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CHEM 213 Quantitative Analysis II Introduction to Instrumental Analysis
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CHEM 213 Quantitative Analysis IIIntroduction to Instrumental Analysis
CHEM 213 Quantitative Analysis IIIntroduction to Instrumental Analysis
Course Information Sheet
Lecture 10:00 – 10:50 am MWFRoom: CCIS L1-140
Dr. James Harynuk Chem [email protected]
Office Hours: Monday 1:00-2:30Wednesday 1:00-2:30or by appointment
Webpage: www.ualberta.ca/elearning
Labs
Dr. Greg Kiema Chem W2–[email protected]
Webpage:
http://www.chem.ualberta.ca/undergrad.html then “Courses” then “Chem 213”
Much of this info is/will be duplicated on the eClass site
CHEM 213 Quantitative Analysis IIIntroduction to Instrumental Analysis
Course Information Sheet
Grading
Mid-term (in class Wed, Feb 29) 25%
Final (Monday, April 23 9:00 AM) 37% location TBD
Laboratory 35%
Class/Laboratory Participation 3%
CHEM 213 Quantitative Analysis IIIntroduction to Instrumental Analysis
Course Information Sheet
For some Participation points
Help Dr. Harynuk and the TAs get to know you
Attach a photo of yourself to your Moodle profile so that we can see who you are when answering your questions
Please do this by January 20th
Analytical Chemistry seeks ever improved means of measuring the chemical composition of natural and artificial materials.
ACS .
Instrumental AnalysisUV spectroscopy Ion trap MSIR spectroscopy Time of flight MSRaman spectroscopy Electrospray MSFlame atomic absorbance MALDI-TOFMSElectrothermal AAS PotentiometryFlame atomic emission CoulometryICP-optical emission VoltammetryICP-Mass Spec AmperometryX-ray fluorescence Surface probe microscopyFluorescence spectroscopy Gas chromatographyMagnetic sector MS HPLCDouble focusing MS Ion chromatographyQuadrupole MS Capillary Electrophoresis
If you happened to have already taken 313…
Why are you here???
You MAY NOT take this course for credit if you already have credit for CHEM 313.
Labs
Start Monday January 16
213 Lab Manual (2011-2012) (bookstore)Lab notebook – black ‘Physics notes’ bookSafety glassesLab coat
CHEM 213 Quantitative Analysis IIIntroduction to Instrumental Analysis
How to do well in the 213 Lab ?
Read procedures BEFORE entering lab
Will preview labs in class (Hot Tips)
Hot Tip sheets are posted on Moodle
Talk to your friends
Take care in sample preparation
Take care in calculations/data handling
CHEM 213 Quantitative Analysis IIIntroduction to Instrumental Analysis
Labs
Trace Iron by SpectrophotometryFluoride by Ion Selective ElectrodeBenzene by Gas ChromatographyNitroanilines Isomers by Liquid Chromatography Sucrose and Glucose by Autoanalysis of GlucoseQuinine in Tonic Water by FluorescenceCopper by Atomic Absorption SpectroscopyDextromethorphan in Cough Syrup by Solvent Extraction
Literature Search
Lab Notebook
CHEM 213 Quantitative Analysis IIIntroduction to Instrumental Analysis
Lockers 1 – 12 start with
Lockers 13 – 24 start with one of
Lectures
Preview of Lab Experiments (5 lectures) Ch. 4 Statistics (Sec. 4.7, 4.8) Ch. 5 Calibration Methods (Sec. 5.3, 5.4)
Spectroscopy (12 lectures) Ch. 18 Fundamentals of Spectrophotometry Ch. 20 Spectrophotometers, UV-VIS, FTIR Ch. 21 Atomic Spectroscopy
Midterm: (in class February 29) 25%
CHEM 213 Quantitative Analysis IIIntroduction to Instrumental Analysis
MidtermBased on: lectures
suggested problemsassigned readingsexperiments
Will include some:Multiple choice/matching, Definitions, descriptions, diagrams, calculations
~75% descriptive ~25% calculation
CHEM 213 Quantitative Analysis IIIntroduction to Instrumental Analysis
Lectures (post midterm)Separations
Ch. 23 Introduction to Analytical SeparationsCh. 24 Gas ChromatographyCh. 25 High Performance Liquid ChromatographyCh. 26 Other Chromatographic Methods
Mass SpectroscopyCh. 22 Mass spectrometry
Electrochemistry Ch. 15 Potentiometry and Ion-Selective Electrodes (ISEs)(Ch. 8 Activity)
Final (April 23, 9:00 AM, location TBD) 37%
CHEM 213 Quantitative Analysis IIIntroduction to Instrumental Analysis
Final
Semi-cumulative~1/3 on material before midterm~2/3 on material after midterm
Similar format to midtermprobably more choice and more calculations
CHEM 213 Quantitative Analysis IIIntroduction to Instrumental Analysis
• attend class• read text• do suggested problems• will post answers for these problems
• do additional problems • focus on descriptive
• ask questions•online forum in Lecture section of course website
How to do well in 213 exams ?
CHEM 213 Quantitative Analysis IIIntroduction to Instrumental Analysis
Course Information Sheet
www.uofaweb.ualberta.ca/tie/
You have a set of handouts about academic integrity, plagiarism, and ways to avoid plagiarism. It is understood that you will have read them and be familiar with the Code of Student Behaviour. This is your warning.
