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WDS.:iNGE; G 1-880 LABEL; N 2, 2.0 QUAN: A 1, 3.8 J 8 BASE: U100- 50

382 , .; 35965.

278698. 36096.

5203135.83129. 708

948.„ 234.̂ "

5007:55

6009:30

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DATA: EPAUOA1668'ltlCALI; EPAUOA1668:*!

RIC :08/12/84 3;52se0SAMPLE! 10 UG/L STD.CONOS.!RftHGE: G 1,1300 LflBEL; N 0, 4.0 QUAH; A 0- 1.0,1 0 BASE; U 20, 3

SCANS 1 TO 1300

5981034

857

468

384

37

1

286

334

528

1210

208.6:50

40013:40

60020:30

800'•27;20

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08/12/81 3:52:00 . . .SAMPLE: 10 UO/L STD. "SUBMITTED BY: USTCO -"ANALYST: RJM

AMOUNT-AREA

n-BKUPlUUtllZU I K It-LUUN 1D£ ( SURROGATE )0-3,ETHYLBENZENE-(SURROGATE) .TOLUENE-DB (SURROGATE)P-BROfiaFLUOROBENZEWOORROGATe)

M/E1301 1 41 1 7

SO94626484

NOTNOT

6163968362975876

1 1 78363759578

129837563

173728643

,6584

NOTNOTNOT166B391

1 1 29143

SCAN38469883780

139170214286

FOUNDFOUND

369410430449471516302335528540584591605631-628631

. 630-662713467527725468-616

FOUNDFOUNDFOUND

780783822861937772

T13232924579

121414151617

-101 118181920202121213.12224-1518241521

262628.293226

IME:07: 31: 17: 44:49:48: 19:46

:36:00:41:20:06:38: 19:27:02:27: 57: 12:40: 13-:27:34:-31:37^-33-

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AREA(HGHT)147920.^71692.353919.28760.

" 40683.35319.17585.86068.

63376. :75081.

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3118.93316.81630.

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17609.3885.17.

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1 1 .1 1 .1 1 .1 1 .9.

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487 UG/L559 UG/L643 UG/L403 UG/L738 UG/L632 UG/L353 UG/L556 UG/L163 UG/L451 UG/L039 UG/L643 UG/L099 UG/L341-UG/L398 UG/L694 UG/L569 yG7t-692 UG/L593--UC/L-967 UG/L155 UG/L776 UG/L300 UG/L269 UG/L

507 UG/L537 UG/L927 UG/L301 UG/L709 UG/L415 UG/L

XTOT3. 523. 525. 321-. 261. 451.311-. 30-1. 81'

1.271. 281.29!> 261. 081. 281. 141. 281. 121. 041. 1 11. 061. 12

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RIC DATA; EPAV&A1669 «1 SCANS 1 TO 1380CALI: EPAUOA1669 fl08/12/84 4:52;00

SAMPLE; 20 UG/t STD.CONDS.;RANGE; G 1,1303 LABEL; N 6/ 4,0 QUAM; A 0, 1.0 J 0 BASE: U 20, 3

' 814

QUANT I TAT I ON REPORT FILE: EPAVOA1669

DATA: EPAVOA1669. TI08/12/84 4:52:00SAMPLE: 20 UG/L STD.SUBMITTED BY: USTCO ANALYST: RJW

AMOUNT°AREA(H::HT) • REF.AMNT/CREF.AREA(HGHT)» RESP.FACT)RESP. FAC. FROM AVERAGE-OFWHOLE .RL •

NO NAME1 »2 »3. ..-it . : •

BROMOCHLORMETHANE (INTERAL STANDARD)P-DIFLUOROBENZENE (IN-IERNAL STANDARD)DICHLOROBENZENE-D5 (INTERNAL STAMOARD)CHLOROMETHANFBROMOMETHANE : 'VINyL CHLORIDE • ;.CHLOROETHANE •METHYLENE CHLORIDEACROLEIN .ACRYLONITRILE :1.1-DICHLOROETHYLENE :

1, 1-DICHLOROETHANe :TRANS-1.2-DICHLOROETHYLENE :CHLOROFORM ' '1.2-DICHLOROETHANE1, 1, t-TRICHLOROETHANE

17 HSL ACETONF T_ .L-Z—'—^ll---- _ -—. , - - - -18-'HSL CARBON DISULFIDE ;19 CARBON TETRACHLORIDE20 BROMODICHLOROMEI.HANE. , . . _„__ ._ , . :21 112-DICHLORdpROPBNE"-""""22 _ TRANSr_»;.3-»rCHl-aBat?.ROPYLENE23 TRICHLOROETHYLENE24 BENZENE25 DIBRGMOCHLOROMETHANE26 1,1,2-TRICHLOROETHANE27 CIS-1,3-DICHLOROPROPYLENF28 2-CHLOROETHYL VINYL ETHER29 BROMOFORM :30 HSL METHYL ETHYL KETONE31 HSL VINYL ACETATE ^32 HSL METHYL ISOBUTYL KETONE33 1,2-DICHLOROETHANE-D4 (SURROGATE)34 BENZEW-D& (SURROGATE)35 DIBROMOTETRAFLUOROETHANE (SURROGATE)36 BIS(PERFLUOROISOPROPYL}KETONE (SURROGATE)37 FLUOROBENZENE (SURROGATE) ;38 TETRACHLOROETHYLEhlE-. . :39 1, 1, 2, 2-TETRACHLOROETHANE40 TOLUENE41 CHLOROBENZENfc42 ETHYLBENZEN&43 HSL 2-HEXANONE"44 HSL STYRENE45 HSL 0-XYLENE46 HSL M-XYLENE

M-BROMOBENZOTRIFLUORIDE (SURROGATE;)D-5 ETHYLBENZENE (SURROGATE)TOLUENE-D8 (SURROGATE)P-BROMOFLUOROBENZENE (SURROGATE.)

SCAN33469785683

1421742172B7

FOUNDFOUND

369410429448470515302335527539583589604620627629629660712465527724467615

FOUNDFOUNDFOUND

779781820860936770

T13232924

' S79

121414151617101118181920202121212122241518241521

262628293126

IME0749155051372549

3600391803361927002555073S113"i

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292933205300445701

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RRT KETH WE.000 A BB 128000--: A SB 413000 A SB 266aj^-^A BB 4137Q-...-A-.J3B. .,..— 524S3 '•"A "BB 46565 . A BB 23747 A BB 93

961 A BB 87068 A BB 103117 A BB 50167 :A BB 132224 A BB 90341 A BB 107786 A BB 6872 A BB 136756 A VB 107

-Z73——A-B8——.- -4-18836 A BB 67845 A BB 78867 A-BB .——77BW—A'W 158-?dd 'A" SB. - '-Q3902 A BB 52902 A VB 74947 A BB 11022 A BB 40667 A BB 5756 A»BB 5039 A BB 34670 A BB 403882 A BV 806

'910 A BB 7::912 A BB 71958 A BS 186005. A BB 124093 A BB 19E900 A VB 3S

ROMOBENZOTRIFLUORIDE (SURROGATE;)ETHYLBENZENE (SURROGATE)

UENE-D8 (SURROGATE)ROMOFLUOROBENZENE (SURROGATI:.)

TIME REF RRT KETH AREA(HG13 07 1 1.000 A BB 128085.23 49 2- 1.000--: A BB 413960.29 15 3 1.000 A SB 266677.2 50 1 0. 2J16- : A BB 41175.4 51 .l.....Q.,37Q-...-A-..BB..— 52830.557 1 0. 4S3 "A'BB 46906;7 25 1 0.565 . A BB 23431,9 48 10. 747 A BB 93850,

12 36 1 0.961 A BB 87250.14 00 1 1. 068 A BB 103935.14 39 1 1. 117 A BB 50499.15 18 1 1 . 167 :A BB 132820.16 03 1 1.224 A BB 90827.17 36 1 1.341 A BB 107414.1019 1 0. 786 A B B 6147.11 27 1 0.872 A BB 126471.18 00 2 0. 756 A VB 10742.5.18 25 2 0-Z73——A-B8——.- -4-18893.19 55 2 0.836 A BB 67611.20 07 2 0. 845 A BB 78614.20 3S 2 0.867 A-BB ———77.170,'21 11 2 0: BW—A'W 158749:21 25.....2.r-0--?d0 ^A-SB. - -83646.21 29 2 0. 902 A BB 52419.21 29 2 0.902 A VB 74793.22 33 2 0.947 A BB 11503.24 20 2 1.022 A BB 40372.15 53 2 0.667 A B B 5133.18 00 2 0 . 756 A»BB 5486.24 44 2 1.039 A BB 34305.15 57 2 0.670 A BB 403103.21 01 2 0.882 A BV 806241.

26 37 3 0.910 A BB 73654.26 41 3 0. 912 A BB 71355.28 01 3 0 . 958 A BS 188873.29 23 3 1.005. A BB 124352-31 59 3 1.093 A BB 198353.26 18 3 0.900 A VB 35947.

HT) AMC50.50.50.18.

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19.20.19.20.17.22.19.20.

102.101.

17.19.20.17.1822

3UNT000000000934.746239082A18

262479.077454530940571087470892-048706874968245415596496731287364922164081

614162851841010569

UG/Lue/LUG/LUG/LUG/LUG/LUG/LUG/L

UG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/L

-UG/L"UG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/L

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0. 880. 961 . 040. 890. 901 . 130. 930. 681. 84

NO RET

DATA: EPAUOA1670 »1 ;SCANS 1 TO 1390CALIs EPAVOA1670 »1

RIC08/12/'84 5:53803SAMPLE: 50 UG/L 5TD.CONDS.;RANGE: G 1-1300 LABEL: N 0 - 4 . 8 QUANi A 0, 1.0 J 0 BASE; U 23, 3

100.0n ! '629 ! 815

QUANTITATION REPORT FILE: EPAVOA1670

DATA: EPAVOA1670. TI08/12/84 3:53:00SAMPLE: 50 UG/L STD.SUBMITTED BY: USTCO ANALYST; RJW

AMOUNT-AREA • REF.AMNT/(REF. AREA)* RESP.FACT)RESP. FAC. FROM AVERAGE OF WHOLE . R L

NO NAME1 * BROMOCHLORMETHANE;(IN1ERAL STANDARD)2 » P-DIFLUOROBENZENE (INTERNAL STANDARD)3 * -BICHLdROBENZENE-DS (INTERNAL •STANDARD)4 CHLOROMETHAME . .5 BROMOMETHANE ^6 VINYL CHLORIDE ••-• • — - • • ; •7 CHLOROETHANE8 METHYLENE CHLORIDEf ACROLEIN

10 . . . . _ ACRYLONITRILE-—————-— —11 1,1-DICHLOROETHYLeNE12 1,1-DICHLOROETHANE13 TRANS-1.2-DICHLOROETHYLENE14 CHLOROFORM -.15 1,2-DICHLOROETHANE ;16 1,1-I-TRICHLOROETHANE17 HSL ACETONE _ : "'_;_:'""^_. _ . - . . - - . . — -IS' HSL "CARBON-biSULFIDE ; :19 CARBON TETRACHLORIDE20 BROMODICHLOROMETHANE . .._ -21. : l ; 2 - & I C + l L a R O P R e ) P A h ® — ' ~ " ' "22 - TRANS-l_.3-blCHL-OROPROPYLENE '23 ' ' T R i C H L O R O E f H Y L E N E24 BENZENE . . _ _. .25 DIBRGMOCHLOROMETHANE26 I,1,2-TRICHLOROETHANE27 CIS-1,3-DICHLOROPROPYLENE28 2-CHLOROETHYL VINYL ETHER29 BROMOFORM30 HSL METHYL ETHYL KETONE31 HSL VINYL ACETATE32 HSL METHYL ISOBUTYL KETON£33 1,2-DICHLOROETHANE-D4 (SURROGATE)34 BENZEN6.-D6 (SURROGATE)35 DIBROMOTETRAFLUOROETHANE (SURROGATE)36 BIS(PERFLUOROISOPROPYL)KETONE (SURROGATE)37 FLUOROBENZENt (SURROGATE) .33 TETRACHLOROETHYLENE \". . ' .39 1.1.2,2-TETRACHLOROETHANE40 TOLUENE.41 CHLOROBENZENF42 ETHYLBENZENE43 HSL 2-HEXANONE44 HSL STYRENF45 HSL O-XYLENE •46 HSL M-XYLENE

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DUAL MASS SPECTRUM03̂ 12/84 6:54:00 + 9 ; 4 6SAMPLE; 189 UG/L STD.CONDS.;ENHANCED (S 15B 2N 0T>

DATA; EPAUOA1671 #286CALl! EPWOA1671 #1

BASE M/-E! 49/ 49RIC; 166655../ 178431.

40 60 79 88

DUAL MASS SPECTRUM88/12/34 6;54;08 + 12s36SAMPLE; 103 UG/-L STD.CONDS.:;ENHANCED

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DUAL MASS SPECTRUM08/-12/84 6; 54! 80 +20! 33SAMPLE: 108 UG/L STD.CONDS.:ENHANCED

DATA; EPflUOfll671 »620CALl! EPIWOA1671 #1

BASE M/E; 78/ 73RIC; 213903./• 293337.

DUAL MUSS SPECTRUMa8/12/'34 6;54;99 + 21:11SffllPLE: 100 UG/L STO.CONDS,!ENHANCED (S 15B 2N 0T)

40 98 160 113 120 69 70

- 108928.

DUAL MASS SPECTRUM08/12/84 , 6i 54; 80 + 13:00SAMPLE; 180 UG/L STD.CONDS.: :ENHANCED (5 15B 2N 0T)

DATA; EPAUOA1671 #527 BASE M/'E: 117/ 117CALIs EPAUOA1671 #1 RIC; 27S527,/- 296447.

£-40 80:: . ! 90 110 120 199 60 70

0 0 2. 0 6 7

DUAL MASS SPECTRUMe^^S^ 6!54!@S + 15; 57SAMPLE: 100 UG/L STD.CONDS.s :ENHANCED (S 15B 2N 0T)

DATA: EPAUOA1671 #467 BASE M/'E: G5/ 65CALI: EPAUOA1671 #1 RIC: 162383./ 239151.

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DUAL MASS SPECTRUM@3/'12/'84 6!54!00 + 26; 43SAMPLE! 108 LIG4. STD.COWS.;ENHANCED (S 158 2N 0T)

DATA: EPAWA1G71 #782 BASE M/E: 83/- 83CALl! EPAWA1671 #1 RIC; 21759d,.-' 359935.

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DUAL ?55 SPECTRUM98-/12/S4 6!54!08 + 29i25SAMPLE: 160 UG/L STD.CONDS.;ENHANCED (S 15B 2N 8T)

DATA: EPAUOA1671 #861 BASE H/E: 112/- 112CALIi EPAUOA1671 »1 RIC; 255231..' 311295.

1- 77184.0 0 2 0 7 3

DUAL MASS SPECTRUMeS/'̂ 'W. 6s 54; 89 + 26s 21SAMPLES 108 UG/t 5TD.CONDS.sENHANCED (S 15B 2N OT)

DATA; EPftUOA1671 #771 BASE M/E; 43/' 43CALIi EPAUOA1671 #1 RIC; 53823./' 66815.

-T—]——I——T

150 230-I——I——L

0 0 2 0 7 4

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DATA: EPA1A3A1672 «1CALI: EPAUOA1672#1

RIC ;

08/12/84 7:54': 09:. SAMPLE; 200 UGz-L STO.

CONDS.;i RANGE; G 1-1300 LABEL: N

QUANTITATION REPORT FILE: ;EPAVOA1672

DATA: EPAVOA1672.TI08/12/84 7:54:00SAMPLE: 200 US/L STD.SUBMITTED BY: USTCO ANALYST: RJW

AMOUNT°AREA

NO-47484930

N01

2345

.6'7-89

101 11'2131 41516171819202122232425262728293031323334353637383940

^1»2t3

-NAME

M/E1301 1 41 1 75094626484

NOTNOT

6163968362975876

1 1 78363759578129837563

1737286436584

NOTNOTNOT1668391

1 1 29143

M-BR(D-5 (TOLUEP-BRC

SCAN38469885684"

143174217287

FOUNDFOUND

3704 1 1429448471515304334528540584590605621628630629661713466527725468616

FOUNDFOUNDFOUND

780782820861936771

DMOETHENEDMOf

T13

.2329

--•Z4579

121414151617101 118181920202121212122241518241521

262628293126

BENZYLBE-D8FLUO

IME0751133253572548

380339180636232502275709401327312935225500465903

394301255921

OTRINZEIS(SUPROBE

REF1

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- 111

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11

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[FLUORIDE

NO M7E—SCAN——ITIME.44 104 1088 37:1043 106 1133 38:4746 106 1097 37:2947 NOT FOUND48 NOT FOUND49 98 814 27:4950 93 1034 33:20

REF RR'3 1. 273 1.32,3 1.28:

3 0. 933 1.201

.) RATIO> 1. 00 : "> 1. 00» 1 . 00[ I. 02' 1 . 01 :1 I. 01 :> 1 . 01> 1. 00) - — -, - . - . — - , -1 1. 01) 1 . 00> 1. 00^ 1. 00 :

[ 1.00> 1.00> 1. 01' 1. 00 ;

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1 0. 93 '? 0. 93 :3 0. 933 0. 933 0. 931 0. 93:> 0. 93t 0. 931 1 . 287

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1 9 1 . 1 1133.08187.98189.59143. 42

190.02192.17193 .12190.76195. 22193.53163.79197.76213.36211.03206.47213.71203.74193.94212.37201.09215.36218. 87234.08200.46210.38210.311 1 3 . 1 7100.74

186.85198.591 9 7 . 1 1190.64197.02193. 04194. 76187. 56379.88

AREA1.000 -1. 0001'. 0000. 8491. 0441. 0040. 5061. 7770. 0310. 1091. 8652. 1961 . 0912. 8101. 8152. 3370. 1022. 7300. 702

.0. 7600. 429

- 6; 508"0. 4941 . 0 1 10. 5250. 3100. 4610. 0680. 2750. 0280. 0340. 1980. 477

0. 9633. 0740. 0070. 0040. 7840. 6981 . 6981 . 3072. 0650. 2991. 0450. 6320. 3381 . 637

%TOT2. 302. 414. 87

1. 291. 31

RATIO1. 001. 001. 000. 960. 67

" '0.940. 950. 72

0. 950. 960. 970. 950. 980. 970. 820. 991. 07

: 1. 061. 03

~ 1'.'071 . 020. 971. 061. 011. 081. 091 . 171. 001. 051. 051. 131. 01

0. 930. 990. 990. 950. 990. 970. 970. 941 . 90

NO484950

RET

' Continuing Calibration Check

Volatile HSL Compounds

Case No:

Contractor: U . S "Tt

Contract No: 1^0!~^W

Instrument ID: 1/0 fi

Calibration Date: ' ^J /^JP 7

Time: _____7 . / ^______Time:

Laboratory ID:

Initial Calibration Date: ^1 /a I ̂ /

Minimum RF for SPCC is 0.300 Maximum %D forCCC is 25%

Compound

Chloromethane

Bromomethane

Vinyl Chloride

Chloroethane

Methylene Chloride

AcetoneCarbon Djsulfide

t, 1-Dichloroelhene

1, 1-Dichloroelhane

Trans-1, 2-Dichloroeihene

Chloroform

1 , 2-Dichloroelhane

2-Butanone :

1 , 1 , 1 -Trichloroethane

Carbon Tetrachloride

Vinyl Acetate

Bromodichloromethane

1. 2-Dichloropropane

Trans-1, 3-DichloropropeneTrichtoroethene

Dibromochloromethane

1 , 1 . 2-Trichloroethane

Benzene ' '

cis-1. 3-Dichloropropene2-ChloroethylvinyletherBromoform - - - - - -

2-Hexanone

4-Methyl-2-Pentanone

Tetrachloroethene

1. 1-, 2. 2-Telrachloroethane

Toluene

Chlorobenzene

Ethylbenzene

Slyrene

Total Xylenes

RF .

0.^°!/.o^f.no^

0.5T3 lo

l.-t^o. io7

^ 43&I.^S^. ivQ/.oy/3.^,10

i.,^^,^ ,a // •

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866160.

SCANTIME

uL'rtNI 1 1 A I ION REPORT FILE: EPAVOA1704

DATA: EPAYOA17G4., T.I . ; . . . _ ....6g/18/84 9: 12:00 ... -—^-_- _._——.—__:——•-—

SAMPLE: 50 UG/L STD. VERIFICATIONSUBMITTED BY: USTCO ANALYST: RJW

AMOUNT=AREA » REP.AMNT/(REI-.AREA)» RESP.FACT)RESP. FAC. FROM AVERAGE OF WHOLE .RL

NO NAME1 * BROMOChfLORMETHANE ( INTERAL STANDARD >2 * P-DIFLUOROBENZENE (INTERNAL STANDARD!3 » ._..DiCHLQRDSEy2£NE-D5 -(INTERNAL STANDARD)4 CHLOROMETHANE

5 BROMOMETHANE6 VINYL CHLORIDE7 CHLOROETHANE8 METHYLENE CHLORIDE9 ACROLEIN

10 ACRYLCNITRILE1 1 1,1-DICHLOROETHYLENE12 1,1-DICHLOROETHANE13 TRA^!S-l,2-DICHLOROETHYLE^E: -

14 CHLOROFORM15 1,2-DICHLOROETHANE16 1,I,1-TRICHLOROETHANE17 HSL ACETONE18 HSL. CARBON 'DISULFIDE19 CARBON ;TETRACHLORIDE20 BROMODLCHLOROMETHANE21 1,3-DICHLOROPROPANE22 TRANS-1.3-DICHLOROPROPYLENE23 TRICHLOROETHYLENE24 BENZENE"" " ' ' ' . ' '........ . -25 --DIBROMO'CHLTIROKETHANE26 1,1,2-TRICHLOROETHANE27 CIS-1,3-DICHLOROPROPYLENE28 2-CHLOROETHYL VINYL ETHER29 BRQMOFORM30 HSL METHYL ETHYL KETONE31 HSL VINYL ACETATE32 HSL METHYL .IS03UTYL KETONE - .33 1 , 2-DICHLOROETHANE-D4 (SWROGATE?34 BENZENE-D6 (SURROGATE)35 DIBROMOTETRAFLUOROETHANE (SURROGATE)36 - —•BIS(PEKFLUOROISOPROPYL)KETONE (SURROGATED37 FLUOROBENZENE (SURROGATE)38 TETRACHLOROE1HYLENE39 1 , 1, 2, 2-T6-TRACHLOROETHANE40" TOLUENE^41 CHLOROBENZENE42 ETHYLBENZENE43 HSL 2-; IEXANONE44 HSL. STYRENE45 HSL 0-XYLENE46 HSL M-XYLENE

NO47

4'?50

N0123456789

101 112131415161718192021222324252627282930313233343536373839

404142

NAM

M/E1301 1 4

1 1 75094

A36484

NOTNOT

6163968362975876

1 1 7S363759578

129837563

1737286436584

NOTNOTNOT166

- 8391

11291

M-BRGfl-S F

TOLUEP-BRd

SCAN38469885784

143174217287

FOUNDFOUND

370411429448471515304335527539

583590605621627630629661712466527725467616

FOUNDFOUNDFOUND

779

— 78S--821861938

MOTHNEMO

T1323293A

579

131414151617101 1

181819

20202121212122241518241521

2626282932

BENZCn.BFh

-D8 (FLUOR

IME0751175253

57.2548

38033918063623270025

5509401325312935205500465703

3743-032503

3TRIilZEMSURQBE

REF1231

1

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JORIDEtsuaaa?ATti):NE

NO M/43 444 1045 1046 1047 N048 N049 950 9

NO RE1 132 233 294 25 46 57 78 99 10

10 1111 1212 1413 1414 1515 1616 1717 1018 1119,..,1720 1821 1922 2023 2024 "2125 2126 2127 2128 2229 2430 1531 1732 2433 1534 2035 1336 1437 . 1638 2639 2640 2741 2942 3143 2644 3645 3846 37

E SCAN TIKE REF RRT METH3 772 26 23 3 0. 901 A BB4 1089 37 12 3 1 . 271 A BB6 1137 38 51 3 1.327 A BB6 1098 37 31 3 1. 281 A BBT FOUNDT FOUND8 815 27 51 3 0.951 A BB3 1035 35 22 3 1.208 A BB

T < L > RATIO R R T < L » RATIO AMNT07 1.00 1.000 .00 . 50. 0049 1. 00 . 1, 000 . 00 50. 0011 1.00 1.000 . 00 50. 0048 1.02 0.214 .02 46.6849 1.01 0.367 .01 44. 0653 1.01 0.448 .01 44.9421 1. 01 0. 560 . 01 49. 4446 1.00' 0.745 .00 36.4819 0. 78602 0.84134 1.01 0.958 .01 52.4000 1.00 1.068 .00 49.5737 1.00 1.115 .00 51. 5316 1.00 1.164 .00 52. 7703 1.00; 1.224 1.00 55.1234 1.00 1.339 1.00 54.0919 1.01 0.786 1.01 75. 2423 1.01 0.867 1.01 40.5058 1.00, 0.787 0.96 51.2025 1.00 0.807 0.96 44.5753 1.00 0.871 0.96 44.9807 1. 00 : 0. 882 0. 96 43. 8836 1.00' 0.903 0.96 48.8409 1.00 0.927 0.96 46.0423 1.00 0.937 0.96 40.2527 1.00 0.940 0.96 41.8537 1.00 0.940 0.96 47. 7931 1.00 0.987 0.96 107.0218 1.00 1.064 0.96 40.1253 1.00 0.696 0.96 80.1158 1. 00 • 0. 787 0. 96 57. 5042 1.00 1.082 0.96 115.7157 1.00 0.699 0.96 104.7559 1.00 0.919 0.96 94.4749 • 0. 704 - • . . - . -00 0.61430 . 0..70433 1 .00 '0 .981 0.93 48.9739 1.00 '. 0.985 0.93 43. 3457 1.00 1.033 0.93 52.9219 1.00 1.083 0.93 47.9153 1.01 1.178 0.93 45.7216 1.00 0.971 0.93 53.1658 1.01 1.366 0.93 44.6732 1.01 1.424 0.93 44.6117 1.01 1.000 1.28 44 78

AREA(HGHT> AMOUNT XTOT122512. . 53. 162: UG/L... 2. 183&007&. 44 &70 UG/1. 1 pi.-.. - . . .217422. • 44. 61 T UG/L 1'. 83229786. 44.777 UG/L 1.83

1174950. 107.521 UG/L 4.40732108. 97.481 UG/L 3. 99

A K N T < L > R . F A C R . P A C ( L ) RATIO50.00 1.000 1.000 1.0050.00 1.000 1,000 1.0050.00 1.000 1.000 1.0050. 00 0. 793 0. 849 0. 93 .'.,50.00 0.920 1.044 0.8850.00 0.902 1.004 0.9050. 00 0. 500 0. 506 0. 99 •C1

50.00 1.297 .1:777 0.73 C.,;250. 00 0. 031 ^250. 00 0. 109 —

50.00 1.954 1.865 1.0550. 00 2. 177 2. 196 0. 9950.00 1.124 1.091 1. 0350.00 2.965 2.810 1.0650. 00 2. 001 1. 815 1. 1050.00 2.528 2.337 1.0850.00 0.153 0.102 1.5050.00 2.211 2.730 0.8150.00 0.719 0.702 1.0250. 00 0. 678 0. 760 0. 8950.00 0.386 0.429 0. 9050.00 0.445 0.508 0.8850.00 0.482 0.494 0..9850.00 0.931 1.011 0.9250. 00 0. 423 0. 525 0. 8050.00 0.260 0.310 0. 8450.00 0.441 0. 461 0. 9650.00 0.145 0.068 2.1450. 00 0. 221 0. 275 0. 8050.00 0.045 0.028 1.6050.00 0.039 0.034 1.1550.00 0.458 0.198 2. 31

100.00 0.499 0.477 1.05100.00 0.910 0.963 0.94100.00 3. 074100.00 0. 007100.00 O.:00450.00 0.768 0..784 0 .98.50.00 0.605 0..698 0.8750.00 1.458 1.378 1.0650.00 1.252 1.307 0.9650.00 1.888 2.065 0.9150.00 0.318 0.299 1.0650.00 0.933 1.045 0.8950.00 0.564 0.632 0.8950.00 0.596 0. 665 0. 90

NO R E T < L > RATIO R R T ( L > R A T I O AMNT A M N T < L ) R FAC R F A C ( L > RATIO47 27:49 1..197. . . . . . . . . 100.00 . ..1.637 - -48 23:43 1.102 100.00 2.050 :-49 27:45 1.00 1.025 0.93 107.52 100.00 1.523 1.416 1'0850 35:11 t . O O 1.301 0.93 97.48 100-00 0.949 0.973 0,97

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/ ^ 0 ^ 0 0MID MASS CHROMATOGRAMS DATA: ST5840924B #1268 SCANS 1185 TO 123009/24/84 17(45809 CALI; F5840924 #21SAMPLE: 2UL OF 0.2N&/UL TCDO STD, CALI ItlRANGE; G 1,1268 LABEL: N -4, 2.5 QUAN; A 4- 2.0 BASE: U 20, 3

119811:14

-T——'———'——————I——1200 1210ll»19 11:25

122011:31

0 ?: 0 0

Colifornio Rnolvticol Loborotories, Inc.'2544 Industriol Boulevard • LUest Sacramento, Cfl 9 5691

U6 EPft A^7 //

^wi^1 \&-t^^iU^

7^y/

^: CJ

Continuing Calibration Check

Volatile HSL Compounds

Case No;

Contract No:

Instrument ID:

^0^? :

U.STcs-^'/iO,

i.%-o/-fc7'eo1/OA • -

Calibrating Oatf*—; O.J

Tim«. S',0'?-

Labnratnry ID--

Initial Calibration Date:

iWl-——T-——-t——

Z)/s-/ yi Q'yP^——

Minimum RF for SPCC is 0.300 Maximum %D for CCC is 25%

Compound

ChloromethaneBromomethaheVinyl ChlorideChloroelhaneMethylene ChlorideAcetone -"Carbon Disuldde1 . 1 -Dichloroethene1. 1-DichloroethaneTraris-1. 2-DichIocoetheneChloroform1. 2-Oichloroeihane2-Butanone1 , 1 , 1 -TrichloroeihaneCarbon TelrachlondeVinyl Acetale . - . ,Bromodichloromelhane1.2-Oichroropropane -Trans-1. 3-DichloropropeneTrichloroetheneDibromochloromethanel.-l.^-Trichloroeihane'"Benzenecis-1. 3-Dichloropropene2-Chloroethylvinylether -Bromoform2-Hexanone

4-Methyl-2-PentanoneTetrachlofoelhene1 , 1 . 2 , 2-TelrachloroethaneTolueneChlorobenzeneElhylberiieneStyreneTolal Xylenes

RF

o-^^/.Oî.ôu

0.50 lo

f '^77& . 1 0 7^--30J,^S•^.^^

/.o?/

S.O£?O.OS,î ;

o.^fcO' ••

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0. ̂ W

0,5^--0.^)0

f.Ollo.^ fc lO.QW,-

O'^'-l

o. a'?"?O./l/^

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C', '607-

l .~'Sl23

• /•0^^'b.S?'/./ . ^ ?>o .0,0t , 'a, .m,

^,)2. 1

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CCC

/

.. •y•-„ . . . . - . .

/. t/

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/v

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. SPCC-

• 4

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0

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RF50 -Respons® Factor Irom daily siandard file at 50 ug/1RF -Average Response Factor (rom iniTial calibration Fofrn VI

%D -Percent DifferenceCCC -Calibration Check Compounds (.1 ^SPCC -System Performance Check Compounds (-.)

Form Vll

. 0 ';• 0 6 0 0

SCANS 1 TO 1300RIC DATA: EPAUOA1718 #1CALI; EPAUWH718 ;#168/19/84 2;07;00

SAMPLES 50 UG/L STD. yERIFICATIONCONDS.; ;RANGE: G 1,1390 LABEL: N 0- 4.8 QUAN: A 0, 1.0 J 0 BASE; I) 20, 3

81400.0-1

RIC

|

|

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3t! Ifti. JUuLi '. .

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216tA

!006:59

I.

\

i

36 3

334

HI

i

9;

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40013;40

468

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339

; 7

93

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il

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1000

34:10

33

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413184

94

1 1 3 4A :

11

J V1185r ^-——^——^ . . .

' 1 '1200 SCAN41;00 TIME

QUANTITATION REPORT FILE:; EPAVOA171B

DATA- FpAUOAlTIR TT08/19/84 2:07:00 1 1SAMPLE: 50 UG/L STD. VERIFICATIONSUBMITTED BY: USTCO ANA4YST: RJM

AMOUNT-AREA(HGHT) » REF.AMNT/(REF. AREA(HGHT)* RESP.FACT)RESP. FAC: FROM A-VERAGE-OF-BHOt-E—Rt-——-————————————-

NO NAME1 » BROMOCHLORMETHANE (INTERAL STANDARD)2 * P-OIFLUOROBENZENE (INTERNAL STANDARD)3 * DICHLOROBENZENE-D5 (INTERNAL STANDARD)

. 4 . CHLOROMETHANE - •• : ; . . . . . . .5 BROMOMETHANE^ . . . VINYL CHLORIDE——,-——- -7 CHLORDETHANE ; •8 METHYLENE CHLORIDE9 ACROLEIN . . . . , . . , . .

10 ACRYLONITRILE11 1, 1-OICHLOROETHYLENE ,12 1.i-DICHLOROETHANE--——13 TRANS-1,2-OICHLOROETHYLENE1.4 . CHLOROFORM......-.....-.:---.-... : . .......15 1, 2-OICHLOROETHANE16 1. 1 - 1-TRICHLOROEtHANE17 HSL ACETONEIB HSL CARBON._DISULFIDE_.____. . .._.IB HSL CARBON DISULFIDE_ ___19 CARBOIM-TETRACHLORIDE——20 BROMODICHLOROMETHANE21 1, 2-DICHLOROPROPANE22 TRANS-1, 3-DICHLOROPROPYLENE23 TRICHLOROETHYLENE ..24 BENZENE25 DIBROMOCHLOROMETHANE26 1. 1. 2-TRICHLOROETHANE27 CIS-1, 3-DICHLOROPROPYLENE28 2-CHLOROETHYL.yiNYL-.ETHER .29 BROMOFORM - . - . - . . . .30 HSL METHYL ETHYL KETONE"31 HSL VINYL ACETATE32 HSL METHYL ISOBUTYL:-KETONE ———————33 1 2-DICHLOROETHANE-D4 (SURROGATE)34 BENZENE-06 (SUBBOGA^e-}:-:- - • : •: - -.. -i- -35 DIEROMOTETRAFLUOROETHANE (SURROGATE)36 BISCPERFLUOROISOPROPYDKETONE (SURROGATE)37 FLUOROEENZENE (SURROGATE)3B TETRftCHLOROETHYLENE39 1, 1, 2, 2-TETRACHLOROETHANE40 TOLUENE41 CHLOROBENZENE ' • •42 Ei-HYLBENZENE :

43 HSL 2-HEXANONE44 HSL STYRENE '•• ^•- -45 HSL 0-XYLEME ' "46 HSL M-XYLENE : .:

NOV!_

NAME - .

iB-4950

M-BROMOBei\17QTRTFI UnRTDF (gi IpRQgftTE)'D-5 ETHYLBENZENE ^SURROGATE)TOLUENE-OS (SURROGATE)P-BROMOPLUOROBENZENE (SURROGATE)

NO1-a345678

.....9...10111213141516171B192021222324252627282930313233343536373B3940414243

M/E13011411750946264B4

NOTNOT

616396836297.5876

1178363759578

129837563

1737286436584

NOTNOTNOT166

8391

1129143

8CAN-3S369885682

141173.216286

f—f\t unrvf-OUNt./FOUND

3694104384484715.15

. .-332.3345275395B3589664

• 6216276:2'?629661711466527

' 7244&7616

FOUNDFOUNDFOUND

7797S182686i3937771

T13232924579

121414

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-1011181B1920202123.212122241518241321

• 262628293226

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360041180636192500255507381325292935185500445703

374101230121

RE

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. 2222

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F RRT1; 000-1; 0001. 0000. 2140. 3680. 4520-5640. 747

0.; 9631. 0701. 1231.: 1701. 230

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0. 8720. 7550. 7720. 8350. 8440.; 8650. 8900. 8930. 9010. 9010. 9471. 0190.:6680.. 755.l.:0370;'66?0. 883

0.!9100. 9120. 9581..0051. 0950. 901

M—A

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BBBBBBBBBBBBBB- - • -BBVBVBBBBBBBBBBBVBBBBBBBBBBBBBBBVB

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AREACHGHS'0694.

421063.270424.

73182.110959.93619.52495.

125137.

195747.223113.102423.292127.182308.2427B9.

-5510.217319.246878.229425.143740.155035.177237.359159.136876.

86260.143230.

3286.57480.5182,

10673.: 51831.357650.70779B.

— — — - • . • - •

1B7353.'92589.

382610.280743.441490.

41443.

T) AMOUNT"SB:60050. 00050. 00047. 527SB. 37251. 411ST. 21238. 826

57.864" 56". 022

51. 77957. 323

- 55-. 364-57.26T-29-84043;89341. 73235. 84039.81336.26942.61642. 19130. 96133.00836.893

5. 75624.81822.12037, /03731. 07789. 11587. 242

44.18324.52041.65539.72239,53025.658

UG7LUG/LUG/LUG/LUG/LUG/LUG/LUG/L

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98—95—;

RET(L13: 0723: 4929:112: 484:49

- 3:537:219:46

10:1911: 0212: 3414.0014: 37

.151.1616: 0317: 3410: 1911: 2317: 5818:2519: 5320:0720:3621:0921:2321:2721:2722: 31^4T1815:5317:53:2-4:4215: 5720:59

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0. 930. 93 ,0. 930. 930. 930. 930. 930. 931. 28

METH,--A BBA BBA BB

A BBA BB -'

AMNT50. 0050. 0050. 0047. 5358. 5731.4157. 2138. 83

57. 8656. 0251. 7857. 3255. 3657. 2729. 8443. 8941. 7335. 8439. 8136. 2742. 6242. 1930. 9633. 0136. 89

5. 7624. 8222. 1237. 0431. 08- -89. 1287. 24

44. 1824. 5241. 6539. 7239. 5325. 6635. 1638, 1169. 85

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130178:127640,

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AMNT(L)50. 0050. 0050. 0030. 0050. 00507:0050. 0050. 0050. 00

250.00- 50.00

50. 0050. 0050. 0050. 0050. 0050. 0050- 0050. 0050. 0050. 0050. 0050. 0050. 0050. 0050. 0050. 0050. .00.50. 0050: 0050. 0050. 00

100. 00100. 00100. 00100. 00100. 0050. 0050. 0050. 0050. 0050. 0050. 0050. 0050. 8050. 00

100. 00

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2. 1582; 4601/1293.--2212. 0102. 6770. 0612. 3960. 5860. 5450. 3410. 3680. 4210. 8530. 3250. 2050. 3400. 008

-0.1370. 0120. 025

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0. 6930. 3421. 4151. 0381. 6330. 1530. 7350. 4810. 472

OUNT-rA5?-.-110.847

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CASE NO. 3089: BATCH NO. 5; CLP DIOXIN SHIPMENT RECORD · 2020. 8. 23. · 12:40 time. i-v q z 0 0...

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