected 0.47 Not DetectedBenzene

0.058 Not Detected 0.24 Not Detected1,2-Dichloroethane0.058 Not Detected 0.31 Not DetectedTrichloroethene0.058 0.89 0.22 3.4Toluene0.058 Not Detected 0.32 Not Detected1,1,2-Trichloroethane0.058 0.25 0.40 1.7Tetrachloroethene0.058 0.54 0.25 2.4Ethyl Benzene0.058 Not Detected 0.40 Not Detected1,1,2,2-Tetrachloroethane0.29 Not Detected 1.2 Not Detectedtrans-1,2-Dichloroethene0.29 Not Detected 1.0 Not DetectedMethyl tert-butyl ether





Page 16 of 31

Client Sample ID: Lab BlankLab ID#: 0911256B-06A





0.10 Not Detected 0.43 Not Detectedm,p-Xylene0.10 Not Detected 0.43 Not Detectedo-Xylene0.10 Not Detected 0.49 Not DetectedFreon 120.10 Not Detected 0.70 Not DetectedFreon 1140.10 Not Detected 0.21 Not DetectedChloromethane0.10 Not Detected 0.22 Not Detected1,3-Butadiene0.10 Not Detected 0.39 Not DetectedBromomethane0.10 Not Detected 0.26 Not DetectedChloroethane0.10 Not Detected 0.56 Not DetectedFreon 110.50 Not Detected 0.94 Not DetectedEthanol0.10 Not Detected 0.77 Not DetectedFreon 1130.50 Not Detected 1.2 Not DetectedAcetone0.50 Not Detected 1.2 Not Detected2-Propanol0.50 Not Detected 1.6 Not DetectedCarbon Disulfide0.50 Not Detected 1.6 Not Detected3-Chloropropene0.20 Not Detected 0.69 Not DetectedMethylene Chloride0.10 Not Detected 0.35 Not DetectedHexane0.10 Not Detected 0.29 Not Detected2-Butanone (Methyl Ethyl Ketone)0.50 Not Detected 1.5 Not DetectedTetrahydrofuran0.10 Not Detected 0.49 Not DetectedChloroform0.10 Not Detected 0.34 Not DetectedCyclohexane0.10 Not Detected 0.63 Not DetectedCarbon Tetrachloride0.50 Not Detected 2.3 Not Detected2,2,4-Trimethylpentane0.10 Not Detected 0.41 Not DetectedHeptane0.10 Not Detected 0.46 Not Detected1,2-Dichloropropane0.10 Not Detected 0.36 Not Detected1,4-Dioxane0.10 Not Detected 0.67 Not DetectedBromodichloromethane0.10 Not Detected 0.45 Not Detectedcis-1,3-Dichloropropene0.10 Not Detected 0.41 Not Detected4-Methyl-2-pentanone0.10 Not Detected 0.45 Not Detectedtrans-1,3-Dichloropropene0.50 Not Detected 2.0 Not Detected2-Hexanone0.10 Not Detected 0.85 Not DetectedDibromochloromethane0.10 Not Detected 0.77 Not Detected1,2-Dibromoethane (EDB)0.10 Not Detected 0.46 Not DetectedChlorobenzene0.10 Not Detected 0.42 Not DetectedStyrene0.10 Not Detected 1.0 Not DetectedBromoform0.10 Not Detected 0.49 Not DetectedCumene0.10 Not Detected 0.49 Not DetectedPropylbenzene0.10 Not Detected 0.49 Not Detected4-Ethyltoluene

Page 17 of 31

Client Sample ID: Lab BlankLab ID#: 0911256B-06A





0.10 Not Detected 0.49 Not Detected1,3,5-Trimethylbenzene0.10 Not Detected 0.49 Not Detected1,2,4-Trimethylbenzene0.10 Not Detected 0.60 Not Detected1,3-Dichlorobenzene0.10 Not Detected 0.60 Not Detected1,4-Dichlorobenzene0.10 Not Detected 0.52 Not Detectedalpha-Chlorotoluene0.10 Not Detected 0.60 Not Detected1,2-Dichlorobenzene0.50 Not Detected 3.7 Not Detected1,2,4-Trichlorobenzene0.50 Not Detected 5.3 Not DetectedHexachlorobutadiene




Page 18 of 31

Client Sample ID: Lab BlankLab ID#: 0911256B-06B





0.010 Not Detected 0.026 Not DetectedVinyl Chloride0.010 Not Detected 0.040 Not Detected1,1-Dichloroethene0.020 Not Detected 0.081 Not Detected1,1-Dichloroethane0.020 Not Detected 0.079 Not Detectedcis-1,2-Dichloroethene0.020 Not Detected 0.11 Not Detected1,1,1-Trichloroethane0.050 Not Detected 0.16 Not DetectedBenzene0.020 Not Detected 0.081 Not Detected1,2-Dichloroethane0.020 Not Detected 0.11 Not DetectedTrichloroethene0.020 Not Detected 0.075 Not DetectedToluene0.020 Not Detected 0.11 Not Detected1,1,2-Trichloroethane0.020 Not Detected 0.14 Not DetectedTetrachloroethene0.020 Not Detected 0.087 Not DetectedEthyl Benzene0.020 Not Detected 0.14 Not Detected1,1,2,2-Tetrachloroethane0.10 Not Detected 0.40 Not Detectedtrans-1,2-Dichloroethene0.10 Not Detected 0.36 Not DetectedMethyl tert-butyl ether




Page 19 of 31

Client Sample ID: Lab BlankLab ID#: 0911256B-06C





5.0 Not Detected 25 Not DetectedFreon 125.0 Not Detected 35 Not DetectedFreon 11420 Not Detected 41 Not DetectedChloromethane5.0 Not Detected 13 Not DetectedVinyl Chloride5.0 Not Detected 11 Not Detected1,3-Butadiene5.0 Not Detected 19 Not DetectedBromomethane5.0 Not Detected 13 Not DetectedChloroethane5.0 Not Detected 28 Not DetectedFreon 1120 Not Detected 38 Not DetectedEthanol5.0 Not Detected 38 Not DetectedFreon 1135.0 Not Detected 20 Not Detected1,1-Dichloroethene20 Not Detected 48 Not DetectedAcetone20 Not Detected 49 Not Detected2-Propanol5.0 Not Detected 16 Not DetectedCarbon Disulfide20 Not Detected 63 Not Detected3-Chloropropene5.0 Not Detected 17 Not DetectedMethylene Chloride5.0 Not Detected 18 Not DetectedMethyl tert-butyl ether5.0 Not Detected 20 Not Detectedtrans-1,2-Dichloroethene5.0 Not Detected 18 Not DetectedHexane5.0 Not Detected 20 Not Detected1,1-Dichloroethane5.0 Not Detected 15 Not Detected2-Butanone (Methyl Ethyl Ketone)5.0 Not Detected 20 Not Detectedcis-1,2-Dichloroethene5.0 Not Detected 15 Not DetectedTetrahydrofuran5.0 Not Detected 24 Not DetectedChloroform5.0 Not Detected 27 Not Detected1,1,1-Trichloroethane5.0 Not Detected 17 Not DetectedCyclohexane5.0 Not Detected 31 Not DetectedCarbon Tetrachloride5.0 Not Detected 23 Not Detected2,2,4-Trimethylpentane5.0 Not Detected 16 Not DetectedBenzene5.0 Not Detected 20 Not Detected1,2-Dichloroethane5.0 Not Detected 20 Not DetectedHeptane5.0 Not Detected 27 Not DetectedTrichloroethene5.0 Not Detected 23 Not Detected1,2-Dichloropropane20 Not Detected 72 Not Detected1,4-Dioxane5.0 Not Detected 34 Not DetectedBromodichloromethane5.0 Not Detected 23 Not Detectedcis-1,3-Dichloropropene5.0 Not Detected 20 Not Detected4-Methyl-2-pentanone5.0 Not Detected 19 Not DetectedToluene5.0 Not Detected 23 Not Detectedtrans-1,3-Dichloropropene

Page 20 of 31

Client Sample ID: Lab BlankLab ID#: 0911256B-06C





5.0 Not Detected 27 Not Detected1,1,2-Trichloroethane5.0 Not Detected 34 Not DetectedTetrachloroethene20 Not Detected 82 Not Detected2-Hexanone5.0 Not Detected 42 Not DetectedDibromochloromethane5.0 Not Detected 38 Not Detected1,2-Dibromoethane (EDB)5.0 Not Detected 23 Not DetectedChlorobenzene5.0 Not Detected 22 Not DetectedEthyl Benzene5.0 Not Detected 22 Not Detectedm,p-Xylene5.0 Not Detected 22 Not Detectedo-Xylene5.0 Not Detected 21 Not DetectedStyrene5.0 Not Detected 52 Not DetectedBromoform5.0 Not Detected 24 Not DetectedCumene5.0 Not Detected 34 Not Detected1,1,2,2-Tetrachloroethane5.0 Not Detected 24 Not DetectedPropylbenzene5.0 Not Detected 24 Not Detected4-Ethyltoluene5.0 Not Detected 24 Not Detected1,3,5-Trimethylbenzene5.0 Not Detected 24 Not Detected1,2,4-Trimethylbenzene5.0 Not Detected 30 Not Detected1,3-Dichlorobenzene5.0 Not Detected 30 Not Detected1,4-Dichlorobenzene5.0 Not Detected 26 Not Detectedalpha-Chlorotoluene5.0 Not Detected 30 Not Detected1,2-Dichlorobenzene20 Not Detected 150 Not Detected1,2,4-Trichlorobenzene20 Not Detected 210 Not DetectedHexachlorobutadiene




Page 21 of 31

Client Sample ID: CCVLab ID#: 0911256B-07A




%RecoveryCompound

120m,p-Xylene118o-Xylene101Freon 1298Freon 114

106Chloromethane1011,3-Butadiene94Bromomethane

102Chloroethane106Freon 1197Ethanol91Freon 113

109Acetone1042-Propanol104Carbon Disulfide1093-Chloropropene95Methylene Chloride

114Hexane1232-Butanone (Methyl Ethyl Ketone)112Tetrahydrofuran106Chloroform113Cyclohexane123Carbon Tetrachloride1102,2,4-Trimethylpentane122Heptane1051,2-Dichloropropane1141,4-Dioxane116Bromodichloromethane124cis-1,3-Dichloropropene

132 Q4-Methyl-2-pentanone116trans-1,3-Dichloropropene1172-Hexanone118Dibromochloromethane1121,2-Dibromoethane (EDB)101Chlorobenzene119Styrene126Bromoform123Cumene121Propylbenzene1234-Ethyltoluene

Page 22 of 31

Client Sample ID: CCVLab ID#: 0911256B-07A




%RecoveryCompound

1221,3,5-Trimethylbenzene134 Q1,2,4-Trimethylbenzene1161,3-Dichlorobenzene1211,4-Dichlorobenzene





Page 23 of 31

Client Sample ID: CCVLab ID#: 0911256B-07B




%RecoveryCompound

101Vinyl Chloride1041,1-Dichloroethene1071,1-Dichloroethane112cis-1,2-Dichloroethene1111,1,1-Trichloroethane103Benzene1191,2-Dichloroethane101Trichloroethene109Toluene1071,1,2-Trichloroethane103Tetrachloroethene118Ethyl Benzene1041,1,2,2-Tetrachloroethane111trans-1,2-Dichloroethene

142 QMethyl tert-butyl ether




Page 24 of 31

Client Sample ID: CCVLab ID#: 0911256B-07C




%RecoveryCompound

108Freon 12113Freon 114113Chloromethane112Vinyl Chloride1061,3-Butadiene113Bromomethane118Chloroethane110Freon 11112Ethanol113Freon 1131121,1-Dichloroethene110Acetone1102-Propanol108Carbon Disulfide1123-Chloropropene108Methylene Chloride

134 QMethyl tert-butyl ether110trans-1,2-Dichloroethene111Hexane1111,1-Dichloroethane1112-Butanone (Methyl Ethyl Ketone)109cis-1,2-Dichloroethene109Tetrahydrofuran108Chloroform1091,1,1-Trichloroethane111Cyclohexane110Carbon Tetrachloride1132,2,4-Trimethylpentane112Benzene1101,2-Dichloroethane115Heptane110Trichloroethene1111,2-Dichloropropane1111,4-Dioxane110Bromodichloromethane110cis-1,3-Dichloropropene1124-Methyl-2-pentanone113Toluene108trans-1,3-Dichloropropene

Page 25 of 31

Client Sample ID: CCVLab ID#: 0911256B-07C




%RecoveryCompound

1131,1,2-Trichloroethane117Tetrachloroethene1122-Hexanone115Dibromochloromethane1111,2-Dibromoethane (EDB)111Chlorobenzene113Ethyl Benzene112m,p-Xylene114o-Xylene118Styrene122Bromoform112Cumene1141,1,2,2-Tetrachloroethane111Propylbenzene1114-Ethyltoluene1091,3,5-Trimethylbenzene1201,2,4-Trimethylbenzene1101,3-Dichlorobenzene1141,4-Dichlorobenzene117alpha-Chlorotoluene1131,2-Dichlorobenzene1051,2,4-Trichlorobenzene105Hexachlorobutadiene




Page 26 of 31

Client Sample ID: LCSLab ID#: 0911256B-08A




%RecoveryCompound

119m,p-Xylene118o-Xylene96Freon 1294Freon 11492Chloromethane

1021,3-Butadiene92Bromomethane99Chloroethane98Freon 11

119Ethanol82Freon 11384Acetone962-Propanol99Carbon Disulfide

1063-Chloropropene84Methylene Chloride

109Hexane1152-Butanone (Methyl Ethyl Ketone)104Tetrahydrofuran99Chloroform

111Cyclohexane123Carbon Tetrachloride1072,2,4-Trimethylpentane114Heptane1031,2-Dichloropropane1031,4-Dioxane108Bromodichloromethane118cis-1,3-Dichloropropene1244-Methyl-2-pentanone118trans-1,3-Dichloropropene1192-Hexanone116Dibromochloromethane1151,2-Dibromoethane (EDB)100Chlorobenzene119Styrene122Bromoform118Cumene118Propylbenzene1224-Ethyltoluene

Page 27 of 31

Client Sample ID: LCSLab ID#: 0911256B-08A




%RecoveryCompound

1191,3,5-Trimethylbenzene1301,2,4-Trimethylbenzene1141,3-Dichlorobenzene1191,4-Dichlorobenzene129alpha-Chlorotoluene1191,2-Dichlorobenzene1121,2,4-Trichlorobenzene107Hexachlorobutadiene




Page 28 of 31

Client Sample ID: LCSLab ID#: 0911256B-08B




%RecoveryCompound

104Vinyl Chloride911,1-Dichloroethene991,1-Dichloroethane

108cis-1,2-Dichloroethene1061,1,1-Trichloroethane96Benzene

1071,2-Dichloroethane96Trichloroethene98Toluene

1081,1,2-Trichloroethane104Tetrachloroethene120Ethyl Benzene1031,1,2,2-Tetrachloroethane107trans-1,2-Dichloroethene140Methyl tert-butyl ether




Page 29 of 31

Client Sample ID: LCSLab ID#: 0911256B-08C




%RecoveryCompound

85Freon 1286Freon 11486Chloromethane86Vinyl Chloride821,3-Butadiene87Bromomethane88Chloroethane83Freon 11

133Ethanol76Freon 113761,1-Dichloroethene81Acetone822-Propanol81Carbon Disulfide833-Chloropropene74Methylene Chloride

105Methyl tert-butyl ether82trans-1,2-Dichloroethene83Hexane801,1-Dichloroethane812-Butanone (Methyl Ethyl Ketone)79cis-1,2-Dichloroethene82Tetrahydrofuran80Chloroform811,1,1-Trichloroethane83Cyclohexane82Carbon Tetrachloride862,2,4-Trimethylpentane83Benzene801,2-Dichloroethane85Heptane82Trichloroethene831,2-Dichloropropane841,4-Dioxane80Bromodichloromethane82cis-1,3-Dichloropropene824-Methyl-2-pentanone82Toluene81trans-1,3-Dichloropropene

Page 30 of 31

Client Sample ID: LCSLab ID#: 0911256B-08C




%RecoveryCompound





Page 31 of 31

12/1/2009


Project Name: Tarr IRAM SVEProject #: 1073-06





Regards,







CLIENT: BILL TO:

PHONE:


503-924-4704x113

503-924-4707

11/20/2009DATE COMPLETED: 12/01/2009

P.O. #

PROJECT # 1073-06 Tarr IRAM SVE

Work Order Summary

FAX:



PRESSUREFINAL

03A DEEP-POSTCARBON-111909 Modified TO-15 2.5 "Hg 5 psi03B DEEP-POSTCARBON-111909 Modified TO-15 2.5 "Hg 5 psi05A VCP-POSTCARBON-111909 Modified TO-15 2.5 "Hg 5 psi05B VCP-POSTCARBON-111909 Modified TO-15 2.5 "Hg 5 psi06A Lab Blank Modified TO-15 NA NA06B Lab Blank Modified TO-15 NA NA07A CCV Modified TO-15 NA NA07B CCV Modified TO-15 NA NA08A LCS Modified TO-15 NA NA08B LCS Modified TO-15 NA NA

CERTIFIED BY:

Laboratory Director

DATE:



12/01/09

Page 2 of 21







Two 6 Liter Summa Canister (SIM Certified) samples were received on November 20, 2009. Thelaboratory performed analysis via modified EPA Method TO-15 using GC/MS in the Full Scan and SIMacquisition modes. The method involves concentrating up to 1.0 liters of air. The concentrated aliquot is then flash vaporized and swept through a water management system to remove water vapor. Following dehumidification, the sample passes directly into the GC/MS for analysis.












Receiving Notes

Sample collection date was incomplete on the Chain of Custody (COC) for all samples. The sampling date was taken from the tags.

The results for each sample in this report were acquired from two separate data files originating from the

Analytical Notes

Page 3 of 21


same analytical run. The two data files have the same base file name and are differentiated with a "sim" extension on the SIM data file.




Page 4 of 21


Client Sample ID: DEEP-POSTCARBON-111909

Lab ID#: 0911465A-03A


0.15 0.26 0.72 1.3Freon 120.15 0.43 0.30 0.89Chloromethane0.15 0.18 0.57 0.70Bromomethane0.73 4.4 1.4 8.3Ethanol0.73 4.5 1.7 11Acetone0.73 1.6 1.8 4.02-Propanol0.15 0.15 0.51 0.53Hexane0.15 0.50 0.43 1.52-Butanone (Methyl Ethyl Ketone)0.15 0.19 0.50 0.66Cyclohexane0.15 0.17 0.60 0.70Heptane0.15 0.15 0.72 0.74Propylbenzene0.15 0.79 0.72 3.94-Ethyltoluene0.15 0.31 0.72 1.51,3,5-Trimethylbenzene0.15 1.3 0.72 6.31,2,4-Trimethylbenzene


Lab ID#: 0911465A-03B


0.015 9.9 0.037 25Vinyl Chloride0.015 0.026 0.058 0.101,1-Dichloroethene0.029 1.3 0.12 5.3cis-1,2-Dichloroethene0.029 0.18 0.16 0.991,1,1-Trichloroethane0.073 0.18 0.23 0.58Benzene0.029 4.6 0.16 25Trichloroethene0.029 2.5 0.11 9.4Toluene0.029 1.3 0.20 8.7Tetrachloroethene0.029 0.44 0.13 1.9Ethyl Benzene0.058 1.7 0.25 7.3m,p-Xylene0.029 0.71 0.13 3.1o-Xylene

Client Sample ID: VCP-POSTCARBON-111909

Lab ID#: 0911465A-05A


Page 5 of 21



Lab ID#: 0911465A-05A


0.15 0.49 0.72 2.4Freon 120.15 0.43 0.30 0.89Chloromethane0.15 0.20 0.57 0.77Bromomethane0.73 7.1 1.4 13Ethanol0.73 3.5 1.7 8.4Acetone0.73 1.9 1.8 4.72-Propanol0.15 0.32 0.43 0.942-Butanone (Methyl Ethyl Ketone)0.15 0.19 0.60 0.774-Methyl-2-pentanone0.15 0.51 0.72 2.54-Ethyltoluene0.15 0.20 0.72 0.961,3,5-Trimethylbenzene0.15 0.78 0.72 3.91,2,4-Trimethylbenzene


Lab ID#: 0911465A-05B


0.015 0.35 0.037 0.90Vinyl Chloride0.073 0.13 0.23 0.42Benzene0.029 0.10 0.16 0.55Trichloroethene0.029 2.2 0.11 8.3Toluene0.029 0.050 0.20 0.34Tetrachloroethene0.029 0.25 0.13 1.1Ethyl Benzene0.058 1.0 0.25 4.4m,p-Xylene0.029 0.34 0.13 1.5o-Xylene

Page 6 of 21


Lab ID#: 0911465A-03A


e112709File Name:Dil. Factor: 1.46



0.15 0.26 0.72 1.3Freon 120.15 Not Detected 1.0 Not DetectedFreon 1140.15 0.43 0.30 0.89Chloromethane0.15 Not Detected 0.32 Not Detected1,3-Butadiene0.15 0.18 0.57 0.70Bromomethane0.15 Not Detected 0.38 Not DetectedChloroethane0.15 Not Detected 0.82 Not DetectedFreon 110.73 4.4 1.4 8.3Ethanol0.15 Not Detected 1.1 Not DetectedFreon 1130.73 4.5 1.7 11Acetone0.73 1.6 1.8 4.02-Propanol0.73 Not Detected 2.3 Not DetectedCarbon Disulfide0.73 Not Detected 2.3 Not Detected3-Chloropropene0.29 Not Detected 1.0 Not DetectedMethylene Chloride0.15 0.15 0.51 0.53Hexane0.15 0.50 0.43 1.52-Butanone (Methyl Ethyl Ketone)0.73 Not Detected 2.2 Not DetectedTetrahydrofuran0.15 Not Detected 0.71 Not DetectedChloroform0.15 0.19 0.50 0.66Cyclohexane0.15 Not Detected 0.92 Not DetectedCarbon Tetrachloride0.73 Not Detected 3.4 Not Detected2,2,4-Trimethylpentane0.15 0.17 0.60 0.70Heptane0.15 Not Detected 0.67 Not Detected1,2-Dichloropropane0.15 Not Detected 0.53 Not Detected1,4-Dioxane0.15 Not Detected 0.98 Not DetectedBromodichloromethane0.15 Not Detected 0.66 Not Detectedcis-1,3-Dichloropropene0.15 Not Detected 0.60 Not Detected4-Methyl-2-pentanone0.15 Not Detected 0.66 Not Detectedtrans-1,3-Dichloropropene0.73 Not Detected 3.0 Not Detected2-Hexanone0.15 Not Detected 1.2 Not DetectedDibromochloromethane0.15 Not Detected 1.1 Not Detected1,2-Dibromoethane (EDB)0.15 Not Detected 0.67 Not DetectedChlorobenzene0.15 Not Detected 0.62 Not DetectedStyrene0.15 Not Detected 1.5 Not DetectedBromoform0.15 Not Detected 0.72 Not DetectedCumene0.15 0.15 0.72 0.74Propylbenzene0.15 0.79 0.72 3.94-Ethyltoluene0.15 0.31 0.72 1.51,3,5-Trimethylbenzene0.15 1.3 0.72 6.31,2,4-Trimethylbenzene

Page 7 of 21


Lab ID#: 0911465A-03A





0.15 Not Detected 0.88 Not Detected1,3-Dichlorobenzene0.15 Not Detected 0.88 Not Detected1,4-Dichlorobenzene0.15 Not Detected 0.76 Not Detectedalpha-Chlorotoluene0.15 Not Detected 0.88 Not Detected1,2-Dichlorobenzene0.73 Not Detected 5.4 Not Detected1,2,4-Trichlorobenzene0.73 Not Detected 7.8 Not DetectedHexachlorobutadiene




Page 8 of 21


Lab ID#: 0911465A-03B


e112709simFile Name:Dil. Factor: 1.46



0.015 9.9 0.037 25Vinyl Chloride0.015 0.026 0.058 0.101,1-Dichloroethene0.029 Not Detected 0.12 Not Detected1,1-Dichloroethane0.029 1.3 0.12 5.3cis-1,2-Dichloroethene0.029 0.18 0.16 0.991,1,1-Trichloroethane0.073 0.18 0.23 0.58Benzene0.029 Not Detected 0.12 Not Detected1,2-Dichloroethane0.029 4.6 0.16 25Trichloroethene0.029 2.5 0.11 9.4Toluene0.029 Not Detected 0.16 Not Detected1,1,2-Trichloroethane0.029 1.3 0.20 8.7Tetrachloroethene0.029 0.44 0.13 1.9Ethyl Benzene0.058 1.7 0.25 7.3m,p-Xylene0.029 0.71 0.13 3.1o-Xylene0.029 Not Detected 0.20 Not Detected1,1,2,2-Tetrachloroethane0.15 Not Detected 0.58 Not Detectedtrans-1,2-Dichloroethene0.15 Not Detected 0.53 Not DetectedMethyl tert-butyl ether




Page 9 of 21


Lab ID#: 0911465A-05A





0.15 0.49 0.72 2.4Freon 120.15 Not Detected 1.0 Not DetectedFreon 1140.15 0.43 0.30 0.89Chloromethane0.15 Not Detected 0.32 Not Detected1,3-Butadiene0.15 0.20 0.57 0.77Bromomethane0.15 Not Detected 0.38 Not DetectedChloroethane0.15 Not Detected 0.82 Not DetectedFreon 110.73 7.1 1.4 13Ethanol0.15 Not Detected 1.1 Not DetectedFreon 1130.73 3.5 1.7 8.4Acetone0.73 1.9 1.8 4.72-Propanol0.73 Not Detected 2.3 Not DetectedCarbon Disulfide0.73 Not Detected 2.3 Not Detected3-Chloropropene0.29 Not Detected 1.0 Not DetectedMethylene Chloride0.15 Not Detected 0.51 Not DetectedHexane0.15 0.32 0.43 0.942-Butanone (Methyl Ethyl Ketone)0.73 Not Detected 2.2 Not DetectedTetrahydrofuran0.15 Not Detected 0.71 Not DetectedChloroform0.15 Not Detected 0.50 Not DetectedCyclohexane0.15 Not Detected 0.92 Not DetectedCarbon Tetrachloride0.73 Not Detected 3.4 Not Detected2,2,4-Trimethylpentane0.15 Not Detected 0.60 Not DetectedHeptane0.15 Not Detected 0.67 Not Detected1,2-Dichloropropane0.15 Not Detected 0.53 Not Detected1,4-Dioxane0.15 Not Detected 0.98 Not DetectedBromodichloromethane0.15 Not Detected 0.66 Not Detectedcis-1,3-Dichloropropene0.15 0.19 0.60 0.774-Methyl-2-pentanone0.15 Not Detected 0.66 Not Detectedtrans-1,3-Dichloropropene0.73 Not Detected 3.0 Not Detected2-Hexanone0.15 Not Detected 1.2 Not DetectedDibromochloromethane0.15 Not Detected 1.1 Not Detected1,2-Dibromoethane (EDB)0.15 Not Detected 0.67 Not DetectedChlorobenzene0.15 Not Detected 0.62 Not DetectedStyrene0.15 Not Detected 1.5 Not DetectedBromoform0.15 Not Detected 0.72 Not DetectedCumene0.15 Not Detected 0.72 Not DetectedPropylbenzene0.15 0.51 0.72 2.54-Ethyltoluene0.15 0.20 0.72 0.961,3,5-Trimethylbenzene0.15 0.78 0.72 3.91,2,4-Trimethylbenzene

Page 10 of 21


Lab ID#: 0911465A-05A









Page 11 of 21


Lab ID#: 0911465A-05B





0.015 0.35 0.037 0.90Vinyl Chloride0.015 Not Detected 0.058 Not Detected1,1-Dichloroethene0.029 Not Detected 0.12 Not Detected1,1-Dichloroethane0.029 Not Detected 0.12 Not Detectedcis-1,2-Dichloroethene0.029 Not Detected 0.16 Not Detected1,1,1-Trichloroethane0.073 0.13 0.23 0.42Benzene0.029 Not Detected 0.12 Not Detected1,2-Dichloroethane0.029 0.10 0.16 0.55Trichloroethene0.029 2.2 0.11 8.3Toluene0.029 Not Detected 0.16 Not Detected1,1,2-Trichloroethane0.029 0.050 0.20 0.34Tetrachloroethene0.029 0.25 0.13 1.1Ethyl Benzene0.058 1.0 0.25 4.4m,p-Xylene0.029 0.34 0.13 1.5o-Xylene0.029 Not Detected 0.20 Not Detected1,1,2,2-Tetrachloroethane0.15 Not Detected 0.58 Not Detectedtrans-1,2-Dichloroethene0.15 Not Detected 0.53 Not DetectedMethyl tert-butyl ether




Page 12 of 21


Lab ID#: 0911465A-06A





0.10 Not Detected 0.49 Not DetectedFreon 120.10 Not Detected 0.70 Not DetectedFreon 1140.10 Not Detected 0.21 Not DetectedChloromethane0.10 Not Detected 0.22 Not Detected1,3-Butadiene0.10 Not Detected 0.39 Not DetectedBromomethane0.10 Not Detected 0.26 Not DetectedChloroethane0.10 Not Detected 0.56 Not DetectedFreon 110.50 Not Detected 0.94 Not DetectedEthanol0.10 Not Detected 0.77 Not DetectedFreon 1130.50 Not Detected 1.2 Not DetectedAcetone0.50 Not Detected 1.2 Not Detected2-Propanol0.50 Not Detected 1.6 Not DetectedCarbon Disulfide0.50 Not Detected 1.6 Not Detected3-Chloropropene0.20 Not Detected 0.69 Not DetectedMethylene Chloride0.10 Not Detected 0.35 Not DetectedHexane0.10 Not Detected 0.29 Not Detected2-Butanone (Methyl Ethyl Ketone)0.50 Not Detected 1.5 Not DetectedTetrahydrofuran0.10 Not Detected 0.49 Not DetectedChloroform0.10 Not Detected 0.34 Not DetectedCyclohexane0.10 Not Detected 0.63 Not DetectedCarbon Tetrachloride0.50 Not Detected 2.3 Not Detected2,2,4-Trimethylpentane0.10 Not Detected 0.41 Not DetectedHeptane0.10 Not Detected 0.46 Not Detected1,2-Dichloropropane0.10 Not Detected 0.36 Not Detected1,4-Dioxane0.10 Not Detected 0.67 Not DetectedBromodichloromethane0.10 Not Detected 0.45 Not Detectedcis-1,3-Dichloropropene0.10 Not Detected 0.41 Not Detected4-Methyl-2-pentanone0.10 Not Detected 0.45 Not Detectedtrans-1,3-Dichloropropene0.50 Not Detected 2.0 Not Detected2-Hexanone0.10 Not Detected 0.85 Not DetectedDibromochloromethane0.10 Not Detected 0.77 Not Detected1,2-Dibromoethane (EDB)0.10 Not Detected 0.46 Not DetectedChlorobenzene0.10 Not Detected 0.42 Not DetectedStyrene0.10 Not Detected 1.0 Not DetectedBromoform0.10 Not Detected 0.49 Not DetectedCumene0.10 Not Detected 0.49 Not DetectedPropylbenzene0.10 Not Detected 0.49 Not Detected4-Ethyltoluene0.10 Not Detected 0.49 Not Detected1,3,5-Trimethylbenzene0.10 Not Detected 0.49 Not Detected1,2,4-Trimethylbenzene

Page 13 of 21


Lab ID#: 0911465A-06A









Page 14 of 21


Lab ID#: 0911465A-06B





0.010 Not Detected 0.026 Not DetectedVinyl Chloride0.010 Not Detected 0.040 Not Detected1,1-Dichloroethene0.020 Not Detected 0.081 Not Detected1,1-Dichloroethane0.020 Not Detected 0.079 Not Detectedcis-1,2-Dichloroethene0.020 Not Detected 0.11 Not Detected1,1,1-Trichloroethane0.050 Not Detected 0.16 Not DetectedBenzene0.020 Not Detected 0.081 Not Detected1,2-Dichloroethane0.020 Not Detected 0.11 Not DetectedTrichloroethene0.020 Not Detected 0.075 Not DetectedToluene0.020 Not Detected 0.11 Not Detected1,1,2-Trichloroethane0.020 Not Detected 0.14 Not DetectedTetrachloroethene0.020 Not Detected 0.087 Not DetectedEthyl Benzene0.040 Not Detected 0.17 Not Detectedm,p-Xylene0.020 Not Detected 0.087 Not Detectedo-Xylene0.020 Not Detected 0.14 Not Detected1,1,2,2-Tetrachloroethane0.10 Not Detected 0.40 Not Detectedtrans-1,2-Dichloroethene0.10 Not Detected 0.36 Not DetectedMethyl tert-butyl ether




Page 15 of 21


Lab ID#: 0911465A-07A




%RecoveryCompound

93Freon 1294Freon 11494Chloromethane901,3-Butadiene89Bromomethane88Chloroethane93Freon 1188Ethanol93Freon 11390Acetone902-Propanol99Carbon Disulfide933-Chloropropene91Methylene Chloride90Hexane952-Butanone (Methyl Ethyl Ketone)92Tetrahydrofuran90Chloroform90Cyclohexane112Carbon Tetrachloride892,2,4-Trimethylpentane91Heptane901,2-Dichloropropane921,4-Dioxane86Bromodichloromethane92cis-1,3-Dichloropropene924-Methyl-2-pentanone95trans-1,3-Dichloropropene972-Hexanone101Dibromochloromethane901,2-Dibromoethane (EDB)91Chlorobenzene96Styrene105Bromoform94Cumene97Propylbenzene1024-Ethyltoluene1041,3,5-Trimethylbenzene1011,2,4-Trimethylbenzene

Page 16 of 21


Lab ID#: 0911465A-07A




%RecoveryCompound

891,3-Dichlorobenzene901,4-Dichlorobenzene106alpha-Chlorotoluene901,2-Dichlorobenzene1091,2,4-Trichlorobenzene101Hexachlorobutadiene




Page 17 of 21


Lab ID#: 0911465A-07B




%RecoveryCompound

89Vinyl Chloride871,1-Dichloroethene901,1-Dichloroethane89cis-1,2-Dichloroethene921,1,1-Trichloroethane86Benzene871,2-Dichloroethane82Trichloroethene87Toluene811,1,2-Trichloroethane79Tetrachloroethene88Ethyl Benzene91m,p-Xylene90o-Xylene841,1,2,2-Tetrachloroethane89trans-1,2-Dichloroethene93Methyl tert-butyl ether




Page 18 of 21


Lab ID#: 0911465A-08A




%RecoveryCompound

102Freon 12103Freon 114103Chloromethane1021,3-Butadiene98Bromomethane98Chloroethane101Freon 11

147 QEthanol91Freon 11394Acetone952-Propanol99Carbon Disulfide1013-Chloropropene91Methylene Chloride97Hexane1002-Butanone (Methyl Ethyl Ketone)97Tetrahydrofuran95Chloroform98Cyclohexane122Carbon Tetrachloride972,2,4-Trimethylpentane98Heptane981,2-Dichloropropane951,4-Dioxane115Bromodichloromethane100cis-1,3-Dichloropropene974-Methyl-2-pentanone106trans-1,3-Dichloropropene1072-Hexanone111Dibromochloromethane1051,2-Dibromoethane (EDB)101Chlorobenzene106Styrene116Bromoform101Cumene105Propylbenzene1114-Ethyltoluene1141,3,5-Trimethylbenzene1091,2,4-Trimethylbenzene

Page 19 of 21


Lab ID#: 0911465A-08A




%RecoveryCompound





Page 20 of 21


Lab ID#: 0911465A-08B




%RecoveryCompound





Page 21 of 21

12/10/2009







Regards,







CLIENT: BILL TO:

PHONE:


503-924-4704x113

503-924-4707

11/20/2009DATE COMPLETED: 12/09/2009

P.O. #


Work Order Summary

FAX:



PRESSUREFINAL

01A DEEP-PRECARBON-111909 Modified TO-15 1.5 "Hg 5 psi02A DEEP-MIDCARBON-111909 Modified TO-15 3.5 "Hg 5 psi04A VCP-PRECARBON-111909 Modified TO-15 2.0 "Hg 5 psi04B VCP-PRECARBON-111909 Modified TO-15 2.0 "Hg 5 psi05A Lab Blank Modified TO-15 NA NA05B Lab Blank Modified TO-15 NA NA05C Lab Blank Modified TO-15 NA NA05D Lab Blank Modified TO-15 NA NA06A CCV Modified TO-15 NA NA06B CCV Modified TO-15 NA NA06C CCV Modified TO-15 NA NA06D CCV Modified TO-15 NA NA07A LCS Modified TO-15 NA NA07B LCS Modified TO-15 NA NA07C LCS Modified TO-15 NA NA07D LCS Modified TO-15 NA NA

CERTIFIED BY:

Laboratory Director

DATE:



12/10/09

Page 2 of 34







Three 6 Liter Summa Canister (SIM Certified) samples were received on November 20, 2009. Thelaboratory performed analysis via modified EPA Method TO-15 using GC/MS in the Full Scan and SIMacquisition modes. The method involves concentrating up to 1.0 liters of air. The concentrated aliquot is then flash vaporized and swept through a water management system to remove water vapor. Following dehumidification, the sample passes directly into the GC/MS for analysis.












Receiving Notes


Page 3 of 34


The results for sample VCP-PRECARBON-111909 in this report were acquired from two separate datafiles originating from the same analytical run. The two data files have the same base file name and are differentiated with a "sim" extension on the SIM data file.

Samples DEEP-PRECARBON-111909 and DEEP-MIDCARBON-111909 were transferred fromSIM/Low Level analysis to full scan TO-15 due to high levels of target compounds.


Analytical Notes




Page 4 of 34


Client Sample ID: DEEP-PRECARBON-111909

Lab ID#: 0911465B-01A


350 420 900 1100Vinyl Chloride350 2700 1200 9500Hexane350 9700 1400 38000cis-1,2-Dichloroethene350 1200 1900 66001,1,1-Trichloroethane350 2400 1200 8300Cyclohexane350 790 1600 37002,2,4-Trimethylpentane350 480 1100 1500Benzene350 4400 1400 18000Heptane350 18000 1900 97000Trichloroethene350 5500 1300 20000Toluene350 120000 2400 840000Tetrachloroethene350 640 1500 2800m,p-Xylene

Client Sample ID: DEEP-MIDCARBON-111909

Lab ID#: 0911465B-02A


3.0 650 7.8 1700Vinyl Chloride3.0 5.4 8.0 14Chloroethane12 26 23 50Ethanol3.0 52 10 180Methylene Chloride

Client Sample ID: VCP-PRECARBON-111909

Lab ID#: 0911465B-04A


14 230 27 430Ethanol14 250 34 600Acetone14 63 35 1502-Propanol2.9 14 10 50Hexane2.9 18 8.5 552-Butanone (Methyl Ethyl Ketone)2.9 8.4 9.9 29Cyclohexane2.9 75 12 300Heptane2.9 4.6 12 194-Methyl-2-pentanone

Page 5 of 34



Lab ID#: 0911465B-04B


0.58 12 2.3 48cis-1,2-Dichloroethene0.58 1.3 3.1 7.11,1,1-Trichloroethane0.58 36 3.1 190Trichloroethene0.58 300 2.2 1100Toluene0.58 400 3.9 2700Tetrachloroethene0.58 6.1 2.5 26Ethyl Benzene1.2 41 5.0 180m,p-Xylene

0.58 14 2.5 61o-Xylene

Page 6 of 34


Lab ID#: 0911465B-01A


w120721File Name:Dil. Factor: 70.5




1400 Not Detected 2900 Not DetectedChloromethane350 420 900 1100Vinyl Chloride350 Not Detected 780 Not Detected1,3-Butadiene350 Not Detected 1400 Not DetectedBromomethane350 Not Detected 930 Not DetectedChloroethane350 Not Detected 2000 Not DetectedFreon 11

1400 Not Detected 2600 Not DetectedEthanol350 Not Detected 2700 Not DetectedFreon 113350 Not Detected 1400 Not Detected1,1-Dichloroethene


1400 Not Detected 4400 Not Detected3-Chloropropene350 Not Detected 1200 Not DetectedMethylene Chloride350 Not Detected 1300 Not DetectedMethyl tert-butyl ether350 Not Detected 1400 Not Detectedtrans-1,2-Dichloroethene350 2700 1200 9500Hexane350 Not Detected 1400 Not Detected1,1-Dichloroethane350 Not Detected 1000 Not Detected2-Butanone (Methyl Ethyl Ketone)350 9700 1400 38000cis-1,2-Dichloroethene350 Not Detected 1000 Not DetectedTetrahydrofuran350 Not Detected 1700 Not DetectedChloroform350 1200 1900 66001,1,1-Trichloroethane350 2400 1200 8300Cyclohexane350 Not Detected 2200 Not DetectedCarbon Tetrachloride350 790 1600 37002,2,4-Trimethylpentane350 480 1100 1500Benzene350 Not Detected 1400 Not Detected1,2-Dichloroethane350 4400 1400 18000Heptane350 18000 1900 97000Trichloroethene350 Not Detected 1600 Not Detected1,2-Dichloropropane


Page 7 of 34


Lab ID#: 0911465B-01A






1400 Not Detected 5800 Not Detected2-Hexanone350 Not Detected 3000 Not DetectedDibromochloromethane350 Not Detected 2700 Not Detected1,2-Dibromoethane (EDB)350 Not Detected 1600 Not DetectedChlorobenzene350 Not Detected 1500 Not DetectedEthyl Benzene350 640 1500 2800m,p-Xylene350 Not Detected 1500 Not Detectedo-Xylene350 Not Detected 1500 Not DetectedStyrene350 Not Detected 3600 Not DetectedBromoform350 Not Detected 1700 Not DetectedCumene350 Not Detected 2400 Not Detected1,1,2,2-Tetrachloroethane350 Not Detected 1700 Not DetectedPropylbenzene350 Not Detected 1700 Not Detected4-Ethyltoluene350 Not Detected 1700 Not Detected1,3,5-Trimethylbenzene350 Not Detected 1700 Not Detected1,2,4-Trimethylbenzene350 Not Detected 2100 Not Detected1,3-Dichlorobenzene350 Not Detected 2100 Not Detected1,4-Dichlorobenzene350 Not Detected 1800 Not Detectedalpha-Chlorotoluene350 Not Detected 2100 Not Detected1,2-Dichlorobenzene





Page 8 of 34


Lab ID#: 0911465B-02A

MODIFIED EPA METHOD TO-15 GC/MS FULL SCAN

s120807File Name:Dil. Factor: 6.08



3.0 Not Detected 15 Not DetectedFreon 123.0 Not Detected 21 Not DetectedFreon 11412 Not Detected 25 Not DetectedChloromethane3.0 650 7.8 1700Vinyl Chloride3.0 Not Detected 6.7 Not Detected1,3-Butadiene3.0 Not Detected 12 Not DetectedBromomethane3.0 5.4 8.0 14Chloroethane3.0 Not Detected 17 Not DetectedFreon 1112 26 23 50Ethanol3.0 Not Detected 23 Not DetectedFreon 1133.0 Not Detected 12 Not Detected1,1-Dichloroethene12 Not Detected 29 Not DetectedAcetone12 Not Detected 30 Not Detected2-Propanol3.0 Not Detected 9.5 Not DetectedCarbon Disulfide12 Not Detected 38 Not Detected3-Chloropropene3.0 52 10 180Methylene Chloride3.0 Not Detected 11 Not DetectedMethyl tert-butyl ether3.0 Not Detected 12 Not Detectedtrans-1,2-Dichloroethene3.0 Not Detected 11 Not DetectedHexane3.0 Not Detected 12 Not Detected1,1-Dichloroethane3.0 Not Detected 9.0 Not Detected2-Butanone (Methyl Ethyl Ketone)3.0 Not Detected 12 Not Detectedcis-1,2-Dichloroethene3.0 Not Detected 9.0 Not DetectedTetrahydrofuran3.0 Not Detected 15 Not DetectedChloroform3.0 Not Detected 16 Not Detected1,1,1-Trichloroethane3.0 Not Detected 10 Not DetectedCyclohexane3.0 Not Detected 19 Not DetectedCarbon Tetrachloride3.0 Not Detected 14 Not Detected2,2,4-Trimethylpentane3.0 Not Detected 9.7 Not DetectedBenzene3.0 Not Detected 12 Not Detected1,2-Dichloroethane3.0 Not Detected 12 Not DetectedHeptane3.0 Not Detected 16 Not DetectedTrichloroethene3.0 Not Detected 14 Not Detected1,2-Dichloropropane12 Not Detected 44 Not Detected1,4-Dioxane3.0 Not Detected 20 Not DetectedBromodichloromethane3.0 Not Detected 14 Not Detectedcis-1,3-Dichloropropene3.0 Not Detected 12 Not Detected4-Methyl-2-pentanone3.0 Not Detected 11 Not DetectedToluene3.0 Not Detected 14 Not Detectedtrans-1,3-Dichloropropene

Page 9 of 34


Lab ID#: 0911465B-02A








98 70-130Toluene-d8105 70-1301,2-Dichloroethane-d4109 70-1304-Bromofluorobenzene

Page 10 of 34


Lab ID#: 0911465B-04A





2.9 Not Detected 14 Not DetectedFreon 122.9 Not Detected 20 Not DetectedFreon 1142.9 Not Detected 5.9 Not DetectedChloromethane2.9 Not Detected 6.4 Not Detected1,3-Butadiene2.9 Not Detected 11 Not DetectedBromomethane2.9 Not Detected 7.6 Not DetectedChloroethane2.9 Not Detected 16 Not DetectedFreon 1114 230 27 430Ethanol2.9 Not Detected 22 Not DetectedFreon 11314 250 34 600Acetone14 63 35 1502-Propanol14 Not Detected 45 Not DetectedCarbon Disulfide14 Not Detected 45 Not Detected3-Chloropropene5.8 Not Detected 20 Not DetectedMethylene Chloride2.9 14 10 50Hexane2.9 18 8.5 552-Butanone (Methyl Ethyl Ketone)14 Not Detected 42 Not DetectedTetrahydrofuran2.9 Not Detected 14 Not DetectedChloroform2.9 8.4 9.9 29Cyclohexane2.9 Not Detected 18 Not DetectedCarbon Tetrachloride14 Not Detected 67 Not Detected2,2,4-Trimethylpentane2.9 75 12 300Heptane2.9 Not Detected 13 Not Detected1,2-Dichloropropane2.9 Not Detected 10 Not Detected1,4-Dioxane2.9 Not Detected 19 Not DetectedBromodichloromethane2.9 Not Detected 13 Not Detectedcis-1,3-Dichloropropene2.9 4.6 12 194-Methyl-2-pentanone2.9 Not Detected 13 Not Detectedtrans-1,3-Dichloropropene14 Not Detected 59 Not Detected2-Hexanone2.9 Not Detected 24 Not DetectedDibromochloromethane2.9 Not Detected 22 Not Detected1,2-Dibromoethane (EDB)2.9 Not Detected 13 Not DetectedChlorobenzene2.9 Not Detected 12 Not DetectedStyrene2.9 Not Detected 30 Not DetectedBromoform2.9 Not Detected 14 Not DetectedCumene2.9 Not Detected 14 Not DetectedPropylbenzene2.9 Not Detected 14 Not Detected4-Ethyltoluene2.9 Not Detected 14 Not Detected1,3,5-Trimethylbenzene2.9 Not Detected 14 Not Detected1,2,4-Trimethylbenzene

Page 11 of 34


Lab ID#: 0911465B-04A





2.9 Not Detected 17 Not Detected1,3-Dichlorobenzene2.9 Not Detected 17 Not Detected1,4-Dichlorobenzene2.9 Not Detected 15 Not Detectedalpha-Chlorotoluene2.9 Not Detected 17 Not Detected1,2-Dichlorobenzene14 Not Detected 110 Not Detected1,2,4-Trichlorobenzene14 Not Detected 150 Not DetectedHexachlorobutadiene




Page 12 of 34


Lab ID#: 0911465B-04B





0.29 Not Detected 0.74 Not DetectedVinyl Chloride0.29 Not Detected 1.1 Not Detected1,1-Dichloroethene0.58 Not Detected 2.3 Not Detected1,1-Dichloroethane0.58 12 2.3 48cis-1,2-Dichloroethene0.58 1.3 3.1 7.11,1,1-Trichloroethane1.4 Not Detected 4.6 Not DetectedBenzene

0.58 Not Detected 2.3 Not Detected1,2-Dichloroethane0.58 36 3.1 190Trichloroethene0.58 300 2.2 1100Toluene0.58 Not Detected 3.1 Not Detected1,1,2-Trichloroethane0.58 400 3.9 2700Tetrachloroethene0.58 6.1 2.5 26Ethyl Benzene1.2 41 5.0 180m,p-Xylene

0.58 14 2.5 61o-Xylene0.58 Not Detected 4.0 Not Detected1,1,2,2-Tetrachloroethane2.9 Not Detected 11 Not Detectedtrans-1,2-Dichloroethene2.9 Not Detected 10 Not DetectedMethyl tert-butyl ether




Page 13 of 34


Lab ID#: 0911465B-05A






Page 14 of 34


Lab ID#: 0911465B-05A









Page 15 of 34


Lab ID#: 0911465B-05B









Page 16 of 34


Lab ID#: 0911465B-05C






Page 17 of 34


Lab ID#: 0911465B-05C









Page 18 of 34


Lab ID#: 0911465B-05D





0.50 Not Detected 2.5 Not DetectedFreon 120.50 Not Detected 3.5 Not DetectedFreon 1142.0 Not Detected 4.1 Not DetectedChloromethane

0.50 Not Detected 1.3 Not DetectedVinyl Chloride0.50 Not Detected 1.1 Not Detected1,3-Butadiene0.50 Not Detected 1.9 Not DetectedBromomethane0.50 Not Detected 1.3 Not DetectedChloroethane0.50 Not Detected 2.8 Not DetectedFreon 112.0 Not Detected 3.8 Not DetectedEthanol

0.50 Not Detected 3.8 Not DetectedFreon 1130.50 Not Detected 2.0 Not Detected1,1-Dichloroethene2.0 Not Detected 4.8 Not DetectedAcetone2.0 Not Detected 4.9 Not Detected2-Propanol

0.50 Not Detected 1.6 Not DetectedCarbon Disulfide2.0 Not Detected 6.3 Not Detected3-Chloropropene

0.50 Not Detected 1.7 Not DetectedMethylene Chloride0.50 Not Detected 1.8 Not DetectedMethyl tert-butyl ether0.50 Not Detected 2.0 Not Detectedtrans-1,2-Dichloroethene0.50 Not Detected 1.8 Not DetectedHexane0.50 Not Detected 2.0 Not Detected1,1-Dichloroethane0.50 Not Detected 1.5 Not Detected2-Butanone (Methyl Ethyl Ketone)0.50 Not Detected 2.0 Not Detectedcis-1,2-Dichloroethene0.50 Not Detected 1.5 Not DetectedTetrahydrofuran0.50 Not Detected 2.4 Not DetectedChloroform0.50 Not Detected 2.7 Not Detected1,1,1-Trichloroethane0.50 Not Detected 1.7 Not DetectedCyclohexane0.50 Not Detected 3.1 Not DetectedCarbon Tetrachloride0.50 Not Detected 2.3 Not Detected2,2,4-Trimethylpentane0.50 Not Detected 1.6 Not DetectedBenzene0.50 Not Detected 2.0 Not Detected1,2-Dichloroethane0.50 Not Detected 2.0 Not DetectedHeptane0.50 Not Detected 2.7 Not DetectedTrichloroethene0.50 Not Detected 2.3 Not Detected1,2-Dichloropropane2.0 Not Detected 7.2 Not Detected1,4-Dioxane

0.50 Not Detected 3.4 Not DetectedBromodichloromethane0.50 Not Detected 2.3 Not Detectedcis-1,3-Dichloropropene0.50 Not Detected 2.0 Not Detected4-Methyl-2-pentanone0.50 Not Detected 1.9 Not DetectedToluene0.50 Not Detected 2.3 Not Detectedtrans-1,3-Dichloropropene

Page 19 of 34


Lab ID#: 0911465B-05D





0.50 Not Detected 2.7 Not Detected1,1,2-Trichloroethane0.50 Not Detected 3.4 Not DetectedTetrachloroethene2.0 Not Detected 8.2 Not Detected2-Hexanone

0.50 Not Detected 4.2 Not DetectedDibromochloromethane0.50 Not Detected 3.8 Not Detected1,2-Dibromoethane (EDB)0.50 Not Detected 2.3 Not DetectedChlorobenzene0.50 Not Detected 2.2 Not DetectedEthyl Benzene0.50 Not Detected 2.2 Not Detectedm,p-Xylene0.50 Not Detected 2.2 Not Detectedo-Xylene0.50 Not Detected 2.1 Not DetectedStyrene0.50 Not Detected 5.2 Not DetectedBromoform0.50 Not Detected 2.4 Not DetectedCumene0.50 Not Detected 3.4 Not Detected1,1,2,2-Tetrachloroethane0.50 Not Detected 2.4 Not DetectedPropylbenzene0.50 Not Detected 2.4 Not Detected4-Ethyltoluene0.50 Not Detected 2.4 Not Detected1,3,5-Trimethylbenzene0.50 Not Detected 2.4 Not Detected1,2,4-Trimethylbenzene0.50 Not Detected 3.0 Not Detected1,3-Dichlorobenzene0.50 Not Detected 3.0 Not Detected1,4-Dichlorobenzene0.50 Not Detected 2.6 Not Detectedalpha-Chlorotoluene0.50 Not Detected 3.0 Not Detected1,2-Dichlorobenzene2.0 Not Detected 15 Not Detected1,2,4-Trichlorobenzene2.0 Not Detected 21 Not DetectedHexachlorobutadiene




Page 20 of 34


Lab ID#: 0911465B-06A




%RecoveryCompound

105Freon 1299Freon 114116Chloromethane991,3-Butadiene103Bromomethane106Chloroethane103Freon 1191Ethanol97Freon 11384Acetone932-Propanol102Carbon Disulfide973-Chloropropene92Methylene Chloride99Hexane1092-Butanone (Methyl Ethyl Ketone)101Tetrahydrofuran105Chloroform96Cyclohexane

136 QCarbon Tetrachloride982,2,4-Trimethylpentane116Heptane1111,2-Dichloropropane1021,4-Dioxane120Bromodichloromethane110cis-1,3-Dichloropropene1204-Methyl-2-pentanone113trans-1,3-Dichloropropene1072-Hexanone116Dibromochloromethane1061,2-Dibromoethane (EDB)104Chlorobenzene108Styrene120Bromoform105Cumene110Propylbenzene1084-Ethyltoluene1101,3,5-Trimethylbenzene1091,2,4-Trimethylbenzene

Page 21 of 34


Lab ID#: 0911465B-06A




%RecoveryCompound

981,3-Dichlorobenzene1001,4-Dichlorobenzene





Page 22 of 34


Lab ID#: 0911465B-06B




%RecoveryCompound

106Vinyl Chloride901,1-Dichloroethene1101,1-Dichloroethane92cis-1,2-Dichloroethene1081,1,1-Trichloroethane104Benzene

133 Q1,2-Dichloroethane101Trichloroethene106Toluene1011,1,2-Trichloroethane88Tetrachloroethene99Ethyl Benzene96m,p-Xylene100o-Xylene1021,1,2,2-Tetrachloroethane99trans-1,2-Dichloroethene125Methyl tert-butyl ether




Page 23 of 34


Lab ID#: 0911465B-06C




%RecoveryCompound

105Freon 12109Freon 11499Chloromethane110Vinyl Chloride1111,3-Butadiene116Bromomethane111Chloroethane108Freon 11112Ethanol110Freon 1131111,1-Dichloroethene108Acetone1032-Propanol111Carbon Disulfide1143-Chloropropene104Methylene Chloride124Methyl tert-butyl ether112trans-1,2-Dichloroethene112Hexane1091,1-Dichloroethane1182-Butanone (Methyl Ethyl Ketone)111cis-1,2-Dichloroethene110Tetrahydrofuran107Chloroform1081,1,1-Trichloroethane115Cyclohexane106Carbon Tetrachloride1142,2,4-Trimethylpentane105Benzene1051,2-Dichloroethane109Heptane107Trichloroethene1061,2-Dichloropropane1091,4-Dioxane105Bromodichloromethane116cis-1,3-Dichloropropene1154-Methyl-2-pentanone104Toluene110trans-1,3-Dichloropropene

Page 24 of 34


Lab ID#: 0911465B-06C




%RecoveryCompound





Page 25 of 34


Lab ID#: 0911465B-06D




%RecoveryCompound


Page 26 of 34


Lab ID#: 0911465B-06D




%RecoveryCompound





Page 27 of 34


Lab ID#: 0911465B-07A




%RecoveryCompound

104Freon 1299Freon 114113Chloromethane1001,3-Butadiene103Bromomethane105Chloroethane105Freon 11128Ethanol92Freon 11381Acetone852-Propanol100Carbon Disulfide973-Chloropropene85Methylene Chloride99Hexane1082-Butanone (Methyl Ethyl Ketone)102Tetrahydrofuran102Chloroform98Cyclohexane

134 QCarbon Tetrachloride1002,2,4-Trimethylpentane117Heptane1151,2-Dichloropropane1021,4-Dioxane121Bromodichloromethane114cis-1,3-Dichloropropene1214-Methyl-2-pentanone

131 Qtrans-1,3-Dichloropropene1192-Hexanone130Dibromochloromethane1231,2-Dibromoethane (EDB)117Chlorobenzene118Styrene130Bromoform111Cumene115Propylbenzene1154-Ethyltoluene1171,3,5-Trimethylbenzene1161,2,4-Trimethylbenzene

Page 28 of 34


Lab ID#: 0911465B-07A




%RecoveryCompound






Page 29 of 34


Lab ID#: 0911465B-07B




%RecoveryCompound





Page 30 of 34


Lab ID#: 0911465B-07C




%RecoveryCompound


149 QEthanol79Freon 113801,1-Dichloroethene89Acetone782-Propanol88Carbon Disulfide893-Chloropropene78Methylene Chloride96Methyl tert-butyl ether90trans-1,2-Dichloroethene91Hexane841,1-Dichloroethane952-Butanone (Methyl Ethyl Ketone)94cis-1,2-Dichloroethene89Tetrahydrofuran85Chloroform851,1,1-Trichloroethane91Cyclohexane86Carbon Tetrachloride922,2,4-Trimethylpentane84Benzene821,2-Dichloroethane88Heptane84Trichloroethene841,2-Dichloropropane911,4-Dioxane83Bromodichloromethane89cis-1,3-Dichloropropene884-Methyl-2-pentanone80Toluene89trans-1,3-Dichloropropene

Page 31 of 34


Lab ID#: 0911465B-07C




%RecoveryCompound





Page 32 of 34


Lab ID#: 0911465B-07D




%RecoveryCompound


Page 33 of 34


Lab ID#: 0911465B-07D




%RecoveryCompound





Page 34 of 34


Project Name: Tarr IRAMProject #: 1073-06





Regards,







CLIENT: BILL TO:

PHONE:


503-924-4704x113

503-924-470711/25/2009


P.O. #

PROJECT # 1073-06 Tarr IRAM

Work Order Summary

FAX:



PRESSUREFINAL

02A DSVE-POST-112409 Modified TO-15 3.5 "Hg 5 psi02B DSVE-POST-112409 Modified TO-15 3.5 "Hg 5 psi03A DSVE-MID-112409 Modified TO-15 3.5 "Hg 5 psi03B DSVE-MID-112409 Modified TO-15 3.5 "Hg 5 psi04A SSVE-POST-112409 Modified TO-15 3.5 "Hg 5 psi04AA SSVE-POST-112409 Lab Duplicate Modified TO-15 3.5 "Hg 5 psi04B SSVE-POST-112409 Modified TO-15 3.5 "Hg 5 psi04BB SSVE-POST-112409 Lab Duplicate Modified TO-15 3.5 "Hg 5 psi05A Lab Blank Modified TO-15 NA NA05B Lab Blank Modified TO-15 NA NA05C Lab Blank Modified TO-15 NA NA05D Lab Blank Modified TO-15 NA NA06A CCV Modified TO-15 NA NA06B CCV Modified TO-15 NA NA06C CCV Modified TO-15 NA NA06D CCV Modified TO-15 NA NA07A LCS Modified TO-15 NA NA


Page 2 of 37

Continued on next page



CLIENT: BILL TO:

PHONE:


503-924-4704x113

503-924-470711/25/2009


P.O. #

PROJECT # 1073-06 Tarr IRAM

Work Order Summary

FAX:



PRESSUREFINAL

07B LCS Modified TO-15 NA NA07C LCS Modified TO-15 NA NA07D LCS Modified TO-15 NA NA

CERTIFIED BY:

Laboratory Director

DATE:



12/04/09

Page 3 of 37







Three 6 Liter Summa Canister (SIM Certified) samples were received on November 25, 2009. The laboratory performed analysis via modified EPA Method TO-15 using GC/MS in the Full Scan and SIM acquisition modes. The method involves concentrating up to 1.0 liters of air. The concentrated aliquot is then flash vaporized and swept through a water management system to remove water vapor. Following dehumidification, the sample passes directly into the GC/MS for analysis.












Receiving Notes


The results for each sample in this report were acquired from two separate data files originating from the same analytical run. The two data files have the same base file name and are differentiated with a "sim" extension on the SIM data file.

Analytical Notes

Page 4 of 37


All Quality Control Limit exceedences and affected sample results are noted by flags. Each flag is defined at the bottom of this Case Narrative and on each Sample Result Summary page. Target compound non-detects in the samples that are associated with high bias in QC analyses have not been flagged.

Dilution was performed on sample SSVE-POST-112409 due to the presence of high level non-target species.




Page 5 of 37


Client Sample ID: DSVE-POST-112409

Lab ID#: 0911572A-02A


1.1 1.2 5.3 6.1Freon 125.4 13 10 24Ethanol5.4 10 13 25Acetone5.4 6.1 13 152-Propanol5.4 46 17 140Carbon Disulfide1.1 5.1 3.2 152-Butanone (Methyl Ethyl Ketone)

Client Sample ID: DSVE-POST-112409

Lab ID#: 0911572A-02B


0.11 150 0.28 380Vinyl Chloride0.22 4.2 0.81 16Toluene0.22 0.24 1.5 1.7Tetrachloroethene0.22 0.79 0.94 3.4Ethyl Benzene0.43 2.2 1.9 9.7m,p-Xylene0.22 0.76 0.94 3.3o-Xylene

Client Sample ID: DSVE-MID-112409

Lab ID#: 0911572A-03A


1.5 580 3.9 1500Vinyl Chloride1.5 7.4 4.0 20Chloroethane7.6 24 14 44Ethanol

Client Sample ID: DSVE-MID-112409

Lab ID#: 0911572A-03B


0.30 5.2 1.1 20Toluene0.30 0.88 1.3 3.8Ethyl Benzene0.61 2.6 2.6 11m,p-Xylene0.30 0.79 1.3 3.4o-Xylene

Page 6 of 37


Client Sample ID: SSVE-POST-112409

Lab ID#: 0911572A-04A


3.8 5.6 7.2 10Ethanol3.8 10 9.0 24Acetone3.8 4.3 9.3 102-Propanol

0.76 0.79 3.7 3.91,2,4-Trimethylbenzene

Client Sample ID: SSVE-POST-112409 Lab Duplicate

Lab ID#: 0911572A-04AA


7.6 8.0 14 15Ethanol7.6 8.4 18 20Acetone

Client Sample ID: SSVE-POST-112409

Lab ID#: 0911572A-04B


0.076 2.3 0.19 6.0Vinyl Chloride0.38 0.57 1.2 1.8Benzene0.15 5.0 0.57 19Toluene0.15 0.24 1.0 1.6Tetrachloroethene0.15 0.92 0.66 4.0Ethyl Benzene0.30 3.0 1.3 13m,p-Xylene0.15 0.85 0.66 3.7o-Xylene

Client Sample ID: SSVE-POST-112409 Lab Duplicate

Lab ID#: 0911572A-04BB


0.15 2.4 0.39 6.2Vinyl Chloride0.30 4.8 1.1 18Toluene0.30 0.99 1.3 4.3Ethyl Benzene0.61 3.0 2.6 13m,p-Xylene0.30 1.1 1.3 4.6o-Xylene

Page 7 of 37

Client Sample ID: DSVE-POST-112409Lab ID#: 0911572A-02A



Date of Collection: 11/24/09 12:50:00 PDate of Analysis: 12/2/09 06:25 PM


1.1 1.2 5.3 6.1Freon 121.1 Not Detected 7.6 Not DetectedFreon 1141.1 Not Detected 2.2 Not DetectedChloromethane1.1 Not Detected 2.4 Not Detected1,3-Butadiene1.1 Not Detected 4.2 Not DetectedBromomethane1.1 Not Detected 2.8 Not DetectedChloroethane1.1 Not Detected 6.1 Not DetectedFreon 115.4 13 10 24Ethanol1.1 Not Detected 8.3 Not DetectedFreon 1135.4 10 13 25Acetone5.4 6.1 13 152-Propanol5.4 46 17 140Carbon Disulfide5.4 Not Detected 17 Not Detected3-Chloropropene2.2 Not Detected 7.5 Not DetectedMethylene Chloride1.1 Not Detected 3.8 Not DetectedHexane1.1 5.1 3.2 152-Butanone (Methyl Ethyl Ketone)5.4 Not Detected 16 Not DetectedTetrahydrofuran1.1 Not Detected 5.3 Not DetectedChloroform1.1 Not Detected 3.7 Not DetectedCyclohexane1.1 Not Detected 6.8 Not DetectedCarbon Tetrachloride5.4 Not Detected 25 Not Detected2,2,4-Trimethylpentane1.1 Not Detected 4.4 Not DetectedHeptane1.1 Not Detected 5.0 Not Detected1,2-Dichloropropane1.1 Not Detected 3.9 Not Detected1,4-Dioxane1.1 Not Detected 7.2 Not DetectedBromodichloromethane1.1 Not Detected 4.9 Not Detectedcis-1,3-Dichloropropene1.1 Not Detected 4.4 Not Detected4-Methyl-2-pentanone1.1 Not Detected 4.9 Not Detectedtrans-1,3-Dichloropropene5.4 Not Detected 22 Not Detected2-Hexanone1.1 Not Detected 9.2 Not DetectedDibromochloromethane1.1 Not Detected 8.3 Not Detected1,2-Dibromoethane (EDB)1.1 Not Detected 5.0 Not DetectedChlorobenzene1.1 Not Detected 4.6 Not DetectedStyrene1.1 Not Detected 11 Not DetectedBromoform1.1 Not Detected 5.3 Not DetectedCumene1.1 Not Detected 5.3 Not DetectedPropylbenzene1.1 Not Detected 5.3 Not Detected4-Ethyltoluene1.1 Not Detected 5.3 Not Detected1,3,5-Trimethylbenzene1.1 Not Detected 5.3 Not Detected1,2,4-Trimethylbenzene

Page 8 of 37

Client Sample ID: DSVE-POST-112409Lab ID#: 0911572A-02A





1.1 Not Detected 6.5 Not Detected1,3-Dichlorobenzene1.1 Not Detected 6.5 Not Detected1,4-Dichlorobenzene1.1 Not Detected 5.6 Not Detectedalpha-Chlorotoluene1.1 Not Detected 6.5 Not Detected1,2-Dichlorobenzene5.4 Not Detected 40 Not Detected1,2,4-Trichlorobenzene5.4 Not Detected 58 Not DetectedHexachlorobutadiene




Page 9 of 37

Client Sample ID: DSVE-POST-112409 Lab ID#: 0911572A-02B





0.11 150 0.28 380Vinyl Chloride0.11 Not Detected 0.43 Not Detected1,1-Dichloroethene0.22 Not Detected 0.87 Not Detected1,1-Dichloroethane0.22 Not Detected 0.86 Not Detectedcis-1,2-Dichloroethene0.22 Not Detected 1.2 Not Detected1,1,1-Trichloroethane0.54 Not Detected 1.7 Not DetectedBenzene0.22 Not Detected 0.87 Not Detected1,2-Dichloroethane0.22 Not Detected 1.2 Not DetectedTrichloroethene0.22 4.2 0.81 16Toluene0.22 Not Detected 1.2 Not Detected1,1,2-Trichloroethane0.22 0.24 1.5 1.7Tetrachloroethene0.22 0.79 0.94 3.4Ethyl Benzene0.43 2.2 1.9 9.7m,p-Xylene0.22 0.76 0.94 3.3o-Xylene0.22 Not Detected 1.5 Not Detected1,1,2,2-Tetrachloroethane1.1 Not Detected 4.3 Not Detectedtrans-1,2-Dichloroethene1.1 Not Detected 3.9 Not DetectedMethyl tert-butyl ether




Page 10 of 37

Client Sample ID: DSVE-MID-112409Lab ID#: 0911572A-03A



Date of Collection: 11/24/09 1:00:00 PMDate of Analysis: 12/2/09 07:01 AM


1.5 580 3.9 1500Vinyl Chloride1.5 Not Detected 7.5 Not DetectedFreon 121.5 Not Detected 11 Not DetectedFreon 1141.5 Not Detected 3.1 Not DetectedChloromethane1.5 Not Detected 3.4 Not Detected1,3-Butadiene1.5 Not Detected 5.9 Not DetectedBromomethane1.5 7.4 4.0 20Chloroethane1.5 Not Detected 8.5 Not DetectedFreon 117.6 24 14 44Ethanol1.5 Not Detected 12 Not DetectedFreon 1137.6 Not Detected 18 Not DetectedAcetone7.6 Not Detected 19 Not Detected2-Propanol7.6 Not Detected 24 Not DetectedCarbon Disulfide7.6 Not Detected 24 Not Detected3-Chloropropene3.0 Not Detected 10 Not DetectedMethylene Chloride1.5 Not Detected 5.4 Not DetectedHexane1.5 Not Detected 4.5 Not Detected2-Butanone (Methyl Ethyl Ketone)7.6 Not Detected 22 Not DetectedTetrahydrofuran1.5 Not Detected 7.4 Not DetectedChloroform1.5 Not Detected 5.2 Not DetectedCyclohexane1.5 Not Detected 9.6 Not DetectedCarbon Tetrachloride7.6 Not Detected 36 Not Detected2,2,4-Trimethylpentane1.5 Not Detected 6.2 Not DetectedHeptane1.5 Not Detected 7.0 Not Detected1,2-Dichloropropane1.5 Not Detected 5.5 Not Detected1,4-Dioxane1.5 Not Detected 10 Not DetectedBromodichloromethane1.5 Not Detected 6.9 Not Detectedcis-1,3-Dichloropropene1.5 Not Detected 6.2 Not Detected4-Methyl-2-pentanone1.5 Not Detected 6.9 Not Detectedtrans-1,3-Dichloropropene7.6 Not Detected 31 Not Detected2-Hexanone1.5 Not Detected 13 Not DetectedDibromochloromethane1.5 Not Detected 12 Not Detected1,2-Dibromoethane (EDB)1.5 Not Detected 7.0 Not DetectedChlorobenzene1.5 Not Detected 6.5 Not DetectedStyrene1.5 Not Detected 16 Not DetectedBromoform1.5 Not Detected 7.5 Not DetectedCumene1.5 Not Detected 7.5 Not DetectedPropylbenzene1.5 Not Detected 7.5 Not Detected4-Ethyltoluene1.5 Not Detected 7.5 Not Detected1,3,5-Trimethylbenzene

Page 11 of 37

Client Sample ID: DSVE-MID-112409Lab ID#: 0911572A-03A





1.5 Not Detected 7.5 Not Detected1,2,4-Trimethylbenzene1.5 Not Detected 9.1 Not Detected1,3-Dichlorobenzene1.5 Not Detected 9.1 Not Detected1,4-Dichlorobenzene1.5 Not Detected 7.9 Not Detectedalpha-Chlorotoluene1.5 Not Detected 9.1 Not Detected1,2-Dichlorobenzene7.6 Not Detected 56 Not Detected1,2,4-Trichlorobenzene7.6 Not Detected 81 Not DetectedHexachlorobutadiene




Page 12 of 37

Client Sample ID: DSVE-MID-112409Lab ID#: 0911572A-03B





0.15 Not Detected 0.60 Not Detected1,1-Dichloroethene0.30 Not Detected 1.2 Not Detected1,1-Dichloroethane0.30 Not Detected 1.2 Not Detectedcis-1,2-Dichloroethene0.30 Not Detected 1.6 Not Detected1,1,1-Trichloroethane0.76 Not Detected 2.4 Not DetectedBenzene0.30 Not Detected 1.2 Not Detected1,2-Dichloroethane0.30 Not Detected 1.6 Not DetectedTrichloroethene0.30 5.2 1.1 20Toluene0.30 Not Detected 1.6 Not Detected1,1,2-Trichloroethane0.30 Not Detected 2.1 Not DetectedTetrachloroethene0.30 0.88 1.3 3.8Ethyl Benzene0.61 2.6 2.6 11m,p-Xylene0.30 0.79 1.3 3.4o-Xylene0.30 Not Detected 2.1 Not Detected1,1,2,2-Tetrachloroethane1.5 Not Detected 6.0 Not Detectedtrans-1,2-Dichloroethene1.5 Not Detected 5.5 Not DetectedMethyl tert-butyl ether




Page 13 of 37

Client Sample ID: SSVE-POST-112409Lab ID#: 0911572A-04A





0.76 Not Detected 3.8 Not DetectedFreon 120.76 Not Detected 5.3 Not DetectedFreon 1140.76 Not Detected 1.6 Not DetectedChloromethane0.76 Not Detected 1.7 Not Detected1,3-Butadiene0.76 Not Detected 3.0 Not DetectedBromomethane0.76 Not Detected 2.0 Not DetectedChloroethane0.76 Not Detected 4.3 Not DetectedFreon 113.8 5.6 7.2 10Ethanol

0.76 Not Detected 5.8 Not DetectedFreon 1133.8 10 9.0 24Acetone3.8 4.3 9.3 102-Propanol3.8 Not Detected 12 Not DetectedCarbon Disulfide3.8 Not Detected 12 Not Detected3-Chloropropene1.5 Not Detected 5.3 Not DetectedMethylene Chloride

0.76 Not Detected 2.7 Not DetectedHexane0.76 Not Detected 2.2 Not Detected2-Butanone (Methyl Ethyl Ketone)3.8 Not Detected 11 Not DetectedTetrahydrofuran

0.76 Not Detected 3.7 Not DetectedChloroform0.76 Not Detected 2.6 Not DetectedCyclohexane0.76 Not Detected 4.8 Not DetectedCarbon Tetrachloride3.8 Not Detected 18 Not Detected2,2,4-Trimethylpentane

0.76 Not Detected 3.1 Not DetectedHeptane0.76 Not Detected 3.5 Not Detected1,2-Dichloropropane0.76 Not Detected 2.7 Not Detected1,4-Dioxane0.76 Not Detected 5.1 Not DetectedBromodichloromethane0.76 Not Detected 3.4 Not Detectedcis-1,3-Dichloropropene0.76 Not Detected 3.1 Not Detected4-Methyl-2-pentanone0.76 Not Detected 3.4 Not Detectedtrans-1,3-Dichloropropene3.8 Not Detected 16 Not Detected2-Hexanone

0.76 Not Detected 6.5 Not DetectedDibromochloromethane0.76 Not Detected 5.8 Not Detected1,2-Dibromoethane (EDB)0.76 Not Detected 3.5 Not DetectedChlorobenzene0.76 Not Detected 3.2 Not DetectedStyrene0.76 Not Detected 7.8 Not DetectedBromoform0.76 Not Detected 3.7 Not DetectedCumene0.76 Not Detected 3.7 Not DetectedPropylbenzene0.76 Not Detected 3.7 Not Detected4-Ethyltoluene0.76 Not Detected 3.7 Not Detected1,3,5-Trimethylbenzene0.76 0.79 3.7 3.91,2,4-Trimethylbenzene

Page 14 of 37

Client Sample ID: SSVE-POST-112409Lab ID#: 0911572A-04A









Page 15 of 37

Client Sample ID: SSVE-POST-112409 Lab DuplicateLab ID#: 0911572A-04AA





1.5 Not Detected 7.5 Not DetectedFreon 121.5 Not Detected 11 Not DetectedFreon 1141.5 Not Detected 3.1 Not DetectedChloromethane1.5 Not Detected 3.4 Not Detected1,3-Butadiene1.5 Not Detected 5.9 Not DetectedBromomethane1.5 Not Detected 4.0 Not DetectedChloroethane1.5 Not Detected 8.5 Not DetectedFreon 117.6 8.0 14 15Ethanol1.5 Not Detected 12 Not DetectedFreon 1137.6 8.4 18 20Acetone7.6 Not Detected 19 Not Detected2-Propanol7.6 Not Detected 24 Not DetectedCarbon Disulfide7.6 Not Detected 24 Not Detected3-Chloropropene3.0 Not Detected 10 Not DetectedMethylene Chloride1.5 Not Detected 5.4 Not DetectedHexane1.5 Not Detected 4.5 Not Detected2-Butanone (Methyl Ethyl Ketone)7.6 Not Detected 22 Not DetectedTetrahydrofuran1.5 Not Detected 7.4 Not DetectedChloroform1.5 Not Detected 5.2 Not DetectedCyclohexane1.5 Not Detected 9.6 Not DetectedCarbon Tetrachloride7.6 Not Detected 36 Not Detected2,2,4-Trimethylpentane1.5 Not Detected 6.2 Not DetectedHeptane1.5 Not Detected 7.0 Not Detected1,2-Dichloropropane1.5 Not Detected 5.5 Not Detected1,4-Dioxane1.5 Not Detected 10 Not DetectedBromodichloromethane1.5 Not Detected 6.9 Not Detectedcis-1,3-Dichloropropene1.5 Not Detected 6.2 Not Detected4-Methyl-2-pentanone1.5 Not Detected 6.9 Not Detectedtrans-1,3-Dichloropropene7.6 Not Detected 31 Not Detected2-Hexanone1.5 Not Detected 13 Not DetectedDibromochloromethane1.5 Not Detected 12 Not Detected1,2-Dibromoethane (EDB)1.5 Not Detected 7.0 Not DetectedChlorobenzene1.5 Not Detected 6.5 Not DetectedStyrene1.5 Not Detected 16 Not DetectedBromoform1.5 Not Detected 7.5 Not DetectedCumene1.5 Not Detected 7.5 Not DetectedPropylbenzene1.5 Not Detected 7.5 Not Detected4-Ethyltoluene1.5 Not Detected 7.5 Not Detected1,3,5-Trimethylbenzene1.5 Not Detected 7.5 Not Detected1,2,4-Trimethylbenzene

Page 16 of 37

Client Sample ID: SSVE-POST-112409 Lab DuplicateLab ID#: 0911572A-04AA










Page 17 of 37

Client Sample ID: SSVE-POST-112409Lab ID#: 0911572A-04B





0.076 2.3 0.19 6.0Vinyl Chloride0.076 Not Detected 0.30 Not Detected1,1-Dichloroethene0.15 Not Detected 0.62 Not Detected1,1-Dichloroethane0.15 Not Detected 0.60 Not Detectedcis-1,2-Dichloroethene0.15 Not Detected 0.83 Not Detected1,1,1-Trichloroethane0.38 0.57 1.2 1.8Benzene0.15 Not Detected 0.62 Not Detected1,2-Dichloroethane0.15 Not Detected 0.82 Not DetectedTrichloroethene0.15 5.0 0.57 19Toluene0.15 Not Detected 0.83 Not Detected1,1,2-Trichloroethane0.15 0.24 1.0 1.6Tetrachloroethene0.15 0.92 0.66 4.0Ethyl Benzene0.30 3.0 1.3 13m,p-Xylene0.15 0.85 0.66 3.7o-Xylene0.15 Not Detected 1.0 Not Detected1,1,2,2-Tetrachloroethane0.76 Not Detected 3.0 Not Detectedtrans-1,2-Dichloroethene0.76 Not Detected 2.7 Not DetectedMethyl tert-butyl ether




Page 18 of 37

Client Sample ID: SSVE-POST-112409 Lab DuplicateLab ID#: 0911572A-04BB





0.15 2.4 0.39 6.2Vinyl Chloride0.15 Not Detected 0.60 Not Detected1,1-Dichloroethene0.30 Not Detected 1.2 Not Detected1,1-Dichloroethane0.30 Not Detected 1.2 Not Detectedcis-1,2-Dichloroethene0.30 Not Detected 1.6 Not Detected1,1,1-Trichloroethane0.76 Not Detected 2.4 Not DetectedBenzene0.30 Not Detected 1.2 Not Detected1,2-Dichloroethane0.30 Not Detected 1.6 Not DetectedTrichloroethene0.30 4.8 1.1 18Toluene0.30 Not Detected 1.6 Not Detected1,1,2-Trichloroethane0.30 Not Detected 2.1 Not DetectedTetrachloroethene0.30 0.99 1.3 4.3Ethyl Benzene0.61 3.0 2.6 13m,p-Xylene0.30 1.1 1.3 4.6o-Xylene0.30 Not Detected 2.1 Not Detected1,1,2,2-Tetrachloroethane1.5 Not Detected 6.0 Not Detectedtrans-1,2-Dichloroethene1.5 Not Detected 5.5 Not DetectedMethyl tert-butyl ether




Page 19 of 37

Client Sample ID: Lab BlankLab ID#: 0911572A-05A





0.10 Not Detected 0.26 Not DetectedVinyl Chloride0.10 Not Detected 0.49 Not DetectedFreon 120.10 Not Detected 0.70 Not DetectedFreon 1140.10 Not Detected 0.21 Not DetectedChloromethane0.10 Not Detected 0.22 Not Detected1,3-Butadiene0.10 Not Detected 0.39 Not DetectedBromomethane0.10 Not Detected 0.26 Not DetectedChloroethane0.10 Not Detected 0.56 Not DetectedFreon 110.50 Not Detected 0.94 Not DetectedEthanol0.10 Not Detected 0.77 Not DetectedFreon 1130.50 Not Detected 1.2 Not DetectedAcetone0.50 Not Detected 1.2 Not Detected2-Propanol0.50 Not Detected 1.6 Not DetectedCarbon Disulfide0.50 Not Detected 1.6 Not Detected3-Chloropropene0.20 Not Detected 0.69 Not DetectedMethylene Chloride0.10 Not Detected 0.35 Not DetectedHexane0.10 Not Detected 0.29 Not Detected2-Butanone (Methyl Ethyl Ketone)0.50 Not Detected 1.5 Not DetectedTetrahydrofuran0.10 Not Detected 0.49 Not DetectedChloroform0.10 Not Detected 0.34 Not DetectedCyclohexane0.10 Not Detected 0.63 Not DetectedCarbon Tetrachloride0.50 Not Detected 2.3 Not Detected2,2,4-Trimethylpentane0.10 Not Detected 0.41 Not DetectedHeptane0.10 Not Detected 0.46 Not Detected1,2-Dichloropropane0.10 Not Detected 0.36 Not Detected1,4-Dioxane0.10 Not Detected 0.67 Not DetectedBromodichloromethane0.10 Not Detected 0.45 Not Detectedcis-1,3-Dichloropropene0.10 Not Detected 0.41 Not Detected4-Methyl-2-pentanone0.10 Not Detected 0.45 Not Detectedtrans-1,3-Dichloropropene0.50 Not Detected 2.0 Not Detected2-Hexanone0.10 Not Detected 0.85 Not DetectedDibromochloromethane0.10 Not Detected 0.77 Not Detected1,2-Dibromoethane (EDB)0.10 Not Detected 0.46 Not DetectedChlorobenzene0.10 Not Detected 0.42 Not DetectedStyrene0.10 Not Detected 1.0 Not DetectedBromoform0.10 Not Detected 0.49 Not DetectedCumene0.10 Not Detected 0.49 Not DetectedPropylbenzene0.10 Not Detected 0.49 Not Detected4-Ethyltoluene0.10 Not Detected 0.49 Not Detected1,3,5-Trimethylbenzene

Page 20 of 37






0.10 Not Detected 0.49 Not Detected1,2,4-Trimethylbenzene0.10 Not Detected 0.60 Not Detected1,3-Dichlorobenzene0.10 Not Detected 0.60 Not Detected1,4-Dichlorobenzene0.10 Not Detected 0.52 Not Detectedalpha-Chlorotoluene0.10 Not Detected 0.60 Not Detected1,2-Dichlorobenzene0.50 Not Detected 3.7 Not Detected1,2,4-Trichlorobenzene0.50 Not Detected 5.3 Not DetectedHexachlorobutadiene




Page 21 of 37

Client Sample ID: Lab BlankLab ID#: 0911572A-05B









Page 22 of 37

Client Sample ID: Lab BlankLab ID#: 0911572A-05C






Page 23 of 37










Page 24 of 37

Client Sample ID: Lab BlankLab ID#: 0911572A-05D









Page 25 of 37

Client Sample ID: CCVLab ID#: 0911572A-06A




%RecoveryCompound

102Vinyl Chloride105Freon 1297Freon 114

103Chloromethane921,3-Butadiene

100Bromomethane99Chloroethane

101Freon 1176Ethanol96Freon 11395Acetone842-Propanol99Carbon Disulfide953-Chloropropene90Methylene Chloride94Hexane

1042-Butanone (Methyl Ethyl Ketone)94Tetrahydrofuran

102Chloroform95Cyclohexane

101Carbon Tetrachloride952,2,4-Trimethylpentane

113Heptane1101,2-Dichloropropane1021,4-Dioxane120Bromodichloromethane109cis-1,3-Dichloropropene1154-Methyl-2-pentanone113trans-1,3-Dichloropropene1042-Hexanone117Dibromochloromethane1051,2-Dibromoethane (EDB)105Chlorobenzene108Styrene116Bromoform104Cumene108Propylbenzene1064-Ethyltoluene1081,3,5-Trimethylbenzene

Page 26 of 37





%RecoveryCompound

1071,2,4-Trimethylbenzene961,3-Dichlorobenzene981,4-Dichlorobenzene

129alpha-Chlorotoluene951,2-Dichlorobenzene901,2,4-Trichlorobenzene87Hexachlorobutadiene




Page 27 of 37

Client Sample ID: CCVLab ID#: 0911572A-06B




%RecoveryCompound

105Vinyl Chloride901,1-Dichloroethene

1091,1-Dichloroethane93cis-1,2-Dichloroethene

1081,1,1-Trichloroethane103Benzene

131 Q1,2-Dichloroethane102Trichloroethene106Toluene1021,1,2-Trichloroethane90Tetrachloroethene

101Ethyl Benzene97m,p-Xylene

102o-Xylene1011,1,2,2-Tetrachloroethane99trans-1,2-Dichloroethene

120Methyl tert-butyl ether




Page 28 of 37

Client Sample ID: CCVLab ID#: 0911572A-06C




%RecoveryCompound

104Freon 1297Freon 114


100Bromomethane103Chloroethane102Freon 1176Ethanol97Freon 11378Acetone852-Propanol99Carbon Disulfide973-Chloropropene89Methylene Chloride97Hexane

1032-Butanone (Methyl Ethyl Ketone)100Tetrahydrofuran103Chloroform94Cyclohexane

134 QCarbon Tetrachloride962,2,4-Trimethylpentane

114Heptane1131,2-Dichloropropane1001,4-Dioxane121Bromodichloromethane110cis-1,3-Dichloropropene1164-Methyl-2-pentanone121trans-1,3-Dichloropropene1092-Hexanone120Dibromochloromethane1091,2-Dibromoethane (EDB)108Chlorobenzene110Styrene118Bromoform107Cumene111Propylbenzene1084-Ethyltoluene1091,3,5-Trimethylbenzene1081,2,4-Trimethylbenzene

Page 29 of 37





%RecoveryCompound






Page 30 of 37

Client Sample ID: CCVLab ID#: 0911572A-06D




%RecoveryCompound




134 Q1,2-Dichloroethane103Trichloroethene107Toluene1071,1,2-Trichloroethane94Tetrachloroethene

103Ethyl Benzene100m,p-Xylene103o-Xylene1041,1,2,2-Tetrachloroethane98trans-1,2-Dichloroethene





Page 31 of 37

Client Sample ID: LCSLab ID#: 0911572A-07A




%RecoveryCompound

103Vinyl Chloride102Freon 1297Freon 11498Chloromethane961,3-Butadiene


1062-Butanone (Methyl Ethyl Ketone)97Tetrahydrofuran99Chloroform95Cyclohexane

132 QCarbon Tetrachloride962,2,4-Trimethylpentane

110Heptane1081,2-Dichloropropane1011,4-Dioxane117Bromodichloromethane110cis-1,3-Dichloropropene1154-Methyl-2-pentanone120trans-1,3-Dichloropropene1112-Hexanone124Dibromochloromethane1151,2-Dibromoethane (EDB)112Chlorobenzene114Styrene123Bromoform106Cumene112Propylbenzene1114-Ethyltoluene1151,3,5-Trimethylbenzene

Page 32 of 37





%RecoveryCompound

1131,2,4-Trimethylbenzene1021,3-Dichlorobenzene1071,4-Dichlorobenzene





Page 33 of 37

Client Sample ID: LCSLab ID#: 0911572A-07B




%RecoveryCompound




1251,2-Dichloroethane101Trichloroethene100Toluene1081,1,2-Trichloroethane94Tetrachloroethene

106Ethyl Benzene102m,p-Xylene106o-Xylene1061,1,2,2-Tetrachloroethane98trans-1,2-Dichloroethene





Page 34 of 37

Client Sample ID: LCSLab ID#: 0911572A-07C




%RecoveryCompound

102Freon 1296Freon 114



1052-Butanone (Methyl Ethyl Ketone)96Tetrahydrofuran98Chloroform91Cyclohexane98Carbon Tetrachloride942,2,4-Trimethylpentane

111Heptane1101,2-Dichloropropane981,4-Dioxane

116Bromodichloromethane109cis-1,3-Dichloropropene1164-Methyl-2-pentanone118trans-1,3-Dichloropropene1082-Hexanone120Dibromochloromethane1101,2-Dibromoethane (EDB)106Chlorobenzene108Styrene119Bromoform102Cumene106Propylbenzene1074-Ethyltoluene1081,3,5-Trimethylbenzene1081,2,4-Trimethylbenzene

Page 35 of 37





%RecoveryCompound






Page 36 of 37

Client Sample ID: LCSLab ID#: 0911572A-07D




%RecoveryCompound




1251,2-Dichloroethane98Trichloroethene98Toluene

1041,1,2-Trichloroethane90Tetrachloroethene

103Ethyl Benzene99m,p-Xylene

103o-Xylene1041,1,2,2-Tetrachloroethane96trans-1,2-Dichloroethene





Page 37 of 37

12/11/2009







Regards,







CLIENT: BILL TO:

PHONE:


503-924-4704x113

503-924-4707

12/04/2009DATE COMPLETED: 12/11/2009

P.O. #


Work Order Summary

FAX:



PRESSUREFINAL

03A DEEP POSTCARBON-120309 Modified TO-15 3.5 "Hg 5 psi03B DEEP POSTCARBON-120309 Modified TO-15 3.5 "Hg 5 psi06A SHALLOW POSTCARBON-120309 Modified TO-15 3.0 "Hg 5 psi06B SHALLOW POSTCARBON-120309 Modified TO-15 3.0 "Hg 5 psi07A Lab Blank Modified TO-15 NA NA07B Lab Blank Modified TO-15 NA NA08A CCV Modified TO-15 NA NA08B CCV Modified TO-15 NA NA09A LCS Modified TO-15 NA NA09B LCS Modified TO-15 NA NA

CERTIFIED BY:

Laboratory Director

DATE:



12/11/09

Page 2 of 21







Two 6 Liter Summa Canister (SIM Certified) samples were received on December 04, 2009. The laboratory performed analysis via modified EPA Method TO-15 using GC/MS in the Full Scan and SIMacquisition modes. The method involves concentrating up to 1.0 liters of air. The concentrated aliquot is then flash vaporized and swept through a water management system to remove water vapor. Following dehumidification, the sample passes directly into the GC/MS for analysis.












Receiving Notes



Analytical Notes

Page 3 of 21






Page 4 of 21



Lab ID#: 0912120A-03A


0.15 0.51 0.31 1.0Chloromethane0.76 75 E 1.4 140 EEthanol0.76 31 1.8 73Acetone0.76 210 E 1.9 510 E2-Propanol0.15 0.94 0.54 3.3Hexane0.15 0.34 0.45 0.992-Butanone (Methyl Ethyl Ketone)0.15 0.26 0.52 0.91Cyclohexane0.15 0.82 0.62 3.3Heptane0.15 0.29 0.65 1.2Styrene0.15 0.16 0.75 0.78Cumene0.15 0.58 0.75 2.9Propylbenzene0.15 3.0 0.75 154-Ethyltoluene0.15 1.5 0.75 7.21,3,5-Trimethylbenzene0.15 6.7 0.75 331,2,4-Trimethylbenzene0.15 0.93 0.91 5.61,3-Dichlorobenzene


Lab ID#: 0912120A-03B


0.015 3.7 0.039 9.5Vinyl Chloride0.015 0.017 0.060 0.0681,1-Dichloroethene0.030 0.57 0.12 2.2cis-1,2-Dichloroethene0.030 0.036 0.16 0.201,1,1-Trichloroethane0.076 0.096 0.24 0.30Benzene0.030 0.54 0.16 2.9Trichloroethene0.030 1.5 0.11 5.8Toluene0.030 0.056 0.21 0.38Tetrachloroethene0.030 0.59 0.13 2.6Ethyl Benzene0.061 2.3 0.26 10m,p-Xylene0.030 1.1 0.13 4.7o-Xylene


Lab ID#: 0912120A-06A

Page 5 of 21



Lab ID#: 0912120A-06A


0.15 0.62 0.74 3.1Freon 120.15 0.18 0.31 0.38Chloromethane0.74 23 1.4 44Ethanol0.74 27 1.8 64Acetone0.74 82 E 1.8 200 E2-Propanol0.15 0.78 0.52 2.8Hexane0.15 0.34 0.44 0.992-Butanone (Methyl Ethyl Ketone)0.15 0.19 0.51 0.64Cyclohexane0.15 0.79 0.61 3.2Heptane0.15 0.16 0.63 0.69Styrene0.15 0.15 0.73 0.76Cumene0.15 0.56 0.73 2.8Propylbenzene0.15 2.8 0.73 144-Ethyltoluene0.15 1.4 0.73 6.71,3,5-Trimethylbenzene0.15 6.4 0.73 311,2,4-Trimethylbenzene0.15 0.46 0.90 2.81,3-Dichlorobenzene


Lab ID#: 0912120A-06B


0.015 1.3 0.038 3.4Vinyl Chloride0.074 0.077 0.24 0.25Benzene0.030 0.95 0.11 3.6Toluene0.030 0.042 0.20 0.28Tetrachloroethene0.030 0.55 0.13 2.4Ethyl Benzene0.060 2.1 0.26 9.3m,p-Xylene0.030 1.0 0.13 4.5o-Xylene

Page 6 of 21


Lab ID#: 0912120A-03A





0.15 Not Detected 0.75 Not DetectedFreon 120.15 Not Detected 1.1 Not DetectedFreon 1140.15 0.51 0.31 1.0Chloromethane0.15 Not Detected 0.34 Not Detected1,3-Butadiene0.15 Not Detected 0.59 Not DetectedBromomethane0.15 Not Detected 0.40 Not DetectedChloroethane0.15 Not Detected 0.85 Not DetectedFreon 110.76 75 E 1.4 140 EEthanol0.15 Not Detected 1.2 Not DetectedFreon 1130.76 31 1.8 73Acetone0.76 210 E 1.9 510 E2-Propanol0.76 Not Detected 2.4 Not DetectedCarbon Disulfide0.76 Not Detected 2.4 Not Detected3-Chloropropene0.30 Not Detected 1.0 Not DetectedMethylene Chloride0.15 0.94 0.54 3.3Hexane0.15 0.34 0.45 0.992-Butanone (Methyl Ethyl Ketone)0.76 Not Detected 2.2 Not DetectedTetrahydrofuran0.15 Not Detected 0.74 Not DetectedChloroform0.15 0.26 0.52 0.91Cyclohexane0.15 Not Detected 0.96 Not DetectedCarbon Tetrachloride0.76 Not Detected 3.6 Not Detected2,2,4-Trimethylpentane0.15 0.82 0.62 3.3Heptane0.15 Not Detected 0.70 Not Detected1,2-Dichloropropane0.15 Not Detected 0.55 Not Detected1,4-Dioxane0.15 Not Detected 1.0 Not DetectedBromodichloromethane0.15 Not Detected 0.69 Not Detectedcis-1,3-Dichloropropene0.15 Not Detected 0.62 Not Detected4-Methyl-2-pentanone0.15 Not Detected 0.69 Not Detectedtrans-1,3-Dichloropropene0.76 Not Detected 3.1 Not Detected2-Hexanone0.15 Not Detected 1.3 Not DetectedDibromochloromethane0.15 Not Detected 1.2 Not Detected1,2-Dibromoethane (EDB)0.15 Not Detected 0.70 Not DetectedChlorobenzene0.15 0.29 0.65 1.2Styrene0.15 Not Detected 1.6 Not DetectedBromoform0.15 0.16 0.75 0.78Cumene0.15 0.58 0.75 2.9Propylbenzene0.15 3.0 0.75 154-Ethyltoluene0.15 1.5 0.75 7.21,3,5-Trimethylbenzene0.15 6.7 0.75 331,2,4-Trimethylbenzene

Page 7 of 21


Lab ID#: 0912120A-03A





0.15 0.93 0.91 5.61,3-Dichlorobenzene0.15 Not Detected 0.91 Not Detected1,4-Dichlorobenzene0.15 Not Detected 0.79 Not Detectedalpha-Chlorotoluene0.15 Not Detected 0.91 Not Detected1,2-Dichlorobenzene0.76 Not Detected 5.6 Not Detected1,2,4-Trichlorobenzene0.76 Not Detected 8.1 Not DetectedHexachlorobutadiene

E = Exceeds instrument calibration range.Container Type: 6 Liter Summa Canister (SIM Certified)



Page 8 of 21


Lab ID#: 0912120A-03B





0.015 3.7 0.039 9.5Vinyl Chloride0.015 0.017 0.060 0.0681,1-Dichloroethene0.030 Not Detected 0.12 Not Detected1,1-Dichloroethane0.030 0.57 0.12 2.2cis-1,2-Dichloroethene0.030 0.036 0.16 0.201,1,1-Trichloroethane0.076 0.096 0.24 0.30Benzene0.030 Not Detected 0.12 Not Detected1,2-Dichloroethane0.030 0.54 0.16 2.9Trichloroethene0.030 1.5 0.11 5.8Toluene0.030 Not Detected 0.16 Not Detected1,1,2-Trichloroethane0.030 0.056 0.21 0.38Tetrachloroethene0.030 0.59 0.13 2.6Ethyl Benzene0.061 2.3 0.26 10m,p-Xylene0.030 1.1 0.13 4.7o-Xylene0.030 Not Detected 0.21 Not Detected1,1,2,2-Tetrachloroethane0.15 Not Detected 0.60 Not Detectedtrans-1,2-Dichloroethene0.15 Not Detected 0.55 Not DetectedMethyl tert-butyl ether




Page 9 of 21


Lab ID#: 0912120A-06A





0.15 0.62 0.74 3.1Freon 120.15 Not Detected 1.0 Not DetectedFreon 1140.15 0.18 0.31 0.38Chloromethane0.15 Not Detected 0.33 Not Detected1,3-Butadiene0.15 Not Detected 0.58 Not DetectedBromomethane0.15 Not Detected 0.39 Not DetectedChloroethane0.15 Not Detected 0.84 Not DetectedFreon 110.74 23 1.4 44Ethanol0.15 Not Detected 1.1 Not DetectedFreon 1130.74 27 1.8 64Acetone0.74 82 E 1.8 200 E2-Propanol0.74 Not Detected 2.3 Not DetectedCarbon Disulfide0.74 Not Detected 2.3 Not Detected3-Chloropropene0.30 Not Detected 1.0 Not DetectedMethylene Chloride0.15 0.78 0.52 2.8Hexane0.15 0.34 0.44 0.992-Butanone (Methyl Ethyl Ketone)0.74 Not Detected 2.2 Not DetectedTetrahydrofuran0.15 Not Detected 0.73 Not DetectedChloroform0.15 0.19 0.51 0.64Cyclohexane0.15 Not Detected 0.94 Not DetectedCarbon Tetrachloride0.74 Not Detected 3.5 Not Detected2,2,4-Trimethylpentane0.15 0.79 0.61 3.2Heptane0.15 Not Detected 0.69 Not Detected1,2-Dichloropropane0.15 Not Detected 0.54 Not Detected1,4-Dioxane0.15 Not Detected 1.0 Not DetectedBromodichloromethane0.15 Not Detected 0.68 Not Detectedcis-1,3-Dichloropropene0.15 Not Detected 0.61 Not Detected4-Methyl-2-pentanone0.15 Not Detected 0.68 Not Detectedtrans-1,3-Dichloropropene0.74 Not Detected 3.0 Not Detected2-Hexanone0.15 Not Detected 1.3 Not DetectedDibromochloromethane0.15 Not Detected 1.1 Not Detected1,2-Dibromoethane (EDB)0.15 Not Detected 0.68 Not DetectedChlorobenzene0.15 0.16 0.63 0.69Styrene0.15 Not Detected 1.5 Not DetectedBromoform0.15 0.15 0.73 0.76Cumene0.15 0.56 0.73 2.8Propylbenzene0.15 2.8 0.73 144-Ethyltoluene0.15 1.4 0.73 6.71,3,5-Trimethylbenzene0.15 6.4 0.73 311,2,4-Trimethylbenzene

Page 10 of 21


Lab ID#: 0912120A-06A






E = Exceeds instrument calibration range.Container Type: 6 Liter Summa Canister (SIM Certified)



Page 11 of 21


Lab ID#: 0912120A-06B





0.015 1.3 0.038 3.4Vinyl Chloride0.015 Not Detected 0.059 Not Detected1,1-Dichloroethene0.030 Not Detected 0.12 Not Detected1,1-Dichloroethane0.030 Not Detected 0.12 Not Detectedcis-1,2-Dichloroethene0.030 Not Detected 0.16 Not Detected1,1,1-Trichloroethane0.074 0.077 0.24 0.25Benzene0.030 Not Detected 0.12 Not Detected1,2-Dichloroethane0.030 Not Detected 0.16 Not DetectedTrichloroethene0.030 0.95 0.11 3.6Toluene0.030 Not Detected 0.16 Not Detected1,1,2-Trichloroethane0.030 0.042 0.20 0.28Tetrachloroethene0.030 0.55 0.13 2.4Ethyl Benzene0.060 2.1 0.26 9.3m,p-Xylene0.030 1.0 0.13 4.5o-Xylene0.030 Not Detected 0.20 Not Detected1,1,2,2-Tetrachloroethane0.15 Not Detected 0.59 Not Detectedtrans-1,2-Dichloroethene0.15 Not Detected 0.54 Not DetectedMethyl tert-butyl ether




Page 12 of 21


Lab ID#: 0912120A-07A






Page 13 of 21


Lab ID#: 0912120A-07A









Page 14 of 21


Lab ID#: 0912120A-07B









Page 15 of 21


Lab ID#: 0912120A-08A




%RecoveryCompound


Page 16 of 21


Lab ID#: 0912120A-08A




%RecoveryCompound






Page 17 of 21


Lab ID#: 0912120A-08B




%RecoveryCompound






Page 18 of 21


Lab ID#: 0912120A-09A




%RecoveryCompound

107Freon 1297Freon 114103Chloromethane1031,3-Butadiene105Bromomethane109Chloroethane130Freon 11117Ethanol94Freon 11382Acetone792-Propanol102Carbon Disulfide943-Chloropropene84Methylene Chloride98Hexane1052-Butanone (Methyl Ethyl Ketone)100Tetrahydrofuran104Chloroform93Cyclohexane104Carbon Tetrachloride1012,2,4-Trimethylpentane130Heptane1201,2-Dichloropropane1061,4-Dioxane127Bromodichloromethane113cis-1,3-Dichloropropene1284-Methyl-2-pentanone

132 Qtrans-1,3-Dichloropropene1182-Hexanone130Dibromochloromethane1221,2-Dibromoethane (EDB)115Chlorobenzene116Styrene127Bromoform109Cumene115Propylbenzene1144-Ethyltoluene1171,3,5-Trimethylbenzene1151,2,4-Trimethylbenzene

Page 19 of 21


Lab ID#: 0912120A-09A




%RecoveryCompound






Page 20 of 21


Lab ID#: 0912120A-09B




%RecoveryCompound






Page 21 of 21

12/21/2009







Regards,







CLIENT: BILL TO:

PHONE:


503-924-4704x113

503-924-4707

12/04/2009DATE COMPLETED: 12/21/2009

P.O. #


Work Order Summary

FAX:



PRESSUREFINAL

01A DEEP PRECARBON-120309 Modified TO-15 2.5 "Hg 5 psi02A DEEP MIDCARBON-120309 Modified TO-15 2.5 "Hg 5 psi02B DEEP MIDCARBON-120309 Modified TO-15 2.5 "Hg 5 psi04A SHALLOW PRECARBON-120309 Modified TO-15 4.0 "Hg 5 psi05A SHALLOW MIDCARBON-120309 Modified TO-15 2.5 "Hg 5 psi05B SHALLOW MIDCARBON-120309 Modified TO-15 2.5 "Hg 5 psi06A Lab Blank Modified TO-15 NA NA06B Lab Blank Modified TO-15 NA NA06C Lab Blank Modified TO-15 NA NA06D Lab Blank Modified TO-15 NA NA07A CCV Modified TO-15 NA NA07B CCV Modified TO-15 NA NA07C CCV Modified TO-15 NA NA07D CCV Modified TO-15 NA NA08A LCS Modified TO-15 NA NA08B LCS Modified TO-15 NA NA08C LCS Modified TO-15 NA NA


Page 2 of 39

Continued on next page



CLIENT: BILL TO:

PHONE:


503-924-4704x113

503-924-470712/04/2009


P.O. #


Work Order Summary

FAX:



PRESSUREFINAL

08D LCS Modified TO-15 NA NA

CERTIFIED BY:

Laboratory Director

DATE:



12/21/09

Page 3 of 39







Four 6 Liter Summa Canister (SIM Certified) samples were received on December 04, 2009. The laboratory performed analysis via modified EPA Method TO-15 using GC/MS in the Full Scan and SIMacquisition modes. The method involves concentrating up to 1.0 liters of air. The concentrated aliquot is then flash vaporized and swept through a water management system to remove water vapor. Following dehumidification, the sample passes directly into the GC/MS for analysis.












Receiving Notes


Samples DEEP PRECARBON-120309 and SHALLOW PRECARBON-120309 were transferred fromSIM/Low Level analysis to full scan TO-15 due to high levels of target compounds.

Analytical Notes

Page 4 of 39


The Laboratory Control Spikes (LCS) did not meet acceptance criteria for Ethanol. Recovery for thiscompound was (>150%). Results are reported as estimated.




Page 5 of 39



Lab ID#: 0912120B-01A


240 290 1400 1600Freon 11240 2100 860 7500Hexane240 5300 960 21000cis-1,2-Dichloroethene240 630 1300 34001,1,1-Trichloroethane240 2000 840 6800Cyclohexane240 710 1100 33002,2,4-Trimethylpentane240 370 780 1200Benzene240 4000 1000 17000Heptane240 8800 1300 47000Trichloroethene240 5900 920 22000Toluene240 65000 1600 440000Tetrachloroethene240 610 1000 2700m,p-Xylene


Lab ID#: 0912120B-02A


1.5 3.8 3.8 10Chloroethane7.3 79 J 14 150 JEthanol7.3 21 17 51Acetone7.3 110 18 2802-Propanol1.5 2.2 5.1 7.8Hexane1.5 2.0 6.0 8.1Heptane1.5 3.1 7.2 154-Ethyltoluene1.5 1.8 7.2 8.81,3,5-Trimethylbenzene1.5 7.7 7.2 381,2,4-Trimethylbenzene


Lab ID#: 0912120B-02B


0.15 190 0.37 480Vinyl Chloride0.29 0.57 1.6 3.0Trichloroethene0.29 1.1 1.1 4.2Toluene0.29 0.74 1.3 3.2Ethyl Benzene

Page 6 of 39



Lab ID#: 0912120B-02B0.58 2.9 2.5 12m,p-Xylene0.29 1.4 1.3 6.3o-Xylene


Lab ID#: 0912120B-04A


220 220 J 530 520 JAcetone56 130 220 510cis-1,2-Dichloroethene56 120 300 6301,1,1-Trichloroethane56 150 230 610Heptane56 700 300 3800Trichloroethene56 75 230 3104-Methyl-2-pentanone56 20000 380 140000Tetrachloroethene


Lab ID#: 0912120B-05A


0.15 0.42 0.72 2.1Freon 120.15 0.15 0.30 0.31Chloromethane0.73 17 J 1.4 32 JEthanol0.73 23 1.7 55Acetone0.73 44 1.8 1102-Propanol0.15 2.0 0.51 7.0Hexane0.15 0.58 0.43 1.72-Butanone (Methyl Ethyl Ketone)0.15 1.5 0.60 6.3Heptane0.15 0.25 0.62 1.0Styrene0.15 0.23 0.72 1.1Cumene0.15 0.78 0.72 3.8Propylbenzene0.15 3.3 0.72 164-Ethyltoluene0.15 1.6 0.72 8.11,3,5-Trimethylbenzene0.15 6.9 0.72 341,2,4-Trimethylbenzene0.15 0.17 0.88 1.01,3-Dichlorobenzene


Lab ID#: 0912120B-05B

Page 7 of 39



Lab ID#: 0912120B-05B


0.015 0.26 0.037 0.67Vinyl Chloride0.073 0.10 0.23 0.32Benzene0.029 0.86 0.11 3.2Toluene0.029 0.042 0.20 0.29Tetrachloroethene0.029 0.68 0.13 3.0Ethyl Benzene0.058 2.9 0.25 12m,p-Xylene0.029 1.4 0.13 6.2o-Xylene

Page 8 of 39


Lab ID#: 0912120B-01A





240 Not Detected 1200 Not DetectedFreon 12240 Not Detected 1700 Not DetectedFreon 114970 Not Detected 2000 Not DetectedChloromethane240 Not Detected 620 Not DetectedVinyl Chloride240 Not Detected 540 Not Detected1,3-Butadiene240 Not Detected 940 Not DetectedBromomethane240 Not Detected 640 Not DetectedChloroethane240 290 1400 1600Freon 11970 Not Detected 1800 Not DetectedEthanol240 Not Detected 1900 Not DetectedFreon 113240 Not Detected 960 Not Detected1,1-Dichloroethene970 Not Detected 2300 Not DetectedAcetone970 Not Detected 2400 Not Detected2-Propanol240 Not Detected 760 Not DetectedCarbon Disulfide970 Not Detected 3000 Not Detected3-Chloropropene240 Not Detected 840 Not DetectedMethylene Chloride240 Not Detected 880 Not DetectedMethyl tert-butyl ether240 Not Detected 960 Not Detectedtrans-1,2-Dichloroethene240 2100 860 7500Hexane240 Not Detected 980 Not Detected1,1-Dichloroethane240 Not Detected 720 Not Detected2-Butanone (Methyl Ethyl Ketone)240 5300 960 21000cis-1,2-Dichloroethene240 Not Detected 720 Not DetectedTetrahydrofuran240 Not Detected 1200 Not DetectedChloroform240 630 1300 34001,1,1-Trichloroethane240 2000 840 6800Cyclohexane240 Not Detected 1500 Not DetectedCarbon Tetrachloride240 710 1100 33002,2,4-Trimethylpentane240 370 780 1200Benzene240 Not Detected 980 Not Detected1,2-Dichloroethane240 4000 1000 17000Heptane240 8800 1300 47000Trichloroethene240 Not Detected 1100 Not Detected1,2-Dichloropropane970 Not Detected 3500 Not Detected1,4-Dioxane240 Not Detected 1600 Not DetectedBromodichloromethane240 Not Detected 1100 Not Detectedcis-1,3-Dichloropropene240 Not Detected 1000 Not Detected4-Methyl-2-pentanone240 5900 920 22000Toluene240 Not Detected 1100 Not Detectedtrans-1,3-Dichloropropene

Page 9 of 39


Lab ID#: 0912120B-01A





240 Not Detected 1300 Not Detected1,1,2-Trichloroethane240 65000 1600 440000Tetrachloroethene970 Not Detected 4000 Not Detected2-Hexanone240 Not Detected 2100 Not DetectedDibromochloromethane240 Not Detected 1900 Not Detected1,2-Dibromoethane (EDB)240 Not Detected 1100 Not DetectedChlorobenzene240 Not Detected 1000 Not DetectedEthyl Benzene240 610 1000 2700m,p-Xylene240 Not Detected 1000 Not Detectedo-Xylene240 Not Detected 1000 Not DetectedStyrene240 Not Detected 2500 Not DetectedBromoform240 Not Detected 1200 Not DetectedCumene240 Not Detected 1700 Not Detected1,1,2,2-Tetrachloroethane240 Not Detected 1200 Not DetectedPropylbenzene240 Not Detected 1200 Not Detected4-Ethyltoluene240 Not Detected 1200 Not Detected1,3,5-Trimethylbenzene240 Not Detected 1200 Not Detected1,2,4-Trimethylbenzene240 Not Detected 1500 Not Detected1,3-Dichlorobenzene240 Not Detected 1500 Not Detected1,4-Dichlorobenzene240 Not Detected 1300 Not Detectedalpha-Chlorotoluene240 Not Detected 1500 Not Detected1,2-Dichlorobenzene970 Not Detected 7200 Not Detected1,2,4-Trichlorobenzene970 Not Detected 10000 Not DetectedHexachlorobutadiene




Page 10 of 39


Lab ID#: 0912120B-02A





1.5 Not Detected 7.2 Not DetectedFreon 121.5 Not Detected 10 Not DetectedFreon 1141.5 Not Detected 3.0 Not DetectedChloromethane1.5 Not Detected 3.2 Not Detected1,3-Butadiene1.5 Not Detected 5.7 Not DetectedBromomethane1.5 3.8 3.8 10Chloroethane1.5 Not Detected 8.2 Not DetectedFreon 117.3 79 J 14 150 JEthanol1.5 Not Detected 11 Not DetectedFreon 1137.3 21 17 51Acetone7.3 110 18 2802-Propanol7.3 Not Detected 23 Not DetectedCarbon Disulfide7.3 Not Detected 23 Not Detected3-Chloropropene2.9 Not Detected 10 Not DetectedMethylene Chloride1.5 2.2 5.1 7.8Hexane1.5 Not Detected 4.3 Not Detected2-Butanone (Methyl Ethyl Ketone)7.3 Not Detected 22 Not DetectedTetrahydrofuran1.5 Not Detected 7.1 Not DetectedChloroform1.5 Not Detected 5.0 Not DetectedCyclohexane1.5 Not Detected 9.2 Not DetectedCarbon Tetrachloride7.3 Not Detected 34 Not Detected2,2,4-Trimethylpentane1.5 2.0 6.0 8.1Heptane1.5 Not Detected 6.7 Not Detected1,2-Dichloropropane1.5 Not Detected 5.3 Not Detected1,4-Dioxane1.5 Not Detected 9.8 Not DetectedBromodichloromethane1.5 Not Detected 6.6 Not Detectedcis-1,3-Dichloropropene1.5 Not Detected 6.0 Not Detected4-Methyl-2-pentanone1.5 Not Detected 6.6 Not Detectedtrans-1,3-Dichloropropene7.3 Not Detected 30 Not Detected2-Hexanone1.5 Not Detected 12 Not DetectedDibromochloromethane1.5 Not Detected 11 Not Detected1,2-Dibromoethane (EDB)1.5 Not Detected 6.7 Not DetectedChlorobenzene1.5 Not Detected 6.2 Not DetectedStyrene1.5 Not Detected 15 Not DetectedBromoform1.5 Not Detected 7.2 Not DetectedCumene1.5 Not Detected 7.2 Not DetectedPropylbenzene1.5 3.1 7.2 154-Ethyltoluene1.5 1.8 7.2 8.81,3,5-Trimethylbenzene1.5 7.7 7.2 381,2,4-Trimethylbenzene

Page 11 of 39


Lab ID#: 0912120B-02A






J = Estimated value.Container Type: 6 Liter Summa Canister (SIM Certified)



Page 12 of 39


Lab ID#: 0912120B-02B





0.15 190 0.37 480Vinyl Chloride0.15 Not Detected 0.58 Not Detected1,1-Dichloroethene0.29 Not Detected 1.2 Not Detected1,1-Dichloroethane0.29 Not Detected 1.2 Not Detectedcis-1,2-Dichloroethene0.29 Not Detected 1.6 Not Detected1,1,1-Trichloroethane0.73 Not Detected 2.3 Not DetectedBenzene0.29 Not Detected 1.2 Not Detected1,2-Dichloroethane0.29 0.57 1.6 3.0Trichloroethene0.29 1.1 1.1 4.2Toluene0.29 Not Detected 1.6 Not Detected1,1,2-Trichloroethane0.29 Not Detected 2.0 Not DetectedTetrachloroethene0.29 0.74 1.3 3.2Ethyl Benzene0.58 2.9 2.5 12m,p-Xylene0.29 1.4 1.3 6.3o-Xylene0.29 Not Detected 2.0 Not Detected1,1,2,2-Tetrachloroethane1.5 Not Detected 5.8 Not Detectedtrans-1,2-Dichloroethene1.5 Not Detected 5.3 Not DetectedMethyl tert-butyl ether




Page 13 of 39


Lab ID#: 0912120B-04A





56 Not Detected 270 Not DetectedFreon 1256 Not Detected 390 Not DetectedFreon 114220 Not Detected 460 Not DetectedChloromethane56 Not Detected 140 Not DetectedVinyl Chloride56 Not Detected 120 Not Detected1,3-Butadiene56 Not Detected 220 Not DetectedBromomethane56 Not Detected 150 Not DetectedChloroethane56 Not Detected 310 Not DetectedFreon 11220 Not Detected 420 Not DetectedEthanol56 Not Detected 420 Not DetectedFreon 11356 Not Detected 220 Not Detected1,1-Dichloroethene220 220 J 530 520 JAcetone220 Not Detected 540 Not Detected2-Propanol56 Not Detected 170 Not DetectedCarbon Disulfide220 Not Detected 690 Not Detected3-Chloropropene56 Not Detected 190 Not DetectedMethylene Chloride56 Not Detected 200 Not DetectedMethyl tert-butyl ether56 Not Detected 220 Not Detectedtrans-1,2-Dichloroethene56 Not Detected 200 Not DetectedHexane56 Not Detected 220 Not Detected1,1-Dichloroethane56 Not Detected 160 Not Detected2-Butanone (Methyl Ethyl Ketone)56 130 220 510cis-1,2-Dichloroethene56 Not Detected 160 Not DetectedTetrahydrofuran56 Not Detected 270 Not DetectedChloroform56 120 300 6301,1,1-Trichloroethane56 Not Detected 190 Not DetectedCyclohexane56 Not Detected 350 Not DetectedCarbon Tetrachloride56 Not Detected 260 Not Detected2,2,4-Trimethylpentane56 Not Detected 180 Not DetectedBenzene56 Not Detected 220 Not Detected1,2-Dichloroethane56 150 230 610Heptane56 700 300 3800Trichloroethene56 Not Detected 260 Not Detected1,2-Dichloropropane220 Not Detected 800 Not Detected1,4-Dioxane56 Not Detected 370 Not DetectedBromodichloromethane56 Not Detected 250 Not Detectedcis-1,3-Dichloropropene56 75 230 3104-Methyl-2-pentanone56 Not Detected 210 Not DetectedToluene56 Not Detected 250 Not Detectedtrans-1,3-Dichloropropene

Page 14 of 39


Lab ID#: 0912120B-04A





56 Not Detected 300 Not Detected1,1,2-Trichloroethane56 20000 380 140000Tetrachloroethene220 Not Detected 910 Not Detected2-Hexanone56 Not Detected 470 Not DetectedDibromochloromethane56 Not Detected 430 Not Detected1,2-Dibromoethane (EDB)56 Not Detected 260 Not DetectedChlorobenzene56 Not Detected 240 Not DetectedEthyl Benzene56 Not Detected 240 Not Detectedm,p-Xylene56 Not Detected 240 Not Detectedo-Xylene56 Not Detected 240 Not DetectedStyrene56 Not Detected 570 Not DetectedBromoform56 Not Detected 270 Not DetectedCumene56 Not Detected 380 Not Detected1,1,2,2-Tetrachloroethane56 Not Detected 270 Not DetectedPropylbenzene56 Not Detected 270 Not Detected4-Ethyltoluene56 Not Detected 270 Not Detected1,3,5-Trimethylbenzene56 Not Detected 270 Not Detected1,2,4-Trimethylbenzene56 Not Detected 330 Not Detected1,3-Dichlorobenzene56 Not Detected 330 Not Detected1,4-Dichlorobenzene56 Not Detected 290 Not Detectedalpha-Chlorotoluene56 Not Detected 330 Not Detected1,2-Dichlorobenzene220 Not Detected 1600 Not Detected1,2,4-Trichlorobenzene220 Not Detected 2400 Not DetectedHexachlorobutadiene




Page 15 of 39


Lab ID#: 0912120B-05A





0.15 0.42 0.72 2.1Freon 120.15 Not Detected 1.0 Not DetectedFreon 1140.15 0.15 0.30 0.31Chloromethane0.15 Not Detected 0.32 Not Detected1,3-Butadiene0.15 Not Detected 0.57 Not DetectedBromomethane0.15 Not Detected 0.38 Not DetectedChloroethane0.15 Not Detected 0.82 Not DetectedFreon 110.73 17 J 1.4 32 JEthanol0.15 Not Detected 1.1 Not DetectedFreon 1130.73 23 1.7 55Acetone0.73 44 1.8 1102-Propanol0.73 Not Detected 2.3 Not DetectedCarbon Disulfide0.73 Not Detected 2.3 Not Detected3-Chloropropene0.29 Not Detected 1.0 Not DetectedMethylene Chloride0.15 2.0 0.51 7.0Hexane0.15 0.58 0.43 1.72-Butanone (Methyl Ethyl Ketone)0.73 Not Detected 2.2 Not DetectedTetrahydrofuran0.15 Not Detected 0.71 Not DetectedChloroform0.15 Not Detected 0.50 Not DetectedCyclohexane0.15 Not Detected 0.92 Not DetectedCarbon Tetrachloride0.73 Not Detected 3.4 Not Detected2,2,4-Trimethylpentane0.15 1.5 0.60 6.3Heptane0.15 Not Detected 0.67 Not Detected1,2-Dichloropropane0.15 Not Detected 0.53 Not Detected1,4-Dioxane0.15 Not Detected 0.98 Not DetectedBromodichloromethane0.15 Not Detected 0.66 Not Detectedcis-1,3-Dichloropropene0.15 Not Detected 0.60 Not Detected4-Methyl-2-pentanone0.15 Not Detected 0.66 Not Detectedtrans-1,3-Dichloropropene0.73 Not Detected 3.0 Not Detected2-Hexanone0.15 Not Detected 1.2 Not DetectedDibromochloromethane0.15 Not Detected 1.1 Not Detected1,2-Dibromoethane (EDB)0.15 Not Detected 0.67 Not DetectedChlorobenzene0.15 0.25 0.62 1.0Styrene0.15 Not Detected 1.5 Not DetectedBromoform0.15 0.23 0.72 1.1Cumene0.15 0.78 0.72 3.8Propylbenzene0.15 3.3 0.72 164-Ethyltoluene0.15 1.6 0.72 8.11,3,5-Trimethylbenzene0.15 6.9 0.72 341,2,4-Trimethylbenzene

Page 16 of 39


Lab ID#: 0912120B-05A









Page 17 of 39


Lab ID#: 0912120B-05B





0.015 0.26 0.037 0.67Vinyl Chloride0.015 Not Detected 0.058 Not Detected1,1-Dichloroethene0.029 Not Detected 0.12 Not Detected1,1-Dichloroethane0.029 Not Detected 0.12 Not Detectedcis-1,2-Dichloroethene0.029 Not Detected 0.16 Not Detected1,1,1-Trichloroethane0.073 0.10 0.23 0.32Benzene0.029 Not Detected 0.12 Not Detected1,2-Dichloroethane0.029 Not Detected 0.16 Not DetectedTrichloroethene0.029 0.86 0.11 3.2Toluene0.029 Not Detected 0.16 Not Detected1,1,2-Trichloroethane0.029 0.042 0.20 0.29Tetrachloroethene0.029 0.68 0.13 3.0Ethyl Benzene0.058 2.9 0.25 12m,p-Xylene0.029 1.4 0.13 6.2o-Xylene0.029 Not Detected 0.20 Not Detected1,1,2,2-Tetrachloroethane0.15 Not Detected 0.58 Not Detectedtrans-1,2-Dichloroethene0.15 Not Detected 0.53 Not DetectedMethyl tert-butyl ether




Page 18 of 39


Lab ID#: 0912120B-06A






Page 19 of 39


Lab ID#: 0912120B-06A









Page 20 of 39


Lab ID#: 0912120B-06B






Page 21 of 39


Lab ID#: 0912120B-06B









Page 22 of 39


Lab ID#: 0912120B-06C






Page 23 of 39


Lab ID#: 0912120B-06C









Page 24 of 39


Lab ID#: 0912120B-06D









Page 25 of 39


Lab ID#: 0912120B-07A




%RecoveryCompound


Page 26 of 39


Lab ID#: 0912120B-07A




%RecoveryCompound





Page 27 of 39


Lab ID#: 0912120B-07B




%RecoveryCompound


Page 28 of 39


Lab ID#: 0912120B-07B




%RecoveryCompound





Page 29 of 39


Lab ID#: 0912120B-07C




%RecoveryCompound


Page 30 of 39


Lab ID#: 0912120B-07C




%RecoveryCompound





Page 31 of 39


Lab ID#: 0912120B-07D




%RecoveryCompound





Page 32 of 39


Lab ID#: 0912120B-08A




%RecoveryCompound



Page 33 of 39


Lab ID#: 0912120B-08A




%RecoveryCompound





Page 34 of 39


Lab ID#: 0912120B-08B




%RecoveryCompound



Page 35 of 39


Lab ID#: 0912120B-08B




%RecoveryCompound





Page 36 of 39


Lab ID#: 0912120B-08C




%RecoveryCompound



Page 37 of 39


Lab ID#: 0912120B-08C




%RecoveryCompound





Page 38 of 39


Lab ID#: 0912120B-08D




%RecoveryCompound





Page 39 of 39


Project Name: Tarr SVE IRAMProject #: 1073-06





Regards,







CLIENT: BILL TO:

PHONE:


503-924-4704x113

503-924-470712/12/2009


P.O. #

PROJECT # 1073-06 Tarr SVE IRAM

Work Order Summary

FAX:



PRESSUREFINAL

02A DEEP POSTCARBON-121109 Modified TO-15 1.5 "Hg 5 psi02B DEEP POSTCARBON-121109 Modified TO-15 1.5 "Hg 5 psi04A SHALLOW POSTCARBON-121109 Modified TO-15 1.0 "Hg 5 psi04B SHALLOW POSTCARBON-121109 Modified TO-15 1.0 "Hg 5 psi05A Lab Blank Modified TO-15 NA NA05B Lab Blank Modified TO-15 NA NA05C Lab Blank Modified TO-15 NA NA05D Lab Blank Modified TO-15 NA NA06A CCV Modified TO-15 NA NA06B CCV Modified TO-15 NA NA06C CCV Modified TO-15 NA NA06D CCV Modified TO-15 NA NA07A LCS Modified TO-15 NA NA07B LCS Modified TO-15 NA NA07C LCS Modified TO-15 NA NA07D LCS Modified TO-15 NA NA

CERTIFIED BY:

Laboratory Director

DATE:



12/21/09

Page 2 of 30







Two 6 Liter Summa Canister (SIM Certified) samples were received on December 12, 2009. The laboratory performed analysis via modified EPA Method TO-15 using GC/MS in the Full Scan and SIM acquisition modes. The method involves concentrating up to 1.0 liters of air. The concentrated aliquot is then flash vaporized and swept through a water management system to remove water vapor. Following dehumidification, the sample passes directly into the GC/MS for analysis.












Receiving Notes

The Chain of Custody (COC) was not relinquished properly. An incomplete date was not provided by the field sampler.


Page 3 of 30


The Laboratory Control Spikes (LCS) did not meet acceptance criteria for Ethanol on 12/17/09 and 12/18/09. Recoveries for this compound were 155% and 152% respectively. Results are reported asestimated.


Analytical Notes




Page 4 of 30



Lab ID#: 0912310A-02A


0.14 0.34 0.29 0.71Chloromethane0.70 9.5 J 1.3 18 JEthanol0.70 10 1.7 24Acetone0.70 23 1.7 562-Propanol0.14 0.97 0.50 3.4Hexane0.14 0.36 0.42 1.12-Butanone (Methyl Ethyl Ketone)0.14 0.26 0.48 0.89Cyclohexane0.14 0.61 0.58 2.5Heptane0.14 0.16 0.60 0.66Styrene0.14 0.34 0.69 1.7Propylbenzene0.14 1.6 0.69 7.84-Ethyltoluene0.14 0.79 0.69 3.91,3,5-Trimethylbenzene0.14 3.2 0.69 161,2,4-Trimethylbenzene0.14 0.28 0.85 1.71,3-Dichlorobenzene


Lab ID#: 0912310A-02B


0.014 1.2 0.036 3.0Vinyl Chloride0.028 0.060 0.11 0.24cis-1,2-Dichloroethene0.028 0.034 0.15 0.181,1,1-Trichloroethane0.070 0.074 0.22 0.24Benzene0.028 0.24 0.15 1.3Trichloroethene0.028 0.66 0.11 2.5Toluene0.028 2.2 0.19 15Tetrachloroethene0.028 0.35 0.12 1.5Ethyl Benzene0.056 1.4 0.24 6.3m,p-Xylene0.028 0.69 0.12 3.0o-Xylene


Lab ID#: 0912310A-04A


0.14 0.18 0.29 0.38Chloromethane0.70 11 J 1.3 20 JEthanol

Page 5 of 30



Lab ID#: 0912310A-04A0.70 10 1.6 24Acetone0.70 26 1.7 632-Propanol0.14 0.96 0.49 3.4Hexane0.14 0.64 0.41 1.92-Butanone (Methyl Ethyl Ketone)0.14 0.22 0.48 0.76Cyclohexane0.14 0.64 0.57 2.6Heptane0.14 0.14 0.59 0.61Styrene0.14 0.15 0.68 0.73Cumene0.14 0.41 0.68 2.0Propylbenzene0.14 1.7 0.68 8.54-Ethyltoluene0.14 0.88 0.68 4.31,3,5-Trimethylbenzene0.14 3.6 0.68 181,2,4-Trimethylbenzene0.14 0.29 0.84 1.71,3-Dichlorobenzene


Lab ID#: 0912310A-04B


0.014 0.20 0.036 0.51Vinyl Chloride0.028 0.072 0.15 0.39Trichloroethene0.028 0.69 0.10 2.6Toluene0.028 1.3 0.19 8.6Tetrachloroethene0.028 0.36 0.12 1.6Ethyl Benzene0.056 1.4 0.24 6.3m,p-Xylene0.028 0.71 0.12 3.1o-Xylene

Page 6 of 30

Client Sample ID: DEEP POSTCARBON-121109Lab ID#: 0912310A-02A



Date of Collection: 12/11/09 12:56:00 PDate of Analysis: 12/18/09 11:36 AM


0.14 Not Detected 0.70 Not DetectedFreon 120.14 Not Detected 0.98 Not DetectedFreon 1140.14 0.34 0.29 0.71Chloromethane0.14 Not Detected 0.31 Not Detected1,3-Butadiene0.14 Not Detected 0.55 Not DetectedBromomethane0.14 Not Detected 0.37 Not DetectedChloroethane0.14 Not Detected 0.79 Not DetectedFreon 110.70 9.5 J 1.3 18 JEthanol0.14 Not Detected 1.1 Not DetectedFreon 1130.70 10 1.7 24Acetone0.70 23 1.7 562-Propanol0.70 Not Detected 2.2 Not DetectedCarbon Disulfide0.70 Not Detected 2.2 Not Detected3-Chloropropene0.28 Not Detected 0.98 Not DetectedMethylene Chloride0.14 0.97 0.50 3.4Hexane0.14 0.36 0.42 1.12-Butanone (Methyl Ethyl Ketone)0.70 Not Detected 2.1 Not DetectedTetrahydrofuran0.14 Not Detected 0.69 Not DetectedChloroform0.14 0.26 0.48 0.89Cyclohexane0.14 Not Detected 0.89 Not DetectedCarbon Tetrachloride0.70 Not Detected 3.3 Not Detected2,2,4-Trimethylpentane0.14 0.61 0.58 2.5Heptane0.14 Not Detected 0.65 Not Detected1,2-Dichloropropane0.14 Not Detected 0.51 Not Detected1,4-Dioxane0.14 Not Detected 0.94 Not DetectedBromodichloromethane0.14 Not Detected 0.64 Not Detectedcis-1,3-Dichloropropene0.14 Not Detected 0.58 Not Detected4-Methyl-2-pentanone0.14 Not Detected 0.64 Not Detectedtrans-1,3-Dichloropropene0.70 Not Detected 2.9 Not Detected2-Hexanone0.14 Not Detected 1.2 Not DetectedDibromochloromethane0.14 Not Detected 1.1 Not Detected1,2-Dibromoethane (EDB)0.14 Not Detected 0.65 Not DetectedChlorobenzene0.14 0.16 0.60 0.66Styrene0.14 Not Detected 1.4 Not DetectedBromoform0.14 Not Detected 0.69 Not DetectedCumene0.14 0.34 0.69 1.7Propylbenzene0.14 1.6 0.69 7.84-Ethyltoluene0.14 0.79 0.69 3.91,3,5-Trimethylbenzene0.14 3.2 0.69 161,2,4-Trimethylbenzene

Page 7 of 30

Client Sample ID: DEEP POSTCARBON-121109Lab ID#: 0912310A-02A










Page 8 of 30

Client Sample ID: DEEP POSTCARBON-121109Lab ID#: 0912310A-02B





0.014 1.2 0.036 3.0Vinyl Chloride0.014 Not Detected 0.056 Not Detected1,1-Dichloroethene0.028 Not Detected 0.11 Not Detected1,1-Dichloroethane0.028 0.060 0.11 0.24cis-1,2-Dichloroethene0.028 0.034 0.15 0.181,1,1-Trichloroethane0.070 0.074 0.22 0.24Benzene0.028 Not Detected 0.11 Not Detected1,2-Dichloroethane0.028 0.24 0.15 1.3Trichloroethene0.028 0.66 0.11 2.5Toluene0.028 Not Detected 0.15 Not Detected1,1,2-Trichloroethane0.028 2.2 0.19 15Tetrachloroethene0.028 0.35 0.12 1.5Ethyl Benzene0.056 1.4 0.24 6.3m,p-Xylene0.028 0.69 0.12 3.0o-Xylene0.028 Not Detected 0.19 Not Detected1,1,2,2-Tetrachloroethane0.14 Not Detected 0.56 Not Detectedtrans-1,2-Dichloroethene0.14 Not Detected 0.51 Not DetectedMethyl tert-butyl ether





Page 9 of 30

Client Sample ID: SHALLOW POSTCARBON-121109Lab ID#: 0912310A-04A





0.14 Not Detected 0.69 Not DetectedFreon 120.14 Not Detected 0.97 Not DetectedFreon 1140.14 0.18 0.29 0.38Chloromethane0.14 Not Detected 0.31 Not Detected1,3-Butadiene0.14 Not Detected 0.54 Not DetectedBromomethane0.14 Not Detected 0.37 Not DetectedChloroethane0.14 Not Detected 0.78 Not DetectedFreon 110.70 11 J 1.3 20 JEthanol0.14 Not Detected 1.1 Not DetectedFreon 1130.70 10 1.6 24Acetone0.70 26 1.7 632-Propanol0.70 Not Detected 2.2 Not DetectedCarbon Disulfide0.70 Not Detected 2.2 Not Detected3-Chloropropene0.28 Not Detected 0.96 Not DetectedMethylene Chloride0.14 0.96 0.49 3.4Hexane0.14 0.64 0.41 1.92-Butanone (Methyl Ethyl Ketone)0.70 Not Detected 2.0 Not DetectedTetrahydrofuran0.14 Not Detected 0.68 Not DetectedChloroform0.14 0.22 0.48 0.76Cyclohexane0.14 Not Detected 0.87 Not DetectedCarbon Tetrachloride0.70 Not Detected 3.2 Not Detected2,2,4-Trimethylpentane0.14 0.64 0.57 2.6Heptane0.14 Not Detected 0.64 Not Detected1,2-Dichloropropane0.14 Not Detected 0.50 Not Detected1,4-Dioxane0.14 Not Detected 0.93 Not DetectedBromodichloromethane0.14 Not Detected 0.63 Not Detectedcis-1,3-Dichloropropene0.14 Not Detected 0.57 Not Detected4-Methyl-2-pentanone0.14 Not Detected 0.63 Not Detectedtrans-1,3-Dichloropropene0.70 Not Detected 2.8 Not Detected2-Hexanone0.14 Not Detected 1.2 Not DetectedDibromochloromethane0.14 Not Detected 1.1 Not Detected1,2-Dibromoethane (EDB)0.14 Not Detected 0.64 Not DetectedChlorobenzene0.14 0.14 0.59 0.61Styrene0.14 Not Detected 1.4 Not DetectedBromoform0.14 0.15 0.68 0.73Cumene0.14 0.41 0.68 2.0Propylbenzene0.14 1.7 0.68 8.54-Ethyltoluene0.14 0.88 0.68 4.31,3,5-Trimethylbenzene0.14 3.6 0.68 181,2,4-Trimethylbenzene

Page 10 of 30

Client Sample ID: SHALLOW POSTCARBON-121109Lab ID#: 0912310A-04A










Page 11 of 30

Client Sample ID: SHALLOW POSTCARBON-121109Lab ID#: 0912310A-04B





0.014 0.20 0.036 0.51Vinyl Chloride0.014 Not Detected 0.055 Not Detected1,1-Dichloroethene0.028 Not Detected 0.11 Not Detected1,1-Dichloroethane0.028 Not Detected 0.11 Not Detectedcis-1,2-Dichloroethene0.028 Not Detected 0.15 Not Detected1,1,1-Trichloroethane0.070 Not Detected 0.22 Not DetectedBenzene0.028 Not Detected 0.11 Not Detected1,2-Dichloroethane0.028 0.072 0.15 0.39Trichloroethene0.028 0.69 0.10 2.6Toluene0.028 Not Detected 0.15 Not Detected1,1,2-Trichloroethane0.028 1.3 0.19 8.6Tetrachloroethene0.028 0.36 0.12 1.6Ethyl Benzene0.056 1.4 0.24 6.3m,p-Xylene0.028 0.71 0.12 3.1o-Xylene0.028 Not Detected 0.19 Not Detected1,1,2,2-Tetrachloroethane0.14 Not Detected 0.55 Not Detectedtrans-1,2-Dichloroethene0.14 Not Detected 0.50 Not DetectedMethyl tert-butyl ether





Page 12 of 30







Page 13 of 30











Page 14 of 30

Client Sample ID: Lab BlankLab ID#: 0912310A-05B










Page 15 of 30







Page 16 of 30











Page 17 of 30

Client Sample ID: Lab BlankLab ID#: 0912310A-05D










Page 18 of 30





%RecoveryCompound

98Freon 12102Freon 11495Chloromethane


110Ethanol102Freon 113110Acetone1102-Propanol109Carbon Disulfide1133-Chloropropene96Methylene Chloride

102Hexane1112-Butanone (Methyl Ethyl Ketone)110Tetrahydrofuran100Chloroform101Cyclohexane99Carbon Tetrachloride

1062,2,4-Trimethylpentane103Heptane1021,2-Dichloropropane1081,4-Dioxane104Bromodichloromethane106cis-1,3-Dichloropropene1114-Methyl-2-pentanone105trans-1,3-Dichloropropene1162-Hexanone110Dibromochloromethane1031,2-Dibromoethane (EDB)100Chlorobenzene114Styrene113Bromoform106Cumene106Propylbenzene1104-Ethyltoluene1071,3,5-Trimethylbenzene1061,2,4-Trimethylbenzene

Page 19 of 30





%RecoveryCompound


115alpha-Chlorotoluene1051,2-Dichlorobenzene1231,2,4-Trichlorobenzene109Hexachlorobutadiene




Page 20 of 30

Client Sample ID: CCVLab ID#: 0912310A-06B




%RecoveryCompound


1001,1-Dichloroethane102cis-1,2-Dichloroethene981,1,1-Trichloroethane97Benzene941,2-Dichloroethane98Trichloroethene96Toluene

1001,1,2-Trichloroethane92Tetrachloroethene99Ethyl Benzene

101m,p-Xylene103o-Xylene971,1,2,2-Tetrachloroethane

100trans-1,2-Dichloroethene103Methyl tert-butyl ether




Page 21 of 30





%RecoveryCompound

95Freon 1299Freon 11492Chloromethane


114Ethanol100Freon 113115Acetone1082-Propanol108Carbon Disulfide1103-Chloropropene96Methylene Chloride

102Hexane1122-Butanone (Methyl Ethyl Ketone)108Tetrahydrofuran98Chloroform

100Cyclohexane96Carbon Tetrachloride

1062,2,4-Trimethylpentane104Heptane1031,2-Dichloropropane1061,4-Dioxane101Bromodichloromethane105cis-1,3-Dichloropropene1114-Methyl-2-pentanone102trans-1,3-Dichloropropene1142-Hexanone109Dibromochloromethane1011,2-Dibromoethane (EDB)98Chlorobenzene

109Styrene111Bromoform102Cumene103Propylbenzene1054-Ethyltoluene1001,3,5-Trimethylbenzene971,2,4-Trimethylbenzene

Page 22 of 30





%RecoveryCompound


112alpha-Chlorotoluene991,2-Dichlorobenzene

1121,2,4-Trichlorobenzene108Hexachlorobutadiene




Page 23 of 30

Client Sample ID: CCVLab ID#: 0912310A-06D




%RecoveryCompound

97Vinyl Chloride981,1-Dichloroethene981,1-Dichloroethane

101cis-1,2-Dichloroethene951,1,1-Trichloroethane96Benzene901,2-Dichloroethane96Trichloroethene93Toluene991,1,2-Trichloroethane92Tetrachloroethene96Ethyl Benzene97m,p-Xylene99o-Xylene961,1,2,2-Tetrachloroethane

100trans-1,2-Dichloroethene102Methyl tert-butyl ether




Page 24 of 30





%RecoveryCompound


155 QEthanol77Freon 11393Acetone892-Propanol91Carbon Disulfide953-Chloropropene76Methylene Chloride86Hexane972-Butanone (Methyl Ethyl Ketone)91Tetrahydrofuran83Chloroform85Cyclohexane83Carbon Tetrachloride902,2,4-Trimethylpentane88Heptane881,2-Dichloropropane901,4-Dioxane87Bromodichloromethane91cis-1,3-Dichloropropene954-Methyl-2-pentanone94trans-1,3-Dichloropropene

1062-Hexanone98Dibromochloromethane951,2-Dibromoethane (EDB)89Chlorobenzene

102Styrene101Bromoform91Cumene94Propylbenzene974-Ethyltoluene941,3,5-Trimethylbenzene921,2,4-Trimethylbenzene

Page 25 of 30





%RecoveryCompound

871,3-Dichlorobenzene861,4-Dichlorobenzene99alpha-Chlorotoluene921,2-Dichlorobenzene





Page 26 of 30

Client Sample ID: LCSLab ID#: 0912310A-07B




%RecoveryCompound






Page 27 of 30





%RecoveryCompound


152 QEthanol74Freon 11392Acetone852-Propanol88Carbon Disulfide923-Chloropropene72Methylene Chloride82Hexane892-Butanone (Methyl Ethyl Ketone)91Tetrahydrofuran77Chloroform82Cyclohexane78Carbon Tetrachloride862,2,4-Trimethylpentane88Heptane861,2-Dichloropropane891,4-Dioxane84Bromodichloromethane88cis-1,3-Dichloropropene934-Methyl-2-pentanone90trans-1,3-Dichloropropene

1022-Hexanone94Dibromochloromethane911,2-Dibromoethane (EDB)87Chlorobenzene99Styrene97Bromoform90Cumene91Propylbenzene954-Ethyltoluene901,3,5-Trimethylbenzene891,2,4-Trimethylbenzene

Page 28 of 30





%RecoveryCompound






Page 29 of 30

Client Sample ID: LCSLab ID#: 0912310A-07D




%RecoveryCompound






Page 30 of 30


Project Name: Tarr SVE IRAMProject #: 1073-06





Regards,


Workorder #: 0912492




WORK ORDER #: 0912492

CLIENT: BILL TO:

PHONE:


503-924-4704x113

503-924-470712/19/2009


P.O. #

PROJECT # 1073-06 Tarr SVE IRAM

Work Order Summary

FAX:



PRESSUREFINAL

01A SHALLOW POST CARBON-121809 Modified TO-15 2.0 "Hg 5 psi01B SHALLOW POST CARBON-121809 Modified TO-15 2.0 "Hg 5 psi02A DEEP POSTCARBON-121809 Modified TO-15 2.0 "Hg 5 psi02B DEEP POSTCARBON-121809 Modified TO-15 2.0 "Hg 5 psi03A Lab Blank Modified TO-15 NA NA03B Lab Blank Modified TO-15 NA NA04A CCV Modified TO-15 NA NA04B CCV Modified TO-15 NA NA05A LCS Modified TO-15 NA NA05B LCS Modified TO-15 NA NA

CERTIFIED BY:

Laboratory Director

DATE:



12/28/09

Page 2 of 21





Ash Creek AssociatesWorkorder# 0912492


Two 6 Liter Summa Canister (100% Certified) samples were received on December 19, 2009. The laboratory performed analysis via modified EPA Method TO-15 using GC/MS in the Full Scan and SIM acquisition modes. The method involves concentrating up to 1.0 liters of air. The concentrated aliquot is then flash vaporized and swept through a water management system to remove water vapor. Following dehumidification, the sample passes directly into the GC/MS for analysis.












Receiving Notes



Analytical Notes

Page 3 of 21





Page 4 of 21


Client Sample ID: SHALLOW POST CARBON-121809

Lab ID#: 0912492-01A


0.14 0.46 0.71 2.3Freon 120.14 0.31 0.30 0.65Chloromethane0.72 3.7 1.4 7.0Ethanol0.72 2.9 1.7 6.8Acetone0.72 3.4 1.8 8.42-Propanol0.14 0.68 0.51 2.4Hexane0.14 0.28 0.42 0.822-Butanone (Methyl Ethyl Ketone)0.14 0.22 0.50 0.77Cyclohexane0.14 0.60 0.59 2.5Heptane0.14 0.15 0.61 0.65Styrene0.14 0.16 0.71 0.77Cumene0.14 0.48 0.71 2.4Propylbenzene0.14 2.2 0.71 114-Ethyltoluene0.14 1.2 0.71 5.91,3,5-Trimethylbenzene0.14 5.1 0.71 251,2,4-Trimethylbenzene0.14 0.15 0.86 0.921,4-Dichlorobenzene

Client Sample ID: SHALLOW POST CARBON-121809

Lab ID#: 0912492-01B


0.014 5.7 0.037 14Vinyl Chloride0.029 0.081 0.15 0.44Trichloroethene0.029 0.58 0.11 2.2Toluene0.029 0.96 0.20 6.5Tetrachloroethene0.029 0.36 0.12 1.6Ethyl Benzene0.058 1.6 0.25 6.8m,p-Xylene0.029 0.80 0.12 3.5o-Xylene


Lab ID#: 0912492-02A


0.29 0.40 0.59 0.83Chloromethane1.4 7.5 2.7 14Ethanol1.4 2.7 3.4 6.4Acetone

Page 5 of 21



Lab ID#: 0912492-02A1.4 11 3.5 282-Propanol

0.29 0.94 1.0 3.3Hexane0.29 0.69 1.2 2.8Heptane0.29 0.50 1.4 2.4Propylbenzene0.29 2.0 1.4 9.74-Ethyltoluene0.29 2.4 1.4 121,3,5-Trimethylbenzene0.29 6.8 1.4 341,2,4-Trimethylbenzene0.29 0.47 1.7 2.81,3-Dichlorobenzene


Lab ID#: 0912492-02B


0.029 29 0.074 75Vinyl Chloride0.058 0.12 0.31 0.65Trichloroethene0.058 0.77 0.22 2.9Toluene0.058 1.4 0.39 9.6Tetrachloroethene0.058 0.44 0.25 1.9Ethyl Benzene0.12 1.9 0.50 8.1m,p-Xylene

0.058 0.99 0.25 4.3o-Xylene

Page 6 of 21

Client Sample ID: SHALLOW POST CARBON-121809Lab ID#: 0912492-01A





0.14 0.46 0.71 2.3Freon 120.14 Not Detected 1.0 Not DetectedFreon 1140.14 0.31 0.30 0.65Chloromethane0.14 Not Detected 0.32 Not Detected1,3-Butadiene0.14 Not Detected 0.56 Not DetectedBromomethane0.14 Not Detected 0.38 Not DetectedChloroethane0.14 Not Detected 0.81 Not DetectedFreon 110.72 3.7 1.4 7.0Ethanol0.14 Not Detected 1.1 Not DetectedFreon 1130.72 2.9 1.7 6.8Acetone0.72 3.4 1.8 8.42-Propanol0.72 Not Detected 2.2 Not DetectedCarbon Disulfide0.72 Not Detected 2.2 Not Detected3-Chloropropene0.29 Not Detected 1.0 Not DetectedMethylene Chloride0.14 0.68 0.51 2.4Hexane0.14 0.28 0.42 0.822-Butanone (Methyl Ethyl Ketone)0.72 Not Detected 2.1 Not DetectedTetrahydrofuran0.14 Not Detected 0.70 Not DetectedChloroform0.14 0.22 0.50 0.77Cyclohexane0.14 Not Detected 0.91 Not DetectedCarbon Tetrachloride0.72 Not Detected 3.4 Not Detected2,2,4-Trimethylpentane0.14 0.60 0.59 2.5Heptane0.14 Not Detected 0.66 Not Detected1,2-Dichloropropane0.14 Not Detected 0.52 Not Detected1,4-Dioxane0.14 Not Detected 0.96 Not DetectedBromodichloromethane0.14 Not Detected 0.65 Not Detectedcis-1,3-Dichloropropene0.14 Not Detected 0.59 Not Detected4-Methyl-2-pentanone0.14 Not Detected 0.65 Not Detectedtrans-1,3-Dichloropropene0.72 Not Detected 2.9 Not Detected2-Hexanone0.14 Not Detected 1.2 Not DetectedDibromochloromethane0.14 Not Detected 1.1 Not Detected1,2-Dibromoethane (EDB)0.14 Not Detected 0.66 Not DetectedChlorobenzene0.14 0.15 0.61 0.65Styrene0.14 Not Detected 1.5 Not DetectedBromoform0.14 0.16 0.71 0.77Cumene0.14 0.48 0.71 2.4Propylbenzene0.14 2.2 0.71 114-Ethyltoluene0.14 1.2 0.71 5.91,3,5-Trimethylbenzene0.14 5.1 0.71 251,2,4-Trimethylbenzene

Page 7 of 21

Client Sample ID: SHALLOW POST CARBON-121809Lab ID#: 0912492-01A





0.14 Not Detected 0.86 Not Detected1,3-Dichlorobenzene0.14 0.15 0.86 0.921,4-Dichlorobenzene0.14 Not Detected 0.74 Not Detectedalpha-Chlorotoluene0.14 Not Detected 0.86 Not Detected1,2-Dichlorobenzene0.72 Not Detected 5.3 Not Detected1,2,4-Trichlorobenzene0.72 Not Detected 7.7 Not DetectedHexachlorobutadiene

Container Type: 6 Liter Summa Canister (100% Certified)




Page 8 of 21

Client Sample ID: SHALLOW POST CARBON-121809Lab ID#: 0912492-01B





0.014 5.7 0.037 14Vinyl Chloride0.014 Not Detected 0.057 Not Detected1,1-Dichloroethene0.029 Not Detected 0.12 Not Detected1,1-Dichloroethane0.029 Not Detected 0.11 Not Detectedcis-1,2-Dichloroethene0.029 Not Detected 0.16 Not Detected1,1,1-Trichloroethane0.072 Not Detected 0.23 Not DetectedBenzene0.029 Not Detected 0.12 Not Detected1,2-Dichloroethane0.029 0.081 0.15 0.44Trichloroethene0.029 0.58 0.11 2.2Toluene0.029 Not Detected 0.16 Not Detected1,1,2-Trichloroethane0.029 0.96 0.20 6.5Tetrachloroethene0.029 0.36 0.12 1.6Ethyl Benzene0.058 1.6 0.25 6.8m,p-Xylene0.029 0.80 0.12 3.5o-Xylene0.029 Not Detected 0.20 Not Detected1,1,2,2-Tetrachloroethane0.14 Not Detected 0.57 Not Detectedtrans-1,2-Dichloroethene0.14 Not Detected 0.52 Not DetectedMethyl tert-butyl ether





Page 9 of 21

Client Sample ID: DEEP POSTCARBON-121809Lab ID#: 0912492-02A





0.29 Not Detected 1.4 Not DetectedFreon 120.29 Not Detected 2.0 Not DetectedFreon 1140.29 0.40 0.59 0.83Chloromethane0.29 Not Detected 0.64 Not Detected1,3-Butadiene0.29 Not Detected 1.1 Not DetectedBromomethane0.29 Not Detected 0.76 Not DetectedChloroethane0.29 Not Detected 1.6 Not DetectedFreon 111.4 7.5 2.7 14Ethanol

0.29 Not Detected 2.2 Not DetectedFreon 1131.4 2.7 3.4 6.4Acetone1.4 11 3.5 282-Propanol1.4 Not Detected 4.5 Not DetectedCarbon Disulfide1.4 Not Detected 4.5 Not Detected3-Chloropropene

0.58 Not Detected 2.0 Not DetectedMethylene Chloride0.29 0.94 1.0 3.3Hexane0.29 Not Detected 0.85 Not Detected2-Butanone (Methyl Ethyl Ketone)1.4 Not Detected 4.2 Not DetectedTetrahydrofuran


0.29 0.69 1.2 2.8Heptane0.29 Not Detected 1.3 Not Detected1,2-Dichloropropane0.29 Not Detected 1.0 Not Detected1,4-Dioxane0.29 Not Detected 1.9 Not DetectedBromodichloromethane0.29 Not Detected 1.3 Not Detectedcis-1,3-Dichloropropene0.29 Not Detected 1.2 Not Detected4-Methyl-2-pentanone0.29 Not Detected 1.3 Not Detectedtrans-1,3-Dichloropropene1.4 Not Detected 5.9 Not Detected2-Hexanone

0.29 Not Detected 2.4 Not DetectedDibromochloromethane0.29 Not Detected 2.2 Not Detected1,2-Dibromoethane (EDB)0.29 Not Detected 1.3 Not DetectedChlorobenzene0.29 Not Detected 1.2 Not DetectedStyrene0.29 Not Detected 3.0 Not DetectedBromoform0.29 Not Detected 1.4 Not DetectedCumene0.29 0.50 1.4 2.4Propylbenzene0.29 2.0 1.4 9.74-Ethyltoluene0.29 2.4 1.4 121,3,5-Trimethylbenzene0.29 6.8 1.4 341,2,4-Trimethylbenzene

Page 10 of 21

Client Sample ID: DEEP POSTCARBON-121809Lab ID#: 0912492-02A





0.29 0.47 1.7 2.81,3-Dichlorobenzene0.29 Not Detected 1.7 Not Detected1,4-Dichlorobenzene0.29 Not Detected 1.5 Not Detectedalpha-Chlorotoluene0.29 Not Detected 1.7 Not Detected1,2-Dichlorobenzene1.4 Not Detected 11 Not Detected1,2,4-Trichlorobenzene1.4 Not Detected 15 Not DetectedHexachlorobutadiene




Page 11 of 21

Client Sample ID: DEEP POSTCARBON-121809Lab ID#: 0912492-02B





0.029 29 0.074 75Vinyl Chloride0.029 Not Detected 0.11 Not Detected1,1-Dichloroethene0.058 Not Detected 0.23 Not Detected1,1-Dichloroethane0.058 Not Detected 0.23 Not Detectedcis-1,2-Dichloroethene0.058 Not Detected 0.31 Not Detected1,1,1-Trichloroethane0.14 Not Detected 0.46 Not DetectedBenzene

0.058 Not Detected 0.23 Not Detected1,2-Dichloroethane0.058 0.12 0.31 0.65Trichloroethene0.058 0.77 0.22 2.9Toluene0.058 Not Detected 0.31 Not Detected1,1,2-Trichloroethane0.058 1.4 0.39 9.6Tetrachloroethene0.058 0.44 0.25 1.9Ethyl Benzene0.12 1.9 0.50 8.1m,p-Xylene

0.058 0.99 0.25 4.3o-Xylene0.058 Not Detected 0.40 Not Detected1,1,2,2-Tetrachloroethane0.29 Not Detected 1.1 Not Detectedtrans-1,2-Dichloroethene0.29 Not Detected 1.0 Not DetectedMethyl tert-butyl ether





Page 12 of 21

Client Sample ID: Lab BlankLab ID#: 0912492-03A






Page 13 of 21

Client Sample ID: Lab BlankLab ID#: 0912492-03A










Page 14 of 21

Client Sample ID: Lab BlankLab ID#: 0912492-03B










Page 15 of 21

Client Sample ID: CCVLab ID#: 0912492-04A




%RecoveryCompound

95Freon 1294Freon 11485Chloromethane941,3-Butadiene

100Bromomethane94Chloroethane90Freon 1195Ethanol92Freon 11398Acetone942-Propanol95Carbon Disulfide963-Chloropropene83Methylene Chloride90Hexane962-Butanone (Methyl Ethyl Ketone)98Tetrahydrofuran91Chloroform90Cyclohexane92Carbon Tetrachloride942,2,4-Trimethylpentane94Heptane911,2-Dichloropropane941,4-Dioxane94Bromodichloromethane92cis-1,3-Dichloropropene994-Methyl-2-pentanone91trans-1,3-Dichloropropene

1002-Hexanone96Dibromochloromethane901,2-Dibromoethane (EDB)89Chlorobenzene

102Styrene100Bromoform96Cumene98Propylbenzene

1024-Ethyltoluene961,3,5-Trimethylbenzene

1001,2,4-Trimethylbenzene

Page 16 of 21

Client Sample ID: CCVLab ID#: 0912492-04A




%RecoveryCompound


106alpha-Chlorotoluene981,2-Dichlorobenzene





Page 17 of 21

Client Sample ID: CCVLab ID#: 0912492-04B




%RecoveryCompound





Page 18 of 21

Client Sample ID: LCSLab ID#: 0912492-05A




%RecoveryCompound


137Ethanol71Freon 11382Acetone772-Propanol80Carbon Disulfide843-Chloropropene

68 QMethylene Chloride75Hexane812-Butanone (Methyl Ethyl Ketone)82Tetrahydrofuran75Chloroform76Cyclohexane76Carbon Tetrachloride812,2,4-Trimethylpentane79Heptane781,2-Dichloropropane791,4-Dioxane80Bromodichloromethane80cis-1,3-Dichloropropene844-Methyl-2-pentanone82trans-1,3-Dichloropropene912-Hexanone88Dibromochloromethane851,2-Dibromoethane (EDB)82Chlorobenzene91Styrene90Bromoform84Cumene84Propylbenzene914-Ethyltoluene931,3,5-Trimethylbenzene901,2,4-Trimethylbenzene

Page 19 of 21

Client Sample ID: LCSLab ID#: 0912492-05A




%RecoveryCompound






Page 20 of 21

Client Sample ID: LCSLab ID#: 0912492-05B




%RecoveryCompound

74Vinyl Chloride66 Q1,1-Dichloroethene731,1-Dichloroethane76cis-1,2-Dichloroethene751,1,1-Trichloroethane73Benzene731,2-Dichloroethane72Trichloroethene70Toluene801,1,2-Trichloroethane73Tetrachloroethene79Ethyl Benzene82m,p-Xylene82o-Xylene821,1,2,2-Tetrachloroethane76trans-1,2-Dichloroethene78Methyl tert-butyl ether





Page 21 of 21

1/6/2010


Project Name: Project #: 1073-06





Regards,


Workorder #: 1001003




WORK ORDER #: 1001003

CLIENT: BILL TO:

PHONE:


503-924-4704x113

503-924-4707

01/02/2010DATE COMPLETED: 01/06/2010

P.O. #

PROJECT # 1073-06

Work Order Summary

FAX:



PRESSUREFINAL

01A SSVE_POSTCARBON_123109 Modified TO-15 3.0 "Hg 5 psi01B SSVE_POSTCARBON_123109 Modified TO-15 3.0 "Hg 5 psi02A DSVE_POSTCARBON_123109 Modified TO-15 5.0 "Hg 5 psi02B DSVE_POSTCARBON_123109 Modified TO-15 5.0 "Hg 5 psi03A Lab Blank Modified TO-15 NA NA03B Lab Blank Modified TO-15 NA NA04A CCV Modified TO-15 NA NA04B CCV Modified TO-15 NA NA05A LCS Modified TO-15 NA NA05B LCS Modified TO-15 NA NA

CERTIFIED BY:

Laboratory Director

DATE:



01/06/10

Page 2 of 21





Ash Creek AssociatesWorkorder# 1001003


Two 6 Liter Summa Canister (100% Certified) samples were received on January 02, 2010. The laboratoryperformed analysis via modified EPA Method TO-15 using GC/MS in the Full Scan and SIM acquisitionmodes. The method involves concentrating up to 1.0 liters of air. The concentrated aliquot is then flashvaporized and swept through a water management system to remove water vapor. Followingdehumidification, the sample passes directly into the GC/MS for analysis.












Receiving Notes



Analytical Notes

Page 3 of 21


The Laboratory Control Spike (LCS) did not meet acceptance criteria for Ethanol. Recovery for thiscompound was (179 %). Results are reported as estimated.





Page 4 of 21


Client Sample ID: SSVE_POSTCARBON_123109

Lab ID#: 1001003-01A


0.15 0.16 0.74 0.80Freon 120.74 6.5 J 1.4 12 JEthanol0.74 4.4 1.8 10Acetone0.74 1.3 1.8 3.32-Propanol0.15 7.2 0.44 212-Butanone (Methyl Ethyl Ketone)0.74 1.2 2.2 3.6Tetrahydrofuran0.15 0.19 0.61 0.77Heptane0.15 0.48 0.73 2.44-Ethyltoluene0.15 0.20 0.73 1.01,3,5-Trimethylbenzene0.15 0.74 0.73 3.61,2,4-Trimethylbenzene


Lab ID#: 1001003-01B


0.015 0.10 0.038 0.27Vinyl Chloride0.074 0.093 0.24 0.30Benzene0.030 1.1 0.11 4.1Toluene0.030 0.030 0.20 0.20Tetrachloroethene0.030 0.36 0.13 1.6Ethyl Benzene0.060 1.1 0.26 4.8m,p-Xylene0.030 0.30 0.13 1.3o-Xylene

Client Sample ID: DSVE_POSTCARBON_123109

Lab ID#: 1001003-02A


0.16 0.67 0.33 1.4Chloromethane0.80 4.7 J 1.5 8.8 JEthanol0.80 12 1.9 27Acetone0.80 2.3 2.0 5.62-Propanol0.16 6.1 0.47 182-Butanone (Methyl Ethyl Ketone)0.80 1.0 2.4 3.0Tetrahydrofuran0.16 0.28 0.66 1.1Heptane0.16 0.42 0.79 2.14-Ethyltoluene

Page 5 of 21



Lab ID#: 1001003-02A0.16 0.19 0.79 0.911,3,5-Trimethylbenzene0.16 0.58 0.79 2.91,2,4-Trimethylbenzene


Lab ID#: 1001003-02B


0.016 0.080 0.041 0.20Vinyl Chloride0.080 0.088 0.26 0.28Benzene0.032 0.053 0.17 0.28Trichloroethene0.032 3.2 0.12 12Toluene0.032 0.076 0.22 0.52Tetrachloroethene0.032 0.30 0.14 1.3Ethyl Benzene0.064 0.96 0.28 4.2m,p-Xylene0.032 0.25 0.14 1.1o-Xylene

Page 6 of 21


Lab ID#: 1001003-01A





0.15 0.16 0.74 0.80Freon 120.15 Not Detected 1.0 Not DetectedFreon 1140.15 Not Detected 0.31 Not DetectedChloromethane0.15 Not Detected 0.33 Not Detected1,3-Butadiene0.15 Not Detected 0.58 Not DetectedBromomethane0.15 Not Detected 0.39 Not DetectedChloroethane0.15 Not Detected 0.84 Not DetectedFreon 110.74 6.5 J 1.4 12 JEthanol0.15 Not Detected 1.1 Not DetectedFreon 1130.74 4.4 1.8 10Acetone0.74 1.3 1.8 3.32-Propanol0.74 Not Detected 2.3 Not DetectedCarbon Disulfide0.74 Not Detected 2.3 Not Detected3-Chloropropene0.30 Not Detected 1.0 Not DetectedMethylene Chloride0.15 Not Detected 0.52 Not DetectedHexane0.15 7.2 0.44 212-Butanone (Methyl Ethyl Ketone)0.74 1.2 2.2 3.6Tetrahydrofuran0.15 Not Detected 0.73 Not DetectedChloroform0.15 Not Detected 0.51 Not DetectedCyclohexane0.15 Not Detected 0.94 Not DetectedCarbon Tetrachloride0.74 Not Detected 3.5 Not Detected2,2,4-Trimethylpentane0.15 0.19 0.61 0.77Heptane0.15 Not Detected 0.69 Not Detected1,2-Dichloropropane0.15 Not Detected 0.54 Not Detected1,4-Dioxane0.15 Not Detected 1.0 Not DetectedBromodichloromethane0.15 Not Detected 0.68 Not Detectedcis-1,3-Dichloropropene0.15 Not Detected 0.61 Not Detected4-Methyl-2-pentanone0.15 Not Detected 0.68 Not Detectedtrans-1,3-Dichloropropene0.74 Not Detected 3.0 Not Detected2-Hexanone0.15 Not Detected 1.3 Not DetectedDibromochloromethane0.15 Not Detected 1.1 Not Detected1,2-Dibromoethane (EDB)0.15 Not Detected 0.68 Not DetectedChlorobenzene0.15 Not Detected 0.63 Not DetectedStyrene0.15 Not Detected 1.5 Not DetectedBromoform0.15 Not Detected 0.73 Not DetectedCumene0.15 Not Detected 0.73 Not DetectedPropylbenzene0.15 0.48 0.73 2.44-Ethyltoluene0.15 0.20 0.73 1.01,3,5-Trimethylbenzene0.15 0.74 0.73 3.61,2,4-Trimethylbenzene

Page 7 of 21


Lab ID#: 1001003-01A





0.15 Not Detected 0.90 Not Detected1,3-Dichlorobenzene0.15 Not Detected 0.90 Not Detected1,4-Dichlorobenzene0.15 Not Detected 0.77 Not Detectedalpha-Chlorotoluene0.15 Not Detected 0.90 Not Detected1,2-Dichlorobenzene0.74 Not Detected UJ 5.5 Not Detected UJ1,2,4-Trichlorobenzene0.74 Not Detected UJ 7.9 Not Detected UJHexachlorobutadiene

J = Estimated value.UJ = Non-detected compound associated with low bias in the CCVContainer Type: 6 Liter Summa Canister (100% Certified)



Page 8 of 21


Lab ID#: 1001003-01B


s010510simFile Name:Dil. Factor: 1.49



0.015 0.10 0.038 0.27Vinyl Chloride0.015 Not Detected 0.059 Not Detected1,1-Dichloroethene0.030 Not Detected 0.12 Not Detected1,1-Dichloroethane0.030 Not Detected 0.12 Not Detectedcis-1,2-Dichloroethene0.030 Not Detected 0.16 Not Detected1,1,1-Trichloroethane0.074 0.093 0.24 0.30Benzene0.030 Not Detected 0.12 Not Detected1,2-Dichloroethane0.030 Not Detected 0.16 Not DetectedTrichloroethene0.030 1.1 0.11 4.1Toluene0.030 Not Detected 0.16 Not Detected1,1,2-Trichloroethane0.030 0.030 0.20 0.20Tetrachloroethene0.030 0.36 0.13 1.6Ethyl Benzene0.060 1.1 0.26 4.8m,p-Xylene0.030 0.30 0.13 1.3o-Xylene0.030 Not Detected 0.20 Not Detected1,1,2,2-Tetrachloroethane0.15 Not Detected 0.59 Not Detectedtrans-1,2-Dichloroethene0.15 Not Detected 0.54 Not DetectedMethyl tert-butyl ether




Page 9 of 21


Lab ID#: 1001003-02A





0.16 Not Detected 0.80 Not DetectedFreon 120.16 Not Detected 1.1 Not DetectedFreon 1140.16 0.67 0.33 1.4Chloromethane0.16 Not Detected 0.36 Not Detected1,3-Butadiene0.16 Not Detected 0.62 Not DetectedBromomethane0.16 Not Detected 0.42 Not DetectedChloroethane0.16 Not Detected 0.90 Not DetectedFreon 110.80 4.7 J 1.5 8.8 JEthanol0.16 Not Detected 1.2 Not DetectedFreon 1130.80 12 1.9 27Acetone0.80 2.3 2.0 5.62-Propanol0.80 Not Detected 2.5 Not DetectedCarbon Disulfide0.80 Not Detected 2.5 Not Detected3-Chloropropene0.32 Not Detected 1.1 Not DetectedMethylene Chloride0.16 Not Detected 0.57 Not DetectedHexane0.16 6.1 0.47 182-Butanone (Methyl Ethyl Ketone)0.80 1.0 2.4 3.0Tetrahydrofuran0.16 Not Detected 0.79 Not DetectedChloroform0.16 Not Detected 0.55 Not DetectedCyclohexane0.16 Not Detected 1.0 Not DetectedCarbon Tetrachloride0.80 Not Detected 3.8 Not Detected2,2,4-Trimethylpentane0.16 0.28 0.66 1.1Heptane0.16 Not Detected 0.74 Not Detected1,2-Dichloropropane0.16 Not Detected 0.58 Not Detected1,4-Dioxane0.16 Not Detected 1.1 Not DetectedBromodichloromethane0.16 Not Detected 0.73 Not Detectedcis-1,3-Dichloropropene0.16 Not Detected 0.66 Not Detected4-Methyl-2-pentanone0.16 Not Detected 0.73 Not Detectedtrans-1,3-Dichloropropene0.80 Not Detected 3.3 Not Detected2-Hexanone0.16 Not Detected 1.4 Not DetectedDibromochloromethane0.16 Not Detected 1.2 Not Detected1,2-Dibromoethane (EDB)0.16 Not Detected 0.74 Not DetectedChlorobenzene0.16 Not Detected 0.68 Not DetectedStyrene0.16 Not Detected 1.7 Not DetectedBromoform0.16 Not Detected 0.79 Not DetectedCumene0.16 Not Detected 0.79 Not DetectedPropylbenzene0.16 0.42 0.79 2.14-Ethyltoluene0.16 0.19 0.79 0.911,3,5-Trimethylbenzene0.16 0.58 0.79 2.91,2,4-Trimethylbenzene

Page 10 of 21


Lab ID#: 1001003-02A






J = Estimated value.UJ = Non-detected compound associated with low bias in the CCVContainer Type: 6 Liter Summa Canister (100% Certified)



Page 11 of 21


Lab ID#: 1001003-02B





0.016 0.080 0.041 0.20Vinyl Chloride0.016 Not Detected 0.064 Not Detected1,1-Dichloroethene0.032 Not Detected 0.13 Not Detected1,1-Dichloroethane0.032 Not Detected 0.13 Not Detectedcis-1,2-Dichloroethene0.032 Not Detected 0.18 Not Detected1,1,1-Trichloroethane0.080 0.088 0.26 0.28Benzene0.032 Not Detected 0.13 Not Detected1,2-Dichloroethane0.032 0.053 0.17 0.28Trichloroethene0.032 3.2 0.12 12Toluene0.032 Not Detected 0.18 Not Detected1,1,2-Trichloroethane0.032 0.076 0.22 0.52Tetrachloroethene0.032 0.30 0.14 1.3Ethyl Benzene0.064 0.96 0.28 4.2m,p-Xylene0.032 0.25 0.14 1.1o-Xylene0.032 Not Detected 0.22 Not Detected1,1,2,2-Tetrachloroethane0.16 Not Detected 0.64 Not Detectedtrans-1,2-Dichloroethene0.16 Not Detected 0.58 Not DetectedMethyl tert-butyl ether




Page 12 of 21


Lab ID#: 1001003-03A






Page 13 of 21


Lab ID#: 1001003-03A






UJ = Non-detected compound associated with low bias in the CCVContainer Type: NA - Not Applicable



Page 14 of 21


Lab ID#: 1001003-03B









Page 15 of 21


Lab ID#: 1001003-04A




%RecoveryCompound


Page 16 of 21


Lab ID#: 1001003-04A




%RecoveryCompound


67 Q1,2,4-Trichlorobenzene62 QHexachlorobutadiene




Page 17 of 21


Lab ID#: 1001003-04B




%RecoveryCompound





Page 18 of 21


Lab ID#: 1001003-05A




%RecoveryCompound



Page 19 of 21


Lab ID#: 1001003-05A




%RecoveryCompound

921,3-Dichlorobenzene931,4-Dichlorobenzene111alpha-Chlorotoluene881,2-Dichlorobenzene761,2,4-Trichlorobenzene

66 QHexachlorobutadiene




Page 20 of 21


Lab ID#: 1001003-05B




%RecoveryCompound





Page 21 of 21

Appendix G

Vacuum Response Assessment

Table G-1

Tarr Facility – Portland, Oregon

Test Conditions

Date 10-Nov-09

Air Pressure 1018.9 mbar

1.006 atm

10,390 kgf/m2

Temperature 55 °F

Shallow Wells

Q 8.5 scfm 4.01E-03 m3/s 4.8 g/s

P 9.6 inH2O 10146.3 kgf/m20.982 atm

µ 1.87E-06 kgf*s/m21.87E-06 kgf*s/m2

Bottom of sceen 15 ft 4.572 m 457.2 cm

Top of screen 5 ft 1.524 m 152.4 cm

Borehole Radius 2 in 0.0508 m 5.08 cm

Casing Radius 1 in 0.0254 m 2.54 cm

Air2D Radius of Influence 20 ft 6 m 600 cm

Deep Wells

Q 22 scfm 1.04E-02 m3/s 12.5 g/s

P 44 inH2O 9273.4 kgf/m20.898 atm

µ 1.87E-06 kgf*s/m21.87E-06 kgf*s/m2

Bottom of sceen 50 ft 15.24 m 1524 cm

Top of screen 18 ft 5.4864 m 548.64 cm

Borehole Radius 2 in 0.0508 m 5.08 cm

Casing Radius 1 in 0.0254 m 2.54 cm

Air2D Radius of Influence 42 ft 12.85 m 1285 cm

Summary of Radius of Influence Calculations

SVE IRAM Construction Report1073-06

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Appendix D - deq.state.or.us Inlet (bottom side) 6”-12” RF weld neck 150# flange (refer to chart...

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