Catalog 98-1400 0702 Bitumen · Bitumen and bituminous binders: ASTM D 36 - AASHTO T 53 EN 1427...

WWW.PETROTEST.COMManufacturer since 1873

2

Softening-Point (RKA)

Breaking-Point (BPA)

Flash-Point (CLA)

Petrotest® Instruments GmbH & Co KG... is producing high quality laboratory instruments for the research of petroleum products under quality control according to ISO 9001.

A wide range of equipment for the determination of the physical behavior of bitumen is offered.

Users of these instruments are mainly: • Refi neries• Road Construction Companies• Roofi ng Felt Manufacturers • Producers of Protective Coating for Architecture• Material Testing Authorities • Research Sections of Universities and Independent Test Institutions

Order Information:

Preview (upcoming instruments) .................................................................. 3

Softening-Point (RKA) ............................................................................ 4 - 9

Tensile Properties (DDA, DD) ................................................................ 10 - 15

Penetration & Texture (PNR, Rheotex) ................................................... 16 -19

Breaking-Point (BPA) ............................................................................. 20 - 23

Stiffness (BBR) .............................................................................................. 24

Viscosity (DSR, RV) ............................................................................... 25 - 35

Aging (LOH, TFOT, RTFOT, RFT, PAV) .................................................. 36 - 40

Flash-Point (CLA, PMA, TAG) ................................................................ 41 - 51

Paraffi n Content ............................................................................................ 52

Water Content ......................................................................................... 53 - 55

Distillation ............................................................................................... 56 - 59

Density & Weight .................................................................................... 61 - 64

Sampling ........................................................................................................ 65

General Equipment Reference Material ..................................................................................... 66Miscellaneous Equipment .......................................................................... 67Tempering Equipment ......................................................................... 68 - 69

Tables of Contents Keywords .................................................................................................... 71Order Numbers ................................................................................... 72 - 74Standards ................................................................................................... 75

Petrotest® Company ..................................................................... on the rear

Table of ContentsTable of Contents

3

Display

10-0800 &Keyboard & Barcode-Scanner

18-1120

Softening-Point - Ring & Ball Method - RKA 5 (automatic)

10-080010-0801

RKA 5 - Automatic Softening-Point Tester Ring and Ball MethodASTM D 36 - AASHTO T 53 - EN 1427 (DIN 52 011, NF T66-008) - IP 58 - JIS K2207 EN 13 179-1 (With optional accessories for: DIN 1996-15 or referee tests acc. IP & NF)Further for resins (ASTM E 28), paints and varnishes (ISO 4625-1 - BS 6782-6) and thermoplastic adhesives (EN 1238 (NF T76-106))Consisting of:CPU:Up-to-date dual OMAP controller technology featuring a DSP and a real-time multimedia coprocessor, 4.7” full graphical color display, graphical menu guidance and intuitive user concept (Pmove), help key (explanation of important device/ program features), Jog-Wheel operation (turn & push), large-area device status indicator (light ring), zooming temperature reading to a visual distance of 10 m (33 ft), device & data management via LAN, USB or RS232, extended statistical and database functionality, automatic assessment of results according to individual standards, printout on heat gradient conformity.Electronic device features:Automatic self check of sensors and system, multipoint calibration of temperature sensor (PT-100), compact ball sensing system consisting of a precise 3D-adjustable laser scanner.Mechanical device features:Infrared radiator technology with temperature control, CERAN heat plate with spill protection, standardized beaker with barcode imprint, test rack with slide bearing and single-hand fi xation, PT-100 gold plated four-wire system (also available with calibration certifi cate), test rings, load balls, centering guides, stirring wheel, holding tong, mechanical ball centering system, software controlled stirrer system, transparent draft defl ector.Supplied with:10 rings (shouldered), 10 load balls, 2 ball centering guides (for shouldered rings), 1 test rack with mechanical ball centering unit, 1 glass-beaker bath (600 ml) with barcode, 1 temperature probe (Pt-100), 1 magnetic stirrer wheel, 1 pouring plate (brass)Note:Accessories like external illuminated USB-keyboard outline 86 keys, barcode handy scanner for sample identifi cation, USB memory stick, CF-card for internal memory extension, laser or needle printer (EPSON), electro-magnetic ball & centering unit, bath liquid and optional test accessories are not included.Technical Data: Test places : 2 (for simultaneous tests)Housing : stainless steel, two colored powder coatingInterface : 1 serial RS232, 3 USB, 1 LAN (LIMS)Dimensions : 230 x 470 x 460 cm (WxDxH), Weight: 10 kgPower supply : 230 V, 50/60 Hz, EU-plugPower supply : 115 V, 50/60 Hz

PreviewPreview

Plastic Properties - Penetrometer Method - PNR 12

18-1120 PNR 12 - Automatic PenetrometerAccessories have to be selected according to the standard. (Suitable for: Needle-, Cone-, Rod-Penetration and further methods)Consisting of:Microcomputer, electronic distance measuring device, stepper motor for exact positioning, 24 V safety voltage supply, stable base plate and housing.Microcomputer: Large graphical monochrome display, intuitive graphical menu, status feedback to operator, Jog-Wheel driven menu (turn & push), storage of last 200 measurements.Electronic Elements: Distance measuring device (1/100 mm), stepper motor, ultra bright LED-sample illumination on fl exible arm, electronic detector for conductive samples, USB-interface for printer & memorystick.Mechanical Elements:Penetrometer base plate with leveling feet and removable aluminum test table, instrument housing two colored powder coated, splash water protected membrane keyboard, plunger holder with solenoid release mechanism.To be ordered separately: Test Accessories (test kit, needle, cone etc.) are required!

Technical Data:Measuring range : 0 to 55 mmMax. test load : 2 kgResolution : 0.01 mm Test duration : 0.1 to 9999.9 seconds (preset standard duration: 5 seconds)Start delay : adjustable up to to max. of 9999.9 sec. (2.78 hours)Data output : USB interface to connect printer or USB-stick0-Point detector : for electrically conductive samples Dimensions : 300 x 310 x 580 mm (WxHxD), weight 10 kgPower supply : 100/240 V, 50/60 Hz, EU-plug

Features:• Pmove™ - innovative

operation platform• large color display

- visible from 10 m (30 ft.)• easy Firmware-Upload

via USB• compact ball detection

system• Ready-to-Go Unit

for 2 simultaneous tests

Features:• manual positioning

by Jog-Wheel operation• electronic positioning

to a preset depth with Memory-function

• surface detection by conductivity sensor

• 10 user programs possible• data transfer to USB-Stick

possible• extra bright LED-sample

illumination

4

Test-Run

Softening-Point - Ring & Ball Method - RKA 2 (automatic)

Bitumen and bituminous binders: ASTM D 36 - AASHTO T 53 EN 1427 (DIN 52 011, NF T66-008) IP 58 JIS K2207Filler aggregats in bituminous mixtures: EN 13179-1Wilhelmi-Option: DIN 1996-15 EN 1871-F

The RKA 2 automatic tester is microprocessor controlled, with separate programs for testing in 3 bath fl uids (water, glycerin or silicon oil) and 2 Wilhelmi programs. An additional program can be modifi ed and optimized by the user.

A backlit LC-display shows test conditions of the two test positions simultaneously with:• expected softening point• program selected• actual bath temperature

The following parameters may be entered using the membrane keypad:• selected program to run• temperature display in °C or °F

Over-temperature protection is also included as a standard feature. The housing is durable stainless steel.

A Pt-100 sensor measures the temperature. A low-mass heating device, especially designed for maintaining precise temperature gradients, is designed with infrared heater to protect the user.

Stirring motion is program-controlled to optimize the heating gradient. The low-mass design of the heating and stirring assembly allows rapid and convenient cool-down by an effi cient fan.

An automatic load-ball-holder ensures automatic application of load balls at the proper moment in the program sequence.

Two light barriers detect the softening-point. The test result is stored until a new test is started.

External output includes an RS232 printer interface to give a full report of the two positions, including:• test result• selected program

Scope of ApplicationTo determine the temperature at which a substance attains a particular degree of softness.

Suitable for bitumen & bituminous binders, fi ller aggregates used in bituminous mixtures, binders for paints and varnishes and resins derived from naval stores.

Summary of MethodTwo horizontal disks of a sample (cast in shouldered rings) are heated at a controlled rate in a liquid bath (up to 80°C in distilled water or silicon oil, above +80°C in glycerin or silicon oil) while each supports a steel ball. The softening-point is reported as the mean of the temperatures at which the two disks soften enough to allow each ball to fall a distance of 25 mm.

SofteningSoftening-Point-Point

5

10-0181

RKALog Cable & 10-0599

Set-Up "Wilhelmi"

Set-Up "Ring & Ball"

Main Units

10-018110-0182

RKA 2 - Automatic Softening-Point Tester, Ring & Ball MethodASTM D 36 - AASHTO T 53 - EN 1427 (DIN 52 011, NF T66-008) - IP 58 - JIS K2207 EN 13 179-1 (With optional accessories for: DIN 1996-15 or referee tests acc. IP & NF)Further for resins (ASTM E 28), paints and varnishes (ISO 4625-1 - BS 6782-6)Features:• automatic heating with over-temperature protection• automatic ball application with delay period by magnetic ball holders• automatic softening-point detection of both samples by separate light-barriers• automatic temperature display and storage at the moment of softening • standardized softening-point determination of: bituminous binders, resins,

adhesives, paraffi n, polymers, sealing compounds (Wilhelmi-Option), waxesConsisting of:stainless steel housing, membrane keypad, digital display (LCD), heater with over-temperature protection and automatic temperature regulation, program-operated stirrer, two light-barriers for automatic softening-point detection, support for two test rings, automatic ball application by two magnetic ball holders.Three basic programs for the following bath liquids: water, glycerin, silicon oil. Additional user defi nable program to store a special heating program with variable parameter and 2 Wilhelmi-programs.Supplied with: 10 rings (shouldered), 10 load balls, 2 ball centering guides (for shouldered rings), 1 gage-ball for light barrier adjustment, 1 glass-beaker bath (600 ml), 1 heater support board (70 mm bored ), 1 temperature probe (Pt-100), 1 magnetic stirrer rod, 1 pouring plateNote: bath liquids, accessories for PC connection are not included.Technical Data:Test places : 2Working range : approx. +25 to +200 °C Connections for : serial printerDimensions / Weight : 36 x 32 x 40 cm (W x D x H), 10 kgPower supply : 230 V, 50/60 Hz, 1000 W, EU-plugPower supply : 115 V, 50/60 Hz, US-plug

10-026410-0265

RKA 2a - Automatic Softening-Point Tester, Ring & Ball Methodwithout magnetic ball-holders and automatic ball application.Otherwise same like RKA 2Power supply : 230 V, 50/60 Hz, 1000 W, EU-plugPower supply : 115 V, 50/60 Hz, US-plug

Accessories

10-1181 PC Software - RKALog (Windows®)A program for transfer the RKA values (like parameters, date, time, user, fi le etc.) to a PC. Replacing the serial data-printer.Supplied with: 1 serial printer-data-cable (RS232, 25-pin), 1 adapter (9-pin & 25-pin), 1 adapter (25-pin & 25-pin)Note: For a faultless data-transmission to an USB-port

the verifi ed USB/RS232-converter is recommended.

11-0599 USB/RS232-Converter with 2 m cable (verifi ed for Petrotest®-units)connecting 1 serial port with the USB-port of a PC or Hub.

25-028225-0283

Serial Impact Printer to record data like test results, duration of test, etc. without a PC.For details see: General Equipment, page 67Power supply : 220/240 V, 50/60 HzPower supply : 110/130 V, 50/60 Hz

50-5315 Tongs for beaker

50-9167 Bath Liquid, silicon oil, water clear, 1 kg, heat resistant up to approx. +250 °C, viscosity at +25 °C: 190 till 210 mPa·s


6

10-0285

10-0052 & 10-0049

Load Balls (10-0055 & 10-0077)

10-0079 & Rings

10-0480 & 10-0289

10-0051 & 10-0048

RKA & Wilhelmi-Set

Options10-0070 Mortar with pestle (acc. ISO 4625, ASTM E 28)

For former referee tests acc. IP 58 & NF T66-008:

10-0048 Rings, tapered (former IP & NF), pack of 10

10-0051 Ball Centering Guide for tapered rings (former IP & NF)

For tests acc. Wilhelmi-Method:

10-0285 Conversion Set “Softening-Point - Wilhelmi“ (DIN 1996-15)used for Mastix determinationConsisting of: 1 holder assembly 1 ring with bayonet lock 1 ball-centering gauge,10 load balls (Ø 15 mm, 13.9 g) 1 magnetic suspender, 1 heater support board with center hole (Ø 89 mm / 3½”), 1 glass beaker (1000 ml)

Spare Parts10-0055 Load Balls, steel

(Ø 9.5 mm, 3.5 g), pack of 10

10-0077 Load Balls (Wilhelmi), steel (Ø 15 mm, 13.9 g), pack of 10

10-0289 Gauge-Ball for light barrier adjustment

10-0052 Ball Centering Guide for shouldered rings

10-0480 Ring-Holder Assembly for 2 rings

10-0049 Rings, shouldered, nickel-plated brass, pack of 10 (acc. ASTM, ISO, EN, IP, NF)

10-0075 Ring (Wilhelmi) with bayonet lock

10-0056 Glass Beaker (600 ml) as bath

10-0106 Glass Beaker (Wilhelmi) (1000 ml)

50-5229 Magnetic Stirrer Rod (8.5 x 70 mm)

10-0079 Pouring Plate, brass, U-shape (50 x 75 mm) to fi ll the rings

12-0378 Temperature Probe Pt-100 with plug (Ø 4.5 x 85 mm)

11-013911-0140

Support Board for heater, glass ceramics, (150 x 150 x 4 mm)... center hole (Ø 70 mm / 2¾”),... center hole (Ø 89 mm / 3½”),

11-0018 Heater Rod, 200 W, 115-230 V

11-001911-0029

Heating Element (4 heater rods)... 230 V, 50/60 Hz, 800 W ... 115 V, 50/60 Hz, 800 W

25-000425-0009

Control Module “M2” to regulate the heating power... 230 V, 50/60 Hz... 115 V, 50/60 Hz


7

10-0281

50-5315

Ring & Ball Accessories

Softening-Point - Ring & Ball Method (manual)

Bitumen and bituminous binders: ASTM D 36 - AASHTO T 53EN 1427 (DIN 52 011, NF T66-008) - IP 58JIS K2207

Filler aggregats in bituminous mixtures: EN 13179-1(Wilhelmi-Option: see next page)

Main Units

10-028110-0284

Manual Softening-Point Tester, Ring & Ball MethodASTM D 36 - AASHTO T 53 - EN 1427 (DIN 52 011, NF T66-008) - IP 58 - JIS K2207 EN 13 179-1 (with optional accessories for referee tests acc. IP & NF)Further for resins (ASTM E 28), paints and vanishes (ISO 4625-1 - BS 6782-6)Features: • 2 simultaneous tests• electric heating• electric stirrerConsisting of:electric heater (800 W) in stainless steel housing with electronic power regulator, 4 heater rods, electric stirrer and support for two test ringsSupplied with: 10 shouldered rings, 10 load balls, 2 ball centering guides, 2 thermometers (precision made, 1 x ASTM 15C, 1 x ASTM 16C), 1 glass beaker (600 ml), 1 heater support board (bored, 50 mm / 2”), 1 pouring plate (brass), 1 mortar with pestleTechnical Data:Test places : 2Working range : approx. +25 to +200 °C Dimensions / Weight : 16 x 18.5 x 20.5 cm (W x D x H), 3 kgPower supply : 230 V, 50/60 Hz, 800 W, EU-plugPower supply : 115 V, 50/60 Hz, 800 W, US-plug

Options & Accessories50-5315 Tongs for beaker

50-9167 Bath Liquid, silicon oil, water clear, 1 kg, water clear, heat resistant up to approx. +250 °C, viscosity at +25 °C: 190 till 210 mPa·s

For former referee tests acc. IP 58 & NF T66-008:10-0048 Rings, tapered (former IP & NF), pack of 1010-0051 Ball Centering Guide for tapered rings (former IP & NF)

Thermometers

Precision Made

Offi cially Certifi ed

TypeRange

ASTM IP10-0061 10-0062 15C 60C -2 to +80 : 0.2 °C10-0063 10-0064 15F - +30 to +180 : 0.5 °F10-0065 10-0066 16C 61C +30 to +200 : 0.5 °C10-0067 10-0068 16F - +85 to +392 : 1.0 °F

Spare Parts10-0052 Ball Centering Guide

for shouldered rings

10-0055 Load Balls, steel (Ø 9.5 mm, 3.5 g), pack of 10

10-0049 Rings, shouldered, nickel-plated brass, pack of 10 (acc. ASTM, ISO, EN, IP, NF)

10-0455 Ring-Holder Assembly for 2 rings

10-0056 Glass Beaker (600 ml) as bath

10-0070 Mortar with pestle (ISO 4625, ASTM E 28)

10-0079 Plate, brass, U-shape (50 x 75 mm) as pouring plate to fi ll the rings

11-0138 Support Board for heater, glass ceramics, (150 x 150 x 4 mm), with center hole (Ø 50 mm / 2”)

11-0018 Heater Rod, 200 W, 115-230 V

11-001911-0029


25-000425-0009

Control Module “M2” to regulate the heating power... 230 V, 50/60 Hz... 115 V, 50/60 Hz

25-004225-0043

Electric Stirrer with propeller blade... 230 V, 50/60 Hz, EU-plug... 115 V, 50/60 Hz, US-plug

Scope of ApplicationTo determine the temperature at which a substance attains a particular degree of softness.

Suitable for bitumen & bituminous binders, fi ller aggregates used in bituminous mixtures, binders for paints and varnishes and resins derived from naval stores.

Summary of MethodTwo horizontal disks of a sample (cast in shouldered rings) are heated at a controlled rate in a liquid bath (up to +80 °C in distilled water or silicon oil, above +80 °C in glycerin or silicon oil) while each supports a steel ball. The softening-point is reported as the mean of the temperatures at which the two disks soften enough to allow each ball to fall a distance of 25 mm.


8

Wilhelmi-Ring (10-0075)

10-0071

Scope of ApplicationTo determine the temperature at which a hot casting substance used in road construction attains a particular degree of softness.

Suitable for joint sealing compounds in road construction and thermoplastic materials for pavement marking.

Summary of MethodA horizontal disk of a sample casted in a ring supports a steel ball and is heated at a controlled rate in a liquid bath (up to +80°C in distilled water or silicon oil, above +80°C in glycerin or silicon oil).The softening-point is reported as the temperature at which the softening disk experiences a plastic deformation.

Softening-Point - Wilhelmi Method (manual)

Bituminous materials: DIN 1996-15 Thermoplastic materials: EN 1871-F

Main Unit

10-0071

Manual Softening-Point Tester, Wilhelmi MethodFeatures: • single test place• electric heating• electronic power regulatorConsisting of:electric heater (800 W) in stainless steel housing with electronic power regulator “M2”, 4 heater rods, laboratory stand (1 bar, 1 special clamp, 1 ring support)Supplied with: 1 Wilhelmi-ring, 10 load balls 2 thermometers (precision made, 1 x ASTM 15C, 1 x ASTM 16C), 1 glass beaker (1000 ml), 1 heater support board (bored, 50 mm / 2”), 1 pouring plate (glass)Technical Data:Test place : 1Working range : approx. +25 to +200 °C Dimensions / Weight : 16 x 18.5 x 20.5 cm (W x D x H), 3 kgPower supply : 230 V, 50/60 Hz, 800 W, EU-plug



For automatic tests see Ring & Ball-Apparatus RKA 2:10-0181 RKA 2 - Automatic Softening-Point Tester, Ring & Ball Method10-0285 Conversion Set “Softening-Point - Wilhelmi“

Thermometers

Precision Made


TypeRange


Spare Parts10-0077 Load Balls (Wilhelmi), steel

(Ø 15 mm, 13.9 g), pack of 10

10-0075 Rings (Wilhelmi) with bayonet lock

10-0076 Ring-Holder (Wilhelmi)

10-0106 Glass Beaker with spout (1000 ml) low shape, as bath

10-0057 Plate, glass (120 x 120 x 6 mm) as pouring plate to fi ll the rings

11-0138 Support Board for heater, glass ceramics, (150 x 150 x 4 mm)with center hole (Ø 50 mm / 2”)

11-0018 Heater Rod, 200 W, 115-230 V

11-0019Heating Element (4 heater rods)... 230 V, 50/60 Hz, 800 W

25-0004

Control Module “M2” to regulate to heating power... 230 V, 50/60 Hz


9

10-0081

Softening-Point Tester - Kraemer-Sarnow Method (manual)

Carbonaceous materials: DIN 52 025

Main Unit

10-008110-0082

Manual Softening-Point Tester, Kraemer-Sarnow MethodFeatures: • 4 test-places• electric heating• electronic power regulatorConsisting of:electric heater (800 W) in stainless steel housing with electronic power regulator „M2“, 4 heater rods, support with ring (for 250 ml beaker) and bored plate (for 4 glass-tubes & 1 thermometer)Supplied with: 4 BARTA-tubes (stainless steel) 4 glass tubes (Ø 8 x 100 mm), 4 connecting hoses (Ø 6 x 6 mm), 4 rubber bungs (7 mm bored), 2 thermometers (precision made, 1 x ASTM 15C, 1 x ASTM 16C), 2 glass beakers (1 x 250 ml, 1 x 600 ml), 1 heater support board (bored, 38 mm / 1½“), 1 glass plate Note: Mercury measuring device (5 g) is not includedTechnical Data: Test places : 4Working range : approx. +25 to +200 °C Dimensions / Weight : 16 x 18.5 x 20.5 cm (W x D x H), 3 kgPower supply : 230 V, 50/60 Hz, 800 W, EU-plugPower supply : 115 V, 50/60 Hz, 800 W, US-plug



Thermometers

Precision Made


TypeRange


Spare Parts10-0087 BARTA Tube, stainless steel,

(Ø 8 x 5 mm), as sample container

10-0089 Glass Tube (Ø 8 x 100 mm)

10-0096 Bung, NBR-rubber (7 mm bored) as glass tube holder

10-0097 Hose, rubber (Ø 6 x 6 mm), connecting glass-tube with BARTA-tube

10-0057 Plate, glass (120 x 120 x 6 mm) for sample preparation

10-008613-0147

Glass Beaker, high shape... as inner bath (250 ml), w/o spout... as outer bath (600 ml) with spout

10-0084 Support with ring (for 250 ml beaker) and bored plate (for 4 glass-tubes & 1 thermometer)

11-0137 Support Board for heater, glass ceramics, (150 x 150 x 4 mm)with center hole (Ø 38 mm / 1½”)

11-0018 Heater Rod, 200 W, 115-230 V

11-001911-0029


25-000425-0009

Control Module “M2” to regulate to heating power... 230 V, 50/60 Hz... 115 V, 50/60 Hz

Scope of ApplicationTo determine the lowest temperature at which a mercury load deforms a sample under standardized conditions.

Suitable for carbonaceous materials like pitch and other materials melting above +30°C.

Summary of MethodA BARTA-tube fi lled with a sample is connected to a glass-tube and loaded with mercury. Two samples are heated in a liquid bath. At rising temperatures the sample deforms under the weight of the mercury.The softening-point is reported as the temperature at which the mercury breaks through the softening sample.


10

Temperature Probes

Molds

Scope of ApplicationThe Ductility or Elongation is measured by the distance to which a sample will elongate before breaking when two ends of a specimen briquette are pulled apart at a specifi ed speed and at a specifi ed temperature.It may be used for quality specifi cations.

The Force-Ductility measures tensile properties on the basis of the performed force and the specimen strain.A specimen briquette is pulled apart at a specifi ed speed and at a specifi ed temperature until the briquette ruptures or a specifi ed strain is achieved.

The Elastic Recovery is measured by the recoverable strain determined after severing an elongated briquette specimen. The specimens are pulled to a specifi ed distance at a specifi ed speed and at a specifi ed temperature.This is useful in confi rming that a material has been added to the asphalt to provide a signifi cant elastomeric characteristic.

Tensile Properties - Force-Ductilometer Method - DDA 3 (automatic)

Elongation: ASTM D 113 - AASHTO T 51 - JIS K2207 (DIN 52 013, IP 32, NF T 66-006)Force-Ductility: EN 13589 - IP 520 EN 13703 - IP 515 - AASHTO T 300

Elastic Recovery: ASTM D 5892 (ASTM P 226) - ASTM D 6084 - AASHTO T 301 - EN 13398 (DIN V 52 021-1) - IP 516

With the ductility machines of the DDA 3 series the afore mentioned procedures can be performed automatically. Except for recovery tests, 3 tests can be performed simultaneously.

The drive is microprocessor controlled and uses a stepping motor and a feed rod. Both are located outside the tempering bath and therefore are not affected by corroding infl uences of the bath liquid.The tempering bath itself is double-walled with an outer water circulation system.The tractor cradle is made of stainless steel as well as the bath walls.

If extremely thin threads are measured, the built-in circulation pump for the inner bath can be switched off.

A very even and exact temperature can be obtained in the bath by the connection of a good coolant circulator and due to several temperature probes plus the transparent bath cover.

Traction speed, elongation and pauses can be pre-set on the control unit.During the whole test run the tensile force on each line is permanently measured. The maximum tensile force may be up to 300 Newton’s per line.

With the DDA 3 a minimum tensile force margin can be set. When a bitumen briquette ruptures and the tensile falls below this setting, the pertinent elongation will be stored and the machine will be stopped automatically after all three briquettes have broken.

There is a special program for recovery tests of polymer-modifi ed bitumen.The bitumen briquette will be expanded to a pre-set elongation, then the tractor (after a pause) returns to a position where no more stress is in the material, equivalent to the cut-up state of the specimen. If due to any recovery of the material a tension should occur, the tractor will move until there is a stress-free condition again.

The control unit is equipped with two RS232 interface. This allows to connect a serial printer and a PC to record all test parameters, the fi nal values on each test line as well as peaks with their pertinent elongation.Further, the DDA 3 has analog output sockets so that force/elongation curves can be drawn.

The ductility meters are also available as DD 3 in a basic version without force measurement. These models have a digital indication of the elongation only.

Tensile PropertiesTensile Properties

11

Software Diagram "Force"

Recovery Test

Elongation Test

Software Diagram "Recovery"

Printer Chart "Recovery"

Printer Chart

Located Points

DDACon-SoftwareA program for recording, saving and graphic presentation of DDA values.Replacing analog line recorder or serial data-printer, allows to control the DDA by PC, the data-transfer to MS EXCEL® or LIMS and simplifi es the download of fi rmware-upgrades.The sample status of up to 3 samples will be displayed simultaneously, indicating the traction distance or for Recovery-tests the percentage of relief and the total energy.Signifi cant points like the local minimum, maximum, turn-points of in- & decreasing fl anks and tangent-points can be determined automatically and displayed as diagram or chart.The numerical display of force or distance for a single point on the curve is possible, too.

Individual diagram areas can be increased, curves can be hidden or indicated numerically.Since every sample will be saved under an individual fi lename, it is possible to compare 3 samples of different tests with each other.The evaluated data can be exported as ASCII-fi les. They include information like the sample name, fi le name, user ID, date & time, duration, program, speed, temperature at start & end, status and distance & force.Printing of numerical or graphic evaluations, including relevant point like maxima and fracture are possible on a usual printer.

Main UnitsDDA 3 - Automatic Tensile Property Tester, Force-Ductilometer MethodDepending on the accessories suitable for: Elongation: ASTM D 113 - AASHTO T 51 - JIS K2207Recovery : ASTM D 5892 - ASTM D 6084 - AASHTO T 301 - EN 13 398 - IP 516Force : EN 13 589 - IP 520 - EN 13 703 - IP 515 - AASHTO T 300 (obs.: ASTM P 226, DIN 52 013, DIN V 52021-1, IP 32, NF T 66-006)Features: • 2 elongation & 2 recovery programs• variable traction speed up to 140 mm/min.• force detection by high resolution (10 mN) 300 N-sensors• automatic rupture detection above 20 mN is possible• constancy of speed and temperature at minor bath motion is better than demanded by the standards• without cooling coils, therefore easy to cleanConsisting of:Bath: for 3 simultaneous tests, made of stainless steel, double-walled and full insulated, closed cycle cooling system, circulation pump to be switched off, temperature probe, bath illumination and acrylic bath cover.Control Unit: with microprocessor, membrane keypad, digital display (LCD) of program, traction speed, distance, tensile force and temperature; analog output for 3 force-channel line-recorder, RS232-interfaces for printer & PC4 Programs: - Semi-Automatic Elongation for rupture forces below 20 mN

- Automatic Elongation for rupture forces of 20 mN to 300 N- Semi-Automatic Elastic Recovery for polymer modifi ed bitumen (in accordance with ASTM D 6084, EN 13 398 and other methods)- Automatic Elastic Recovery for polymer modifi ed bitumen (similar to ASTM D 6084 and other methods)

Serial Printer: for continuous paper (incl. data transmission cable)makes printouts of 3 test points with following parameters:program, traction speed, distance, tensile forces, temperatures, percentage of elastic recovery, energy (the result of integral) (not suitable for DDACon-software printouts)Note: External cooling device for fi lling the bath-jacket is required.

Windows® PC-Software DDACon is available.Technical Data : Working range : approx. -10 to +60 °C (depending on the cooler)Travel length : 100 cm or 150 cm (maximum)Test positions : 3 (in a 30 l or 45 l bath)Traction speed : Standard: 50 mm/min. / Variable: 2.5 to 140 mm/min.Tension force : 300 N (maximum)Connections for : line-recorder, serial printer, PC (RS232), cooler as tempering & fi lling device (Ø 8 mm)


12

11-0360 & 10-0364

10-0335 & 10-0333

25-0228

Printer Chart

10-0404

10-0380

Main Units

10-036010-0361

DDA 3/100 - for test length up to 100 cmSupplied with: 3 molds (acc. ASTM D 113, if not ordered otherwise), 3 mold-holders, 2 corrosion protection specimen, 2 contrast inlays and distance piecesTechnical Data: Travel length : 100 cm (maximum)Dimensions of Bath : 170 x 40 x 50 cm (W x D x H), weight: 70 kg Controller : 35 x 25 x 15 cm (W x D x H), weight: 6 kg Printer : 34 x 29 x 15 cm (W x D x H), weight: 5 kgPower supply : 220/240 V, 50/60 Hz, EU-plugPower supply : 115 V, 60 Hz, US-plug

10-036410-0365

DDA 3/150 - for test length up to 150 cm Supplied with: 3 molds (acc. ASTM D 113, if not ordered otherwise), 3 mold-holders, 2 corrosion protection specimen, 3 contrast inlays and distance piecesTechnical Data: Travel length : 150 cm (maximum)Dimensions of Bath : 220 x 40 x 50 cm (W x D x H), weight: 92 kg Controller : 35 x 25 x 15 cm (W x D x H), weight: 6 kg Printer : 34 x 29 x 15 cm (W x D x H), weight: 5 kgPower supply : 220/240 V, 50/60 Hz, EU-plugPower supply : 115 V, 60 Hz, US-plug

10-038010-0381

Circulator (for external & internal cooling & heating)Necessary as tempering & fi lling device for the DD/DDA bath jacket and for reaching a bath-temperature of approx. -10 to +60 °C (at +20 °C ambient temperature).Consisting of:Cooler with stainless steel bath. Thermostat with digital display, splash-proof keypad, heater, pump, RS232/RS485-interface, Pt-100-socket, programmer, over/under-temperature & low-level protection, adjustable pump-pressure, proportional cooling control.Supplied with: 1 bath cover, 1 drain tap, 1 junction line for temperature probeNote: Insulated hose matter is not included but recommended.

For details see: General Equipment, page 68Dimensions / Weight : 37 x 46 x 71 cm (W x D x H), 49 kgPower supply : 230 V, 50 Hz, EU-plugPower supply : 230 V, 60 Hz

25-0228 Hose-Set, insulated (Ø 8 mm, 2x 2 m, incl. fi ttings)

Data Evaluation

10-0404 PC Software - DDACon (Windows®)A program for recording, saving and graphic presentation of DDA values.Replacing analog line recorder or serial printer, allows to control the DDA by PC, the data-transfer to MS EXCEL® or LIMS and simplifi es the download of fi rmware-upgrades.Supplied with: 1 PC-data-cable, 1 USB/RS232-converter


13

10-0332

10-0334

10-0335

10-0336

10-0403 & DDA

18-0403

10-0379

Options and Accessories

10-033210-033410-033510-0336

Mold (4-piece), brass, for the preparation of bitumen briquettes... according to EN 13 398 - IP 516... according to former DIN 52 013 - NF T 66-006 - IP 32... according to ASTM D 113 - AASHTO T 51... according to ASTM D 5892 - ASTM D 6084 - AASHTO T 300 & 301 - EN 13 589 - EN 13 703 (former ASTM P 226) - IP 515 - IP 520

10-0333 Mold Holder (fi ts 10-0332, 10-0334, 10-0335 and 10-0336)

10-0379 Calibration Set - DDA/DDConsisting of: 1 set of precision resistor plugs, 3 weights with steel-rope, 1 pulley, 1 certifi ed thermometer (0 to +50 : 0.1 °C), 1 thermometer holder,1 digital stop watch, 1 tape-measure with mm-division

10-038310-0384

Thermometer, for DDA/DD-calibration set... DIN 12 775, range 0 to +50 :0.1°C, precision made... DIN 12 775, range 0 to +50 :0.1°C, offi cially certifi ed (incl. in calibration set)

10-0403 Rack 80 x 25 x 42 cm (L x W x H) to place controller and printer behind the ductilometer

18-040318-0402

Circulator-Bath (for external & internal heating)Used for pre-tempering of samples (e.g. DD/DDA-molds)Note: It requires counter-cooling by a circulation cooler or thermostatic circulator for

applications near ambient temperatures. Hose matter is not included.For details see: General Equipment, page 68

Dimensions / Weight : 37.5 x 45 x 47.5 cm (W x D x H), 3.4 kgPower supply : 230 V, 50 Hz, EU-plugPower supply : 115 V, 60 Hz

11-0181 Hose, silicon (Ø 8 mm, 8 m)

Spare Parts10-0377 Contrast Inlay

(6 x 170 x 550 mm) pack of 1

10-0406 Corrosion Protection Specimen (200 x 100 mm) pack of 2

11-0599 USB/RS232-Converter with 2 m cable (verifi ed for Petrotest®-units)connecting 1 serial port with the USB-port of a PC or Hub.


14

Molds in Bath

Themometer in Bath

Tensile Properties - Ductilometer Method - DD 3 (semi-automatic)

Elongation: ASTM D 113 - AASHTO T 51 - JIS K2207 (DIN 52 013, IP 32, NF T 66-006)

Elastic Recovery: ASTM D 5892 (ASTM P 226) - ASTM D 6084 - AASHTO T 301 - EN 13398 (DIN V 52 021-1) - IP 516

Ductility gives an indication of the suitability of bituminous materials for specifi c applications such as road construction etc.

In order to determine the particular properties of polymer modifi ed bitumen, the method of elastic recovery has turned out to be more expedient.

Main Units

DD 3 - Semi-Automatic Tensile Property Tester, Ductilometer Method

Depending on accessories suitable for:Elongation : ASTM D 113 - AASHTO T 51 - JIS K2207Recovery : ASTM D 5892 - ASTM D 6084 - AASHTO T 301 - EN 13 398 - IP 516(obs.: ASTM P 226, DIN 52 013, DIN V 52021-1, IP 32, NF T 66-006)Features: • 1 elongation & 1 recovery program• variable traction speed up to 140 mm/min.• constancy of speed and temperature at minor bath motion is better than demanded by the standards• without cooling coils, therefore easy to cleanConsisting of:Bath: for 3 simultaneous tests, made of stainless steel, double-walled and full insulated, closed cycle cooling system, circulation pump to be switched off, bath illumination and acrylic bath cover.Control Unit: with microprocessor, membrane keypad, digital display (LCD) of program, traction speed, distance, RS232-interface for printer 2 Programs: - Semi-Automatic Elongation for rupture forces below 20 mN

- Semi-Automatic Elastic Recovery for polymer modifi ed bitumenSerial Printer: for continuous paper (incl. data transmission cable)makes printouts of 3 test points with following parameters: program, traction speed, distanceNote: External cooling device for fi lling the bath-jacket is required.

Technical Data : Working range : approx. -10 to +60 °C (depending on the cooler)Travel length : 100 cm or 150 cm (maximum)Test positions : 3 (in a 30 l or 45 l bath)Traction speed : Standard: 50 mm/min. / Variable: 2.5 to 140 mm/min.Tension force : 300 N (maximum)Connections for : serial printer, cooler as tempering & fi lling device (Ø 8 mm) Dimensions: Bath (100 cm travel length) : 170 x 40 x 50 cm (W x D x H), weight: 70 kg

Bath (150 cm travel length) : 220 x 40 x 50 cm (W x D x H), weight: 92 kgController : 35 x 25 x 15 cm (W x D x H), weight: 6 kg Printer : 34 x 29 x 15 cm (W x D x H), weight: 5 kg

10-035010-0351

DD 3/100 - for test length up to 100 cmSupplied with: 3 molds (acc. ASTM D 113, if not ordered otherwise), 3 mold-holders, 2 corrosion protection specimen, 2 contrast inlays, 2 distance pieces, 3 thermometers ASTM 63C, 3 thermometer-holdersTravel length : 100 cm (maximum)Power supply : 220/240 V, 50/60 Hz, EU-plugPower supply : 115 V, 60 Hz, US-plug

10-035410-0355

DD 3/150 - for test length up to 150 cm Supplied with: 3 molds (acc. ASTM D 113, if not ordered otherwise), 3 mold-holders, 2 corrosion protection specimen, 3 contrast inlays, 3 distance pieces, 3 thermometers ASTM 63C, 3 thermometer-holdersTravel length : 150 cm (maximum)Power supply : 220/240 V, 50/60 Hz, EU-plugPower supply : 115 V, 60 Hz, US-plug

Scope of ApplicationThe Ductility or Elongation is measured by the distance to which a sample will elongate before breaking when two ends of a specimen briquette are pulled apart at a specifi ed speed and at a specifi ed temperature.It may be used for quality specifi cations.

The Elastic Recovery is measured by the recoverable strain determined after severing an elongated briquette specimen. The specimens are pulled to a specifi ed distance at a specifi ed speed and at a specifi ed temperature.This is useful in confi rming that a material has been added to the asphalt to provide a signifi cant elastomeric characteristic.

Our ductilometers are also available as an automatic version with force measure-ment - DDA 3.


15

10-0335 & 10-0333

10-0336 & 10-0333

10-0334 & 10-0333

10-0332 & 10-0333

Thermometer & Holder

10-0403 & Ductilometer

10-0380

10-038010-0381

Circulator (for external & internal cooling & heating)Necessary as tempering & fi lling device for the DD/DDA-bath jacket and for reaching a bath-temperature of approx. -10 to +60°C (at +20°C ambient temperature).Note: Insulated hose matter is not included but recommended.

For details see: General Equipment, page 68Dimensions / Weight : 37 x 46 x 71 cm (W x D x H), 49 kgPower supply : 230 V, 50 Hz, EU-plugPower supply : 230 V, 60 Hz


21-0697 Digital Stop WatchFor details see: General Equipment, page 67

Options & Accessories

10-033210-033410-033510-0336

Mold (4-piece), brass, for the preparation of bitumen briquettes... according to EN 13 398 - IP 516... according to former DIN 52 013 - NF T 66-006 - IP 32... according to ASTM D 113 - AASHTO T 51... according to ASTM D 5892 - ASTM D 6084 - AASHTO T 300 & 301 - EN 13 589 - EN 13 703 (former ASTM P 226) - IP 515 - IP 520

10-0333 Mold Holder (fi ts 10-0332, 10-0334, 10-0335 and 10-0336)

10-0379 Calibration Set - DDA/DDConsisting of: 1 set of precision resistor plugs , 3 weights with steel-rope, 1 pulley, 1 certifi ed thermometer DIN 12 775 (0 to +50 :0.1°C), 1 thermometer holder,1 digital stop watch, 1 tape-measure with mm-division

10-0403 Rack 80 x 25 x 42 cm (L x W x H) to place controller and printer behind the ductilometer

18-040318-0402

Circulator-Bath (for external & internal heating)Used for pre-tempering of samples (e.g. DD/DDA-molds).Note: It requires counter-cooling by a circulation cooler or thermostatic circulator for

applications near ambient temperatures. Hose matter is not included.For details see: General Equipment, page 68

Dimensions / Weight : 37.5 x 45 x 47.5 cm (WxDxH), 3.4 kgPower supply: 230 V, 50 Hz, EU-plugPower supply: 115 V, 60 Hz


Thermometers (for DDA/DD-calibration set & DD-bath)

Precision Made


TypeRange

ASTM DIN10-0383 10-0384 - 12 775 0 to +50 : 0.1 °C10-0385 10-0386 63C - +8 to +32 : 0.1 °C

Spare Parts10-0377 Contrast Inlay

(6 x 170 x 550 mm) pack of 110-0406 Corrosion Protection Specimen

(200 x 100 mm) pack of 2


16

18-1017 PNR Log

18-1000 + Test Kit

Plastic Properties - Penetrometer Method - PNR 10Bituminous MaterialsNeedle-Penetration: ASTM D 5 - EN 1426 (DIN 52 010 - IP 49)Rod-Penetration (Bitumen Number): EN 13179-2 - van der Baan

Hot-Applied Sealants & FillersCone-Penetration : ASTM D 5329 EN 13880-2Ball-Penetration : EN 13880-3

The PNR 10, belongs to the group of conventional gravity-penetrometers used for the determination of consistency of highly viscous and plastically workable stuff.A test body is precisely lowered to the surface of the material under test, and then sinks into the matter by its own weight during a defi ned test duration. This penetration, which is indicated in Penetration Units of 0.1 mm per unit or directly in millimeters, and allows a rating of the plasticity or consistency.

Main Units

18-100018-1014

PNR 10 - Digital Penetrometer, Bitumen Method

Depending on accessories suitable for:Needle-Penetration : ASTM D 5 - EN 1426 (DIN 52 010 - IP 49)Rod-Penetration : EN 13 179-2 - van der BaanCone-Penetration : ASTM D 5329 - EN 13 880-2Ball-Penetration : EN 13 880-3

Features: • electronic depth gauge• audible & visible signals when test value falls out off preset values• solenoid release mechanism• with illuminator and observation lens

Consisting of:digitally indicating instrument on microprocessor base, large face milled penetrometer platform with leveling screws and control panel in the form of a splash water protected membrane key-board, which also contains the LED indicating penetration depth in millimeters. Penetrometer head with hand wheels for coarse and fi ne adjustment, solenoid release mecha-nism and electronic depth gauge. Further with low voltage illuminator and observation lens on fl exible arms.Note: Test accessories like needles, cones etc. are required.

Technical Data: Working range : 0 ... 48 mmMax. test load : 2 kg Resolution : 1/100 mm in the range 0 to 10 mm

1/10 mm in the range 10.1 to 48 mm (automatically changing)Test duration : 0.1 sec. ... 9999 sec. (standard time preset to 5 sec.)Start delay : adjustable up to to max. of 9999 sec.(2.78 hours)Pause mode : for delayed plunger releaseExcess value device : with audible alarm for penetration values overstepping the adjusted

tolerancesZero-point detector : for electrically conductive sampleConnections for : line recorder, serial printer, PC Dimensions : 30 x 36 x 41 cm (W x D x H), weight: 10 kgPower supply : 220/230 V, 50/60 HzPower supply : 110/115 V, 50/60 Hz

Scope of ApplicationUsed to determine the plasticity of a wide range of materials, as well as for the evaluation of such theological characteristics as rheopexy and thixotropy.

Suitable for bituminous materials and hot-applied pavement sealants & fi llers.

Needle-Penetration:To measure the consistency of semi-solid and solid bituminous mixtures.Rod-Penetration:To measure the apparent viscosity (Bitumen N°) of fi ller aggregates used in bituminous mixtures.Cone-Penetration:To determinate the consistency of hot-applied, fuel-resistant joint sealants with or without being immersed in fuel or oil.Ball-Penetration:To determinate penetration and the elastic recovery (resilience) of hot-applied sealants & fi llers.

Summary of MethodPenetration is the resistance which a material under specifi ed conditions of test provides against being pierced by a specifi cally shaped penetrator.Beside the confi guration of the penetrator used, prime importance attaches to such factors of temperature, time and load of test as are specifi ed by the different standard methods of test.A sample is fi lled in a specifi ed container and conditioned in a temperature bath. Then a standardized penetrator is vertically dropped on the specimen to measure the penetration depth. Higher values of penetration indicate softer consistency.

Penetration & TexturePenetration & Texture

17

18-2200

18-2215

18-2213

18-2370

18-2220

18-2221

Testbodies18-2220 Test Kit “Needle - ASTM” (ASTM D 5 - AASHTO T49 - JIS K2207)

3 standard needles, 2.5 g, brass/steel, precision made (18-1160)1 plunger, 47.5 g (18-0042)1 load weight, 50 g (18-0051)5 sample jars I, Ø 55 x 35 mm (18-0066)1 tempering bath (18-0065)Note! 100 g load weight (18-0052) has to be ordered separately.

18-2221 Test Kit “Needle - EN” (EN 1426 - IP 49) 3 standard needles, 2.5 g, brass/steel, precision made (18-1160)1 plunger, 47.5 g (18-0042)1 load weight, 50 g (18-0051)5 sample jars I, Ø 55 x 35 mm (18-0066)1 sample jar III, Ø 70 x 45 mm (18-0068)1 sample jar V, Ø 55 x 60 mm (18-0069)1 reduction ring, Ø 36 / 53 x 20 mm (18-0076)1 reduction ring, Ø 36 / 53 x 30 mm (18-0077)1 tempering bath with serpentine heat exchanger tube (18-0070)1 spacer plate for tempering bath (18-0091)1 thermometer holder (18-0094)1 thermometer ASTM 63C, -8/+32/0.1 °C (90-0106)1 thermometer ASTM 64C, +25/+55/0.1 °C (90-0107)

18-2370 Test Kit “Rod - Bitumen Number (van der Baan)” (EN 13 179-2)1 rod, Ø 8 mm, 15 g, aluminum (18-0251)1 sample jar, Ø 30 mm x 30 mm (18-0252)

18-2213 Test Kit “Ball - Filler” (ASTM D 5329-12 - EN 13 880-3 - BS 2499-3)1 ball rod, Ø 17 mm, 27.5 g, stainless steel (18-2355)1 plunger, 37.5 g (18-0038)2 sample jars III, Ø 70 x 45 mm (18-0068)2 beakers, 600 ml (10-0056)

18-2215 Test Kit “Standard Hollow Cone - Filler” (ASTM D 5329-6/7 - EN 13 880-2)1 optional hollow cone, 102.5 g, brass/steel (18-0101)1 plunger, 47.5 g (18-0042)1 sample jar I, Ø 55 x 35 mm (18-0066)1 tempering bath, Ø 160 x 80 mm (18-0065)1 spacer plate for tempering bath (18-0091)

18-116018-116118-116318-1164

Standard Needle, 2.5 g... Precision Made (ASTM D 5 - AASHTO T 49 - EN 1426 - IP 49 - ISO / DIS 3997)... Works Certifi cate Petrotest® (ASTM D 5 - AASHTO T 49 - EN 1426 - IP 49 - ISO / DIS 3997)... Offi cially Certifi ed, with UKAS certifi cate (EN 1426 - IP 49)... Offi cially Certifi ed, with UKAS certifi cate (ASTM D 5 - AASHTO T 49 - EN 1426 - IP 49)

Options & Accessories18-2200 Calibration Set - PNR

to check the correctness of the penetration depth, consisting of: 4 gauge blocks (5 mm, 9 mm, 15 mm, 25 mm), special screw-driver and instructions.

18-1007 Digital Stop WatchDetails: General Equipment, page 67

18-0708 Halogen Lampextra bright, to be placed beside the penetrometer; especially useful when testing bituminous materials under water surface. Power supply: 230 V, 50 Hz

18-040318-0402

Circulator-Bath (for external & internal heating)Used for sample tempering (e.g. with tempering bath 18-0065, 18-0070).Details: General Equipment, page 68Power supply: 230 V, 50 Hz, EU-plugPower supply: 115 V, 60 Hz

18-1017 PNRLog Software (WIN 95 / 98 / NT compatible) complete with serial data transfer cable, to record the measured data such as test time, date and user’s name automatically and allow the data transfer to other application like EXCEL®, LIMS etc.

25-028225-0283

Serial Impact Printer to record data like test results, duration of test, etc. without a PC.Details: General Equipment, page 67Power supply: 220/240 V, 50/60 HzPower supply: 110/130 V, 50/60 Hz

25-038825-0389

Circulator-Bath (for ex- & internal heating & cooling)Used for sample tempering (e.g. with tempering bath 18-0065, 18-0070).Details: General Equipment, page 69Power supply: 230 V, 50 Hz, EU-plugPower supply: 115 V, 60 Hz

Thermometers (for sample tempering)

Precision Made


TypeRange

ASTM IP21-0601 21-0607 17C - +19 to +27 : 0.1 °C21-0621 21-0627 17F - +66 to +80 : 0.2 °C11-0087 11-0088 38C 78C +24 to +78 : 0.2 °C


18

18-1700 + Testbody

supplied with 18-1700

18-1721PNR Pro

Plastic & Elastic Properties - Texture Method - PNR 21

Main Units

18-170018-1701

PNR 21 - Rheotex Texture Analyzer

Features: User-generateable test programs including• automatic contact of the sample surface• alternating load tests or oscillating programs• program loops with constant load• pauses and no motion stages

Consisting of:testing machine for texture and consistency examinations, with splash water protected membrane control panel with LCD showing actual test parameters and measured values directly, control and programming software PNRCon (used to record measured values, their graphic display, as well as to save test results and test programs), RS232-interfaces for printer and PC connectionSupplied with: 1 clamping support (2 groove stones with bolds)

1 test cylinder (Ø 10 mm)1 PNRCon software (for Windows).

Note: Ordinary Pentium PC with printer and extended software PNRProor parallel printer are recommended.Further the Penetration Accessories of PNR 10 like needles, cones etc. can be used also.

Technical Data: Load & tensile force : 100 NewtonsResolution : up to 9 Newtons: 0.01 N / more than 9 Newtons: 0.1 NDisplacement : 100 mm (start position of measuring carriage is variable)Resolution : 0.01 mmTravelling speed : 0.1 - 8 mm/s ±0.1 %Pause mode : for delayed plunger releaseConnections for : parallel printer, PC Dimensions : 32 x 37.5 x 50 cm (W x D x H), weight: 11 kgPower supply : 230 V, 50/60 Hz, 0.4 A Power supply : 115 V, 50/60 Hz, 1.0 A

The PNR 21 is a compact but highly fl exible texture analyzer, that demonstrates the forces, which occur when the properly chosen test body is pushed into the tested material or withdrawn.Especially due to its easy and convenient handling the apparatus allows a quick and economical examination of the plastic & elastic properties of pasty materials. PNR 21 Rheotex uses different test bodies. It depends on the measurement problem, whether a needle, a cone, a cylindrical or platelike ram is applied. These test bodies are mounted to a support-arm with force sensor which is attached to a vertically movable carriage.The load or tensile forces, which affect the force sensor, when the carriage moves up or down are indicated on a computer screen as a force/displacement diagram or as a displacement/time function.

The instrument permits to monitor curing and congealing reactions of adhesives, mortars etc. or to observe the behaviour of sealing matter and cements.

The creation of test programs is very easy. Either made directly on the instrument or by using PNRCon software and a PC with Windows.The use of a computer does not only enable a much easier and more extensive creation of test procedures, but also allows their storage and reloading.

Scope of ApplicationUsed to measure load forces as well as tensile stresses, which occur when a test body is pushed into the tested material or withdrawn.

Suitable for bituminous materials, hot-applied pavement sealants & fi llers and cement.

Summary of MethodA texture analyzer measures the forces, which occur when a test body is pushed with a pre-programmed speed into the tested material or pulled out.

The forces affecting the test body are measured and indicated in the form of a “displacement/force curve“ or as a“force/time function“This allows to determine information about the aging, the maturity or the curing, as well as the estimated subsequent processing of a sample.


19

18-0279

18-1721 PNR Pro

18-0255

18-1728

18-0251

The PNR 10 penetrometer measures the penetration depth in millimeters. The texture analyzer PNR 21-Rheotex measures load and tensile forces.

PNR 10 gives one solitary displacement value at the end of a test. PNR 21 provides a series of values, which can be shown as a force/displacement curve or as a diagram “force versus time“.

You will fi nd further information about the PNR-instruments and their available accessories in our Texture Testing-catalog.


Testbodies18-0279 Test Needle “VICAT”,

fl attened, Ø 1 mm, effective length 35 mm

18-0255 Test Ball, Ø 6.3 mm with shaft 100 mm long

18-0045 Plunger (penetrometer clamping rod) 10 g, length 107 mm, aluminum, for test needle 18-0279, test ball 18-0255 and other penetrators

18-025118-1726

Test CylinderØ 8 mm, 40 mm effective length, with plane end face, aluminumØ 10 mm, 100 mm overall length, with plane end face

18-024718-0248

Platelike Test Ram “Adhesion”10 cm² (Ø 35.7 mm)20 cm² (Ø 50.5 mm)

Options & Accessories18-1728 Test Kit “Adhesive Strength”

with sample & ram temperature control and 3 easy-to-change sample containers. By use of a circulation thermostat (not included), the ram (Ø=3 mm or Ø=10 mm), the sample and the container can be heated up to the requested temperature, without that the test equipment gets into contact with the tempering fl uid.

18-1721 PNRPro Softwareoffering additional possibilities like simultaneous display of stored master curves and comparison of actual test curve, statistical analysis, storage of test series in a data base for comfortable comparison and their statistical evaluation, programmable zero setting for a defi ned program step (labelling), menu in English.

Circulator-Baths with intermediate bottom are used for - sample pre-tempering (e.g. Tempering Bath 18-0065) and / or - connection to small external units (e.g. Tempering Bath 18-0070 or Adhesive Strength Device 18-1728)

25-038825-0389

Circulator-Bath (for internal & external sample heating & cooling)Note: Insulated hose-set (25-0228) is recommended.

For details see: General Equipment, page 69Dimensions / Weight : 36 x 75 x 40 cm (W x D x H), 31 kgPower supply : 230 V, 50/60 Hz, 2500 W, EU-plugPower supply : 115 V, 60 Hz, 1700 W

18-040318-0402

Circulator-Bath ( for external & internal sample heating)Note: It requires counter-cooling by a circulation cooler or thermostatic circulator

for applications near ambient temperatures. Hose matter is not included.For details see: General Equipment, page 68



25-0228 Hose-Set, insulated (Ø 8 mm, 2 x 2 m, incl. fi ttings)

Spare Partsdepending on the used Test Kit

20

BPACon Permanent Bending

BPACon Glass Transition Temperature

BPA 5 (10-0457)

BPA 5 Bending Mechanism

Breaking-Point - FRAASS Method - BPA 5 (automatic)

Bitumen and bituminous binders: IP 80 - EN 12593 (DIN 52 012, NF T 66-026) - JIS K 2265

Easy to OperateDue to its principle of construction ”measuring the bending force of a steel plaque coated with the material to be examined“ and the use of thermoelectric elements for the cooling of the test chamber, the Automatic Breaking-Point Tester BPA 5 offers a series of outstanding advantages.The handling of the BPA 5 is very easy. The operator only needs to place the specimen on the plaque support and the BPA 5 automatically clamps and adjusts the test plaque.The large LC-display, visible up to 10 m distance, provides the operator with additional instructions during a test. When a test is completed, the fi nal result remains on the display until a new measurement is started.

VersatilityThe scope not only covers the examination of bitumen according to the conventional FRAASS Method but also allows the user to adapt the test procedure to particular conditions (e.g. research of glass transition temperatures) or to perform a permanent bending program.

With the Standardized-FRAASS-Test-Method the instrument detects a distinct variation of the bending force or a typical deformation of the force/temperature curve respectively. Just as if the BPA 5 user could look inside the material under test.

These striking force characteristics can even be recognized with diffi cult materials (such as certain kinds of bitumen), where ruptures of the bitumen coating cannot be observed visually.

In particular with Polymer-modifi ed Bitumen (PmB), the Permanent-Bending-Program is an interesting alternative to the conventional FRAASS method. The sample is cooled to a specifi ed temperature and then the number of bending strokes is counted which are necessary to cause a rupture.

This program, however, requires a PC with BPACon-software to remote-control the BPA 5, for storage and evaluation of the measured data. Thus, test proceedings (e.g. variation of the bending force) can be easily watched via a graphic diagram on the PC screen.

For samples with a very low breaking-point a Rapid-Test-Program is included. It cools with an accelerated rate of 2 K/min in the beginning and then changes to the standardized cooling rate during the actual test period.

In order to avoid unnecessary tests, with samples where the breaking-point is not known at all, the SEARCH-Mode, which is preset in the USER program, can be used benefi cially. The instrument works with a refrigeration rate of 2 K/min and makes a bending test every 2 Kelvin.

The BPA 5 also offers the possibility to change test parameters like bending speed, cooling rate or bending intervals and to store them as a USER-Defi ned-Program.

Scope of ApplicationTo determine the temperature at which a bitumen tends to break rather than to fl ow when stressed.Suitable for any homogeneous road or industrial bitumen.

Summary of MethodA thin fl at steel plaque, coated with the sample, is fl exed under specifi ed conditions at a descending series of temperatures.The FRAASS-Breaking-Point is the temperature at which the fi rst cracks appear in the coating.

Breaking-PointBreaking-Point

21

10-0460

Printer Test Chart

BPACon Standardized

Test

Data OutputAlthough not required, the connection of a serial printer is recommended.The user will receive a test result for each fl exion or any other interval (time or temperature according to the parameters set by the operator).

BPACon-SoftwareMost comfortable is the use of the BPA 5 together with a PC with BPACon-software. This software package (for Windows®) includes the Permanent-Bending-program. Further it permits to remote control the BPA 5 by PC, to create additional user-defi ned test programs and to store or reload them from a PC. The measured data can be easily saved and evaluated on a PC in numerical form and as well as a graphical diagram.BPACon is, for instance, mandatory to run Permanent-Bending-Tests or when Glass-Transition-Temperatures are determined, where the trend of the bending force versus the temperature drops and the recovery trend serves as the criteria for the material under test.

EconomicalThe BPA 5 is a very economical instrument. It uses Peltier-elements for the refrigeration of the test chamber. These solid-state cooling elements require a light auxiliary refrigerant only and thus avoid investing in a bulky and high energy consuming cooler.

Cooling Source Coolant Temperature

Achievable Breaking Point(at ambient temperature of +20 °C)

Tap Water +17 °C approx. -24 °CCirculation Cooler -10 °C approx. -36 °CCirculator -20 °C approx. -46 °C

Note: These coolers are designed to be opperated at ambient temperatures of approximately +5 to +40 °C. All mentioned values are basically detected at an ambient temperature of approx. +20 °C.

Main Units

10-046010-0461

BPA 5 Set - Fraass Method- Automatic Breaking-Point Tester with Circulation CoolerIP 80 - EN 12 593 - JIS K2207Consisting of:- Measuring and Control Unit:

high-grade stainless steel housing with two-color powder coating, measuring head with bending mechanism, automatic fi xture and adjustment of test plaques; test chamber cooled by solid-state components (Peltier-elements), chamber ventilator, touch-key panel with large LC-display visible up to 10 m distance for measured values and user guidance for temperature pre-selction and test-plaque clamping.

- Programs: Standardized-FRAASS-Test RAPID-Test for very low breaking-points USER-Defi nable-Program SEARCH-Mode for samples with unknown breaking-point. In combination with a PC and BPACon-software: Permanent-Bending-Program. Further the graphic display and evaluation of the bending forces.

- Circulation Cooler: as auxiliary refrigeration of the Peltier-elements.Supplied with: 10 test-plaques (41 x 20 x 0.15 mm), 1 insulated hose-set (Ø 8 mm, 2 x 2 m)Note: serial printer or PC-software BPACon are recommended.Technical Data: Resolution : 10 mNWorking range : approx. -36 to +60 °C (due to external cooling)Cooling : Peltier-elements (internal) & circulation cooler (external)Connections for : serial printer, PC (RS232), cooler (Ø 8 mm) Dimensions BPA : 23 x 40 x 29/43 cm (W x D x H), weight: 15 kgDimensions Cooler : 23 x 36 x 38 cm (W x D x H), weight: 23 kgPower supply : 230 V, 50/60 Hz, 450 W, 2 A, EU-plugPower supply : 115 V, 60 Hz, 450 W, 4 A, US-plug

Technical DataOperating Range:approx. -36 to +60°C

Programs:• Standard-Program

(cooling rate of 1 K/min)for FRAASS-Breaking-Point

• RAPID-Program (cooling rate of 2 K/min)for very low breaking-points

• SEARCH-Mode to fi nd the approximated breaking-point

• USER-Defi nable-Program for program modifi cations

In connection with the PC-software BPACon:• Permanent-Bending-

Program for fatigue tests• Glass-Transition-Temperature • Graphic display and

evaluation of bending forces• LIMS ability

Interface:serial RS232 for printerserial RS232 for PC (USB-converter available)

Refrigeration: Peltier-elements counter-cooled by the circulation cooler

For special applications the BPA 5 can be delivered with an extended working range or a 1 mN-resolution.


22

10-0473

10-0474

25-0282

Plaques

11-0599

10-0233

12-1763


10-0473 PC Software - BPACon (Windows®)The program includes the Permanent-Bending-Test-Software and is used to store / modify and display curves of force for - Breakpoint-Tests - Permanent-Bending-Tests - Glass-Transition-Temperature-Test. It replaces the serial printer and makes it possible to start/stop the BPA 5 by PC, as well as to load self-defi ned test-programs.The progression in elasticity, plasticity, glass-transition-temperatures and of cause cracking will be displayed numerical or graphically in different scales. With special created curves of trends for bending or recovery force even very small, nearly not visible, breaks of the material can be found in an unknown high precision.Supplied with: 1 PC-data-cable, 1 USB/RS232-converter

10-0474 Calibration Set - BPA 5Consisting of:1 set of precision resistor plugs, 2 weights, 1 thermometer IP 42C (calibrated)

10-0475 Laboratory Stand for calibration set

10-0233 Tongs to handle stest-plaques

12-1763 Storage Box for spare parts and tools

10-0007 Melting Apparatus for bitumen samples having a ring & ball softening point <100 °C.Consisting of:heater plate (steplessly regulated) with thermometer socket and cooling plate with hose connections; magnetic test-plaque holder (40 x 60 x 8 mm) with coverSupplied with: 1 thermometer (0 to +200 : 1 °C)Note: a circulation cooler is recommended.Technical Data:Dimensions : 23 x 35 x 13 cm (W x D x H), weight: 5 kgPower supply : 230 V, 50 Hz, 150 W, EU-plug

25-028225-0283


Spare Parts10-0006 Test-Plaques, 10 pieces

(41 x 20 x 0.15 mm), steel

10-0016 Test-Plaques, 10 pieces (41 x 20 x 0.15 mm),steel, with works certifi cate

25-0228 Hose-Set, insulated (Ø 8 mm, 2 x 2 m)

25-0262 PC-Data-Cable (0-modem), serial, RS232 (9 & 25-pin)

11-0599 USB/RS232-Converter with 2 m cable (verifi ed for Petrotest®-units)connecting 1 serial port to the USB-port of a PC or Hub

25-0274 Printer-Data-Cable, serial (2 m)standard 25-pin


23

10-0007

10-0090

10-0000

10-0233

Breaking-Point - FRAASS Method (manual)

Bitumen and bituminous binders: IP 80 - EN 12 593 (DIN 52 012, NF T 66-026) - JIS K 2265

Main Unit10-0000 Manual Breaking-Point Tester, Fraass-Method

Consisting of:cooling apparatus (test tube, stopper and Dewar-fl ask with metal stand); bending apparatus with small stopper.Supplied with: 10 test-plaques (41 x 20 x 0.15 mm), 1 thermometer IP 42CNote: protection vessel for Dewar-fl ask and tongs on separate order.Technical Data: Dimensions : Ø 12 x 48 cm, weight: 3 kg


10-0090 Protection Vessel (Acryl) (inside Ø 125 x 245 mm) for Dewar-fl ask

10-0233 Tongs to handle test-plaques

10-0007 Melting Apparatus for bitumen samples having a ring & ball softening point <100 °C.Consisting of:heater plate (steplessly regulated) with thermometer socket and cooling plate with hose connections; magnetic test-plaque holder (40 x 60 x 8 mm) with coverSupplied with: 1 thermometer (0 to +200 : 1 °C)Note: circulation cooler is recommended.Technical Data:Dimensions : 23 x 35 x 13 cm (W x D x H), weight: 5 kgPower supply : 230 V, 50 Hz, 150 W, EU-plug

Spare Parts10-0002 Bending Apparatus

Consisting of:two concentric tubes fi tted with plaque-holding clips, curved spacer, crank-operated cone-and-peg mechanism, setting screw and rubber stopper

10-0003 Cone-and-Peg Mechanism, hardened and polished

10-0004 Setting Screw with a hardened tip

10-0006 Test-Plaques, 10 pieces (41 x 20 x 0.15 mm), steel

10-0008 Test-Tube

10-0009 Dewar-Flask (borosilicate glass), 1 litre, Ø 75 x 205 mm, without stand.

10-0010 Stopper (NBR-rubber), Ø 83/71 x 60 mm, bored twice (Ø 15 & 38 mm), to support the test-tube in the Dewar-fl ask and allow fi lling at the same time

10-0017 Thermometer IP 42C (-38 to +30 : 0.5 °C)

20-0106 Metal Stand for Dewar-fl ask


24

StiffnessStiffness

Scope of ApplicationTo determine the fl exural creep stiffness of asphalt binders at low temperatures like ambient to -36°C

Summary of MethodDuring testing, a contant load (0 to 450 g) is applied to a asphalt beam for a selected duration. The defl ection of the beam is measured and monitored continuously by PC. Further the test parameters are set by the PC, which displays & prints a plot of load vs. defl ection and calculates the stiffness at the lowest temperature anticipated.For tests acc. ASTM D 6648 an auxiliary cooler is required to cool down the molds, so that the sample is stiff enough to be demolded without distortion.

Creep Stiffness - Bending Beam Rheometer Method - BBR (automatic)

Superpave®: SHRP B-002 - SHRP 1002 AASHTO TP1 ASTM P 245 Flexual Creep Stiffness of Asphalt binders: ASTM D 6648 - EN 14771 (NF T66-062)

Main Unit

10-070010-0701

BBR - Automatic Bending Beam Rheometer

SHRP B-002 - SHRP 1002 - AASHTO TP1 - ASTM P 245 - Superpave® ASTM D 6648 - EN 14771Consisting of:- Tempering Bath: with heating module and compressor cooling- Test Frame: motor displaceable between charging and measuring position- Control Electronics: consisting of servo amplifi er with load control and

amplifi er for the measured force signal- Software: for the measuring process,

as well as for the display, evaluation and storage of the measured data on a PCNote: molds, cooling bath (for ASTM D 6648), PC and printer are recommended.Technical Data: Tempering bath: Working range : approx. -47 to +150 °C Temp. constancy : ±0.01 KTest frame: Beam support distance : 102 ±0.5 mm Load range : 0 to 1500 mN (accuracy class 0.1) Max. bending : 10 mm with 1µm resolutionPower supply : 230 V, 50 Hz, EU-plugPower supply : 115 V, 60 Hz, US-plug

10-0706 Beam Molds (AASHTO), pack of 5


10-0090 Force Calibration Kit

10-0233 Temperature Calibration KitConsisting of:1 precision digital thermometer1 probe with cable and DKD-calibration certifi cate for two different temperature points

25-039325-0394

Circulator (external & internal heating & cooling) regulated by Main-Unit(for ASTM D 6648 sample preparation)Note: Insulated hose-set (25-0228) is recommended.

For details see: General Equipment, page 69Dimensions / Weight : 23 x 46 x 58 cm (W x D x H), 30 kgPower supply : 230 V, 50/60 Hz, 2400 W, EU-plugPower supply : 115 V, 60 Hz, 1600 W, EU-plug

The U.S. Government funded Strategic Highway Research Program (SHRP) brought new rheology tools and procedures to the market to improve performance and commerce with Superpave® Performance Graded Binders.

25

ViscosityViscosity

Viscoelastic Properties - Dynamic Shear Rheometer Method - DSR II (automatic)

Superpave®: SHRP B-003 - SHRP 1007 - AASHTO TP5 ASTM P 246

Paving grade: EN 12591 (NF T65-001)

Main Units

10-0770 DSR II - Automatic Dynamic Shear RheometerSHRP B-003 - SHRP 1007 - AASHTO TP5 - ASTM P 246 - Superpave® - EN 12591A rheometer system confi gured for dynamic testing of asphalt and bitumen according the temperatures and frequencies specifi ed by SHRP and Superpave®.It offers precise and stable temperature control, a rapid sample equilibrium to settemperature, an automatic expansion compensation keeps the pre-set gap constant with temperature.Consisting of:1 rheometer with mechanical bearing and fl uid cell 1 cooling circulator with hose1 Windows-software SHRP for Superpave® specifi cation and grade determination 1 measuring plate (PU) Ø 8 mm (for average temperature tests)1 measuring plate (PU) Ø 25 mm (for high temperature tests)

Note: PC and Printer sets are required.Technical Data: Torque : 0.05 to 10 mNmTemperature Range : 5 °C to +80 °C (DSR)Heating / Cooling Rate : 2 °C / 1.5 °C (circulator)Power supply : 230 V, 50/60 Hz


10-0771 Computer Set - DSRConsisting of:minitower with CD-ROM drive and Windows©-software, monitor, keyboard, mouseNote: Confi guration details upon requestPower supply: 230 V, 50/60 Hz

10-0772 Printer Package - DSR (Color-Inkjet with printer-cable)Power supply: 230 V, 50/60 Hz

A range of research-grade software is available to enable the following tests:• Oscillation as a function of time, temperature, frequency and shear stress• Viscosity as a function of shear rate, shear stress, temperature and time• Creep and Creep Recovery (for compliance measurement and analysis) including accumulated strain testing.• Time Temperature Superposition and Viscoelastic Analysis

Scope of ApplicationUsed to measure the linear viscoelastic properties of modifi ed or unmodifi ed (aged or unaged) asphalt binders in a temperature range of +5 to +80 °C.

Summary of MethodFor AASHTO MP1 tests a sample disc is confi ned between circular parallel plates and tested at a specifi c temperature.Dynamic shear is determined by applying a known torque to oscillate one of the plates and measuring the resulting strain.The phase angle, in radiants or degrees between the sinusoidal stress & strain, is measured, too. Resultant stress is measured in a strain control mode, while resultant strain in a stress control mode.

The measurement of the rheo-logical properties, or viscoelastic behavior, of binder, like range and degree of stiffness, elasticity, and relaxation times measured over the working temperatures, helps to improve the performance life of asphalt road systems.

Rheometers measure the rheo-logical data concerning the fl ow and the deformation behavior of substances by:

- Rotational tests for liquids:Flow curves (shear stress and shear rate), viscosity function, yield point, thixotropy (structuraldecomposition and regeneration), temperature behavior.

- Oscillatory tests for low viscous liquids to solids:

Viscoelastic behavioras an amplitude sweep as a function of the deformation or load (or shear stress); as a frequency sweep as a function of time (speed or frequency)

Time-dependent behavior (thixotropy, structural decomposition and regeneration)

Temperature-dependent behavior(glass-transition-temperature, melting-temperature, crystallization-temperature)

Jellifi cation and hardening behavior

- Creep and relaxation tests to investigate the viscoelastic behavior and material structure (e.g. molar mass distribution) of polymers

26

RV with spindle

ViscosityViscosity

Apparent Viscosity - Rotational Viscometer Method - RV (automatic)

Superpave®: SHRP 1006 - AASHTO TP48 - ASTM D 4402

EN 13302

Main Units

10-060010-1600

RV - Digital Rotational Viscometer with Brookfi eld Thermosel

SHRP 1006 - AASHTO TP48 - Superpave® - ASTM D4402 - EN 13 302Consisting of:measuring head (without spindle), temperature probe (Pt-100), digital display, RS232, parallel and anaolg output, stadia materialSupplied with: 1 carry caseNote: Spindle, viscosity standard, tempering unit (& controller for 115 V) are required.

The application PC-software is recommended.Technical Data: Working range : depending on spindle from 50 up to 3.3 million mPa·s Display of : torque, viscosity, shear rate, shear stress and temperatureSerial RS232 interface : for data transfer to PCParallel output : for printer Analog output : for torque (0-1 V) and temperature (0-4 V)Power supply : 230 V, 50 Hz, EU-plugPower supply : 115 V, 60 Hz, US-plug

10-0602 Spindle (Viscosity range: 50 to 170 000 mPa·s)Note: Since the viscosity range depends on the speed, the max. viscosity can only be

reached at the lowest speed!

10-0604 Spindle Extension, including link and coupling nut(only for test without Tempering Unit - RV)


10-060110-1601

Tempering Unit - RV(temperature controller with thermo-container)Temperature range: ambient to +300 °CPower supply: 230 V, 50 HzPower supply: 115 V, 60 Hz

10-1602 Tempering Controller - RV (for 115 V -Tempering Unit)

10-0603 PC-Software - RVprovides automatic data collection and instant fl ow curves (rheograms), for Windows®, data transfer cable included.

10-0605 Viscosity Standard 1000 cPs, 500 ml (for calibration at 10, 20, 30 rpm)

Scope of ApplicationUsed to determine the apparent viscosity at elevated temperatures.(e.g. +38 to +260°C).

Suitable for asphalt.

Summary of MethodThe torque on a spindle rotating in a special thermostatically controlled sample holder containing a small sample of asphalt is used to measure the relative resistance to rotation.A factor is applied to the torque dial reading to yield the viscosity of the asphalt in millipascal seconds.

27

10-0312 with accessories

25-0001 / 25-0108

ViscosityViscosity

Apparent Viscosity - Road Tar Viscometer Method (manual)Cutback & Flux-Bitumen: EN 13357 (DIN 52 023) IP 502 (IP 72)

Bitumen emulsions: EN 12846

Main Units

10-031210-0313

Road Tar ViscometerEN 13 357 - IP 502 - EN 12 846Consisting of:electrically-heated single-place viscometer heating bath with stirrer and ball valve supportSupplied with:2 test cups (with 4 mm or 10 mm orifi ce, 1 each),2 ball-tipped valve rods, 1 graduated (100 ml) receiver,1 set of 6 different stoppers.Note: Thermometers & Electronic Energy Regulator are required.

The ball valve is 143.1 mm in length, which is not acc. EN 13 357.Power supply : 230 V, 50/60 HzPower supply : 115 V, 50/60 Hz

25-000125-0108

Electronic Energy Regulator for heating coilsConsisting of:Potentiometer on/off switch, 10 A overload fuse; DIN-socket, 1.5 m cable with DIN-plug.Technical Data: Capacity : up to 2000 WWeight : 500 gDimension : 150 x 80 x 55 mm (L x W x H)Power supply : 230 V, 50/60 Hz, 2000 WPower supply : 115 V, 60 Hz


21-0697 Digital Stop WatchFor details see: General Equipment, page 67

Thermometer

Precision Made


TypeRange Dimensions (mm) /

Immersion (mm)DIN10-0317 10-0318 12 775 / E 0.1/0/50 0 to +50 : 0.1 °C10-0319 10-0320 12 775 / E 0.2/0/100 0 to +100 : 0.2 °C

Precision Made



Immersion (mm)ASTM IP11-0155 11-0156 8C 6C -2 to +400 : 1 °C 385 x Ø 7 / total21-0361 21-0362 - 8F +30 to +100 : 0.5 °F 340 x Ø 7 / 6521-0367 21-0368 - 8C 0 to +45 : 1 °C 340 x Ø 7 / 65

Spare Parts

10-029410-032110-0323

Test Cup, brass, with... 2 mm orifi ce... 4 mm orifi ce... 10 mm orifi ce

10-029510-032210-0324

Ball-Tipped Valve Rod for... 2 mm orifi ce... 4 mm orifi ce... 10 mm orifi ce

10-033710-0338

Electric HeaterMains: 230 V, 500 WMains: 115 V, 250 W

11-0130

Measuring Cylinder, 100 ml, graduated, with stand, glass, 1 ml subdivision, 254 mm high

10-0329 Stopper Set, NBR-rubberConsisting of:1x each for orifi ces

12 /15 mm (10-0325 pack of 10)6.5/15 mm (22-0082 pack of 10)5 /20 mm (22-0081 pack of 10)

1x for sample thermometer DIN44/30/bored Ø 8.6 mm (10-0326 slotted)

1x for sample thermometer ASTM / IP44/30/bored Ø 6 mm (10-0327 slotted)

1x for bath thermometer DIN14.5/20/bored Ø 8.6 mm (10-0328)

1x for bath thermometer ASTM / IP14.5/20/bored Ø 6 mm (16-0739)

Scope of ApplicationTo measure the viscosity by determining the effl ux time of a warm sample, through a 10 or 4 mm orifi ce.

Suitable for road tars, cutback asphalts and high-viscous bitumen emulsions with effl ux times in the range of 15 to 500 sec.

Summary of MethodThe viscometer cup is fi lled with the warm sample, then placed in the bath to settle at a specifi c temperature, before the ball valve is pulled.

28

21-0695

ViscosityViscosity

Saybolt Viscosity - Universal & Furol Method (semi-automatic)

Bituminous and Residual materials:ASTM D 88 - AASHTO T72 - FTM 791-304 (FTM 141A-4285)JIS K2207Bitumen and Residual materials at high temperatures: ASTM E 102

Universal and Furol viscometers are technically identical designs, except for orifi ce tips which differ in diameter.

Being built-in as interchangeable units in the viscometer, the orifi ce tips, Universal or Furol, can be universally used for all types of Saybolt viscosity measurements.

Main Units

21-050121-0502

Two-Tube Saybolt-Viscometer ASTM D 88 - AASHTO T72 - FTM 791-304 - JIS K2207ASTM E 102Consisting of:stainless steel housing with thermostatically controlled test bath, and electric stirrerSupplied with: 2 receiving fl asks, 60 ml2 pipettes with rubber suction bulb2 thermometer protection tube2 thermometer holders2 cork stoppers2 rubber suction bulbs3 lids for bath opening with Ø 51 mm1 orifi ce spanner1 tube cleaning plungerNote: Thermometers are not includedTechnical Data: Working range : +20 to +230 °C (+68 to +450 °F) Temperature Accuracy : ± 0.03 °C (± 0,05 °F)Power supply : 230 V, 50 Hz, EU-plugPower supply : 115 V, 60 Hz, US-plug.


21-0695 8-Channel Stop WatchFor details see: General Equipment, page 67

21-0697 Digital Stop Watch, For details see: General Equipment, page 67

21-0703 Filter Funnel No. 100, ASTM E 11

21-0713 Viscosity Tube Cap, ASTM E 102

21-0714 Displacement Ring, ASTM E 102

Scope of ApplicationUsed to determine the Saybolt Universal Viscosityof lubricants and distillates with effl ux times > 32 s orthe Saybolt Furol Viscosity of residual materials with effl ux times > 25 s. Further of petroleum products such as fuel oils and other residual materials having Saybolt Universal viscosities > 1000 s.

Summary of MethodThe effl ux time in seconds of a sample, fl owing through a calibrated orifi ce, is measured under carefully controlled conditions. The time is corrected by an orifi ce factor and reported as the viscosity of the sample at that temperature.

ASTM D 88 temperature range:+21 to +99 °C (70 to 210 °F)ASTM E 102 temperature range:+120 to +240 °C (248 to 464 °F)

29

21-0699

21-0693

ViscosityViscosity

Thermometer

Precision Made



Immersion (mm)ASTM IP

acc. ASTM D 8821-6000 — Set of 1 each: ASTM 17C, 18C, 19C, 20C, 21C, 22C

21-0601 21-0607 17C — +19 to +27 : 0.1 °C 275 x Ø 6.5 / total21-0602 21-0608 18C 23C +34 to +42 : 0.1 °C 275 x Ø 6.5 / total21-0603 21-0609 19C — +49 to +57 : 0.1 °C 275 x Ø 6.5 / total21-0604 21-0610 20C — +57 to +65 : 0.1 °C 275 x Ø 6.5 / total21-0605 21-0611 21C — +79 to +87 : 0.1 °C 275 x Ø 6.5 / total21-0606 21-0612 22C 24C +95 to +103 : 0.1 °C 275 x Ø 7 / total

21-0621 21-0627 17F — +66 to +80 : 0.2 °F 275 x Ø 6.5 / total21-0622 21-0628 18F 23F +94 to +108 : 0.2 °F 275 x Ø 6.5 / total21-0623 21-0629 19F — +120 to +134 : 0.2 °F 275 x Ø 6.5 / total21-0624 21-0630 20F — +134 to +148 : 0.2 °F 275 x Ø 6.5 / total21-0625 21-0631 21F — +174 to +188 : 0.2 °F 275 x Ø 6.5 / total21-0626 21-0632 22F 24F +204 to +218 : 0.2 °F 275 x Ø 7 / total

acc. ASTM E 102 21-0641 21-0646 77F — +245 to +265 : 0.5 °F 275 x Ø 6.5 / total21-0642 21-0647 78F — +295 to +315 : 0.5 °F 275 x Ø 6.5 / total21-0643 21-0648 79F — +345 to +365 : 0.5 °F 275 x Ø 6.5 / total21-0644 21-0649 80F — +395 to +415 : 0.5 °F 275 x Ø 6.5 / total21-0645 21-0650 81F — +445 to +465 : 0.5 °F 275 x Ø 6.5 / total

Reference MaterialThe factory certifi ed viscosity-oil-standards have been tested to perform according to the following list.Content: 470 ml/one pint acc. ASTM D 2162

Factory certifi ed Type

Saybolt Universal Seconds

SUS 100 °F (37.8 °C)Saybolt Universal Seconds

SUS 210 °F (98.9 °C)Saybolt Furol Seconds

SFS 122 °F (50 °C)

24-0606 S 20 96 mm²/s 24-0607 N 35 160 mm²/s24-0616 S 60 280 mm²/s24-0608 N 100 600 mm²/s24-0609 S 200 950 mm²/s 90 mm²/s24-0610 N 350 130 mm²/s24-0611 S 600 180 mm²/s 140 mm²/s24-0613 N 2000 420 mm²/s

For details see: General Equipment, page 66

Spare Parts

21-0375 Saybolt Viscosity Tubebrass, gold plated, interchangeable Universal- and Furol-orifi ces (1 ea.) including calibration certifi cate

21-0693 Receiving Flask, 60 ml capacity

21-0699 Oil Pipette with rubber suction bulb21-0700 Oil Withdrawal Tube

21-0701 Cleaning Plunger21-0704 Stopper, NBR-rubber (18/20) with loop

25-060725-0608

Heating Element HD 2000 W, 230 VHeating Element HD 1000 W, 115 V

30

21-0030

21-0695

Specifi c Viscosity - Engler Method (semi-automatic)

Tar & Tar destillates: ASTM D 1665 - JIS K2208Bituminous emulsions: IP 212 (DIN 51 560)

Main Units

21-0030 Engler Viscometer

ASTM D 1665 - IP 212 - JIS K2208Consisting of:Basic instrument with gold plated test vessel, tempering bath with digital controller, heater 300 W with over-temperature protection, cooling coil for counter cooling, mains cord.Supplied with: 1 miniature spirit level1 Kohlrausch fl ask 200 ml1 measuring fl ask, 50 ml (ASTM)1 thermometer (ASTM 54C/18C)3 thermometers (ASTM 23C - 25C)1 silicone stopper1 m tubingTechnical Data: Working temperature : max. +100 °CStorage temperature : -10 to +70 °CRelative Humidity : to 90%Dimensions :32 x 26 x 55 cm (W x D x H), weight: 8 kgPower supply : 230 V, 50 Hz, EU-plug


21-0695 8-Channel Stop WatchContaining 8 individual stop watches.Each operated by a single button to run, stop or reset.Auto-power-off when no stop watches are running.After power-off individual values are kept in memory.All values can be reset together or per channel.9 V-battery-block included. Expected life time approx. 6 months.The stop watch can be supplied with a calibration certifi cate.Dimensions (L x W x H): 195 x 112 x 46 mm

21-069721-0698

Digital Stop Watch, for details see: General Equipment, page 67... precision made... certifi ed

21-0158 Measuring Flask, 50:1 ml, Tol. +/-0.5 ml

Thermometer

Precision Made



Immersion (mm) / collarASTM IP21-0113 21-0114 23C – -18 to + 28 : 0.2 °C 212 x Ø 6 / 90 / Ø 821-0115 21-0116 24C – -39 to + 54 : 0.2 °C 237 x Ø 6 / 90 / Ø 821-0117 21-0118 25C – -95 to +105 : 0.2 °C 212 x Ø 6 / 90 / Ø 890-0103 90-1103 54C 18C -20 to +100.6 : 0.2 °C 310 x Ø 7 / total

Spare Parts10-0377 Kohlrausch Flask, 200 ml

(ASTM and IP)

Measuring Flask, 50 ml (ASTM)

50-0001 Spirit Level - Miniaturevertical and horizontal, Dimension: 100 x 40 x 15 mm

11-0395 Stopper, Silicone (14.5/20 / bored Ø 6 mm)

Scope of ApplicationUsed for characterising the consistency by measuring the fl ow properties to determinate the specifi c viscosity.

Suitable for tar and their fl uid products.

Summary of MethodThe time, in s, is measured for a fi xed volume of liquid material to fl ow through an effl ux tube under an accurately reproducible head and at a closely controlled temperature.The Engler specifi c viscosity is then calculated by dividing the effl ux time by the viscometer calibration factor as determined by making the same effl ux measurement for water.It does not determine absolute viscosity, but is an empirical fl ow test.

ViscosityViscosity

31

CFOV - type

22-0097

ViscosityViscosity

Kinematic Viscosity - Glass Capillary Methods (manual)

Liquid petroleum products (transparent & opaque):ASTM D 445 - IP 71-1 (DIN 51 550 - NF T60-100 - FTM 791-305)ISO 3104 - JIS K2283 (DIN 51 366 (CFOV) - DIN 51 372 (BS/IP-RFV))

Glass Capillary specifi cations: ASTM D 446 - IP 71-2 ISO 3105 - JIS K2207

Liquid asphalts (bitumens), road oils (under gravity):ASTM D 2170 - IP 319 - EN 12595 - DIN 52 007-1(FTM 791-305)

Kinematic Viscosity -Cannon-Fenske Opaque Viscometer Method - CFOV (manual)

CFOV - Cannon-Fenske Opaque Viscometer (CR-type) (length: 295 mm, required sample: ~ 12 ml)

Factory Certifi ed

Offi cially Certifi ed Size Constant

[cSt/s or mm2/s2]Viscosity Rangeν [cSt or mm2/s]

22-0070 – Set (1 each) of25 - 600 0.002 - 20.0 0.4 - 20 000

22-0050 22-2050 25 0.002 0.4 - 222-0051 22-2051 50 0.004 0.8 - 422-0052 22-2052 75 0.008 1.6 - 822-0053 22-2053 100 0.015 3 - 1522-0054 22-2054 150 0.035 7 - 3522-0055 22-2055 200 0.1 20 - 10022-0056 22-2056 300 0.25 50 - 25022-0057 22-2057 350 0.5 100 - 50022-0058 22-2058 400 1.2 240 - 1 20022-0059 22-2059 450 2.5 500 - 2 50022-0060 22-2060 500 8.0 1 600 - 8 00022-0061 22-2061 600 20.0 4 000 - 20 000

Note: Holders, tempering bath, fi lling & cleaning equipment are required!

CFOV Accessories

22-0097 Holder "CFRV-CFOV" with suspension bracket (for factory certifi ed viscometers)

22-2065 Holder "CFOV" with suspension (for offi cially certifi ed viscometers)

22-0164 Stopper, NBR-rubber (18/20, bored Ø 6 mm)

22-0528 Stopper, solid rubber, Ø 2-6 mm, 20 mm high, pack of 10 (to close the viscometer tube)

22-0093 Conical Silicone Tubing (for suction of liquids)

23-0204 Suction Syringe, made of glass

Scope of ApplicationUsed to characterizes the fl ow behavior at +60°C (140°F) and +135°C (275°F).

Suitable for liquid asphalts (bitumens), their distillation residues and road oils at +60°C (140°F) or of asphalt cements at +135°C (275°F) with a viscosity from 6 to 100 000 cSt.

Kinematic Viscosity: ν [mm²/s = cSt]

Dynamic Viscosity: η [mPa·s = cP]

Dynamic Viscosity: η [dPa·s = P = poise]

Summary of MethodThe time is measured for a fi xed volume of the liquid to fl ow under gravity through the capillary tube, under an accurately reproducible head and at a closely controlled temperature.The kinematic viscosity is then calculated by multiplying the effl ux time in seconds by the viscometer calibration factor.The dynamic viscosity can be obtaint by multiplying the measured kinematic viscosity by the density of the liquid.

32

ZCAV - type

RFV - type

22-0278

22-0278

ViscosityViscosity

Kinematic Viscosity - Zeitfuchs Cross-Arm Viscometer Method - ZCAV (manual)

ZCAV - Zeitfuchs Cross-Arm Viscometers(length: 295 mm, required sample: ~ 3 ml)

Factory Certifi ed



– 22-0530 1 0.003 0.6 - 3– 22-0531 2 0.01 2 - 10– 22-0532 3 0.03 6 - 30– 22-0533 4 0.1 20 - 100– 22-0534 5 0.3 60 - 300– 22-0535 6 1 200 - 1 000– 22-0536 7 3 600 - 3 000– 22-0537 8 10 2 000 - 10 000– 22-0538 9 30 6 000 - 30 000– 22-0539 10 100 20 000 - 100 000


ZCAV Accessories22-0540 Holder "UNIVERSAL" with suspension bracket (for ZCAV viscometer)22-0528 Stopper, solid rubber, Ø 2-6 mm, 20 mm high, pack of 10

(to close the viscometer tube)

Kinematic Viscosity - BS/IP Reverse Flow Viscometer Method - RFV (manual)

RFV - U-Tube Reverse Flow Viscometer (length: 275 mm, required sample: ~ 12 - 25 ml)

Factory Certifi ed



22-0220 – Set (1 each) of1 - 11 0.003 - 300 0.6 - 300 000

22-0200 22-2200 1 0.003 0.6 - 322-0201 22-2201 2 0.01 2 - 1022-0202 22-2202 3 0.03 6 - 3022-0203 22-2203 4 0.1 20 - 10022-0204 22-2204 5 0.3 60 - 30022-0205 22-2205 6 1 200 - 1 00022-0206 22-2206 7 3 600 - 3 00022-0207 22-2207 8 10 2 000 - 10 00022-0208 22-2208 9 30 6 000 - 30 00022-0209 22-2209 10 100 20 000 - 100 00022-0210 22-2210 11 300 60 000 - 300 000


RF - U-tube Accessories22-0278 Holder "RFV" with suspension bracket (for BS/IP viscometer)22-0270 Pipette, 50 ml with stopper (to withdraw air by suction)22-0528 Stopper, solid rubber, Ø 2-6 mm, 20 mm high, pack of 10

(to close the viscometer tube)

33

22-0529 22-0528

22-0515 & 22-0516

AIVV - type

CMVV - type

ViscosityViscosity

Dynamic Viscosity - Vacuum Capillary Method (manual)ASTM D 2171 - IP 222 - EN 12596

Summary of MethodThe time is measured for a fi xed volume of the liquid to be drawn-up by vacuum through a capillary tube, under closely controlled conditions of vacuum and temperature. The viscosity in poises is calculated by multiplying the fl ow time in seconds by the viscometer calibration factor.

1 dPa·s = 1 P = poise1 Pa•s = 10 P = 10 poises

Dynamic Viscosity - Cannon-Manning Vacuum Viscometer Method - CMVV (manual)

CMVV - Cannon-Manning Vacuum Viscometer (length: 180 mm, required sample: ~ 6 ml)

Factory Certifi ed

Offi cially Certifi ed Size Viscosity Range

[Poise or dPa·s]

22-0500 – 4 0.036 - 0.822-0501 – 5 0.12 - 2.422-0502 – 6 0.36 - 822-0503 – 7 1.2 - 2422-0504 – 8 3.6 - 8022-0505 – 9 12 - 24022-0506 – 10 36 - 80022-0507 – 11 120 - 2 40022-0508 – 12 360 - 8 00022-0509 – 13 1 200 - 24 00022-0510 – 14 3 600 - 80 000


Dynamic Viscosity - Asphalt Institute Vacuum Viscometer Method - AIVV (manual)

AIVV - Asphalt Institute Vacuum Viscometer(length: 180 mm, required sample: ~ 3 ml)

Factory Certifi ed

Offi cially Certifi ed Size Viscosity Range

[Poise or dPa·s]

22-0520 – 25 42 - 80022-0521 – 50 180 - 3 20022-0522 – 100 600 - 12 80022-0523 – 200 2 400 - 52 00022-0524 – 400R 9 600 - 1 400 00022-0525 – 800R 38 000 - 5 800 000


CMVV & AIVV Accessories

22-0529 Holder "VV" without suspension bracket(for CM- & AI-Vacuum-Viscometer) neoprene rubber, fi ts Ø 51 mm bath openings

22-0528 Stopper, solid rubber, Ø 2-6 mm, 20 mm high, pack of 10(to close the viscometer tube)

22-0515 Vacuum Manifold

22-0516 Digital Vacuum Regulator with pump, 240 V, 175 W horizontal orientation, non-mercury system, CE-approved

Scope of ApplicationUsed to characterizes the fl ow behavior at +60°C (140°F).

Suitable for: cutbacks and asphalt cements at 60°C (140°F) with a viscosity from 0.036 to over 200 000 P.

34

Reference Material

21-0695

22-0450

20-0030

ViscosityViscosity

Capillar Viscometer - Options & Accessories 22-0528 Stopper, solid rubber, Ø 2-6 mm, 20 mm high, pack of 10 (to close the viscometer tube)

21-0695 8-Channel Stop WatchFor details see: General Equipment, page 67


20-003020-0040

Luminous BackgroundLarge fi eld lamp for convenient glare-free observation of the viscometers immersed in the thermostatic bath.Power supply: 220/250 V, 50/60 Hz, 22 WPower supply: 115 V, 50/60 Hz

Filling & Cleaning Devices

22-0270 Pipette, 50 ml with stopper (for fi lling of RFV-type)

23-0204 Suction Syringe, made of glass (for fi lling of CFOV-type)

22-0093 Conical Silicone Tubing (for suction of liquids)

10-0013 Water Jet Pump acc. to Hanff, made of glass

25-048525-0486

Vacuum-Pump with Mini-Compressor & AccessoriesConsisting of:1 oil-free diaphragm pump with fi lter1 hose (Ø 6 mm x 1 m, silicon, clear)1 T-piece connection (Ø 7.5 mm)1 Hoffmann-ClipTechnical Data:Max. capacity : 6 l/minEnd vacuum : 100 mbarOperating pressure : 2.4 bar (overpressure)Dimensions / Weight : 9 x 17 x 12 cm (W x D x H), 1.9 kgPower supply : 220/230 V, 50 Hz, EU-plugPower supply : 115 V, 60 Hz

20-009520-0096

Viscometer Tube Cleaner and Dryerwashes (with solvents) and dries (with pressurized air) up to six glass capillary tubes at a time.Note: Requires pressurized air source (150 psi maximum)Dimensions (L x W x H): 41 x 18 x 32 cm (7 kg) & solvent tank (15 kg)... with solvent container... without solvent container

22-0450 ViscoHanger - Universal Glass Capillary Viscometer StandAllows to hang-up all viscometer-types fi tted into holders with suspension (not ViscoClock - holders) to let the bath fl uid from into the detached leakage tray (stainless steel, chemical resistant).Dimensions (L x W x H): 51 x 28 x 49 cmAvailable holders with suspension:Cannon Fenske (22-0097), BS/IP Viscometer (22-0278), Ubbelohde (22-0155), Zeitfuchs Cross-Arm (22-0540)

Reference MaterialThe values listed in the following table are to be considered as nominal and approximate only (depending on the batch). The actual and exact data will be printed on the container-lable or on a separate certifi cate.Content: 470 ml / 1 pint Shelf life: 2 years

UKAS Type

Kinematic Viscosity ν [mm²/s = cSt] Dynamic Viscosity η [mPa·s = cP]

certifi ed approx. 20°C68°F

25°C77°F

37.8°C100°F

40°C104°F

50°C122°F

60°C140°F

80°C176°F

99°C210°F

100°C212°F

24-0616 S 60 mm²/smPa·s

160140

120100

6051

5446

3529

−−

1311

7.96.4

7.76.3

24-0609 S 200 mm²/smPa·s

650570

460400

210180

180160

11092

−−

3226

1815

1814

24-0611 S 600 mm²/smPa·s

22001900

15001300

600520

520450

290250

−−

7361

3831

3630

24-0613 S 2 000 mm²/smPa·s

81007100

53004700

20001700

17001500

900780

−−

189160

9075

8672

24-0615 S 8 000 mm²/smPa·s

3500031000

2300020000

79007000

67005900

33002900

−−

591507

−−

240200

24-0618 S 30 000 mm²/smPa·s

−−

8100073000

2800024000

2300021000

110009700

−−

17441510

−−

660560

35

20-0150

20-0154

ViscosityViscosity

Tempering Bath

20-015020-0151

High Temperature Liquid BathConsisting of:digital temperature read-out, 7 test places (Ø 50 mm) and front window (270 x 285 mm)Note: Bath thermometers ASTM 47 / IP 35 or ASTM 110 are surgested.Technical Data: Working range : +5 °C above ambient (or cooling water) up to +150 °CConstant : 0.02 KIncreasement : 0.1 °C Stability : ±0.01° C and better (with water at +55 °C)Bath opening : 26 x 24 x 30 cm (W x D x H)Volume : 40 lDimensions / Weight : 59 x 35 x 56 cm (W x D x H), 41 kgPower supply : 230 V, 50/60 Hz, 1500 W, EU-plugPower supply : 115 V, 50/60 Hz, 1500 W

20-015420-0155

Circulator (external & internal heating & cooling)Used for counter-cooling the Liquid BathSupplied with: 1 bath coverNote: Insulated hose-set (25-0228) is recommended.

For details see: General Equipment, page 68 Dimensions / Weight : 22 x 36 x 47 cm (W x D x H), 18 kgPower supply : 230 V, 50 Hz, 1050 W, EU-plugPower supply : 115 V, 60 Hz

22-0164 Stopper, NBR-rubber (18/20, bored Ø 6 mm)

50-916150-9162

Bath Fluid Silicon Oil basedTemperature Range : approx. +10 to +200 °CColor : Water Clear 5 liters10 liters

Thermometers (acc. ASTM E 1)

Precision Made



Immersion (mm)ASTM IP90-0285 90-1285 74C 69C -55.6 to -53.9 : 0.05 °C 305 x Ø 7 / total90-0173 90-0252 73C 68C -41.4 to -38.6 : 0.05 °C 305 x Ø 7 / total90-0212 90-1212 126C 71C -27.4 to -24.6 : 0.05 °C 305 x Ø 7 / total90-0214 90-1214 127C 99C -21.4 to -18.6 : 0.05 °C 305 x Ø 7 / total90-0284 90-1284 72C 67C -19.4 to -16.6 : 0.05 °C 305 x Ø 7 / total90-0125 90-1215 128C 33C -1.4 to +1.4 : 0.05 °C 305 x Ø 7 / total90-0100 90-0250 44C 29C -80.0 to +20.0 : 1 °C 305 x Ø 7 / total90-0101 90-1101 45C 30C +23.6 to +26.4 : 0.05 °C 305 x Ø 7 / total90-0204 90-1204 118C − +28.6 to +31.4 : 0.05 °C 305 x Ø 7 / total90-0241 90-1241 28C 31C +36.6 to +39.4 : 0.05 °C 305 x Ø 7 / total90-0136 90-0253 120C 92C +38.6 to +41.4 : 0.05 °C 305 x Ø 7 / total90-0102 90-0251 46C 66C +48.6 to +51.4 : 0.05 °C 305 x Ø 7 / total90-0281 90-1281 29C 34C +52.6 to +55.4 : 0.05 °C 305 x Ø 7 / total90-0149 90-1149 47C 35C +58.6 to +61.4 : 0.05 °C 305 x Ø 7 / total90-0311 90-1311 − 100C +78.6 to +81.4 : 0.05 °C 280 x Ø 6.5 / total90-0240 90-1240 48C 90C +80.6 to +83.4 : 0.05 °C 305 x Ø 7 / total90-0217 90-1217 129C 36C +91.6 to +94.4 : 0.05 °C 305 x Ø 7 / total90-0137 90-0254 121C 32C +98.6 to +101.4 : 0.05 °C 305 x Ø 7 / total90-0196 90-1196 110C 93C +133.6 to +136.4 : 0.05 °C 305 x Ø 7 / total90-0315 90-1315 132C 102C +148.6 to +151.4 : 0.05 °C 305 x Ø 7 / total

Thermometers (High-Precision acc. DIN 12 771)

Precision Made



Immersion (mm)DIN22-0157 22-0158 − +18 to +24 : 0.01 °C22-0159 22-0160 − +36 to +42 : 0.01 °C22-0161 22-0162 − +50 to +60 : 0.01 °C

22-0163 Protective Sleeve for bath-thermometers

36

10-1117 (with Timer)

10-0117

AgingAging

Effect of Heat and Air - Loss-On-Heat Method - LOH (semi-automatic)

Semi-solid Bitumen: ASTM D 6 (AASHTO T 47) - JIS K2207 EN 13 303 (IP 45, NF T66-011) - IP 506

To determine the loss in mass a sample is weighed before and after being heated at a certain temperature for a specifi ed time. Requires an shelf with 9 metal sample containers (Ø 55 mm x 35 mm).

Effect of Heat and Air - Thin-Film-Oven Method - TFOT (semi-automatic)

Semi-solid Bitumen: ASTM D 1754 - JIS K2207 EN 12607-2 (NF T66-047) - IP 460-2

The loss in mass (by analytical balance) and the changed properties (by Viscosity, Penetration, Ductility (ASTM) or Softening-Point (EN)) are examined. Requires a shelf with 4 stainless steel sample containers (Ø 140 mm x 9.5 mm).

Main Units

10-011710-0118

TFOT & LOH 4 - Semi-Automatic Thin-Film & Loss-On-Heat Oven

Depending on accessories suitable for:TFOT - Resistance to Hardening (Thin-Film-Oven-Test): ASTM D 1754 - JIS K2207 - EN 12 607-2 - IP 460-2LOH - Loss in Mass (Loss-On-Heat): ASTM D 6 (AASHTO T 47) - JIS K2207 - EN 13 303 - IP 506

Features: • for bitumen, fl ux oil & bituminous compounds• digital display of temperature with a 1°C resolution • overheat protection acc. to DIN 12 880 class 2• venting continuously variable• multi-purpose use due to removable gratings and motor switch-off

Consisting of:double-walled electrically heated convection type oven with illuminated stainless steel chamber, door with twin paned observation window (260 x 200 mm), safety thermostat with cut-off limit (thermal safety class 2), electronic PID-temperature controller with Pt-100 temperature probe and digital display of set point & actual values, continuously variable venting, switchable gear-motor assembly with axle (Ø 10 mm) to connect a horizontal rotating shelf.

Supplied with: 1 thermometer ASTM 13C, 1 thermometer support, 2 removable gratings

Note: Test equipment according to the standards is to be ordered separately!

Technical Data: Test places : acc. to the accessoriesTemperature max. : 300 °C (resolution: 1°C) (572 °F)Warming-up rate : 8 - 10 K/minAir change : 2 m³/h continuously variableRotating speed : 5- 6 rpmDimensions, interior : 403 x 370 x 380 mm (W x D x H), 57 literDimensions : 744 x 535 x 576 mm (W x D x H)Weight : approx. 50 kgPower supply : 220-250 V, 50/60 Hz, 6.5 A, EU-plugPower supply : 110-125 V, 50/60 Hz, 13 A

10-1117

TFOT & LOH 4/Ti - Semi-Automatic Thin-Film & Loss On Heat Oven with Timerlike TFOT & LOH 4 but additionally with: daily program timer (15 minutes intermittent) and high temperature-resolution (0.1°C)Power supply : 220-250 V, 50/60 Hz, 6.5 A, EU-plug

Scope of ApplicationTo determine the effects of heat & air during conventional hot-mixing on a thin fi lm of semi-solid bitumen.The determination of the loss in mass is used to determine the volatility upon heating.

Suitable for bitumen (asphalt), fl ux oil & bituminous binders.

Summary of MethodThe effects of heat and air are determined by physical tests measured before and after the oven treatment. Therefore a thin fi lm of a sample is heated in an constantly vented oven with a horizontal rotating shelf.

ASTM D 6 - EN 13 303 - IP 506:To determine the loss in mass a sample is weighed before and after being heated at a certain temperature for a specifi ed time. Requires a shelf with: 9 sample containers (metal, Ø 55 mm x 35 mm)

ASTM D 1754 - EN 12 607-2 - IP 460-2:Examine the loss in mass (by analytical balance) and the changed properties (by Viscosity, Penetration, Ductility or Softening-Point).Requires a shelf with: 4 sample containers (stainless steel, Ø 140 mm x 9.5 mm)

37

10-0123

10-0211

10-0212

10-0117 & 10-0211 (LOH)

10-0117 & 10-0212 (TFOT)

10-0117 & 10-0123 (TFOT & LOH)

AgingAging


10-0123 Test Kit - LOH & TFOT (Petrotest® modifi cation) ASTM D 6 - EN 13 303 - IP 506 and in analogy to ASTM D 1754 - EN 12 067-2 - IP 460-2Consisting of:1 rotating shelf, nickel-plated brass (Ø 266 mm x 3 mm), dual-purpose, 9 sample jars LOH, nickel-plated brass (Ø 55 mm x 35 mm), fl anged rim 3 sample dish TFOT, stainless steel (Ø 140 x 9.5 mm), fl at-bottom

10-0211 Test Kit - LOH ASTM D 6 - EN 13 303 - IP 506 Consisting of:1 rotating shelf, nickel-plated brass (Ø 266 mm x 3 mm), dual-purpose, 9 sample jars LOH, nickel-plated brass (Ø 55 mm x 35 mm), fl anged rim

10-0212 Test Kit - TFOT ASTM D 1754 - EN 12 067-2 - IP 460-2Consisting of:1 rotating shelf, cast aluminum (Ø 345 mm) 3 sample dish TFOT, stainless steel (Ø 140 x 9.5 mm), fl at-bottom

Thermometer

Precision Made



Immersion (mm)ASTM IP10-0126 10-0127 13C 47C +155 to +170 : 0.5 °C 155 x Ø 6.5 / total

Spare Parts18-0066 Sample Jar, nickel-plated brass

(Ø 55 mm x 35 mm), fl anged rim (for LOH - ASTM D 6, EN 13 303, IP 506)

10-0128 Sample Dish, aluminum, fl at-bottom(Ø 140 x 9.5 mm) (Ø 5½" x 3/8") (for TFOT - EN 12 607-2, IP 460-2)

10-0146 Sample Dish, stainless steel (Ø 140 x 9.5 mm) (Ø 5½" x 3/8") fl at-bottom (for TFOT - ASTM D 1754, EN 12 607-2, IP 460-2)

10-0150 Rotating Shelf - LOH & TFOT nickel-plated brass, dual-purpose, (Ø 266 mm x 3 mm), suitable for 9 LOH-sample jars (18-0066) or 3 TFOT-sample dishes (10-0128 / 10-0146)

10-0149 Rotating Shelf - TFOT cast aluminum (Ø 345 mm) suitable for4 TFOT-sample dishes (10-0128 / 10-0146)

10-0222 Thermometer Holder for shelf-axle

10-0242 Grating, chromium-plated steel (2 shelfs with supports)Dimensions (W x D): 387 x 365 mm

10-0243 Axle (Ø 10 mm) for rotating shelf

10-013410-0135

Gear-Motor for TFOT & LOH oven with connection-tube for shelf-axle, cable with plug and connectionsPower supply: 230 V, 50/60 HzPower supply: 115 V, 50/60 Hz

10-0244 Light bulb, 220 V, 15 W, E14

10-0245 Light bulb, 110 V, 15 W, E14

38

10-0618

10-0110

AgingAging

Effect of Heat and Air - Rolling Thin Film Oven Test Method - RTFOT (semi-automatic)

Bitumen : ASTM D 2872 - Superpave® (AASHTO T 240) - JIS K2207Bituminous binders: EN 12607-1 (NF T66-032) - IP 460-1

Main Units

10-061810-0640

RTFOT/ASTM - Semi-Automatic Rolling-Thin-Film Oven TesterASTM D 2872 - Superpave® - JIS K2207

Features: • for semi-solid bitumen (asphalts)• digital display of temperature & settings • squirrel cage protected fan• venting continuously variable• fl owmeter control

Consisting of:double-walled electrically heated convection type oven made of stainless steel, door with heat resistant twin paned glass window, safety thermostat, electronic controller with PT-100-probe and digital display, internal fan, symmetrical top and bottom vents, circular and vertical rotating 8-place aluminum rotating shelf, fl owmeter controlled air jet at the lowest point blows pre-heated air with a constant volume into each passing glass.

Supplied with: 8 sample jars & 1 thermometer ASTM 13C

Note: Pressure reducer is recommended

Technical Data: Test places : 2 - 8Working temperature : +163 °C (325 °F)Rotating speed : 15 rpmAir volume : 4000 ml/minInside dimensions : 483 x 445 x 381 mm (W x D x H)Weight : approx. 75 kgPower supply : 230 V, 50 Hz, EU-plugPower supply : 230 V, 60 Hz

10-0608

RTFOT/EN - Semi-Automatic Rolling-Thin-Film Oven TesterEN 12 607-1 - IP 460-1Same as RTFOT/ASTM but for bituminous bindersInside dimensions : 405 x 445 x 340 mm (W x D x H)Power supply : 230 V, 50 Hz, EU-plug

10-0621 Pressure Reducer with valve and manometer, 0.2 to 7 bar


25-048925-0490

Vacuum Pump with Mini-Compressor For details see: page 39 Power supply : 220/230 V, 50 Hz, EU-plugPower supply : 110/115 V, 60 Hz, US-plug

16-0700 Air Volume Meter to calibrate the fl owmeter of the RTFOT-ovenTechnical Data:Type : drum-gasmeter for small quantities Range : 5 - 360 l/h Volume min. : 0.02 l readable Accuracy : ±0,2 %Drum volume : 3 l

Thermometer

Precision Made




Spare Parts10-0625 Sample Jar, heat-resistant glass

(Ø 64 mm x 140 mm)50-5172 Hose-Clip, Hoffmann-type

Scope of ApplicationTo determine the effects of heat and air during conventional hot-mixing on a thin moving fi lm of semi-solid bitumen or bituminous binders.Indicating the resistance to hardening under infl uence of heat and air and the change in sample mass (Loss on Heat).

Suitable for bitumen (asphalt), fl ux oil & bituminous binders.

Summary of MethodThe effects of heat and air are determined by physical tests measured before and after the oven treatment. A moving fi lm of a sample is heated in an oven with a constant air fl ow and a vertical rotating shelf.

ASTM D 2872:The samples are cooled down in horizontal position in a metal rack. The change in sample mass (by analytical balance) and the changed properties of bitumen (by Ductility, Viscosity) are examined.

EN 12 607-1 - IP 460-1:The samples are cooled down in a desiccator.The change in sample mass (by analytical balance) and the changed properties of binders (by Penetration, Softening-Point, Viscosity).

39

10-0110

AgingAging

Effect of Heat and Air - Rotating Flask Method - RFT (semi-automatic)

Bituminous binders: EN 12607-3 (DIN 52 016, NF T66-048) - IP 460-3

Main Units

10-0110

RFT - Semi-Automatic Rotating Flask Testerin analogy to EN 12 607-3 (DIN 52 016, NF T66-048) - IP 460-3Features: • for bituminous binders• digital display of rotation speed, bath & steam temperature• adjustable dip-in depth• manual lift• timer

Consisting of:Rotary evaporator with double-walled stainless steel oil bath, manual lift, adjustable dip-in depth, electronic controlled rotation drive, LED of rotation speed, bath temperature, build-in timer

Supplied with: 1 bitumen-glass-set incl. 1000 ml round fl ask

Technical Data: Test places : 1Working temperature : +20 to +180 °C Rotating speed : 20 - 270 rpmAir volume : ml/minDimensions : 400 x 396 mm (W x D)Power supply : 230 V, 50/60 Hz, 1300 W, EU-plug


25-048925-0490

Vacuum Pump with Mini-Compressor Consisting of:1 oil-free diaphragm pump with fi lter, 1 hose (Ø 6 mm x 1 m, silicon, clear), 1 T-piece connection (Ø 7.5 mm)1 Hoffmann-ClipTechnical Data: Max. capacity : 11.5 l/minEnd vacuum : 240 mbarOperating pressure : 2 bar (overpressure)Dimensions / Weight : 9 x 20 x 13 cm (W x D x H), 2.2 kgPower supply : 220/230 V, 50 Hz, EU-plugPower supply : 110/115 V, 60 Hz, US-plug

16-0773 Flowmeter 4 - 40 l/h, calibrated, with accessoriesConsisting of:1 fl owmeter (150 mm glass-tube, mm-scale and V-shaped metal fl oat) mounted on a tripod-stand with leveling screws and leveling bulb,1 hose (Ø 6 mm x 1 m, silicon, clear), 1 T-piece connection (Ø 7.5 mm) 2 angled hose connectionsNote: The correlation between scale readings and fl ow volumes are listed in the calibration sheet.

Technical Data: Range : 4 - 40 l/h Factory calibration : at +20 °C and 1000 mbar ambient pressure Dimensions / Weight : 180 x 180 x 230 mm (W x D x H), 1 kg

Thermometer

Precision Made




Scope of ApplicationTo determine the effects of heat and air during conventional hot-mixing on a thin moving fi lm of bituminous binders.The loss in mass is used to determine the volatility upon heating.Suitable for bituminous binders.

Summary of MethodThe effects of heat and air are determined by physical tests measured before and after the rotation treatment. Therefore a moving thin fi lm of a sample is heated in an rotating fl ask of a rotary evaporator. The rotation shall prevent a surface hardening.

EN 12 607-3The samples are cooled down in a desiccator.The change in sample mass (by analytical balance) and the changed properties of binders (by Penetration, Softening-Point, Viscosity) are measured.

40

PAV

10-0146

AgingAging

Accelerated Aging - Pressure Aging Vessel Method - PAV (automatic)Accelerated long-term aging ASTM D 6521 - EN 14769 - SHRP 1001 - Superpave® AASHTO R28 - AASHTO MP1 - AASHTO PP1 - (ASTM PS 36)

(Short-term aging/conditioning: see RTFOT- TFOT - RFT Methods)

Summary of MethodSamples aged by this method have previously been prepared in the condition they would be applied to the road.At fi rst a binder is aged using the RTFOT-Method (to simulate plant aging), than it is placed in TFOT stainless steel pans before beeing aged acc. PAV.

A fi lm of binder is heated to a specifi ed temperature, under a specifi ed air pressure for a given period of time to simulate the changes occurring to the binder within the pavement during use.

Main Units

10-072010-0721

PAV - Automatic Pressure Aging VesselASTM D 6521- EN 14 769 - SHRP 1001 - Superpave® AASHTO R 28 - AASHTO MP 1 - AASHTO PP 1Features: • Ready-to-Go Set • Bench Top Unit • Integral Vessel & Oven Design • CE Conform & certifi ed

Consisting of:bench top unit, top opening, front panel with LCD, function-, cursor- & Enter/Return-keys,a vertical integrated stainless steel pressure vessel with encased band heaters,a pressure controller, temperature controller, pressure and temperature measurement devices, temperature recorder, built-in timer, programmable logic controller (PLC) to control and monitor the process including collecting the data (temperature and pressure) at regular intervals, 2 ports for direct controll by front panel and for remote controll & data access by PC or network).

Supplied with: 1 pressure vessel (3.15 MPa approved & CE-conform acc. EU-code 94/12/EG), 1 holder for 10 samples, 10 TFOT sample dishes, 1 specimen handling tool

Note: Compressed air (min. 23 bar) and an air pressure regulator are required.

Technical Data: Operating Pressure : 2.1 ±0.05 MPaThermo Control : Platinum RTD; microprocessor-basedTemperature Range : +80°C to +115°C Resolution : ±0.1°C Uniformity : ±0.5°CTime to Setpoint : ~ 3h (pre-heating), ~120 min. (after inserting specimen)Dimensions / Weight : 700 x 460 x 760 mm (W x D x H) / approx. 195 kgPower supply : 230 V, 50/60 Hz, 10 A, 1 Phase... with factory certifi ed vessel... with offi cially (TÜV) certifi ed vessel


10-0146 Sample Dish, stainless steel (Ø 140 x 9.5 mm) (Ø 5½" x 3/8") fl at-bottom (acc. TFOT - ASTM D 1754, EN 12 607-2, IP 460-2)

10-0724 Specimen Dish (acc. AASHTO T 179) pack of 10

10-0725 Stand (Table), steel (Dimension: 560 x 915 x 660 mm (H x W x D))

10-0726 Compressed Air Reducer with connection to European pressure vessels, incl. hose.

10-0727 Remote Control Option allows user to access graphical displays, to retrieve data and remotely control and monitor one PAV-unit.Including: Windows®-PC, CD-RW-drive, 31/2" fl oppy drive, color-monitor, mouse, modem

50-0001 Miniature Spirit Level vertical and horizontal (Dimension: 100 x 40 x 15 mm)

Available upon request:Air Pressure Regulator, single stage, 0-280 bar high pressure gage, 0-40 bar low pressure gage incl. relief valve

Precision Level with parallel bar (to level the pan fi xture after PAV installation)

Scope of ApplicationUsed to measure the accelerated aging (oxidation) by means of pressurized air and elevated temperature.It simulates the type of in-service oxidative aging that occurs in binders during pavement service. Residue from this conditioning practice may be used to estimate the physical or chemical properties of binders after several years of in-service aging in the fi eld.

Suitable for bitumen and bituminous (asphalt) or modifi ed binders.

41

Set-up with Skimmer

Flash- & Fire-PointFlash- & Fire-Point (open cup) (open cup)

Flash- & Fire-Point - Cleveland Open Cup Method - CLA 4 (automatic)

Cleveland Method:Binder & Petroleum Products:Superpave® AASHTO T48 - ASTM D 92

Petroleum Products (except fuel oil)ASTM D 92 - JIS K2265 AASHTO T48 - FTM 791-1103IP 36 (BS 4689)ISO 2592 (EN 22592, DIN 51 376, NF T60-118)

Main Units

12-094012-0941

CLA 4 - Automatic Flash- & Fire-Point Tester, Cleveland MethodPetroleum Products: ASTM D 92 - JIS K2265 - AASHTO T48 - FTM 791-1103 IP 36 (BS 4689) - ISO 2592 (EN 22 592, DIN 51 376, NF T60-118)Binder, Petroleum Products: Superpave®

Features: - automatic barometric pressure correction- 5 user defi nable test programs- rapid heating mode- display of values in degrees Celsius or Fahrenheit

Consisting of:stainless steel housing with two-color powder coating, touch-key panel with large LC-display (visible in up to 10 m distance), two RS232-interfaces for data printer and computer connection, different test-programs, data-transfer and fi rmware upgrading through bi-directional interface, automatic barometric pressure correction, electric heater, automatic overheat protection, gas igniter with auto-relighting and safety shut-off, re-cooling fan

Supplied with:1 cup “CL”1 temperature probe Pt-100 (glass)1 gas igniter with thermocouple1 electric igniter1 fl ame detection unit 1 fl ame arrest cover

Technical Data: Working temperature : +79 to +400 °C (+175 to +752 °F)Ignition : Gas fl ame (electrical ignited and automatically controlled)Sensing System : Ionization MethodAir Pressure : Automatic Barometric Pressure Correction of measured valuesSafety : Overheat protection, automatic ignition fl ame, fl ame arrest coverInterface : RS232 (for printer), RS232 (for downloads on PC)Dimensions, Weight : 230 x 470 x 460 mm (W x D x H), approx. 12 kgPower supply : 230 V, 50/60 Hz, 600 W, EU-plugPower supply : 110/115 V, 50/60 Hz, US-plug

Programs: (acc. to international standards)2 ASTM-programs 2 Search-programms1 Bitumen-program5 Customized-Programs, (user defi ned)

Scope of ApplicationUsed to defi ne the hazards of fl ammable and combustible materials used in shipping and safety regulations.

Suitable for viscous materials having a fl ash-point between +79°C (175°F) and +400°C (752°F).

Summary of MethodThe temperature of the approximately 70 ml test specimen is increased rapidly at fi rst and then at a slower constant rate as the fl ash-point is approached. At specifi ed intervals a test fl ame is passed across the cup until the sample infl ames.Used to measure the tendency of the test specimen to form a fl ammable mixture with air.

The fl ash-point is the lowest liquid temperature at which the application of an ignition source causes the specimen vapors to ignite.

To determine the fi re-point, the test is continued until the application of the ignition source causes the test specimen to ignite and sustain burning for a minimum of 5 s.

42

12-0958

12-1763

12-0962

12-0950


12-0956 Calibration Set “CLA”Consisting of:1 base plate, 1 support rod, 1 boss head, 1 clamp and 1 thermometer ASTM 11C / IP 28C (offi cially certifi ed)

50-9111 Reference Liquid “ASTM D 92” (approx. +250 °C), 250 ml

12-0958 Draft Defl ector “CL”


12-028212-0283


12-0954 Skimmer for skin removal

12-0962 Cup “CL-DRAIN” with handle and drainage, approx. 70 ml, made of brass

12-0970 Cup “CL-NIRO” with handle, approx. 70 ml (with fi lling mark), standard size, stainless steelNote! Flash-point results of stainless steel test inserts may deviate from standard results.

12-0949 Temperature Probe Pt-100 (Metal) for sample temperature

Spare Parts12-0950 Standard Cup “CL” with handle,

approx. 70 ml (with fi lling mark), brass

12-0951 Temperature Probe Pt-100 (Glass) for sample temperature measuring

12-0952 Gas Igniterwith thermocouple for fl ame monitoring

12-0778 Electric Igniterwith connector cable and plugs

12-0953 Flame Detection Unit for fl ash- & fi re-point detection

12-0960 Indicator-Ring

12-0955 Flame Arrest Cover for extinguishing the fi re in the cup


43

12-0710

12-1030

12-0629

12-0950


Main Units

12-073012-0731

CL 1 - Semi-Automatic Flash- & Fire-Point Tester, Cleveland MethodASTM D 92 - JIS K2265 - AASHTO T48 - FTM 791-1103 - Superpave®IP 36 (BS 4689)ISO 2592 (EN 22 592, DIN 51 376, NF T60-118)Consisting of: stainless steel housing, electric heater, electronic controlled motor-driven arm, gas ignition device with control valve and interchangeable gas jets, hose connection, thermometer holderSupplied with: 1 cup with handle1 thermometer ASTM 11C/IP 28CTechnical Data: Temperature range : approx. +79 to +400 °C (+175 to +752 °F)Ignition : gas Dimensions : 40 x 30 x 40 cm (W x D x H)Weight : 10 kgPower supply: 230 V, 50/60 HzPower supply: 115 V, 50/60 Hz

Options & Accessories12-1030 Flash-Point Assistant - FPA 2

microprocessor controlled, intelligent temperature measuring device with Pt-100 and integrated barometric pressure sensor to enable much more comfortable work.Features: standard and expected fl ash-point pre-selection; continious sample gradient display; acoustic igniter application signal; remote button or -key for fl ash-point value storage; automatic barometric pressure correction of fl ash-point value

12-0710 Draft Defl ector

12-0629 Pre-Regulating Valve for gas supply with hose adapter, suitable for all types of burning gases

50-9111 Reference Liquid “ASTM D 92” (approx. +250 °C), 250 ml

12-0970 Cup “CL-NIRO” with handle, approx. 70 ml (with fi lling mark), standard size, stainless steelNote! Flash-point results of stainless steel test inserts may deviate from standard results.

12-0962 Cup “CL-DRAIN” with handle and drainage, approx. 70 ml, made of brass

Thermometer

Precision Made


TypeRange

ASTM IP12-0751 12-0752 11C 28C -6 to + 400 : 2°C

12-0753 12-0754 11F 28F +20 to + 760 : 5°F

Spare Parts12-0950 Standard Cup “CL” with handle,

approx. 70 ml (with fi lling mark), brass12-0758 Ignition Device with control valve

12-0768 Heating Plate, 450 W, 220 V

Flash- & Fire-Point - Cleveland Open Cup Method - CL 1 (semi-automatic)

Cleveland Method:Binder & Petroleum Products:

Superpave® AASHTO T48 - ASTM D 92

Petroleum Products (except fuel oil)

ASTM D 92 - JIS K2265 AASHTO T48 - FTM 791-1103IP 36 (BS 4689)ISO 2592 (EN 22 592, DIN 51 376, NF T60-118)

Scope of ApplicationUsed to defi ne the hazards of fl ammable and combustible materials used in shipping and safety regulations.

Suitable for viscous materials having a fl ash-point between +79°C (175°F) and +400°C (752°F).

Summary of MethodThe temperature of the approximately 70 ml test specimen is increased rapidly at fi rst and then at a slower constant rate as the fl ash-point is approached. At specifi ed intervals a test fl ame is passed across the cup until the sample infl ames.Used to measure the tendency of the test specimen to form a fl ammable mixture with air.

The fl ash-point is the lowest liquid temperature at which the application of an ignition source causes the specimen vapors to ignite.

To determine the fi re-point, the test is continued until the application of the ignition source causes the test specimen to ignite and sustain burning for a minimum of 5 s.

44

(12-1770)

PMA 4 F (12-1767) with Fire-Extinguishing Device(Test-Insert included)

Flash-PointFlash-Point (closed cup) (closed cup)

Scope of ApplicationUsed in shipping & safety regulations to defi ne fl ammable and combustible materials.

Suitable for liquids with a viscosity above 5.5 cSt at +40°C.

Summary of MethodThe fl ash-point determination of petroleum products is using:Method A:for distillate fuels (diesel, kerosene, heating oil, turbine fuels), new lubricating oils, paints, vanishes and other homogeneous liquids.

Method B:for residual fuel oils, cutback residual, used lubricating oils, non-homogeneous materials like mixtures of petroleum liquids & solids, surface-fi lm building petroleum liquids or liquids with a viscosity above 5.5 cSt at +40°C.

A brass test cup is fi lled to the inside mark with test specimen, fi tted with a cover and heated, while the specimen is stirred at specifi ed rates. An ignition source is directed into the test cup at regular intervals with simultaneous interruption of the stirring, until a fl ash is detected.

Flash-Point - Pensky-Martens Method - PMA 4 (automatic)

Bitumen & bituminous binders (Method B):

ASTM D 93-B - IP 34-B - ISO 2719-B AASHTO T73-B - AASHTO T172-B FTM 791-1102 - FTM 141-4293

PMA - Single Place Units

12-177012-1771

PMA 4 - Automatic Flash-Point Tester, Pensky-Martens MethodPensky-Martens Method: ASTM D 93-A&B - JIS K2265 FTM 791-1102 - FTM 141-4293 AASHTO T73-A&B - AASHTO T172-A&B IP 34-A&B (BS 2839) ISO 2719-A&B (DIN 51 758, NF M07-019) EN 22719 Biodiesel Method: ASTM D 6751 Limit Test (eatable oils &fats): ISO 15267 - BS 684-1.17

Features: - swivel-around multi-function-head - ONE TWIST- automatic barometric pressure correction- electric & gas igniter (with auto-relighting and safety shut-off)- suitable for Standard-tests (70 ml) & Milli-tests (2 - 15 ml)- PC-software

Consisting of:high-grade stainless steel housing with two-color powder coating, touch-key panel with large LC-display (visible in up to 10 m distance), swivel-mounted multi-function-head - ONE-TWIST, two RS232-interfaces for data printer and computer connection, different test-programs, data-transfer and software upgrading through bi-directional interface, automatic barometric pressure correction, automatic overheat protection, power controlled/monitored electric igniter, gas igniter with auto-relighting and safety shut-off, re-cooling fan

PC-Software “PMACon” (Windows® compatible):for easy handling and storing of data as well as program transfer from the PC-Memory into the PMA 4. Easy to read tableau. Numerous programs can easily be set, copied from the memory and modifi ed. Permanent indication of test status. Due to the most comfortable properties of this software to display and modify actual and future test sequences, it is most recommendable for samples of permanently changing characteristics.

Supplied with:1 cup “PM”1 cover “PM”1 multi-detector “PM”1 gas igniter1 electric igniter1 tong for cup1 tray for cup and multi-detector1 stirrer coupling1 PC-software “PMACon”

Technical Data: Working temperature : +40 to +360 °C (+104 to +680 °F)Stirring Speed : 60 and 250 min-1 (adjustable)Ignition : gas and electric-type (both included)Sensing System : Differential-Thermocouple MethodAir Pressure : Automatic Barometric Pressure Correction of measured valuesSafety : Overheat protection, automatic ignition fl ame, fl ame arrest coverInterface : 1 RS232 (for printer) & 1 RS232 (for downloads on PC)Dimensions, Weight : 230 x 470 x 460 mm (W x D x H), approx. 12 kgPower supply: 115/230 V, 50/60 Hz, EU-plug Power supply: 115/230 V, 50/60 Hz, US-plug

12-176712-1768

PMA 4 F - Automatic Flash-Point Tester, Pensky-Martens Methodwith Fire-Extinguishing Device

Consisting of:like Standard Unit (12-1770), but with automatic fi re-suppression system for connection to an external Nitrogen- or Carbon Dioxide supply.Power supply: 115/230 V, 50/60 Hz, EU-plug Power supply: 115/230 V, 50/60 Hz, US-plug

Programs:4 ASTM-Programs4 ISO-Programs 2 Rapid-Heating-Programs2 Search-Programs 2 Customized-Programs, (user defi ned)

45

12-1509 with multi-detector

Chilled PMA 4 Sample Changer (12-2776) (Test Inserts not included)

PMA 4 Sample Changer (12-2770)(Test Inserts not included)

PMA - 12 Place Units (with 12-place carrousel)

Automatic Flash-Point Tester, Pensky-Martens Method with Sample Changer(for Standerds see Single-Place Unit)Features: - for up to 12 samples- suitable for Standard “PM” (72 ml) & Milli-test inserts “pPM” (< 15 ml)- PMA4 with “Sample Changer”- fi rmwareConsisting of:PMA 4 in a high-grade stainless steel housing with two-color powder coating, touch-key panel and 2-line LC-display, swivel-mounted multi-function-head - ONE-TWIST, two RS232-interfaces for data printer and computer connection, different test-programs, data-transfer and software upgrading through bi-directional interface, automatic barometric pressure correction, automatic overheat protection, power controlled/monitored electric igniter, gas igniter with auto-relighting and safety shut-off, re-cooling fan. (Optional with automatic fi re-suppression system).Sample Changer with 12-place carrousel, transfer arm with housing and positioning devices. (Optional with insulating cover and coolant circulator with insulated tubing.)PC-Software “PMACon” (Windows® compatible):for easy handling and storing of data, as well as program transfer from the PC-Memory into the PMA 4. Easy to read tableau. Numerous programs can easily be set, copied from the memory and modifi ed. Permanent indication of test status. Due to the most comfortable properties of this software to display and modify actual and future test sequences, it is most recommendable for samples of permanently changing characteristics.PC-Software “QuickRun” (Windows®):“QuickRun” is a module which runs in addition with the delivered “PMACon” software. Under full compliance with the standards this software is able to increase the performance of this instrument up to 50 % compared with conventional automated testers.Supplied with: 1 gas igniter, 1 electric igniter, 1 tong for cup, 1 stirrer coupling, 1 PC-software “PMACon” & “QuickRun”To be ordered separately: cups, covers & multi-detectors (e.g. 12-0777 & 12-0787)Temperature Range: +40 to +360 °C (+104 to +680 °F)

12-277012-2771

PMA 4 S - with Sample ChangerPower supply: 115/230 V, 50/60 Hz, EU-plugPower supply: 115/230 V, 50/60 Hz, US-plug

12-277212-2773

PMA 4 FS - with Fire-Extinguishing Device & Sample ChangerPower supply: 115/230 V, 50/60 Hz, EU-plugPower supply: 115/230 V, 50/60 Hz, US-plug

12-277612-2777

PMA 4 SC - with Chilled Sample ChangerPower supply: 115/230 V, 50/60 Hz, EU-plugPower supply: 115/230 V, 50/60 Hz, US-plug

12-277812-2779

PMA 4 FSC - with Fire-Extinguishing Device & Chilled Sample ChangerPower supply: 115/230 V, 50/60 Hz, EU-plugPower supply: 115/230 V, 50/60 Hz, US-plug

Options & Accessories12-0782 Calibration Set “PMA/PM”

Consisting of:1 calibration cover, 1 thermometer ASTM 9C/IP 15C, 1 thermometer ASTM 10C/IP 16C

12-1762 Calibration-Adapter for Pt-100 in multi-detector

12-0793 Handle for permanent fi xing at the cup

12-1508 Draft Guard (recommended for gas ignition tests)

12-1509 Stand to hold 12 multi-detectors

12-0600 Tray for cup and multi-detectorNote: An option for all PMA 4 units built before 05/2004, since than allready included.


25-0804Computer with 17“ monitor (detailed specifi cations upon request)Power supply: 230 V, 50 Hz

25-028225-0283



For more details see our catalogs:

Pensky-Martens Flash-Point TesterFlash-Point & Auto-Ignition Tester

46

12-0777

12-1790

12-1777

12-1763 & PMA accessories


Test InsertsStandard Brass Test Equipment:12-0777 Standard Test Insert “PM” (incl. in PMA4)

Consisting of: 1 cover and 1 cup (standard dimensions, made of brass)

12-0785 Standard Cup “PM”, approx. 75 ml (with fi lling mark), made of brass

12-0786 Standard Cover “PM” with shutter assembly, made of brass

12-0787 Standard Multi-Detector “PM” with fl ash-point detector (thermocouple) and temperature probe, made of glass

Stainless Steel Test Equipment:12-1790 Test Insert “NIRO”

Consisting of: 1 cover and 1 cup (standard dimensions, made of stainless steel)

12-1791 Cup “NIRO”, approx. 75 ml (with fi lling mark), made of stainless steel

12-1792 Cover “NIRO” with shutter assembly, made of stainless steel

12-0784 Multi-Detector “NIRO” with fl ash-point detector (thermocouple) and temperature probe, made of stainless steel

Milli Test Equipment (for small sample amounts):

12-1777 Milli Test Insert “pPM” Consisting of: 1 cover and 1 cup (sample quantity 2 to 15 ml, ideal 7 ml), made of brass

12-1785 Milli Cup “pPM”, approx. 15 ml, made of brass12-1786 Milli Cover “pPM” with shutter assembly, made of brass

12-1787 Milli Multi-Detector “pPM” with fl ash-point detector (thermocouple) and temperature probe, made of stainless steel

Note! Flash-point results of NIRO & pPM test inserts may deviate from standard results.

Reference Liquids Flash- & Fire-PointPart-No Standard Test Name Material Flash-Point approx. Size50-9110 * ASTM D 93 Pensky-Martens Gas Oil + 65 °C 255 ml50-9111 ASTM D 92 Cleveland Lubricant + 250 °C 250 ml50-9112 ASTM D 93 Pensky-Martens Lubricant + 213 °C 250 ml50-9113 * ASTM D 93 Pensky-Martens Diesel +74.5 °C 250 ml50-9114 * ASTM D 56 TAG + 47 °C 255 ml50-9024 * ASTM D 93, IP 34 Flash-Point Gas Oil approx. 56 to 80 °C 500 ml

* Note: These liquids require special shipment as hazadous goods, due to their low fl ash-point

Spare Parts12-0778 Electric Igniter

with connector cable and plugs

12-0779 Gas Igniter with 20 cm hose

12-0781 Gas Supply Tubing, 1 meter

12-0788 Safety Detector to control gas igniter and external infl ammation

12-0790 Tong for safe hot test cup handling

12-0791 Stopper, brass (Ø 18 mm), to close the covers multi-detector opening

12-078012-1507

Stirrer Couplings, pack of 10for units built until 12/2001for units built since 1/2002

The pPM - CupThis is a special test insert with a volume of approx. 15 ml for cases, where a small sample volume is available only (Milli-Test-Insert).

Although this cup does not comply with the offi cial standards, experiments have shown that in many cases and even with a sample volume of only 2 ml, good reproducibility and test results can be achieved which agree well with those measuring strictly according to the standards.

The pPM-cup extends the application of the PMA 4 to a domain where only small sample quantities are available, e.g. cosmetics industry with very expensive perfume oils.

47

12-1030

12-1669

12-0777

12-1650


Flash-Point - Pensky-Martens Method - PM 4 (semi-automatic)

Bitumen & bituminous binders (Method B):

ASTM D 93-B - IP 34-B - ISO 2719-BAASHTO T73-B - AASHTO T172-BFTM 791-1102 - FTM 141-4293

Main Unit

12-165012-1651

PM 4 - Semi-Automatic Flash-Point Tester, Pensky-Martens MethodFeatures: - easy to manipulate- automatic overheat protection- gas and electric igniterConsisting of: stainless steel housing with two-color powder coating, swivel-mounted head, automatic overheatprotection, electric heating, electronic heater control, electric stirrer 120 rpm (method A) and250 rpm (method B) and automatic stirrer shut-off during dipping of igniter, re-cooling fanSupplied with:1 cup “PM”, 1 cover “PM”, 1 handle for cup, 1 gas igniter, 1 electric igniter, 1 stirrer coupling, 1 thermometer ASTM 9C/IP 15C, 1 thermometer ASTM 10C/IP 16CNote: Stopper (12-0791) for thermometer opening is required.Technical Data: Working temperature : approx. +40 to +360 °C (+104 to +680 °F)Stirring Speed : 120 and 250 rpmIgnition : gas and electric-type (both included) Safety : overheat protection Interface : 1 RS232 (for printer) & 1 RS232 (for downloads on PC)Dimensions, Weight : 230 x 470 x 460 mm (W x D x H), approx. 10 kgPower supply: 230 V, 50/60 Hz, 850 WPower supply: 115 V, 50/60 Hz



12-1669 Digital-Thermometer alternative for glass-thermometer. Hold-key stops the display for easy storing of the fl ash-point, while the normal display runs further. Measuring Range: up to +400°C

12-1750 Digital Precision Barometer, 0 to 1300 mbar : 1 mbar12-1751 Case for barometer12-1752 Certifi cate for barometer - 5 measuring points12-1753 Certifi cate for barometer - 10 measuring points12-1754 Battery, 9V-Block, for barometer

12-0600 Tray for cup

12-0790 Tong for handling hot handleless test cups

12-1508 Draft Defl ector (recommended for gas ignition tests)


Test Insert12-0777 Standard Test Insert “PM” (incl. in PM4)

Consisting of: 1 cup and 1 cover (standard dimensions, made of brass)

12-0785 Standard Cup “PM”, approx. 75 ml, made of brass12-0786 Standard Cover “PM” for standard cup with shutter assembly, made of brass12-0791 Stopper, brass (Ø 18 mm), to close the thermometer opening of the cover before use

ThermometerPrecision

MadeOffi cially Certifi ed

TypeRangeASTM IP

12-0657 12-0658 9C 15C -5 to + 110 : 0.5°C12-0659 12-0660 9F 15F +20 to + 230 : 1°F12-0661 12-0662 10C 16C +90 to + 370 : 2°C12-0663 12-0664 10F 16F +200 to + 700 : 5°F12-0665 12-0666 88C - +10 to + 200 : 1°C12-0667 12-0668 88F - +50 to + 392 : 2°F

Spare Parts12-0793 Handle for permanent fi xing at the cup

12-1507 Stirrer Couplings for units built since 1/2002, pack of 10

12-0778 Electric Igniter with connector cable and plugs


12-0781 Gas Supply Tubing, 1 meter

Scope of ApplicationUsed in shipping & safety regulations to defi ne fl ammable and combustible materials.Method B: Suitable for residual fuel oils, cutback residua, used lubricating oils, non-homogeneous materials like mixtures of petroleum liquids & solids, surface-fi lm building petroleum liquids or liquids with a viscosity above 5.5 cSt at +40°C.

Summary of MethodA brass test cup of specifi ed dimensions, fi lled to the inside mark with test specimen and fi tted with a cover of specifi ed dimensions is heated, while the specimen is stirred at specifi ed rates. An ignition source is directed into the test cup at regular intervals with simultaneous interruption of the stirring, until a fl ash is detected.

48

12-0540


Scope of ApplicationThis method can indicate the possible presence of highly volatile and fl ammable materials in a relatively nonvolatile or nonfl ammable material.

For the determination of the fl ash-point of liquids with a viscosity below 5.5 mm²/s (cSt) at +40°C (104°F) or below 9.5 mm²/s (cSt) at +25°C (77°F) and a fl ash-point below +93°C (200°F).

Summary of MethodA brass test cup is fi lled to the inside mark with test specimen, fi tted with a cover and heated. An ignition source is directed into the test cup at regular intervals until a fl ash is detected.For the FLASH / NO FLASH determination ignition source is applied to a tempered sample to observe whether or not a fl ash occurs. Used to detect the ability to yield fl ammable vapors.The FLASH-POINT is the lowest temperature at which the application of an ignition source causes the specimen vapors to ignite.

Flash-Point - TAG Closed Cup Method - TAG 4 (automatic)TAG Method:ASTM D 56 - FTM 791-1101 - JIS K2265

Equilibrium Method (Flashpoint):ISO 1523 - IP 492 (IP 304-1)ASTM D 3941Equilibrium Method (Flash/no Flash):ISO 1516 - IP 491 (IP 304-2) ASTM D 3934Rapid Equilibrium-Simulation:ISO 3679 (EN 456) - ISO 3680 (DIN 55 680)

Main Units

12-054012-0541

TAG 4 / Air - Automatic Flash-Point Tester, TAG Method (air cooled)TAG Method: ASTM D 56 - FTM 791-1101 - JIS K2265Equilibrium Method: ASTM D 3941 (fl ash/no fl ash) ASTM D 3934 with further accessories for:Rapid Equilibrium-Simulation: ISO 3679 - ISO 3680

Features:- swivel-around multi-function-head - ONE TWIST- automatic barometric pressure correction- automatic overheat protection- Peltier element system- fl ash-point control, also for external ignition- rapid heating mode- PC-software

Consisting of:stainless steel housing with two-color powder coating, touch-key panel with large LC-display (visible in up to 10 m distance) swivel-mounted multi-function-head - ONE-TWIST, two RS232-interfaces for data printer and computer connection, different test-programs, data-transfer and software upgrading through bi-directional interface, Peltier element system, automatic barometric pressure correction, automatic overheat protection, power controlled & monitored electric igniter, gas igniter with auto-relighting and safety shut-off, re-cooling fan.

PC-Software “TAGCon” (Windows®):for easy handling and storing of data as well as program transfer from the PC-Memory into the TAG 4. Easy to read tableau. Numerous programs can easily be set, copied from the memory and modifi ed. Permanent indication of test status. Due to the most comfortable properties of this software to display and modify actual and future test sequences, it is most recommendable for samples of permanently changing characteristics.

Supplied with:1 cup “TAG”1 cover “TAG”1 multi-detector “TAG”1 gas igniter1 electric igniter1 stopper1 tong for cup1 tray for cup and multi-detector1 PC-software “TAGCon”

Technical Data: Working temperature : 0 to +110 °C (+32 to +230 °F)Ignition : gas and electric-type (both included)Sensing System : Differential-Thermocouple MethodAir Pressure : Automatic Barometric Pressure Correction of measured values max error 0.6% full scale (FS=115 kPa)Safety : Overheat protection, automatic ignition fl ame, automatic shut-offInterface : 1 RS232 (for printer) & 1 RS232 (for downloads on PC)Dimensions, Weight : 230 x 470 x 460 mm (W x D x H), approx. 8 kgGas supply : Propane/butane or natural gas, preset to max. 0.05 barPower supply : 115/230 V, 50/60 Hz, EU-Plug Power supply : 115/230 V, 50/60 Hz, US-Plug

Programs:2x ASTM standard Program 2x Rapid-Heating-Program2x Rapid-Test Simulation2x Equilibrium Program2x Search-Program 2x Customized-Program, (user defi ned)

49

12-1508

12-1763

12-0600

25-0382

12-054212-0543

TAG 4 / Liquid - Automatic Flash-Point Tester, TAG Method (liquid cooled)TAG Method: ASTM D 56 - FTM 791-1101 - JIS K2265Equilibrium Method: ISO 1523 - IP 492 (fl ash/no fl ash) ISO 1516 - IP 491

Consisting of:like Standard Unit (12-0540), but with connections for external liquid cooling.

Note: Circulation cooler (e.g. 25-0382) is required.

Technical Data: Working temperature : -30 to +110 °C (-22 to +230 °F)(if externally cooled)

Power supply : 230 V, 50/60 Hz, EU-plugPower supply : 115 V, 60 Hz, US-plug

Tempering Accessories

25-038225-0383

Circulation Cooler (for external cooling)Necessary for counter-cooling the Peltier element system (to let the TAG 4 reach a test-temperature of approx. -30 °C (at +20°C ambient temperature)).Supplied with: 1 insulated hose-set (Ø 8 mm, 2x 2 m)Note: For details see : General Equipment, page 69 Dimensions / Weight : 23 x 36 x 38 cm (W x D x H), 23 kgPower supply : 230 V, 50/60 Hz, 3.5 A, EU-plugPower supply : 115 V, 60 Hz

25-0228 Insulating Hose Set for circulation coolerConsisting of: 2x 2 m hoses (Ø 8 mm), 4 hose clamps

12-0518 Insulating Hood as ice protection to protect the cover and shutter assembly from icing.Recommended for low temperature fl ash-point tests, made of Styrofoam®.

Options & Accessories12-0559 Calibration Set “TAG”

Consisting of:1 calibration cover, 1 thermometer ASTM 9C/IP 15C, 1 thermometer IP 57C

12-1762 Calibration-Adapter for Pt-100 in multi-detector

12-1508 Draft Defl ector (recommended for gas ignition tests)

12-1509 Stand to hold 12 multi-detectors

12-0600 Tray for cup and multi-detectorNote: An option for all TAG 4 units built before 05/2004, since than allready included.


12-0572 PC-Software “TAGpro” (Windows®):to extend the TAGcon-functions and allow the direct data export to Excel® (not included).Further possibilities are the connection of up to 4 TAG-units to 1 PC.Note: For each TAG-unit a seperate TAGpro-software is to be ordered.

25-028225-0283


Test Inserts


50

12-1514

12-0553


Standard Test Equipment12-0553 Standard Test Insert “TAG” (incl. in TAG 4)

Consisting of: 1 cup and 1 cover

12-0548 Standard Cup “TAG”, 50 ml

12-0549 Standard Cover “TAG”, with shutter assembly

12-0550 Standard Multi-Detector “TAG”, with fl ash-point detector (thermocouple) and temperature probe

Rapidfl ash Simulation Test Equipment12-1514 Rapidfl ash Simulation Set

Consisting of: 1 rapidfl ash cup, 1 rapidfl ash cover, 1 stopper, 1 syringe and 1 multi-detector

12-1515 Rapidfl ash Cup12-1516 Rapidfl ash Cover, with shutter assembly

12-0577 Multi-Detector “pAB/pTA“, for rapidfl ash-tests

12-1518 Syringe for sample introduction, 10 mlNote: Flash-point results of rapidfl ash simulation may deviate from standard results.

Milli Test Equipment (for small sample amounts), composed of:12-0560 Milli Cup “pTA”, approx. 10 ml

12-0549 Standard Cover “TAG”, with shutter assembly

12-0577 Multi-Detector “pAB/pTA” for milli-testsNote! Flash-point results of milli test inserts may deviate from standard results.

Reference Liquids Flash- & Fire-PointPart-No Standard Test Name Material Flash-Point approx. Size50-9110 * ASTM D 93 Pensky-Martens Gas Oil + 65 °C 255 ml50-9111 ASTM D 92 Cleveland Lubricant + 250 °C 250 ml50-9112 ASTM D 93 Pensky-Martens Lubricant + 213 °C 250 ml50-9113 * ASTM D 93 Pensky-Martens Diesel +74.5 °C 250 ml50-9114 * ASTM D 56 TAG + 47 °C 255 ml50-9024 * ASTM D 93, IP 34 Flash-Point Gas Oil approx. +56 to +80 °C 500 ml

* Note: These liquids require special shipment as hazadous goods, due to their low fl ash-point

Spare Parts12-0778 Electric Igniter

with connector cable and plugs


12-0514 Safety Detector to control gas igniter and external infl ammation

12-0790 Tong for safe hot test cup handling

12-0791 Stopper, brass (Ø 18 mm), to close the covers multi-detector opening before use

51

12-1540

12-0629

12-1250

Flash-PointFlash-Point (open cup) (open cup)

Scope of ApplicationFor Flash- and Fire-Point measurements of liquids having fl ash-points between −18 and 165°C (0 and 325°F) and fi re-points up to +165°C according to ASTM D 1310 and of cutback asphalt having fl ash-points below +93°C according to ASTM D 3143.

Flash-point and fi re-point of a liquid are used to defi ne their fl ammability hazards.

Summary of MethodThe specimen is placed in the cup of a Tag Open-Cup Apparatus and heated at a slow, but constant rate. A small test fl ame is passed at a uniform rate across the cup at specifi ed intervals until a fl ash occurs.

The fl ash-point is the lowest temperature at which the vapor at the liquid surface will fl ash.

For the fi re-point, the test is continued until the test fl ame causes the specimen to ignite and burn for at least 5 s.

Flash-Point - TAG Open Cup Method - (semi-automatic)

Cut-Back Bitumen:

ASTM D 3143 (AASHTO T 79)

Main Unit

12-1540

Semi-Automatic Flash-Point Tester, TAG MethodASTM D 1310 - ASTM D 3143Consisting of:stainless steel housing, bath with electric heater, electrically driven sweep arm for the test fl ame applicationSupplied with: 1 open glas cupNote: pre-regulating valve for gas or LPG-gas tank and thermometer are required.Technical Data:Temperature range : ... to +93 °C (.... to +199 °F)Ignition : gas Dimensions : 31 x 29 x 33 cm (W x D x H), weight: 6 kgPower supply: 220-240 V, 50/60 Hz, 500 W (110-120 V available upon request)



12-0629 Pre-Regulating Valve for gas supply with hose adapter, suitable for all types of burning gases

12-1250 Gas Tank (portable and refi llable)Consisting of: built-in on/off switch, igniter and standSupplied with: 1 m gas tubingNote: To be fi lled by using any standard gas lighter refi ll cartridge.

We highly recommend to buy the LPG - Refi ll Container locally, because it would require special shipment as hazardous goods.

50-9114 Reference Liquid “ASTM D 56” (approx. +47°C), 255 mlNote: Requires special shipment as hazardous goods.

Thermometer

Precision Made


TypeRange

ASTM

12-0683 12-0689 9C -5 to + 110 : 0.5°C (for bath)

12-0684 12-0690 9F +20 to + 230 : 1°F (for bath)

13-0161 13-0162 33C -38 to + 42 : 0.2°C (for cup)

90-0141 90-1141 33F -36.5 to + 107.5 : 1°F (for cup)

Spare Parts12-1542 Cup, made of glass 12-0109 Silicone Tubing, 4 m

52

Filtration Unit

Distillation Unit

17-0710

17-0802

Paraffi n ContentParaffi n Content

Scope of ApplicationA procedure for determination the paraffi n wax content of bitumen and bituminous binder.

Paraffi n Wax Content - Distillation Method - (manual)

Cut-Back Bitumen:EN 12606-1 (DIN 52 015) - IP 459-1

Main Unit

10-016010-0161

Paraffi n Wax Content ApparatusEN 12 606-1 (DIN 52 015) - IP 459-1

Consisting of:Distillation Unit: 1 distillation fl ask (100 ml) with stopper and protecting ring,

1 Erlenmeyer fl ask (100 ml) with bored rubber stopper, 1 glass vessel (Ø 140 x 75 mm)support stand, universal gas burner and adjustable table

Filtration Unit: 1 cooling bath (for direct cooling) with sockets for tempering unit, 1 suction fl ask (500 ml) with bored stopper, 1 water jet pump with U-tube vacuum meter and 2 meters tubing, 3 test tubes with spout, bored stopper, 3 special test tubes (NS 29/32) with splash bulb attachment, 1 bath thermometer (-30 ... +50:0.5 °C), 1 sample thermometer (-38 ... +50:1 °C), 1 congealing point thermometer (0 ... +100 °C) with sleeve stand

Note: Cooling bath requires counter-cooling.Power supply: 230 V, 50/60 Hz, EU-plugPower supply: 115 V, 50/60 Hz


17-071017-0711

Circulator (external & internal heating & cooling) programmable & regulated by Main-UnitFor counter-cooling the fi ltration cooling bath.Consisting of: Cooler with stainless steel bath. Thermostat with digital display, splash-proof keypad, heater, pump, RS232-interface, Pt-100-socket, programmer, over/under-temperature & low-level protection, adjustable pump-pressure, cooling control.Supplied with: 1 bath cover, 1 drain tap, 1 insulated hose-set (Ø 8 mm, 2x 2m)Note: For details see: General Equipment, page 68Dimensions / Weight: 31 x 42 x 66 cm (W x D x H), 38 kgPower Supply: 230 V, 50 Hz, EU-plugPower Supply: 230 V, 60 Hz

17-080217-0804

Circulation Air Oven14 l capacity, thermostatically-controlled between +60 and +200 °C, temperature constancy of +/- 2-3 K, includes time switch, thermometer for temperature inspection and perforated intermediate bottom.Dimensions (W x H x D): outside 31 x 38.5 x 47 cm / inside 19 x 20 x 36 cmWeight: 17 kg.Power supply: 230 V, 50/60 HzPower supply: 115 V, 50/60 Hz

25-047025-0471

Vacuum-Pump with Mini-Compressor (oil-free diaphragm pump with fi lter)Max. capacity: 6 l/minEnd vacuum: 100 mbarOperating pressure: 2.4 bar (overpressure)Dimensions / Weight: 9 x 17 x 12 cm (W x D x H), 1.9 kgPower supply: 220/230 V, 50 Hz, EU-plugPower supply: 110/115 V, 60 Hz

ThermometerPrecision

MadeStopper

(NBR-rubber) Type Range

16-0264 11-0030 DIN 12 775 -30 to -50 : 0.5°C (for bath)16-0313 10-0236 DIN 12 785 -38 to +50 : 1 °C (for sample)17-0010 — ISO 2207 0 to +100 : 0.5°C (congealing point)

Spare Parts10-0013 Water Jet Pump, Hanff, glass

10-0136 Vacuum Flask, 500 ml10-0239 Stopper for vacuum fl ask

10-0144 Distillation Flask (EN 12606-1), 100 ml10-0145 Protecting Ring for distillation fl ask10-0234 Stopper for distillation fl ask

10-0166 Receiver, Erlenmeyer Flask, 100 ml10-0235 Stopper for Receiver Erlenmeyer fl ask

10-0167 Test Tube with spout (EN 12606-1)

10-0168 Reagent Tube (standard taper NS 29/32)

10-0169 Splash Head (standard taper NS 29/32)

10-0170 U-Tube-Manometer 500-0-500 mm Acrylic tube on metal plate for wall mounting. Suitable for measuring pressures to 98 mbar with water or 1.33 bar with mercury fi lling. Note! Mercury is not included

10-0171 Round Filter Ø 110 mm, pack of 100

11-0110 Universal Gas Burner for butane, propane, town & natural gases

13-0923 Hose, 1 m (5x 1.5 mm, Silicon)

16-0925 Test Cup (DIN 12 338), 700 ml, glass

53

Dean & StarkASTM D 95 / ISO 3733

ASTM D 244

WaterWater Content Content

Water Content - Distillation Method - (manual)

Petroleum Products & Bituminous Materials (Dean & Stark App.)ASTM D 95 - JIS K2275 - AASHTO T55 - IP 74 (BS 4385)- ISO 3733 (DIN 51 582, DIN 1995)

DIN 1996-5

Emulsifi ed Asphalts (Dean & Stark App.)ASTM D 244 - AASHTO T59 - IP 291 (BS 434)

EN 1428 (DIN 52 048, DIN 1995)

Main Unit

16-083016-1430

Water Content Determination Apparatus for Petroleum Products and Bituminous Materials (Dean & Stark)ASTM D 95 - JIS K2275 - AASHTO T55 - IP 74 - EN 1428 (DIN 52 048)Consisting of:- 1 fl ask (500 ml), standard taper (NS 29) - 1 glass trap (10 ml), standard taper (NS 29) - 1 refl ux condenser (400 mm), standard taper (NS 29)

Supplied with: - 1 electric heater (800 W), stainless steel housing - 1 heating board (center hole Ø 70 mm) - support rod (600 mm) with 4 adjustable clampsPower supply: 230 V, 50 Hz, EU-plugPower supply: 230 V, 60 Hz

16-183916-1452

Supplied with: - 1 heating mantle (565 W) & support ring for 500 ml fl ask - 1 electronic energy regulator (2000 W) - support rod (600 mm) with 4 adjustable clamps and base platePower supply: 230 V, 50 Hz, EU-plugPower supply: 230 V, 60 Hz

16-085016-1450

Water Content Determination Apparatus for Petroleum Products and Bituminous Materials (Extended Dean & Stark)ISO 3733 (DIN 51 582, DIN 1995) but also for: ASTM D 95 - JIS K2275 - AASHTO T55 - IP 74 - EN 1428 (DIN 52 048)Consisting of:- 3 fl asks (250, 500 and 1000 ml), standard taper (NS 29)- 3 glass traps (6, 10 and 25 ml), standard taper (NS 29)- 1 refl ux condenser (400 mm), standard taper (NS 29)

Supplied with: - 1 electric heater (800 W), stainless steel housing- 3 heating boards (center hole Ø 50, 70 and 89 mm) - support rod (600 mm) with 4 adjustable clampsPower supply: 230 V, 50 Hz, EU-plugPower supply: 230 V, 60 Hz

16-185016-1458

Supplied with: - 1 heating mantle (345 W) & support ring for 250 ml fl ask - 1 heating mantle (565 W) & support ring for 500 ml fl ask - 1 heating mantle (875 W) & support ring for 1000 ml fl ask - 1 electronic energy regulator (2000 W) - support rod (600 mm) with 4 adjustable clamps and base platePower supply: 230 V, 50 Hz, EU-plugPower supply: 230 V, 60 Hz

16-084416-1444

Water Content Determination Apparatus for Emulsifi ed AsphaltsASTM D 244 - AASHTO T59 - IP 291Consisting of:- 1 fl ask (500 ml), standard taper (NS 29)- 1 glass trap (25 ml), standard taper (NS 29)- 1 refl ux condenser (400 mm), standard taper (NS 29)

Supplied with: - 1 electric heater (800 W), stainless steel housing - 1 heating board (center hole Ø 70 mm) - support rod (600 mm) with 4 adjustable clampsPower supply: 230 V, 50 Hz, EU-plugPower supply: 230 V, 60 Hz

16-184416-1454


Scope of ApplicationFor the determination of water in petroleum products, tars, and other bituminous materials by the distillation method.

The test arrangement consists of a set of glassware and a suitable heater.As far as the standard taper joints fi t together, many other individual combinations are possible, dependent upon customer’s requirements.

Summary of MethodBituminous Material Methods: The material to be tested is heated under refl ux with a water-immiscible solvent, which co-distills with the water in the sample. Condensed solvent and water are continuously separated in a trap, the water settling in the graduated section of the trap and the solvent returning to the still.

Emulsifi ed Asphalts Methods: They are determining the water content of an emulsifi ed asphalt by refl ux distillation, using a water trap to measure the amount of water present in the emulsifi ed asphalt, as distinguished from either bitumen or petroleum solvent.

54

DIN 1996-5


16-084516-1445

Water Content Determination Apparatus for Bituminous MaterialsDIN 1996-5Consisting of:- 1 fl ask (500 ml), standard taper (NS 45) - 1 adapter, standard taper (NS 45 to NS 29) - 1 glass trap (10 ml), standard taper (NS 29) - 1 refl ux condenser (400 mm), standard taper (NS 29)

Supplied with: - 1 electric heater (800 W), stainless steel housing - 1 heating board (center hole Ø 70 mm) - support rod (600 mm) with 4 adjustable clamps Power supply: 230 V, 50 Hz, EU-plugPower supply: 230 V, 60 Hz

16-184516-1455


Glassware (Options & Accessories & Spares)

16-087816-0879

Liebig Refl ux Condenser NS 29 with special drip tip for easy counting of drops... 250 mm... 400 mm

16-0898 Drying Tube for ASTM D 4006

FlasksVolume Erlenmeyer fl ask

DIN 12 387with standard taper

Round fl ask DIN 12 348 with standard taper

Round fl ask DIN 12 394 with standard taper and side neck

[ml] NS 29/32 NS 45/40 NS 29/32 NS 45/40 NS 29/32 NS 45/40

250 16-0859 16-0862 16-0865 16-0869 16-0873 500 16-0860 16-0863 16-0866 16-0870 16-08741000 16-0861 16-0864 16-0867 16-0871 16-08752000*) 16-0868 16-0872 16-0876 16-0877

Adapter(NS 29 to 40) 16-0897 16-0897 16-0897

Sleves (PTFE) with

Rips 50-7027 50-7030 50-7027 50-7030 50-7027 50-7030Gripping Ringmultiple use, pack of 10

50-7047 50-7050 50-7047 50-7050 50-7047 50-7050

TrapsOrder No. Size [ml] Measuring Tube End 0-Point16-0880 2 : 0.05 round at bottom

16-0901 5 : 0.05 round at bottom

16-0881 * 6 : 0.05 conical at tip

16-0882 * 6 : 0.05 with cock at cock

16-0883 * 6 : 0.05 round above bottom

16-0884 * 6 : 0.05 with cock above cock

16-0886 10 : 0.1 conical at tip

16-0887 10 : 0.1 round above bottom

16-0888 10 : 0.1 with cock above cock

16-0889 10 : 0.1 with cock at cock

16-0890 25 : 0.1 conical at tip

16-0891 25 : 0.1 round above bottom

16-0892 25 : 0.1 with cock above cock

16-0902 25 : 0.1 with cock at cock

* Can be used when 5 : 0.1 ml types are recommended.

*) For electrical heating of a 2000 ml fl ask, heating mantle (16-0825), stand (16-0824) and electronic energy regulator (25-0001) are recommended.

The sleeves are recommended for assembling the glassware. They prevent a sticking together and on the other hand assure tightness.

55

17-0802

25-0001 / 25-0108

Heating Mantle


CylindersVolume [ml] Graduated cylinder (DIN 12 680) Mixing cylinder (DIN 12 685)

50 16-0899 100 11-0130 250 16-0820 17-0584 500 16-0705 16-07421000 26-0014 16-0675

Sample Thermometer DIN 12 784 with collar NS 14/23, Range 0 ... +250 : 1 °C

Precision Made insertation depth for fl ask with side neck

16-0893 120 mm 16-0873

16-0894 150 mm 16-0874

16-0895 160 mm 16-0875

16-0896 195 mm 16-0876 / 16-0877

Heating Mantles

Flask Size ≤ 250 ml




Electronic Energy

Regulator

Power supply 230 V, 50 Hz 25-0706 25-0700 25-0702 16-0825 25-0001

115 V, 60 Hz 25-0707 25-0701 25-0703 16-0829 25-0108

Support Ring 25-0708 25-0704 25-0705 incl.

Support Stand(base plate, 750 mm rod, 2 adjustable clamps Ø 40 mm, 3 boss heads)

16-0824 16-0824 16-0824 16-0824

Heating Devices

11-013811-013911-0140

Heater Board, 150 x 150 x 4 mm ceramic, with a ... 50 mm Ø center hole... 70 mm Ø center hole... 89 mm Ø center hole

16-0898 Gas Heating Device Consisting of:universal gas burner, ring holder, wire net and support stand (base plate, 750 mm rod, 2 adjustable clamps Ø 40 mm, 3 boss heads)

17-080217-0804

Circulation Air Oven14 l capacity, thermostatically-controlled between +60 and +200 °C, temperature constancy of +/- 2-3 K, includes time switch, thermometer for temperature inspection and perforated intermediate bottom.Dimensions (W x H x D): outside 31 x 38.5 x 47 cm / inside 19 x 20 x 36 cmWeight: 17 kg.Power supply: 230 V, 50/60 HzPower supply: 115 V, 50/60 Hz

Spare Parts for Electric Heater11-0018 Heater Rod,

encased shape with rear-gold coating

11-0019 Heater Plate, complete with 4 heater rods

25-000425-0009

Heater Module "m2" for sensitive regulation of heating energyPower supply: 230 V, 50/60 HzPower supply: 115 V, 50/60 Hz

56

DistillationDistillation

Scope of ApplicationThis procedure measures the amount of the more volatile constituents in cut-back asphaltic products. The presence of silicone in the cut-back may affect the distillation residue by retarding the loss of volatile material after the residue has been poured into the residue container.

Suitable for the distillation of cut-back asphaltic (bituminous) products.

Summary of Method200 ml of a sample are distilled in a 500 ml fl ask at a controlled rate to a sample temperature of +360 °C (680°F) and the volumes of distillate obtained at a specifi c temperature are measured.

The residue from the distillation, and also the distillate, may be tested as required.

Distillation Analysis - Cut-Back Bitumen ASTM-Method (manual)

Cut-Back (Fluxed) Bitumen:ASTM D 402 - AASHTO T 79 - IP 27 (BS 4453) - EN 13358 (NF T66-003)

Main Unit10-0213 Distillation Apparatus - Cut-Back Bitumen (ASTM-type)

ASTM D 402 - AASHTO T 79 - IP 27 (BS 4453) - EN 13358 (NF T66-003)Consisting of:1 thermometer ASTM 8C (precision made) with holder (bored stopper)1 distillation fl ask (500 ml) 1 fl ask shield with two-part ceramic cover 1 ring support with wire gauze 2 support rods with clamps and base plates1 adjustable universal gas burner1 condenser tube (400 mm) with special jacket 1 cylindrical graduated receiver (100 : 1 ml) and connection material (adapter etc)

Thermometer

Precision Made


TypeRange Holder

(Stopper)ASTM IP

11-0155 11-0156 8C 6C -2 to +400 : 1 °C 10-0210

Spare Parts11-0130 Cylindrical Graduated Receiver

(100 ml : 1 ml division)

11-0503 Graduated Receiver (100 ml : 1 ml division, BS 658) with conical lower part (0 ... 10 ml) and base

10-0220 Adapter10-0217 Condenser Tube (400 mm)

10-0204 Stopper for condenser tube, DIN 12 871, NS 24/30, Ø 12 mm

10-0218 Condenser Jacket10-0214 Connecting Tube, Silicon, 1 m

(Ø 10 x 2 mm)

10-0210 Stopper, NBR, to hold thermometer, NS 29/30, bored Ø 6.5 mm

11-0155 Distillation Thermometer ASTM 8C/ IP 6C

10-0216 Distillation Flask (500 ml, Ø 102 mm) short-necked

10-0205 Flask Shield, stainless-steel with ceramic insulation and windows

10-0208 Insulating Cover, ceramic, 2-part

10-0178 Ring Support with wire gauze

11-0110 Universal Gas Burner for butane, propane, town & natural gas

57


Distillation Analysis - Cut-Back Bitumen DIN-Method (manual)

Cut-Back (Fluxed) Bitumen:DIN 52 024

Main Unit10-0173 Distillation Apparatus - Cut-Back Bitumen (DIN-type)

DIN 52 024Consisting of:1 distillation thermometer (precision made)1 distillation fl ask (500 ml) 1 fl ask shield of stainless steel with windows and ceramic insulation1 two-part ceramic cover1 ring support 2 support rods with 3 boss heads, 1 clamp and 2 base plates1 Universal gas burner 1 glass condenser tube (360 mm)6 Erlenmeyer fl ask (100 ml) 1 base for 100 ml fl askand connection material (2 silicon stoppers (bored Ø 4 & 10 mm))

Thermometer

Precision Made


TypeRange Holder

(Stopper)DIN

10-0154 10-0155 12 779 0 to +360 : 1 °C 10-1298

Spare Parts10-0166 Erlenmeyer Flask (100 ml)

10-0175 Distillation Flask (500 ml)

10-0176 Condenser Tube (360 mm), glass

10-129810-1297

Stopper, silicon NS 27/30, bored... Ø 4 mm for thermometer... Ø 10 mm for side-neck

10-0177 Flask Shield, stainless-steel with ceramic insulation and windows


10-1178 Ring Support 11-0110 Universal Gas Burner for butane,

propane, town & natural gas

Scope of ApplicationThis procedure measures the amount of the volatile constituents and the residue in in cut-back asphaltic products. Suitable for the distillation of cut-back asphaltic (bituminous) products.

Summary of MethodA 200 g sample is distilled at a controlled rate up to +360 °C (680°F) into tared receivers.

The masses of distillate fractions and of the residue are determined at a specifi ed temperature.

58


Scope of ApplicationDistillation devices according to these standards are used for determination of boiling characteristics, asphalt residue, total distillate and fractions of bituminous materials, tar products and creosote at specifi ed distillation temperatures.

Suitable for the distillation of bituminous material, tar products and creosote.

Summary of MethodA 100 g sample is distilled at a controlled rate from a 300 ml fl ask into tared receivers.

The masses of distillate fractions at a series of specifi ed temperatures and of residue at the maximum specifi ed temperature are determined.

Distillation Analysis - Road Tar ASTM-Method (manual)

Road Tars:ASTM D 20 (ASTM D 246)

Main Unit10-0203 Distillation Apparatus - Road Tar Products (ASTM-type)

ASTM D 20 (ASTM D 246)Consisting of:1 distillation fl ask (diameter 86 mm) 1 thermometer ASTM 8C (precision made) 1 stopper to hold thermometer1 fl ask shield and two-part ceramic cover1 ring support with wire gauze 2 support rods with clamps and base plate1 adjustable universal gas burner1 condenser tube (360 mm) 6 receivers, and connection material (adapter etc.)

Thermometer

Precision Made


TypeRange

Holder(Stopper)ASTM IP

11-0155 11-0156 8C 6C -2 to +400 : 1 °C 17-0047

Spare Parts10-0166 Receiver Erlenmeyer Flask (100 ml)

10-0220 Adapter10-0207 Condenser Tube (360 mm long)

17-0047 Stopper, NBR, to hold thermometer, NS 29/30, bored Ø 6 mm


10-0206 Distillation Flask (Ø 86 mm) short necked

10-0205 Flask Shield, stainless-steel with ceramic insulation and 2 windows


10-0178 Ring Support with wire gauze

11-0110 Universal Gas Burner for butane, propane, town & natural gas

59


Distillation Analysis - Road Tar DIN-Method (manual)

Road TarsDIN 52 027

Main Unit10-0152 Distillation Apparatus - Road Tar Products (DIN-type)

DIN 52 027Consisting of:1 heater housing of stainless-steel 1 universal gas burner 1 fractionation fl ask (500 ml) 1 thermometer (precision made) 1 Liebig condenser tube 400 1 condenser tube (600 mm) 6 receivers 1 support rod with 1 boss head, 1 clamp and 1 base plate and connection material (2 silicon stoppers (bored Ø 4 & 12 mm))



Thermometer

Precision Made


TypeRange Holder

(Stopper)DIN

10-0154 10-0155 12 779 0 to +360 : 1 °C 10-0298

Spare Parts10-0166 Erlenmeyer Flask (100 ml)

10-0153 Fractionating Flask (500 ml)

10-0156 Condenser Tube (600 mm, Ø 22 mm)

10-0157 Liebig Condenser Tube “400”(for cold tars to +170 °C)

10-029810-1297

Stopper, silicon, pack of 20, bored... Ø 4 mm, NS 30/32, for thermometer... Ø 12 mm, NS 22/25, for side-neck

10-0159 Heater Housing, stainless-steel, with holding ring and wire gauze


10-0158 Universal Gas Burner, special shape

Scope of ApplicationThis procedure measures the amount of the more volatile constituents in fl uxed bitumen. Suitable for the distillation of fl uxed bitumen.

Summary of Methodapprox. 250 g of a sample are distilled at temperature up to +350 °C. The reciver will be changed at +170°C, +270°C and +300°C.

60

Distillation Analysis - Pitch-Method (manual)

ASTM D 2569

Main Unit10-0179 Distillation Apparatus - Pitch

ASTM D 2569Consisting of:electric heater 800 W with high-capacity low-mass heater elements for precise energy input control, triac controller, heater carrier infi nitely adjustable in heightSupplied with:1 ceramic insulation cover1 distillation fl ask Ø 86 mm1 thermometer ASTM 8C (-2 to +400 °C)1 condenser tube1 fl ask shield1 heater board6 Erlenmeyer fl ask2 support rods2 clamps2 stoppers2 base plate2 boss head1 lifting tablePower supply: 230 V, 50/60 Hz

Thermometer

Precision Made


TypeRange

Holder(Stopper)ASTM IP

11-0155 11-0156 8C 6C -2 to +400 : 1 °C 17-004711-0157 11-0158 8F +30 to +760 : 2 °C

Spare Parts10-0166 Receiver Erlenmeyer Flask (100 ml)

10-0207 Condenser Tube (360 mm long)

17-0047 Stopper, NBR, to hold thermometer, NS 29/30, bored Ø 6 mm


10-1297 Stopper, silicon, pack of 20, boredØ 12 mm, NS 22/25, for side-neck

10-0206 Distillation Flask (Ø 86 mm) short necked

10-0205 Flask Shield, stainless-steel with ceramic insulation and 2 windows


11-0119 Support Board center hole Ø 80 mm glass ceramic (150 x 150 x 4 mm)

50-5242 Lifting Table, mechanical Base plate: 160 x 130 mm Weight: 60 kg capacity

Scope of ApplicationThis test method covers a distillation test for pitch applicable whenever the amount of distillate below +270 °C is less than 2.0 % by this test method.

Suitable for the distillation of pitch.

Summary of MethodA 100 g sample is distilled at a designated rate.

The weight of the destillate fractions at specifi ed temperatures and the time required to collect the main fraction are recorded.


61

HubbardGay-Lussac

Lipkin

DensityDensity

Density, Relative Density - Pycnometer Method (manual)

Capillary-Stopperd Hubbard Pycnometer:ISO 3838 (DIS 3658) - JIS K2249ASTM D 70 - IP 190 (BS 4699) DIN 52 004 (DIN 1995)Capillary-Stopperd Gay-Lussac Pycnometer:ISO 3838 (DIS 3658) - JIS K2249IP 190 (BS 4699)

Graduated Bicapillary Lipkin Pycnometer:ISO 3838 (DIS 3658) - JIS K2249ASTM D 1481 - IP 189 (BS 4699)

Pycnometer26-0712 Lipkin-Pycnometer, 5 ml

Bitumen: ASTM D 1481 - IP 189 (BS 4699) ISO 3838 - JIS K2265 Suitable for very small sample amounts with a kinematic viscosity <50 cSt (mm²/s) at test temperature.

26-0721 Gay-Lussac-Pycnometer, 25 mlBitumen: ISO 3838 - JIS K2265 - IP 190 (BS 4699)Suitable for non-volatile liquids

26-0740 Hubbard Pycnometer, 24 mlBitumen : ASTM D 70 - ISO 3838 - JIS K2265

26-0741 Hubbard-Pycnometer, 25 mlBitumen : ASTM D 70 - IP 190 (BS 4699) ISO 3838 - JIS K2265 - DIN 52 004Suitable for solids or high viscous liquids.

Options & Accessories26-0790 Holder (for Lipkin-Pycnometer)

26-0791 Holder (for Gay-Lussac-Pycnometer)

26-0793 Clamp (for Gay-Lussac-holder 26-0791), polyethylene coated

26-0792 Holder (for Hubbard-Pycnometers 26-0740 and -0741)

26-0794 Clamp (for Hubbard-holder 26-0792)

Scope of ApplicationFor the determination of the density and relative density of petroleum products like liquid, semi-solid or solid bituminous materials, asphalt cements, and soft tar pitches by use of a pycnometer.

Capillary-StopperdGay-Lussac Pycnometer: suitable for non-volatile liquids.Hubbard Pycnometer: suitable for high viscous liquids or solids.Graduated BicapillaryLipkin Pycnometer: suitable for very small sample amounts with a kinematic viscosity <50 cSt (mm²/s) at test temperature.

Summary of MethodGraduated Bicapillary PycnometerThe liquids sample is drawn into the graduated pycnometer arms, and after it has reached equilibrium at the test temperature, the liquid levels are noted and the pycnometer weighed.

Capillary-Stopperd PycnometerThe mass of equal volumes of a sample and of water are compared. Equal volumes are ensured by the pycnometer beeing fi lled so as to overfl ow when placed in a bath at the test temperature until equilibrium is reached.

62

26-0010 / 26-0011

Hydrometer (example)

DensityDensity

Density, Relative Density - Hydrometer Method (manual)

Liquid Bitumen:ASTM D 3142

HydrometerASTM D 3142

Precision Made Hydrometer-Type Series Range : Div. Overall

LengthRef.

Temp.

26-0500

API Gravity(ASTM E 100)

1H-62 -1 to +11 : 0.1 °API

max. 330 mm

60 °F26-0501 2H-62 +9 to +21 : 0.1 °API

26-0502 3H-62 +19 to +31 : 0.1 °API

25-0503 4H-62 +29 to +41 : 0.1 °API

26-0603

ASTM Specifi c Gravity(ASTM E 100)

85H-62 0.800 to 0.850 : 0.0005 sp gr

max. 330 mm

60/60°F

26-0604 86H-62 0.850 to 0.900 : 0.0005 sp gr

26-0605 87H-62 0.900 to 0.950 : 0.0005 sp gr

26-0606 88H-62 0.950 to 1.000 : 0.0005 sp gr

26-0607 89H-62 1.000 to 1.050 : 0.0005 sp gr

26-0608 90H-62 1.050 to 1.100 : 0.0005 sp gr

Note: °F-type not available with certifi cate. Suitable hydrometer cylinder (26-0014)

Scope of ApplicationThe Hydrometer Method is suitable for determining the density of cutback asphalts which are liquid at room temperature by using a glass hydrometer.

For materials that are solid or semi-solid at room temperature, use Hubbard Pycnometer Method ASTM D 70

Summary of MethodThe sample is brought to the testing temperature and transferred to a cylinder at approximately the same temperature.The cylinder and its contents are placed in a constant temperature bath to avoid excessive temperature variation during the test. The appropriate hydrometer is lowered into the sample and allowed to settle.After temperature equilibrium, the hydrometer is read and the temperature of the sample is noted.The hydrometer reading is converted to the density at +15°C using standard tables.

Pycnometer & Hydrometer Tempering Equipment

26-001026-0011

Tempering Bath for determinations up to +60°C by pycnometer, hydrometer or viscometer.

Consisting of:Acrylic glass bath (foot print 280 x 430 mm, depth of the bath 300 mm) with cooling-coil.Thermostat with digital display, splash-proof keypad, heater, pump and over-temperature protection.

Supplied with:1 pycnometer bath cover with 4 openings (Ø 50.5 mm)1 hydrometer bath insert with clamps, 4 openings (Ø 55 mm) and 4 cylinders (Ø 54 x 300 mm)5 lids (20-0024) for the unused openings1 bath-thermometer, -2 to +105 :0.5 °C (incl. stopper)

Note: Bath is suitable for hydrometer with an overall length of maximal 275 mm or viscometers. Measurements at temperatures lower than +25 °C require a counter-cooling device, (e.g. Recirculating Cooler 25-0368 or 25-0373)

Technical Data: Testplaces : 4Working range : approx. +25 to +60 °C (without counter-cooling)Display / Resolution : LED / 0.1°CControl : PIDHeater capacity : 2000 W (115 V = 1000 W)Pump-Pressure capacity : 15 l/min, 340 mbarBath opening : 26 x 26 x 30 cm (W x D x H)Safety class / Bath fl uid : 1 / NFL (water / water-antifreeze-mix only)Volume : 30 lSockets for : hose (Ø 8 / 10 mm)Dimensions : 28 x 43 x 50 cm (W x D x H) Power supply : 230 V, 50 Hz, EU-plugPower supply : 115 V, 50/60 Hz

63

26-0017 / 26-0018

25-0368 / 25-0373

DensityDensity

26-001726-0018

Tempering Bath for determinations up to +150°C by pycnometer, hydrometer or viscometer

Consisting of:borosilicate glass bath jar with cooling-coil.Thermostat with digital display, splash-proof keypad, integrated heater, pump, RS232-interface, over-temperature- & low-level-protection

Supplied with:1 bath insert (heat protected stainless steel) with 4 openings (Ø 67 mm) and clamps4 pycnometer adapter rings (inside Ø 50.5 mm)4 hydrometer cylinders (Ø 65 x 420 mm)5 lids (20-0024) for the unused openings1 leakage protection vessel complete with temperature insulation

Note: Bath is suitable for hydrometer with an overall length of maximal 400 mm or viscometers. Measurements at temperatures lower than +25 °C require a counter-cooling device, (e.g. Recirculating Cooler 25-0368 or 25-0373)

Technical Data: Testplaces : 4Working range : approx. +25 to +150 °C (without counter-cooling)Display / Resolution : LED / 0.01°CControl : PIDHeater capacity : 2000 W (115 V = 1000 W)Pump-Pressure capacity : 15 l/min, 320 mbarSafety class / Bath fl uid : 3 / FL (Flammable Liquids possible)Volume : 20 lInterface : RS232Sockets for : hose (Ø 8 mm)Dimensions / Weight : 35 x 37 x 60 cm (W x D x H), 20 kg Power supply : 230 V, 50/60 Hz, EU-plugPower supply : 115 V, 50/60 Hz

25-036825-0373

Circulation Cooler (tap water replacement, external cooling) with insulated hoseFor counter-cooling the tempering baths.Consisting of:Cooler with tank, digital display, splash-proof keypad, integrated pump, liquid level indication, over-/low-temperature & low-level protection.Supplied with: 1 insulated hose-set (Ø 8 mm, 2x 2 m, incl. fi ttings)Note: For details see: General Equipment, page 69Dimensions / Weight : 35 x 45 x 57 cm (W x D x H), 38 kgPower supply : 230 V, 50 Hz, 450 W, EU-plugPower supply : 115 V, 60 Hz

Bath-ThermometerPrecision

MadeOffi cially Certifi ed

TypeRangeASTM IP

13-0715 13-0716 12C 64C -20 to +102 : 0.2 °C13-0717 13-0718 12F 64F -5 to +215 : 0:5 °F21-0601 21-0607 17C +19 to +27 : 0.1 °C21-0621 21-0627 17F +66 to +80 : 0.2 °F21-0606 21-0612 22C 24C +95 to +103 : 0.1 °C21-0626 21-0632 22F +204 to +218 : 0.2 °F10-0385 10-0386 63C -8 to +32 : 0.1 °C10-0387 10-0388 63F +18 to +89 : 0.2 °F26-0036 26-0037 39C -1 to +38 : 0.1 °C26-0038 26-0039 39F +30 to +100 : 0.2 °C

DIN11-0022 bath 0 to +105 : 0.5°C10-0383 10-0384 12 775 0 to +50 : 0.1°C

Spare PartsBath up to +60°C

11-0030 Stopper, NBR-rubber, to hold bath thermometer (18/20 / bored Ø 7.5 mm)

11-0022 Bath Thermometer (0 to +105 : 0.5°C)

26-0004 Hydrometer Cylinder (Ø 54 mm x 300 mm)

Bath up to +150°C13-0565 Thermometer Protection Tube26-0026 Adaptor Ring, inside Ø 50.5 mm

for pycnometer holders

26-0014 Measuring Cylinder, borosilicate glass, 1000 : 10 ml with plastic stand asHydrometer Cylinder (Ø 65 x 420 mm)

64

25-0282

25-0418 & 25-0420

Scope of ApplicationThe Displacement Method for the determination of the density or relative density of hard pitches and asphalts with softening points above +70°C.

The Balance Method is suitable for determining quickly and accurately the density or relative density of petroleum products, such as gasoline, kerosene and gas oil, particularly when the quantities available for test are small.

Summary of MethodDisplacement Method:The sample is suspended from a thin wire and weighed, fi rst in air, then submerged in water at +25.0 °C. The relative density is calculated from these weights.

Balance Method:To determine the density at test temperature, a balance is measuring the buoyancy of a bob suspended from a thin wire and immersed in a liquid sample at ambient temperature.

Density, Relative Density - Displacement / Balance Method (semi-automatic)

Displacement Method:ASTM D 71 (IP 59-B)

Balance Method:DIN 51 757-2 (IP 59-A)

Main Unit

26-001926-0020

Digital Density Test Rig

Bitumen: ASTM D 71 (IP 59-B) Fuel/Oil: DIN 51 757-2 (IP 59-A)

Consisting of:1 digital balance with electronic computation module to convert measured boyance to density1 stand with platform for balance1 lift for test cylinderSupplied with: 1 test cylinder (120 ml)1 thermometer (+10 to +30:0.1 °C)1 underfl oor hook1 bob (10 ml)1 test weight, 100 g (for balance control)

Technical Data: Density measuring range : 0.0 to 2.1 g/qcm Resolution : 0.0001 g/qcm Balance weighing range : max. 320 g : 0.001 g Weighing plate : 135 x 135 mm, stainless steelInterface : RS232Dimensions / Weight : 35 x 37 x 60 cm (W x D x H), 20 kgPower supply : 110/230 V, 50/60 Hz, EU-plugPower supply : 115 V, 60 Hz, US-plug


25-028225-0283


Spare Parts25-0417 Thermometer for density-applications

(Range: +10 to +30 : 0.1 °C)25-0418 Test Cylinder, 120 ml

25-0420 Bob, 10 ml

DensityDensity

65

19-0041 19-0032

19-0039

19-0080

19-0051 / 19-0052

19-0056 / 19-0057

19-0011

19-0005

Scope of ApplicationSolid MaterialsThe boring sampling procedure is applicable for waxes, solid bitumens and other soft solids in barrels, cases, bags, and cakes when they cannot be melted and sampled as liquids.

Semi-Solid MaterialsThe grease sampling procedure is applicable for lubricating greases, soft waxes or soft bitumens similar to grease in consistency from kettles, drums, cans, tubes.

Liquid MaterialsThe tube sampling procedure is applicable for sampling liquids of 13.8 kPa (2 psia) RVP or less and semi-liquids in drums, barrels, and cans.The bottle sampling procedure may be used for sampling liquids of 101 kPa (14.7 psia) RVP or less in tank cars and storage tanks.The core thief sampling procedure is applicable for emulsifi ed asphalts and other semi-liquids in tank cars and

Sampling Devices (manual)

Bituminous binders, Sealants & Fillers:ASTM D 140 EN 58 - DIN 52001 (DIN 1996-2)

Petroleum Products: ASTM D 4057 - (AASHTO T 79)

Solid Materials

19-005119-0052

Sampling Auger with handle ASTM D 4057 - DIN 51 750-3 (ASTM D 270, DIN 53 242-3)to take samples of non-liquid materials from any specifi ed level, brass construction... effective length 30.5 cm... effective length 50.0 cm

Semi-Solid Materials

19-005619-0057

Grease Sampling Tube with handleASTM D 4057 - EN 58 - DIN 51 750-3 (ASTM D 270)to take samples from any specifi ed level of hard greases and waxes, brass... effective length 500 mm... effective length 1000 mm

Liquid Materials19-0005 Open-End Sampling Tube

EN 58 - DIN 51 750-2 - ISO 3170 brass, 102 cm long To take individual samples from smaller containers such as barrels, drums etc.

19-0011 Closed-End Sampling TubeEN 58 - DIN 51 750-2alloy steel, 300 cm long To take samples from any specifi ed level of larger containers such as barrels, drums etc.

19-0041 Sampling Bottle with metal cage, 1 lASTM D 4057 - EN 58 - DIN 51 750-2 - ISO 3170 (ASTM D 270) Sample bottle: glass, neck 29/32, height 200 mm, outside Ø 111 mmTo take samples from any specifi ed container level, except the bottom.

19-0032 Tank Sampling Thief (BACON-bomb) ASTM D 4057 - ASTM D 923 - DIN 51 750-2 - ISO 3170 - JIS C 2101 - JIS K2254 (ASTM D 270, DIN 53 242-1) for mineral oils and mineral oil products, insulating oils, special gasolines and solvent naphthas, light gas oils, fuel oils etc. Brass construction, nickel plated with automatically opening bottom valve, outer Ø 80 mm. Capacity approx. 1 liter. Without lowering chain and pull cord.To take samples from the bottom or any specifi ed container level.

19-0039 Valve Pull Cord, Perlon, 100 m

19-0080 Hand-Wheel with 30 m steel wire (Ø 1 mm) and snaphook Note! Only for non fl ammable samples, because the steel-rope may cause sparks.

SamplingSampling

66

Viscosity & Density

MTVM

MTVM - Calibration Fluid (Multi- and Single-Test Verifi cation Material)

50-9026 MTVM - Reference Liquid (Bitumen) with certifi cate (ISO 9001), 500 ml

Test Name Method Range Units Amount / Test

Softening Point IP 58 +36.8 to +44 °C 7.5 ml

Needle Penetration IP 49 +184 to +200 °C 130 ml

Viscosity & Density Oil StandardsSuitable for calibration of master viscometers and viscosity oil standards as described in ASTM D 445 & D 446.Certifi ed by UKAS under ISO 17 025 at all stated temperatures.The values listed in the following table are to be considered as nominal and approximate only (depending on the batch). The actual and exact data will be printed on the container-lable or on a separate certifi cate.Content: 470 ml / 1 pint Shelf life: 2 years

UKAScertifi ed Type

Kinematic Viscosity ν [mm²/s = cSt] Dynamic Viscosity η [mPa•s = cP]

Density [g/ml]

Saybolt Viscosity

SUS SUS SFS

approx. 20°C68°F

25°C77°F

37.8°C100°F

40°C104°F

50°C122°F

60°C140°F

80°C176°F

99°C210°F

100°C212°F 100°F 210°F 122°F

24-0601 N 0.4mm²/smPa•sg/ml

0.470.31

0.6669

0.450.30

0.6624

0.410.27

0.6491


0.730.54

0.7303

0.700.5

0.7261

0.610.44

0.7154

0.600.43

0.7136


1.31.0

0.7827

1.20.93

0.7789

1.00.78

0.7691

0.990.76

0.7674

0.880.67

0.7596

24-0603 S 3mm²/smPa•sg/ml

4.63.3

0.8148

4.13.3

0.8113

3.12.5

0.8025

2.92.3

0.8010

2.41.9

0.7941

1.51.2

0.7735

1.20.92

0.7603

1.20.91

0.7596


108.5

0.8263

8.77.2

0.8229

64.9

0.8144

5.74.6

0.8129

4.53.6

0.8063

2.52.0

0.7864

1.91.5

0.7738

1.91.4

0.7729

24-0605 N 10mm²/smPa•sg/ml

2117

0.8367

1714

0.8333

118.8

0.8250

108.2

0.8235

7.56.1

0.8169

3.83.0

0.7977

2.72.1

0.7852

2.72.1

0.7843


4236

0.8438

3328

0.8407

2016

0.8325

1815

0.8310

1311

0.8246

5.84.7

0.8059

4.03.2

0.7937

3.93.1

0.7930

96


7968

0.8582

6051

0.8551

3328

0.8469

3025

0.8456

2017

0.8392

8.36.8

0.8204

5.44.4

0.8085

5.34.3

0.8078

160


160140

0.8598

120100

0.8567

6051

0.8487

5446

0.8473

3529

0.8412

1311

0.8228

7.96.4

0.8111

7.76.3

0.8105

280


390340

0.8667

280240

0.8636

130110

0.8557

12099

0.8544

7160

0.8483

4639

0.8423

2218

0.8303

1311

0.8189

1310

0.8182

600


650570

0.8699

460400

0.8668

210180

0.8591

180160

0.8578

11092

0.8518

3226

0.8340

1815

0.8227

1814

0.8221

950 90


13001100

0.8744

860750

0.8715

370320

0.8639

320280

0.8627

180160

0.8565

5042

0.8389

2722

0.8277

2621

0.8271

130


22001900

0.8760

15001300

0.8730

600520

0.8654

520450

0.8641

290250

0.8582

7361

0.8410

3831

0.8300

3630

0.8293

180 140

24-0612 N 1 000mm²/smPa•sg/ml

44003900

0.8806

30002600

0.8777

1000860

0.8690

530460

0.8632

300260

0.8575

121103

0.8463

5847

0.8346

24-0613 S 2 000mm²/smPa•sg/ml

81007100

0.8833

53004700

0.8802

20001700

0.8728

17001500

0.8715

900780

0.8658

189160

0.8490

9075

0.8382

8672

0.8376

420

24-0614 N 4 000mm²/smPa•sg/ml

1800016000

0.8873

11000100000.8844

25003100

0.8761

18001500

0.8704

975843

0.8650

343293

0.8539

150120

0.8429

24-0615 S 8 000mm²/smPa•sg/ml

3500031000

0.8909

23000200000.8883

79007000

0.8811

67005900

0.8799

33002900

0.8583

591507

0.8583

240200

0.8583

24-0618 S 30 000mm²/smPa•sg/ml

81000730000.8954

28000240000.8886

23000210000.8873

110009700

0.8820

17441510

0.8660

660560

0.8554

Reference MaterialReference Material

67

25-0282

21-0695

Miscellaneous Equipment

21-0695 8-Channel Stop WatchContaining 8 individual stop watches.Each operated by a single button to run, stop or reset.Auto-power-off when no stop watches are running.After power-off individual values are kept in memory.All values can be reset together or per channel.9 V-Battery-block included. Expected life time approx. 6 months.The stop watch can be supplied with a calibration certifi cate.Dimensions (L x W x H): 195 x 112 x 46 mm

21-069721-0698

Digital Stop Watch7-digit LC display, max. 10 hours countdown with 1/100 sec. precisionquartz-controlled, water resistant, memory function, calendarNote: Lithium battery operated (battery lifetime 1 year)... precision made... certifi ed

25-028225-0283

Serial Impact Printer for single sheet & continuous paper to record data like test results, duration of test, etc. Supplied with: 1 data-cable, 1 ink ribbon (black)Technical Data: Line spacing : 80 characters per line (10 cpi)Page size (W x H) : 257 x 364 mm (sheet), 254 x 558.8 mm (roll)Ports : serial, USB (1.1) & parallelDimensions : 37 x 28 x 16 cm (WxDxH), weight 4.4 kgPower supply : 220/240 V, 50/60 HzPower supply : 110/130 V, 50/60 Hz

25-0274 Printer Data-Cable, serial (2 m), for manual & semi-automatc units

25-0304 Printer Data-Cable, serial (2 m), for automatic Petrotest® units

25-0284 Ink Ribbon, black

General EquipmentGeneral Equipment

68

10-0380

17-0710

20-0154

18-0403

Tempering EquipmentCirculator (for external & internal cooling & heating) programmable (with accessories)Consisting of:Cooler with stainless steel bath. Thermostat with digital display, splash-proof keypad, heater, pump, RS232/RS485-interface, Pt-100-socket, programmer, over/under-temperature & low-level protection, adjustable pump-pressure, proportional cooling control.Supplied with: 1 bath cover, 1 drain tap, 1 junction line for temperature probeNote: Insulated hose matter is not included but recommended.Technical Data: Working range : -40 to +200°CDisplay / Resolution : VFD & LCD / 0.01°CControl : ICC / ProgrammerHeater capacity (115 V) : 2000 W (1000 W)Cooling capacity : 680 W at +20 °CPump-Pressure : 22-26 l/min, 700 mbarPump-Suction : 22-26 l/min, 400 mbar

Bath opening (WxDxH) : 23 x 14 x 20 cm Safety class : 3Bath fl uid (possible) : FL (Flammable Liquids)Volume : 16 lInterface (capability) : RS232 (LIMS) / RS485Sockets for : hose (Ø 8 / 12 mm), Pt-100, solenoid valve

10-038010-0381

Dimensions / Weight : 37 x 46 x 71 cm (W x D x H), 49 kgPower supply : 230 V, 50 Hz, EU-plugPower Supply : 230 V, 60 Hz

Circulator (external & internal heating & cooling) programmable & regulated by Main-UnitConsisting of: Cooler with stainless steel bath. Thermostat with digital display, splash-proof keypad, heater, pump, RS232-interface, Pt-100-socket, programmer, over/under-temperature & low-level protection, adjustable pump-pressure, cooling control.Supplied with: 1 bath cover, 1 drain tap, 1 insulated hose-set (Ø 8 mm, 2x 2m)Technical Data: Working range : -35 to +200°CDisplay / Resolution : VFD / 0.01°CControl : ICC / ProgrammerHeater capacity (115 V) : 2000 W (1000 W)Cooling capacity : 450 W at +20 °CPump-Pressure : 22-26 l/min, 700 mbarPump-Suction : 22-26 l/min, 400 mbar

Bath opening (WxDxH) : 18 x 12 x 15 cm Safety class : 3Bath fl uid (possible) : FL (Flammable Liquids)Volume : 8 lInterface (capability) : RS232 (LIMS)Sockets for : hose (Ø 8 / 12 mm), Pt-100, solenoid valve

17-071017-0711

Dimensions / Weight : 31 x 42 x 66 cm (W x D x H), 38 kgPower supply : 230 V, 50 Hz, EU-plugPower supply : 115 V, 60 Hz, US-plug

Circulator-Bath (for external & internal heating) with cooling-coil & intermediate bottomConsisting of: Stainless steel bath with adjustable intermediate bottom and cooling-coil.Thermostat with digital display, splash-proof keypad, heater, pump, RS232-interface, over-temperature- & low-level-protection.Supplied with: 1 bath cover Ø 5 cm, 1 bath cover 20 x 20 cm, 1 thermometer (-2 to +105:0.5°C)Note: Requires counter-cooling for applications near ambient temperature.

Hose matter is not included.Technical Data: Working range : +20 to +150°CDisplay / Resolution : LED / 0.01°CControl : PIDHeater capacity (115 V) : 2000 W (1000 W)Cooling capacity : --Pump-Pressure : 15 l/min, 320 mbarPump-Suction : --

Bath opening (WxDxH) : 20 x 20 x 25 cmSafety class : 3Bath fl uid (possible) : FL (Flammable Liquids)Volume : 20 lInterface (capability) : RS232 (LIMS)Sockets for : hose (Ø 8 mm)

18-040318-0402


Circulator (external & internal heating & cooling)Consisting of:Cooler with stainless steel bath. Thermostat with digital display, splash-proof keypad, heater, pump, over-temperature & low-level protection.Supplied with: 1 bath coverNote: Insulated hose-set (25-0228) is recommended.Technical Data: Working range : -10 to +100°CDisplay / Resolution : LED / 0.1 °CControl : PIDHeater capacity : 1000 W Cooling capacity : 240 W at +20 °CPump-Pressure : 7 l/min, 300 mbarPump-Suction : --

Bath opening (WxDxH) : 15 x 10 x 15 cm Safety class : 1Bath fl uid (possible) : NFL (Non Flammable Liquids)Volume : 5.5 lInterface (capability) : --Sockets for : hose (Ø 8 / 12 mm), Pt-100

20-015420-0155

Dimensions / Weight : 22 x 36 x 47 cm (W x D x H), 18 kgPower supply : 230 V, 50 Hz, 1050 W, EU-plugPower supply : 115 V, 60 Hz


VFD = Vacuum Flourescence DisplayLCD = Liquid Crystal Display

6925-0228

25-0393

25-0368

25-0386

25-0382

Circulation Cooler (tap water replacement, external cooling) with insulated hoseFor cooling or counter-cooling of instruments with no circulation pump (e.g. Peltier-cooling).Consisting of:Cooler with tank, digital display, splash-proof keypad, integrated pump, liquid level indication, over-/low-temperature & low-level protection.Supplied with: 1 insulated hose-set (Ø 8 mm, 2x 2 m, incl. fi ttings)Technical Data: Working range : -20 to +40 °CDisplay / Resolution : LED / 0.1°CControl : --Heater capacity (115 V) : -- (--)Cooling capacity : 500 W at +20 °CPump-Pressure : 10 l/min, 500 mbarPump-Suction : --

Bath opening (WxDxH) : -- Safety class : 1Bath fl uid (possible) : NFL (Non Flammable Liquids)Volume : 7 lInterface (capability) : -- Sockets for : hose (Ø 8 / 12 mm)

25-036825-0373

Dimensions / Weight : 35 x 45 x 57 cm (WxDxH), 38 kgPower supply : 230 V, 50 Hz, 450 W, EU-plugPower supply : 115 V, 60 Hz

Circulation Cooler (for external cooling)Consisting of: Cooler with tank, digital display, pump and liquid level indication.Supplied with: 1 insulated hose-set (Ø 8 mm, 2x 2m)Technical Data: Working range : -20 to +40 °CDisplay / Resolution : digital / 0.1°CControl : digitalHeater capacity (115 V) : -- (--)Cooling capacity : 300 W at +15°CPump-Pressure : 12 l/min, 200 mbarPump-Suction : 12 l/min, 100 mbar

Bath opening (WxDxH) : -- Safety class : 1Bath fl uid (possible) : NFL (Non Flammable Liquids)Volume : 1.4 lInterface (capability) : -- Sockets for : hose (Ø 8 / 12 mm), Pt-100

25-038225-0383

Dimensions / Weight : 23 x 36 x 38 cm (W x D x H), 23 kgPower supply : 230 V, 50/60 Hz, 3.5 A, EU-plugPower supply : 115 V, 60 Hz

Circulator-Bath (internal & external heating & cooling) with intermediate bottom Consisting of: Stainless steel bath with intermediate bottom. Thermostat with digital display, splash-proof keypad, heater, cooler, pump, over-temperature protection, pump-pressure control.

Supplied with: 2 bath covers, 1 pump-set for external tasks

Note: Insulated hose-set (25-0228) is recommendedTechnical Data: Working range : -10 to +100°CDisplay / Resolution : LED / 0.1 & 0.01°CControl : PIDHeater capacity (115 V) : 2000 W (1200 W)Cooling capacity : 250 W at +20°CPump-Pressure : 17 l/min, 300 mbarPump-Suction : --

Bath opening : 30 x 35 x 20 cm (WxDxH)

Safety class : 1Bath fl uid : NFL (water / water-antifreezemix)Volume : 19-26 lInterface : --Sockets for : hose (Ø 8 / 12 mm)

25-038825-0389

Dimensions / Weight : 36 x 75 x 40 cm (W x D x H), 31 kgPower supply : 230 V, 50/60 Hz, 2500 W, EU-plugPower supply : 115 V, 60 Hz, 1700 W

Circulator (external & internal heating & cooling) regulated by Main-UnitConsisting of:Cooler with stainless steel bath. Thermostat with digital display, splash-proof keypad, heater, pump, RS232-interface, over-temperature & low-level protection, pump-pressure control.Supplied with: 1 bath coverNote: Insulated hose-set (25-0228) is recommendedTechnical Data: Working range : +28 to +150°CDisplay / Resolution : LED / 0.1 & 0.01 °CControl : PIDHeater capacity (115 V) : 2000 W (1200 W)Cooling capacity : 320 W at +20 °CPump-Pressure : 12.5 l/min, 300 mbarPump-Suction : --

Bath opening (WxDxH) : 13 x 10 x 15 cm Safety class : 3Bath fl uid (possible) : FL (Flammable Liquids)Volume : 4.5 lInterface (capability) : --Sockets for : hose (Ø 8 mm)

25-039325-0394

Dimensions / Weight : 23 x 46 x 58 cm (W x D x H), 30 kgPower supply : 230 V, 50/60 Hz, 2400 W, EU-plugPower supply : 115 V, 60 Hz, 1600 W, EU-plug




70

Tables of ContentsKeywords ....................... page 71Order Numbers ......... page 72-74Standards ...................... page 75

71

page

Aging ........................................................................................... 36 - 40Accelerated Aging ...................................................................... 40Effect of Heat and Air ..................................................... 36, 38, 39Resistance to Hardening ............................................... 36, 38, 39Loss-On-Heat - LOH ................................................................... 36Rolling Thin Film Oven Test - RTFOT ...................................... 38Rotating Flask Test - RFT .......................................................... 39Moving Thin Film Test - RFT ..................................................... 39Pressure Aging Vessel - PAV .................................................... 40Thin-Film-Oven Test - TFOT ...................................................... 36

API Gravity Hydrometer .................................................................... 62

Apparent Viscosity ...................................................................... 26, 27

Asphalt Binder Analyzer ................................................. 38, 40, 41, 43

Asphalt Institute Vacuum Viscometer - AIVV ................................ 33

ASTM Specifi c Gravity Hydrometer ................................................ 62

Balance .............................................................................................. 64

Bending Beam Rheometer - BBR .................................................... 24

Bitumen Number ................................................................................ 16

Breaking-Point ............................................................................. 20, 23

Brookfi eld Viscometer - RV .............................................................. 26

BS/IP Reverse Flow Viscometer - RFV ........................................... 32

Cannon-Fenske Opaque Viscometer - CFOV ............................... 31

Cannon-Manning Vacuum Viscometer - CMVV ............................. 33

Cleveland Flash- & Fire-Point .................................................... 41, 43

Creep Stiffness .................................................................................. 24

Cut-Back Bitumen Distillation .................................................. 56, 57

Dean & Stark Distillation ................................................................. 53

Density, Relative Density Displacement / Balance ............................................................. 64Hydrometer ................................................................................. 62Pycnometer ................................................................................. 61

Distillation Cut-Back Bitumen ................................................................ 56, 57Paraffi n Wax Content ................................................................. 52Pitch ............................................................................................. 60Road Tar Products ............................................................... 58, 59Water Content ............................................................................. 53

Ductility ......................................................................................... 10, 14

Dynamic Shear Rheometer - DSR ................................................... 25

Dynamic Viscosity ............................................................................. 33

Effect of Heat & Air ........................................................................... 36

Elastic Properties ........................................................................ 10, 18

Equilibrium Method ..................................................................... 48, 49

Fire-Point (open cup) ........................................................... 41, 43, 51

Flash-Point (closed cup) Pensky-Martens - PMA 4 ........................................................... 44Pensky-Martens - PM 4 .............................................................. 47TAG - TAG 4 ........................................................................... 48, 49

Flash-Point (open cup) Cleveland (COC) - CLA 4 ........................................................... 41Cleveland (COC) - CL 1 .............................................................. 43TAG ............................................................................................... 51

Fraass-Method ............................................................................. 20, 23

Gay-Lussac Pycnometer ................................................................. 61

General Equipment ............................................................................ 67

Glass Capillary Viscosity Asphalt Institute Vacuum Viscometer - AIVV .......................... 33BS/IP Reverse Flow Viscometer - RFV .................................... 32Cannon-Manning Vacuum Viscometer - CMVV ...................... 33Cannon-Fenske Opaque Viscometer - CFOV ......................... 31U-Tube Reverse Flow Viscometer - RFV ................................. 32Zeitfuchs Cross-Arm Viscometer - ZCAV ................................ 32High Temperature Liquid Bath ................................................. 35

Gravity ................................................................................................. 62

Hubbard Pycnometer ....................................................................... 61

Hydrometer ......................................................................................... 62

Kinematic Viscosity ......................................................................... 31

Kraemer-Sarnow Softening-Point ..................................................... 9

page

Lipkin Pycnometer ........................................................................... 61

Loss-On-Heat - LOH .......................................................................... 36

Moving Thin Film - RFT .................................................................... 39

Paraffi n Wax Content ....................................................................... 52

Penetration ................................................................................... 16, 18

Penetrometer - PNR 10 ...................................................................... 16

Pensky-Martens Flash-Point ..................................................... 44, 47

Pitch Distillation ................................................................................. 60

Plastic Properties ........................................................................ 16, 18

Pressure Aging Vessel - PAV ........................................................... 40

Pycnometer ........................................................................................ 61

Reference Material ........................................................................... 66

Resistance to Hardening ...................................................... 36, 38, 39

Reverse Flow Viscometer - RFV ...................................................... 32

Rheometer Method Bending Beam - BBR ................................................................. 24Dynamic Shear - DSR ................................................................. 25Texture - PNR 21 ......................................................................... 18

Rheotex Texture Analyzer - PNR 21 ................................................ 18

Ring & Ball Softening-Point ........................................................... 4, 7

Road Tar Distillation .......................................................................... 58

Road Tar Viscometer ......................................................................... 27

Rolling Thin Film Oven Test - RTFOT .............................................. 38

Rotating Flask Test - RFT ................................................................. 39

Rotary Viscometer - RV .................................................................... 26

Sampling Devices Closed-End Sampling Tube ...................................................... 65Grease Sampling Tube with handle ......................................... 65Open-End Sampling Tube ......................................................... 65Sampling Bottle with metal cage ............................................. 65Tank Sampling Thief (BACON) ................................................. 65

SHARP Method Bending Beam Rheometer - BBR ............................................. 24Dynamic Shear Rheometer - DSR ............................................ 25Pressure Aging Vessel - PAV .................................................... 40Rotational Viscometer - RV ....................................................... 26

Softening-Point Kraemer-Sarnow .......................................................................... 9Ring & Ball - RKA 2 ...................................................................... 4Ring & Ball ..................................................................................... 7Wilhelmi ......................................................................................... 8

Stiffness .............................................................................................. 24

Superpave® ...................................................................... 38, 40, 41, 43

TAG Flash-Point .................................................................... 48, 49, 51

Tempering Devices ............................................................................ 68

Tensile Properties Ductilometer - DD 3 .................................................................... 14Force-Ductilometer - DDA 3 ...................................................... 10

Texture ......................................................................................... 18 - 19

Thin-Film-Oven Test - TFOT ............................................................. 36

U-Tube Viscometer - RFV ................................................................ 32

Vacuum Capillary Tubes .................................................................. 33

Viscoelastic Properties .................................................................... 25

Viscosity Apparent Viscosity ............................................................... 26, 27Brookfi eld Viscometer - RV ...................................................... 26Dynamic Shear Rheometer - DSR ............................................ 25Dynamic Viscosity ..................................................................... 33Engler Viscometer ...................................................................... 30Glass Capillary Viscometer ...................................................... 31Kinematic Viscosity .................................................................... 31Liquid Bath ................................................................................... 35Reference Material ...................................................................... 66Road Tar Viscometer ................................................................. 27Rotational Viscometer - RV ....................................................... 26Saybolt Viscometer ..................................................................... 28Specifi c Viscosity ........................................................................ 30Universal & Furol Method ........................................................... 28Vacuum Capillary Tubes ............................................................ 33Viscosity Liquid Bath ................................................................. 35

Water Content Distillation ............................................................... 53

Weight ................................................................................................. 64

Wilhelmi Softening-Point Method ..................................................... 8

Zeitfuchs Cross-Arm Viscometers - ZCAV .................................... 32

KeywordsKeywords

72

Order-NumberOrder-Numberss

10-0000 .......................................2310-0002 ........................................2310-0003 ........................................2310-0004 ........................................2310-0006 ..................................22, 2310-0007 ..................................22, 2310-0008 ........................................2310-0009 ........................................2310-0010 ........................................2310-0013 ..................................34, 5210-0016 ........................................2210-0017 ........................................2310-0048 ......................................6, 710-0049 ......................................6, 710-0051 ......................................6, 710-0052 ......................................6, 710-0055 ......................................6, 710-0056 ......................................6, 710-0057 ......................................8, 910-0061 .......................................7-910-0062 .......................................7-910-0063 .......................................7-910-0064 .......................................7-910-0065 .......................................7-910-0066 .......................................7-910-0067 .......................................7-910-0068 .......................................7-910-0070 ......................................6, 710-0071 ..........................................810-0075 ......................................6, 810-0076 ..........................................810-0077 ......................................6, 810-0079 ......................................6, 710-0081 ..........................................910-0082 ..........................................910-0084 ..........................................910-0086 ..........................................910-0087 ..........................................910-0089 ..........................................910-0090 ..................................23, 2410-0096 ..........................................910-0097 ..........................................910-0106 ......................................6, 810-0110 ........................................3910-0117 ........................................3610-0118 ........................................3610-0123 ........................................3710-0126 ...................................37-3910-0127 ...................................37-3910-0128 ........................................3710-0134 ........................................3710-0135 ........................................3710-0136 ........................................5210-0144 ........................................5210-0145 ........................................5210-0146 ..................................37, 4010-0149 ........................................3710-0150 ........................................3710-0152 ........................................5910-0153 ........................................5910-0154 ........................................5710-0154 ........................................5910-0155 ........................................5710-0155 ........................................5910-0156 ........................................5910-0157 ........................................5910-0158 ........................................5910-0159 ........................................5910-0160 ........................................5210-0161 ........................................5210-0166 .............................52, 57-6010-0167 ........................................5210-0168 ........................................5210-0169 ........................................5210-0170 ........................................5210-0171 ........................................5210-0173 ........................................5710-0175 ........................................5710-0176 ........................................57

10-0177 .......................................5710-0178 ..................................56, 5810-0179 ........................................6010-0181 ..........................................510-0182 ..........................................510-0203 ........................................5810-0204 ........................................5610-0205 ............................ 56, 58, 6010-0206 ..................................58, 6010-0207 ..................................58, 6010-0208 ...................... 56, 58, 59, 6010-0210 ........................................5610-0211 ........................................3710-0212 ........................................3710-0213 ........................................5610-0214 ........................................5610-0216 ........................................5610-0217 ........................................5610-0218 ........................................5610-0220 ..................................56, 5810-0222 ........................................3710-0233 ...................................22-2410-0234 ........................................5210-0235 ........................................5210-0236 ........................................5210-0239 ........................................5210-0242 ........................................3710-0243 ........................................3710-0244 ........................................3710-0245 ........................................3710-0264 ..........................................510-0265 ..........................................510-0281 ..........................................710-0284 ..........................................710-0285 ..........................................610-0289 ..........................................610-0294 ........................................2710-0295 ........................................2710-0298 ........................................5910-0312 ........................................2710-0313 ........................................2710-0317 ........................................2710-0318 ........................................2710-0319 ........................................2710-0320 ........................................2710-0321 ........................................2710-0322 ........................................2710-0323 ........................................2710-0324 ........................................2710-0329 ........................................2710-0332 ..................................13, 1510-0333 ..................................13, 1510-0334 ..................................13, 1510-0335 ..................................13, 1510-0336 ..................................13, 1510-0337 ........................................2710-0338 ........................................2710-0350 ........................................1410-0351 ........................................1410-0354 ........................................1410-0355 ........................................1410-0360 ........................................1210-0361 ........................................1210-0364 ........................................1210-0365 ........................................1210-0377 ............................ 13, 15, 3010-0379 ..................................13, 1510-0380 ............................ 12, 15, 6810-0381 ............................ 12, 15, 6810-0383 ............................ 13, 15, 6310-0384 ............................ 13, 15, 6310-0385 ..................................15, 6310-0386 ..................................15, 6310-0387 ........................................6310-0388 ........................................6310-0403 ..................................13, 1510-0404 ........................................1210-0406 ..................................13, 1510-0455 ..........................................7

10-0460 .......................................2110-0461 ........................................2110-0473 ........................................2210-0474 ........................................2210-0475 ........................................2210-0480 ..........................................610-0600 ........................................2610-0601 ........................................2610-0602 ........................................2610-0603 ........................................2610-0604 ........................................2610-0605 ........................................2610-0608 ........................................3810-0618 ........................................3810-0621 ........................................3810-0625 ........................................3910-0640 ........................................3810-0700 ........................................2410-0701 ........................................2410-0706 ........................................2410-0720 ........................................4010-0721 ........................................4010-0724 ........................................4010-0725 ........................................4010-0726 ........................................4010-0727 ........................................4010-0770 ........................................2510-0771 ........................................2510-0772 ........................................2510-0800 ..........................................310-0801 ..........................................310-1117 ........................................3610-1178 ........................................5710-1181 ..........................................510-1296 ........................................5710-1297 ............................ 57, 59, 6010-1298 ........................................5710-1600 ........................................2610-1601 ........................................2610-1602 ........................................26

11-0018 ................................6-9, 5511-0019 .................................6-9, 5511-0022 ........................................6311-0029 .................................. 6, 7, 911-0030 ..................................52, 6311-0087 ........................................1711-0088 ........................................1711-0110 .............................52, 56-5811-0119 ........................................6011-0130 ............................ 27, 55, 5611-0137 ..........................................911-0138 ................................ 7, 8, 5511-0139 ....................................6, 5511-0140 ....................................6, 5511-0155 ...................... 27, 56, 58, 6011-0156 ...................... 27, 56, 58, 6011-0157 ........................................6011-0158 ........................................6011-0181 ...................... 13, 15, 19, 6911-0395 ........................................3011-0503 ........................................5611-0599 .............................. 5, 13, 22

12-0109 .......................................5112-0282 ........................................4212-0283 ........................................4212-0378 ..........................................612-0509 ........................................5012-0514 ........................................5012-0518 ........................................4912-0540 ........................................48

12-0541 .......................................4812-0542 ........................................4912-0543 ........................................4912-0548 ........................................5012-0549 ........................................5012-0550 ........................................5012-0553 ........................................5012-0559 ........................................4912-0560 ........................................5012-0572 ........................................4912-0577 ........................................5012-0600 ............................ 45, 47, 4912-0629 ..................................43, 5112-0657 ........................................4712-0658 ........................................4712-0659 ........................................4712-0660 ........................................4712-0661 ........................................4712-0662 ........................................4712-0663 ........................................4712-0664 ........................................4712-0665 ........................................4712-0666 ........................................4712-0667 ........................................4712-0668 ........................................4712-0683 ........................................5112-0684 ........................................5112-0689 ........................................5112-0690 ........................................5112-0710 ........................................4312-0730 ........................................4312-0731 ........................................4312-0751 ........................................4312-0752 ........................................4312-0753 ........................................4312-0754 ........................................4312-0758 ........................................4312-0768 ........................................4312-0774 ........................................4512-0777 ..................................46, 4712-0778 ...................... 42, 46, 47, 5012-0779 ..................................46, 4712-0780 ........................................4612-0781 ............................ 46, 47, 5012-0782 ........................................4512-0784 ........................................4612-0785 ..................................46, 4712-0786 ..................................46, 4712-0787 ........................................4612-0788 ........................................4612-0790 ............................ 46, 47, 5012-0791 ............................ 46, 47, 5012-0793 ..................................45, 4712-0795 ........................................4512-0940 ........................................4112-0941 ........................................4112-0949 ........................................4212-0950 ..................................42, 4312-0951 ........................................4212-0952 ........................................4212-0953 ........................................4212-0954 ........................................4212-0955 ........................................4212-0956 ........................................4212-0958 ........................................4212-0960 ........................................4212-0962 ..................................42, 4312-0970 ........................................4312-1030 ............................ 43, 47, 5112-1250 ........................................5112-1507 ..................................46, 4712-1508 ............................ 45, 47, 4912-1509 ..................................45, 4912-1514 ........................................5012-1515 ........................................5012-1516 ........................................5012-1518 ........................................5012-1540 ........................................5112-1542 ........................................51

73

12-1650 .......................................4712-1651 ........................................4712-1669 ........................................4712-1750 ........................................4712-1751 ........................................4712-1752 ........................................4712-1753 ........................................4712-1754 ........................................4712-1762 ..................................45, 4912-1763 ................ 22, 42, 45, 47, 4912-1767 ........................................4412-1770 ........................................4412-1777 ........................................4612-1785 ........................................4612-1786 ........................................4612-1787 ........................................4612-1790 ........................................4612-1791 ........................................4612-1792 ........................................4612-1795 ........................................45

13-0147 .........................................913-0161 ........................................5113-0162 ........................................5113-0565 ........................................6313-0715 ........................................6313-0716 ........................................6313-0717 ........................................6313-0718 ........................................6313-0923 ........................................52

16-0264 .......................................5216-0313 ........................................5216-0675 ........................................5516-0700 ........................................3816-0705 ........................................5516-0742 ........................................5516-0773 ........................................3916-0820 ........................................5516-0824 ........................................5516-0825 ........................................5516-0829 ........................................5516-0830 ........................................5316-0844 ........................................5316-0845 ........................................5416-0850 ........................................5316-0859 ........................................5416-0860 ........................................5416-0861 ........................................5416-0862 ........................................5416-0863 ........................................5416-0864 ........................................5416-0865 ........................................5416-0866 ........................................5416-0867 ........................................5416-0868 ........................................5416-0869 ........................................5416-0870 ........................................5416-0871 ........................................5416-0872 ........................................5416-0873 ........................................5416-0874 ........................................5416-0875 ........................................5416-0876 ........................................5416-0877 ........................................5416-0878 ........................................5416-0879 ........................................5416-0880 ........................................5416-0881 ........................................5416-0882 ........................................5416-0883 ........................................5416-0884 ........................................5416-0886 ........................................54

16-0887 .......................................5416-0888 ........................................5416-0889 ........................................5416-0890 ........................................5416-0891 ........................................5416-0892 ........................................5416-0893 ........................................5516-0894 ........................................5516-0895 ........................................5516-0896 ........................................5516-0897 ........................................5416-0898 ..................................54, 5516-0899 ........................................5516-0901 ........................................5416-0902 ........................................5416-0925 ........................................5216-1430 ........................................5316-1444 ........................................5316-1445 ........................................5416-1450 ........................................5316-1452 ........................................5316-1454 ........................................5316-1455 ........................................5416-1458 ........................................5316-1839 ........................................5316-1844 ........................................5316-1845 ........................................5416-1850 ........................................53

17-0010 .......................................5217-0047 ..................................58, 6017-0584 ........................................5517-0710 ..................................52, 6817-0711 ..................................52, 6817-0802 ..................................52, 5517-0804 ..................................52, 55

18-0045 .......................................1918-0066 ........................................3718-0247 ........................................1918-0248 ........................................1918-0251 ........................................1918-0255 ........................................1918-0279 ........................................1918-0402 ................ 13, 15, 17, 19, 6818-0403 ................ 13, 15, 17, 19, 6818-0708 ........................................1718-1000 ........................................1618-1007 ........................................1718-1014 ........................................1618-1017 ........................................1718-1120 ..........................................318-1160 ........................................1718-1161 ........................................1718-1163 ........................................1718-1164 ........................................1718-1700 ........................................1818-1701 ........................................1818-1721 ........................................1918-1726 ........................................1918-1728 ........................................1918-1732 ........................................1918-2200 ........................................1718-2213 ........................................1718-2215 ........................................1718-2220 ........................................1718-2221 ........................................1718-2370 ........................................17

19-0005 .......................................6519-0011 ........................................6519-0032 ........................................6519-0039 ........................................6519-0041 ........................................6519-0051 ........................................6519-0052 ........................................6519-0056 ........................................6519-0057 ........................................6519-0080 ........................................65

20-0030 .......................................3420-0040 ........................................3420-0095 ........................................3420-0096 ........................................3420-0106 ........................................2320-0150 ........................................3520-0151 ........................................3520-0154 ..................................35, 6820-0155 ..................................35, 68

21-0030 .......................................3021-0113 ........................................3021-0114 ........................................3021-0115 ........................................3021-0116 ........................................3021-0117 ........................................3021-0118 ........................................3021-0158 ........................................3021-0361 ........................................2721-0362 ........................................2721-0367 ........................................2721-0368 ........................................2721-0375 ........................................2921-0501 ........................................2821-0502 ........................................2821-0601 ............................ 17, 29, 6321-0602 ........................................2921-0603 ........................................2921-0604 ........................................2921-0605 ........................................2921-0606 ..................................29, 6321-0607 ............................ 17, 29, 6321-0608 ........................................2921-0609 ........................................2921-0610 ........................................2921-0611 ........................................2921-0612 ..................................29, 6321-0621 ............................ 17, 29, 6321-0622 ........................................2921-0623 ........................................2921-0624 ........................................2921-0625 ........................................2921-0626 ..................................29, 6321-0627 ............................ 17, 29, 6321-0628 ........................................2921-0629 ........................................2921-0630 ........................................2921-0631 ........................................2921-0632 ..................................29, 6321-0641 ........................................2921-0642 ........................................2921-0643 ........................................2921-0644 ........................................2921-0645 ........................................2921-0646 ........................................2921-0647 ........................................2921-0648 ........................................2921-0649 ........................................2921-0650 ........................................2921-0693 ........................................2921-0695 ...................... 28, 30, 34, 6721-0697 .....15, 27, 28, 30, 34, 59, 67

21-0698 .................................30, 6721-0699 ........................................2921-0700 ........................................2921-0701 ........................................2921-0703 ........................................2821-0704 ........................................2921-0713 ........................................2821-0714 ........................................2821-6000 ........................................29

22-0050 .......................................3122-0051 ........................................3122-0052 ........................................3122-0053 ........................................3122-0054 ........................................3122-0055 ........................................3122-0056 ........................................3122-0057 ........................................3122-0058 ........................................3122-0059 ........................................3122-0060 ........................................3122-0061 ........................................3122-0070 ........................................3122-0093 ..................................31, 3422-0097 ........................................3122-0157 ........................................3522-0158 ........................................3522-0159 ........................................3522-0160 ........................................3522-0161 ........................................3522-0162 ........................................3522-0163 ........................................3522-0164 ..................................31, 3522-0200 ........................................3222-0201 ........................................3222-0202 ........................................3222-0203 ........................................3222-0204 ........................................3222-0205 ........................................3222-0206 ........................................3222-0207 ........................................3222-0208 ........................................3222-0209 ........................................3222-0210 ........................................3222-0220 ........................................3222-0270 ..................................32, 3422-0278 ........................................3222-0450 ........................................3422-0500 ........................................3322-0501 ........................................3322-0502 ........................................3322-0503 ........................................3322-0504 ........................................3322-0505 ........................................3322-0506 ........................................3322-0507 ........................................3322-0508 ........................................3322-0509 ........................................3322-0510 ........................................3322-0515 ........................................3322-0516 ........................................3322-0520 ........................................3322-0521 ........................................3322-0522 ........................................3322-0523 ........................................3322-0524 ........................................3322-0525 ........................................3322-0528 ...................................31-3422-0529 ........................................3322-0530 ........................................3222-0531 ........................................3222-0532 ........................................3222-0533 ........................................3222-0534 ........................................3222-0535 ........................................3222-0536 ........................................32


74


22-0537 .......................................3222-0538 ........................................3222-0539 ........................................3222-0540 ........................................3222-2050 ........................................3122-2051 ........................................3122-2052 ........................................3122-2053 ........................................3122-2054 ........................................3122-2055 ........................................3122-2056 ........................................3122-2057 ........................................3122-2058 ........................................3122-2059 ........................................3122-2060 ........................................3122-2061 ........................................3122-2065 ........................................3122-2200 ........................................3222-2201 ........................................3222-2202 ........................................3222-2203 ........................................3222-2204 ........................................3222-2205 ........................................3222-2206 ........................................3222-2207 ........................................3222-2208 ........................................3222-2209 ........................................3222-2210 ........................................32

23-0204 .................................31, 34

24-0601 .......................................6624-0602 ........................................6624-0603 ........................................6624-0604 ........................................6624-0605 ........................................6624-0606 ........................................6624-0607 ..................................29, 6624-0608 ..................................29, 6624-0609 ............................ 29, 34, 6624-0610 ..................................29, 6624-0611 ............................ 29, 34, 6624-0612 ........................................6624-0613 ............................ 29, 34, 6624-0614 ........................................66

24-0615 .................................34, 6624-0616 ............................ 29, 34, 6624-0617 ........................................6624-0618 ..................................34, 66

25-0001 .................................27, 5525-0004 .................................6-9, 5525-0009 ............................ 6, 7, 9, 5525-0042 ..........................................725-0043 ..........................................725-0108 ..................................27, 5525-0228 .......... 12, 15, 19, 22, 49, 6925-0262 ........................................2225-0274 ........................................6725-0282 .......5, 17, 22, 45, 49, 64, 6725-0283 .......5, 17, 22, 45, 49, 64, 6725-0284 ........................................6725-0304 ..................................22, 6725-0338 ........................................1725-0368 ..................................63, 6925-0373 ..................................63, 6925-0382 ..................................49, 6925-0383 ..................................49, 6925-0388 ............................ 17, 19, 6925-0389 ............................ 17, 19, 6925-0393 ..................................24, 6925-0394 ..................................24, 6925-0417 ........................................6425-0418 ........................................6425-0420 ........................................6425-0470 ........................................5225-0471 ........................................5225-0485 ........................................3425-0486 ............................ 34, 38, 3925-0490 ..................................38, 3925-0607 ........................................2925-0608 ........................................2925-0700 ........................................5525-0701 ........................................5525-0702 ........................................5525-0703 ........................................5525-0704 ........................................5525-0705 ........................................5525-0706 ........................................5525-0707 ........................................5525-0708 ........................................5525-0804 ........................................4525-0970 ........................................42

26-0004 .......................................6326-0010 ........................................6226-0011 ........................................6226-0014 ..................................55, 6326-0017 ........................................6326-0018 ........................................6326-0019 ........................................6426-0020 ........................................6426-0026 ........................................6326-0036 ........................................6326-0037 ........................................6326-0038 ........................................6326-0039 ........................................6326-0500 ........................................6226-0501 ........................................6226-0502 ........................................6226-0503 ........................................6226-0603 ........................................6226-0604 ........................................6226-0605 ........................................6226-0606 ........................................6226-0607 ........................................6226-0608 ........................................6226-0712 ........................................6126-0721 ........................................6126-0740 ........................................6126-0741 ........................................6126-0790 ........................................6126-0791 ........................................6126-0792 ........................................6126-0793 ........................................6126-0794 ........................................61

50-0001 .................................30, 4050-5172 ........................................3950-5229 ..........................................650-5242 ........................................6050-5315 ...................................5, 7-950-7027 ........................................5450-7030 ........................................5450-7047 ........................................5450-7050 ........................................5450-9024 ..................................46, 5050-9026 ........................................6650-9110 ..................................46, 5050-9111 ...................... 42, 43, 46, 5050-9112 ..................................46, 5050-9113 ..................................46, 5050-9114 ............................ 46, 50, 5150-9161 ........................................3550-9162 ........................................3550-9167 ...................................5, 7-9

90-0100 .......................................3590-0101 ........................................3590-0102 ........................................3590-0103 ........................................3090-0125 ........................................3590-0136 ........................................3590-0137 ........................................3590-0141 ........................................5190-0149 ........................................3590-0173 ........................................3590-0196 ........................................3590-0204 ........................................3590-0212 ........................................3590-0214 ........................................3590-0217 ........................................3590-0240 ........................................3590-0241 ........................................3590-0250 ........................................3590-0251 ........................................3590-0252 ........................................3590-0253 ........................................3590-0254 ........................................3590-0281 ........................................3590-0284 ........................................3590-0285 ........................................3590-0311 ........................................3590-0315 ........................................3590-1101 ........................................3590-1103 ........................................3090-1141 ........................................5190-1149 ........................................3590-1196 ........................................3590-1204 ........................................3590-1212 ........................................3590-1214 ........................................3590-1215 ........................................3590-1217 ........................................3590-1240 ........................................3590-1241 ........................................3590-1281 ........................................3590-1284 ........................................3590-1285 ........................................3590-1311 ........................................3590-1315 ........................................35

99-0143 .......................................1999-0144 ........................................19

75

International StandarInternational Standardsds

AASHTO AASHTO MP 1 ................................................ 40

AASHTO PP 1 ................................................. 40

AASHTO R 28 ................................................. 40

AASHTO T 47 ................................................. 36AASHTO T 48 ........................................... 41, 43AASHTO T 51 ........................................... 10, 14AASHTO T 53 ............................................... 4, 7AASHTO T 55 ................................................. 53AASHTO T 59 ................................................. 53AASHTO T 72 ................................................. 28AASHTO T 73-B ....................................... 44, 47AASHTO T 79 ..................................... 51, 56, 65AASHTO T 172-B ....................................... 44, 47AASHTO T 240 ................................................. 38AASHTO T 300 ................................................. 10AASHTO T 301 ........................................... 10, 14

AASHTO TP 1 ................................................ 24AASHTO TP 5 ................................................ 25AASHTO TP 48 ................................................ 26

ASTM ASTM D 5 ................................................... 16ASTM D 6 ................................................... 36ASTM D 20 ................................................... 58ASTM D 36 ................................................. 4, 7ASTM D 56 ................................................... 48ASTM D 70 ................................................... 61ASTM D 71 ................................................... 64ASTM D 88 ................................................... 28ASTM D 92 ............................................. 41, 43ASTM D 93-B ......................................... 44, 47ASTM D 95 ................................................... 53ASTM D 113 ............................................. 10, 14ASTM D 140 ................................................... 65ASTM D 244 ................................................... 53ASTM D 246 (obs.) ........................................ 58ASTM D 402 ................................................... 56ASTM D 445 ................................................... 31ASTM D 446 ................................................... 31ASTM D 1481 ................................................... 61ASTM D 1665 ................................................... 30ASTM D 1754 ................................................... 36ASTM D 2171 ................................................... 33ASTM D 2569 ................................................... 60ASTM D 2872 ................................................... 38ASTM D 3142 ................................................... 62ASTM D 3143 ................................................... 51ASTM D 3934 ................................................... 48ASTM D 3941 ................................................... 48ASTM D 4057 ................................................... 65ASTM D 4402 ................................................... 26ASTM D 5329 ................................................... 16ASTM D 5892 ............................................. 10, 14ASTM D 6084 ............................................. 10, 14ASTM D 6521 ................................................... 40ASTM D 6648 ................................................... 24ASTM E 102 ..................................................... 28

ASTM P 226 (obs.) .................................... 10, 14ASTM P 245 ..................................................... 24ASTM P 246 ..................................................... 25ASTM PS 36 (obs.) .......................................... 40

BS BS 434 (obs.) ................................................. 53BS 4385 (obs.) ................................................. 53BS 4453 (obs.) ................................................. 56BS 4689 (obs.) ........................................... 41, 43BS 4699 (obs.) ................................................. 61

(obs.) = obsolete

DIN DIN 1995 (obs.) ....................................... 53, 61DIN 1996-2 (obs.) ............................................ 65DIN 1996-5 ....................................................... 53DIN 1996-15 ................................................... 4, 8

DIN 51 366 (obs.) ............................................. 31DIN 51 372 (obs.) ............................................. 31DIN 51 376 (obs.) ....................................... 41, 43DIN 51 550 (obs.) ............................................. 31DIN 51 560 (obs.) ............................................. 30DIN 51 582 (obs.) ............................................. 53DIN 51 757-2 .................................................... 64

DIN 52 001 ....................................................... 65DIN 52 004 ....................................................... 61DIN 52 010 (obs.) ............................................. 16DIN 52 011 (obs.) ........................................... 4, 7DIN 52 012 (obs.) ....................................... 20, 23DIN 52 013 (obs.) ....................................... 10, 14DIN 52 015 (obs.) ............................................. 52DIN 52 016 (obs.) ............................................. 39DIN 52 023 (obs.) ............................................. 27DIN 52 024 ....................................................... 57DIN 52 025 ......................................................... 9DIN 52 027 ....................................................... 59DIN 52 048 (obs.) ............................................. 53

DIN 55 680 (obs.) ............................................. 48

DIN V 52 021-1 (obs.) ................................ 10, 14

DIS DIS 3658 (obs.) ................................................ 61

EN EN 58 ......................................................... 65EN 456 (obs.) .............................................. 48EN 1426 ......................................................... 16EN 1427 ....................................................... 4, 7EN 1428 ......................................................... 53EN 1871-F ................................................... 4, 8EN 12 591 ......................................................... 25EN 12 593 ................................................... 20, 23EN 12 596 ......................................................... 33EN 12 606-1 ..................................................... 52EN 12 607-1 ..................................................... 38EN 12 607-2 ..................................................... 36EN 12 607-3 ..................................................... 39EN 12 846 ......................................................... 27EN 13 179-1 ................................................... 4, 7EN 13 179-2 ..................................................... 16EN 13 302 ......................................................... 26EN 13 303 ......................................................... 36EN 13 357 ......................................................... 27EN 13 358 ......................................................... 56EN 13 398 ................................................... 10, 14EN 13 589 ......................................................... 10EN 13 703 ......................................................... 10EN 13 880-2 ..................................................... 16EN 13 880-3 ..................................................... 16EN 14 769 ......................................................... 40EN 22 592 (obs.) ........................................ 41, 43

FTM FTM 141-4293 ............................................ 44, 47FTM 141A-4285 (obs.) ..................................... 28

FTM 791-1101 .................................................. 48FTM 791-1102 ............................................. 44,47FTM 791-1103 ............................................ 41, 43FTM 791-304 .................................................... 28FTM 791-305 (obs.) ......................................... 31

IP IP 27 ............................................................... 56IP 32 (obs.) .............................................. 10, 14IP 34-B ..................................................... 44, 47IP 36 ......................................................... 41, 43IP 45 (obs.) .................................................... 36IP 49 (obs.) .................................................... 16IP 58 ............................................................. 4, 7IP 59-A (obs.) ................................................. 64IP 59-B (obs.) ................................................. 64IP 71-1 ............................................................ 31IP 71-2 ............................................................ 31IP 72 (obs.) .................................................... 27IP 74 ............................................................... 53IP 80 ......................................................... 20, 23IP 189 ................................................................ 61IP 190 ................................................................ 61IP 212 ............................................................... 30IP 222 ............................................................... 33IP 291 ............................................................... 53IP 304-1 (obs.) . ................................................ 48IP 304-2 (obs.) ................................................. 48IP 459-1 ............................................................ 52IP 460-1 ............................................................ 38IP 460-2 ............................................................ 36IP 460-3 ............................................................ 39IP 491 ............................................................... 48IP 492 ............................................................... 48IP 502 ............................................................... 27IP 506 ............................................................... 36IP 515 ............................................................... 10IP 516 ......................................................... 10, 14IP 520 ............................................................... 10

ISO ISO 1516 .......................................................... 48ISO 1523 .......................................................... 48ISO 2592 .................................................... 41, 43ISO 2719-B ................................................. 44, 47ISO 3104 .......................................................... 31ISO 3105 .......................................................... 31ISO 3679 .......................................................... 48ISO 3680 .......................................................... 48ISO 3733 .......................................................... 53ISO 3838 .......................................................... 61

JIS JIS K 2207 ................... 4, 7, 10, 14, 28, 31, 36, 38JIS K 2208 ........................................................ 30JIS K 2249 ........................................................ 61JIS K 2265 ................................ 20, 23, 41, 43, 48JIS K 2275 ........................................................ 53JIS K 2283 ........................................................ 31

NF NF T 60-100 (obs.) ........................................... 31NF T 60-118 (obs.) ..................................... 41, 43NF T 65-001 (obs.) ........................................... 25NF T 66-003 (obs.) ........................................... 56NF T 66-006 (obs.) ..................................... 10, 14NF T 66-008 (obs.) ......................................... 4, 7NF T 66-011 (obs.) ........................................... 36NF T 66-026 (obs.) ..................................... 20, 23NF T 66-032 (obs.) ........................................... 38NF T 66-047 (obs.) ........................................... 36NF T 66-048 (obs.) ........................................... 39

SHRP SHRP 1001 ....................................................... 40SHRP 1002 ....................................................... 24SHRP 1006 ....................................................... 26SHRP 1007 ....................................................... 25SHRP B-002 ..................................................... 24SHRP B-003 ..................................................... 25

Superpave Superpave® ................................... 38, 40, 41, 43

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98-1400 07/02

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