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Brochure Phosgene

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    i n n o v a t i v e

    www.pentagonchemicals.co.uk

    Fine Chemicals

    Halebank, Widnes,

    Cheshire WA8 8NS

    United Kingdom

    T: +44 (0)151 424 3671

    F: +44 (0)151424 7906

    E: [email protected]

    Specialty Chemicals

    Workington, Northside,

    Cumbria CA14 1JJ

    United Kingdom

    T: +44 (0)1900 604371

    F: +44 (0)1900 66943

    E: [email protected]

    Designed and produced by

    Leeming Creative Communication Limited, Liverpool.

    Tel: 015170 8 0345 www.leeming.net

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    Pentagon is a leading UK based manufacturer of organic intermediates for use in the life science, petroche

    markets. Offering exclusive synthesis and a wide range of own products the privately owned company has

    per annum and employs around 200 people at our ISO 9001 and 14001 accredited sites in Halebank and W

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    Pentagon wa

    in 1975 on th

    works in Work

    established its

    of benzoate e

    paint and foo

    company dive

    of the next 25

    chemistries an

    and pharmace

    Expansion dur

    facilitated by t

    company a n

    national organ

    2002 the opp

    small, flexible

    primarily on th

    customers wa

    Pentagon Che

    formed throu

    out led by me

    management

    WORKINGTON

    HALEBANK 1939

    Ward Blenkinsop

    established to produceanaesthetics andsulphonamide antibiotics

    for the war effort.

    1950sProducing more than 300 products

    including anaesthetics, chemotherapydrugs, fungicides, paracetamol,penicillin intermediates, tranquilisers,

    UV absorbers and vitamins.

    1978Built large scale plant

    initially for penicillinintermediate lateradapted for agrochemical

    manufacture.

    1980Acquired

    by Shell.

    1986Phosgene

    plant built.

    1988Phosgene

    generatorinstalled.

    1992Purchased by

    Great Lakes.

    2003Purchased by

    Pentagon.

    1975Company formed produces sodium

    benzoate andbenzoate esters.

    1985Biocidebusiness

    established.

    1989Acquired bySuter Plc.

    1995Fueladditives

    plantbuilt.

    1996Purchasedby

    Ascot Plc.

    1998Grignardplant built.

    2001Acquiredby

    Dow Plc.

    2002Managementbuy out led by

    Allan Laing.

    Histo

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    A commitment to protectin

    workers and the environme

    central to our philosophy and

    provides the foundation for thfuture development and succe

    our business.

    In recognition that safe and

    environmentally secure

    manufacturing facilities are ess

    to building good relationships

    our customers, neighbours,

    regulators and suppliers both o

    Halebank (a top tier COMAH)

    Workington sites are accredite

    the internationally acknowledg

    standard BS EN ISO 14001.

    As part of our drive for continimprovement in the area of he

    safety and the environment

    Pentagon is a signatory to the

    Safety, Hea

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    Meeting cu

    is the highe

    Pentagon a

    all materials

    exacting stacustomers re

    rigorous app

    stages of th

    In early deve

    closely with

    identify and

    specification

    analysis that

    material is p

    moves into c

    undertake v

    ascertain tha

    reliable and

    In manufact

    carefully sele

    approved su

    operating p

    Qua

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    From new product introduc

    to commercial manufacture

    Pentagon operates a multi-

    disciplinary product teamapproach to drive our contin

    improvement culture. In additi

    ensuring full compliance with

    customer requirements for on-

    in-full deliveries and quality th

    teams focus on key areas to im

    these include the identification

    realisation of yield improveme

    productivity enhancement via

    time reduction and increased b

    size, waste minimisation and s

    recycle.

    Our team of highly trained che

    provide product support from initial lab synthesis through to

    scale manufacture. We pride

    ourselves in providing rapid

    evaluation of new enquiries, fa

    track synthesis of target molec

    Research &

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    FlexibleInnovative

    Responsive

    Service

    Technology

    Our Core Values ...

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    A wide range of chlorinated

    intermediates can be manufactured

    at our Halebank site. As well as fully

    integrated bulk chlorine storage andhandling the site has significant

    experience in the use of phosphorus

    oxychloride, sulphuryl chloride and

    thionyl chloride.

    Key Plant

    9.0m3 GL and SS vessels

    Fully DCS controlled

    Temperature -10C to 140C

    Hastelloy Rosenmund filter dryers

    Isolated product pack off room

    Solvent recycle facility

    Chlorination

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    Our purpose built Grignard plant at

    Workington offers advanced

    capability in the manufacture of

    reagents and their downstreamderivatives. In addition to a wide

    range of own products in standard

    solvents and concentrations we also

    offer custom manufacture of

    downstream products utilising more

    concentrated solutions than could be

    commercially shipped.

    Grignard Plant

    4 4 .5m3 GL vessels

    Fully DCS controlled

    Temperature -15C to 150C

    Distillation unit with 26

    theoretical plates

    Hastelloy filter dryer Bulk and drum handling

    Grignards

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    With over 40 years experience of

    phosgene chemistry Pentagon is at the

    forefront of phosgenated intermediates

    and their downstream derivatives.The state of the art facilities include on

    demand phosgene generation and a

    flexible, fully sequenced plant capable

    of manufacturing solid and liquid

    products. Minimal inventories of

    phosgene combined with continued

    investment in our plant ensure that

    safety and environmental controls meet

    the most exacting standards.

    Phosgenation Unit

    6.3 9.0m3 GL and SS vessels

    Fully sequence DCS controlled

    Temperature -10C to 140C

    Phosgene generation 200Kgper hour

    Hastelloy Rosenmund filter-dryers

    2 x 8.5m2

    2 GL unit distillation units with up

    to 15 theoretical plates

    High vacuum 5mBar

    Phosgenation

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    Sodium dispersio

    The high temperature dissolution of

    sodium metal in a mineral oil to give

    a stable but highly reactive dispersion

    offers a commercially viable, cost

    effective route to the large scale

    manufacture of organo-sodium

    compounds. Benefiting from over

    20 years research and development

    Pentagons unique combination of

    optimised particle size and


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