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Technical Report Documentation Page 1. Report No. FHWA/TX-05/0-4468-2 2. Government Accession No. 3. Recipient's Catalog No. 5. Report Date December 2004 Resubmitted: August 2005 4. Title and Subtitle COMPARISON OF FATIGUE ANALYSIS APPROACHES FOR TWO HOT MIX ASPHALT CONCRETE (HMAC) MIXTURES 6. Performing Organization Code 7. Author(s) Lubinda F. Walubita, Amy Epps Martin, Sung Hoon Jung, Charles J. Glover, Eun Sug Park, Arif Chowdhury, and Robert L. Lytton 8. Performing Organization Report No. Report 0-4468-2 10. Work Unit No. (TRAIS) 9. Performing Organization Name and Address Texas Transportation Institute The Texas A&M University System College Station, Texas 77843-3135 11. Contract or Grant No. Project 0-4468 13. Type of Report and Period Covered Technical Report: September 2002-August 2004 12. Sponsoring Agency Name and Address Texas Department of Transportation Research and Technology Implementation Office P. O. Box 5080 Austin, Texas 78763-5080 14. Sponsoring Agency Code 15. Supplementary Notes Project performed in cooperation with the Texas Department of Transportation and the Federal Highway Administration. Project Title: Evaluate the Fatigue Resistance of Rut Resistance Mixes URL: http://tti.tamu.edu/documents/0-4468-2.pdf 16. Abstract Over the past decade, the Texas Department of Transportation (TxDOT) focused research efforts on improving mixture design to preclude rutting in the early life of the pavement. However, these rut resistant stiff mixtures may be susceptible to long-term fatigue cracking in the pavement structure as the binder stiffens due to oxidative aging. To address this concern, TxDOT initiated a research study with the primary goal of evaluating and recommending a HMAC mixture fatigue design and analysis system to ensure adequate mixture fatigue performance in a particular pavement structure under specific environmental and traffic loading conditions. A secondary goal of the research was to compare the fatigue resistance of commonly used TxDOT HMAC mixtures including investigating the effects of binder aging on fatigue performance. Four fatigue analysis approaches, the mechanistic empirical (ME), the calibrated mechanistic with (CMSE) and without (CM) surface energy measurements, and the proposed NCHRP 1-37A Pavement Design Guide were investigated in this project to evaluate the fatigue resistance of two common TxDOT mixtures (Rut Resistant and Basic Type C) including the effects of aging. Based on the value engineering assessment including test results, statistical analysis, costs, and relative comparison of each analysis procedure, the continuum micromechanics based CMSE fatigue analysis approach was recommended for predicting HMAC mixture fatigue life (N f ). While binder oxidative aging reduced the HMAC mixture resistance to fracture and its ability to heal, the Rut Resistant mixture exhibited better fatigue resistance in terms of N f magnitude compared to the Basic Type C mixture possibly due to an increased polymer modified binder content. Test results also indicated that both binders and mixtures stiffen with oxidative aging, and that mixture aging correlated quantitatively with binder aging. From the binder shear properties and binder-mixture relationships, aging shift factors were developed and produced promising results. Nonetheless, more CMSE laboratory HMAC mixture fatigue characterization and field validation is recommended. 17. Key Words Asphalt, Asphalt Concrete, Fatigue, Aging, Fracture, Microcracking, Healing, Mechanistic Empirical, Calibrated Mechanistic, Surface Energy, Anisotropy 18. Distribution Statement No restrictions. This document is available to the public through NTIS: National Technical Information Service Springfield, Virginia 22161 http://www.ntis.gov 19. Security Classif.(of this report) Unclassified 20. Security Classif.(of this page) Unclassified 21. No. of Pages 312 22. Price Form DOT F 1700.7 (8-72) Reproduction of completed page authorized
Transcript
Page 1: Comparison of Fatigue Analysis Approaches for Two Hot Mix ... · Based on the value engineering assessment including test results, statistical analysis, costs, and relative comparison

Technical Report Documentation Page 1. Report No. FHWA/TX-05/0-4468-2

2. Government Accession No.

3. Recipient's Catalog No. 5. Report Date December 2004 Resubmitted: August 2005

4. Title and Subtitle COMPARISON OF FATIGUE ANALYSIS APPROACHES FOR TWO HOT MIX ASPHALT CONCRETE (HMAC) MIXTURES

6. Performing Organization Code

7. Author(s) Lubinda F. Walubita, Amy Epps Martin, Sung Hoon Jung, Charles J. Glover, Eun Sug Park, Arif Chowdhury, and Robert L. Lytton

8. Performing Organization Report No. Report 0-4468-2

10. Work Unit No. (TRAIS)

9. Performing Organization Name and Address Texas Transportation Institute The Texas A&M University System College Station, Texas 77843-3135

11. Contract or Grant No. Project 0-4468 13. Type of Report and Period Covered Technical Report: September 2002-August 2004

12. Sponsoring Agency Name and Address Texas Department of Transportation Research and Technology Implementation Office P. O. Box 5080 Austin, Texas 78763-5080

14. Sponsoring Agency Code

15. Supplementary Notes Project performed in cooperation with the Texas Department of Transportation and the Federal Highway Administration. Project Title: Evaluate the Fatigue Resistance of Rut Resistance Mixes URL: http://tti.tamu.edu/documents/0-4468-2.pdf 16. Abstract Over the past decade, the Texas Department of Transportation (TxDOT) focused research efforts on improving mixture design to preclude rutting in the early life of the pavement. However, these rut resistant stiff mixtures may be susceptible to long-term fatigue cracking in the pavement structure as the binder stiffens due to oxidative aging. To address this concern, TxDOT initiated a research study with the primary goal of evaluating and recommending a HMAC mixture fatigue design and analysis system to ensure adequate mixture fatigue performance in a particular pavement structure under specific environmental and traffic loading conditions. A secondary goal of the research was to compare the fatigue resistance of commonly used TxDOT HMAC mixtures including investigating the effects of binder aging on fatigue performance. Four fatigue analysis approaches, the mechanistic empirical (ME), the calibrated mechanistic with (CMSE) and without (CM) surface energy measurements, and the proposed NCHRP 1-37A Pavement Design Guide were investigated in this project to evaluate the fatigue resistance of two common TxDOT mixtures (Rut Resistant and Basic Type C) including the effects of aging. Based on the value engineering assessment including test results, statistical analysis, costs, and relative comparison of each analysis procedure, the continuum micromechanics based CMSE fatigue analysis approach was recommended for predicting HMAC mixture fatigue life (Nf). While binder oxidative aging reduced the HMAC mixture resistance to fracture and its ability to heal, the Rut Resistant mixture exhibited better fatigue resistance in terms of Nf magnitude compared to the Basic Type C mixture possibly due to an increased polymer modified binder content. Test results also indicated that both binders and mixtures stiffen with oxidative aging, and that mixture aging correlated quantitatively with binder aging. From the binder shear properties and binder-mixture relationships, aging shift factors were developed and produced promising results. Nonetheless, more CMSE laboratory HMAC mixture fatigue characterization and field validation is recommended. 17. Key Words Asphalt, Asphalt Concrete, Fatigue, Aging, Fracture, Microcracking, Healing, Mechanistic Empirical, Calibrated Mechanistic, Surface Energy, Anisotropy

18. Distribution Statement No restrictions. This document is available to the public through NTIS: National Technical Information Service Springfield, Virginia 22161 http://www.ntis.gov

19. Security Classif.(of this report) Unclassified

20. Security Classif.(of this page) Unclassified

21. No. of Pages 312

22. Price

Form DOT F 1700.7 (8-72) Reproduction of completed page authorized

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Page 3: Comparison of Fatigue Analysis Approaches for Two Hot Mix ... · Based on the value engineering assessment including test results, statistical analysis, costs, and relative comparison

COMPARISON OF FATIGUE ANALYSIS APPROACHES FOR TWO HOT MIX ASPHALT CONCRETE (HMAC) MIXTURES

by

Lubinda F. Walubita Graduate Research Assistant, Texas Transportation Institute

Amy Epps Martin

Associate Research Engineer, Texas Transportation Institute

Sung Hoon Jung Graduate Research Assistant, Texas Transportation Institute

Charles J. Glover

Research Engineer, Texas Transportation Institute

Eun Sug Park Assistant Research Scientist, Texas Transportation Institute

Arif Chowdhury

Associate Transportation Researcher, Texas Transportation Institute

and

Robert L. Lytton Research Engineer, Texas Transportation Institute

Report 0-4468-2 Project 0-4468

Project Title: Evaluate the Fatigue Resistance of Rut Resistance Mixes

Performed in cooperation with the Texas Department of Transportation

and the Federal Highway Administration

December 2004

Resubmitted: August 2005

TEXAS TRANSPORTATION INSTITUTE The Texas A&M University System College Station, Texas 77843-3135

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v

DISCLAIMER

The contents of this report reflect the views of the authors, who are responsible for the

facts and the accuracy of the data presented herein. The contents do not necessarily reflect the

official view or policies of the Federal Highway Administration (FHWA) or the Texas

Department of Transportation (TxDOT). This report does not constitute a standard,

specification, or regulation, nor it is intended for construction, bidding, or permit purposes.

Trade names were used solely for information and not for product endorsement. The engineers

in charge were Amy Epps Martin, P.E. (Texas No. 91053) and Charles J. Glover, P.E. (Texas

No. 48732).

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vi

ACKNOWLEDGMENTS

This project was conducted for TxDOT, and the authors thank TxDOT and FHWA for

their support in funding this research project. In particular, the guidance and technical assistance

provided by the project director (PD) Gregory Cleveland of TxDOT, the project coordinator (PC)

James Travis of FHWA, and German Claros of the Research and Technology Implementation

(RTI) office is greatly appreciated. Special thanks are also due to Lee Gustavus, Rick Canatella,

Scott Hubley, Sharath Krishnamurthy, Amit Bhasin, Jeffrey Perry, and Andrew Fawcett from the

Texas Transportation Institute (TTI) and Texas Engineering Experiment Station (TEES) for their

help in specimen/sample preparation, laboratory testing, and data analysis. The various TxDOT

district offices that provided the material mix-designs and assistance in material procurement are

also thanked.

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vii

TABLE OF CONTENTS

LIST OF FIGURES ..................................................................................................................... xiv

LIST OF TABLES....................................................................................................................... xix

CHAPTER 1. INTRODUCTION ....................................................................................................1

WORK PLAN............................................................................................................................1

SCOPE OF WORK....................................................................................................................3

DESCRIPTION OF CONTENTS..............................................................................................3

SUMMARY...............................................................................................................................4

CHAPTER 2. INFORMATION SEARCH......................................................................................5

FIELD SURVEY QUESTIONNARIES....................................................................................5

LITERATURE REVIEW ..........................................................................................................6

Prediction of HMAC Mixture Fatigue Resistance...............................................................6

Binder Aging and HMAC Mixture Fatigue Resistance.....................................................16

SELECTED FATIGUE ANALYSIS APPROACHES............................................................21

SUMMARY.............................................................................................................................22

CHAPTER 3. EXPERIMENTAL DESIGN..................................................................................23

HMAC MIXTURES AND MIX-DESIGN..............................................................................23

The Bryan (BRY) Mixture – Basic TxDOT Type C (PG 64-22 + Limestone) .................24

The Yoakum (YKM) Mixture – Rut Resistant 12.5 mm Superpave

(PG 76-22 + Gravel) ..........................................................................................................25

Material Properties for the Binders....................................................................................26

Material Properties for the Aggregates ..............................................................................28

HMAC SPECIMEN FABRICATION.....................................................................................29

Aggregate Batching ...........................................................................................................29

Mixing, Short Term Oven-aging, Compaction, and Air Voids .........................................31

Sawing, Coring, Handling, and Storage.............................................................................33

BINDER AND HMAC MIXTURE AGING CONDITIONS .................................................34

HYPOTHETICAL FIELD PAVEMENT STRUCTURES AND TRAFFIC ..........................35

ENVIRONMENTAL CONDITIONS .....................................................................................36

RELIABILITY LEVEL...........................................................................................................38

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viii

TABLE OF CONTENTS (continued)

ELSYM5 STRESS-STRAIN ANALYSIS ..............................................................................39

ELSYM5 Input/Output Data..............................................................................................39

FEM Strain-Adjustment.....................................................................................................40

SUMMARY.............................................................................................................................41

CHAPTER 4. THE MECHANISTIC EMPIRICAL APPROACH ...............................................43

FUNDAMENTAL THEORY..................................................................................................43

INPUT/OUTPUT DATA.........................................................................................................45

LABORATORY TESTING.....................................................................................................46

The BB Fatigue Test Protocol............................................................................................46

Test Conditions and Specimens .........................................................................................48

Test Equipment and Data Measurement ............................................................................49

FAILURE CRITERIA ............................................................................................................50

ANALYSIS PROCEDURE.....................................................................................................50

Step 1. Laboratory Test Data Analysis (N-εt Empirical Relationship) ..............................51

Step 2. Stress-Strain Analysis, εt (Design) .............................................................................52

Step 3. Statistical Prediction of HMAC Mixture Fatigue Resistance, Nf(Supply) .................52

Step 4. Determination of the Required Pavement Fatigue Life, Nf(Demand).........................53

Step 5. Fatigue Design Check for Adequate Performance ................................................54

VARIABILITY, STATISTICAL ANALYSIS, AND Nf PREDICTION ................................54

SUMMARY.............................................................................................................................57

CHAPTER 5. THE CALIBRATED MECHANISTIC APPROACH WITH SURFACE

ENERGY………. ..........................................................................................................................59

FUNDAMENTAL THEORY AND DEVELOPMENT..........................................................59

INPUT/OUTPUT DATA.........................................................................................................62

LABORATORY TESTING.....................................................................................................65

Tensile Strength Test .........................................................................................................65

Relaxation Modulus Test ...................................................................................................66

Uniaxial Repeated Direct-Tension Test.............................................................................69

Anisotropic Test.................................................................................................................72

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ix

TABLE OF CONTENTS (continued)

Surface Energy Measurements for the Binder – The Wilhelmy Plate Test .......................76

Surface Energy Measurements for the Aggregate – The Universal Sorption Device .......81

FAILURE CRITERIA ............................................................................................................87

ANALYSIS PROCEDURE.....................................................................................................87

Shift Factor Due to Anisotropic Effect, SFa ......................................................................88

Shift Factor Due to Healing Effect, SFh.............................................................................89

Other Shift Factors.............................................................................................................93

Number of Load Cycles to Crack Initiation, Ni .................................................................97

Number of Load Cycles to Crack Propagation, Np ..........................................................100

Surface Energies, ∆GhAB, ∆Gh

LW, and ∆Gf .......................................................................102

Relaxation Modulus, Ei, Exponent, mi, and Temperature Correction Factor, aT .............104

DPSE and Constant, b .....................................................................................................105

Crack Density, CD ............................................................................................................110

Shear Strain, γ ..................................................................................................................110

VARIABILITY, STATISTICAL ANALYSIS, AND Nf PREDICTION ..............................111

SUMMARY...........................................................................................................................112

CHAPTER 6. THE CALIBRATED MECHANISTIC APPROACH WITHOUT SURFACE

ENERGY .....................................................................................................................................115

LABORATORY TESTING...................................................................................................118

SE Measurements for Binders and Aggregates ...............................................................118

RM Test in Compression .................................................................................................118

ANALYSIS PROCEDURE...................................................................................................118

Shift Factor Due to Healing, SFh .....................................................................................119

Paris’ Law Fracture Parameters, A and n.........................................................................119

SUMMARY...........................................................................................................................120

CHAPTER 7. THE PROPOSED NCHRP 1-37A 2002 PAVEMENT DESIGN GUIDE...........123

FUNDAMENTAL THEORY................................................................................................123

INPUT/OUTPUT DATA.......................................................................................................125

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TABLE OF CONTENTS (continued)

LABORATORY TESTING...................................................................................................126

Dynamic Shear Rheometer Test ......................................................................................126

Dynamic Modulus Test....................................................................................................126

FAILURE CRITERIA ..........................................................................................................131

ANALYSIS PROCEDURE...................................................................................................131

VARIABILITY, STATISTICAL ANALYSIS, AND Nf PREDICTION..............................132

SUMMARY...........................................................................................................................132

CHAPTER 8. BINDER OXIDATIVE HARDENING BACKGROUND AND TESTING

METHODOLOGY ......................................................................................................................135

BINDER OXIDATION AND EMBRITTLEMENT (52, 93) ...............................................135

BINDERS STUDIED ............................................................................................................140

Laboratory-Aged Binders ................................................................................................140

Binders Recovered from HMAC Mixtures......................................................................140

BINDER TESTS....................................................................................................................141

Size Exclusion Chromatography .....................................................................................141

Dynamic Shear Rheometer .............................................................................................142

Ductility ...........................................................................................................................142

Fourier Transform Infrared Spectrometer (FTIR) ...........................................................143

SUMMARY...........................................................................................................................143

CHAPTER 9. BINDER-HMAC MIXTURE CHARACTERIZATION .....................................145

METHODOLOGY ................................................................................................................146

Binder Data Analysis .......................................................................................................147

HMAC Mixture Tests ......................................................................................................147

HMAC Mixture Visco-Elastic Characterization..............................................................149

RESULTS ..............................................................................................................................153

Recovered Binder Results................................................................................................154

HMAC Mixture Results...................................................................................................159

Binder-Mixture Comparisons ..........................................................................................164

SUMMARY...........................................................................................................................165

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TABLE OF CONTENTS (continued)

CHAPTER 10. HMAC MIXTURE RESULTS AND ANALYSIS ............................................167

MIXTURE PROPERTIES FOR PREDICTING Nf...............................................................167

BB Laboratory Test Results.............................................................................................167

Nf-εt Empirical Relationships...........................................................................................168

Tensile Strength (σt) ........................................................................................................170

Relaxation Modulus Master-Curves ................................................................................172

RM Temperature Shift Factors, aT...................................................................................174

Dissipated Pseudo Strain Energy (DPSE) and Fracture Damage ...................................176

Surface Energy.................................................................................................................177

Mixture Anisotropy..........................................................................................................179

Dynamic Modulus Results...............................................................................................180

HMAC MIXTURE FATIGUE LIVES (Nf)...........................................................................181

ME Lab Nf Results ...........................................................................................................181

CMSE Lab Nf Results ......................................................................................................182

CM Lab Nf Results...........................................................................................................183

Mixture Field Nf Results – ME, CMSE, and CM Analyses.............................................185

Mixture Field Nf Results – The M-E Pavement Design Guide Analysis.........................187

DEVELOPMENT OF CMSE SHIFT FACTORS DUE TO AGING ...................................188

Theoretical Basis and Assumptions .................................................................................188

SFag Formulation and the Binder DSR Master-Curves....................................................189

CMSE-CM Field Nf Prediction Using SFag......................................................................192

SUMMARY...........................................................................................................................193

BB Testing .......................................................................................................................193

Tensile Stress ...................................................................................................................193

Relaxation Modulus .........................................................................................................193

DPSE and SE Results.......................................................................................................194

Mixture Anisotropy..........................................................................................................194

Mixture Nf ........................................................................................................................195

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TABLE OF CONTENTS (continued)

CHAPTER 11. DISCUSSION AND SYNTHESIS OF RESULTS ............................................197

COMPARISON OF MIXTURE FIELD Nf ...........................................................................197

MIXTURE VARIABILITY...................................................................................................201

EFFECTS OF OTHER INPUT VARIABLES ON MIXTURE FIELD Nf ...........................203

Pavement Structure ..........................................................................................................203

Environmental Conditions ...............................................................................................205

BINDER TEST RESULTS AND EFFECTS OF AGING ....................................................206

BINDER-MIXTURE CHARACTERIZATION AND AN AGING SHIFT FACTOR ........212

SUMMARY...........................................................................................................................219

CHAPTER 12. COMPARISON AND SELECTION OF THE FATIGUE ANALYSIS

APPROACH ................................................................................................................................221

COMPARATIVE REVIEW OF THE FATIGUE ANALYSIS APPROACHES .................221

Theoretical Concepts .......................................................................................................223

Input Data.........................................................................................................................224

Laboratory Testing...........................................................................................................224

Failure Criteria .................................................................................................................225

Data Analysis ...................................................................................................................227

Results and Variability.....................................................................................................228

Costs - Time Requirements for Laboratory Testing and Data Analysis..........................229

Costs - Equipment............................................................................................................230

SELECTION OF FATIGUE ANALYSIS APPROACH ......................................................230

TxDOT Evaluation Survey Questionnaire.......................................................................232

Assessment and Rating Criteria of the Fatigue Analysis Approaches.............................234

The Selected Fatigue Analysis Approach – The CMSE Approach .................................235

Incorporation of Aging Effects in Field Nf Prediction ....................................................236

Recommendations on a Surrogate Fatigue Test and Analysis Protocol .........................236

SUMMARY ..........................................................................................................................237

CHAPTER 13. CONCLUSIONS, RECOMMENDATIONS, AND FUTURE WORK .............239

CONCLUSIONS....................................................................................................................239

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TABLE OF CONTENTS (continued)

Selected Fatigue Analysis Approach - CMSE.................................................................239

Comparison of Mixture Field Nf ......................................................................................241

Effects of Binder Oxidative Aging and Other Variables .................................................241

Binder-Mixture Characterization .....................................................................................242

RECOMMENDATIONS.......................................................................................................243

CLOSURE .............................................................................................................................244

CURRENT AND FUTURE FY05 WORK ...........................................................................244

REFERENCES ............................................................................................................................247

APPENDICES .............................................................................................................................263

APPENDIX A: EVALUATION FIELD SURVEY QUESTIONNAIRE

(FOR GOVERNMENT AGENCIES AND THE INDUSTRY)............................................265

APPENDIX B: HMAC ANISOTROPIC ADJUSTMENT FACTORS ...............................267

APPENDIX C: BENDING BEAM LABORATORY TEST DATA FOR THE

MECHANISTIC EMPIRICAL APPROACH .......................................................................269

APPENDIX D: DYNAMIC MODULUS LABORATORY TEST DATA FOR

THE M-E PAVEMENT DESIGN GUIDE ...........................................................................271

APPENDIX E: EXAMPLE OF PERCENTAGE CRACKING ANALYSIS FROM

THE M-E PAVEMENT DESIGN GUIDE SOFTWARE.....................................................273

APPENDIX F: ME MIXTURE LAB Nf RESULTS ............................................................275

APPENDIX G: CMSE MIXTURE LAB Nf RESULTS.......................................................277

APPENDIX H: CM MIXTURE LAB Nf RESULTS............................................................279

APPENDIX I: MIXTURE FIELD Nf RESULTS.................................................................281

APPENDIX J: RESOURCE REQUIREMENTS .................................................................287

APPENDIX K: TxDOT EVALUATION SURVEY QUESTIONNAIRE...........................289

APPENDIX L: RATING CRITERIA OF THE FATIGUE ANALYSIS APPROACHES..291

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LIST OF FIGURES

Figure Page

2-1 Master-Curve for SHRP AAB-1 at Two Aging Times (°F = 32 +1.8(°C)) .......................18

2-2 Effect of Aging on Low Shear-Rate Limiting Viscosity (°F = 32 +1.8(°C)) .....................18

2-3 Continuous Bottom Grade as a Function of PAV Aging Time (°F = 32 +1.8(°C)) ...........19

2-4 Ductility versus DSR Function G’/(η/G’) (°F = 32 +1.8(°C)) ...........................................20

3-1 Limestone Aggregate Gradation Curve for TxDOT Type C Mixture ...............................24

3-2 Gravel Aggregate Gradation Curve for Rut Resistant 12.5 mm Superpave Mixture.........25

3-3 Binder High Temperature Properties – G*/Sin δ, Pascal (°F = 32 +1.8(°C)),

(delta ≅ δ) ...........................................................................................................................26

3-4 Binder Low Temperature Properties - Flexural Creep Stiffness (MPa)

(°F = 32 +1.8(°C)) ..............................................................................................................27

3-5 Binder Low Temperature Properties (m-value) (°F = 32 +1.8(°C))...................................27

3-6 Superpave Gyratory Compactor .........................................................................................32

3-7 Linear kneading Compactor ...............................................................................................32

3-8 Laboratory Test Specimens (Drawing not to Scale) (1 mm ≅ 0.039 inches) .....................33

3-9 Fatigue Analysis Approaches and HMAC Mixture Aging Conditions

(°F = 32 +1.8(°C)) ..............................................................................................................35

3-10 Texas Environmental Zoning (60)......................................................................................37

4-1 The ME Fatigue Design and Analysis System ..................................................................44

4-2 The Bending Beam (BB) Device........................................................................................47

4-3 Loading Configuration for the BB Fatigue Test.................................................................47

4-4 Example of Temperature Plot for the BB Test ...................................................................49

4-5 Example of Stress Response from BB Testing at 20 °C (68 °F)

(374 microstrain level) .......................................................................................................50

5-1 Example of Hysteresis Loop (Shaded Area is DPSE)........................................................60

5-2 The CMSE Fatigue Design and Analysis System ..............................................................63

5-3 Loading Configuration for Tensile Strength Test...............................................................65

5-4 Loading Configuration for Relaxation Modulus Test ........................................................67

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LIST OF FIGURES (continued)

5-5 Example of Stress Response from RM Test at 10 °C (50 °F) ............................................68

5-6 Loading Configuration for the RDT Test...........................................................................70

5-7 Stress Response from RDT Testing at 30 °C (86 °F).........................................................71

5-8 Loading Configuration for the AN Test.............................................................................72

5-9 Example of Strain Responses from AN Testing at 20 °C (68 °F)......................................74

5-10 Loading Configuration for the Wilhelmy Plate Test Method ............................................76

5-11 The DCA Force Balance and Computer Setup – Wilhelmy Plate Test .............................78

5-12 Example of the DCA Software Display (Advancing and Receding) .................................79

5-13 USD Setup..........................................................................................................................82

5-14 Example of Adsorption of n-Hexane onto Limestone under USD Testing .......................84

5-15 Output Stress Shape Form from RDT Test ......................................................................108

5-16 Example of WR – Log N Plot ...........................................................................................109

5-17 Brittle Crack Failure Mode (Marek and Herrin [88]).......................................................110

6-1 The CM Fatigue Design and Analysis System.................................................................116

7-1 The Fatigue Design and Analysis System for the M-E Pavement Design guide as

Utilized in this Project......................................................................................................124

7-2 Loading Configuration for Dynamic Modulus Test.........................................................127

7-3 The Universal Testing Machine .......................................................................................128

7-4 Compressive Axial Strain Response from DM Testing at 4.4 °C (40 °F) .......................129

8-1 The Maxwell Model .........................................................................................................136

8-2 Correlation of Aged-Binder Ductility with the DSR Function G’/(η’/G’) for

Unmodified Binders (52) (°F = 32 + 1.8(°C)) .................................................................137

8-3 Binder Aging Path on a G’ vs. η’/G’ Map (Pavement-aged Binders) (52)

(°F = 32 + 1.8(°C)). ..........................................................................................................138

9-1 Binder Oxidative Aging and Testing (°F = 32 + 1.8(°C))................................................146

9-2 Binder-Mixture Characterization Test Procedure (°F = 32 + 1.8(°C)).............................148

9-3 Relaxation Master-Curve for 0 Month Aged Yoakum Mixture Used for CMSE

(°F = 32 + 1.8(°C)) .........................................................................................................149

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LIST OF FIGURES (continued)

9-4 Shear Modulus Master-Curve for 0 Month Aged Yoakum Mixture Used for CMSE

(°F = 32 + 1.8(°C)) ...........................................................................................................153

9-5 Master-Curves of Recovered Binders for G*(ω) from Bryan Mixture

(°F = 32 + 1.8(°C)) .......................................................................................................155

9-6 Master-Curves of Recovered Binders for G*(ω) from Yoakum Mixture

(°F = 32 + 1.8(°C)) .......................................................................................................155

9-7 Master-Curve of Recovered Binders for G’(ω), G”(ω) from Bryan Mixture

(°F = 32 + 1.8(°C)) .......................................................................................................156

9-8 Master-Curve of Recovered Binders for G’(ω), G”(ω) from Yoakum Mixture

(°F = 32 + 1.8(°C)) .......................................................................................................156

9-9 DSR Function of Recovered Binders from Bryan Mixture (°F = 32 + 1.8(°C)) ..............157

9-10 DSR Function of Recovered Binders from Yoakum Mixture (°F = 32 + 1.8(°C)) ..........158

9-11 Master-Curves of Bryan Mixture for E(t) (°F = 32 + 1.8(°C)).........................................159

9-12 Master-Curves of Yoakum Mixtures for E(t) (°F = 32 + 1.8(°C)) ...................................160

9-13 Master-Curves of Bryan Mixture for G’(ω), G”(ω) (°F = 32 + 1.8(°C)).........................161

9-14 Master-Curves of Yoakum Mixture for G’(ω), G”(ω) (°F = 32 + 1.8(°C)).....................162

9-15 Master-Curve Comparisons between Bryan and Yoakum Mixtures for G*(ω)

(°F = 32 + 1.8(°C)) ...........................................................................................................162

9-16 VE Function of Bryan Mixture (°F = 32 + 1.8(°C)).........................................................163

9-17 VE Function of Yoakum Mixture (°F = 32 + 1.8(°C)).....................................................164

9-18 VE Function vs. DSR Function (°F = 32 + 1.8(°C)) ........................................................165

10-1(a) N vs. εt at 20 °C (68 °F) (Bryan Mixture) ......................................................................169

10-1(b) N vs. εt at 20 °C (68 °F) (Yoakum Mixture)..................................................................169

10-2(a) Mixture Tensile Stress at 20 °C (68 °F) (Bryan Mixture)...............................................171

10-2(b) Mixture Tensile Stress at 20 °C (68 °F) (Yoakum Mixture) ..........................................171

10-2(c) Failure Tensile Strain (εf) at Break at 20 °C (68 °F).......................................................172

10-3(a) RM (Tension) Master-Curve at 20 °C (68 °F) (Bryan Mixture).....................................173

10-3(b) RM (Tension) Master-Curve at 20 °C (68 °F) (Yoakum Mixture).................................173

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LIST OF FIGURES (continued)

10-4(a) Temperature Shift Factors, aT Tref = 20 °C (Bryan Mixture) (°F = 32 + 1.8(°C))...............175

10-4(b) Temperature Shift Factors, aT at Tref = 20 °C (Yoakum Mixture) (°F = 32 + 1.8(°C)).......175

10-5 Mixture DPSE at 20 °C (68 °F): Constant b vs. Aging Condition .................................176

10-6(a) Mixture Fracture Energy (∆Gf), ergs/cm2 (adhesive, dry-conditions) . .........................177

10-6(b) Mixture Healing Energy (∆Gh), ergs/cm2 (adhesive, dry-conditions) ............................178

10-7 Mixture Lab Nf at 20 °C (68 °F) for PS#1, WW Environment

(Bryan vs. Yoakum Mixture) – ME Analysis.................................................................182

10-8 Mixture Lab Nf at 20 °C (68 °F) for PS#1, WW Environment

(Bryan vs. Yoakum Mixture) – CMSE Analysis ..........................................................183

10-9 Mixture Lab Nf at 20 °C (68 °F) for PS#1, WW Environment

(Bryan vs. Yoakum Mixture) – CM Analysis...............................................................184

10-10(a) Field Nf for PS#1, WW Environment – ME Analysis...................................................185

10-10(b) Field Nf for PS#1, WW Environment – CMSE Analysis .............................................186

10-10(c) Field Nf for PS#1, WW Environment – CM Analysis ..................................................186

10-11 Field Nf for PS#1, WW Environment – M-E Design Guide Analysis. ........................187

10-12 Binder DSRf (ω) Master-Curves @ 20 °C (68 °F) .........................................................191

11-1(a) Mixture Field Nf (0 Months, PS#1, WW Environment) ................................................197

11-1(b) Mixture Field Nf (3 Months, PS#1, WW Environment)................................................198

11-1(c) Mixture Field Nf (6 Months, PS#1, WW Environment)................................................198

11-1(d) Mixture Field Nf Comparison (PS#1, WW Environment) ............................................199

11-2 Effect of Pavement Structure on Mixture Field Nf

(Bryan Mixture, WW Environment)..............................................................................204

11-3 Effect of Environmental Conditions on Mixture Field Nf (PS#1).................................205

11-4 SEC Chromatogram for Recovered Binders from Bryan Mixtures

(°F = 32 + 1.8 (°C)) ..........................................................................................................207

11-5 CA Rate of Bryan Binder (PG 64-22) (°F = 32 + 1.8 (°C)) ..........................................208

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LIST OF FIGURES (continued)

11-6 Zero Shear Viscosity Hardening Rate of Bryan Binder (PG 64-22)

(°F = 32 + 1.8 (°C)) ..........................................................................................................208

11-7 DSR Function vs. Carbonyl Area of Bryan Binder (PG 64-22) (°F = 32 + 1.8(°C)) ....209

11-8 DSR Function Hardening Rate of Yoakum Binder (PG 76-22) (°F = 32 + 1.8(°C)) ....210

11-9 CA Rate of Yoakum Binder (PG 76-22) (°F = 32 + 1.8(°C)) .......................................211

11-10 DSR Function vs. CA of Yoakum Binder (PG 76-22) (°F = 32 + 1.8(°C)) ..................212

11-11 Decline of Field Nf with Binder DSR Function Hardening (°F = 32 + 1.8(°C))...........214

11-12 DSR Function Hardening Rate of Neat Binder after Initial Jump

(°F = 32 + 1.8 (°C)) ..........................................................................................................215

11-13 Calculated Decline of Remaining Pavement Fatigue Service Life ...............................216

11-14 Hypothetical Decline of Pavement Fatigue Service life, Initial Fatigues Equal ..........217

11-15 Hypothetical Decline of Pavement Fatigue Service life, Ki Values Equal...................219

12-1 Assessment Factors/Sub-factors and Associated Weighting Scores ............................233

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LIST OF TABLES

Table Page

3-1 Intermediate Temperature Properties of the Binders at 25 °C (77 °F)...............................28

3-2 Aggregate Properties ..........................................................................................................29

3-3 Limestone Aggregate Gradation for TxDOT Type C Mixture ..........................................30

3-4 Gravel Aggregate Gradation for 12.5 mm Superpave Mixture..........................................30

3-5 HMAC Mixture Mixing and Compaction Temperatures...................................................31

3-6 Aging Conditions for Binders and HMAC Compacted Specimens...................................34

3-7 Selected Pavement Structures and Traffic .........................................................................36

3-8 Computed Critical Design Strains......................................................................................41

4-1 Summary of ME Fatigue Analysis Input and Output Data ...............................................46

5-1 Summary of CMSE Fatigue Analysis Input and Output Data...........................................64

5-2 Surface Energy Components of Water, Formamide, and Glycerol...................................78

5-3 Surface Energy Components of Water, n-hexane, and MPK............................................83

5-4 Fatigue Calibration Constants Based on Backcalculation of Asphalt Moduli from FWD

Tests (Lytton et al. [45]) ...................................................................................................92

5-5 Fatigue Calibration Constants based on Laboratory Accelerated Tests

(Lytton et al. [45]) ..............................................................................................................92

6-1 Summary of CM Fatigue Analysis Input and Output Data .............................................117

7-1 Analysis Input/Output Data for the M-E Pavement Design Guide Software..................125

7-2 Example of Output Data from DM Testing at 4.4 °C (40 °F) .........................................130

10-1 BB Laboratory Test Results ............................................................................................167

10-2 Mixture Empirical Fatigue Relationships........................................................................168

10-3 Mixture Tensile Strength .................................................................................................170

10-4 Mixture Relaxation Modulus (Tension) Test Data..........................................................172

10-5 Paris’ Law Fracture Coefficient A and SFh Values .........................................................178

10-6 Mixture Anisotropic Results............................................................................................180

10-7 CM vs. CMSE Mixture Lab Nf Results for PS#1, WW Environment.............................184

10-8 CMSE-CM SFag Values...................................................................................................190

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LIST OF TABLES (Continued)

10-9 Example of Field Nf Predictions at Year 20 (PS#1, WW Environment).........................192

11-1 Example of HMAC Specimen AV Variability................................................................201

11-2 Example of Mixture Field Nf Variability (PS# 1, WW Environment) ............................202

11-3 Summary of Pavement Fatigue Life Parameters .............................................................215

12-1(a) Summary Comparison of the Fatigue Analysis Approaches ..........................................221

12-1(b) Summary Comparison of the Fatigue Analysis Approaches ..........................................222

12-1(c) Summary Comparison of the Fatigue Analysis Approaches ..........................................223

12-1(d) Summary Comparison of the Fatigue Analysis Approaches ..........................................223

12-2 Summary Comparison of Figure Analysis Approaches .................................................231

12-3 Weighted Scores and Rating of the Fatigue Analysis Approaches ................................234

13-1 Example of a Factorial Experimental Design for FY05.................................................245

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CHAPTER 1 INTRODUCTION

Hot mix asphalt concrete (HMAC) mixtures are designed to resist aging and

distress induced by traffic loading and changing environmental conditions. Common

HMAC distresses include rutting, fatigue, and thermal cracking. Over the past decade, the

Texas Department of Transportation (TxDOT) focused research efforts on improving

mixture design to preclude rutting in the early life of the pavement. Improvements in

rutting resistance also offered increased resistance to moisture damage. However, a

concern arose that these stiff mixtures may be susceptible to fatigue cracking in the long

term in the pavement structure, particularly if the binder stiffens excessively due to

oxidative aging. Therefore, in 2002 TxDOT initiated a research study with the following

two primary objectives:

(1) To evaluate and recommend a fatigue HMAC mixture design and analysis system

for TxDOT to ensure adequate mixture performance in a particular pavement

structure under specific environmental and traffic loading conditions that

incorporates the effects of binder oxidative aging.

(2) To comparatively evaluate and establish a database of fatigue resistance of

commonly used TxDOT HMAC mixtures.

WORK PLAN

To accomplish these goals, researchers utilized four fatigue analysis approaches

to predict fatigue lives of one common TxDOT mixture and another TxDOT mixture

frequently used for rutting resistance under representative environmental conditions and

typical loading conditions in standard pavement structures.

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The selected approaches included the following:

• the mechanistic empirical (ME) approach developed during the Strategic Highway

Research Program (SHRP) using the bending beam fatigue test (1,2);

• the proposed National Cooperative Highway Research Program (NCHRP) 1-37A

2002 Pavement Design Guide using the dynamic modulus test (3, 4);

• a calibrated mechanistic (CM) approach developed at Texas A&M University that

requires strength and repeated loading tests in uniaxial tension and relaxation tests in

uniaxial tension and compression for material characterization and monitoring

dissipated pseudo strain energy (5); and

• an updated calibrated mechanistic (CMSE) approach developed at Texas A&M

University that also requires measuring surface energies of component materials in

addition to the material characterization tests from the original calibrated mechanistic

approach (6).

At the conclusion of the original project in August 2004, the research team

recommended the best approach for fatigue design and analysis based on a value

engineering assessment. This comparison of the four fatigue analysis approaches

considered variability; required resources; implementation issues; the ability to

incorporate the important effects of aging, fracture, and healing; practicality; and the

capability to interface with pavement design. A key element of this two-year research

effort was progress made in the investigation of the relationship between the change in

mixture fatigue resistance due to aging and aged binder properties. With a better

understanding of this relationship, the effects of aging on fatigue life may be quantified.

In a modified third year of the project, fatigue lives of additional mixtures will be

predicted using the recommended CMSE design and analysis system. These additional

mixtures will explore the effects on fatigue life of mixture parameters, including binder

content and binder or modifier type. Further investigation of the effects of aging on

mixture fatigue resistance is also being pursued.

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SCOPE OF WORK

This interim report documents the following:

(1) detailed descriptions of the four fatigue analysis approaches used to predict fatigue

life,

(2) a comparison of fatigue lives of two TxDOT HMAC mixtures,

(3) the effect of binder oxidative aging on binder and mixture properties and fatigue

resistance,

(4) binder-mixture relationships with respect to binder oxidative aging, and

(5) development of shift factors due to aging based on binder visco-elastic properties.

The report describes fatigue analysis results for the two selected mixtures in five

specific pavement structures designed over a range of typical traffic loading conditions

and under two representative Texas environmental conditions.

DESCRIPTION OF CONTENTS

The interim report is divided into 13 chapters including this chapter (Chapter 1)

that provides the motivation for the project, the overall objectives and work plan, and the

scope of this report. The subsequent chapters describe the information search (Chapter 2)

and experimental design (Chapter 3) that includes selection of fatigue analysis

approaches, materials, specimen fabrication protocols, aging conditions, and typical

pavement structures. Next, the four fatigue analysis approaches are described in detail in

Chapters 4 through 7. Chapter 8 describes binder testing followed by the testing and

analysis utilized to explore the relationship between binder and HMAC mixture aging in

Chapter 9. Then, the results, including the resulting fatigue lives from all the approaches

and the aging evaluation, are described and discussed in Chapters 10, 11, and 12. This

report concludes in Chapter 13 with a summary of findings, recommendations, and a

work plan to complete the project in a modified third year. Appendices of detailed

laboratory test results and other important data are also included.

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SUMMARY

The following bullets summarize the project objectives, the work plan, scope of

work, and the contents of this interim report:

• The primary objectives of this project were twofold:

(1) to evaluate and recommend a fatigue HMAC mixture design and analysis system

for TxDOT to ensure adequate mixture performance in a particular pavement

structure under specific environmental and traffic loading conditions that

incorporates the effects of binder oxidative aging, and

(2) to comparatively evaluate and establish a database of fatigue resistance of

commonly used TxDOT HMAC mixtures.

• The work plan entailed utilization of four fatigue analysis approaches (mechanistic

empirical and calibrated mechanistic) to predict fatigue lives of one common TxDOT

mixture and another TxDOT mixture frequently used for rutting resistance under

representative environmental conditions and typical loading conditions in standard

pavement structures. Thereafter, the best approach for fatigue design and analysis

was recommended based on a value engineering assessment including the ability to

incorporate practicality and the important effects of aging, fracture, and healing.

• The scope of the research work was limited to: a) two TxDOT HMAC mixtures,

b) four fatigue analysis approaches, c) three binder oxidative aging conditions, d) five

standard pavement structures, and e) two Texas environmental conditions.

• The report consists of 13 chapters. Chapter 1 is the introduction, and Chapters 2 and 3

are the information search and experimental design, respectively. Chapters 4 through

7 describe the four fatigue analysis approaches, followed by binder testing in Chapter

8. Chapter 9 describes the binder-mixture characterization with respect to aging.

Mixture results are presented in Chapter 10, followed by a discussion, conclusions,

recommendations, and future work plans in Chapters 11, 12, and 13. Other data

including detailed laboratory test results are included in the appendices.

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CHAPTER 2

INFORMATION SEARCH

An information search utilizing a field survey questionnaire, electronic databases, and

resulting publications was conducted to gather data on current fatigue design and analysis

approaches; related laboratory tests, materials, pavement structures and design; corresponding

standards or references; and resources or methodologies used to obtain fatigue resistant HMAC

mixtures. Effects of aging, healing, and fracture on fatigue HMAC mixture performance were

also reviewed; and the literature found was summarized and documented. Researchers also

reviewed and documented commonly used TxDOT mixtures, material characteristics, and other

general input parameters including pavement structures, traffic loading, environmental

conditions, mix designs, aging conditions, and reliability levels.

Data gathered from the information search aided the research team in selecting the

appropriate fatigue analysis approaches for a comparative evaluation and subsequent

recommendation to TxDOT. These data also served as the basis for formulating the

experimental design including materials selection for this project.

FIELD SURVEY QUESTIONNAIRES

A field survey of government agencies and the industry addressed some of the

key aspects of fatigue analysis approaches, laboratory tests, material characteristics, pavement

structures and design, corresponding standards or references, and resources used for fatigue

resistant HMAC mixtures. Appendix A shows an example of the field survey questionnaire.

Thirty-nine surveys were emailed to a list of contacts familiar to the research team in the

industry, academia, and relevant personnel at state Departments of Transportation (DOTs).

Approximately half (10) of the 23 responses received do not consider fatigue in their HMAC

mixture design and analysis. Some of the responses referred the survey to other contacts, and

seven responses, primarily from research agencies, provided valuable references and information

that were reviewed and provided an input into the research methodology and experimental

design for the project. The results from these field survey questionnaires are summarized in

Appendix A from six respondents.

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Of the positive responses received, a majority of the DOTs and private industry use the

Superpave, mechanistic empirical, association of American State Highway and Transportation

Officials (AASHTO), Asphalt Institute, and visco-elastic continuum-damage analysis either for

mixture design and analysis or just to check for fatigue resistance in the final pavement structural

design (Appendix A). Laboratory tests include bending beam, dynamic modulus, indirect

tension, uniaxial fatigue, moisture sensitivity, and retained indirect tensile strength. Some of

these approaches and associated laboratory tests have been included in the experimental design

and are discussed subsequently.

LITERATURE REVIEW

From a detailed review of the information search, the research team summarized

information on the prediction of HMAC mixture fatigue resistance and binder aging and its

effects on HMAC mixture fatigue resistance.

Prediction of HMAC Mixture Fatigue Resistance

An approach that predicts HMAC mixture resistance to fatigue requires an understanding

and description of material behavior under repeated loads that simulate field conditions (1). This

broad description is valid for approaches that are mechanistic empirical to varying degrees. A

more empirically based approach requires that the laboratory test simulate field conditions, but a

constitutive law for material behavior in a more mechanics-based approach requires only

material properties determined from laboratory test(s) measured using a simple stress state if

possible.

In a review of flexure, supported flexure, direct uniaxial, diametral or indirect tension,

triaxial, fracture mechanics, and wheel-tracking test methods conducted a decade ago, continued

research in the use of dissipated energy and fracture mechanics approaches with flexure or direct

or indirect tension testing were recommended (1). This recommendation highlighted the shift

from more empirically based approaches to those able to incorporate a more fundamental

mechanistic understanding of fatigue crack initiation, crack propagation, and failure.

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This shift over the last decade toward the use of more applicable material behavior

models and numerical analysis methods to simulate the fatigue mechanism and failure was

possible due to the rapid increase in computing power. This section provides a brief review of

previous and current approaches that are more empirical in nature, those that provided a bridge

toward mechanistic analysis methods, and current mechanistic analysis approaches.

Mechanistic Empirical Approaches

Most previous approaches for predicting fatigue resistance of HMAC involve either

controlled stress or controlled strain laboratory testing at a single representative temperature over

a series of stress or strain levels, respectively, and determination of fatigue life at a stress or

strain level assumed to be critical and caused by a single type of vehicle load. These approaches

predict the number of stress or strain cycles to crack initiation in flexure, direct or indirect

tension, or semi-circular bending tests. A method to determine a single representative

temperature for laboratory testing and a temperature conversion factor to account for the fact that

loading occurs over a range in temperatures is required. A shift factor is also required to account

for other differences between field and laboratory conditions, including the effects of wander,

healing, and crack propagation. A lengthy testing program is required with replicate tests (to

account for relatively large variability) at different stress or strain levels to define an empirical

fatigue relationship for a specific HMAC mixture. The determination of the critical stress or

strain constitutes the mechanistic part of this type of approach, and this calculated value varies

depending on the assumed model of material behavior (where layered elastic is most commonly

used). The location of the critical stress or strain also limits the analysis to either bottom-up or

top-down fatigue cracking without consideration of both.

Even with the limitations of mechanistic-empirical approaches, validation has been

illustrated through comparisons with fatigue life measured in the field, particularly at accelerated

pavement testing (APT) facilities. The mechanistic empirical approach developed at the

University of California at Berkeley during the Strategic Highway Research Program as part of

Project A-003A provides a widely used example with results validated with full-scale Heavy

Vehicle Simulator (HVS) tests (2, 7, 8).

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Another mechanistic empirical approach explored at the University of Nottingham in

conjunction with the SHRP A-003A project was validated using a laboratory scale APT device.

Indirect tensile fatigue testing was also utilized at the University of Nottingham, and this testing

method was included in a comprehensive APT project that included scaled testing with the

Model Mobile Load Simulator (MMLS3). These approaches are described in brief detail in

subsequent subsections, followed by a subsection on improvements in mechanistic-empirical

approaches to account for changing environmental and loading conditions.

SHRP A-003A (University of California at Berkeley). The SHRP A-003A approach

utilizes the flexural beam fatigue test (third-point loading); incorporates reliability concepts that

account for uncertainty in laboratory testing, construction, and traffic prediction; and considers

environmental factors, traffic loading, and pavement design (2). Specimen preparation by rolling

wheel compaction is strongly recommended as part of this approach to simulate the engineering

properties of extracted pavement cores. Conditioning prior to testing to a representative or

worst-case aging state is also suggested. This approach was selected for this project as the

mechanistic empirical approach discussed in more detail in Chapter 4.

University of Nottingham. Fatigue research at the University of Nottingham provided

validation of the SHRP A-003A analysis system through wheel tracking tests and trapezoidal

fatigue testing (2, 9). Validation of flexural beam fatigue tests for one aggregate type was

successful for the thick wheel tracking slabs that approximated a controlled stress mode of

loading. Mixture rankings by the laboratory scale APT device were also approximately

equivalent to those based on indirect tensile stiffness and fatigue life determined by an indicator

of the ability to dissipate energy. Large variability in the wheel tracking results was highlighted.

Fatigue analysis continued at the University of Nottingham with the inclusion of a

visco-elastic model for material behavior that utilizes improvements in the conversion of

dynamic shear test results to dynamic flexural results first developed as part of the

SHRP A-003A system (2, 10).

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A visco-elastic material model was used in a mechanistic-empirical fatigue relationship

to predict crack initiation based on dissipated energy to account for nonsymmetrical stress/strain

response measured under full-scale loads and remove the effect of mode of loading during

laboratory testing. This model provides dissipated energy contour maps where the maximum

value can be located throughout the HMAC layer.

Indirect Tension Testing. Indirect tension offers a simple mode for dynamic

frequency sweep, fatigue, or strength testing, although a biaxial stress state and the inability to

test with stress reversal have been cited as disadvantages (11). The University of Nottingham

has utilized this testing mode in measuring stiffness and evaluating the fatigue resistance of

HMAC mixtures for overlay design (10).

More extensive indirect tensile fatigue testing for a range of materials in a complex

layered pavement structure was included in a comprehensive evaluation of two rehabilitation

strategies by TxDOT (12, 13). Relative fatigue lives were defined as the ratio of fatigue

resistance of untrafficked materials in these structures compared with those of the same materials

trafficked with a scaled APT device (MMLS3). These ratios provided an indication of the

detrimental effect of moisture damage and the improvement in fatigue resistance due to

increased temperatures and subsequent compaction. A series of time-consuming tests with an

average duration of 20 hours was completed at a single representative temperature

(20 °C [68 °F]) and frequency (10 Hz) with no rest periods in a controlled stress mode at a stress

level equal to 20 percent of the indirect tensile strength of the same HMAC material.

Tensile strength tests were also conducted in a semi-circular bending mode that induces a

direct tensile load to the center zone of a semi-circular shaped specimen to supplement the

indirect tensile test results. This test was considered as a possible candidate for fatigue testing in

this project due to reduced load requirements for the same stress level as compared to indirect

tensile testing, but it was not selected for evaluation because the associated analysis system is

still under development (14).

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Improvements to Mechanistic Empirical Approaches

The approach first developed during SHRP A-003A has been expanded further using the

full-scale APT WesTrack project to develop fatigue models and associated pay factors based on

construction quality (15, 16). The models developed were used to predict fatigue crack initiation

in the 26 original WesTrack sections.

Hourly changes in both environmental and traffic conditions (wander) were incorporated

in this mechanistic empirical analysis that assumed: (1) a critical binormal strain distribution

beneath dual tires at the base of the HMAC surface layer, (2) layered elastic behavior, and (3)

valid extrapolation of fatigue life for temperatures greater than 30 °C (86 °F). No shift factor

was applied to the fatigue life relationship that must be defined through laboratory testing for

each HMAC mixture type that is different from the Superpave WesTrack HMAC mixtures.

Empirical fatigue relationships developed by the Asphalt Institute and Shell have also

been improved through the definition of a continuous function of cumulative fatigue damage

using Miner’s Law to replace prediction of a specific level of fatigue cracking (17, 18). This

function assumes bottom-up cracking and utilizes a layered elastic material behavior model but

accounts for changing environmental and loading conditions in the accumulation of fatigue

damage. Further refinement with an expanded Long Term Pavement Performance (LTPP)

dataset that contains pavements exhibiting fatigue failure was recommended.

Tsai et al. have also adopted the Recursive Miner’s Law for cumulative fatigue damage

analysis of HMAC mixtures (18, 19). This Recursive Miner’s Law approach attempts to directly

incorporate the significant effects of traffic, environment, material properties, and pavement

structure in HMAC mixture fatigue modeling using mechanistic empirical relationships and a

Weibull-type fatigue life deterioration function. In their findings, Tsai et al. observed that

mixture properties played the most significant role in the fatigue damage accumulation of

HMAC pavement structures under traffic loading, while the randomness of vehicle speed and

traffic wander had the least effect (18).

Other research to further improve mechanistic empirical fatigue analysis has accounted

for the effects of dynamic loads (20). This approach considers a moving and fluctuating

concentrated load and utilizes Miner’s Law (19) with the assumption of bottom-up cracking to

predict fatigue crack initiation and cumulative fatigue damage.

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The Proposed NCHRP 1-37A 2002 Pavement Design Guide Methodology for Fatigue Resistance

The NCHRP 1-37A 2002 Pavement Design Guide adopts a mechanistic empirical

approach for the structural design of HMAC pavements (3). The basic inputs for pavement

design include environmental, materials, and traffic data. There are two major aspects of ME-

based material characterization: pavement response properties and major distress/transfer

functions (4).

Pavement response properties are required to predict states of stress, strain, and

displacement within the pavement structure when subjected to external wheel loads. These

properties for assumed elastic material behavior are the elastic modulus and Poisson’s ratio. The

major distress/transfer functions for asphalt pavements are load related fatigue fracture,

permanent deformation, and thermal cracking.

The current version of the NCHRP 1-37A 2002 Pavement Design Guide (and its

software), which is discussed in greater detail in Chapter 7, utilizes the Asphalt Institute damage

predictive equation (21). Unlike most ME-based approaches, this procedure incorporates two

types of fatigue damage criteria. Bottom-up fatigue cracking assumes crack initiation at the

bottom of the asphalt layer and propagation through the HMAC layer thickness to the surface.

Top-down fatigue cracking assumes crack initiation at the pavement surface and propagation

downward through the HMAC layer. In both failure criteria, tensile strain is the primary

mechanistic failure load-response parameter associated with crack growth. As discussed in

Chapter 7, this new design guide characterizes pavement materials in a hierarchical system

comprised of three input levels. Level 1 represents a design philosophy of the highest practically

achievable reliability, and Levels 2 and 3 have successively lower reliability.

For the 2002 Pavement Design Guide approach, NCHRP Project 9-19 researchers

suggested constructing a dynamic modulus master-curve for all HMAC mixtures. This master-

curve is developed by conducting frequency sweeps at five different temperatures and six

frequencies. The same master-curve can be used as an input for predicting rutting damage.

Preliminary efforts in NCHRP Project 9-19 did not show a strong correlation between dynamic

modulus and fatigue cracking at full-scale APT facilities (22). This finding provided increased

motivation to explore other approaches in this project.

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Toward Mechanistic Analysis

The shift toward mechanistic analysis of fatigue cracking was recognized and encouraged

through a review of the use of fracture mechanics in both HMAC and Portland cement concrete

(PCC) pavements (23). This history highlighted early efforts utilizing linear elastic fracture

mechanics and a single material property (K1c) providing the driving force for crack propagation

characterized by Paris’ Law.

Further efforts to consider a process zone ahead of the crack tip were also reviewed, and

the concept of similitude to provide a dimensionless parameter equivalent for both field and

laboratory conditions was described. A warning considering the specimen-size effect and its

implications for scaling cracking behavior was also issued.

The application of fracture mechanics to composite materials to advance the

understanding of the mechanism of fatigue cracking was recognized as a slow process but one

worth pursuing. This pursuit has continued to address the limitations of previous ME approaches

and expand the knowledge base and application of HMAC fatigue analysis.

Laboratory Test Programs. To address the limitation of a lengthy testing program,

researchers suggested characterizing the stiffness of HMAC using a master-curve from simple

dynamic direct or indirect tensile tests that reflects the dependence on time of loading and

temperature (24). Parameters from the master-curve were successfully used to predict the

coefficients in empirical fatigue relationships. The range of HMAC mixture variables, including

modified binders utilized in developing the regression relationships, were also provided.

Linear Visco-Elastic Models. To address the limitation of assumed layered elastic

material behavior, other researchers produced an integrated HMAC mixture and pavement

design that allows for more realistic linear visco-elastic behavior (25). This type of material

model accounts for asymmetrical stress-strain distributions under moving wheel loads and the

effect of time of loading history. In a multi-tiered analysis, the approach separately utilized two

conventional empirical fatigue relationships (based on strain and dissipated energy) for crack

initiation and Paris’ Law for crack propagation as described by Schapery (26).

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Laboratory testing requirements include frequency sweep, creep, and strength testing in

direct tension or compression at relevant temperatures. A nonlinear finite element simulation of

a multi-layer pavement structure that selects an appropriate HMAC stiffness as a function of a

more realistic asymmetrical stress state was also utilized in conjunction with mechanistic

empirical fatigue relationships (27). Numerical techniques were also used to model the behavior

of three specific materials using elastic-plastic fracture mechanics (28). Both crack initiation and

propagation were modeled, but the viscous behavior of HMAC was not taken into account.

Fracture Mechanics Approach. Further research toward improving the linear elastic

fracture mechanics approach with Paris’ Law as described by Schapery related the fracture

coefficients A and n and described the use of uniaxial dynamic and strength tests to determine

both parameters from a master stiffness curve and mixture correction factors (29). Crack

propagation using Paris’ Law was also incorporated successfully in two- and three-dimensional

finite element simulations (30). This approach spread complex simulation computations over the

material lifetime, incorporating damage and resulting stress redistribution. Crack propagation

was extrapolated between simulations to determine fatigue life from propagation of an initial

crack size assumed related to maximum aggregate size. This approach that assumes elastic

material response to a single type of load was validated using flexural beam fatigue tests.

Nonlinear fracture mechanics were applied to compare crack propagation parameters of different

materials at low temperatures and highlight the need to include effects of inelastic dissipated

energy in fatigue analysis (31).

Continuum Mechanics Approach. Research in fatigue analysis over the past decade has

expanded to include investigation of both damage due to repeated loading and healing due to

repeated rest periods (32, 33). Recovery of a loss in stiffness monitored during fatigue testing

was noted for short rest periods in direct uniaxial testing in a review of laboratory fatigue tests,

and the lack of fatigue cracking in thick HMAC pavements was attributed to a healing effect in

an evaluation toward revising design procedures (11, 34).

A continuum mechanics approach developed through research efforts at North Carolina

State University and Texas A&M University successfully accounted for damage growth through

crack initiation and propagation and healing for any load history or mode of loading (32, 33).

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This approach utilizes the visco-elastic correspondence principle and work potential

theory described by Schapery (26) to remove viscous effects in monitoring changes in pseudo-

stiffness in repeated uniaxial tensile tests. Coefficients in the visco-elastic constitutive model

describe differences in damage and healing behavior of different materials. This model was

validated with both laboratory and field results and behavior predicted from the micromechanical

approach also developed at Texas A&M University and described in a subsequent subsection

(33).

The continuum approach has also led to the development of two simplified fatigue

analysis systems (35, 36). One system predicts fatigue behavior for temperatures less than 20 °C

(68 °F) from a characteristic damage curve generated based on frequency sweep and strength

tests in uniaxial tension at multiple temperatures (35). Improvements to this system to consider

aging and healing and application to other HMAC mixture types were recommended. The other

system utilizes indirect tensile creep and strength testing with a longer gauge length than the

standard Superpave mixture test and visco-elastic analysis of material response (36, 37). The use

of fracture energy based on tests at 20 °C (68 °F) to predict fatigue cracking was validated using

data from the full-scale APT WesTrack project.

With a shift toward more mechanics-based approaches, fatigue analysis is expected to

become independent of many factors and variables that limit the application of ME approaches

that were the only available analysis tools prior to the rapid increase in computing power. These

factors and variables include mode of loading (controlled stress or controlled strain), laboratory

test type, time of loading, temperature, type and location of loading, rest periods, and HMAC

mixture variables.

Empirical to ME to Calibrated Mechanistic

A major reason for the gradual change of mixture fatigue analysis from empirical or

phenomenological to ME to calibrated mechanistic is the greatly increased capabilities of

computers to model material behavior realistically, using mechanics and user friendly

computational packages such as finite element programs. As computers become faster with

larger memories in the future, these approaches will be the simplest, most direct, and probably

most practical way to design HMAC mixtures and pavements.

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These computational packages can only utilize material properties as input, instead of

empirical constants or ME regression coefficients used in previous approaches. This

development brings with it an added bonus that laboratory or non-destructive field measurement

of material properties is much simpler than determination of these constants and coefficients

through extensive laboratory testing.

Calibrated Mechanistic Approaches. The calibrated mechanistic approaches are based

on the theory that HMAC is a complex composite material that behaves in a nonlinear visco-

elastic manner, ages, heals, and requires that energy be stored on fracture surfaces as load-

induced damage in the form of fatigue cracking progresses. Energy is also released from fracture

surfaces during the healing process. HMAC mixture resistance to fatigue cracking thus consists

of two components, resistance to fracture (both crack initiation and propagation) and the ability

to heal, that both change over time.

Several approaches that predict fatigue life require material characterization and account

for both the fracture and healing processes in HMAC that have been developed over the past

decade. In the SHRP A-005 project, a complete model of fatigue fracture and healing was

developed (38). Other researchers showed the importance of the use of fracture and dissipated

energy in measuring the fracture resistance of a HMAC mixture (39). This same concept of

dissipated energy per load cycle provides the driving force for fatigue crack initiation and

propagation, and researchers demonstrated that the fracture energy approach was able to

accurately predict the fatigue life of a wide variety of HMAC mixture designs as compared to

other approaches (40, 41). SHRP A-005 results and a finite element computer program have

been used to illustrate substantial agreement with these results in predicting the two phases of

crack growth, initiation, and propagation (42).

The Texas A&M Calibrated Mechanistic Approach. A micromechanical approach

developed at Texas A&M University based on the SHRP A-005 results requires only creep or

relaxation, strength, and repeated load tests in uniaxial tension and compression and a catalog of

fracture and healing surface energy components of asphalt binders and aggregates measured

separately (43, 44, 45).

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Surface energy components of various common aggregates and binders have been

measured at Texas Transportation Institute (TTI) in various studies (43, 44, 46, 47). The results

have been cataloged and are also proving useful in other ongoing TTI studies including moisture

damage prediction in HMAC pavements. In this approach selected for evaluation in this project,

HMAC behavior in fatigue is governed by the energy stored on or released from crack faces that

drive the fracture and healing processes, respectively, through these two different mechanisms.

Chapter 5 discusses this approach in greater detail.

Computational models that incorporate more realistic material behavior for HMAC are

expected to be increasingly faster and user-friendly in the near future. Convenient and efficient

methods of characterizing the fracture and healing properties of HMAC mixtures will be useful

to take advantage of these continued advances that promise improved mixture and pavement

design.

Binder Aging and HMAC Mixture Fatigue Resistance

TTI’s Center for Asphalt and Materials Chemistry (CMAC) has studied the effect of

oxidative aging on asphalt binders over the last 15 years. During this time, CMAC researchers

have conducted a comprehensive study of the oxidation kinetics of binders under varying

conditions of temperature and oxygen pressure and of the effect of this oxidation on the physical

properties of binders. Both of these issues are crucial to understanding the rate at which asphalt

binders age in service in the field and the results of these changes on performance. This section

briefly summarizes CMAC’s relevant results.

Fundamentally, the oxidation of binder results in compounds that are more polar and

therefore form strong associations with each other. These associations result in both a greater

resistance to flow (higher viscosity) and larger elastic modulus. Together these effects result in

higher stresses in HMAC under load. This greater resistance to flow can be beneficial at high

temperatures by reducing permanent deformation. A problem emerges, however, when aging is

excessive, leading to excessively large stresses that result in binder failure at lower temperatures

(thermal cracking).

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This effect of oxidative aging must also contribute to failure by repeated load (fatigue

cracking) through its effect on HMAC stiffness that governs material response to load. It also

explains why producing binders that have higher high-temperature Superpave grades (and thus

provide stiffer mixtures at rutting temperatures) may be more prone to premature fatigue

cracking. Starting out stiffer puts these HMAC mixtures at a disadvantage as stiffness

age-hardening proceeds throughout the lifetime of the HMAC pavement.

The following subsections provide more detail on these effects of oxidation on binders

and thus on HMAC mixture fatigue resistance.

Effect of Aging on Binder Viscosity

Binder viscosity increases dramatically due to oxidation, in fact, by orders of magnitude

over the life of a pavement. Figure 2-1 shows typical changes in the dynamic viscosity

master-curve for a binder at a reference temperature of 4 °C (39.2 °F). The effect is most

significant at high temperatures (low frequency) but plays a role in pavement performance at all

practical temperatures. The increase in log viscosity with oxidation is linear and has no bound

within the practical limits encountered by binder during a normal pavement life.

Figure 2-2 shows the increase in low shear-rate dynamic viscosity (η0*) measured at

60 °C (140 °F) versus aging time at 60 °C (140 °F) and atmospheric air pressure for two binders.

These data were obtained in thin films, and thus the hardening rates reflected by the slope of

these lines are higher than those that occur in the field, but the effect and ultimate result that is

dependent on binder type is clear nonetheless.

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10 6

10 7

10 8

10 9

10 10

10 11

10 12

10 -9 10 -7 10 -5 10 -3 10 -1 10 1 10 3

112 hr216 hr

η∗ (p

oise

)

Reduced Angular Frequency (rad/s)

Reference Temperature: 4 oC

SHRP AAB-1 Air B lowing: 93.3 oC

Figure 2-1. Master-Curve for SHRP AAB-1 at Two Aging Times

(°F = 32 + 1.8(°C)).

103

104

105

0 50 100 150 200 250

AAB-1 (Unaged)AAB-1 (RTFOT Aged)

AAB-1 (RTFOT plus 60 oC Aged)AAG-1AAG-1 (RTFOT Aged)

AAG-1 (RTFOT plus 60 oC Aged)

η0

* (60

°C

) (p

oise

)

Aging Time (60 oC, day)

Figure 2-2. Effect of Aging on Low Shear-Rate Limiting Viscosity

(°F = 32 + 1.8(°C)).

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Effect of Aging on Low-Temperature Superpave Performance Grade

Viscosity is inversely related to the m-value in the Superpave low-temperature

performance grade for binders and elastic modulus is related to stiffness. Thus as binders age, m

decreases and stiffness increases. This increase in stiffness (and decrease in m) results in a

deterioration of the low-temperature grade as a binder oxidizes (48). Figure 2-3 shows this

deterioration that results from extended exposure to long-term aging in the Pressure Aging

Vessel (PAV). Similar effects occur due to aging at pavement field conditions.

-32

-30

-28

-26

-24

-22

-20

-18

-16

-10 0 10 20 30 40 50

AAF-1AAS-1Exxon AC-10Exxon AC-20Shell AC-20

Con

tinuo

us B

ott

om G

rade

(o C)

PAV Aging Time in hours @ 100oC, 20 atm air Figure 2-3. Continuous Bottom Grade as a Function of PAV Aging Time

(°F = 32 + 1.8(°C)).

Effect of Aging on Ductility and Shear Properties

One of the significant results from the literature is that ductility at 15 °C (59 °F) relates

well to pavement performance (49, 50). According to these studies, when the ductility of a

binder decreases to a minimum value in the range of about of 3 to 5 cm (1.18 to 1.98 inches) (at

an extension rate of 1 cm/min (0.39 inches/min)), the pavement condition tends to suffer from

fatigue cracks. CMAC researchers have related this ductility to the dynamic shear rheometer

(DSR) loss (G’’) and storage moduli (G’). As these moduli increase, the binder breaks at smaller

values of strain (loss of ductility) due to higher values of stress.

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This correlation between ductility and the DSR function G′/(η′/G′) is shown in Figure 2-4

for some 20 conventional binders in the low ductility region thought to be near HMAC pavement

failure (51). The DSR function increases and the ductility decreases with oxidative aging.

TxDOT Project 0-1872 evaluated the correlation between this DSR function and field

performance (52).

1

1 0

1 0 -5 1 0 -4 1 0 -3 1 0 -2 1 0 -1

Duc

tilit

y (c

m) (

15 °

C, 1

cm

/min

)

G '/ (η '/G ') (M P a /s ) (1 5 °C , 0 .0 0 5 r a d /s )

Figure 2-4. Ductility versus DSR Function G’/(η’ /G’) (°F = 32 + 1.8(°C)).

Hypothetical Mechanisms

Based on the results described, CMAC researchers hypothesize a correlation between

oxidative aging and pavement failure by two mechanisms:

• Increased stresses under load (compared to new pavements) result from a decreased

ability to flow and an increased elastic stiffness, both leading to cracking.

• A decreased ability to self heal results in a decrease in fatigue life.

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Data described in this section lead to the following conclusion: oxidative aging produces

a material that is more susceptible to fatigue cracking or other distress that occurs later in the life

of the pavement. Consequently, an approach that predicts mixture fatigue resistance must be

sensitive to changes in binder properties that occur due to oxidative aging. These changes vary

for binder types that are different chemically and will thus exhibit different physical properties

over time depending on the effects of oxidation. Assessment of the impact of aging on HMAC

mixture fatigue resistance and the ability of different approaches to incorporate this effect in

predicting fatigue life is therefore important and thus selected as part of this project. Binder tests

and results are discussed in Chapters 8 through 11.

SELECTED FATIGUE ANALYSIS APPROACHES

Based on this extensive literature review and subsequent consultation with TxDOT

project personnel, the research team selected the following fatigue analysis approaches for

comparative evaluation in this project:

(1) The mechanistic empirical with flexural bending beam fatigue testing.

(2) The calibrated mechanistic with Surface Energy measurements.

(3) The calibrated mechanistic without surface energy measurements.

(4) The proposed NCHRP 1-37A 2002 Pavement Design Guide with dynamic modulus

testing.

These approaches together with binder aging effects are discussed in more detail in

Chapters 4, 5, 6, 7, and 8, respectively. Binder-mixture characterization that relates binder

oxidative aging to HMAC mixture fatigue properties is presented in Chapter 9.

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SUMMARY

The following bullets summarize the key points from the information search:

• Of the positive responses received, the field survey questionnaire indicated that the majority

of the DOTs use Superpave, mechanistic empirical, AASHTO, Asphalt Institute, and

visco-elastic continuum-damage analysis for their fatigue mixture design, analysis, and/or

structural design check with laboratory tests including the bending beam, dynamic modulus,

indirect tension, uniaxial fatigue, moisture sensitivity, and retained indirect tensile strength.

• A detailed literature review indicated that the major disadvantage of most ME approaches are

the lengthy test programs and the fact that these approaches are phenomenologically or

empirically based and often assume HMAC linear elastic behavior.

• With advances in computer technology, there has been a drive towards more simple and

realistic calibrated mechanistic approaches that utilize continuum micro-mechanics with

fracturing and healing as the two primary mechanisms governing HMAC fatigue damage.

Utilization of finite element analysis provides HMAC modeling the potential to include

visco-elastic behavior while calibration constants are used to realistically simulate field

conditions.

• Binder oxidative aging has a significant impact on HMAC pavement fatigue performance

primarily in terms of the HMAC mixture’s resistance to fracture under traffic loading and

ability to heal. The inclusion of aging in HMAC fatigue mixture designs is profoundly

significant.

• Four fatigue analysis approaches: ME, CMSE, CM, and the proposed NCHRP 1-37A 2002

Pavement Design Guide, were selected for comparative evaluation and subsequent

recommendation to TxDOT. This evaluation and recommendation are discussed in this

interim report.

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CHAPTER 3 EXPERIMENTAL DESIGN

The research methodology for this project involved an information search (discussed in

Chapter 2) and subsequent selection of fatigue analysis approaches, drafting an experimental

design program, laboratory testing, and subsequent data analysis. This chapter discusses the

experimental design including materials selection and the corresponding specimen fabrication

protocols and aging conditions. Field conditions in terms of the selected pavement structures,

traffic, and environmental conditions are also presented. Laboratory testing including the

appropriate fatigue analysis approaches and binder-mixture characterization are discussed in

Chapters 4 through 9, respectively.

HMAC MIXTURES AND MIX-DESIGN

HMAC mixtures commonly used by TxDOT include Type C, Coarse Matrix High Binder

(CMHB)-Type C, CMHB-Type F, Type A, Type B, Type D, Type F, Superpave, Stone Mastic

Asphalt (SMA), Stone Filled Mixture, and Porous Friction Course (PFC) (53). Type C and

CMHB-Type C are the most common. More specialized mixtures include the SMA and stone

filled designs developed to provide superior rutting performance.

Aggregates generally include limestone, igneous, and gravel characterized and blended to

typical TxDOT or Superpave standards. Among the Performance-Graded (PG) binders used by

TxDOT, notable ones include PG 58-22, PG 64-22, PG 70-22, and PG 76-22 for the

environmental conditions in Texas.

For this project, the research team selected two commonly used TxDOT HMAC mixtures

for comparative fatigue performance evaluation. These were basic TxDOT Type C and rut

resistant Superpave HMAC mixtures, defined as the Bryan (BRY) and Yoakum (YKM)

mixtures, respectively, to represent the districts where the mix designs were obtained. Note that

development of mix designs was not part of this project.

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The Bryan Mixture – Basic TxDOT Type C (PG 64-22 + Limestone)

The Bryan HMAC mixture was designed using standard TxDOT gyratory design

protocols from the Bryan District (54). This mixture consists of a performance-graded PG 64-22

binder mixed with limestone aggregates to produce a dense-graded TxDOT Type C mixture. The

aggregate gradation curve for this mixture is shown in Figure 3-1. This mixture was used on

highways US 290 and SH 47 in the Bryan District (54).

0

20

40

60

80

100

0 1 2 3 4 5

Sieve Size (k0.45)

% P

assi

ng

Specification Limits

Figure 3-1. Limestone Aggregate Gradation Curve for TxDOT Type C Mixture.

The PG 64-22 binder was supplied by Eagle Asphalt, and the limestone aggregate was

supplied by Colorado Materials, Inc. from its Caldwell plant. The mix design was 4.6 percent

binder content by weight of aggregate (4.4 percent by weight of total mix) with a HMAC

mixture theoretical maximum specific gravity of 2.419 (54). The target specimen fabrication air

void (AV) content was 7±0.5 percent to simulate after in situ field construction and trafficking

when fatigue resistance is critical.

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The Yoakum Mixture – Rut Resistant 12.5 mm Superpave (PG 76-22 + Gravel)

The Yoakum HMAC mixture from the Yoakum District was a 12.5 mm Superpave

mixture designed with a PG 76-22 binder and crushed river gravel. This mixture was used on US

Highway 59 near the City of Victoria in Jackson County and is considered a rut resistant

mixture. This type of HMAC mixture was selected to examine its fatigue properties consistent

with the title and motivation of this project.

The binder and aggregates were sourced from Eagle Asphalt (Marlin Asphalt), Inc. and

Fordyce Materials, respectively. Unlike PG 64-22, PG 76-22 is a modified binder with about 5

percent styrene-butadiene-styrene (SBS) polymer.

In addition to the crushed river gravel, the Yoakum mixture used 14 percent limestone

screenings and 1 percent hydrated lime. Figure 3-2 shows the combined dense gradation of the

Yoakum river gravel.

0

20

40

60

80

100

0 1 2 3 4

Size Size (k0.45)

% P

assi

ng

Restricted ZoneSpecification Limits

Figure 3-2. Gravel Aggregate Gradation Curve for Rut Resistant 12.5 mm Superpave

Mixture.

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The mix design was 5.6 percent binder content by weight of aggregate (5.3 percent by

weight of total mix) with a HMAC mixture theoretical maximum specific gravity of 2.410. Like

the Bryan mixture, the target specimen fabrication AV for the Yoakum HMAC mixture was

7±0.5 percent.

Material Properties for the Binders

Laboratory characterization of the binder materials based on the AASHTO PP1, PP6,

T313, and T315 test protocols produced the results shown in Figures 3-3 through 3-5 (55, 56).

These results represent mean values of at least two binder test samples.

Note that for most of the binder test results, metric units are used consistent with the PG

specifications used by TxDOT for binders (55, 56). English (U.S.) units or unit conversions are

provided in parentheses to meet TxDOT requirements for other units including length and

temperature.

100

1,000

10,000

52 58 64 70 76 82 88

Test Temperature, oC

G*/

Sin

(del

ta), P

asca

l

52 58 64 70 76 82 88

High Temperature PG Grade

PG 64-22PG 76-22

Threshold ≥ 1,000 Pascal

Figure 3-3. Binder High Temperature Properties – G*/Sin (delta) (Pascal)

(°F = 32 + 1.8(°C)), (delta ≅ δ).

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100

1,000

-24 -18 -12 -6

Test Temperature, oC

Cre

ep S

tiffn

ess,

MPa

-34 -28 -22 -16

Low Temperature PG Grade

PG 64-22PG 76-22

Threshold ≤ 300 MPa

Figure 3-4. Binder Low Temperature Properties – Flexural Creep Stiffness (MPa)

(°F = 32 + 1.8(°C)).

0.2

0.3

0.4

-24 -18 -12 -6

Test Temperature, oC

m-v

alue

-34 -28 -22 -16

Low Temperature PG Grade

PG 64-22PG 76-22

Threshold ≥ 0.30

Figure 3-5. Binder Low Temperature Properties (m-value)

(°F = 32 + 1.8(°C)).

These verification results shown in Figures 3-3 through 3-5 indicate that the binders meet

the PG specification consistent with the material properties for PG 64-22 and PG 76-22 binders

(55, 56).

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Table 3-1 shows the measured intermediate temperature properties of the binders at 25 °C

(77 °F) in terms of the complex shear modulus (G*) and the phase angle (δ). The results

represent average values of three replicate binder-sample tests. These properties quantify the

binders’ resistance to fatigue associated cracking. As shown in Table 3-1, both the PG 64-22 and

PG 76-22 met the required maximum specified threshold value of a G* Sin δ of 5,000 kPa

(55, 56).

Table 3-1. Intermediate Temperature Properties of the Binders at 25 °C (77 °F).

Average Value Binder

δ (°) G*Sin δ (kPa)

Standard Deviation of G*Sin δ

(kPa)

CV (G*Sin δ) (%)

PG Specification

(kPa)

PG 64-22 65 600 10.91 1.82 ≤ 5000

PG 76-22 62 1019 70 6.90 ≤ 5000

Note that these measured binder properties also constitute input parameters for the

proposed NCHRP 1-37A Pavement Design Guide Level 1 analysis discussed in subsequent

chapters. These material property results also indicate that, as expected, the complex shear

modulus and flexural stiffness of the modified PG 76-22 binder at any test temperature is

relatively higher than that of the PG 64-22.

Material Properties for the Aggregates

Material properties for the aggregates listed in Table 3-2 indicate that the aggregate meets

the specification consistent with the respective test methods shown in the table (57). The bulk

specific gravity for the combined aggregates was 2.591 and 2.603 for limestone and gravel,

respectively.

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Table 3-2. Aggregate Properties.

Test Parameter Limestone Gravel Specification Test Method

Soundness 18% 20% ≤ 30% Tex-411-A

Crushed faces count

100% 100% ≥ 85% Tex-460-A

Los Angeles (LA) abrasion 28% 25% ≤ 40% Tex-410-A

Sand equivalent 74% 77% ≥ 45% Tex-203-F

HMAC SPECIMEN FABRICATION

The basic HMAC specimen fabrication procedure involved the following steps: aggregate

batching, binder-aggregate mixing, short-term oven aging (STOA), compaction, sawing and

coring, and finally volumetric analysis to determine the AV. These steps are briefly discussed in

this section.

Aggregate Batching

Aggregates were batched consistent with the gradations shown in Tables 3-3 and 3-4,

which correspond to those shown in Figures 3-1 and 3-2, respectively.

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Table 3-3. Limestone Aggregate Gradation for TxDOT Type C Mixture.

Sieve Size TxDOT Specification (53)

mm Upper Limit (%) Lower Limit (%)

% Passing

5/8″ 15.9 100 98 100.0

1/2″ 12.5 100 95 100.0

3/8″ 9.5 85 70 84.8

#4 4.75 63 43 57.9

#10 2.0 40 30 36.9

#40 0.425 25 10 19.0

#80 0.175 13 3 5.0

#200 0.075 6 1 1.0

Table 3-4. Gravel Aggregate Gradation for 12.5 mm Superpave Mixture.

Sieve Size TxDOT Specification (53)

mm Upper Limit (%) Lower Limit (%)

% Passing

3/4″ 19.00 100 -- 100.01/2″ 12.50 100 90 94.63/8″ 9.50 90 81.0

#4 4.75 54.4#8 2.36 58 28 32.9

#16 1.18 22.4#30 0.60 16.2#50 0.30 11.0

#100 0.150 7.6#200 0.075 10 2 5.5

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Mixing, Short Term Oven-Aging, Compaction, and Air Voids

The HMAC mixture mixing and compaction temperatures shown in Table 3-5 are

consistent with the TxDOT Tex-205-F and Tex-241-F test specifications for PG 64-22 and

PG 76-22 binders (57). Prior to binder-aggregate mixing, the limestone and gravel aggregates

were pre-heated to a temperature of 144 °C (291 °F) and 163 °C (325 °F), respectively, for at

least 4 hrs to remove any moisture. The binder was also heated at the mixing temperature for at

most 30 minutes before mixing to liquefy it.

Table 3-5. HMAC Mixture Mixing and Compaction Temperatures.

HMAC Mixture Temperature (°C) Process

Bryan Mixture Yoakum Mixture

Aggregate pre-heating 144 (291 °F) 163 (325 °F)

Binder-aggregate mixing 144 (291 °F) 163 (325 °F)

4 hrs short-term oven aging 135 (275 °F) 135 (275 °F)

Compaction 127 (261 °F) 149 (300 °F)

HMAC mixture STOA lasted for 4 hrs at a temperature of 135 °C (275 °F), consistent

with the AASHTO PP2 standard aging procedure for Superpave mixture performance testing

(58). STOA simulates the time between HMAC mixing, transportation, and placement up to the

time of in situ compaction in the field (58). Note that the acronym AASHTO PP2 is also used

synonymously with the acronym STOA in this interim report.

Gyratory Compaction

All the cylindrical specimens for the Dynamic Modulus and CMSE/CM tests were

gyratory compacted using the standard Superpave Gyratory Compactor (SGC) shown in Figure

3-6. Compaction parameters were 1.25° compaction angle and 600 kPa (87 psi) vertical pressure

at rate of 30 gyrations per minute.

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Figure 3-6. Superpave Gyratory Compactor.

Kneading Beam Compaction

Researchers compacted beam specimens for the flexural bending beam fatigue tests using

the linear kneading compactor shown in Figure 3-7 up to the target AV content consistent with

the specified beam thickness at a maximum compaction pressure of 6900 kPa (1000 psi)

(11, 12).

Figure 3-7. Linear Kneading Compactor.

All HMAC specimens were compacted to a target AV content of 7±0.5 percent, as stated

previously, to simulate after in situ field construction and trafficking when fatigue resistance is

critical.

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Sawing, Coring, Handling, and Storage

Cylindrical specimens were gyratory compacted to a size of 165 mm (6.5 inches) height

by 150 mm (6 inches) diameter, while actual test specimens were sawn and cored to a 150 mm

(6 inches) height and 100 mm (4 inches) diameter. Beam specimens were kneading compacted to

a size of 457 mm (18 inches) length by 150 mm (6 inches) width by 63 mm (2.5 inches)

thickness, and test specimens were sawn to a 380 mm (15 inches) length by 63 mm (2.5 inches)

width by a 50 mm (2 inches) thickness (11). Figure 3-8 shows the dimensions of the final test

specimens (where 1 mm ≅ 0.039 inches).

150 mm

100 mm

380 mm

50 mm

Width = 63 mm

Beam

Cylindrical

Figure 3-8. Laboratory Test Specimens (Drawing not to Scale)

(1 mm ≅ 0.039 inches).

After the specimens were sawn and cored, volumetric analysis based on the fundamental

principle of water displacement was completed to determine the actual specimen AV. HMAC

specimens that did not meet the target AV content were discarded or used as dummies in trial

tests. In total, a cylindrical specimen took approximately 40 hrs to fabricate while a beam

specimen, because of the difficulty in sawing, took an additional 5 hrs. While beam specimens

require delicate handling, the cylindrical specimens are not as sensitive to handling. Prior to

laboratory testing, specimens were generally stored on flat surfaces in a temperature-controlled

room at approximately 20±2 °C (68±36 °F).

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BINDER AND HMAC MIXTURE AGING CONDITIONS

Researchers selected three aging conditions listed in Table 3-6 for this project for both

the binder and HMAC compacted specimens. Consistent with the Superpave procedure, all

HMAC mixtures were subjected to 4 hrs STOA, as discussed previously, prior to the simulated

aging period for the three selected aging conditions.

Table 3-6. Aging Conditions for Binders and HMAC Compacted Specimens.

Aging Condition

@ 60 °C (140 °F)

Description Comment

0 months Simulates time period just after in situ field construction at the end of compaction (58)

3 months Simulates 3 to 6 years of Texas environmental exposure (52)

6 months Simulates 6 to 12 years of Texas environmental exposure (52)

All HMAC mixtures

(prior to compaction)

were subjected to 4 hrs

STOA (AASHTO PP2).

The aging process for HMAC specimens involved keeping the compacted specimens in a

temperature-controlled room at 60 °C (140 °F) and at the same time allowing the heated air to

circulate freely around the specimens. This allowed for accelerated oxidative aging of the binder

within the HMAC specimens. An aging temperature of 60 °C (140 °F) was selected to accelerate

aging because this temperature realistically simulates the critical pavement service temperature

in Texas for HMAC aging. Based on previous research, the process also simulates the field

HMAC aging rate (52). Chapter 8 discusses the aging process for the binder in detail.

Figure 3-9 is a schematic illustration of the HMAC specimen aging conditions considered

in each respective fatigue analysis approach. The NCHRP 1-37A 2002 Pavement Design Guide

software encompasses a Global Aging Model that takes into account the aging effects, which are

discussed in Chapter 7. Therefore, it was deemed unnecessary to test aged specimens for the

proposed NCHRP 1-37A 2002 Pavement Design Guide fatigue analysis.

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ME

, CM

SE, &

CM

All HMAC Mixtures:

Subjected to AASHTO PP2 @ 135 °C for 4 hrs

Age HMAC compacted specimens @ 60 °C for 0 months

(Total aging period = PP2 + 0 months)

Age HMAC compacted specimens @ 60 °C for 3 months

(Total aging period = PP2 + 3 months)

Age HMAC compacted specimens @ 60 °C for 6 months

(Total aging period = PP2 + 6 months)

Des

ign

Gui

de

Glo

bal A

ging

Mod

el

Figure 3-9. Fatigue Analysis Approaches and HMAC Mixture Aging Conditions

(°F = 32 + 1.8(°C)).

HYPOTHETICAL FIELD PAVEMENT STRUCTURES AND TRAFFIC

Table 3-7 displays a list of the five selected TxDOT pavement structures (PS) and five

associated traffic levels ranging between 0.25 to 11.00 × 106 equivalent single axle loads

(ESALs) that were considered in this project. These pavement structures represent actual

material properties and layer thicknesses that are commonly used on TxDOT highways (60).

Typical traffic conditions consisted of an 80 kN (18 kip) axle load, 690 kPa (100 psi) tire

pressure, 97 km/hr (60 mph) speed, and about 10 to 25 percent truck traffic over a design life of

20 years (60). In Table 3-7, PS# 5 represents the actual pavement structure where the Bryan

mixture was used.

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Table 3-7. Selected Pavement Structures and Traffic.

Material Type, Layer Thickness, and Elastic Modulus PS# Surfacing Base Subbase Subgrade

Traffic ESALs

% Trucks

1 HMAC, 6 inches, 500,000 psi

Flex, 14 inches*, 28,000 psi**

- 9000 psi 5,000,000 25

2 HMAC, 2 inches, 500,000 psi

Flex, 10 inches, 60,000 psi

Lime stabilized, 6 inches, 35,000 psi

12,400 psi 1,399,000 23.7

3 HMAC, 2 inches, 500,000 psi

Asphalt stabilized, 7 inches, 500,000 psi

Flex, 8 inches, 24,000 psi

Silt-clay, 9600 psi 7,220,000 13

4 HMAC, 2 inches, 500,000 psi

Flex, 6 inches, 50,000 psi

Stabilized subgrade, 5 inches, 30,000 psi

10,000 psi 390,000 10.7

5 US 290 HMAC, 4 inches, 500,000 psi

Cemented, 14 inches, 150,000 psi

- 15,000 psi 10,750,000 15.2

*1 inch ≅ 25.4 mm. ** 1 psi ≅ 0.0069 MPa

ENVIRONMENTAL CONDITIONS

Figure 3-10 shows five Texas environmental zones based on annual precipitation, annual

freezing index, and the number of wet days and freeze/thaw days (60). As shown in Figure 3-10,

the TxDOT districts have been grouped into five environmental zones namely; Dry-Cold (DC),

Wet-Cold (WC), Dry-Warm (DW), Wet-Warm (WW), and Moderate.

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Figure 3-10. Texas Environmental Zoning (60).

The italicized environmental zones (DC, WW, and DW) in Figure 3-10 indicate zones that

are critical to alligator (fatigue) cracking according to the TxDOT Pavement Management

Information System (PMIS) report (61). Based on this PMIS report, 20 to 100 percent of the

PMIS pavement sections in these locations exhibited alligator (fatigue) cracking.

AMA

SAT

LRD

PHR

CRP

YKM

HOU ELP

ODA

SJT AUS

WAC BWD

LBB ABL

CHS WFS

BMT

LFK

ATL FTW

DAL

TYL

PAR

Dry-Warm (DW)

Dry-Cold (DC)

Wet-Cold (WC)

Wet-Warm (WW)

Moderate (M)

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Pavement material performance depends on both traffic and environment. It is therefore

not uncommon that for a given design traffic level, a material that performs well in a particular

environment may perform poorly in a different environmental location. Material properties for

pavement design and performance evaluation are thus generally characterized as a function of

environmental conditions.

HMAC, for instance, is very sensitive to temperature changes, while unbound materials

in the base, subbase, or subgrade are generally more sensitive to moisture variations. Most often,

the HMAC elastic modulus is characterized as a function of seasonal or monthly temperature

variations, with the critical pavement temperature being at the mid-depth or two-thirds depth

point in the HMAC layer. This pavement temperature generally exhibits a decreasing trend with

depth. The subgrade elastic modulus is normally characterized as a function of the seasonal

moisture conditions, with the wettest period of the year as the worst-case scenario assuming a

conservative design approach. Note also that water seepage through cracks and/or accumulation

in AV can accelerate damage, including fatigue cracking in HMAC materials.

In this project, two environmental conditions, WW and DC were considered (Figure 3-

10). WW and DC are the two extreme Texas weather conditions the research team considered to

have a significant impact on HMAC mixture fatigue performance. In fact, the 2003 TxDOT

“Condition of Texas Pavements PMIS Annual Report” indicates that highway pavements in

these environmental locations (WW and DC) are comparatively more susceptible to fatigue-

associated cracking (61).

RELIABILITY LEVEL

For this project, the research team selected and utilized a reliability level of 95 percent.

This is a typical value used for most practical HMAC pavement designs and analyses. In

statistical terms, this means that for a given test or assessment criteria, there is 95 percent pass

expectance or data accuracy, and that up to 5 percent failure or result inaccuracy is anticipated

and tolerable. In simpler terms, for a 95 percent reliability level, it means that the acceptable risk

level is 5 percent.

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ELSYM5 STRESS-STRAIN ANALYSIS

For the five selected hypothetical PSs and environmental conditions (WW and DC)

considered, elastic ELSYM5 stress-strain computations were adjusted based on FEM simulations

to account for the HMAC visco-elastic behavior (62, 63).

ELSYM5 Input and Output Data

The bullets below summarize the typical input data requirement for ELSYM5 analysis:

• pavement structure (i.e., number of layers and layer thicknesses),

• material properties (i.e., elastic modulus and Poisson’s ratio), and

• Traffic loading (i.e., axle load and tire pressure).

Table 3-7 displayed the PSs and the respective elastic moduli used for ELSYM5 analysis

in this project. The axle load and tire pressure used were as discussed previously, 80 kN and

690 kPa. Typical Poisson’s ratios used by the researchers in the analysis were 0.33, 0.40, and

0.45 for the HMAC layer, the base, and subgrade, respectively (64).

The basic output response parameters from the ELSYM5 computational analysis include

the stresses, strains, and deformations. The strain response parameters were, however, adjusted

according to FEM simulations discussed in the subsequent text to account for HMAC

visco-elastic behavior.

These tensile (εt) and shear (γ) strains constitute input parameters for the ME, CMSE, and

CM fatigue analysis, respectively, discussed in Chapters 4 through 6. Stress-strain computations

for the proposed NCHRP 1-37A 2002 Pavement Design Guide (Chapter 7) is built into the

analysis software.

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FEM Strain-Adjustment

The FEM strain-adjustment factor for elastic strain analysis to account for HMAC

visco-elastic behavior was determined as follows:

5)(

ELSYM

FEMiVEadj Strain

StrainS = (Equation 3-1)

where:

Sadj(VE) = FEM strain-adjustment factor for HMAC visco-elastic behavior

StrainFEM = Strain (εt or γ) computed via FEM analysis (mm/mm)

StrainELSYM5 = Strain (εt or γ) computed via ELSYM5 analysis (mm/mm)

Subscript i = Stands for εt or γ

For this project, Sadj(VE) values of 1.25 and 1.175 were used for εt and γ, respectively,

based on the previous FEM work by Park (63, 65). Note that while it is possible that these

visco-elastic adjustments may vary for different mixtures, the adjustment from layered elastic to

elasto-viscoplastic was assumed to be constant across both mixtures in this project. In addition,

the elastic moduli values at 0 months aging for these two mixtures did not vary significantly.

Thus for each computed ELSYM5 strain (εt and γ) for the PSs shown in Table 3-7, the Sadj(VE)i

was applied as follows:

( ) ( 5) ( 5)1.25tt adj VE e t ELSYM t ELSYMSε ε ε= × = (Equation 3-2)

( ) ( 5) ( 5)1.175adj VE ELSYM ELSYMS γγ γ γ= × = (Equation 3-2)

An example of the resulting strains (εt and γ) for the PSs shown in Table 3-7 for both

WW and DC environments is shown in Table 3-8.

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Table 3-8. Computed Critical Design Strains.

WW Environment DC Environment PS#

Tensile strain

(εt)

Shear strain

(γ)

Tensile strain

(εt)

Shear strain

(γ)

1 1.57 × 10-4 1.56 × 10-2 1.51 × 10-4 1.51 × 10-2

2 2.79 × 10-4 1.98 × 10-2 2.71 × 10-4 1.89 × 10-2

3 2.73 × 10-4 1.91 × 10-2 2.66 × 10-4 1.86 × 10-2

4 2.89 × 10-4 2.06 × 10-2 2.78 × 10-4 1.96 × 10-2

5 0.98 × 10-4 1.41 × 10-2 0.91 × 10-4 1.46 × 10-2

SUMMARY

Salient points from this chapter are summarized as follows:

• Two commonly used TxDOT HMAC mixtures, Bryan (PG 64-22 + limestone) and Yoakum

(PG 76-22 + gravel) mixtures were selected for fatigue analysis in this project. Bryan is a

normal basic TxDOT Type C HMAC mixture, while Yoakum is a Rut Resistant 12.5 mm

Superpave HMAC mixture. Both the binder and aggregate material properties were

consistent with the Superpave PG and TxDOT standards.

• Two laboratory compactors, the standard SGC and kneading beam, were utilized for

compacting cylindrical and beam HMAC specimens, respectively. The target specimen

fabrication AV content was 7±0.5 percent to simulate the in situ AV field compaction after

construction and trafficking when fatigue resistance is critical.

• Three aging conditions for both binders and HMAC mixtures at a critical temperature of

60 °C (140 °F) were selected to investigate the effects of oxidative aging on binder and

HMAC mixture fatigue properties, including fatigue life. These aging conditions were 0, 3,

and 6 months that simulate up to 12 years of Texas environmental-field HMAC aging.

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• Five commonly used TxDOT HMAC pavement structures with corresponding traffic levels

of 0.25 to 11.00 million ESALs and 10 to 25 percent truck traffic were selected for analysis.

Using layered elastic analyses (ELSYM5) and adjusting based on FEM simulations, tensile

and shear strains within the pavement HMAC layer were determined and utilized as the

failure load-response parameters associated with fatigue cracking when predicting the

HMAC mixture fatigue resistance.

• Two Texas environmental conditions (Wet-Warm and Dry-Cold) critical to fatigue

associated (alligator) cracking in HMAC pavements were selected for the analysis.

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CHAPTER 4 THE MECHANISTIC EMPIRICAL APPROACH

This chapter discusses the mechanistic empirical approach for HMAC pavement fatigue

analysis including the fundamental theory, input/output data, required flexural bending beam

laboratory testing, failure criteria, analysis procedure, and variability.

FUNDAMENTAL THEORY

The selected SHRP A-003A ME approach in this project utilizes the flexural bending

beam fatigue test (third-point loading) and considers bottom-up cracking to determine an

empirical fatigue relationship of the simple power form shown in Equation 4-1 (25).

2

1kkN −= ε (Equation 4-1)

where:

N = Number of load cycles to fatigue failure

ε = Applied tensile strain (mm/mm)

ki = Laboratory determined material constants

The SHRP A-003A fatigue analysis approach incorporates reliability concepts that

account for uncertainty in laboratory testing, construction, and traffic prediction; and considers

environmental factors, traffic loading, and pavement design. The SHRP A-003A is the ME

fatigue analysis approach utilized in this project, and the BB testing to determine the HMAC

mixture fatigue empirical relationship shown in Equation 4-1 was based on the AASHTO

TP8-94 test protocol (59, 66). The AASHTO TP8-94 test protocol is discussed later in this

chapter.

HMAC specimen preparation by rolling or kneading wheel compaction is strongly

recommended as part of this ME approach to simulate the engineering properties of extracted

field pavement cores. Conditioning prior to testing to a representative or worst-case aging state is

also suggested.

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The AASHTO TP8-94 test protocol requires testing conditioned specimens at two

different controlled strain levels under sinusoidal repeated loading to generate an empirical

fatigue relationship, as shown in Equation 4-1 (59).

Determination of the experimental fatigue relationship, as expressed by Equation 4-1,

constitutes the empirical part of the ME approach of fatigue modeling of HMAC mixtures. This

empirical fatigue relationship (Equation 4-1) is then used in the design and analysis system

illustrated schematically in Figure 4-1.

ME FATIGUE ANALYSIS

Pavement structure

Pavement materials

Traffic

Environment

Trial HMAC mix

Nf (Mixture Fatigue Resistance) Nf(Demand)

Empirical fatigue relationship

Design strain

Shift factor

Temperature correction factor

Reliability multiplier (M)

Traffic ESALs

Nf ≥ M × Traffic ESALs

YES

NO

Final Fatigue Design

Figure 4-1. The ME Fatigue Design and Analysis System.

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The fatigue analysis system shown in Figure 4-1 evaluates the likelihood that the selected

design HMAC mixture will adequately resist fatigue cracking in a specific pavement structure

under anticipated in situ conditions including traffic and environment. The designer must,

however, select a specific level of reliability commensurate with the pavement site for which the

mixture will be utilized as well as the required level of service of the pavement structure.

A HMAC mixture is expected to perform adequately if the number of load repetitions

sustainable in laboratory testing after correcting for field conditions exceeds the number of load

repetitions anticipated in service. The design strain at which the pavement fatigue life must be

estimated using the empirical fatigue relationship developed based on laboratory test results is

often computed using a simple multilayer elastic theory. For this computation, the design strain

of interest is the maximum principal tensile strain at the bottom of the HMAC layer in the

specific pavement structure, assuming the bottom-up mode of fatigue cracking. The

determination of this field critical design tensile strain within a representative field pavement

structure at the bottom of the HMAC layer constitutes the mechanistic part of the ME approach.

INPUT/OUTPUT DATA

Table 4-1 summarizes the general ME fatigue analysis input and the expected output data

based on the SHRP A-003A approach and the AASHTO TP8-94 BB test protocol (59). These

parameters and their respective components are discussed in more detail in subsequent sections.

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Table 4-1. Summary of ME Fatigue Analysis Input and Output Data.

Source Parameter

Laboratory test data (HMAC mixture testing of beam specimens)

- Strain (εt) & stress - # of fatigue load cycles (N)

Analysis of laboratory test data

- Flexural stiffness or dissipated energy - Empirical fatigue relationship (N = f(εt))

Field conditions (design data)

- Pavement structure (layer thickness) - Pavement materials (elastic modulus & Poisson’s ratio) - Traffic (ESALs, axle load, & tire pressure) - Environment (temperature & moisture conditions) - Field correction/shift factors (i.e., temperature)

Computer stress-strain analysis

- Design tensile strain (εt) @ bottom of the top HMAC layer

Other - Reliability level (i.e., 95%) - Reliability multiplier (M)

OUTPUT - HMAC mixture fatigue resistance (Nf(Supply)) - Pavement fatigue life (Nf(Demand)) - Assessment of adequate or inadequate performance

LABORATORY TESTING

The BB fatigue test, including the test equipment, specimen setup, and data acquisition,

was conducted consistent with the AASHTO TP8-94 test procedure (11, 12). This section

summarizes the BB fatigue test protocol.

The BB Fatigue Test Protocol

The BB fatigue test consists of applying a repeated constant vertical strain to a beam

specimen in flexural tension mode until failure or up to a specified number of load cycles. In this

project, the test was strain controlled, and the input strain waveform was sinusoidal shaped,

applied at a frequency of 10 Hz. The BB device and the loading configuration are shown in

Figures 4-2 and 4-3, respectively.

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47

Figure 4-2. The Bending Beam (BB) Device.

0 0.2 0.4 0.6 0.8 1 1.2

Time, s

Stra

in

0.5F 0.5F

Deflection

Figure 4-3. Loading Configuration for the BB Fatigue Test.

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48

As evident in Figure 4-3, repeated vertical loading causes tension in the bottom zone of

the specimen, from which cracking will subsequently initiate and propagate, thus simulating

pavement fatigue failure under traffic loading. The test was conducted at two strain levels of

approximately 374 and 468 microstrains (i.e., an equivalence of 0.20 and 0.25 mm deflections,

respectively), consistent with the AASHTO TP8-94 test protocol to generate the required

material N-εt empirical relationship shown in Equation 4-1 (59). These test strain levels are

within the recommended AASHTO TP8-94 test protocol range to reduce test time while at the

same time capturing sufficient data for analysis.

A 10 Hz frequency (Figure 4-3) without any rest period was used for the test. The

average duration of each test was approximately 5 hrs. Note that the BB test time is inversely

proportional to the magnitude of the input strain wave. Testing can, however, be terminated

either when the initial application load response (stress) recorded at the 50th load cycle decreases

to 50 percent in magnitude or when a preset number of load cycles such as 100,000 is reached.

The former approach was used in this project.

Test Conditions and Specimens

HMAC is temperature sensitive, so the test was conducted in an environmentally

controlled chamber at a test temperature of 20±0.5 °C (68 ±32.9 °F), consistent with the

AASHTO TP8-94 test procedure (59). The minimum specimen conditioning time was 2 hrs.

However, specimens were actually preconditioned at 20 °C (68 °F) on a more convenient 12 hrs

overnight-time period. The test temperature was monitored and recorded every 600 s via a

thermocouple probe attached inside a dummy specimen also placed in the environmental

chamber. Figure 4-4 is an example of a temperature plot captured during the BB test at 20 °C

(68 °F).

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Tmean, 19.96

TLower Limit, 19.50

TUpper Limit, 20.50

19.00

19.50

20.00

20.50

21.00

0 6,000 12,000 18,000

Time, s

Tem

pera

ture

, oC

Figure 4-4. Example of Temperature Plot for the BB Test.

As evident in Figure 4-4, the average temperature for this particular test was 19.96 °C

(67.93 °F) with a coefficient of variation of 0.84 percent. Three replicate beam specimens were

tested for each strain level, so a complete BB test cycle for low and high strain level tests

required a minimum of six beam specimens per aging condition per mixture type.

Test Equipment and Data Measurement

A servo electric-hydraulic controlled material testing system (MTS) equipped with an

automatic data measuring system applied the sinusoidal input strain waveform. Actual loading of

the specimen was transmitted by the BB device shown in Figure 4-2, to which the beam

specimen is securely clamped.

Loading data were measured via the MTS load cell, and flexural deflections were

recorded via a single linear differential variable transducer (LVDT) attached to the center of the

specimen. During the test, load and flexural deformation data were captured electronically every

0.002 s. Figure 4-5 is an example of the output stress response from the BB test at 20 °C (68 °F)

based on a 374 test microstrain level.

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50

100

150

200

250

0 4,000 8,000 12,000 16,000

Time, s

Stre

ss, p

si

Figure 4-5. Example of Stress Response from BB Testing at 20 °C (68 °F)

(374 microstrain level).

FAILURE CRITERIA

For HMAC compacted specimens subjected to repeated flexural bending, failure is

defined as the point at which the specimen flexural stiffness is reduced to 50 percent of the initial

flexural stiffness (59, 66). This initial stiffness is generally defined as the specimen flexural

stiffness measured at the 50th load cycle. With this criterion, fatigue cracking was considered to

follow the bottom-up failure mode assuming a service temperature of 20 °C (68 °F).

ANALYSIS PROCEDURE

The ME fatigue analysis utilized in this project was a five-step procedure involving

laboratory test data analysis to determine the HMAC Nf-εt empirical relationship expressed by

Equation 4-1, computer stress-strain analysis to determine the design maximum εt within a

selected and representative pavement structure at the bottom of the HMAC layer, statistical

analysis to predict the design HMAC mixture fatigue resistance, determination of the required

pavement life, and finally, a design check for adequate performance. These analyses, which are

illustrated schematically in Figure 4-1, are discussed in this section.

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Step 1: Laboratory Test Data Analysis (N-εt Empirical Relationship)

Laboratory test data from the BB fatigue test, which is discussed subsequently, was

analyzed using the AASHTO TP8-94 calculation procedure. Equations 4-2 to 4-4 are the

fundamental basis for BB test data analysis (59).

t

tSεσ

= (Equation 4-2)

1

%50

%50 69315.0ln

−−=⎟⎠⎞

⎜⎝⎛

= bbA

S

N (Equation 4-3)

where:

S = Flexural stiffness (MPa)

σt = Maximum measured tensile stress per load cycle (kPa)

εt = Maximum measured tensile strain per load cycle (mm/mm)

N50% = Number of load cycles to failure during BB testing

S50% = Flexural stiffness at failure during BB testing (MPa)

A = Initial peak flexural stiffness measured at the 50th load cycle (MPa)

b = Exponent constant from log S versus log load cycles (N) plot

The solution of Equation 4-3 for two different input strain levels (i.e., low and high), and

a plot of the resultant N50% versus the respective applied εt on a log-log scale will generate the

required empirical fatigue relationship of the simple power form shown in Equation 4-1.

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Step 2: Stress-Strain Analysis, εt (Design)

Following establishment of the HMAC Nf-εt empirical relationship through laboratory

test data analysis, computer stress-strain analysis was executed to determine the actual maximum

design εt of a given pavement structure at the bottom of the HMAC layer. Input parameters for

this analysis include traffic loading, pavement structure (layer thicknesses), material properties,

and the desired response location, which in this project was (t – 0.01), where t is the thickness of

the top HMAC layer in inches (or mm, where 1 inch ≅ 25.4 mm). Traffic loading data include

the standard axle load (e.g., 80 kN [18 kip]), ESALs, and axle and tire configurations. Material

properties including the elastic modulus and Poisson’s ratio should be defined as a function of

the environment in terms of temperature and subgrade moisture conditions.

In this project, a user-friendly and simple multi-layer linear-elastic software, ELSYM5,

was used for εt computations at the bottom of the HMAC layer (62). Ideally, a FEM software

that takes into account the visco-elastic nature of the HMAC material is desired for this kind of

analysis. Consequently, adjustments were applied to the ELSYM5 linear-elastic analysis results,

consistent with the FEM adjustment criteria discussed in Chapter 3.

Step 3: Statistical Prediction of HMAC Mixture Fatigue Resistance, Nf(Supply)

Nf(Supply) is the laboratory design HMAC mixture fatigue resistance that was statistically

determined as a function of the design εt (ELSYM5 analysis) and the laboratory determined

empirical fatigue N-εt (Equation 4-1) relationship at a given reliability level. This is discussed in

great detail in the subsequent section.

While Nf(Supply) represents laboratory fatigue life, the final field fatigue life for this ME

approach in this project was obtained as expressed by Equation 4-4.

[ ]( )TCFNSF

TCFkSF

N Supplyfk

tif

)(2 ×

==−ε

(Equation 4-4)

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53

where:

TCF = Temperature conversion factor to laboratory test temperature

SF = Shift factor that accounts for traffic wander, construction variability, loading frequency, crack propagation, and healing

For simplicity, TCF and SF values of 1.0 and 19, respectively, were used in this project

(1, 2). Determination of these parameters generally requires local calibration to field conditions,

which was beyond the scope of this project.

Step 4: Determination of the Required Pavement Fatigue Life, Nf(Demand)

Nf(Demand) is the expected pavement fatigue life, which is representative of the actual

applied traffic loading. It is a function of the total traffic ESALs summed over the entire

pavement design life determined as expressed by Equation 4-5.

)()( DesignDemandf ESALsTrafficMN ×= (Equation 4-5)

where:

M = Reliability multiplier

In the ME fatigue analysis approach, the safety factor associated with a specified level of

reliability is often defined in terms of reliability multiplier (M) and applied to traffic demand

(i.e., ESALs) as shown in Equation 4-5 (1, 2). This factor accounts for mixture variability and

the anticipated uncertainties in traffic estimate (demand) and mixture fatigue resistance (supply)

and performance during service. For a reliability level of 95 percent, some studies have used an

M value of 3.57, and this was the value used in this study (1, 2).

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Step 5: Fatigue Design Check for Adequate Performance

A fatigue design check for adequate performance requires that the HMAC mixture

fatigue resistance be greater than or equal to the required pavement fatigue life as expressed by

Equation 4-6.

)(Demandff NN ≥ (Equation 4-6)

If Nf is less than Nf(Demand), a wide range of options including the following are available:

• redesigning the HMAC mixture by changing the binder content and/or type, AV,

aggregate type or gradation;

• redesigning the pavement structure by changing the layer thicknesses, for example;

• redesigning the underlying pavement materials including the subbase, base, and/or

subgrade,

• reducing the pavement design life; and/or

• allowing an increased risk of premature failure.

VARIABILITY, STATISTICAL ANALYSIS, AND Nf PREDICTION

Precision is inversely proportional to uncertainty/variability in a testing method. If N is

the measured fatigue life and f(supply)N is the predicted fatigue life at a given design strain level,

then the precision of the method (on a log scale) can be represented by the estimated variance of

[ ]f(supply)NLn as follows:

( )( ) ⎟

⎟⎠

⎞⎜⎜⎝

−−

++=∑

∗ 2

222 11

xxqxX

nss

py

(Equation 4-7)

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where:

y* = [ ]f(supply)NLn

2∗y

s = Estimated variance of [ ]f(supply)NLn

s2 = ( )[ ]NLnVar

n = Number of test specimens

X = Ln[in situ strain] at which [ ]f(supply)NLn must be predicted

x = Average Ln[test strain]

q = Number of replicate specimens at each test strain level

xp = Ln[strain] at the pth test strain level

A prediction interval for [ ]f(supply)NLn is another way of assessing the precision of the

prediction. If the resulting interval is narrow, there is little uncertainty in [ ]f(supply)NLn , and the

prediction is quite precise. An explicit formula for a 1-α prediction interval for the linear

regression exists as follows:

∗−−±+yn stbXa 2,2/1 α (Equation 4-8)

where:

a, b = The estimated intercept and the estimated slope of the least squares

line fitted on the ( ) ( )( )fNLnstrainLn , data

2,2/1 −− nt α = The t-critical value corresponding to the right tail probability of

2α of the t distribution with n-2 degrees of freedom 2

∗ys = The estimated variance of [ ]f(supply)NLn as given in Equation 4-7

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The estimated intercept and the estimated slope, a and b, respectively, can also be given

explicitly as follows:

xbya += (Equation 4-9)

and

( )( )( )∑

∑−

−−= 2xxq

yyxxqb

p

pp (Equation 4-10)

where:

yp = ( )NLn at the pth test strain level

y = Average ( )NLn

Note that the predicted fatigue life [ ]f(supply)NLn or the prediction interval estimate

[ ]∗∗ −−−− ++−+ynyn stbXastbXa 2,2/12,2/1 , αα can be back-transformed by taking ( )exp to provide

the estimates in the original scale, but the variance estimate 2∗y

s itself cannot be transformed in

the same manner.

In summary, Ln Nf(supply) values were predicted based on the least squares line regression

analysis. Next, a 95 percent Ln Nf prediction interval was estimated based on the selected 95

percent reliability level. The predicted value and the prediction interval estimate estimates for

Nf(supply) were then obtained by back-transformation. As another measure of variability, a

coefficient of variation (COV) of Ln Nf was computed based on the estimated standard deviation

for the predicted Ln Nf value and the predicted mean Ln Nf value.

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SUMMARY

This section summarizes the ME fatigue analysis approach as utilized in this project.

• The ME approach is mechanistic empirical and based on the fundamental concepts that

fatigue cracking in HMAC pavements occurs due to critical tensile strains (εt) at the bottom

of the HMAC layer and that the predominant mode of crack failure is bottom-up crack

growth.

• Laboratory determination of the experimental N-εt fatigue relationship (i.e., the ki constants)

constitutes the empirical part of the ME approach, and determination of the field critical

design εt within a representative field pavement structure at the bottom of the HMAC layer

constitutes the mechanistic part.

• The flexural bending beam fatigue test conducted at 20 °C (68 °F) and 10 Hz in sinusoidal

strain-controlled mode is the principal HMAC mixture fatigue characterization test for the

ME approach. Under this BB testing, kneading or rolling compacted beam specimens are

required.

• For HMAC compacted specimens subjected to repeated flexural bending, fatigue failure

according to the ME approach is defined as the number of repetitive load cycles at which the

specimen flexural stiffness is reduced to 50 percent of the initial flexural stiffness measured

at the 50th load cycle.

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CHAPTER 5 THE CALIBRATED MECHANISTIC APPROACH

WITH SURFACE ENERGY

In this chapter, the calibrated mechanistic approach with surface energy including the

fundamental theory, input/output data, laboratory testing, failure criteria, analysis procedure, and

variability is discussed.

FUNDAMENTAL THEORY AND DEVELOPMENT

HMAC is a complex composite material that behaves in a non-linear visco-elastic

manner, ages, heals, and requires that energy be stored on fracture surfaces as load-induced

damage in the form of fatigue cracking. Energy is also released from fracture surfaces during the

healing process. HMAC mixture resistance to fatigue cracking thus consists of two components,

resistance to fracture (both crack initiation and propagation) and the ability to heal, processes

that both change over time. Healing, defined as the closure of fracture surfaces that occurs

during rest periods between loading cycles, is one of the principal component of the laboratory-

to-field shift factor used in traditional empirical fatigue analysis. Prediction of fatigue life or the

number of cycles to failure (Nf) must account for this healing process that affects both the

number of cycles for microcracks to coalesce to macrocrack initiation (Ni) and the number of

cycles for macrocrack propagation through the HMAC layer (Np) that add to Nf. Both

components of mixture fatigue resistance or the ability to dissipate energy that causes primarily

fracture at temperatures below 25 °C (77 °F), called dissipated pseudo strain energy (DPSE), can

be directly measured in simple uniaxial tensile and compression tests (5-6, 43-44,67).

The CMSE approach is a micromechanical approach developed at Texas A&M

University based on the SHRP A-005 results (44-45). The approach characterizes HMAC

materials both in terms of fracture and healing processes, and requires only creep or relaxation

tests in uniaxial tension and compression, strength and repeated load tests in uniaxial tension,

and a catalog of fracture and healing surface energy components of binders and aggregates

measured separately.

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In this CMSE approach, HMAC behavior in fatigue is governed by the energy stored on

or released from crack faces that drive the fracture and healing processes, respectively, through

these two mechanisms of fracture and healing.

DPSE and pseudo strain are defined to quantify and monitor fracture and healing in

HMAC mixtures. DPSE in an undamaged non-linear visco-elastic material is expected due to

the viscous lag in material response. This pseudo strain energy is represented by the area in the

pseudo hysteresis loop of a measured stress versus calculated PS after correcting for

non-linearity, plotted as shown in Figure 5-1. Pseudo strain is determined by calculating the

expected stress in a linear visco-elastic material under damaged conditions and dividing by a

measured reference modulus (from the first stress cycle of a repeated load test), and a non-

linearity correction factor (ψ(t)). This ψ(t) is introduced to account for any non-linearity of the

undamaged visco-elastic material (68).

Any departure from the initial pseudo hysteresis loop requires additional dissipated

energy, indicating that fracture is occurring for temperatures less than 25 °C (77 °F). As fracture

progresses with additional load cycles, DPSE will increase, while the HMAC mixture stiffness

will decrease. The healing process, on the other hand, produces opposite results, with DPSE

decreasing and the HMAC mixture stiffness increasing.

Pseudo Strain (calculated)

Stress (measured)

Figure 5-1. Example of Hysteresis Loop (Shaded Area is DPSE).

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Monitoring of both DPSE and PS in repeated uniaxial tension tests is required in this

micromechanical CMSE approach. The relationship between DPSE and N is modeled using

either of two functional forms, linear logarithmic or simple power law, and calibrated using

measured data. In this project, the research team used the former functional form, linear

logarithmic.

These calibration coefficients and Paris’ Law fracture coefficients determined by

monitoring both DPSE and PS with microcrack growth are required to determine Ni for

macrocrack initiation at an average microcrack size of 7.5 mm (0.30 inches) (67, 69). This

calibration is required because the coefficients of the equation for microcrack growth are not

widely known as compared to those for macrocrack growth. The size and shape of a microcrack

is controlled by microscopic quantities such as mastic film thickness, aggregate particle size, and

the degree of bonding of crack-arresting obstacles dispersed in the mastic. Nevertheless,

microcrack growth is still controlled by the rate of change of DPSE and indicated by a reduction

in HMAC mixture stiffness.

Np for microcrack propagation is a function of the difference between fracture and

healing speed. This Np is primarily quantified in terms of Paris’ Law fracture coefficients

(A and n) and the shear strain. Fracture speed depends on material properties determined in

uniaxial tensile creep or relaxation and strength tests at multiple temperatures and total fracture

surface energy.

Healing occurs as a result of both short-term and long-term rates of rest periods, and

depends on traffic rest periods, healing surface energy components, and the material properties

measured in compression creep or relaxation modulus tests. Because the HMAC mixture healing

properties are climatic dependent, fatigue healing calibration constants must be used to account

for the climatic location of a given HMAC pavement structure (67). In determining the final

field Nf, an anisotropic shift factor (discussed subsequently) is also introduced to account for the

anisotropic nature of HMAC.

The surface energies of the binder and aggregate in HMAC are made up of contributions

from nonpolar short-range Lifshitz-van der Waals forces and longer-range polar acid-base forces

mainly associated with hydrogen bonding (68, 70-71).

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The polar acid-base surface energy is itself also a combination of the acid surface energy

and the base surface energy. These polar forces typical of hydrogen bonding take longer to form

and act perpendicular to the crack faces to actively pull them together, while the nonpolar tensile

short-range and short-lived Lifshitz-van der Waals forces act in the plane of the crack face to

form a contractile skin that resists healing (44-45, 68, 70-71).

The difference between the total fracture and healing surface energies lies in the

measurement of the individual surface energy components using carefully selected materials

with known surface energy component values. Fracture components are found when dewetting,

and healing components are determined when wetting (44-45, 68, 70-71).

Figure 5-2 is a schematic illustration of the CMSE design and analysis system. The figure

shows that if the predicted Nf is less the design traffic ESALs, possible options include the

following:

• modifying the pavement structure, materials, and reliability level; and/or

• changing the HMAC mix-design and/or material type;

• reducing the pavement design life; and/or

• allowing an increased risk of premature failure, i.e., reducing the reliability level.

In this CMSE approach, the design shear strain (Figure 5-2) computed within the HMAC

layer of the pavement structure for Np analysis constitutes the failure load-response parameter.

This critical design shear strain is determined at the edge of a loaded wheel-tire using either a

layered linear-elastic or visco-elastic model of material behavior characterization. The utilization

of calibration constants in modeling SFh, Ni, and Np constitutes the calibration part of the CMSE

approach. This calibration simulates the field mechanism of microcrack growth in the HMAC

layer thickness with respect to traffic loading and environmental conditions.

INPUT/OUTPUT DATA

Table 5-1 summarizes the general CMSE fatigue analysis input and the expected output

data. These parameters and their respective components are discussed in more detail in

subsequent sections.

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63

NO

CMSE FATIGUE ANALYSIS

Pavement structure

Pavement materials

Traffic

Environment

Reliability

Nf Prediction

HMAC mixture characterization properties (from lab test or existing data from catalog)

Calibration, healing, & regression constants

Paris’ Law coefficients

Microcrack length failure threshold value

Design shear strain

Temperature correction factors

Anisotropy and healing shift factors

HMAC mixture fatigue resistance

Reliability factor (Q)

Nf ≥ Q × Traffic

YES

Final Fatigue Design

Figure 5-2. The CMSE Fatigue Design and Analysis System.

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Table 5-1. Summary of CMSE Fatigue Analysis Input and Output Data.

Source Parameter

Laboratory test data (HMAC mixture testing of cylindrical specimens)

- Tensile stress & strain - Relaxation modulus (tension & compression) - Uniaxial repeated direct-tension test data (strain, stress, time,

& N) - Anisotropic data (vertical & lateral modulus) - Dynamic contact angle for binder surface energy (SE) - Vapor pressure and adsorbed gas mass for aggregate SE

Analysis of laboratory test data

- Tensile strength - Relaxation modulus master-curves (tension & compression) - Non-linearity correction factor - DPSE & slope of DPSE vs. Log N plot - SE (∆Gf & ∆Gh) for binder & aggregates - Healing indices - Healing calibration constants - Creep compliance - Shear modulus - Load pulse shape factor

Field conditions (design data)

- Pavement structure (layer thickness) - Pavement materials (elastic modulus & Poisson’s ratio) - Traffic (ESALs, axle load, & tire pressure) - Environment (temperature & moisture conditions.) - Field calibration coefficients - Temperature correction factor

Computer stress-strain analysis - Design shear strain (γ) @ edge of a loaded tire

Other Parameters

- Reliability level (i.e., 95%) - Crack density - Microcrack length - HMAC brittle-ductile failure characterization - Stress intensity factors - Regression constants - Shear coefficient

OUTPUT

- Paris’ Law fracture coefficients (A and n) - Shift factor due to anisotropy (SFa) - Shift factor due to healing (SFh) - Fatigue load cycles to crack initiation (Ni) - Fatigue load cycles to crack propagation (Np) - HMAC mixture fatigue resistance (Nf)

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65

LABORATORY TESTING

The required laboratory tests for the CMSE approach of HMAC mixture fatigue analysis

include tensile strength, relaxation modulus in both tension and compression, uniaxial repeated

direct-tension, and surface energy (45, 68-69, 71). These tests are described in this section. For

each of these tests, at least two replicate cylindrical specimens were tested per aging condition

per mixture type. The cylindrical HMAC specimen fabrication procedure, including the final

dimensions consistent with the SGC compaction protocol, is described in Chapter 3.

Tensile Strength Test

The tensile strength test was conducted to determine the HMAC mixture tensile strength

(σt), which is a required input parameter for CMSE Nf analysis.

Test Protocol

The tensile strength (TS) test protocol involves applying a continuous increasing tensile

load to a cylindrical HMAC specimen at a constant elongation (deformation) rate of 1.27

mm/min (0.05 in/min) till failure (break point). This test is destructive and took at most

2 minutes to complete the test. Figure 5-3 shows the loading configuration for and typical results

from the tensile strength test.

Deformat ion

Load

(P)

Pmax Load

Load

Figure 5-3. Loading Configuration for Tensile Strength Test.

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66

Test Conditions and Data Acquisition

The tensile strength test was conducted in an environmentally controlled chamber at a

test temperature of 20±0.5 °C (68±32.9 °F). Specimens were preconditioned to 20 °C (68 °F) for

a minimum period of 2 hrs. The temperature was monitored and controlled through a

thermocouple probe attached inside a dummy HMAC specimen also placed in the environmental

chamber. An MTS equipped with an automatic data measuring system applied the loading.

Loading data were measured via the MTS load cell, and deformations were recorded via three

LVDTs attached vertically to the sides of the specimen. During the test, load and axial

deformation data were captured electronically every 0.1 s. Two replicate specimens were tested

per aging condition per mixture type.

Mixture tensile strength (σt) was calculated simply as the maximum tensile load at break

divided by the specimen cross-sectional area as follows:

2max

rP

t πσ = (Equation 5-1)

where:

σt = Tensile strength (MPa)

Pmax = Maximum tensile load at break (MPa)

r = Radius of cylindrical specimen (mm)

Relaxation Modulus Test

The time-dependent elastic relaxation modulus (Ei), modulus relaxation rate (mi), and

temperature correction factor (aT) constitute input parameters for the CMSE fatigue analysis.

These material properties were determined from the relaxation modulus test (30).

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Test Protocol

Relaxation modulus (RM) is a strain-controlled test. The test involves applying a

constant axial strain to a cylindrical HMAC specimen either in tension or compression for a

given time period and then releasing the strain for another given time period, thereby allowing

the specimen to rest or relax (elastic recovery). The test loading configuration is shown in

Figure 5-4.

-200

0

200

0 200 400 600 800 1000 1200 1400

Time, s

Mic

rostr

ain

Tension

Compression

Load

Load

Figure 5-4 Loading Configuration for Relaxation Modulus Test.

As shown in Figure 5-4, the loading sequence consisted of a 200 tensile microstrain

sitting for a period of 60 s followed by a 600 s rest period and application of a 200 compression

microstrain for 60 s followed by another 600 s rest period (30). Researchers selected 200

microstrain because, for the HMAC mixtures considered in this project, prior trial testing with

microstrains above 200 proved to be destructive, while those below 200 were too small to

produce meaningful results. A 60 s strain loading time was considered adequate to prevent

irrecoverable damage while a 600 s rest period was considered adequate to allow for elastic

recovery. The time interval for the strain load application from 0 to +200 or -200 microstrain

was 0.6 s, and the input strain waveform was actually a trapezoidal shape. Thus, the total test

time for both the tensile and compressive loading cycle for a given test temperature, say 10 °C

(50 °F), was approximately 25 minutes.

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Test Conditions and Data Acquisition

The research team conducted RM testing in an environmentally controlled chamber at

three temperatures, 10, 20, and 30 °C (50, 68, and 86 °F), to facilitate development of a

time-dependent RM master-curve. This master-curve is a graphical representation of the HMAC

mixture properties as a function of temperature and loading time. Note that HMAC is sensitive to

temperature and time of loading.

The temperatures were monitored and controlled at a tolerance of ±0.5 °C (±32.9 °F)

through a thermocouple probe attached inside a dummy HMAC specimen also placed in the

environmental chamber. For each temperature-test sequence, the minimum specimen

conditioning time was 2 hrs. The MTS provided the loading while an automated data

measurement system captured the data (time, load, and deformation) electronically every 0.5 s.

Loading data were measured via the MTS load cell, and deformations were recorded via three

LVDTs attached vertically to the sides of the specimen. Three replicate specimens were tested

per aging condition per mixture type.

Figure 5-5 is an example of the output stress response from the relaxation modulus test at

a single test temperature of 10 °C (50 °F).

-250

0

250

0 200 400 600 800 1000 1200 1400

Time, s

Stre

ss, p

si

Figure 5-5. Example of Stress Response from RM Test at 10 °C (50 °F).

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69

Equation 5-2 was used to calculate the elastic relaxation modulus as a function of the

measured load (stress) and strain.

επεσ

2rP

E == (Equation 5-2)

where:

E = Elastic modulus (MPa)

P = Load (kN)

ε = Strain (mm/mm)

A time-reduced superposition logarithmic analysis of the elastic modulus data for each

test temperature to a reference temperature of 20 °C (68 °F) generates the required time-

dependent RM master-curve. This master-curve is represented in the form of a simple power law.

By the same logarithmic analysis, temperature correction factors (aT) are determined, where aT

has a value of 1.0 for the 20 °C (68 °F) reference temperature.

Uniaxial Repeated Direct-Tension Test

The time-dependent tensile stress (σ (t)) is an input parameter required to calculate the

rate of dissipation of PS energy (b) that is necessary to calculate Ni. This material property was

determined from the uniaxial repeated direct-tension test discussed subsequently.

Test Protocol

Like the RM test, the uniaxial repeated direct-tension (RDT) test was conducted in a

strain controlled mode (68). An axial direct tensile microstrain of 350 was applied repeatedly to a

cylindrical HMAC specimen at a frequency of 1 Hz for a total of 1000 load cycles. The input

strain waveform was haversine shaped.

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The actual loading time was 0.1 s with a 0.9 s rest period between load pulses. Thus, a

complete load cycle including the rest period was 1.0 s. Figure 5-6 shows the loading

configuration. The 0.9 s rest period allowed for HMAC relaxation between the load pulses and

prevented the buildup of undesirable residual stresses discussed subsequently. This rest period

can also promote a limited amount of healing.

Nu mber of Load Cycles

350

Mic rostrain

(1,000)Load

Load

Figure 5-6. Loading Configuration for the RDT Test.

The haversine-shaped input strain waveform is representative of the field load pulse

developed under moving wheel loads of commercial vehicles on interstate highways (68). A

relatively high input strain magnitude of 350 microstrain was selected because this value

(350 microstrain) was considered substantial enough to induce cumulative micro fatigue damage

(microcracking) within the HMAC specimen during the test. In this test, while micro fatigue

damage is desirable, an appropriate input strain level must be selected that will allow the test to

continue to an appreciable number of load cycles to capture sufficient data that will allow for

calculation of the b slope parameter needed in the CMSE analysis. For this project, testing was

terminated at 1000 load cycles, during which time sufficient data had been captured for DPSE

analysis and subsequent calculation of the constant b. A complete RDT test thus took about

20 minutes.

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Test Conditions and Data Acquisition

The haversine input strain waveform was supplied by the MTS, and axial deformations

were measured via three LVDTs. Data (time, load, and deformations) were captured

electronically every 0.005 s. The research team conducted the RDT test in an environmentally

controlled chamber at a test temperature of 30±0.5 °C (86±32.9 °F). The minimum conditioning

period for the specimens was 2 hrs. The temperature was monitored and controlled through a

thermocouple probe attached inside a dummy HMAC specimen also placed in the environmental

chamber.

Three replicate cylindrical HMAC specimens that had previously been subjected to a

series of RM tests at 10, 20, and 30 °C (50, 68, and 86 °F) were used for this test for each aging

condition and each mixture type. It should be noted that the RM test was assumed to be non-

destructive in this project. However, the RDT test is a destructive test since some microdamage

occurs within the HMAC specimen even though damage may not be physically visible.

Figure 5-7 is an example of the stress response from the uniaxial repeated direct-tension

test at 30 °C (86 °F). The measured stress (σ(t)), strain (ε(t)), and time (t) are the required input

parameters for CMSE fatigue analysis to calculate DPSE.

-250

0

250

500

0 1 2 3 4 5

Time, s

Stre

ss, p

si

Figure 5-7. Stress Response from RDT Testing at 30 °C (86 °F).

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72

Anisotropic Test

The modulus of HMAC is an important input parameter used in predicting HMAC

mixture fatigue properties. HMAC is not an isotropic material, and therefore, its mechanical

properties (i.e., elastic modulus) are directionally dependent (72-73). The objective of the

anisotropic test was thus to measure the variation of HMAC modulus measured from different

directions, vertical (Ez) and horizontal or lateral (Ex and Ey), which constitute input parameters

for CMSE fatigue analysis. Primarily, the research team conducted the anisotropic (AN) test to

determine the shift factor due to anisotropy (SFa) discussed in the subsequent sections of this

chapter.

Test Protocol

In this project, the research team conducted the AN test consistent with the HMAC

elastic-resilient modulus test, but with both axial and radial deformation measurements for Ez

and Ex determination, respectively (64). AN is a destructive stress-controlled test with a

sinusoidal-shaped input stress waveform. The test involved repeated application of a sinusoidal-

shaped stress magnitude of 690 kPa (100 psi) at a loading frequency of 1 Hz for a total of 200

load cycles without any rest period. Figure 5-8 shows the AN test loading configuration.

Figure 5-8. Loading Configuration for the AN Test

0 2 4 6 8 10 12

Time s)

Stre

ss

(200)

690 kPa (100 psi)

Load

Load

Axi

al d

efor

mat

ion

Radial deformation

Ez

Ex Ey

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An input stress magnitude of 690 kPa is simulative of a truck tire pressure on an in situ

field HMAC pavement structure. For this project, AN testing was terminated at 200 load cycles,

during which time sufficient data had been captured for moduli analysis. With a loading

frequency of 1 Hz, the total AN test time was at most 5 minutes. Although AN is a destructive

test, the 200 load cycles was in most cases not sufficient enough to cause visible damage to some

specimens.

For an AN test of this nature, it is always a normal practice to subject the test specimens

to lateral pressure confinement to simulate field triaxial stress state, particularly when testing

unbound granular materials (74-75). In this project, the AN test was conducted under

unconfined lateral pressure conditions. However, the AN analysis models were adjusted to the

lateral pressure confinement conditions to simulate the laboratory triaxial stress state. This

adjustment was achieved through trial testing of several HMAC specimens under both

unconfined and confined laboratory lateral (345 kPa) pressure conditions and then comparing the

moduli results. The moduli results measured without pressure confinement were then

adjusted/modified to match the moduli results under lateral pressure confinement conditions,

thus accounting for triaxial stress state conditions. Note that it is much more convenient, easier,

and practical to conduct the HMAC AN test under unconfined lateral pressure conditions.

Test Conditions and Data Acquisition

The sinusoidal input stress waveform was supplied by the MTS, while axial and radial

deformations were measured via three LVDTs. Two LDVTs attached vertically to the sides of

the specimen were used for axial measurements, and one LVDT attached radially around the

center of the specimen was used for radial deformation measurements, as shown in Figure 5-8.

Data (time, load, and deformations) were captured electronically every 0.02 s.

Like other HMAC mixture tests in this project, the research team conducted the AN test

in an environmentally controlled chamber at a test temperature of 20±0.5 °C (68±32.9 °F). The

minimum conditioning period for the specimens was 2 hrs. The temperature was monitored and

controlled through a thermocouple probe attached inside a dummy HMAC specimen also placed

in the environmental chamber. Three replicate specimens were tested per aging condition per

mixture type.

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Figure 5-9 is an example of the strain responses from the AN test at 20 °C (68 °F)

recorded for a period of 60 s. While the AN test gives both the elastic and plastic strain responses

as shown in Figure 5-9, the response component of interest that is critical to fatigue is the elastic

strain. By contrast, the plastic strain is critical to permanent deformation, which was beyond the

scope of this project.

0

100

200

300

0 10 20 30 40 50 60

Time (s)

Rad

ial m

icro

stra

in

Plastic

Elastic

0

400

800

1,200

0 10 20 30 40 50 60

Time (s)

Axia

l mic

rost

rain

Plastic

Elastic

Figure 5-9. Example of Strain Responses from AN Testing @ 20 °C (68 °F).

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From the measured AN test data, the elastic moduli were calculated as a function of the

applied load (stress) and elastic strain response, as expressed by Equations 5-3 and 5-4 below

(64, 74-75). For simplicity, HMAC was assumed to be laterally isotropic, and therefore, Ex was

considered equivalent to Ey in magnitude

zz

zz a

σ= (Equation 5-3)

x

zxyx aEE

ενσ

== (Equation 5-4)

where:

Ez = Elastic modulus in the vertical direction (MPa)

Ex = Elastic modulus in the lateral direction (MPa)

σz = Applied compressive axial stress (MPa)

εz,εx = Axial and radial deformation, respectively (mm/mm)

ν = Poisson’s ratio (ν≅ 0.33)

ax, az = Anisotropic adjustment factors that account for laboratory lateral pressure

confinement conditions (ax ≅ 1.15, az ≅ 0.75)

In this project, the mean ax and az values were determined to be 1.15 and 0.75,

respectively (for both mixtures), and these were the values used for moduli computations. The

determination of these ai adjustment factors is illustrated in Appendix B.

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76

Surface Energy Measurements for the Binder – The Wilhelmy Plate Test

The surface energy measurements for the binders in this project were completed using the

Wilhelmy plate method (68, 71). Compared to other methods such as the drop weight, Du Nouy

ring, pendant drop, Sessile drop, capillary rise, and maximum bubble pressure, the Wilhelmy

plate method is relatively simple and does not require complex corrections factors to the

measured data (68, 71).

The contact angle between binder and any liquid solvent can be measured using the

Wilhelmy plate method. This method is based on kinetic force equilibrium when a very thin plate

is immersed or withdrawn from a liquid solvent at a very slow constant speed, as illustrated in

Figure 5-10 (76).

Figure 5-10. Loading Configuration for the Wilhelmy Plate Method.

The dynamic contact angle between binder and a liquid solvent measured during the

immersing process is called the advancing contact angle, while the dynamic contact angle during

the withdrawal process is called the receding contact angle.

Liquid solvent

Asphalt

F

F Advancing

Receding

Liquid solvent

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77

The advancing contact angle, which is a wetting process, is associated with the healing

process, while the receding angle is associated with the fracture mechanism. The total surface

free energy and its components for binder are calculated from these advancing and receding

contact angles. The surface free energy calculated from the advancing contact angles is called the

surface free energy of wetting or healing, while the surface free energy computed from the

receding contact angle is called the surface free energy of dewetting or fracturing.

Test Protocol and Data Acquisition

To complete the Wilhelmy plate test, approximately 0.65 g of hot-liquid binder heated to

about 144 °C (291.2 °F) was coated onto glass plates 50 mm ( ≅2 inches) in length by 25 mm (≅1

inch) in width with a 0.15 mm (0.006 inches) thickness. By dipping the glass plate into a mass

of hot-liquid binder to a depth of about 15 mm (0.6 inches), a thin binder film of approximately 1

mm (0.039 inches) thickness was created on the glass plate after allowing the excess binder to

drain off (68, 71).

As shown in Figure 5-7, the actual test protocol involves an automatically controlled

cycle (s) of immersion and withdrawal (receding) processes of the binder coated glass plates

into a liquid solvent to a depth of about 5 mm (0.2 inches) at an approximate uncontrolled

ambient temperature of 20±2 °C (68±32.9 °F). The temperature is not tightly controlled in this

test because previous research has indicated that the measurable contact angle, and consequently

the surface free energy, are not very temperature sensitive (68, 71). The total test time for both

the immersion and withdrawal processes took approximately 15 minutes.

Prior to testing, the binder-coated glass plate must be vacuumed for about 12 hrs in a

diseccator to de-air the binder. Three test binder samples are required per test per three liquid

solvents, and thus a total of nine samples were used per aging condition (i.e., 0, 3, and 6 months).

Distilled water, formamide, and glycerol were the three selected liquid solvents used in

this project because of their relatively large surface energies, immiscibility with binder, and wide

range of surface energy components. Table 5-2 lists the surface energy components of these

three liquid solvents (distilled water, formamide, and glycerol) (68, 71).

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78

Table 5-2. Surface Energy Components of Water, Formamide, and Glycerol.

Surface Free Energy Components (ergs/cm2) (68, 71) Solvent

ΓLi ΓLiLW ΓLi

+ ΓLi- ΓLi

AB

Distilled water 72.60 21.60 25.50 25.50 51.00

Formamide 58.00 39.00 2.28 39.60 19.00

Glycerol 64.00 34.00 3.60 57.40 30.00

During the test, the loading force for the immersion and receding processes was provided

by an automatically controlled Dynamic Contact Analyzer (DCA) balance shown in Figure 5-11.

Data (dynamic contact angle) were measured and captured electronically via the WinDCA

software. Figure 5-12 is an example of the measured dynamic advancing and receding contact

angles at 20±2 °C (68±35.6 °F).

Figure 5-11. The DCA Force Balance and Computer Setup - Wilhelmy Plate Test.

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79

Receding angle = 59.75° (De wetting or fracturing process)

Advancing angle = 61.67° (W etting or healing process)

Figure 5-12. Example of the DCA Software Display (Advancing and Receding).

For clarity, the vertical axis title in Figure 5-10 is “mass” in mg with a scale of -100 to

200 mg, and the horizontal axis title is “position” in mm with a scale of 0 to 7 mm (0 to 0.28

inches).

Binder Surface Energy Calculations

Equation 5-3 is the force equilibrium equation resulting from the immersion (advancing)

or the withdrawal (receding) processes during the Wilhelmy plate test. Based on the Young-

Dupre theory and the assumption that binder equilibrium film pressure is zero, Equation 5-5

reduces to Equation 5-6 (71).

gVgVCosPF AirLLt ρρθ +−Γ=∆ (Equation 5-5)

( ) −++− ΓΓ+ΓΓ+ΓΓ=+Γiiii LiLi

LWL

LWiiL Cos 2221 θ (Equation 5-6)

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80

where:

F = Applied force (kN)

Pt = Perimeter of the binder coated glass plate (m)

θ = Dynamic contact angle between binder and the liquid solvent, degrees (°)

V = Volume of immersed section of glass plate (m3)

ρ = Density (subscript “L” for liquid solvent and “Air” for air) (g/cm3)

g = Acceleration due to gravity (m/s2)

Γ = Surface free energy (ergs/cm2)

The dynamic contact angle θ (°) is the measurable parameter, advancing (wetting) or

receding (dewetting). ΓLiLW, ΓLi

+, and ΓLi- are known surface free energy components of the

liquid solvent. Γi LW, Γ i+, and Γ i

- are the three unknown components of the binder surface

free energy from Lifshtz-van der Waals forces, Lewis base, and Lewis acid, respectively, that

need to be determined. Note that the advancing (wetting) and receding (dewetting) contact

angles are used for determining the surface energy due to healing and fracturing, respectively.

Mathematically, three liquid solvents of known surface free energies must be used to

solve Equation 5-6 for the three unknown parameters Γi LW, Γ i+, and Γ i

-. Algebraically,

Equation 5-6 can easily be transformed into a familiar matrix form of simple linear simultaneous

equations expressed by Equation 5-7 (71):

⎥⎥⎥

⎢⎢⎢

⎡=

⎥⎥⎥

⎢⎢⎢

⎥⎥⎥

⎢⎢⎢

3

2

1

3

2

1

333231

232221

131211

YYY

xxx

aaaaaaaaa

(Equation 5-7)

i

i

i

i

i

i

L

Li

L

Li

L

LWL

i aaaΓ

Γ=

Γ

Γ=

Γ

Γ=

−+

2 ,2 ,2 321 (Equation 5-8)

+− Γ=Γ=Γ= iiLW

i xxx 321 , , (Equation 5-9)

( ) ii CosxY θ+= 1 (Equation 5-10)

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81

where:

aki = Known surface energy components of the three liquid solvents

(distilled water, formamide, and glycerol) (ergs/cm2) (Table 5-2)

xi = The unknown surface energy components (Γi LW, Γ i+, and Γ i

-) of the

binder that need to be determined (ergs/cm2)

Yi(x) = Known function of the measured contact angles of the binder in the three

liquid solvents (θWater, θFormamide, and θGlycerol)

The solution of Equation 5-10 provides the surface free energy components of the binder

required for the CMSE fatigue analysis.

Surface Energy Measurements for the Aggregate – The Universal Sorption Device

In this project, the research team used the Universal Sorption Device (USD) for the

surface energy measurements of aggregates. The USD method utilizes a vacuum gravimetric

static sorption technique that identifies gas adsorption characteristics of selected solvents with

known surface free energy to indirectly determine the surface energies of the aggregate.

Sorption methods are particularly suitable for aggregate surface energy measurements because of

their ability to accommodate the peculiarity of sample size, irregular shape, mineralogy, and

surface texture associated with the aggregates (71).

Test Protocol and Data Acquisition

The USD setup is comprised of a Rubotherm magnetic suspension balance system, a

computer system (with Messpro software), a temperature control unit, a high quality vacuum

unit, a vacuum regulator, pressure transducers, a solvent container, and a vacuum dissector. A

schematic of the main components of the USD setup is illustrated in Figure 5-13.

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82

Solvent vapor supply

Magnetic suspension

balancePressure control and measurement

Balance, reading, tare, calibration, zero point and measuring point

Tem

per a

ture

con

trol

Sample chamber

Figure 5-13. USD Setup.

A Mettler balance is securely established on a platform with the hang-down Rubotherm

magnetic suspension balance and sample chamber beneath it. This magnetic suspension balance

has the ability to measure a sample mass of up to 200 g to an accuracy of 10-5 g, which is

sufficient for precise measurement of mass increase due to gas adsorbed onto the aggregate

surface. The whole USD system is fully automated with about 8 to 10 predetermined pressure

set-points that automatically trigger when the captured balance readings reach equilibrium.

With this USD sorption method, an aggregate fraction between the No.4 and No.8 sieve

size is suspended in the sample chamber, in a special container. Essentially, the size of

aggregate tested is that which passes the No.4 (4.75 mm [0.19 inches]) sieve but is retained on

the No. 8 sieve (2.36 mm [0.09 inches]). Theoretically, the surface free energy of aggregate is

not affected by the size of the aggregate because size is accounted for during the SE calculation

process (71). However, this aggregate fraction size (No.4 < aggregate size < No. 8) used in the

USD test is dictated by the limitation of the sample chamber size and the desired aggregate

surface area for sufficient gas adsorption that is representative of all aggregate fractional sizes.

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During the USD test process, once the chamber is vacuumed, a solvent vapor is injected

into the aggregate system. A highly sensitive magnetic suspension balance is used to measure

the amount of solvent adsorbed on the surface of the aggregate. The vapor pressure at the

aggregate surface is measured at the same time. The surface energy of the aggregate is

calculated after measuring the adsorption of three different solvents with known specific surface

free energy components. In this project, three solvents: distilled water, n-Hexane, and Methyl

Propyl Ketone 74 (MPK) with surface free energy components listed in Table 5-3, were used

(71).

Table 5-3. Surface Energy Components of Water, n-hexane, and MPK.

Surface Free Energy Components (ergs/cm2) (68, 71) Solvent

ΓLi ΓLiLW ΓLi

+ ΓLi- ΓLi

AB

Distilled water 72.60 21.60 25.50 25.50 51.00

n-hexane 18.40 18.40 0.00 19.60 0.00

MPK 24.70 24.70 0.00 0.00 0.00

Like binder SE measurements, aggregate SE measurements are also insensitive to

temperature, so the research team conducted the USD test at uncontrolled ambient temperature of

approximately 25±2 °C (77±35.6 °F). The total test time for a complete test set with three

solvents is about 60 to 70 hrs. For each solvent, 50 g sample of aggregates were tested for 0

months aging condition only. Note that aggregates are by nature insensitive to aging and thus 3

and 6 months aging at 60 °C (140 °F) were not considered for the aggregate SE measurements.

Prior to testing, the aggregate sample must be thoroughly cleaned with distilled water and oven-

dried (at about 120 °C (248 °F) for at least 8 hrs) to remove any dusty particles and moisture that

might negatively impact the results.

Data (vapor pressure, adsorbed gas mass, and test time) were measured and captured

electronically via the Messpro software. Figure 5-14 is an example of a typical output obtained

from the USD adsorption test for n-hexane adsorption on limestone aggregate at 25 °C (77 °F).

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84

Hexane adsorbed onto colorado limestone

0

0.05

0.1

0.15

0.2

0.25

0 50 100 150 200 250 300 350

Time, (min)

Mas

s ad

sorb

ed, (

mg/

g)adsorption without bouyancy correction

"adsorption with bouyancy correction"

Figure 5-14. Example of Adsorption of n-Hexane onto Limestone under USD Testing.

Aggregate SE Calculations

Once the adsorbed solvent mass and vapor pressure on the aggregate surface have been

measured and the adsorption data corrected for solvent vapor buoyancy using the generalized

Pitzer correlation model, the specific surface area of the aggregate was then calculated using the

BET (Brunauer, Emmett, and Teller) model shown by Equation 5-11 (68, 71):

( ) cnPP

cnc

PPnP

mm

11

00

+⎟⎟⎠

⎞⎜⎜⎝

⎛ −=

− (Equation 5-11)

where:

P = Vapor pressure (MPa)

P0 = Saturated vapor pressure of the solute (MPa)

n = Specific amount adsorbed on the surface of the absorbent (mg)

nm = Monolayer capacity of the adsorbed solute on the absorbent (mg)

c = Parameter theoretically related to the net molar enthalpy of adsorption

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85

For the type of isotherms associated with the pressure conditions in this USD test, mn can

be obtained from the slope and the intercept of the straight line that best fits the plot of P/n(P-Po)

versus P/Po. The specific surface area (A) of the aggregate can then be calculated through the

following equation:

α⎟⎟⎠

⎞⎜⎜⎝

⎛=

MNn

A om (Equation 5-12)

And for a hexagonal close-packing model;

3/2

091.1 ⎟⎟⎠

⎞⎜⎜⎝

⎛=

ρα

oNM

(Equation 5-13)

where:

α = Projected area of a single molecule (m2)

No = Avogadros’ number (6.02 ×1023)

M = Molecular weight (g)

ρ = Density of the adsorbed molecule in liquid at the adsorption conditions

(g/cm3)

The result from the BET equation is used to calculate the spreading pressure at saturation

vapor pressure (πe) for each solvent using Gibbs free energy Equation 5-14 (71):

∫=0

0

p

e dPPn

ARTπ (Equation 5-14)

where:

πe = Spreading pressure at saturation vapor pressure of the solvent (ergs/cm2)

R = Universal gas constant (83.14 cm3 bar/mol.K)

T = Absolute temperature (Kelvin, K) (K = 273 + °C)

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86

The work of adhesion of a liquid on a solid (WA) can be expressed in terms of the surface

energy of the liquid ( lΓ ) and the equilibrium spreading pressure of adsorbed vapor on the solid

surface (πe) as shown in Equations 5-15 and 5-16:

leaW Γ+= 2π (Equation 5-15)

+−−+ ΓΓ+ΓΓ+ΓΓ=Γ+ lslsLW

lLWse 2222π (Equation 5-16)

where:

subscript s = Solid (aggregate)

subscript l = Liquid (solvent)

From Equations 5-15 and 5-16, the surface energy components and the total surface

energy of the aggregate can be determined by employing Equations 5-17 through 5-20):

( )LW

l

leLWs Γ

Γ+=Γ

42 2π (Equation 5-17)

Equation 5-17 is used to calculate the LWsΓ of the surface for a non-polar solvent on the

surface of the solid (aggregate). For a known mono-polar basic liquid vapor (subscript m ) and a

known bipolar liquid vapor (subscriptb ), the +Γs and −Γs values were calculated using

Equations 5-18 and 5-19 as follows:

( )−

+

ΓΓΓ−Γ+

=Γlm

LWlm

LWslme

s 42

(Equation 5-18)

( )+

−+−

ΓΓΓ−ΓΓ−Γ+

=Γlb

lbsLW

lbLWslbe

s 422

(Equation 5-19)

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87

Finally, the total surface energy of the aggregate ( sΓ ) is calculated as expressed by

Equation 5-20:

−+ΓΓ+Γ=Γ 2LWss (Equation 5-20)

Note, however that the current USD test protocol is still under development, in particular

to improve its test time efficiency as well as a general review of the SE data analysis procedures

(77). Appendix B provides a summary of the current USD test protocol and SE analysis

procedure as utilized in this project.

FAILURE CRITERIA

For the CMSE approach, fatigue failure is defined as crack initiation and propagation

through the HMAC layer thickness. In this project, researchers selected a maximum microcrack

length of 7.5 mm (0.30 inches) as the failure threshold value for crack initiation. This 7.5 mm

(0.30 inches) threshold value was selected based on Lytton et al.’s findings in their extensive

fatigue tests that crack propagation in the HMAC layer begins when microcracks grow and

coalesce to form a small crack of approximately 7.5 mm (0.30 inches) long (45).

ANALYSIS PROCEDURE

Equation 5-21, which relates field fatigue life (Nf) to the number of load cycles to crack

initiation (Ni) and crack propagation (Np) as a function of shift factors (SFi), is the fundamental

principle of the CMSE approach for fatigue modeling of HMAC mixtures (45).

( )piif NNSFN += (Equation 5-21)

where:

Nf = Fatigue life or number of load cycles to fatigue failure

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88

SFi = Product of the shift factors including HMAC anisotropy (SFa),

healing (SFh), aging (SFag), residual stresses (SFrs), stress state (SFss),

resilient dilation (SFd), and traffic wander ( SFtw).

Ni = Number of load cycles to crack initiation

Np = Number of load cycles to crack propagation

Each of these terms in Equation 5-21 is discussed in the subsequent subsections. In

Equation 5-21, the sum (Ni + Np) constitutes the laboratory fatigue life and the product of the

shift factors (SFi) and the sum (Ni + Np) constitute the field fatigue life.

Shift Factor due to Anisotropic Effect, SFa

Anisotropy arises due to the fact that HMAC is not isotropic as often assumed. The

mixture stiffness (modulus) in the lateral (horizontal) direction is not equal to that in the vertical

direction due to the differences in the particle orientation during compaction/construction.

During construction, there is always a high compactive effort in the vertical direction relative to

other directions. So the HMAC behavior or response to loading and/or the environment is

different in different directions. Consequently, the HMAC anisotropy must be considered in

fatigue analysis. However, most laboratory test protocols measure only the vertical stiffness and

assume isotropic behavior.

In the CMSE analysis, SFa takes care of the anisotropic behavior of the HMAC mixture.

Equation 5-22 shows the elastic modular relationship between the vertical (Ez) and horizontal

(Ex) moduli used in this project. Ez and Ex are measurable parameters from the AN test (34).

75.1

⎟⎟⎠

⎞⎜⎜⎝

⎛=

x

za E

ESF (Equation 5-22)

where:

SFa = Shift factor due to anisotropy, ranging between 1 and 5

Ez = Elastic modulus in vertical direction (MPa)

Ex = Elastic modulus in lateral or horizontal direction (MPa)

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89

Generally, because of the vertical orientation of the compactive effort during field

construction or laboratory compaction, Ez is always greater than Ex on the order of magnitude of

about 1.5 times (78). For simplicity purposes, HMAC was assumed to be laterally isotropic, and

therefore, Ex was considered as being equivalent to Ey in magnitude.

Shift Factor due to Healing Effect, SFh

Due to traffic rest periods and temperature variations, the asphalt binder has a tendency to

heal (closure of fracture surfaces), which often results in improvement in the overall HMAC

mixture fatigue performance. The CMSE approach takes this into account and relates healing to

traffic rest periods and temperature by the following equations (45, 71):

6

51g

TSF

rh a

tgSF ⎟⎟⎠

⎞⎜⎜⎝

⎛ ∆+= (Equation 5-23)

ESALs Traffic 8010536.31 6

kNP

t DLr

×=∆ (Equation 5-24)

( ) 65

gohag = (Equation 5-25)

⎟⎟⎟⎟⎟⎟

⎜⎜⎜⎜⎜⎜

⎥⎥⎦

⎢⎢⎣

⎡⎟⎟⎠

⎞⎜⎜⎝

⎛ ∆⎟⎟⎠

⎞⎜⎜⎝

⎛ −+

−+=

TSF

sr

o

atC

hhh

hhhh

β

21

212

1

(Equation 5-26)

[ ] ⎟⎟⎟

⎜⎜⎜

∆=

⎟⎟⎠

⎞⎜⎜⎝

cmc

LWh EG

Ch1

11 (Equation 5-27)

⎟⎟⎟⎟

⎜⎜⎜⎜

+⎥⎦

⎤⎢⎣

⎡⎟⎟⎠

⎞⎜⎜⎝

⎛ ∆=

⎟⎟⎠

⎞⎜⎜⎝

3

1

22 CEGCh

cm

c

ABh (Equation 5-28)

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90

⎟⎟⎠

⎞⎜⎜⎝

⎛⎟⎟⎠

⎞⎜⎜⎝

⎛∆∆

=c

LWh

ABh

mC

GGCh 5

4β (Equation 5-29)

where:

SFh = Shift factor due to binder healing effects, ranging between 1 and 10

∆tr = Rest period between major traffic loads (s)

∆t = Loading time (s)

aTSF = Temperature shift factor for field conditions (~1.0)

Csr = Square rest period factor (~1.0 )

a, g5, g6 = Fatigue field calibration constants

h0, 21−h ,= Healing rates

hβ = Healing index, ranging between 0 and 1.0

PDL = Pavement design life in years

80kN Traffic ESALs = Number of equivalent single axle loads over a given

pavement design period (e.g., 5 million over a 20-year design period)

C1-5 = Healing constants

Ec = Elastic relaxation modulus from compression RM master-curve (MPa)

mc = Exponent from compression RM master-curve

∆GhAB, ∆Gh

LW = Surface energies due to healing or dewetting (ergs/cm2)

In Equation 5-23, ∆tr represents the field long-term rest period and depends on the

pavement design life and traffic expressed in terms of traffic ESALs (45). The numerical value

of 31.536 × 106 in Equation 5-24 represents the total time in seconds for a 365 day calendar

year. The parameter aTSF is a temperature shift factor used to correct for temperature differences

between laboratory and field conditions. For simplicity, the research team used an aTSF value of

1.0, but this value can vary depending on the laboratory and field temperature conditions under

consideration. Csr represents the shape of the input strain wave rest period during the RDT test.

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91

As discussed previously, the periodic time interval between the input strain waveforms

for the RDT test in this project simulated a square-shaped form, with a total duration of 0.9 s.

This 0.9 s periodic time interval was considered as the square shaped rest period, so a Csr value

of 1.0 was used in the analysis (79). As stated previously, this rest period allowed for HMAC

relaxation, healing, and prevented the buildup of undesirable residual stresses during RDT

testing.

The parameters a, g5, g6 , h0, and 21−h are fatigue field calibration constants and healing

rates quantifying the HMAC mixture healing properties as a function of climatic location of the

pavement structure in question, SE due to healing, and HMAC mixture properties (Ec and mc)

obtained from compression relaxation modulus tests. These calibration constants and healing

rates also represent the HMAC mixture short-term rest periods and asphalt binder healing rates,

both short-term and long-term, respectively (45). The parameter hβ is a healing index ranging

between 0 and 1.0 that represents the maximum degree of healing achievable by the asphalt

binder (71).

The fatigue calibration coefficients g5 and g6 are climatic dependent. In this project, the

research team used values shown in Table 5-4, assuming Wet-No-Freeze and Dry-No-Freeze

climates. Table 5-5 provides an additional set of gi values based on accelerated laboratory

testing. These values in Tables 5-4 and 5-5 were established by Lytton et al. (45) in their

extensive field calibration study of fatigue cracking through Falling Weight Deflectometer

(FWD) tests in the field and accelerated laboratory tests. In their (Lytton et al.) findings, these

calibration coefficients provided a good fit between measured and predicted fatigue cracking

(45).

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Table 5-4. Fatigue Calibration Constants Based on Backcalculation of Asphalt Moduli from FWD Tests (Lytton et al. [45]).

Climatic Zone Coefficient

Wet-Freeze Wet-No-Freeze Dry-Freeze Dry-No-Freeze

g0 -2.090 -1.615 -2.121 -1.992

g1 1.952 1.980 1.707 1.984

g2 -6.108 -6.134 -5.907 -6.138

g3 0.154 0.160 0.162 1.540

g4 -2.111 -2.109 -2.048 -2.111

g5 0.037 0.097 0.056 0.051

g6 0.261 0.843 0.642 0.466

Table 5-5. Fatigue Calibration Constants Based on Laboratory Accelerated Tests (Lytton et al. [45]).

Climatic Zone Coefficient

Wet-Freeze Wet-No-Freeze Dry-Freeze Dry-No-Freeze

g0 -2.090 -1.429 -2.121 -2.024

g1 1.952 1.971 1.677 1.952

g2 -6.108 -6.174 -5.937 -6.107

g3 0.154 0.190 0.192 1.530

g4 -2.111 -2.079 -2.048 -2.113

g5 0.037 0.128 0.071 0.057

g6 0.261 1.075 0.762 0.492

SE and RM tests were discussed in previous sections of this chapter. ∆Gh Ec, and mc are

material (binder, aggregate, and HMAC mixture) dependent but also vary with the aging

condition of the binder and/or HMAC mixture, which has a net impact on SFh and Nf. As

discussed in Chapter 10, this preliminary study has shown that the variation of these parameters

(∆Gh, Ec, and mc) with 3 and 6 months aging of the binder and HMAC mixture at 60 °C (140 °F)

reduced the value of SFh considerably, particularly the resultant Nf. Analysis procedures for ∆Gh,

Ec, and mc are discussed subsequently.

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93

The healing constants C1 through C5 were backcalculated from regression analysis as a

function of the measured Ec, ∆Gh due to healing, and the healing rates (hi) using a spreadsheet

sum of square error (SSE) minimization technique (45, 68, 71).

Other Shift Factors

The shift factor due to aging (SFag) is discussed in Chapters 10 and 11 of this report. In

this current CMSE analysis, other shift factors including residual stress, stress state, dilation, and

traffic wander were not considered or were simply assigned a numerical value of 1.0 based on

the assumptions discussed in this section. In fact, the research team considered that some of these

factors are already included in the SFa and SFh shift factors. Nonetheless, future CMSE studies

should consider the possibility of exploring these shift factors in greater detail.

Residual Stresses, SFrs

In the field, because of incomplete elastic relaxation/recovery and short time intervals

between some traffic load applications (axles of the same vehicle), residual stresses can remain

in the pavement after the passage of each load cycle and may thus prestress the HMAC layer so

that the tensile stresses that occur with the next load cycle cause less, equivalent, or more

damage. If present, these residual stresses occur either in tension or compression depending

among other factors on the magnitude of the load and the pavement structure. On the same

principle, residual stresses can also buildup in laboratory test fatigue specimens particularly if

there is an insufficient rest period between load applications or if the specimens are not properly

loaded during the test. Equations 5-30 and 5-31 show the estimation of SFr according to Tseung

et al. (80):

( ) ⎟⎠⎞

⎜⎝⎛ −

−− ±=⎟⎟

⎞⎜⎜⎝

⎛±

= mmo

k

mo

r tPtP

SF2

11

1 21

(Equation 5-30)

)()(tEtP

t

ro ε

σ= (Equation 5-31)

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94

where:

Po = The percent of total strain remaining in the pavement as residual strain

after passage of the traffic load ( %)

t = Loading duration (s) (e.g., 0.1 s)

m = Stress relaxation rate (i.e., from tensile RM master-curve)

k21 = Laboratory determined constant as a function of m

σr(t) = Residual stresses (tensile or compressive) at time t (MPa)

εt = Total tensile strain (mm/mm)

E(t) = HMAC elastic modulus at time t (MPa)

Note that the expression k21 = 2/m may be valid only for HMAC subjected to uniaxial

strain-controlled loading tests. A different expression may be required for stress-controlled

loading tests.

According to Lytton et al. (45), SFr commonly ranges between 0.33 and 3.0 depending on

whether the residual stresses are tensile or compressive. In the absence of sufficient field data to

accurately predict the magnitude and/or determine whether these residual stresses (or strains)

will be tensile or compressive, and the fact that there was insignificant residual stress build-up in

the CMSE laboratory fatigue specimens under RDT testing (i.e., σr(t) ≈ Po ≈ 0.0), a SFr value of

1.0 was not an unreasonable assumption.

The RDT test in this project was conducted with a 0.9 s rest period between load pulses,

while the actual loading time was 0.1 s. The RDT out put stress response indicated that this 0.9 s

rest period sufficiently allowed for HMAC relaxation and subsequent prevention of residual

stress buildup. In fact, Equations 5-30 and 5-31 also show that if there are no residual stresses

(σr(t) ≈ 0.0), as in the case of the RDT test in this project, Po will be 0.0, and SFr will have a

numerical value of 1.0.

Note also that the CMSE fatigue analysis approach in this project assumes that there are

no residual stresses due to construction compaction in the field or SGC compaction in the

laboratory.

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Stress State, SFss

In a pavement structure under traffic loading, a triaxial stress state exists. The continuum

nature of the pavement material tends to transfer the applied stress in all three coordinate

directions (x, y, and z) based on the Poisson’s ratio and the interlayer bonding conditions. In the

laboratory, the stress state can be uniaxial, biaxial, or triaxial depending on the test protocol. A

shift factor is thus required to account for this difference in stress state between laboratory and

field conditions.

In a linear elastic stress-strain analysis, Al-Qadi et al. found that a shift factor based on

strain energy that accounts for the differences between laboratory and field pavement stress state

can vary approximately between 1.0 and 6.0 (81). Among others, this stress state depends on

materials, pavement structure, mode of loading (uniaxial, biaxial, or triaxial), and magnitude of

loading. With sufficient laboratory and field data, Al-Qadi et al. proposed that SFss can be

approximated by Equation 5-32 as follows (81):

( )

( )∑

=

=

+

+== y

xizzii

y

xizzii

Field

Labss

EE

EE

WW

SF2

2

σε

σε (Equation 5-32)

where:

WLab = Total work done by laboratory loading ≅ strain energy (J/m3)

WField = Total work done by traffic loading in the field ≅ strain energy (J/m3)

σ, E, ε = stress (MPa), elastic modulus (MPa), and strain (mm/mm)

i = Subscript i, for x, y, and z coordinate directions

However, for the current CMSE analysis, the research team considered that the existence

of stress state (uniaxial, biaxial or triaxial) under laboratory and/or field loading conditions is

directly tied to the anisotropic response of HMAC. For example, the response behavior of

HMAC in terms of the elastic modulus under loading is directionally dependent, which is a

function of the stress state. Therefore, the effect of the stress state was considered to be indirectly

incorporated in the SFa factor.

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Resilient Dilation, SFd

Consistent with the theoretical definition of ν, resilient dilation will occur only for ν

values greater than 0.5. For pavement material subjected to vertical loading, dilation occurs when

the lateral deformation is greater than the vertical deformation, often as a result of inadequate

lateral confinement or support. This tendency to dilate is generally caused by the motion of

particles that tend to roll over one another (45).

Dilation is often very critical in unbound granular materials and the subgrade and can

often have a very significant impact on the overall fatigue performance of the pavement structure

in terms of stress-strain response. HMAC, on the other hand, is a bound material and is not very

sensitive to dilation. However, its stress-strain response to traffic loading and overall

performance can be greatly affected if the underlying pavement layers have potential to dilate.

SFd often ranges between 1.0 and 5.0 depending upon how much larger the Poisson’s

ratio (ν) is greater than 0.5 (45). Since, in this project, all the values of ν used were less than 0.5

(Chapter 3), researchers assumed the minimum value of 1.0 for SFd.

Traffic Wander, SFtw

Controlled laboratory fatigue testing applies loading repetitively to the same exact

location on the specimen. However, traffic loading in the field does not constrain itself to the

same position in the wheelpath. Accordingly, SFtw is needed to account for the traffic wander

when modeling pavement response to loading.

Blab and Litzka (82) postulated that the vehicle positions within the wheelpaths follow a

Laplace distribution function. Al-Qadi et al. (81) assumed a normal distribution around the

wheelpath with a mean of zero and a standard deviation, σ. Based on transverse strain

measurement in the wheelpath, Al-Qadi et al. derived SFtw values ranging between 1.6 and 2.7

for a σ range of 0.5 to 1.0.

However, for a given infinitesimal point within the pavement structure (i.e., in the

HMAC layer), the research team theorizes that the net engineering effect of traffic wander is to

relax and/or rest that particular point, thus minimizing the effect of residual stresses (tensile or

compressive) while simultaneously promoting elastic recovery and subsequent healing.

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97

This stress relaxation or rest period occurs because of traffic wander, and subsequent

loading follows a different path from the preceding one. Based on this theory, it can be assumed

that the effect of traffic wander is indirectly tied to SFrs and SFh. Therefore, an independent SFtw

was not considered in the current CMSE approach.

Also, Al-Qadi et al.’s study seems to indicate that with the assumption of normal traffic

distribution in the wheelpath and a relatively small value of σ (i.e., σ < 0.5), a SFtw value of 1.0

can possibly be derived (59).

Number of Load Cycles to Crack Initiation, Ni

Ni is defined as the number of load cycles required to initiate and grow a microcrack to

7.5 mm (0.30 inches) in length in the HMAC layer. In the CMSE analysis, Ni is determined

according to the following equation as a function of crack density, specimen cross-sectional area,

Paris’ Law fracture coefficients, and the rate that damage accumulates as indicated by DPSE (29,

30, 34):

( )

( )nD

nc

n

i CbA

AC

N ⎟⎟⎠

⎞⎜⎜⎝

⎛⎥⎦⎤

⎢⎣⎡

⎟⎟⎠

⎞⎜⎜⎝

⎛=

+ π421max (Equation 5-33)

⎟⎟⎠

⎞⎜⎜⎝

⎛=

tmn 1 (Equation 5-34)

∫∆

⎟⎟⎠

⎞⎜⎜⎝

⎛⎥⎦

⎤⎢⎣

+−

⎟⎟⎟⎟

⎜⎜⎜⎜

⎥⎥⎦

⎢⎢⎣

∆=

t nnm

f

tm

it

dttwG

EDI

kABDtt

0

)1(11

)1(1

2 )(σ

(Equation 5-35)

⎟⎟⎠

⎞⎜⎜⎝

⎛⎟⎟⎠

⎞⎜⎜⎝

⎛=

ππ

t

t

t mmSin

ED

][11 (Equation 5-36)

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98

( )BDi n

I+

=1

2 (Equation 5-37)

( )ndttt

Sindttwt t nn ln1744.05042.0).(

0 0

2 −=⎟⎟⎠

⎞⎜⎜⎝

⎛⎥⎦⎤

⎢⎣⎡∆

=∫ ∫∆ ∆ π (Equation 5-38)

where:

Cmax = Maximum microcrack length (mm) (i.e., 7.5 mm (0.30 inches))

A, n = Paris’ Law fracture coefficients

Ac = Specimen cross-sectional area (m2)

b = Rate of accumulation of dissipation of pseudo strain energy

CD = Crack density (m/m2)

mt = Exponent obtained from the tension RM master-curve

(slope of the log relaxation modulus versus log time graph)

D1 = Time-dependent creep compliance (MPa-2)

Et = Elastic modulus from tension RM master-curve (MPa)

k = Stress intensity factor (~0.33)

∆Gf = Surface energy due to fracture or dewetting (ergs/cm2)

σt = Maximum mixture tensile strength at break (kPa)

Ii = Dimensionless stress integral factor in crack failure zone,

ranging between 1 and 2

nBD = Dimensionless brittle-ductile factor, ranging between 0 and 1

∆t = Repeated loading time (s) (~0.01 s)

∫∆t

n dttw0

)( = Load pulse shape factor, ranging between 0 and 1

t = Time (s)

The parameter Cmax defines the CMSE failure criterion and the subsequent failure

threshold value discussed previously. The crack density (CD) and rate of accumulation of

dissipation of pseudo strain energy (b) are discussed in the subsequent subsections of this

chapter.

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99

The parameters A and n are Paris’ Law fracture coefficients for material fracture

properties, which quantifies the HMAC mixture’s susceptibility to fracturing under loading.

According to Paris’ Law and Schapery’s theory, the coefficient n can be defined simply as the

inverse of the stress (tensile) relaxation rate (mt) as expressed by Equation 5-34 (26, 68, 71). This

assumption is valid for linear visco-elastic HMAC materials under a constant strain-controlled

RDT test (68, 71). Paris’ Law fracture coefficient A (Equation 5-35), on the other hand, is a

function of many parameters including k, D1, Et, mt, nBD, ∆Gf, σt, Ii, and wn(t). Based on Equation

5-33, a small value of A is desirable in terms of HMAC mixture fatigue resistance. Numerical

analysis, however, indicated that this coefficient A is very sensitive to nBD and σt if other factors

are held constant.

The parameter k is a material coefficient relating the length of the fracture process zone

(∝) to strain energy and mixture tensile strength. While this k is a measurable parameter, a value

of 0.33 was used based on Lytton et al.’s work and the assumption that it (k ≅ 0.33) does not vary

significantly with microcrack length in the fracture process zone (45).

As expressed by Equation 5-36, the time-dependent creep compliance, D1, was

determined as a function of Et and mt. Although an exact value of D1 can be measured from

uniaxial creep tests, this less costly and simple approximation produces a reasonable value that is

sufficient for use in HMAC mixture characterization analysis.

The numerical integration of wn(t) (Equation 5-38) with respect to time (t) describes the

shape of the input load pulse as a function of material fracture coefficient n (Paris’ Law). This

integral exhibits a linear relationship with the Paris’ Law fracture coefficient A, evident from

Equation 5-26, and has a subsequent inverse relationship with Ni. For a haversine-shaped input

strain waveform for the RDT test, as in this project, the integral reduces to a simple linear form

shown in Equation 5-39 with n as the only variable. Note that material response to loading is not

only magnitude dependent but also depends on the shape of the applied load form. As discussed

previously, a haversine-shaped input load form is a close simulation of HMAC load-response

under a moving wheel load (45, 68). The parameters Et, mt, ∆Gf, and σt are discussed

subsequently.

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100

Ii is an elasticity factor due to the integration of the stresses near the microcrack tip over a

small region in the microcrack failure zone (45, 68, 71). This factor, Ii, quantifies the materials’

elasticity ranges between 1.0 and 2.0 for perfectly linear-elastic (brittle) and rigid-plastic

(ductile) materials, respectively (83). Generally, a lower value (i.e., more linear-elastic) of Ii is

indicative of high susceptibility to fatigue damage. As expressed by Equation 5-28, the research

team quantified Ii simply as a function of nBD in this project. This brittle-ductile factor nBD,

which ranges between 0.0 for perfectly plastic materials and 1.0 for brittle materials, is an age-

related adjustment factor that accounts for the brittleness and ductility state of the HMAC

mixture in terms of stress-strain response under loading. In this project, unaged HMAC

specimens were assumed to exhibit plastic behavior and were subsequently assigned an nBD

value of 0.0. All the aged HMAC specimens were assumed to exhibit a brittle-ductile behavior

lying somewhere between perfectly plastic and brittle behavior, and were thus assigned nBD

values of 0.5 and 0.75 for 3 and 6 months aging conditions, respectively.

Number of Load Cycles to Crack Propagation, Np

Np refers to the number of load cycles required to propagate a 7.5 mm (0.30 inch)

microcrack through the HMAC layer thickness. As expressed by Equation 5-39, Np is determined

as a function of the maximum microcrack length, HMAC layer thickness, shear modulus, Paris’

Law fracture coefficients, and a design shear strain (45, 68, 71).

( ) ( ) ( )[ ]( ) nnq

nn

n

p dC

nqSGrAdN ⎟⎟

⎞⎜⎜⎝

⎛⎟⎟⎠

⎞⎜⎜⎝

⎛⎥⎦⎤

⎢⎣⎡−

⎟⎟⎟

⎜⎜⎜

−=

−⎟⎠⎞

⎜⎝⎛ −

γ11

12

1max

21

(Equation 5-39)

( )νν21

)1(−−

=S (Equation 5-40)

⎟⎟⎠

⎞⎜⎜⎝

⎛=

z

xzt E

GEG (Equation 5-41)

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101

where:

A, n = Paris’ Law fracture coefficients

r, q = Regression constants for stress intensity factor (~4.40, 1.18) (45)

S = Shear coefficient

G = Shear modulus (MPa)

Cmax = Maximum microcrack length (mm) (i.e., 7.5 mm (0.30 inches))

d = HMAC layer thickness (mm)

γ = Maximum design shear strain at tire edge (mm/mm)

ν = Poisson’s ratio

Gxz = Resilient shear modulus (MPa)

Et = Elastic modulus from tensile RM master-curve (MPa)

If the elastic modular ratio Gxz/Ez in Equation 5-41 is unknown, Equation 5-42 below can

be used to approximate G (79). Equation 5-42 is a simple shear-elastic modulus relationship

based on elastic theory.

( )ν+=

12tE

G (Equation 5-42)

The parameters A, n, and Cmax were discussed in the previous subsections, and γ is

discussed in the subsequent text. Like Ni, an inverse relationship exists between A and Np,

indicating that a small value of A is desired in terms of HMAC mixture fatigue resistance. The

failure load-response parameter γ also exhibits an inverse relationship with Np.

Unlike for Ni, d is introduced in Np because during the microcrack propagation process,

for fatigue failure to occur, a microcrack length of a defined threshold value must actually

propagate through the HMAC layer thickness. By contrast, the prediction relationship for Ni is a

fatigue model for microcrack initiation and is independent of the parameter d.

Parameters r and q are regression constants that are a function of the stress intensity

distribution in the vicinity of the microcrack tip. In this study, values of 4.40 and 1.18 were

used, respectively, based on Lytton et al.’s work through FEM analysis (45). S is a shear

coefficient, which as defined by Equation 5-40 is a function of the Poisson’s ratio.

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102

Surface Energies, ∆GhAB, ∆Gh

LW, and ∆Gf

To cause load-induced damage in the form of fatigue cracking, energy must be expended

and equally energy must be expended to close the fracture surfaces. Surface energy data thus

constitute input parameters for the healing, crack initiation, and propagation calculations in the

CMSE fatigue analysis (Equations 5-43 through 5-49). The respective equations for the SE data

analysis required for the CMSE approach based on adhesive mode of fracturing under dry

conditions are described in this subsection.

LWj

LWi

LWij

LWhG Γ+Γ+Γ−=∆ (Equation 5-43)

ABj

ABi

ABij

ABhG Γ+Γ+Γ−=∆ (Equation 5-44)

ABj

ABi

ABij

LWj

LWi

LWij

ABf

LWff GGG Γ+Γ+Γ−Γ+Γ+Γ−=∆+∆=∆ (Equation 5-45)

And;

( )2LWj

LWi

LWij Γ−Γ=Γ (Equation 5-46)

( )−+ΓΓ=Γ iiAB

i 2 (Equation 5-47)

( )( )−−−+ Γ−ΓΓ−Γ=Γ jijiAB

ij 2 (Equation 5-48)

( )−+ΓΓ=Γ jjABj 2 (Equation 5-49)

where:

Γ = Surface free energy of binder or aggregate (ergs/cm2)

i,j = Subscript “i” for binder (healing or fracture) and “j” for aggregate

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103

h,f = Subscript “h” for healing and “f” for fracture

LW = Superscript “LW” for Lifshitz-van der Waals component

AB = Superscript “AB” for Acid-Base component

+ = Superscript “+” for Lewis acid component of surface interaction

− = Superscript “−” for Lewis base component of surface interaction

Γij = Interfacial surface energy between binder and aggregate due to “LW” or

“AB” (superscripts) components (ergs/cm2)

∆G = Total surface free energy due to “h” or “f” (subscripts) for “LW” and/or

“AB” (superscripts) components (ergs/cm2)

Equations 5-43 through 5-47 are the nonpolar surface bond energy for healing, the polar

surface bond energy for healing, the interactive term for the nonpolar LW surface bond energy

component, and the polar surface energy component for binder, respectively. These equations

quantify the bond strength within the binder mastic and the binder-aggregate adhesion.

Equation 5-45 is the total bond strength energy for fracture, which is made up of the

Liftshitz-van der Waals nonpolar energy components and the acid-base polar energy

components. Equation 5-45 is also commonly known as the total bond strength or Gibbs free

energy of fracture for the binder (83).

According to Lytton et al., greater resistance to fracture, is provided by larger bond

strength (cohesive or adhesive), and a greater healing capacity is promoted by the smallest LW

bond strength and the largest AB bond strength (45). On this basis, the lower the value of ∆Gh,

the greater the potential to heal; the higher the value of ∆Gf,, the greater the resistance to fracture

for HMAC.

In the simplest fundamental theory of energy, if a relatively higher amount of energy is

required or must be expended to cause fracture damage (i.e., initiate and propagate a

microcrack through the HMAC layer), then the HMAC mixture is substantially resistant to

fracture. If, on the other hand, a higher amount of energy is required or must be expended to

repair the fracture damage (i.e., healing which is defined as the closure of fracture surfaces) that

occurred during the fracturing process, then the HMAC mixture has relatively less potential to

self heal.

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104

Relaxation Modulus, Ei, Exponent, mi, and Temperature Correction Factor, aT

The elastic relaxation modulus (Ei) and exponent (mi) were determined from RM

master-curves of log modulus (Ei) versus log time (t) obtained from tension and compression

RM test data at a reference temperature of 20 oC (68 °F) (68). From the RM master-curve, a

power function of relaxation modulus and loading time was generated as follows:

imiEtE −= ξ)( (Equation 5-50)

Tat

=ξ (Equation 5-51)

where:

E(t) = Elastic relaxation modulus (MPa)

Ei = Initial elastic modulus (MPa) @ ξ = 1.0 s

tension (Et) or compression (Ec)

ξ, t = Reduced and actual test time, respectively (s)

mi = Exponential stress relaxation rate (0 ≤ mi < 1)

i = Subscript “t” for tension and “c” for compression

Equation 5-50 is a simple power law relationship that is valid for most HMAC materials

at intermediate and/or long times of loading (68). The exponent mi refers to the rate of stress

relaxation.

The temperature correction factors (aT) were obtained through utilization of the SSE

regression optimization technique using the spreadsheet “Solver” function and the Arrhenius

time-temperature superposition model shown in Equation 5-52 (84). The reference temperature

was 20 °C (68 °F), and thus, the aT for 20 °C (68 °F) was 1.0.

( ) ⎟⎟⎠

⎞⎜⎜⎝

⎛−=

refaT TT

AaLog 11 (Equation 5-52)

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105

where:

Aa = Material constant that is a function of the activation energy (∆Ha) and

ideal gas constant (Rg) (i.e., Aa = ∆Ha/2.303Rg)

T = Test temperature in degrees Kelvin (K = 273 + °C)

Tref = Reference temperature of interest (°K) (Kref = 273 + 20 = 293)

A default Ca value of 13,631.28 for ∆Ha ≅ 261,000 J/mol and Rg ≅ 8.314 J/(mol.°K) is

often used. However, the constant Aa can also be obtained easily using the spreadsheet SSE

regression optimization analysis.

DPSE and Constant, b

Researchers determined the constant b from a combination of the RM test data (Et and mt)

in tension and the RDT test data. The constant b is defined as the rate of damage (energy

dissipation) due to repeated loading that primarily causes fracture at intermediate temperatures

(68, 85).

For any selected load cycle, the time-dependent linear visco-elastic stress (under

damaged or undamaged conditions) was calculated using the Boltzmann superposition

constitutive equation as a function of the RM and the RDT test data (68, 79, 85-86). A

temperature correction factor (aT) was also introduced into the constitutive equation to normalize

the calculated stress to a given reference temperature.

In this project, aT was obtained from RM analysis, and the selected reference temperature

was 20 °C (68 °F). This temperature is a realistic simulation of field service temperatures at

which HMAC is susceptible to fracture damage under traffic loading. The RDT test was

conducted at 30 °C (86 °F), and therefore, the calculated stress had to be normalized to 20 °C

(68 °F).

Secondly, pseudo strain for damaged conditions was calculated as a function of the

normalized calculated linear visco-elastic stress for damaged conditions, the reference modulus

(ER), and ψ(t) (68). In the analysis, calculated PS rather than physically measured strain is used

to characterize damage and healing to separate and eliminate the time-dependent visco-elastic

behavior of the HMAC material from real damage during the strain controlled RDT test (68).

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ER is the modulus of the undamaged material determined from the first load cycle of the

RDT test. Note that no significant fracture damage was considered to occur during the first

RDT load cycle. The ψ(t), which is a function of the calculated and measured stress at the first

load cycle in an assumed undamaged condition, is introduced primarily to account for any

non-linearity of the undamaged visco-elastic material.

Finally, DPSE was then calculated as a product of the measured stress and the calculated

PS for damaged conditions using the double meridian distance method (DMD) for traverse area

determination (68, 87). This DPSE is simply the area in the pseudo hysteresis loop of the

measured tensile stress versus the calculated pseudo strain plotted as shown in Figure 5-1. The

respective equations are:

( )∑= )()()( tttDPSE dm

dR σεψ (Equation 5-53)

R

dcd

R Et

t)(

)(σ

ε = (Equation 5-54)

)()(

)()1(

)1(

tt

t um

uc

σσ

=Ψ (Equation 5-55)

)()( tt um

uc σσ ≠ , )()( tt d

mdc σσ ≠ (Equation 5-56)

)()()( )...2()1()1( ttt dNc

dc

uc σσσ ≠= , )()()( )...2()1()1( ttt d

Nmdm

um σσσ ≠= (Equation 5-57)

( ) τττε

τσ dd

tEtt

c)()(

0

∂−= ∫ (Equation 5-58)

Equation 5-58 is the general uniaxial stress-strain relationship applicable to most linear

visco-elastic materials including HMAC (68, 85). For a haversine-shaped input strain waveform,

Equation 5-58 can be written in the simple approximate numerical-integration form shown in

Equation 5-59:

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107

( )[ ]( )∑+=

=

−+∞+ −+∆=

1

0111 )(

ik

k

mkikic ttEECt τσ (Equation 5-59)

Assuming E∞ is zero, and using Et and mt for undamaged conditions and aT from RM

analysis, Equation 5-59 reduces to Equation 5-60 shown below:

∑+=

=

++ ⎟

⎜⎜

⎥⎥⎦

⎢⎢⎣

⎡⎟⎟⎠

⎞⎜⎜⎝

⎛ −∆=

1

0

11

)()(

ik

k

m

T

kitkic

t

att

ECt τσ (Equation 5-60[a])

∑+=

=

++ ⎟

⎜⎜

⎛⎟⎟⎠

⎞⎜⎜⎝

⎛ −∆=

1

0

11

()(

ik

k

m

T

kiktic

t

att

CEt τσ (Equation 5-60[b])

where:

)()1( tucσ = Calculated time-dependent linear visco-elastic tensile stress in an assumed

undamaged condition at the first load cycle (kPa)

)(tdcσ = Calculated time-dependent linear visco-elastic tensile stress under

damaged conditions at any load cycle other than the first (kPa)

ti+1,tk = Present and previous time, respectively (s)

τ = Loading time history, e.g., 0.0 to 0.10 s at which strains were measured (s)

∆τ = Time increment (s) (e.g., 0.005 s)

E(t-τ) = Tensile relaxation modulus in assumed undamaged condition at time t-τ

(MPa)

ε(τ) = Measured strain at previous time,τ (mm/mm)

Ck = Mean slope of any segment of the haversine input strain waveform

)(tdRε = Calculated pseudo strain for damaged conditions (mm/mm)

ER = Reference modulus for assumed undamaged material calculated from the

first load cycle (MPa)

ψ(t) = Dimensionless non-linearity correction factor (NLCF)

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108

)()1( tumσ = Measured tensile stress for assumed undamaged condition at the first load

cycle (MPa)

)(tdmσ = Measured tensile stress for damaged conditions (kPa)

aT = Temperature correction factor (from relaxation modulus analysis)

DPSE = Dissipated pseudo strain energy (J/m3)

g = Acceleration due to gravity (m/s2)

For a haversine-shaped input strain waveform, both the measured and approximate

(calculated) stress should exhibit a shape form of the format shown in Figure 5-15.

0 0.02 0.04 0.06 0.08 0.1 0.12

Time, s

Stre

ss

Figure 5-15. Output Stress Shape Form from RDT Test.

DPSE for selected laboratory test load cycles (N) was then plotted against log N to

generate a linear function of the format shown in Equation 5-61. The constant b in Equation 5-61

also defined as the rate of change in DSPE during microcrack growth, is simply the slope of the

DPSE versus log N plot, which is the required input parameter for the CMSE fatigue analysis

(68).

( )NbLogaWR += (Equation 5-61)

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109

where:

WR = DPSE (J/m3)

a = Constant or DPSE at the first load cycle

b = Slope of WR-log N plot

N = Load cycle

A plot of DPSE versus log N should exhibit a simple linear graph of the format shown in

Figure 5-16.

WR = a + b Log N

Log N

WR (J

/m3 )

Figure 5-16. Example of WR – Log N Plot.

The constant b is inversely related to the HMAC mixture fatigue resistance. Generally, a

comparatively small value of b is indicative of a relatively low rate of accumulation of micro

fatigue damage and consequently high HMAC mixture fatigue resistance.

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Crack Density, CD

Crack density calculations were based on the cavitation analysis by Marek and Herrin

(88) assuming a brittle mode of crack failure for the HMAC specimen (Figure 5-17). In their

analysis, Marek and Herrin used an average microcrack length of 0.381 mm (0.015 inches) based

on 281 HMAC specimens (88). Using these data, the research team calculated microcrack

density as a function of the number of cracks per specimen cross-sectional area to be 2.317 mm-2

(1495 in-2). This is the crack density value (2.317 mm-2 (1495 in-2)) used for the CMSE fatigue

analysis in this project.

Areas indicating brittle crack failure

Figure 5-17. Brittle Crack Failure Mode (Marek and Herrin [88]).

Shear Strain, γ

FEM analysis software that takes into account the visco-elastic nature of HMAC is

desirable for pavement stress-strain analysis to determine the maximum design shear strain γ at

the edge of a loaded tire. If a linear elastic analysis software such as ELSYM5 (62) is used, an

adjustment to the calculated γ must be done to account for the visco-elastic nature of HMAC. In

this project, the research team adjusted the computed linear elastic γ consistent with the FEM

adjustment criteria discussed in Chapter 3.

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111

Input parameters for the stress-strain analysis include traffic loading (ESALs and the axle

and tire configuration), pavement structure and material properties defined as a function of

environment (temperature and subgrade moisture conditions), and desired response locations. If

linear-elastic conditions are assumed, Equation 5-62 can be used to calculate γ (79).

SGpσ

γ = (Equation 5-62)

where:

σp = Tire pressure (kPa) (~690 kPa ≅ 100 psi)

S = Shear coefficient

G = Shear modulus (MPa)

VARIABILITY, STATISTICAL ANALYSIS, AND Nf PREDICTION

A COV was utilized as an estimate of the variability of Ln Nf predicted by the CMSE

approach. The COV expresses the standard deviation as a percent of the mean as follows:

xsCOV 100

= (Equation 5-63)

where:

COV = Coefficient of variation

s = Sample standard deviation

x = Sample mean, calculated based on replicate measurements of Nf

The COV is basically a measure of relative variation, and it says that the measurements

lie, on the average, within approximately COV percent of the mean (20). Replicate Nf predictions

obtained by varying the material input parameters based on actual laboratory measured replicate

values also provided a reasonable measure of variability and precision of the CMSE approach.

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112

For this CMSE approach, mean Ln Nf values were predicted from laboratory measured

material properties (i.e., tensile strength [σt]) on at least two replicate specimens. For this

analysis, a typical spreadsheet descriptive statistics tool, supplemented by a one-sample t-test,

was utilized. A 95 percent confidence/prediction interval (CI) for the mean Ln Nf was then

computed as expressed by Equation 5-63 (with a one-sample t-test for an assumed t-value of

zero) under the normality assumption on the distribution of Ln Nf .

⎥⎦

⎤⎢⎣

⎡±=

− nstxN

nf 2,2

CI %95 α (Equation 5-63)

where:

CI = Confidence interval

x = Mean Ln Nf value

s = Standard deviation of Ln Nf

α = Level of significance, i.e., 0.05 for 95% reliability level

n = Number of replicate specimens/measurements

SUMMARY

The following bullets summarize the CMSE fatigue analysis approach as utilized in this

project:

• The CMSE approach was formulated on the fundamental concepts of continuum

micromechanics and energy theory. This approach utilizes the fundamental HMAC mixture

properties including tensile strength, fracture, healing, visco-elasticity, anisotropy, crack

initiation, and crack propagation to estimate Nf. The energy theory in this CMSE approach is

conceptualized on the basis that energy must be expended to cause load-induced damage in

the form of cracking (fracture), and equally, energy must be expended to close up these

fracture surfaces, a process called healing.

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• The computation of the critical design shear strain at the edge of a loaded tire within a

representative field HMAC pavement structure for Np analysis constitutes the failure

load-response parameter for this approach. The utilization of field calibration constants in

modeling the healing process, Ni, and Np constitute the calibration part.

• For this CMSE approach, the HMAC material is characterized in terms of fracture and

healing processes and requires only relaxation tests in uniaxial tension and compression,

tensile strength tests, repeated load tests in uniaxial tension, and a catalog of fracture and

healing surface energy components of asphalt binders and aggregates measured separately.

• HMAC mixture characterization by CMSE laboratory testing utilizes gyratory compacted

cylindrical specimens under strain and temperature controlled conditions.

• Fatigue failure according to the CMSE approach in this project was defined as the number of

repetitive load cycles that are required to initiate and propagate a 7.5 mm (0.30 inches)

microcrack through the HMAC layer thickness.

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115

CHAPTER 6 THE CALIBRATED MECHANISTIC APPROACH

WITHOUT SURFACE ENERGY

The calibrated mechanistic approach without surface energy measurements follows the

same analysis concept and failure criteria as the CMSE approach except for a few differences.

Laboratory testing differences include the absence of SE measurements and RM testing in

compression. The analysis is slightly different to account for the fact that some of the input data

(i.e., SE and RM in compression) are not measured. Figure 6-1 and Table 6-1 summarize the CM

fatigue design and analysis system and input/output data.

The fundamental concepts, failure criteria, statistical analysis, and Nf prediction are

similar to the CMSE approach (Chapter 5) and are therefore not discussed in detail again in this

chapter.

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116

NO

CM FATIGUE ANALYSIS

Pavement structure

Pavement materials

Traffic

Environment

Reliability

Nf Prediction

HMAC material characterization properties (from lab test or existing data from catalog)

Calibration, healing, & regression constants

Paris’ Law coefficients

Microcrack length failure threshold value

Design shear strain

Temperature correction factors

Anisotropy and healing shift factors

HMAC mixture fatigue resistance

Reliability factor (Q)

Nf ≥ Q × Traffic

YES

Final Fatigue Design

Figure 6-1. The CM Fatigue Design and Analysis System.

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117

Table 6-1. Summary of CM Fatigue Analysis Input and Output Data.

Source Parameter

Laboratory test data (HMAC mixture testing of cylindrical specimens)

- Tensile stress & strain - Relaxation modulus (tension) - Uniaxial repeated direct-tension test data (strain, stress, time,

& N) - Anisotropic data (vertical & lateral modulus)

Analysis of laboratory test data

- Tensile strength - Relaxation modulus master-curves (tension & compression) - Non-linearity correction factor - DPSE & slope of DPSE vs. Log N plot - Healing indices - Healing calibration constants - Creep compliance - Shear modulus - Load pulse shape factor

Field conditions (design data)

- Pavement structure (i.e., layer thickness) - Pavement materials (i.e.,elastic modulus & Poisson’s ratio) - Traffic (i.e., ESALs, axle load, & tire pressure) - Environment (i.e., temperature & moisture conditions) - Field calibration coefficients - Temperature correction factor

Computer stress-strain analysis - Design shear strain (γ) @ edge of a loaded tire

Others

- Reliability level (i.e., 95%) - Crack density - Microcrack length - HMAC brittle-ductile failure characterization - Stress intensity factors - Regression constants - Shear coefficient

OUTPUT

- Paris’ Law coefficients of fracture (A, n) - Shift factor due to anisotropy (SFa) - Shift factor due to healing (SFh) - Fatigue load cycles to crack initiation (Ni) - Fatigue load cycles to crack propagation (Np) - HMAC mixture fatigue resistance (Nf)

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118

LABORATORY TESTING

Unlike the CMSE approach, SE measurements (for both binders and aggregates) and

mixture RM tests in compression are not required in the CM approach. However, all other test

protocols are similar to that of the CMSE approach.

SE Measurements for Binders and Aggregates

The complete CMSE analysis procedure involves the determination of the surface

energies of both binder and aggregate. The required SE input parameters for Nf prediction in the

CMSE approach are used to calculate ∆Gf and ∆Gh. Determination of the SE components

required for determining these inputs (∆Gf and ∆Gh) is a time-consuming process, with the

current SE test protocol (the Wilhelmy Plate and USD) requiring approximately 70 hrs to

complete (Chapter 5).

Therefore, in order to improve the practicality of the CMSE approach, Nf were predicted

using the CM procedure without using SE (∆Gf and ∆Gh) as an input parameter. Consequently,

no SE measurements are required in this CM approach.

RM Test in Compression

Mixture RM data in compression are required in the CMSE approach primarily to

compute the SFh. As discussed in the subsequent section, SFh computation in the CM procedure

does not require RM data in compression (i.e., E1c and mc) as input parameters.

ANALYSIS PROCEDURE

In terms of analysis, the major difference between the CMSE and CM approaches is in

the computation of SFh and Paris’ Law fracture coefficients A and n. These differences are

illustrated subsequently.

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119

Shift Factor Due to Healing, SFh

Equation 6-1 expresses the computation of SFh in the CM approach.

6

51g

TSF

rh a

tgSF ⎟⎟⎠

⎞⎜⎜⎝

⎛ ∆+= (Equation 6-1)

ESALs Traffic 8010536.31 6

kNP

t DLr

×=∆ (Equation 6-2)

where:

∆tr = Rest period between major traffic loads (s)

aTSF = Temperature shift factor for field conditions ( ≅1.0)

gi = Fatigue field calibration constants

PDL = Pavement design life (i.e., 20 years)

It is clear that unlike the CMSE approach, ∆Gf, E1c, and mc are not required as input

parameters for the computation of SFh in this CM approach.

Paris’ Law Fracture Coefficients, A and n

The modified and CMSE calibrated empirical Equations 6-3 and 6-4 based on Lytton et

al.’s work show the computation of Paris’ Law fracture coefficients A and n, respectively,

according to the CM approach (45).

⎟⎟⎠

⎞⎜⎜⎝

⎛+=

to m

ggn 1 (Equation 6-3)

( )⎪⎭

⎪⎬⎫

⎪⎩

⎪⎨⎧

+⎟⎟⎠

⎞⎜⎜⎝

⎛++

=t

ttg

EmmSin

mg

g

ππ log)(log1 4

32

10 (Equation 6-4)

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120

where:

A, n = Paris’ Law fracture coefficients

gi = Fatigue field calibration constants

mt = Stress relaxation rate from the tension RM master-curve

Et = Elastic modulus from tension RM master-curve (MPa)

σt = Mixture maximum tensile strength at break (kPa)

Fracture coefficients A and n are required as inputs for the determination of Ni and Np,

and subsequently Nf. The fatigue calibration coefficients gi are climatic dependent values that

were established by Lytton et al. (45) and shown in Table 5-4 in Chapter 5.

Note that empirical Equations 6-1 through 6-4 in this project were calibrated to the

CMSE approach by comparing the actual calculated numerical values to the corresponding

values obtained via the CMSE approach. Equation 6-4, for instance, is the modification of Lytton

et al.’s original Equation 6-5 (45).

( )⎪⎭

⎪⎬⎫

⎪⎩

⎪⎨⎧

+⎟⎟⎠

⎞⎜⎜⎝

⎛+

=t

ttg

EmmSin

mg

g

ππ log)(log 4

32

10 (Equation 6-5)

The A values computed using this empirical Equation 6-5 differed from the CMSE A

values by about 10 times (i.e., ACMSE ≅ 10 × ACM). Consequently, Equation 6-5 was modified as

shown in Equation 6-4 to match the CMSE results. However, more HMAC fatigue

characterization is required to further validate the simplified CM approach.

SUMMARY

The CM fatigue analysis approach, as utilized in this project, is summarized as follows:

• The CM approach follows the same concepts, failure criteria, and Nf prediction procedure as

the CMSE approach. The major differences stem from a reduced laboratory testing program

and resulting changes in the analysis procedure.

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121

• The CM does not require SE measurements (both binder and aggregates) and RM tests in

compression. Instead, these data inputs can be interpolated based on existing material

empirical relationships or obtained from existing catalogued data if desired.

• The SFh is computed primarily as a function of traffic rest periods, temperature shift factor,

fatigue calibration constants, pavement design life, and the design traffic ESALs. In contrast

to the CMSE approach, ∆Gf, E1c, and mc are not required as input parameters for the

computation of SFh in this CM approach.

• Paris’ Law fracture coefficients A and n are computed as a function of the material tensile

strength (σt), RM data in tension (E1t, mt), and fatigue field calibration constants (gi) using

empirically developed relationships that were calibrated to the CMSE approach.

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123

CHAPTER 7 THE PROPOSED NCHRP 1-37A 2002 PAVEMENT DESIGN GUIDE

This chapter summarizes the relevant aspects of the proposed NCHRP 1-37A 2002

Pavement Design Guide as utilized in this project. Further details can be found elsewhere

(3, 4, 89).

FUNDAMENTAL THEORY

The proposed NCHRP 1-37A 2002 Pavement Design Guide (M-E Pavement Design

Guide) adopts a ME approach for the structural design of HMAC pavements (3, 4, 89). There are

two major aspects of ME-based material characterization: pavement response properties and

major distress/transfer functions. Pavement response properties are required to predict states of

stress, strain, and displacement (deformation) within the pavement structure when subjected to

external wheel loads. These properties for assumed elastic material behavior are the elastic

modulus and Poisson’s ratio.

The major distress/transfer functions for HMAC pavements are load-related fatigue

fracture, permanent deformation, and thermal cracking. However, the focus of this project was

on fatigue characterization of HMAC mixtures, and therefore, only the fatigue analysis

component of the M-E Pavement Design Guide is discussed in this chapter. Figure 7-1 is a

schematic illustration of the fatigue design and analysis system for the M-E Pavement Design

Guide as utilized in this project.

Figure 7-1 shows that if the Nf prediction by the M-E Pavement Design Guide software in

terms of traffic ESALs is less than the actual design traffic ESALs, the following options are

feasible:

• reviewing/modifying the input data including the pavement structure, materials, traffic,

environment, reliability level, pavement design life, and analysis parameters (distress failure

limits);

• changing the HMAC mix-design and/or the material types; and

• changing the percentage crack failure criterion (i.e., 25 to 50 percent).

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124

Figure 7-1. The Fatigue Design and Analysis System for the M-E Pavement Design Guide

as Utilized in this Project.

Nf ≥ Design Traffic ESALS

YES

Final Fatigue Design

Nf Prediction

In terms of traffic ESALs for:

50% cracking in wheelpath

Binder & HMAC Mixture Characterization

Dynamic modulus testing

Binder DSR testing

Mixture volumetrics

NCHRP 1-37A PAVEMENT DESIGN GUIDE FATIGUE ANALYSIS

Pavement structure & materials

Traffic & environment

Reliability & design life

Analysis parameters

2002 Design Guide Software

Fatigue Analysis Model

Global Aging Model

Percent cracking in wheelpath

NO

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125

INPUT/OUTPUT DATA

The M-E Pavement Design Guide suggests a hierarchical system for materials

characterization. This system has three input levels. Level 1 represents a design philosophy of

the highest practically achievable reliability, and Levels 2 and 3 have successively lower

reliability. The Level 1 fatigue design procedure requires mixture volumetrics, dynamic modulus

(DM) values for HMAC mixture and a complex shear modulus for unaged binder as input

parameters. The binder data are used in the M-E Pavement Design Guide software to predict

mixture aging using the Global Aging Model (90). Field input data include traffic, pavement

structure, environment, and pavement design life. These input data requirements are summarized

in Table 7-1.

Table 7-1. Input/Output Data for the M-E Pavement Design Guide Software.

Source Parameter

Laboratory test data

- Dynamic modulus test data (i.e., temperature, frequency, & |E*| values)

- Binder DSR test data (i.e., temperature, G*, & δ values)

- Mixture volumetrics (i.e., binder content & AV)

Analysis of laboratory test data

- All calculations are software based

Field conditions (design data)

- Pavement structure (i.e., layer thickness) - Pavement materials (i.e., material type, elastic modulus,

Poisson’s ratio, gradations, and plasticity indices) - Traffic (i.e., AADT, axle load, & tire pressure) - Environment (i.e., climatic location) - Pavement design life (i.e., 20 years)

Computer stress-strain analysis

- All calculations are software based (utilized bottom-up crack failure mode in this project)

Other - Reliability level (i.e., 95%) - Analysis parameters (i.e., distress failure limits)

OUTPUT

- Percentage cracking in wheelpath - Nf in terms of traffic ESALs for 50% cracking in the

wheelpath - Assessment of adequate or inadequate performance

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126

For the output data in terms of fatigue cracking (alligator cracking), the software predicts

the percentage of fatigue cracking (along with other distresses) at any age of the pavement for a

given structure and traffic level under a particular environmental location. The failure criteria can

be set in two ways: setting the limit of percentage of cracks for a given number of traffic loads or

determining the number of traffic loads in terms of ESALS to reach a certain percentage of

cracks at a certain age of the pavement. In this project, the research team used the former

criteria.

The output data in this project thus consisted of percentage cracking in the wheelpath for

two input traffic levels of at least 2.5 and 5.0 million ESALs. Thereafter, Nf in terms of ESALs

was statistically determined for 50 percent cracking in the wheelpath.

LABORATORY TESTING

Characterization of the HMAC mixture and binder properties for Level 1 fatigue analysis

in the M-E Pavement Design Guide software requires the laboratory tests described in this

section.

Dynamic Shear Rheometer Test

Binder dynamic shear complex modulus (G*) and the phase angle (δ) required for

Level 1 fatigue analysis were measured using the standard DSR consistent with the AASHTO

test protocol designation TP5-98 (56). A minimum of two binder samples were tested, and test

results are shown in Table 2-1 (Chapter 2).

Dynamic Modulus Test

For Level 1 fatigue analysis, the M-E Pavement Design Guide software require the

dynamic modulus of the HMAC mixture measured over a range of temperatures and frequencies

using the dynamic modulus test. A typical DM test is performed over a range of different

temperatures by applying sinusoidal axial loading at different frequencies to an unconfined

specimen.

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127

Test Protocol

In this project, the DM test was conducted in accordance with the AASHTO designation:

TP 62-03 Standard Method of Test for Determining Dynamic Modulus of Hot Mix Asphalt

Concrete Mixtures at five test temperatures of -10, 4.4, 20, 38, and 54.4 °C (14, 40, 70, 100, and

130 °F) and six loading frequencies of 25, 10, 5, 1, 0.5, and 0.1 Hz (91).

DM is a stress-controlled test in compressive axial loading mode, and the test protocol in

this project involved applying a sinusoidal dynamic compressive-loading (stress) to gyratory

compacted cylindrical specimens of 150 mm (6 inches) in height by 100 mm (4 inches) in

diameter. Figure 7-2 shows the DM loading configuration.

Time (s)

Stre

ss

Load

Load

Figure 7-2. Loading Configuration for Dynamic Modulus Test.

The stress level for measuring the DM was chosen to maintain the measured resilient

strain (recoverable) within 50 to 150 microstrains, consistent with the TP 62-03 test protocol

(91). The order for conducting each test was from lowest to highest temperature and highest to

lowest frequency of loading at each temperature to minimize specimen damage. For each

temperature-frequency test sequence, the test terminates automatically when a preset number of

load cycles have been reached (91).

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128

Test Conditions and Data Acquisition

The sinusoidal axial stress waveform was supplied by the Universal Testing Machine

(UTM-25) shown in Figure 7-3. Axial deformations were measured via three LVDTs. The

research team conducted the DM test in an environmentally controlled chamber at test

temperatures of -10, 4.4, 20, 38, and 54.4 °C (14, 40, 70, 100, and 130 °F) for each specimen.

For each test temperature, the specimens were subjected to six consecutive loading frequencies

of 25, 10, 5, 1, 0.5, and 0.1 Hz.

Figure 7-3. The Universal Testing Machine.

The minimum conditioning period for the specimens for each test temperature was

2 hrs. This temperature was monitored and controlled through a thermocouple probe attached

inside a dummy HMAC specimen also placed in the environmental chamber. For each mixture

type, three replicate HMAC specimens were tested, but only for 0 months aging condition. Note

that the M-E Pavement Design Guide software encompasses a Global Aging Model that takes

into account binder aging in the fatigue analysis (90).

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During the DM tests, data (time, load, and deformations) were captured electronically

every 0.001 s. Figure 7-4 is an example of the compressive axial strain response from DM

testing at 4.4 °C (40 °F).

Figure 7-4. Compressive Axial Strain Response from DM Testing at 4.4 °C (40 °F).

The typical parameters, which result from DM testing, are the complex modulus (E*) and

the phase angle (δ). The E* is a function of the storage modulus (E′ ) and loss modulus (E″).

The magnitude of the E* is represented as shown in Equation 7-1.

0

0*εσ

=E (Equation 7-1)

δCosEE *' = (Equation 7-2)

δSinEE *"= (Equation 7-3)

where:

0σ = Axial stress (MPa)

0ε = Axial strain (mm/mm)

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However, the E* calculations were automatically done concurrently via the UTM-25

software during DM testing. Table 7-2 is an example of the output data from DM testing using

the UTM test setup. The E*, frequency, and temperature are actual input data to the M-E

Pavement Design Guide software.

Table 7-2. Example of Output Data from DM Testing at 4. 4 °C (40 °F).

Frequency (Hz) Parameter (summed average) 25 10 5 1 0.5 0.1

Dynamic modulus (|E*|)(MPa) 19,056 17,538 16,078 13,343 12,118 9,432Phase angle ( °) 5.24 8.31 9.84 13.15 14.95 18.99Dynamic stress (kPa) 1567.7 1713.6 1653.9 1683.0 1607.7 1505.6Recoverable axial microstrain 82.3 97.7 102.9 126.1 132.7 150.6Permanent axial microstrain 106.6 152.1 160.9 173.7 175.4 271.1

Temperature (°C) 4.4 4.4 4.4 4.4 4.4 4.4

For generating the E* master-curve as a function of loading time or frequency, the

following time-temperature superposition signomoidal model, as demonstrated by Pellinen et al.,

is often used and is in fact built in the M-E Pavement Design Guide software (92):

)log(1*)( ξγβ

αδ−+

+=e

ELog (Equation 7-4)

where:

E* = Complex modulus (MPa)

ξ = Reduced frequency (Hz)

δ = Minimum modulus value (MPa)

α = Span of modulus values

β = Shape parameter

γ = Shape parameter

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FAILURE CRITERIA

The fatigue failure criteria for the M-E Pavement Design Guide software in this project

was defined as the number of traffic ESALs required to cause 50 percent alligator cracking

(bottom-up) on a 152.4 m (500 ft) stretch of the wheelpath. This 50 percent threshold value is

consistent with the TxDOT tolerable limit based on the 2003 TxDOT PMIS report (61).

ANALYSIS PROCEDURE

The fatigue analysis procedure for the M-E Pavement Design Guide is a step-by-step

computerized process based on the modified Asphalt Institute predictive model incorporated in

the software (21, 89).

( ) ( ) 332211

kktff

ff EkN ββεβ −−= (Equation 7-5)

where:

Nf = Number of repetitions to fatigue cracking

εt = Tensile strain at the critical location of the HMAC layer

E = Stiffness of the HMAC mixture

βfi = Calibration parameters

ki = Laboratory regression coefficients

The βfi calibration parameters incorporate state/regional/national calibration coefficients.

In this project, default national calibration factors, which are inbuilt in the M-E Pavement Design

Guide software, were used. Regression coefficients ki are coefficients that relate to material

properties. E is the stiffness of the HMAC mixture, which the M-E Pavement Design Guide

software determines from the DM test data during that analysis. The horizontal tensile strain (εt)

constitutes the mechanistic failure load-response parameter and was computed at the bottom of

the HMAC layer in this project.

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As pointed out previously, the M-E Pavement Design Guide incorporates a Global Aging

Model that takes into account the effects of binder aging with time in the overall fatigue analysis

process (3, 4, 89, 90). The model is based on the change in binder viscosity as a function of

pavement age, AV, environment, traffic loading, and pavement depth to account for both short-

term aging that occurs during mixing and construction operations and long-term aging during

service. The output of the Global Aging Model (GAM) is basically a prediction of the binder

viscosity at any time and any depth in the pavement system, which is ultimately incorporated in

the overall fatigue analysis process.

VARIABILITY, STATISTICAL ANALYSIS, AND Nf PREDICTION

For traffic input levels of 2.5 and 5.0 million ESALs and for each mixture type in each

pavement structure and under each environmental condition, the research team predicted the

percentage cracking in the wheelpath for at least two HMAC specimens using the M-E Pavement

Design Guide software. Using these percentages, cracking output from the M-E Pavement

Design Guide software for these specimens, mean Nf values in terms of ESALs were statistically

predicted for 50 percent cracking. A 95 percent prediction interval was also determined using

the least squares line regression analysis.

SUMMARY

The bullets below summarize the fatigue analysis component of the M-E Pavement

Design Guide as utilized in this project:

• The M-E Pavement Design Guide adopts a ME approach for the structural design of HMAC

pavements. In terms of fatigue analysis, the M-E Pavement Design Guide software utilizes

the modified Shell Oil fatigue damage predictive equation with tensile strain as the primary

mechanistic failure load-response parameter associated with crack growth.

• The M-E Pavement Design Guide software incorporates binder aging effects analysis using a

Global Aging Model. It also incorporates comprehensive traffic and climatic analysis

models.

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• The Guide characterizes pavement materials in a three-level hierarchical system, with Level

1 representing the possible highest achievable reliability level.

• For Level 1 fatigue input analysis, HMAC mixture characterization through dynamic

modulus testing at five different temperatures and six loading frequencies utilizes gyratory

compacted cylindrical HMAC specimens. Other required material tests include mixture

volumetrics and binder DSR data.

• Fatigue failure for the M-E Pavement Design Guide software analysis was defined as the

number of applicable repetitive load cycles expressed in terms of traffic ESALs required to

cause 50 percent cracking in the wheelpath.

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CHAPTER 8 BINDER OXIDATIVE HARDENING BACKGROUND AND TESTING

METHODOLOGY

Binder oxidation is a major contributor to age-related pavement failure (93). Through

oxidation, the binder becomes stiffer and more brittle and thus less able to sustain, without

damage, the deformations of flexible pavements. This project investigated the role that this

binder embrittlement plays in the phenomenon of fatigue resistance.

This chapter includes further discussion of 1) binder oxidation and embrittlement in both

laboratory and pavement aging, 2) the objectives of binder measurements in understanding

pavement fatigue resistance, and 3) the experimental methodology used in this project to

evaluate binder aging and to relate it to HMAC mixture properties.

BINDER OXIDATION AND EMBRITTLEMENT (52, 93)

As briefly introduced above, binders experience hardening and embrittlement over time

that reduces the performance of flexible pavements. The process is relentless and thus, over

time, can destroy the pavement. The constancy of the hardening rate over time and the depth to

which oxidation occurs, based on recent pavement data, is surprising and at the same time

critical to understanding pavement durability for both unmodified and modified binders.

As binders oxidize, carbonyl (– C=O) groups are formed that increase the polarity of their

host compounds and make them much more likely to associate with other polar compounds. As

they form these associations, they create less soluble asphaltene materials, which behave like

solid particles. This composition change, taken far enough, results in orders-of-magnitude

increases in both the binder’s viscous and elastic stiffness properties. Thus the oxidized binder

sustains sheared stress with deformation (high elastic stiffness) and simultaneously the material

cannot relieve the stress by flow (high viscosity), resulting in a pavement that is very brittle and

susceptible to fatigue and thermal cracking.

The Maxwell model is a very simple way of explaining, in a qualitative sense, the

essence of the impact of this increase in both elastic stiffness and viscosity on elongational flow

of a binder. The model is that of an elastic spring in series with a viscous dashpot element, as

shown in Figure 8-1.

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Figure 8-1. The Maxwell Model.

The stress that builds in the combined element is the result of the balance between the

elastic modulus and the viscosity. Upon elongation at constant rate, the stress versus elongation

response rises in response to the elastic spring but then goes through a maximum value before

decaying over time in response to viscous flow. The value of the maximum stress depends upon

the relative values of the elastic modulus and the viscosity. The higher their values, the higher

the maximum stress; the lower the values, the lower the maximum stress. If the maximum stress

exceeds the failure stress of the material, then failure occurs.

This Maxwell model is very simple and certainly is too simple to quantitatively

characterize asphalt materials, but it still captures the basic elements that are important to

understanding binder failure that occurs due to oxidation and embrittlement. As asphalts

oxidize, they harden, a process that simultaneously increases its elastic stiffness and its viscosity.

Consequently, in the context of the Maxwell model, with aging and consequent hardening, a

binder cannot take as much deformation without building to a stress level that results in its

failure stress being exceeded. So, as binders age and harden, their ductilities decrease

dramatically. The binder ductility for a newly constructed pavement may be of the order of 30

cm (11.8 inches) (15 °C,1 cm/min) (59° F, 0.39 inches) where as the binder ductility of a

heavily aged pavement will be much lower, down to 3 cm (1.18 inches) or less.

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Literature reports emphasize the importance of a binder’s ductility to pavement

durability. Several studies report that a value of the 15 °C (59 °F) ductility at 1 cm/min (0.39

inches/min) in the range of 2 to 3 cm (0.79 to 1.18 inches) corresponds to a critical level for age-

related cracking in pavements (93, 94).

This embrittlement of binders has been captured with the discovery of a correlation

between binder ductility (measured at 15 °C, 1 cm/min) (59 °F, 0.39 inches/min) and binder

DSR properties (dynamic elastic shear modulus, G’ and dynamic viscosity, η’, equal to G”/ω)

shown in Figure 8-2. A very good correlation exists between binder ductility and G’/(η’/G’) (or,

equivalently G’/[G”/ωG’]), demonstrating the interplay between elastic stiffness and ability to

flow in determining binder brittleness, as discussed above in the context of the Maxwell model.

Figure 8-2. Correlation of Aged-Binder Ductility with the DSR Function G’/( η’/G’) for Unmodified Binders (52) (°F = 32 + 1.8(°C)).

This correlation is depicted on a “map” of G’ versus η’/G’ (Figure 8-3), which tracks a

pavement binder as it ages in service (94-96). This particular binder is from highway SH 21

between Bryan and Caldwell but represents the trends seen for all conventional binders.

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Figure 8-3. Binder Aging Path on a G’ versus η’/G’ Map (Pavement-aged Binders) (52)

(°F = 32 + 1.8(°C)).

On this type of plot, with increased aging, a binder moves, over time, from the lower

right toward the upper left as the result of increases in both the elastic stiffness and viscosity (but

note that G’ increases more than viscosity, i.e., G”/ω, because movement is toward the left with

smaller values of η’/G’. Note also the dashed lines that represent lines of constant ductility,

calculated from the correlation of Figure 8-2 below 10 cm (3.93 inches).

Recent evidence suggests that pavement binders age at surprisingly constant rates and to

surprising depths. Figure 8-3 illustrates this conclusion from Glover et al. contained in Research

Report 1872-2 (52), through measurements on highway SH 21 between Bryan and Caldwell; all

data shown in this figure are from a single station, #1277. This highway was constructed from

July 1986 to July1988 in three, 50 mm (2 inch) lifts. The solid symbols (with the exception of

the solid diamond) are binder measurements from cores taken from the third lift down from the

surface of the pavement, as originally constructed.

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With each lift being 50 mm (2 inches) thick, this bottom lift had 100 mm (4 inches) of

pavement material on top of it. (Note: In 2000, this pavement had a chip seal and overlay placed

on top of it, burying the original lifts even more.) Yet, even buried this deeply, its binder moves

across the DSR “map” in a relentless fashion and at about the same pace as the top lift (open

symbols). Binder from the 1989 bottom lift has an estimated ductility of 20 cm (7.87 inches) at

15 °C (59 °F). By 1996, it was reduced by aging to 5.6 cm (2.2 inches), and by 2002, it was less

than 5 cm (1.97 inches). Meanwhile, the top lift binder’s ductility was estimated to be 16 cm

(6.3 inches) in 1989, 4.5 cm (1.77 inches) in 1996, and about 4 cm (1.57 inches) in 2002. The

march across the DSR map was not that different for the top lift compared to the bottom lift.

Binder from the middle lift, taken in 1989 and 1992, is also shown and tracks well with the other

lifts. Note that the rolling thin-film oven test (RTFOT) plus pressure aging vessel laboratory-

aged binder matches the 1992 pavement-aged binder, suggesting that for this pavement, RTFOT

plus PAV is approximately equivalent to hot-mix and construction aging plus four years of field

pavement aging. These results are rather remarkable and strongly suggest, as noted above, that

oxidative aging rates are remarkably constant over time and, beyond the very top portion of the

pavement, proceed at remarkably uniform rates, at least to several inches below the surface of

the pavement.

Note that the literature reports that ductility values in the range of 2 to 3 cm (0.79 to 1.18

inches) for 15 °C (59 °F) at 1 cm/min (0.39 inches/min) appear to correspond to a critical level

for age-related cracking. Thus, the top-left corner of the pavement aging figure (Figure 8-3) is a

suspect region for pavement performance. While this region has not yet been verified

conclusively to be a critical zone, recent pavement data, including several long-term pavement

performance pavements, are consistent with this preliminary conclusion.

Clearly, binder properties change drastically over the life of a pavement. These changes

result in a dramatic decrease in flexibility and occur continuously throughout its service lifetime.

It is the objective of this project to investigate how these changes impact the fatigue resistance of

HMAC pavements. Ultimately, the objective is to predict reductions in pavement fatigue

resistance from laboratory measurements of binder oxidation and embrittlement.

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BINDERS STUDIED

Changes in binder properties with aging are to be related to changes in mixture properties

with the objective of learning how to predict changes in mixture (and ultimately pavement)

fatigue lives due to binder stiffening. To this end, a PG 64-22 unmodified binder was used in a

basic mixture (denoted as the Bryan Mixture), and a PG76-22 modified binder was used in a rut

resistant mixture (denoted as the Yoakum Mixture). These binders were tested in both aged and

unaged conditions. Chapters 3 through 7 discussed the aging and testing of HMAC mixtures. The

results from all of these tests are presented in Chapters 9 through 11.

Laboratory-Aged Binders

Two different methods of accelerated aging were used in this project. A stirred air flow

test (SAFT), which stimulates the hot mix process, was used for short-term aging comparisons

(97, 98). An environmental room at 60 °C (140 °F) and atmospheric pressure and 50 percent

relative humidity was used for long-term aging comparisons. Aging at 60 °C (140 °F) is used as

an approximation to field aging.

Neat (original) binder was aged by both of these means and subsequently tested; binder in

compacted mixes was aged in the 60 °C (140 °F) environmental temperature-controlled room

and had to be extracted and recovered before testing.

Binders Recovered from HMAC Mixtures

An effective extraction and recovery process is necessary to compare the properties of

mix-aged binder with those of the original binder. The process used in this project consisted of

two parts: 1) the extraction process, and 2) the filtration and recovery process.

At a mixture binder content of about 5 percent of total mass, approximately 150 g of

HMAC mixture were needed to obtain approximately 7 g of binder. The mixtures were broken

into small pieces with a hammer before extracting the binder from the HMAC specimens.

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Toluene and ethanol were used for the binder extraction process. A total of three

successive washes were used in the extraction process. For the first wash, 100 mL of toluene

was used to extract binder from the aggregate by contact for 20 minutes. The second and third

washes, also for 20 minutes each, used a 15 percent weight ethanol-toluene solution. The washes

were filtered two times using a new doubled coffee filter each time. The filtered solution was

then distributed among six 15 mL conical type tubes (approximately 12 mL solution per tube)

and centrifuged at about 3000 rpm for 10 minutes to remove aggregate from the solution.

The binder was recovered from the solvent with a Buchi, RE 111 rotovap. During

removal of the solvent, the bath temperature was kept at 100 oC (212 °F) to avoid hardening or

softening of the asphalt in dilute solution. When no more solvent could be detected visually

dripping from the condenser, the temperature was increased to 173.9 oC (345 °F) to ensure

sufficient solvent removal. The extraction and recovery procedure took from 3 to 4 hrs for each

specimen. Two replicates were extracted and recovered for each mixture, and the properties of

the recovered binders were compared to each other. When inconsistencies occurred in these

recovered binder properties, additional replicates were extracted, up to four replicates total for a

given mixture (99).

BINDER TESTS

Binder tests conducted included size exclusion chromatography, dynamic shear

rheometry, ductility, and fourier transform infrared spectroscopy. These tests are discussed in the

next sections, and results are presented and discussed in Chapters 9 and 11.

Size Exclusion Chromatography

After extraction and recovery, the binder was analyzed using Size Exclusion

Chromatography (SEC) to ensure complete solvent removal. Test samples were prepared by

dissolving 0.2 ± 0.005 g of binder in 10 mL of tetrahydrofuran (THF). The sample then was

sonicated for 30 minutes to ensure complete dissolution and filtered through a 0.45µm

polytetrafluoroethylene (PTFE) syringe filter. Samples of 100 µL were injected into 1000, 500,

and 50 Å columns in series with THF carrier solvent flowing at 1.0 mL/min.

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The chromatograms of binders obtained from the same replicate should overlay each

other. If there was any solvent residue in the binder, there was a peak located at 38 minutes on

the chromatogram (100).

Dynamic Shear Rheometer

A Carri-Med CSL 500 Controlled Stress DSR Rheometer measured the rheological

properties of the binder.

The rheological properties of interest were the complex viscosity (η) measured at 60 oC

(140 °F) and 0.1 rad/s (approximately equal to the low-shear rate limiting viscosity) and the

storage modulus (G’) and the dynamic viscosity (η’), both at 45 °C (113 °F) and 10 rad/s

measured in a frequency sweep mode. A 2.5 cm (0.98 inches) composite parallel plate geometry

was used with a 500 mm (19.5 inches) gap between the plates.

These rheological properties were used to understand how the physical properties of the

binder changed with time. DSR measurements also were important for deciding whether the

binder was changed in some way by the extraction and recovery process (98-100). If two

extraction and recovery processes yielded binders with matching SEC chromatograms but

significantly different complex viscosities, then at least one of the binders was suspected of

having undergone solvent hardening or softening.

Ductility

Ductilities for long-term aged original binder, aged 3 and 6 months in a 60 oC (140 °F)

room after SAFT for this report, were measured at 15 oC (59 °F) and an extensional speed of 1

cm (0.39 inches) per minute in accordance with ASTM D 113-86 (101). The ductility sample,

which had been made in a mold, had a 3 cm (1.18 inches) initial gauge length and a tapered

throat. The ductility was taken as the amount of extension in centimeters of the asphalt specimen

when the binder fractured at the tapered throat.

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Fourier Transform Infrared Spectroscopy

Carbonyl area (CA) was measured using a Galaxy 5000 fourier transform infrared

spectroscopy (FTIR) spectrometer with an attenuated total reflectance (ATR) zinc selenide prism

(99). CA is the area under the absorption band from 1650 to 1820 cm-1 (4231 to 4667 inches-1)

and relates directly to the oxygen content in the asphalt binder, and thus increases in CA are used

to quantify oxidative aging (102, 103).

SUMMARY

The bullets below provide a summary of binder oxidative hardening in relation to HMAC

mixture fatigue resistance and the testing methodology utilized in this project to characterize this

phenomenon:

• Binder oxidative aging is a major contributor to age-related pavement failure. The prime

objective of this chapter was to present a background of binder oxidative aging and analysis

methodology as a context for understanding the effect of binder aging on HMAC mixture

fatigue resistance, presented in Chapters 9 and 11.

• Over time, binders experience oxidative age-hardening that increases their elastic stiffness

and simultaneously reduces their ability to flow or relieve stress, thus making the binders

more brittle.

• The DSR function map of G’ versus η’/G’ is a useful method for tracking changes in a

binder’s rheology with aging in a way that relates at least for unmodified binders to binder

ductility and, we hypothesize, to HMAC pavement durability.

• The DSR, ductility, SEC and FTIR were the tests utilized in this project to characterize the

binder rheological and chemical properties of binders.

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CHAPTER 9 BINDER-HMAC MIXTURE CHARACTERIZATION

Pavements deteriorate over time and eventually require maintenance or rehabilitation.

While fatigue is considered to be a major factor leading to failure, binder embrittlement due to

oxidative aging almost certainly plays a significant role as well. One objective of this project

was to better understand the impact of oxidative aging on mixture fatigue resistance and on other

mixture properties in general.

Mixture fatigue studies and the extent to which it is impacted by oxidative aging are

documented elsewhere in this report. The effect of binder oxidative aging on fatigue was found

to be significant.

The purpose of the work reported in this chapter was to address other binder-mixture

relations besides fatigue. Of particular interest was the impact of binder aging on mixture

stiffness, as characterized by the mixture’s visco-elastic properties, and the relation of these

mixture properties to changes in binder properties.

Loose mix, aged according to AASHTO PP2 4 hrs short-term aging, was compacted,

tested in a nondestructive relaxation modulus procedure, aged further in a 60 °C (140 °F)

environmental room for intervals of 3 months (from 0 to 6 months), and tested again after each

of these aging intervals. In this way, the same physical specimen was tested at each aging level

so that the effect of binder aging could be determined independent of other mixture variables.

Replicate compacted mixture specimens were aged for the specified intervals and the binder

recovered and tested for DSR properties that could be compared to the mixture properties.

The remainder of this chapter provides further details of binder and mixture experimental

procedures, analysis procedures, and test results.

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AASHTO PP2 (135 °C for 4 hrs, Compact)

Extract & Recover Binders

Age @ 60 oC for 3, 6 Months

Binder Tests

Binder in Mixtures

METHODOLOGY

Changes in binder properties with aging are to be associated with changes in mixture

properties, with the objective of learning how to predict changes in mixture fatigue lives due to

binder stiffening by aging. Two different binders were used: a PG 64-22 from a basic mixture

design (denoted as the Bryan mixture) and a PG 76-22 from a rutting resistance mixture design

(denoted as the Yoakum mixture). Binders in mixtures were conditioned and tested as shown in

Figure 9-1.

Figure 9-1. Binder Oxidative Aging and Testing

(°F = 32 + 1.8(°C)).

Binder aging and the extraction and recovery process were explained in Chapter 8. The binder

tests included size exclusions chromatography and dynamic shear rheometry; details are also

described in chapter 8.

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Binder Data Analysis

'G and "G values were measured at three different temperatures (20, 40, 60 oC) (68, 104,

140 °F), and master-curves for 'G , "G were constructed using time-temperature superposition

(TTSP) at 20 oC (68 °F). Shift factor data as a function of temperature were modeled as shown in

Equation 9-1 (104):

1

2

( )log

( )ref

Tref

C T Ta

C T T− −

=+ −

(Equation 9-1)

where:

Ta = The shift factor at temperature T relative to the reference temperature refT

1 2,C C = Empirically determined coefficients

T = The selected temperature of interest, oC or K

refT = The reference temperature, oC or K

In addition to master-curves, the DSR function ( '/( '/ ')G Gη ), measured at 44.7 oC

(112.5 °F), 10 rad/sec but shifted to 15 oC (59 °F) 0.005 rad/sec by (TTSP), was used to track

changes in binders with oxidative aging (96).

HMAC Mixture Tests

The binder-mixture (BM) test protocol was similar to the CMSE relaxation modulus test

described in Chapter 6, except that the same HMAC specimen was repeatedly tested at different

aging conditions. Thus, data were obtained at each test temperature for which the only variable

mixture parameter was the aging condition of the binder; other mixture parameters (Void in

Mineral Aggregates (VMA), Void Filled with Asphalt (VFA), aggregate size distribution, and

configuration, etc.) were identical within the same specimen. The test was performed with both

mixtures (Bryan and Yoakum) at 0, 3 and 6 months aging conditions with at least two replicate

specimens for each mixture.

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Figure 9-2 is a schematic illustration of the BM characterization test plan with RM

testing.

Figure 9-2. Binder-Mixture Characterization Test Procedure (°F = 32 + 1.8(°C)).

Chapter 5 describes the RM test conditions and loading configuration. Note that RM

testing in this project was assumed non-destructive.

AASHTO PP2(HMAC Mixture @ 135 °C for 4 hrs, compact)

3rd RM Testing @ 10, 20, & 30 oC

(Total aging period = PP2 + 0 months)

Age HMAC compacted specimens @ 60 oC for 3 months (Total aging period = PP2 + 3 months)

Age HMAC compacted specimens @ 60 (Total aging period = PP2 + 6 months)

oC for 3 more months

1st RM Testing @ 10, 20, & 30 oC

2nd RM Testing @ 10, 20, & 30 oC

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HMAC Mixture Visco-Elastic Characterization

The data obtained from the tensile RM test includes the time-dependent elastic relaxation

modulus (E(t)), loading time (t), and test temperature (T). From these data, mixture visco-elastic

properties were determined for comparison with the binder visco-elastic properties. The

following procedure was used to estimate the mixture visco-elastic properties.

Elastic Modulus (E(t)) Master-Curve

A master-curve for E(t) was constructed at a reference temperature of 20 oC (68 °F) from

the data obtained at three different temperatures (10, 20, and 30 oC) (50, 68, and 86 °F) by using

the Williams-Landel-Ferry (WLF) TTSP procedures (104, 105). As an example, the master-

curve for E(t) in Figure 9-3 was constructed from data for a Yoakum mixture used for the

CMSE procedure.

Figure 9-3. Relaxation Master-Curve for 0 Month Aged

Yoakum Mixture Used for CMSE (°F = 32 + 1.8(°C)).

10-1 100 101 102 103 104101

102

103

104

Yoakum MixtureRef T=20

oC

Cal-E(t), MixPP2+0M from CMSE E(t), MixPP2+0M from CMSE

E(t)

(MPa

)

Reduced Time (sec)

E1=1000; m=0.011ln(tr)+0.46

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150

1 1 1( )( )

mm m

r r rT

tE t E E t E t Ea T

− −∞

⎛ ⎞= + ≅ = ⎜ ⎟

⎝ ⎠

( )rm aLn t b= +

While there are some obvious inconsistencies in the data, E(tr) was found to be well

represented by the model given by Equations 9-2 and 9-3:

(Equation 9-2)

(Equation 9-3)

where:

E(t), E(tr) = Time-dependent elastic modulus at time t (MPa)

E1 = Initial (tr = 1 sec) elastic modulus (MPa)

t = Time (s)

tr = Reduced time (s)

T = Temperature (oC)

a, b = Empirically determined coefficients

aT(T) = The shift factor at temperature T relative to

the reference temperature refT

The elastic modulus obtained by the RM test is a function of time because of the

visco-elastic nature of the HMAC mixture. Under deformation, the stress builds because of the

mixture’s elastic nature but then relaxes at fixed strain because of its ability to undergo viscous

flow. This relaxation is reflected in the decrease of E(tr) over time in the RM test. Therefore,

storage (elastic) and loss (viscous) moduli can be calculated from the E(tr) master-curve.

The m value in Equation 9-2 was assumed to be a function of time and temperature

according to Equation 9-3. Once the temperature shift factors are determined through TTSP

alignment of the data, and the model parameters E1, a, and b are estimated, E(tr) can be

calculated. Figure 9-3 shows the result for this example.

( )rT

tta T

=

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151

12 rt

ω ≅

1(1 )( )

2m

m mG G cos πωω −

Γ − ⎛ ⎞= ⎜ ⎟⎝ ⎠

'

1(1 )"( )

2m

m mG G sin πωω −

Γ − ⎛ ⎞= ⎜ ⎟⎝ ⎠

( )1

2 2 2*( ) ( ') ( ")G G Gω = +

11

( )( ) , 2(1 ) 2(1 )

rr

E t EG t Gν ν

= =+ +

Dynamic Mixture Storage and Loss Moduli

The elastic modulus is converted to a shear modulus according to Equation 9-4:

(Equation 9-4)

Converting to frequency by Equation 9-5:

(Equation 9-5)

the dynamic shear storage ( 'G ) and loss ( "G ) moduli are calculated by (45, 108):

(Equation 9-6)

and

(Equation 9-7)

and the magnitude of the complex dynamic shear modulus (G*) is given by:

(Equation 9-8)

where:

tr = Reduced time (s)

t = Actual loading time (s)

aT(T) = Temperature shift factor

m = Exponential stress relaxation rate (0 ≤ m < 1)

ν = Poisson’s ratio (≅ 0.33)

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152

G(t), G(tr) = Time-dependent shear modulus at time t ( MPa)

G1 = Initial shear modulus (MPa)

'( )G ω = Elastic (storage) dynamic shear modulus (MPa)

"( )G ω = Viscous (loss) dynamic shear modulus (MPa)

G*(ω) = Complex dynamic shear modulus (MPa)

Γ = Gamma function

For ν, the research team used a value of 0.33 for the HMAC mixture consistent with the

work done by Huang and Lytton et al. (45, 106). Γ is the Lap lace (or Euler) Gamma

transformation function that is widely used in many mathematical engineering applications.

The results of this procedure for the Yoakum mixture are shown in Figure 9-4. Note that

at higher frequencies (lower temperatures) the storage modulus dominates the loss modulus,

whereas at lower frequencies the reverse is true, typical of visco-elastic materials.

Mixture Visco-elastic (VE) Function

A visco-elastic function for mixtures can be calculated that is analogous to the DSR

function for binders. As a first trial in this project, an angular frequency was arbitrarily selected

where "/ 'G G is of the order of unity at 20 oC (68 °F), as it is for an aged binder at 15 oC (59

°F), 0.005 rad/sec. In this way, it was hoped that aging of the mixture would be readily observed

from the visco-elastic properties. If the frequency is too high or the temperature too low, then the

mixture would reflect elastic limit properties and not be sensitive to aging. So the VE function

was calculated as follows:

VE function = '/( "/( ' ))G G G ω at 20 oC (68 °F), 0.002 rad/sec (Equation 9-9)

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153

Figure 9-4. Shear Modulus Master-Curve for 0 Month Aged Yoakum Mixture used for

CMSE (°F = 32 + 1.8(°C)).

RESULTS

The test results are presented in three sections: recovered binder properties, mixture

visco-elastic properties, and binder-mixture relationships. As discussed at the beginning of this

chapter, aged mixture samples were prepared using the PP2 4-hr short-term procedure. This

aged mixture was then used to make replicate compacted mixtures. One of these replicates was

tested as is (PP2 + 0 months), then aged for three months in the 60 °C (140 °F) environmental

room (PP2 + 3 months) and tested again. The mixture test was the RM test conducted at 10, 20,

and 30 °C (50, 68, and 86 °F). This same specimen has now been aged to a total of 6 months,

but the testing was not complete in time for this report. Instead, a separate replicate sample was

aged for 6 months (PP2 + 6 months), and the corresponding RM data are reported in this chapter.

Binder was recovered from other replicate compacted and aged mixture samples and tested to

provide binder properties to compare to the tested mixtures. From both binder properties and the

corresponding mixture properties, the effect of binder hardening on mixtures was evaluated

directly and without the variability created by mixture parameters other than binder rheology.

10-4 10-3 10-2 10-1 100 101101

102

103

104

Yoakum Mixture from CMSE

G'(w)-MixPP2+0M G"(w)-MixPP2+0M G*(w)-MixPP2+0M

G',

G",

G* (

MPa

)

Angular Frequency (rad/sec)

Ref T=20 o

C

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154

Recovered Binder Results

Binder master-curves for the dynamic shear storage '( )G ω , loss "( )G ω , and complex

*( )G ω moduli were used to track changes in binder properties with aging. Figures 9-5 to 9-8

show the results for binders recovered from Bryan and Yoakum mixtures at three levels of aging.

Figures 9-5 and 9-6 show that the complex moduli increase with aging for both

unmodified (Bryan) and modified (Yoakum) binders. Figures 9-7 and 9-8 show that '( )G ω and

"( )G ω increase with aging. Furthermore, '( )G ω is greater than "( )G ω at high frequency, and

"( )G ω is greater than '( )G ω at low frequency at each aging level.

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155

Figure 9-5. Master-Curves of Recovered Binders for G*(ω) from Bryan Mixture

(°F = 32 + 1.8(°C)).

.

Figure 9-6. Master-Curves of Recovered Binders for G*(ω) from Yoakum Mixture

(°F = 32 + 1.8(°C)).

10-5 10-4 10-3 10-2 10-1 100 101102

103

104

105

106

Ref T=20 o

C

G*(PP2+0M) G*(PP2+3M) G*(PP2+6M)

G*(

Pa)

Angular Frequency (rad/sec)

Recovered Binder from Yoakum Mixture

10-5 10-4 10-3 10-2 10-1 100 101102

103

104

105

106

Ref T=20 o

C

G*(PP2+0M) G*(PP2+3M) G*(PP2+6M)

G*(

Pa)

Angular Frequency (rad/sec)

Recovered Binder from Bryan Mixture

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156

10-5 10-4 10-3 10-2 10-1 100 101101

102

103

104

105

106

Ref T=20 o

C

G'(PP2+0M) G"(PP2+0M) G'(PP2+3M) G"(PP2+3M) G'(PP2+6M) G"(PP2+6M)

G',

G"

(Pa)

Angular Frequency (rad/sec)

Recovered Binder from Bryan Mixture

10-5 10-4 10-3 10-2 10-1 100 101101

102

103

104

105

106

Ref T=20 o

C

G'(PP2+0M) G"(PP2+0M) G'(PP2+3M) G"(PP2+3M) G'(PP2+6M) G"(PP2+6M)

G',

G"

(Pa)

Angular Frequency (rad/sec)

Recovered Binder from Yoakum Mixture

Figure 9-7. Master-Curves of Recovered Binders for '( )G ω , "( )G ω from Bryan Mixture (°F = 32 + 1.8(°C)).

Figure 9-8. Master-Curves of Recovered Binders for '( )G ω , "( )G ω from Yoakum Mixture (°F = 32 + 1.8(°C)).

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157

DSR map aging paths for the binder recovered from aged Bryan and Yoakum mixtures

are shown in Figures 9-9 and 9-10, respectively.

In each case, the recovered binder moves upward and to the left with aging, as has been

observed previously with neat binder aging (52, 96). Interestingly, these two binder paths very

nearly overlap each other, although the Yoakum binder is stiffer than the Bryan binder at each

level of aging.

The curved, dashed lines shown are lines of constant ductility (cm at 15 oC, 1 cm/min)

(59 °F, 0.39 inches/min) that were determined for unmodified binders by Ruan et al. (52, 96); as

a binder ages, its ductility decreases. Kandhal (107) concluded that a ductility of 3 cm (1.18

inches) at 15 oC (59 °F) is a value that corresponds well to age-related cracking failure in HMAC

pavements.

Figure 9-9. DSR Function of Recovered Binders from Bryan Mixture (°F = 32 + 1.8(°C)).

100 200 300 400 500 600 700 8000.01

0.1

1

8

10

5

6

3 42

PP2 PP2+3M PP2+6M

G'(M

Pa)(

15 o C

, 0.0

05 ra

d/s)

η'/G'(s)( 15 oC, 0.005 rad/s)

Recovered Bryan DSR map

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158

100 200 300 400 500 600 700 8000.01

0.1

1

8

10

5

6

3 42

PP2 PP2+3M PP2+6M

G'(M

Pa)(

15 o C

, 0.0

05 ra

d/s)

η'/G'(s)( 15 oC, 0.005 rad/s)

Recovered Yoakum DSR map

Figure 9-10. DSR Function of Recovered Binders from Yoakum Mixture

(°F = 32 + 1.8(°C)).

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159

10-1 100 101 102 103 104101

102

103

104

Bryan MixtureRef T=20

oC

Cal-E(t), MixPP2+0M E(t), MixPP2+0M Cal-E(t), MixPP2+3M E(t), MixPP2+3M Cal-E(t), MixPP2+6M E(t), MixPP2+6M

E(t)

(MPa

)

Reduced Time (sec)

HMAC Mixture Results

Following the procedure described in the previous section for mixture analysis, tensile

RM master-curves were determined for both the Bryan and Yoakum mixtures. The results at a

reference temperature of 20 °C (68 °F) are presented in Figures 9-11 and 9-12.

Figure 9-11. Master-Curves of Bryan Mixture for E(t) (°F = 32 + 1.8(°C)).

Clearly, there are inconsistencies in the data, most notably toward the end of each

relaxation test, that make the master-curve determination problematic. The value of m in

Equation 9-2 is assumed to be a function of time (through Equation 9-3) to allow the master-

curves to be non-linear on the log-log plot, but the amount of curvature built into the model by

the value of a in Equation 9-3 is somewhat subjective. In addition, it is necessary to place

unequal weighting on different parts of each relaxation experiment when performing the time-

temperature shifting, and this weighting also is somewhat subjective. The net effect is that the

master-curves necessarily are subject to some degree of uncertainty. Additional experience with

this method and independent verification with other experiments (dynamic modulus, for

example) is necessary in order to achieve more confidence in the mixture visco-elastic

properties.

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160

Figure 9-12. Master-Curves of Yoakum Mixture for E(t) (°F = 32 + 1.8(°C)).

.

Note that the data for the PP2 and PP2 plus 3 months aging levels were obtained on the

same mixture specimens for both the Bryan and Yoakum mixtures. The PP2 plus 6 months data

for each mixture were from a different specimen, one used for the CMSE data analysis. Six-

month data on the 0 and 3 month specimens will be obtained as part of this project to complete

the 0, 3, and 6 month series on a single specimen.

The objective of obtaining a set of data at different aging levels from the same mixture

specimen is to study the effect of binder aging alone on mixture stiffness and visco-elastic

behavior. If different specimens are studied, then the whole host of mixture variables (aggregate

gradation, VMA, VFA, binder content, and aggregate alignment configuration) is brought in to

play, and greater variability in the aging data would result.

Clearly, oxidative aging stiffens the tensile RM of the mixture significantly, consistent

with stiffening of the neat binder with aging. Also noted is that the Bryan mixture is stiffer than

the Yoakum mixture at comparable levels of aging and test condition.

10-1 100 101 102 103 104101

102

103

104

Yoakum Mixture

Ref T=20 o

C

Cal-E(t), MixPP2+0M E(t), MixPP2+0M Cal-E(t), MixPP2+3M E(t), MixPP2+3M Cal-E(t), MixPP2+6M E(t), MixPP2+6M

E(t)

(MPa

)

Reduced Time (sec)

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161

From these tensile RM master-curves, dynamic shear moduli master-curves, also at a

reference temperature of 20 °C (68 °F), were calculated as defined by Equations 9-4 through 9-8.

The results are given in Figure 9-13 ( 'G , "G ) for the Bryan mixtures and in Figure 9-14

( 'G , "G ) for the Yoakum mixtures.

Figure 9-13. Master-Curves of Bryan Mixture for '( )G ω , "( )G ω (°F = 32 + 1.8(°C)).

Again, stiffening of the mixture with oxidative aging is evident as 'G , "G , and *G all

increase, and the crossover frequency (frequency at which ' "G G= ) moves to a lower frequency.

The effects of 60 °C (140 °F) aging for 0, 3, and 6 months beyond PP2 conditioning are evident

in Figures 9-11 and 9-12.

In addition, Figure 9-15 compares the complex dynamic shear moduli ( *G ) of the Bryan

and Yoakum mixtures. Note that *G increases with aging for both mixtures, and the Bryan

mixture is stiffer than the Yoakum mixture, which is most evident at the lower frequencies.

10-4 10-3 10-2 10-1 100 101101

102

103

104

Bryan Mixture

G'(w)-MixPP2+0M G"(w)-MixPP2+0M G'(w)-MixPP2+3M G"(w)-MixPP2+3M G'(w)-MixPP2+6M G"(w)-MixPP2+6M

G',G

"(M

Pa)

Angular Frequency (rad/sec)

Ref T=20 o

C

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162

Figure 9-14. Master-Curves of Yoakum Mixture for '( )G ω , "( )G ω (°F = 32 + 1.8(°C)).

Figure 9-15. Master-Curve Comparisons between Bryan and Yoakum Mixtures for G*(ω)

(°F = 32 + 1.8(°C)).

10-4 10-3 10-2 10-1 100 101101

102

103

104

Yoakum Mixture

G'(w)-MixPP2+0M G"(w)-MixPP2+0M G'(w)-MixPP2+3M G"(w)-MixPP2+3M G'(w)-MixPP2+6M G"(w)-MixPP2+6M

G',G

"(M

Pa)

Angular Frequency (rad/sec)

Ref T=20 o

C

10-4 10-3 10-2 10-1 100101

102

103

Bryan vs Yoakum Mixtures

Ref T=20 o

C

BRY-MixPP2+0M BRY-MixPP2+3M BRY-MixPP2+6M YKM-MixPP2+0M YKM-MixPP2+3M YKM-MixPP2+6M

G*(

MPa

)

Angular Frequency (rad/sec)

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163

Similar to the DSR map for the recovered binders, a visco-elastic property aging map can

be constructed from the mixture visco-elastic master-curves. As described previously, values

from the 20 °C (68 °F) reference master-curves at 0.002 rad/s were used to plot 'G versus

'/ 'Gη , and the results are shown in Figures 9-16 (Bryan) and 9-17 (Yoakum). Remember that

the PP2+6 months data are from different HMAC mixture specimens than the PP2+0 and PP2+3

months data.

Figure 9-16. VE Function of Bryan Mixture (°F = 32 + 1.8(°C)).

100 200 300 400 500 600 700 80010

100

1000

Mix PP2+0M Mix PP2+3M Mix PP2+6M

G'(M

Pa)(

20 o C

, 0.0

02 ra

d/s)

η'/G'(s)( 20 oC, 0.002 rad/s)

VE map for Bryan Mixture

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164

100 200 300 400 500 600 700 80010

100

1000

Mix PP2+0M Mix PP2+3M Mix PP2+6M

G'(M

Pa)(

20 o C

, 0.0

02 ra

d/s)

η'/G'(s)( 20 oC, 0.002 rad/s)

VE map for Yoakum Mixture

Figure 9-17. VE Function of Yoakum Mixture (°F = 32 + 1.8(°C)).

Binder-Mixture Comparisons

The mixture trends are obvious and very similar to the recovered binder DSR map. With

aging, the mixture moves to the left and upward due to binder stiffening. The good correlation

between the mixture and binder maps is shown in Figure 9-18, where the VE function

( '/( '/ ')G Gη ) is plotted against the DSR function. Interestingly, the slopes of the Bryan and

Yoakum plots are virtually identical, and differences are manifested primarily in an offset

(magnitude) of the two sets of data.

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165

Figure 9-18. VE Function vs. DSR Function (°F = 32 + 1.8(°C)).

SUMMARY

In this project, two HMAC mixtures were tested to obtain mixture visco-elastic properties

at three conditions (0, 3, and 6 months) of binder aging. Nondestructive tensile RM tests were

used to produce mixture dynamic shear storage and loss moduli master-curves. Binders

recovered from aged mixtures were used to determine corresponding master-curves for the

binder. From these binder-mixture aging experiments, the following results were obtained:

• Mixtures stiffen significantly in response to binder oxidative aging. Mixture stiffening

was reflected in both the tensile relaxation modulus and the dynamic shear moduli.

10-4 10-3 10-210-2

10-1

100

101

Yoakum Bryan

Mix

ture

(G

'/(η

'/G')

, MPa

/s),

20

o C, 0

.002

rad/

s

Binder ( G'/( η'/G') , MPa/s) , 15 oC, 0.005 rad/s

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166

• A mixture visco-elastic property map of 'G versus '/ 'Gη at the three levels of mixture

aging (PP2, PP2+3 months, PP2+6 months) provided a useful means of tracking mixture

stiffening with binder oxidative aging. This mixture VE map is analogous to the binder

DSR map developed in Project 0-1872 (52).

• A mixture VE function, defined as '/( '/ ')G Gη at 20 °C (68 °F), 0.002 rad/s correlated

linearly with the binder DSR function '/( '/ ')G Gη at 15 °C (59 °F), 0.005 rad/s.

• The Bryan (PG64-22) binder is softer than the Yoakum (PG76-22) binder. However, the

Bryan mixture is stiffer than the Yoakum mixture, at comparable angular frequency or at

comparable binder stiffness.

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167

CHAPTER 10 HMAC MIXTURE RESULTS AND ANALYSIS

This chapter presents the mixture results analyzed at a typical 95 percent reliability level.

For simplicity and because HMAC fatigue cracking is generally more prevalent at intermediate

pavement service temperatures, most of the laboratory tests were conducted at 20 °C (68 °F).

Otherwise, the results were normalized to 20 °C (68 °F).

MIXTURE PROPERTIES FOR PREDICTING Nf

Laboratory test results for mixture properties related to Nf predictions are presented in

this section for the three aging conditions (0, 3, and 6 months) for both Bryan and Yoakum

mixtures. These results, which include BB, tensile strength, relaxation modulus, DPSE, SE,

anisotropy, and dynamic modulus, represent mean values of at least two test specimens.

BB Laboratory Test Results

Table 10-1 is a summary of the BB fatigue test results conducted at two test strain levels

(374 and 468 microstrain) at 20 °C (68 °F) and 10 Hz frequency. These results are an average of

at least two test specimens per mixture type per aging condition. Detailed results are attached in

Appendix C.

Table 10-1. BB Laboratory Test Results.

Mean N Value Aging Condition

Bryan @ 374 Test

Microstrain

Bryan @ 468 Test

Microstrain

Yoakum @ 374 Test

Microstrain

Yoakum @ 468 Test

Microstrain

0 months 127,000 50,667 223,790 105,350

3 months 80,187 39,833 172,167 86,187

6 months 53,000 27,500 108,200 47,150

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168

In Table 10-1, N (without subscript f) refers to the average number of laboratory load

cycles or repetitions to fatigue failure during the BB test. Fatigue failure, as defined in Chapter 4,

is the point of 50 percent reduction in the initial HMAC flexural stiffness measured at the 50th

load cycle (2, 59). From Table 10-1, while N decreased significantly with aging for both

mixtures, the Yoakum mixture sustained higher N values at both strain levels for all aging

conditions compared to the Bryan mixture.

The reduction in N, which was approximately 25 and 50 percent after 3 and 6 months

aging, respectively, indicates that aging has a very significant effect on the HMAC mixture

fatigue resistance. The relatively higher N for the Yoakum mixture was possibly due to the

higher binder content (5.6 percent compared to 4.6 percent for the Bryan mixture by weight of

aggregate) and the effect of the SBS modifier.

Nf-εt Empirical Relationships

Figures 10-1 (a) and (b) show plots of the average N versus test εt on a log-log scale.

Based on these figures, empirical fatigue relationships of the power format shown in Table 10-2

were derived and used to estimate lab Nf. These empirical fatigue equations and material

constants (ki) in Table 10-2 were derived by fitting power regression trend lines through the N

data points in Figure s 10-1 (a) and (b), and were also checked using least squares line regression

analysis. Each N data point in Figure 10-1 is a mean value of three replicate measurements.

Table 10-2. Mixture Empirical Fatigue Relationships.

Materials Constants Aging Condition

Mixture Equation k1 k2

Bryan ( ) 0984.49101 −−×= tfN ε 1 × 10-9 4.0984 0 months

Yoakum ( ) 3603.37107 −−×= tfN ε 7 × 10-7 3.3603

Bryan ( ) 1205.36102 −−×= tfN ε 2 × 10-6 3.1205 3 months

Yoakum ( ) 0861.36105 −−×= tfN ε 5 × 10-6 3.0861

Bryan ( ) 9263.26105 −−×= tfN ε 5 × 10-6 2.9263 6 months

Yoakum ( ) 7047.38102 −−×= tfN ε 2 × 10-8 3.7047

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169

1.0E+04

1.0E+05

1.0E+06

1.0E+07

100 1000

Microstrain

Load

Cyc

les

(N)

Bryan, 0 MonthsBryan, 3 MonthsBryan, 6 Months

Figure 10-1(a). N vs. εt at 20 °C (68 °F) (Bryan Mixture).

1.0E+04

1.0E+05

1.0E+06

1.0E+07

100 1000

Microstrain

Load

Cyc

les

(N)

Yoakum, 0 MonthsYoakum, 3 MonthsYoakum, 6 Months

Figure 10-1(b). N vs. εt at 20 °C (68 °F) (Yoakum Mixture).

Note that the fatigue results in Figure 10-1 were based on two test strain levels for each

mixture per aging condition. For better Nf predictions and statistical analysis, more data points

(collected at more than two test strain levels) are recommended. Generally, more testing at

different strain levels would lead to a better fatigue relationship, but bearing in mind that BB

testing is quite a lengthy test. However, each data point in Figure 10-1 is a mean value of three

replicate measurements of different HMAC beam specimens.

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170

Tensile Strength (σt)

Table 10-3 is a summary of the average σt results measured at 20 °C (68 °F).

Figures 10-2(a) through 10-2(c) are examples of plots of tensile stress and strain at break as a

function of aging condition for each mixture.

Table 10-3. Mixture Tensile Strength.

Aging Condition Mixture Mean σt @

Break (psi)

Mean Tensile Strain (εf)

@ Break

Bryan 105 1245 × 10-6 0 months

Yoakum 123 3483 × 10-6

Bryan 112 689 × 10-6

3 months Yoakum 152 2342 × 10-6

Bryan 157 401 × 10-6

6 months Yoakum 184 851 × 10-6

Table 10-3 indicates that as the HMAC ages, it becomes more brittle, thus breaking under

tensile loading at a lower strain level (Figure 10-2). For both mixtures, the failure strain (εf) at

break decreased significantly on the order of at least 30 percent per mixture type. The research

team attributed this phenomenon to an increase in mixture brittleness due to binder oxidative

aging.

In terms of mixture comparison, the σt and εf values for the Yoakum mixture were higher

than that of the Bryan mixture at all aging conditions, indicating that for the test conditions

considered in this project:

• the Yoakum mixture was more ductile than the Bryan mixture, and

• the Yoakum mixture had a better resistance to tensile stress than the Bryan mixture.

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0

50

100

150

200

0 500 1000 1500 2000 2500 3000 3500 4000

Microstrain

Tens

ile S

tress

(psi

)

Bryan, 0 MonthsBryan, 3 MonthsBryan, 6 Months

Figure 10-2(a). Mixture Tensile Stress at 20 °C (68 °F) (Bryan Mixture).

0

50

100

150

200

0 500 1000 1500 2000 2500 3000 3500 4000

Microstrain

Tens

ile S

tress

( ps

i)

Yoakum, 0 Months

Yoakum, 3 Months

Yoakum, 6 Months

Figure 10-2(b). Mixture Tensile Stress at 20 °C (68 °F) (Yoakum Mixture).

Figure 10-2(c) is a plot of the εf values as a function of aging condition. The figure shows

the expected decreasing trend of the εf values at 20 °C (68 °F) as a function of binder oxidative

aging due to increasing mixture brittleness. The increased ductility of the Yoakum mixture is

apparent and is indicated by the comparatively higher εf values at all aging conditions, which are

almost double the Bryan mixture εf values.

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100

1,000

10,000

0 3 6

Aging Period (months)

Failu

re M

icro

stra

in

Bryan

Yoakum

Figure 10-2(c). Mixture Failure Tensile Strain (εf) at Break at 20 °C (68 °F).

Relaxation Modulus Master-Curves The RM test results in terms of the E1 and m values are summarized in Table 10-4, and

some examples are presented graphically in Figure 10-3 on a log-log scale. As expected, E1

increased with aging due to HMAC hardening and stiffening effects from oxidation of the

binder. This stiffening effect, however, also causes the material property parameter m, which

describes the rate at which the mixture relaxes the applied stress, to decrease. For visco-elastic

materials like HMAC, the higher the m value, the higher the ability of the mixture to relax the

stress and the greater the resistance to fracture damage.

Table 10-4. Mixture Relaxation Modulus (Tension) Test Data.

Average E1 (psi) Average m Aging Condition Bryan Yoakum Bryan Yoakum

0 months 208,100 178,785 0.3997 0.5116

3 months 675,600 389,325 0.3774 0.4513

6 months 1,010,215 633,505 0.2945 0.4273

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Note that the E(t) values in Figures 10-3(a) and (b) are plotted in metric units (where 1 MPa

≅ 145 psi). This was done in order to allow for easy comparison with the binder-HMAC mixture

master-curves discussed in Chapter 9 (which includes binder test results). Note that metric units

are typically used for binder test results, which is consistent with the PG specification used by

TxDOT for binders.

RM (Tension) Master-Curves, Tref = 20 oC

1.0E+01

1.0E+02

1.0E+03

1.0E+04

1.0E+05

0.01 0.1 1 10 100 1000 10000

Reduced Time (s)

E(t)

(MP

a)

Bryan, 0 MonthsBryan, 3 MonthsBryan, 6 Months

Figure 10-3(a). RM (Tension) Master-Curve at 20 °C (68 °F) (Bryan Mixture).

RM (Tension) Master-Curves, Tref = 20 oC

1.0E+01

1.0E+02

1.0E+03

1.0E+04

1.0E+05

0.01 0.1 1 10 100 1000 10000

Reduced Time (s)

E(t)

(MPa

)

Yoakum, 0 MonthsYoakum, 3 MonthsYoakum, 6 Months

Figure 10-3(b). RM (Tension) Master-Curve at 20 °C (68 °F) (Yoakum Mixture).

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174

From Table 10-4 and Figure 10-3, it is clear that the Bryan mixture, although designed

with a softer PG 64-22 binder, was relatively stiffer than the Yoakum mixture. This difference in

the stiffness is particularly more pronounced with aging, indicating that the Bryan mixture was

probably more susceptible to stiffness age-hardening compared to the Yoakum mixture. While

the Yoakum mixture exhibited comparatively lower E1 values, it exhibited higher m values at all

aging conditions. This result indicates that the Yoakum mixture had a relatively better potential

to relax the stress than the Bryan mixture.

Note also that for all aging conditions, the E1 values in compression were higher than the

values in tension and vice versa for the m values. This is an expected material response behavior

due to the generally higher compactive effort in the vertical direction and confirms the

anisotropic nature of HMAC.

RM Temperature Shift Factors, aT

The aT values plotted in Figure 10-4 were computed when generating the RM

master-curves at a reference temperature of 20 °C (68 °F) using the Arrehnius time-temperature

superposition model via spreadsheet SSE regression optimization analysis (84). The almost

overlapping graphs in Figure 10-4 indicate that the aT values are not very sensitive to HMAC

aging. These values, however, exhibit a linear relationship with temperature. Several

researchers, including Christensien et al. (109) have reported similar findings.

When comparing Figures 10-4(a) and 10-4(b), the aT values seem to be material

(mixture) dependent, as evidenced in Equations 10-1 and 10-2:

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175

Log aT = -0.1095T + 2.1978

-2

-1

0

1

2

0 5 10 15 20 25 30 35

Temperature, oC

Log

a T

Bryan, 0 MonthsBryan, 3 MonthsBryan, 6 Months

Figure 10-4(a). Temperature Shift Factors, aT at TRef =20 °C (Bryan Mixture)

(°F = 32 + 1.8(°C)).

Log aT = -0.132T + 2.6711

-2

-1

0

1

2

0 5 10 15 20 25 30 35

Temperature, oC

Log

a T

Yoakum, 0 MonthsYoakum, 3 MonthsYoakum, 6 Months

Figure 10-4(b). Temperature Shift Factors, aT at TRef =20 °C (Yoakum Mixture)

(°F = 32 + 1.8(°C)).

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• Bryan mixture

( ) 998.0 ,1978.21095.0 2 =+−= RTaLog T (Equation 10-1)

• Yoakum mixture

( ) 996.0 ,6711.2132.0 2 =+−= RTaLog T (Equation 10-2)

where:

aT = Temperature shift factor

T = Temperature of interest (°C)

Dissipated Pseudo Strain Energy and Fracture Damage

Figure 10-5 is a plot of the rate (denoted as constant b) of HMAC mixture fracture

damage accumulation as a function of the aging condition for each mixture. This constant b was

calculated as the slope of the plot of DPSE versus log N during RDT testing for each mixture

type and aging condition, with the test data normalized to 20 °C (68 °F). This parameter b is an

indicator of the rate of fracture damage accumulation under RDT testing.

0

1

2

3

4

0 3 6

Aging Period (months)

b

BryanYoakum

Figure 10-5. Mixture DPSE at 20 °C (68 °F): Constant b vs. Aging Condition.

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177

The increasing trend of the b value in Figure 10-5 for both mixtures is indicative that the

rate of fracture damage accumulation increased with aging. The relatively higher b values and

greater rate of change (slope of the graphs in Figure 10-5) of the b value with aging indicates that

the Bryan mixture was accumulating fracture damage at a much faster rate. This observation is

evidence that the Bryan mixture was perhaps more susceptible to fracture damage under RDT

testing than the Yoakum mixture.

Surface Energy

The average measured SE results in terms of ∆Gf and ∆Gh at 20 °C (68 °F) are shown in

Figure 10-6 as a function of aging condition. These SE results shown in Figure 10-6 represent

the mixture adhesive bond strengths under dry conditions in the absence of water at an ambient

temperature of about 20 °C (68 °F). A minimum of two samples were tested per aging

condition.

03

6

Bryan

Yoakum0

50

100

150

200

250

SE (ergs/cm2)

Aging Period (Months)

Figure 10-6(a). Mixture Fracture Energy (∆Gf), ergs/cm2

(adhesive, dry conditions).

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178

03

6

Bryan

Yoakum0

50

100

150

200

250

SE (ergs/cm2)

Aging Period (Months)

Figure 10-6(b). Mixture Healing Energy (∆Gh), ergs/cm2

(adhesive, dry conditions).

Based on simple energy theory concepts, the higher the ∆Gf value, the greater the

resistance to fracture damage, and the lower the ∆Gh value, the greater the potential to self heal.

With these relationships, the Yoakum mixture has a better adhesive bond strength to resist

fracture damage and a stronger potential to self heal, as indicated by the relatively higher fracture

and lower healing energies, respectively, compared to the Bryan mixture.

From the SE results in Figure 10-6, the effect on SFh and Paris’ Law fracture coefficient

A were determined as shown in Table 10-5. Table 10-5 shows that aging has a significant effect

on these parameters (A increased while SFh decreased with aging). Generally, a lower value of A

and higher value of SFh are indicative of greater resistance to fracture and ability to heal,

respectively.

Table 10-5. Paris’ Law Fracture Coefficient A and SFh Value.

Aging Condition Parameter Mixture

0 Months 3 Months 6 Months

Bryan 6.27 × 10-8 16.00 × 10-8 23.43 × 10-8

A Yoakum 5.31 × 10-8 14.01 × 10-8 20.64 × 10-8

Bryan 6.73 4.74 3.07SFh

Yoakum 7.26 4.76 3.81

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179

For the test conditions considered in this project, these limited SE results indicate that:

• ∆ Gf decreases and ∆Gh increases with aging.

• Binder oxidative aging reduces HMAC mixture resistance to fracture and ability to self

heal. Lytton et al. (94) reported similar findings.

• As indicated by the relatively higher ∆Gf and lower ∆Gh values, respectively, the

Yoakum mixture had a relatively better resistance to fracture damage and potential to self

heal than the Bryan mixture.

In terms of the Yoakum mixture exhibiting relatively better fracture and healing potential

properties, the PG 76-22 plus gravel aggregate for the Yoakum mixture as indicated by the SE

results exhibits a better adhesive bond strength with the corresponding binder than the

component material combination for the Bryan mixture. In other words, the PG 76-22 binder and

gravel aggregates were perhaps more compatible in terms of adhesive bond strength than the PG

64-22 and limestone aggregates for the Bryan mixture. Note that SE data are also often used as a

measure of material compatibility for HMAC mixture characterization.

The high SBS modified binder content could also have possibly played a role in the

relatively better fracture and healing properties of the Yoakum mixture compared to the Bryan

mixture. The research team recommends further laboratory HMAC mixture characterization to

further explore this issue.

Mixture Anisotropy

Table 10-6 shows the SFa results based on mixture AN testing at 20 °C (68 °F). Note that

anisotropy arises due to the fact the HMAC mixture properties, such as the elastic modulus, are

directionally dependent.

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Table 10-6. Mixture Anisotropic Results.

SFa Aging Condition

Bryan Yoakum

0 months 1.63 2.10

3 months 1.65 2.08

6 months 2.09 2.40

Average 1.79 2.19

Table 10-8 shows some degree of differences in the SFa results as a function of mixture

type and aging condition. Since anisotropy is predominantly controlled by particle orientation

due to compaction, the theoretical assumption is that HMAC mixtures should exhibit similar

anisotropic response under all aging conditions. Therefore, the cause of discrepancy could be

related to test variability.

Assuming that the SFa differences are primarily due to test variability and mixture

inhomogeneity, the mean SFa values for the Bryan and Yoakum mixtures can be averaged to be

1.79 and 2.19, respectively, for all aging conditions within an error tolerance of 15 percent (110).

In terms of the effect of mixture type, some difference in the SFa values is expected due to the

differences in the aggregate gradation that has an effect on the particle orientation during

compaction. However, since the 1.79 and 2.19 values do not differ by more than 15 percent, a

mean SFa value of 2.0 is not unreasonable for both the Bryan and Yoakum mixtures for all aging

conditions. Aparicio and Oj have reported similar findings (111, 112).

Dynamic Modulus Results

Appendix D includes the mixture |E*| results at 0 months aging condition required for

Level 1 fatigue analysis in the M-E Pavement Design Guide for estimating field Nf. And

Appendix E is an example of the predicted percent fatigue cracking (in terms of area coverage in

the wheelpath) from the M-E Pavement Design Guide software using the HMAC mixture data

contained in Appendix D. Note that because the M-E Pavement Design Guide software

incorporates Global Aging Model analysis in overall field Nf prediction, the research team

considered DM testing of aged mixtures (HMAC specimens) as unnecessary.

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181

HMAC MIXTURE FATIGUE LIVES (Nf)

In this analysis, the research team defined laboratory fatigue life (lab Nf) as the estimated

HMAC mixture fatigue resistance without inclusion of any shift factors to simulate field

conditions and environmental exposure. Field fatigue life (field Nf ) was then calculated as a

function of the field shift factors and the HMAC laboratory fatigue life (lab Nf).

Throughout this section and subsequent chapters, the units of fatigue life (lab or field Nf)

are defined and expressed in terms of the number of allowable load repetitions to fatigue failure

in the laboratory or traffic ESALs in the field. The reference temperature for all the Nf (lab and

field) results in this section was 20 °C (68 °F).

ME Lab Nf Results

The predicted mixture lab Nf results from ME analysis described in Chapter 4 for the five

pavement structures are attached as Appendix F. These results represent mean values of at least

two test specimens. The overall COV of Ln Nf considering both mixtures (Bryan and Yoakum)

and environmental conditions (WW and DC) ranged between 3.3 percent and 6.8 percent, with a

mean Lab Nf value of about 4.60 × 106. Although the COV seems to be relatively lower when

expressed in terms of Ln Nf, the 95 percent Nf prediction CI margin is very wide, suggesting a

high variability and low precision in the predicted Nf results particularly for the Yoakum mixture

with the modified binder. For example, for PS#1 and WW environment, the mean lab Nf and 95

percent Nf CI are 4.48 × 106 and 2.12 × 106 to 9.46 × 106 for Bryan mixture and 4.11 × 106 and

0.27 × 106 to 62.99 × 106, respectively. Clearly, there is very high variability associated with the

Yoakum mixture for this ME prediction. Inevitably, this result may suggest that the ME

approach utilized in this project may not work well with modified binders, and the results need to

analyzed and interpreted cautiously.

In terms of mixture lab Nf comparison and the effects of aging, Figure 10-7 shows an

example for one pavement structure designated as PS# 1 (Table 3-10) under WW environmental

conditions.

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182

1.0E+05

1.0E+06

1.0E+07

0 3 6

Aging Period (Months)

Lab

Nf

Bryan Yoakum

Figure 10-7. Mixture Lab Nf at 20 °C (68 °F) for PS#1, WW Environment

(Bryan vs. Yoakum Mixture) – ME Analysis.

For both mixtures, Figure 10-7 shows that Nf decreases with aging, and the Yoakum

mixture generally exhibited relatively higher Nf values compared to the Bryan mixture. This

trend was observed for all pavement structures in both the WW and DC environmental

conditions and is consistent with the prediction from the material property results reported in the

preceding sections.

Ln Nf variability in terms of COV was comparatively higher for the Yoakum mixture, on

the order of about 10 percent more than that of the Bryan mixture. This result is in agreement

with Rowe et al.’s suggestion that while the current ME test protocol and analysis procedure may

work well for unmodified binders (Bryan mixture), it may not be so with modified binders, and

thus the results must be analyzed and interpreted cautiously (113).

CMSE Lab Nf Results

Appendix G contains a list of the mixture Nf results consistent with the CMSE analysis

procedure described in Chapter 5. Like the ME approach, these results represent mean values of

at least two test specimens. In terms of variability, the overall COV of Ln Nf ranged between 1.9

and 2.9 percent.

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183

The overall 95 percent lab Nf prediction CI was 0.80 × 106 to 13.12 × 106 with a mean lab

Nf value of 6.10 × 106. Considering HMAC mixture inhomogeneity, test variability, and

experimental errors, these results are reasonable and indicate better precision compared to the

ME approach.

For the given pavement structure (PS# 1, Table 3-7) and environmental conditions

(WW), Figure 10-8 indicates that mixture lab Nf decreases with aging and the Yoakum mixture

exhibited higher lab Nf values at all aging conditions. Like the ME approach, this trend was

observed for all pavement structures in both the WW and DC environmental conditions and was

consistent with the measured CMSE mixture material properties.

1.0E+05

1.0E+06

1.0E+07

0 3 6

Aging Period (Months)

Lab

Nf

Bryan Yoakum

Figure 10-8. Mixture Lab Nf at 20 °C (68 °F) for PS#1, WW Environment

(Bryan vs. Yoakum Mixture) – CMSE Analysis.

CM Lab Nf Results

The predicted mixture CM Lab Nf results are tabulated in Appendix J and do not differ

significantly from the CMSE results both in terms of the Nf magnitude and variability.

Essentially, the mixture Nf results and performance trend were similar to the CMSE results for all

pavement structures and environmental conditions for all aging conditions. The mixture Nf,

when plotted as a function of aging condition, is shown in Figure 10-9 for PS# 1 under WW

environmental conditions.

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184

1.0E+05

1.0E+06

1.0E+07

0 3 6

Aging Period (Months)

Lab

Nf

Bryan Yoakum

Figure 10-9. Mixture Nf at 20 °C (68 °F) for PS#1, WW Environment

(Bryan vs. Yoakum Mixture) – CM Analysis.

Figure 10-9 shows that while the mixture Nf generally decreased with aging, the Yoakum

mixture exhibited relatively higher Nf values at all aging conditions. Table 10-7 shows that these

CM results are insignificantly different from the CMSE results. Both of these CM and CMSE

results (Table 10-7) are for the same pavement structure (PS# 1) under WW environmental

conditions.

Table 10-7. CM vs. CMSE Mixture Lab Nf Results for PS#1, WW Environment.

Mixture Lab Nf Aging Condition Mixture

CMSE CM

Difference

Bryan 6.31 × 106 6.29 × 106 -0.32% 0 months

Yoakum 7.88 × 106 7.28 × 106 -7.61%

Bryan 2.42 × 106 2.31 × 106 -4.55% 3 months

Yoakum 4.95 × 106 5.17 × 106 +4.44%

Bryan 0.94 × 106 0.91 × 106 -3.19% 6 months

Yoakum 3.23 × 106 3.13 × 106 -3.10%

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185

Overall, this correlation between the CM and CMSE Nf results suggests that the CM

approach can be utilized for mixture fatigue analysis in lieu of the CMSE approach, thus

minimizing costs in terms of both laboratory testing and data analysis. Note that SE

measurements (binder and aggregate) and RM tests in compression are not required in the CM

approach. However, this correlation between the CM and CMSE results was expected because

the CM empirical analysis models were modified and calibrated to the CMSE approach as

discussed in Chapter 5. Consequently, more independent HMAC mixtures need to be

characterized for fatigue resistance to validate this CM-CMSE correlation.

Mixture Field Nf Results – ME, CMSE, and CM Analyses

Figure 10-10 is an example of a plot of the field Nf results as a function of aging

condition for PS#1 under WW environmental conditions based on the ME, CMSE, and CM

analyses. Detailed field Nf results are contained in Appendix I. Note that field Nf is simply a

product of field shift factors (SFi) and the estimated lab Nf as described in Chapters 4 through 7.

For this analysis, 0 months aging at 60 °C (140 °F) was considered equivalent to 0 years, 3

months to 6 years, and 6 months to 12 years, respectively, in terms of HMAC pavement age (52).

Consequently, field Nf is plotted as a function of pavement age, as shown in Figure 10-10.

5.00E+06

y = 2E+07e-0.044x

R2 = 0.8446

y = 2E+07e-0.1484x

R2 = 0.9363

1.0E+05

1.0E+06

1.0E+07

1.0E+08

0 5 10 15 20 25 30

Pavement Age (Years)

Fiel

d N

f

Bryan Yoakum

Figure 10-10(a). Field Nf for PS#1, WW Environment – ME Analysis.

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186

5.00E+06

y = 1E+08e-0.1169x

R2 = 0.9756

y = 7E+07e-0.2034x

R2 = 0.9986

1.0E+05

1.0E+06

1.0E+07

1.0E+08

1.0E+09

0 5 10 15 20 25 30

Pavement Age (Years)

Fiel

d N

f

Bryan Yoakum

Figure 10-10(b). Field Nf for PS#1, WW Environment – CMSE Analysis.

5.00E+06

y = 1E+08e-0.1129x

R2 = 0.9933

y = 7E+07e-0.2054x

R2 = 0.9975

1.0E+05

1.0E+06

1.0E+07

1.0E+08

1.0E+09

0 5 10 15 20 25 30

Pavement Age (Years)

Fiel

d N

f

Bryan Yoakum

Figure 10-10(c). Field Nf for PS#1, WW Environment – CM Analysis.

Like for the lab Nf, these results indicate a decreasing trend for both mixtures with aging,

and the Yoakum mixture exhibits a high field Nf magnitude at all aging conditions. In fact,

Figure 10-10, indicates an exponentially declining Nf trend with aging for both mixtures, and the

rate of Nf decay is mixture dependent based on the slopes of the exponential trend lines fitted

through the Nf data points. Based on the 5 × 106 design traffic ESALs over a 20 year service life

at 95 percent reliability level, all fatigue analysis approaches indicate inadequate and adequate

theoretical fatigue performance for the Bryan and Yoakum mixture, respectively.

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187

Mixture Field Nf Results – The M-E Pavement Design Guide Analysis

The mixture field Nf results from the M-E Pavement Design Guide software analysis are

presented in Appendix I as mean values of at least two test specimens. Unlike the ME and

CMSE/CM approaches, these results represent field Nf values that incorporate laboratory-to-field

shift factors and effects of aging over a 20 year design period. Essentially, these field Nf results

represent the number of traffic ESALs that the HMAC pavement structure can carry over a 20

year design life prior to 50 percent fatigue cracking in the wheelpath. Figure 10-11 is an

example of the mixture field Nf results from the M-E Pavement Design Guide software analysis.

6.21E+06

4.71E+06

1.00E+00 5.00E+06 1.00E+07

Yoakum

Bryan

Figure 10-11. Field Nf for PS#1, WW Environment – M-E Design Guide Analysis.

The comparatively higher field Nf values of the Yoakum mixture for PS# 1 under the

WW environment shown in Figure 10-11 are consistent with the predictions made by the other

fatigue analysis approaches. Considering a 20-year design service life with traffic design ESALs

of 5.0 × 106, Figure 10-11 shows that only the Yoakum mixture passes the 50 percent wheelpath

cracking failure criterion at 95 percent reliability level. Among other factors, the research team

attributed the comparatively better performance of the Yoakum mixture in terms of higher field

Nf values to the higher binder content in the mixture. Note that binder content is a direct input

parameter in the M-E Pavement Design Guide software, and therefore, field Nf can be tied

directly to this parameter.

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188

DEVELOPMENT OF A CMSE-CM SHIFT FACTOR DUE TO AGING

As part of this project’s secondary objective, an attempt was made to develop a shift

factor (SFag) that accounts for binder oxidative aging when predicting mixture field Nf using the

CMSE and CM approaches. This section discusses the SFag development based on the binder

dynamic shear rheometer tests that were conducted by CMAC. The CMSE and CM field Nf

predictions using the developed SFag and field Nf at 0 months are also provided.

Theoretical Basis and Assumptions

In this analysis, the SFag was solely based on neat binder shear properties and the

following assumptions, where neat binder refers to binder not mixed with aggregate but that

directly aged in thin films:

• SFag was considered as a multiplicative factor that tends to reduce Nf , and therefore, its

magnitude was postulated to range between 0 and 1 (0 < SFag ≤ 1). A numerical SFag

value of 1 represents unaged conditions or no consideration of aging effects in Nf

analysis.

• SFag was only considered as a function of the neat binder properties in terms of the DSR

function (DSRf) and oxidative aging period (time). The hypothesis is that only the binder

in the HMAC mixture ages, and therefore, it is not unreasonable to determine SFag solely

based on binder properties. The idea is that researchers and/or end-users would only

measure unaged and aged binder properties without having to measure aged mixture

properties and thereafter estimate SFag and ultimately predict aged mixture field Nf from

unaged mixture field Nf.

• The DSRf was utilized on the hypothesis that this function provides a better representation

of the binder shear properties in terms of ductility and durability, properties that are

considered critical to fatigue performance for aged HMAC field pavements (52). The

DSR function’s correlation with ductility, durability, and HMAC pavement age is

discussed in Chapter 8 of this report.

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189

• The binder oxidative aging conditions as conducted by CMAC were consistent with the

stirred air flow test and pressure aging vessel (PAV*) procedures to simulate both short-

term aging that occurs during the hot-mixing process and construction operations and

long-term aging during service (97). These laboratory aging conditions were SAFT +

PAV* 0 hrs, SAFT + PAV* 16 hrs, and SAFT + PAV* 32 hrs, respectively, and simulate

approximately up to 6 years of Texas field HMAC aging exposure (52,97).

• In contrast to SAFT + PAV* laboratory aging of binders, field aging is a relatively

complex process involving fluctuating environmental conditions and a general decreasing

AV content due to traffic compaction. These factors were not directly taken into account

by the SFag developed in this study. It must also be emphasized that the effect of aging on

HMAC mixture fatigue resistance is considered as a three stage process involving binder

oxidation, binder hardening, and mixture field Nf decay. Additionally, mixture design

parameters such as binder content and polymer modification probably also play a

significant role in these three processes.

SFag Formulation and the Binder DSR Master-Curves

In this project, the SFag was formulated as a function of the DSR data from the binder

DSR master-curve, as shown by Equation 10-5.

[ ]w

ag tuSF )(χ= (Equation 10-5)

⎟⎟⎠

⎞⎜⎜⎝

⎛⎟⎟⎠

⎞⎜⎜⎝

⎛=

if

fi

tDSRtDSR

tmtm

t@@

@'@'

)()1(

0)1(

0

χ (Equation 10-6)

( )[ ]'/'/' GGDSRf η= (Equation 10-7)

( ) '

)1()( mff DSRDSR ϖϖ = (Equation 10-8)

where:

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190

SFag = Shift factor due to binder oxidative aging

χ(t) = Material property ratio that relates the aged to the unaged binder shear

properties as a function of time

u, w = Material regression constants

m′ = Slope of the binder DSRf ( ω) master-curve at a reference temperature of

20 °C (68 °F)

ϖ = Reduced angular frequency (rad/s)

DSRf(1) = ( )[ ]'/'/' GG η at 1 rad/s (Pa⋅s)

G’ = Elastic dynamic shear modulus (MPa)

η’ = Dynamic viscosity (Pa⋅s)

Figure 10-12 is a plot of the binder DSR master-curves on a log-log scale in the form of a

power function expressed by Equation 10-8. These binder DSR master-curves were generated

from DSR test data that were measured at three test temperatures of 20, 40, and 60 °C (68, 104,

and 140 °F), respectively within an angular frequency of 0.1 to 100 rad/sec. For analysis

simplicity, SAFT+PAV* 0 hr was assumed to be equivalent to 1 year Texas field HMAC

exposure, SAFT+PAV* 16 hrs to 2 years, and SAFT+PAV* 32 hrs to 6 years, respectively

(52). The SFag at 0 years field HMAC exposure was arbitrary assigned a numerical SFag value of

1.0 on the premise that no significant aging occurs during this period. Based on the data from

Figure 10-12 and using Equation 10-5 (with u ≅ w ≅ 1), SFag values were estimated as a function

of pavement age, as shown in Table 10-8.

Table 10-8. CMSE-CM SFag Values.

SFag Pavement Age (Years) PG 64-22 (Bryan) PG 76-22 (Yoakum)

0 1.000 1.000 1 0.854 0.783 2 0.330 0.303 6 0.160 0.221 12 0.073 0.109 18 0.049 0.081 20 0.045 0.070

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191

PG 64-22

y = 714860x2.0777

R2 = 0.9923

y = 2E+06x1.9256

R2 = 0.9936

y = 4E+06x1.8613

R2 = 0.9942

1.0E-08

1.0E-05

1.0E-02

1.0E+01

1.0E+04

1.0E+07

1.0E+10

1.0E+13

1.0E-06 1.0E-04 1.0E-02 1.0E+00 1.0E+02w (rad/s)

DS

Rf (P

a.s)

SAFT+PAV 0hrs SAFT+PAV 16hrs SAFT+PAV 32hrs

PG 76-22

y = 1E+06x1.9851

R2 = 0.9952

y = 3E+06x1.795

R2 = 0.9983

y = 4E+06x1.7519

R2 = 0.9987

1.0E-08

1.0E-05

1.0E-02

1.0E+01

1.0E+04

1.0E+07

1.0E+10

1.0E+13

1.0E-06 1.0E-04 1.0E-02 1.0E+00 1.0E+02

w (rad/s)

DSR

f (Pa

.s)

SAFT+PAV 0hrs SAFT+PAV 16hrs SAFT+PAV 32hrs

Figure 10-12. Binder DSRf(ω) Master-Curves at 20 °C (68 °F).

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192

Note that SFag values beyond 6 years field HMAC exposure were determined based on

the SAFT+PAV* 0 hrs, SAFT+PAV* 16 hrs, and SAFT+PAV* 32 hrs data. Additional

laboratory aging conditions are recommended, i.e., SAFT+PAV* 64hrs that may be realistically

close to a 20 year field HMAC exposure, which is consistent with typical HMAC pavement

design periods.

CMSE-CM Field Nf Prediction Using SFag

Using the SFag data in Table 10-8 and the field Nf at 0 years field HMAC exposure, the

field Nf at any pavement age can be estimated using the following relationship:

( ) ( ) ( )0 tftagtfNFieldSFNField

ii×= (Equation 10-9)

Table 10-9 provides an example of the estimated field Nf at year 20 for PS#1 and the WW

environment. Predictions for other PSs and the DC environment are contained in Appendix I.

Table 10-9. Example of Field Nf Predictions at Year 20 (PS#1, WW Environment).

Approach Mixture Field Nf Value @ Year 20

Bryan 3.11 × 106 CMSE Yoakum 8.40 × 106 Bryan 3.10 × 106 CM Yoakum 7.77 × 106

Design traffic ESALs over 20 year design period at 95 percent reliability level: 5.00 × 106

From Table 10-9, the field Nf estimate by the two approaches do not differ significantly.

In fact, both approaches indicate inadequate and adequate theoretical fatigue performance for

Bryan and Yoakum mixtures, respectively, based on a 5.00 × 106 design traffic ESAL over a

20-year design period at 95 percent reliability level. For this pavement structure (PS#1), these

results are comparable to the predictions by the M-E Pavement Design Guide of 4.71 × 106 and

6.21 × 106 for the Bryan and Yoakum mixtures, respectively. For the ME approach, the

predictions are approximately 1.03 × 106 and 8.30 × 106 for the Bryan and Yoakum mixture,

respectively, based on extrapolations and the exponential relationships in Figure 10-10(a).

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193

SUMMARY

In this chapter, the HMAC mixture results were presented and the following summarizes

the key findings (based on the test conditions considered in the project).

BB Testing

• The number of laboratory load cycles to failure denoted as N (without subscript f )

decreased with binder oxidative aging.

• The Yoakum mixture performed better in terms of the number of N to failure during BB

testing at 20 °C (68 °F).

Tensile Stress

• Due to more brittle behavior with binder oxidative aging, the mixture tensile failure strain

(εf) at break under tensile loading at 20 °C (68 °F) decreased significantly with aging.

• While the tensile stress at break (σt) did not vary significantly as a function of aging and

was within the expected test variability, the Yoakum mixture exhibited more ductility at

all aging conditions compared to the Bryan mixture.

• With aging, the failure mode under tensile loading for each mixture changed from ductile

to brittle, indicating a decrease in mixture ductility with aging.

Relaxation Modulus

• While the mixture elastic relaxation modulus (E1) increased with binder oxidative aging

due to stiffening effects, the RM results indicated that the Yoakum mixture had a better

potential to relax stress than the Bryan mixture based on a larger m value. However, as

expected, the ability to relax the stress (m value) generally decreased with aging for both

mixtures.

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194

• Although designed with a relatively softer PG 64-22 binder, the relaxation modulus (E1)

of the Bryan mixture was relatively higher than that of the Yoakum mixture designed

with a stiffer SBS modified PG 76-22 binder, particularly after aging. These results are

suggestive that for the test conditions considered in this project, the Bryan mixture was

perhaps more susceptible to stiffness age-hardening due to binder oxidative aging.

• The logarithm of the temperature shift factor (Log aT) determined when generating the

RM master-curves exhibited a linear relationship with temperature, but this parameter

was insensitive to binder oxidative aging conditions. By contrast, Log aT exhibited some

degree of sensitivity to HMAC mixture type.

DPSE and SE Results

• The DPSE results indicated that the Bryan mixture was more susceptible to fracture

damage than the Yoakum mixture, and the rate of fracture damage accumulation

generally increased with aging.

• The SE results indicated better adhesive bond strength for the Yoakum mixture relative to

the Bryan mixture, and mixture resistance to fracture and potential to heal as measured in

terms of SE magnitude generally decreased with aging.

Mixture Anisotropy

• Within a ±15 percent error tolerance, mixture anisotropy (SFa) was observed to be

insignificantly affected by binder oxidative aging and did not vary substantially as a

function of mixture type. Consequently, a mean SFa value of 2.0 was proposed for both

the Bryan and Yoakum mixtures for all aging conditions.

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195

Mixture Nf

• When comparing the two mixtures for the test conditions considered in this project:

­ The Yoakum mixture exhibited better fatigue resistance than the Bryan mixture in

terms of the magnitude of both lab and field Nf .

­ The Yoakum mixture was more resistant to fracture damage, had a better potential to

heal, and was less susceptible to aging compared to the Bryan mixture.

• An attempt was made to develop shift factors due to aging (SFag) based on the binder

DSR function for the CMSE and CM approaches. While the SFag methodology utilized

produced reasonable results, validation of these concepts is still required through testing

of additional binders and HMAC mixtures, possibly with longer laboratory aging periods

that realistically simulate current HMAC pavement design practices. The further

development of representative SFag, particularly as a function of time, with more research

will inevitably allow for realistic Nf predictions at any desired pavement age.

Furthermore, there is a need to incorporate mixture volumetric properties such as AV and

binder content in the SFag model. These volumetric properties are hypothesized to play a

significant role in the aging phenomenon of HMAC mixtures due to binder oxidation.

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CHAPTER 11 DISCUSSION AND SYNTHESIS OF RESULTS

This chapter compares and discusses the mixture field Nf results and variability including

the effects of other input variables, and binder oxidative aging. BM characterization and another

proposed methodology for the aging shift factor (SFaging) analysis for the CMSE approach are

also discussed.

COMPARISON OF MIXTURE FIELD Nf

Generally, all fatigue analysis approaches predicted higher Nf (both lab and field) values

for the Yoakum mixture under all aging and environmental conditions for all pavement

structures. Mixture property results discussed in Chapter 10 also indicated that the Yoakum

mixture had better fatigue resistant properties than the Bryan mixture and was therefore expected

to perform better in terms of Nf (lab or field) magnitude under the test conditions considered in

this project. Figure 11-1 is an example of the mixture field Nf for WW environmental conditions

for PS# 1.

1.0E+051.0E+061.0E+071.0E+081.0E+09

Field Nf

ME CMSE CM

BryanYoakum

Figure 11-1(a). Mixture Field Nf (0 Months, PS#1, WW Environment).

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198

1.0E+051.0E+061.0E+071.0E+081.0E+09

Field Nf

ME CMSE CM

BryanYoakum

Figure 11-1(b). Mixture Field Nf (3 Months, PS#1, WW Environment).

1.0E+051.0E+06

1.0E+071.0E+081.0E+09

Field Nf

ME CMSE CM

BryanYoakum

Figure 11-1(c). Mixture Field Nf (6 Months, PS#1, WW Environment).

Figure 11-1(a) represents field Nf values that were measured at 0 months with no

aging effects being considered. The 3 and 6 months field Nf results for the ME, CMSE, and CM

approaches in Figures 11-1(b) and (c) represent approximately 3 to 6 years of field aging (52).

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199

Figures 11-1(a), (b), and (c) show better fatigue resistance for the Yoakum mixture in

terms of field Nf magnitude. Note that the difference (Figure 11-1) in the field Nf values between

the two mixtures gets more significant as aging progresses, indicating that the Bryan mixture’s

fatigue life was decaying much faster than that of the Yoakum mixture. This result is consistent

with the material property results reported in Chapter 10.

The M-E Pavement Design Guide results represent field Nf values at year 20 and

incorporates laboratory-to-field shift factors and effects of aging through the GAM over the

entire 20 year design period and were not included in Figures 11-1(a), (b), and (c). These M-E

Pavement Design Guide results are included in Figure 11-1(d), which is an example of the

mixture field Nf prediction comparison based on a 20-year design life and 95 percent reliability

level for PS# 1 under the WW environment.

0.0E+00 5.0E+06 1.0E+07

Field Nf

ME

CMSE

CM

Design Guide

Bryan Yoakum

Figure 11-1(d). Mixture Field Nf Comparison (PS#1, WW Environment)

For all the fatigue analysis approaches, Figure 11-1(d) shows better fatigue resistance for

the Yoakum mixture in terms of field Nf magnitude compared to the Bryan mixture. Based on the

5 × 106 design traffic ESALs and 20 years service life at 95 percent design reliability level for

this pavement structure and the environmental conditions under consideration, all the fatigue

analysis approaches (although with different failure criteria) indicate inadequate and adequate

theoretical fatigue performance for the Bryan and Yoakum mixtures, respectively.

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200

Considering that the Yoakum mixture was designed with a relatively stiffer SBS

modified PG 76-22 binder, this relatively better fatigue performance in terms of field Nf results

was theoretically unexpected. In fact, the theoretical expectation was that the Yoakum mixture’s

fatigue performance in terms of field Nf magnitude would be worse compared to the Bryan

mixture. However, the research team attributed this response behavior to the following factors:

• Compared to the Bryan mixture, the Yoakum mixture had relatively higher binder

content (5.6 percent versus 4.6 percent by weight of aggregate).

• Contrary to theoretical expectations based solely on stiffness alone, the SBS modifier

probably improved the Yoakum mixture’s fatigue resistance as well as reduced its

susceptibility to binder oxidative aging.

• The Yoakum mixture incorporated a 1 percent hydrated lime in the mixture design.

Although lime is often added to improve mixture resistance to moisture damage, this lime

perhaps increased the mixture’s resistance to both fatigue damage and aging. Wisneski et

al. made similar observations that lime tended to improve the performance of recycled

asphalt (114).

• SE results in Chapter 10 indicated a better fracture resistance and stronger potential to

heal for the Yoakum mixture than for the Bryan mixture. Based on these SE results, it can

be theorized that the PG 76-22 binder-gravel aggregate has an increased bond strength

compared to that of the PG 64-22 binder-limestone aggregate combination. Note that one

of the SE measurements’ objectives is often to asses the affinity and bond (cohesive

and/or adhesive) strength of binders and aggregates. Theoretically, a comparatively

better bond strength compatibility between the binder and aggregate (in this case for the

Yoakum mixture) is generally expected to exhibit superior performance.

• Tensile strength and RM results in Chapter 10 indicated that the Yoakum mixture was

more ductile and less susceptible to stiffness age-hardening compared to the Bryan

mixture, properties which probably contributed to its higher field Nf values. Additionally,

the Yoakum mixture exhibited better potential to relax the stress, as indicated by higher

m values, compared to the Bryan mixture.

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201

Although theoretically possible, the research team considers that it may be inappropriate

and/or rather complex to make a direct comparison between these two mixtures because their

mix-design characteristics (binder content, aggregate type and gradation) and materials (the

aggregates) were different. Therefore, because of the many existing variable parameters, the

comparison of these two HMAC mixtures may be inconclusive.

Overall, these results, however, suggests that binder stiffness or initial mixture stiffness

alone may not be used as the sole determinant or measure of HMAC mixture fatigue resistance

or field fatigue performance. A mixture designed with a stiffer binder may not necessarily imply

that it will perform poorly in fatigue compared to a mixture designed with a softer binder. The

entire mix-design matrix and spectrum of material properties need to be evaluated, particularly in

performance comparison studies of this nature. Equally to be considered is the pavement

structure, the environmental conditions, and the mixture sensitivity to aging in terms of binder

oxidation and stiffness age-hardening rate and probably even the binder’s potential to heal.

MIXTURE VARIABILITY

As observed in Chapter 10, there was generally a high variability in the Yoakum mixture

results, both in terms of mixture properties and field Nf results (COV of Ln Nf). Compared to the

Bryan mixture, the Yoakum mixture consists of a stiffer SBS modified PG 76-22 binder that is

relatively harder to work with when mixing, compacting, and sawing/coring. Table 11-1 shows

an example of the mixture AV variability.

Table 11-1. Example of HMAC Specimen AV Variability.

Specimen Mixture Target AV Average AV Stdev COV

Bryan 7±0.5% 7.23% 0.20 2.81%Cylindrical

Yoakum 7±0.5% 7.10% 0.35 5.94%

Bryan 7±0.5% 7.18% 0.29 4.04%Beam

Yoakum 7±0.5% 6.98% 0.55 7.87%

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202

Table 11-1 represents the average AV content of 10 random sample specimens per

specimen type per mixture type. Although the COV values are reasonably acceptable, Table 11-1

clearly shows the high variability in the AV content for the Yoakum mixture. Modified binders

are generally more difficult to work with, and consequently, it is more difficult to control the AV

content, which was ultimately reflected in the high variability of the final results. For this

Yoakum mixture, the other compounding factor may have been the higher binder content. Not

only was the PG 76-22 binder stiffer and difficult to work with, its content in the mixture was

also higher relative to the PG 64-22 of the Bryan mixture.

From Table 11-1, it is also worthwhile to note the relatively high variability in the AV for

the beam specimens. In this project, it was generally more difficult to control the AV for the

beam specimens during compaction due to the nature of their shape and the kneading compaction

method. This high variability in the AV content was also reflected in the final ME lab Nf results

discussed in Chapter 10 and the field Nf results shown in Table 11-2. The cylindrical specimens,

on the other hand, are compact and easy to handle, and the gyratory compaction method allows

for better control of the AV content.

Mixture field Nf results generally indicated higher variability with the Yoakum mixture

and for the ME approach for all PSs, environmental, and aging conditions. Table 11-2 gives a

summary example of the mixture field Nf statistical analysis in terms of the COV of Ln Nf and the

95 percent CI for PS#1 and WW environment based on a 20-year design period.

Table 11-2. Example of Mixture Field Nf Variability (PS#1, WW Environment).

Field Nf Approach Mixture

Mean Value COV of Ln Nf 95% CI

Bryan 1.03 × 106 6.87% 0.49 – 2.17 × 106

ME Yoakum 8.30 × 106 9.85% 5.41 – 16.74 × 106

Bryan 3.11 × 106 2.81% 3.08 – 3.21 × 106

CMSE Yoakum 8.40 × 106 3.92% 6.95 – 9.82 × 106

Bryan 3.10 × 106 2.93% 2.98 – 4.47 × 106

CM Yoakum 7.77 × 106 3.98% 6.12 – 8.08 × 106

Bryan 4.71 × 106 ------- 1.93 – 9.74 × 106M-E Design Guide Yoakum 6.21 × 106 ------- 2.04 – 15.34 × 106

Design traffic ESALs over 20 year design period at 95 percent reliability level: 5.00 × 106

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203

From Table 11-2, it is evident that variability in terms of COV of Ln Nf and 95 percent CI

is relatively higher for the Yoakum mixture. These COV values seem low because they are

expressed in terms of logarithmic response, which provides a better statistical analysis in terms

of an assumed normal distribution. However, they nonetheless provide a comparative basis for

the approaches. Note that no COV of Ln Nf values are reported for the M-E Pavement Design

Guide in Table 11-2. This is due to the nature of the back-calculation analysis of field Nf at 50

percent cracking using percentage cracking output values from the M-E Pavement Design Guide

software. The Nf backcalculation analysis does not allow for a realistic determination of

representative COVs. Although three specimens were used for each mixture, the output is just

one single field Nf value.

From Table 11-2, it is clearly evident that the ME exhibited the highest statistical

variability, both in terms of the COV values and 95 percent CI range (particularly for the

Yoakum mixture with the modified binder). The CMSE, in contrast, exhibited the least statistical

variability as measured in terms of the COV values of Ln Nf and 95 percent CI range.

EFFECTS OF OTHER INPUT VARIABLES ON MIXTURE FIELD Nf

Among other variables, mixture fatigue performance is dependent on the pavement

structure and environment. The effect of these variables on mixture field Nf and fatigue

performance assuming similar traffic loading conditions are discussed in this section.

Pavement Structure

HMAC mixture field Nf prediction and fatigue performance is a function of the strain

(tensile or shear) as the failure load-response parameter. For any given pavement structure

(assuming similar traffic loading and environmental conditions), the critical maximum design

strain is computed as a function of the number of structural layers, layer thicknesses, and the Ei

and ν values of the respective layers. Figure 11-2 is an example of the effect of pavement

structure on the mixture field Nf under WW environmental conditions based on a 20 year design

period for the Bryan mixture. Structural details of the pavement structures (PS# 1, PS# 4, and

PS# 5) shown in Figure 11-2 are summarized in Table 3-7.

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204

1.0E+05

1.0E+06

1.0E+07

1.0E+08

Field Nf

PS#4 PS#1 PS#5

MECMSE

CMM-E Design Guide

Figure 11-2. Effect of Pavement Structure on Mixture Field Nf

(Bryan Mixture, WW Environment).

In terms of fatigue analysis, the optimum combination of the number of layers, layer

thicknesses, and Ei values that gives the lowest critical maximum design strain will result in

higher field Nf value and better fatigue performance in the field. Because fatigue cracking

initiates due to horizontal tensile and/or shear strains in the HMAC layer that exceed the capacity

of the HMAC, pavement structures with higher values of the critical maximum design strain will

generally be more susceptible to fatigue cracking than those with lower values.

PS# 5 in Figure 11-2 has the least critical maximum design strain (Table 3-7) and

therefore highest field Nf values for all the fatigue analysis approaches. According to Table 3-7,

PS# 1 and 5 are three-layered pavement structures (including the subgrade), while PS# 4 is

four-layered. However, the relatively 4 inch thick HMAC layer in PS# 5 is resting on a stiff

cemented base that provides support for the loading and produces lower strains in the top HMAC

layer, and subsequently higher field Nf values.

Ultimately, these results demonstrate the inseparable nature of pavement structural design

and HMAC mix-design for fatigue resistance. HMAC mixture fatigue resistance cannot be

modeled explicitly without consideration of a representative field pavement structure.

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Environmental Conditions

As discussed in Chapters 2 and 3, environmental conditions have a significant effect on

the pavement material properties in terms of the Ei values. These Ei values, in turn, have an

effect on the design strain that ultimately has an effect on Nf. Figure 11-3 shows the effect of

environmental conditions for PS# 1 based on the M-E Pavement Design Guide analysis that

incorporates a very comprehensive climatic analysis model.

WWDC

Bryan

Yoakum1.0E+06

1.0E+07

Field Nf

Figure 11-3. Effect of Environmental Conditions on Mixture Field Nf (PS#1).

From Figure 11-3, both mixtures exhibited relatively higher field Nf values in the DC

environment. The lower field Nf values in the WW environment are possibly due to the wetting

effect (presence of moisture) that had a significant effect on the Ei values of the unbound

pavement layers, including the subgrade. Note that the presence of moisture within and/or

underneath a PS is to reduce the Ei value that ultimately results in a higher εt value in the HMAC

layer.

Overall, these results indicate that HMAC mixture fatigue resistance is pavement

structure and environmental location dependent. The results signify the importance of adequately

interfacing HMAC mix-design and fatigue characterization with pavement structural design and

analysis to achieve adequate field fatigue performance.

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206

BINDER TEST RESULTS AND EFFECTS OF AGING

Two binders, an unmodified PG 64-22 and a polymer-modified PG 76-22, were used in

this project. Neat binders and binders recovered from laboratory mixtures, at several levels of

aging, were evaluated. Neat binders were aged in a HMAC simulation, the stirred air-flow test,

to give one level of aging. Then these binders were further aged in the 60 °C (140 °F)

environmental room in thin films (approximately 1 mm [0.039 inches] thick) for 3 and 6 months

to obtain a second and third aging level (SAFT+3M and SAFT+6M). For recovered binders,

aging states were obtained by aging two asphalt-aggregate mixtures (designated Bryan and

Yoakum). The mixtures were prepared using the PP2 short-term aging protocol and then

compacted; this method produced one aging level (PP2+0M). The second and third levels were

obtained by aging the compacted laboratory mixture in the environmental room for 3 and 6

months beyond PP2 conditioning (PP2+3M and PP2+6M). Note that the “0 months,” “3

months,” and “6 months” refer to environmental room aging beyond PP2 aging so that 0 months

aging still has a significant level of aging beyond SAFT aging.

The binders in the compacted mixtures were extracted and recovered according to the

procedure outlined in Chapter 8. SEC was used to check whether the solvent residues exist in

the binder. SEC chromatograms for recovered binders from Bryan mixtures are shown in Figure

11-4 and show that the recovered binders did not have solvent residue, which, if present, would

significantly affect the rheological properties. They also show that the asphaltene peak, centered

at about 23 minutes of retention time, increased with aging, a common result.

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207

-0.20

-0.10

0.0

0.10

0.20

0.30

0.40

0.50

0.60

15 20 25 30 35 40 45

PP2-3MPP2-0M

RI R

ESPO

NSE

RETENTION TIME (minutes)

* 3M- Bryan mix, 3 month aged in 60 oC room*0M- Bryan mix just after it was made

Recovered Bryan

Figure 11-4. SEC Chromatogram for Recovered Binders from Bryan Mixtures

(°F = 32 + 1.8 (°C)).

The aged binders were characterized by DSR and FTIR measurements. Aging increases

carbonyl area (oxygen content), viscosity, and the elastic modulus, but decreases the ductility.

Figures 11-5 and 11-6 are a plot of the CA and zero shear viscosity, respectively, for the Bryan

binder (PG 64-22).

Figure 11-5 shows that CA increases with aging time for neat and recovered binders from

Bryan mixtures. SAFT aging leaves the binder within the initial jump (higher aging rate) region,

whereas PP2 aging is more severe and produces a binder that is past this region. Thus, the three

PP2 data points show a uniform aging rate where as the SAFT points show a higher rate (slope)

between 0 and 3 months than between 3 and 6 months.

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Figure 11-5. CA Rate of Bryan Binder (PG 64-22)

(F = 32 + 1.8(C)).

Figure 11-6. Zero Shear Viscosity Hardening Rate of Bryan Binder (PG 64-22) (F = 32 + 1.8(C)).

0 1 2 3 4 5 6 7 8 90.0

0.5

1.0

1.5

2.0

PP2 + 0, 3, 6M SAFT+ 0, 3, 6M

CA

Aging Time ( months at 60 oC, 1 atm)

Binder for Bryan Mixture

0 1 2 3 4 5 6 7 8 9104

105

106

PP2 + 0, 3, 6M SAFT+ 0, 3, 6M

η* 0(P

oise

, 60

o C, 0

.1 ra

d/s)

Aging Time ( months at 60 oC, 1 atm)

Binder for Bryan Mixture

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209

The zero shear viscosity of the Bryan binder also increases with aging time, and PP2 aged

binder seems to have passed the initial jump period in Figure 11-6, as the data for all three aging

times show the same hardening rate. The DSR function (G’/(η’/G’)) for the Bryan binder, shown

in Figure 11-7, versus the CA, also increases with aging. The DSR function is plotted on a

logarithmic scale against the CA, which represents the amount of aging. Thus, aging time is

removed as a factor, and PP2-aged binder and SAFT-aged binder show the some relation

between CA and DSR function.

Figure 11-7. DSR Function vs. Carbonyl Area of Bryan Binder (PG 64-22)

(°F = 32 + 1.8(°C)).

The Yoakum binder is a polymer modified binder, PG76-22, for which the zero shear

viscosity is not appropriate for characterizing hardening rate (polymer-modified binders typically

do not exhibit a zero shear viscosity). Instead, the DSR function (at a defined temperature and

frequency) hardening rate is used to represent changes of binder physical properties with aging in

Figure 11-8.

0.0 0.5 1.0 1.5 2.010-5

10-4

10-3

10-2

PP2 SAFT before IJ SAFT after IJ

(G'/(

η'/G

')) M

Pa/s

15

o C, 0

.005

rad/

s

CA

Binder for Bryan Mixture Design

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210

The DSR function of the Yoakum binder increases with aging time, and the PP2 aging

process (PP2 + 0M) aged the Yoakum binder more than the SAFT process (SAFT + 0M).

However, after 3 and 6 months additional aging in the 60 oC (140 °F) room, the neat thin-film

aged Yoakum binder was somewhat harder than the mixture aged binder.

The thin film binder catches up with the mixture binder partly because, after SAFT, it is

still in the higher aging-rate initial jump period, but also because binder aging in thin film has

more access to oxygen than binder in compacted mixtures. In the case of the Bryan binder

(Figures 11-5 and 11-6), it appears that the same process is occurring, but the neat binder takes

longer to catch up to the mixture-aged binder. Increase of the CA for the Yoakum binder is

shown in Figure 11-9.

Figure 11-8. DSR Function Hardening Rate of Yoakum Binder (PG 76-22)

(°F = 32 + 1.8(°C)).

0 1 2 3 4 5 6 7 8 910-5

10-4

10-3

10-2

PP2 + 0, 3, 6M SAFT + 0, 3, 6M

(G'/(

η'/G

'))

MPa

/s 1

5 o C

, 0.0

05 ra

d/s

Aging Time ( months at 60 oC, 1 atm)

Binder for Yoakum Mixture

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211

0 1 2 3 4 5 6 7 8 90.5

1.0

1.5

2.0

PP2 + 0, 3, 6M SAFT + 0, 3, 6M

CA

Aging Time ( months at 60 oC, 1 atm)

Binder for Yoakum Mixture

Figure 11-9. CA Rate of Yoakum Binder (PG 76-22)

(°F = 32 + 1.8(°C)).

Figure 11-10 shows the increase in DSR function with CA for the Yoakum binder. Again,

both neat binder and mixture aged binder show the relation, suggesting the same aging

mechanism is followed in both cases.

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212

0.0 0.5 1.0 1.5 2.010-5

10-4

10-3

10-2

PP2 + 0, 3, 6M SAFT + 0, 3, 6M

(G'/(

η'/G

')) M

Pa/s

15

o C, 0

.005

rad/

s

CA

Binder for Yoakum Mixture

. Figure 11-10. DSR Function vs. CA for Yoakum Binder (PG 76-22)

(°F = 32 + 1.8(°C)).

BINDER-MIXTURE CHARACTERIZATION AND AN AGING SHIFT FACTOR

In Chapter 10, the effect of binder oxidative aging on mixture fatigue life was presented.

The decrease in fatigue life with aging is striking, and significant differences in the rate of

decline were noted between the Bryan and Yoakum mixtures. The reasons for these differences

are, as yet, unknown. The discussion in this section elaborates on the possible impact of this

decline in fatigue life on a pavement’s service life. The question addressed is, “What shift factor

should be applied to a pavement’s service life due to binder oxidative aging?”

Another approach, different from the SFag approach discussed in Chapter 10, is presented

in this section. The approach, discussed below, utilizes binder DSR functions and attempts to

incorporate the significant aspect of traffic loading, and is based on field Nf.

First the following definitions are made:

Nf = Field fatigue life, in ESALs, and

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213

Fraction of Life Expended During Time ( ) /f

dtdtN t RL

=

end

01( ) /

t

f

dtN t RL

=∫

1 20( ) K K t

f fN t N e−=

1 2 0end

1 2

ln( / 1)f LK K N Rt

K K+

=

1 2 0

1 2 0

ln( / 1)Age-shortened LifeUnaged Life Expectancy /

f Laging

f L

K K N RSF

K K N R+

= =

RL = Pavement loading rate, ESALs/yr.

Then Nf / RL = Pavement Fatigue Life Expectancy, in years, is a constant over the life of

the pavement value of field Nf . If, however, field Nf is a function of time (and declines with

binder oxidative aging, e.g.), then this decline must be taken into account when estimating the

pavement fatigue life. For a differential time period dt during which the field fatigue life is Nf(t),

the fraction of a pavement’s total available fatigue life consumed during dt is calculated as:

(Equation 11-1)

Then, Miner hypothesis (18, 115) is used to sum over the pavement’s entire life, defined to be

the amount of time to reach an integrated fraction equal to unity as follows:

(Equation 11-2)

From the experimental data for the decline of field Nf with binder oxidative aging, Nf(t)

can be represented by an exponential relation:

(Equation 11-3)

where K1 is the magnitude of the power law slope that relates the decline of Nf to the increase in

the DSR function G’/(η’/G’) with aging, and K2 is the (exponential) rate of increase of the DSR

function with aging time in the pavement. Solving this integral for tend gives the following

equation:

(Equation 11-4)

An aging shift factor can be defined as the ratio of the age-shortened fatigue life to the

unaged fatigue life expectancy:

(Equation 11-5)

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214

From this relation, the bigger K1 and K2 are in magnitude; the smaller the aging shift

factor, the shorter the pavement’s fatigue life expectancy. Equation 11-5 also shows that K1 and

K2 have an identical effect on this shift factor. That is, the impact of aging on the DSR function

and the response of the fatigue life to these changes in DSR function produce the same effect on

the final aging shift factor.

The decline of mixture fatigue with increasing DSR function is shown for both the Bryan

and Yoakum mixtures in Figure 11-11. Values of Nf0 (here equal to the fatigue life of the PP2-

aged compacted mixtures) were reported in Chapter 10, and K2, the ln (DSR function) hardening

rate, is taken from a lab-to-field hardening rate conversion obtained in Project 0-1872

(Table 9-8) (52) and applied to the DSR function hardening rate (Figure 11-12). Hardening

rates, of course, vary from pavement to pavement and depend principally upon the climate, but

also, and perhaps to a lesser degree, on air voids and binder content. Consequently, the value

used here gives only a very approximate indication for any specific pavement.

10-4 10-3 10-2106

107

108

109

For Bryan Field Nf: y = a*x̂ b R^2 = 0.994a 664b -1.37

For Yoakum Field Nf: y = a*x̂ b R^2 = 0.998a 71100b -0.908

YKM-Nf(CMSE) (Field) BRY-Nf(CMSE) (Field)

Mix

ture

Fie

ld N

f

Binder ( G'/( η'/G') ) MPa/s, 15 oC, 0.005 rad/s

IncreasingAging

Field Nf vs Binder DSR Function

Figure 11-11. Decline of Mixture Nf with Binder DSR Function Hardening

(°F = 32 + 1.8(°C)).

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215

Figure 11-12. DSR Function Hardening Rate of Neat Binder after Initial Jump

(°F = 32 + 1.8(°C)).

Table 11-3 summarizes the parameters and calculations for the two mixtures. A loading

rate of 3 million ESALS/yr was arbitrarily selected for these calculations. This number is high,

perhaps corresponding to a heavily traveled freeway in a major city. A lower number will give

longer fatigue lives. These calculations are intended only to represent a calculation procedure

that shows the differences in fatigue life that might be expected between different mixtures,

based upon laboratory measurements that take into account binder oxidative aging. More

laboratory and field data are needed to verify this approach.

Table 11-3. Summary of Pavement Fatigue Life Parameters.

Mixture Nf0 1 ×106 ESALs

RL 1 ×106 ESALs/Yr

K1 K2 SFaging Pavement

Fatigue Life (Yrs after PP2)

Bryan 69 3 1.37 0.26 0.27 6.2Yoakum 120 3 0.91 0.16 0.33 13.2

10-4

10-3

10-2

0 1 2 3 4 5 6 7

BRY-SAFT+3, 6M

YKM-SAFT+3, 6M

y = 0.00011697 * e^(0.32638x)

y = 0.00048389 * e^(0.20036x)

Aging Time (months at 60 oC, 1 atm)

(G'/(

η'/G

')) M

Pa/s

, 15

o C, 0

.005

rad/

s

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216

The calculated shift factors are markedly different, and the differences in the estimated

pavement fatigue life (after PP2 short-term aging) results for the two mixtures are striking. It

should be noted again that the PP2 short-term aging produces a binder in the mixture that is

significantly more aged than the SAFT (RTFOT equivalent) aged binder. How PP2 aging

compares to the aging of an in-service HMAC pavement is yet unknown. However, based upon

SH 21 data, reported in Project 0-1872 (52), the PP2 aging may reflect as much as 4 years of

HMAC pavement in-service life. If so, the 6 years after PP2 (Bryan mixture) amounts to 10

years HMAC pavement total service life, and the 13 years after PP2 for the Yoakum mixture

would correspond to 17 years of HMAC pavement total service life.

The differences in aging shift factors and pavement fatigue lives for the two mixtures are

the results of K1 , the rate at which the fatigue life declines with oxidative hardening of the

binder and K2, the binder’s hardening rate in the pavement. This is seen dramatically in Figures

11-13 through 11-15.

Figure 11-13. Calculated Decline of Remaining Pavement Fatigue Service Life.

0 5 10 15 20 25 30 35 400.0

0.1

0.2

0.3

0.4

0.5

0.6

0.7

0.8

0.9

1.0

Shift Factor=0.33

Rem

aini

ng F

ract

ion

of S

ervi

ce L

ife

Service Time after PP2(4-hr)-Level Aging (year)

Bryan Mixture- With Aging Bryan Mixture- Without Aging Yoakum Mixture- With Aging Yoakum Mixture- Without Aging

The Effect of Oxidative Aging on Estimated Pavement Fatigue Life

Bryan: Nfo = 69x106 ESALs K1 =1.37; K2 = 0.26; RL = 3x106 ESALs/yrYoakum: Nfo = 120 x106 ESALS K1 = 0.91; K2 = 0.16; RL = 3x106 ESALs/yr

Shift Factor=0.27

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217

Figure 11-13 shows the decline of the remaining fatigue life with service time (after PP2

aging), determined by integrating Equation 11-2 for times shorter than tend. Both the Bryan and

Yoakum mixtures are shown, and the straight-line decline assumes that there is no decline in

fatigue life with aging. Without aging, the Yoakum mixture has a longer service life than the

Bryan mixture due to its initially higher fatigue life (120 versus 69 million ESALs). With binder

oxidative aging, the difference remains, and one might reasonably assume this difference is also

because of the different initial fatigue lives.

Figure 11-14 shows a hypothetical calculation with the Bryan mixture the same, but the

hypothetical case for the Yoakum mixture is the same except that the initial fatigue life is nearly

the same as the Bryan mixture (not identical so both straight-line depreciations can be

identified). While the initial fatigue lives are the same, the shift factors, and thus the service

lives, are significantly different.

Figure 11-14. Hypothetical Decline of Pavement Fatigue Service Life,

Initial Fatigue Lives Equal.

0 5 10 15 20 25 30 35 400.0

0.1

0.2

0.3

0.4

0.5

0.6

0.7

0.8

0.9

1.0

Bryan: Nfo = 69x106 ESALs K1 =1.37; K2 = 0.26; RL = 3x106 ESALs/yrYoakum: Nfo = 71 x106 ESALS K1 = 0.91; K2 = 0.16/yr; RL = 3x106 ESALs/yr

Shift Factor=0.43

Rem

aini

ng F

ract

ion

of S

ervi

ce L

ife

Service Time after PP2(4-hr)-Level Aging (year)

Bryan Mixture- With Aging Bryan Mixture- Without Aging Yoakum Mixture- With Aging Yoakum Mixture- Without Aging

The Effect of Oxidative Aging on Estimated Pavement Fatigue Life

Shift Factor=0.27

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218

A second hypothetical case (Figure 11-15) changes the values of K1 and K2 but leaves the

initial fatigue life the same as for the Yoakum mixture. Now, the conclusion is that the initial

difference in fatigue life has minimal impact on the service life, but the rate of decline of fatigue

life with binder hardening has a very profound impact. This conclusion is tentative as the

amount of data is sparse with only two mixtures. Nevertheless, the results are compelling that

the effect of binder oxidative aging in mixtures can have an extremely significant impact on the

pavement service life in terms of fatigue performance.

Additional comments about pavement aging are appropriate. The above data suggest that

when binder aging occurs in the pavement, it can have a very significant impact on pavement

service life in terms of fatigue performance. However, it does not address whether or not binders

in pavements actually age. At least one report in the literature is used to support the idea that

pavements age primarily near the surface and very little more than an inch below the surface

(116). If this is the case, then the issue of the effect of binder oxidative aging on fatigue may be

of little importance.

On the other hand, a recent TxDOT report (52) provides considerable pavement

recovered binder data that support the notion that binders, in fact, do age in HMAC pavements at

depths up to several inches (at least six) and at rates that appear to be minimally abated by depth.

If this is the case, then the impact of binder oxidative aging on HMAC pavement fatigue

performance is of considerable importance and should be considered when designing HMAC

pavements.

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219

0 5 10 15 20 25 30 35 400.0

0.1

0.2

0.3

0.4

0.5

0.6

0.7

0.8

0.9

1.0

Bryan: Nfo = 69x106 ESALs K1 =1.37; K2 = 0.26; RL = 3x106 ESALs/yrYoakum: Nfo = 120 x106 ESALS K1 = 1.37; K2 = 0.26; RL = 3x106 ESALs/yr

Shift Factor=0.19

Rem

aini

ng F

ract

ion

of S

ervi

ce L

ife

Service Time after PP2(4-hr)-Level Aging

Bryan Mixture- With Aging Bryan Mixture- Without Aging Yoakum Mixture- With Aging Yoakum Mixture- Without Aging

The Effect of Oxidative Aging on Estimated Pavement Fatigue Life

Shift Factor=0.27

Figure 11-15. Hypothetical Decline of Pavement Fatigue Service Life, Ki Values Equal.

SUMMARY

Key points from a discussion and synthesis of the results are summarized as follows:

• The Yoakum mixture exhibited higher field Nf values compared to the Bryan mixture. This

was probably due to the higher SBS modified binder content and the lime in the mixture. By

contrast, the Yoakum field Nf results exhibited higher variability in terms of the COV of Ln

Nf and the 95 percent CI.

• While the Yoakum mixture exhibited better fatigue performance in terms of the field Nf

magnitude in all the analysis approaches, the mixture field Nf also depends on the following

input variables; pavement structure and environmental conditions.

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220

• While certain HMAC mixtures may perform satisfactorily well in a particular pavement

structure and environmental location, it may not be true when these variables (pavement

structure and environmental location) are changed.

• For the test protocols and conditions considered in this project, binder test results, when

analyzed as a function of oxidative aging, indicated that:

­ Aging increases the carbonyl area (oxygen content), DSR function, viscosity, and

elastic modulus.

­ Aging decreases both binder and mixture ductility.

­ CA correlates linearly with the DSR function.

­ AASHTO PP2 4 hrs short-term oven aging has a greater oxidative aging impact on

the binder than SAFT aging. This was evident through the absence of the initial jump

periods in the CA rates of extracted binders from mixtures subjected to AASHTO

PP2 4 hrs short-term oven aging as well as the higher level of aging after the PP2

procedure compared to SAFT aging.

• An approach for developing shift factors due to aging, denoted as SFaging (to differentiate

it from the SFag approach), was developed that includes both binder hardening due to

oxidative aging and decline in fatigue life due to binder hardening. This approach

produced an expected pavement fatigue life in years, based upon an assumed ESALs/yr

loading rate. The impact on fatigue life of binder hardening due to oxidation was

dramatic, and the SFaging results indicated that the Bryan mixture was more susceptible to

decline in fatigue life due to aging than was the Yoakum mixture.

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CHAPTER 12 COMPARISON AND SELECTION OF THE

FATIGUE ANALYSIS APPROACH

This chapter presents the comparative evaluation of the fatigue analysis approaches,

including the selection criteria and the selected and recommended fatigue analysis approach.

COMPARATIVE REVIEW OF THE FATIGUE ANALYSIS APPROACHES

Table 12-1 is a summary comparison of the four fatigue analysis approaches in terms of

laboratory testing, equipment, input data, data analysis, failure criteria, and variability of the

results. Tables 12-1(c) and (d) represent field Nf predictions based on a 20-year design period

with aging effects considered. Only Bryan results are given for the corresponding actual field

section PS#5. Statistical analysis for these approaches was based on least squares regression and

typical spreadsheet descriptive statistics tools discussed in Chapters 4 through 7.

Table 12-1(a). Summary Comparison of the Fatigue Analysis Approaches.

Fatigue Analysis Approach Item

Design Guide ME CMSE/CM

Concept Mechanistic-empirically based

Mechanistic-empirically based

Continuum micromechanics & fundamental HMAC properties

Laboratory testing

Easy but lengthy temperature conditioning time

Rigorous & lengthy Numerous but easy to run & less costly (no SE for CM approach)

Testing time ≅ 5 hrs ≅ 30 hrs ≅ 70 hrs (≅ 5 hrs for CM approach)

Equipment cost*

≅ $130,000 (minus the software)

≅ $155,000 (≅ $25,560 for BB device)

≅ $210,000 (≅ $80,000 for SE devices)

Input data Comprehensive/flexible Comparatively few Comprehensive (no SE for CM approach)

COV of input data ≅ 5% - 23% ≅ 5% - 28% ≅ 4% - 12%

Failure criteria

50% cracking in wheelpath

50% reduction in flexural stiffness

7.5 mm microcrack growth & propagation through HMAC layer

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222

Table 12-1(b). Summary Comparison of the Fatigue Analysis Approaches.

Fatigue Analysis Approach Item

Design Guide ME CMSE/CM

Analysis procedure Comprehensive Relatively easy &

straightforward Comprehensive & lengthy

Analysis time** ≅ 4.5 hrs ≅ 3 hrs ≅ 6 hrs (≅ 5 hrs for

CM) Mechanistic failure load-response parameter

Maximum critical design tensile strain (εt) @ bottom of HMAC layer

Maximum critical design tensile strain (εt) @ bottom of HMAC layer

Maximum critical design shear strain (γ) @ edge of loaded tire

Fatigue model ( ) ( ) 3322

11kk

tffff EkN ββεβ −−= ( )[ ]2

1k

tf kSFN −= ε ( )

( ) 21

kp

pif

kN

NNSFN−=

+=

γ

Aging effects

Software incorporates a Global Aging model

None (but can possibly use Miner’s hypothesis)

Shift factor (SFag) being developed

Mean field Nf value*** 5.46 × 106 4.67 × 106 5.60 × 106

COV of Ln Nf (field)***

------------ ≅ 6.87 - 9.85% ≅ 2.81 – 3.98%

95% field Nf CI *** ≅ 1.93 – 15.34 × 106 ≅ 0.49 – 16.74 × 106 ≅ 2.98 – 8.92 × 106

Note: *Equipment costs were based on July 2004 estimates; **Analysis time estimates based solely on the researchers’ experience with each approach

***Field Nf, COV and 95% CI values based on PS# 1 and WW environment only

An example of the analysis used to obtain the field Nf results shown in Tables 12-1 (c)

and (d) for the ME, CMSE, and CM approaches in PS# 1 and the WW environment is given in

Appendix I. For the M-E Pavement Design Guide, the Nf analysis is software-based. Based on

Tables 12-1 (c) and (d), the field Nf varies across pavement structures, particularly for the ME

and M-E Pavement Design Guide approaches. This variation is attributed to the predominant

sensitivity of these approaches, particularly the ME analysis models, to the critical design tensile

strain, εt,, at the bottom of the HMAC layer, a parameter which is itself largely dependent on the

entire pavement structure. For the ME approach, it should also be noted that the field Nf

predictions strongly depend on the selected shift factor (SF) (Chapter 4).

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Table 12-1(c). Summary Comparison of the Fatigue Analysis Approaches.

Field Nf (WW Environment) PS Mixture ME CMSE CM Design Guide

Bryan 1.03 × 106 3.11 × 106 3.10 × 106 4.71 × 106 1 Yoakum 8.30 × 106 8.40 × 106 7.77 × 106 6.21 × 106 Bryan 0.26 × 106 2.13 × 106 2.38 × 106 4.05 × 106 2 Yoakum 0.97 × 106 6.56 × 106 5.55 × 106 5.75 × 106 Bryan 0.25 × 106 2.18 × 106 2.06 × 106 1.93 × 106 3 Yoakum 0.98 × 106 6.57 × 106 6.23 × 106 3.41 × 106 Bryan 0.28 × 106 1.96 × 106 1.96 × 106 2.02 × 106 4 Yoakum 0.99 × 106 4.45 × 106 4.59 × 106 2.97 × 106 Bryan 2.16 × 106 5.49 × 106 5.38 × 106 19.29 × 106 5 Yoakum ----------- ----------- ------------- -------------

Table 12-1(d). Summary Comparison of the Fatigue Analysis Approaches.

Field Nf (DC Environment) PS Mixture ME CMSE CM Design Guide

Bryan 1.18 × 106 3.60 × 106 3.59 × 106 5.19 × 106 1 Yoakum 9.59 × 106 9.07 × 106 8.46 × 106 8.02 × 106 Bryan 0.34 × 106 2.46 × 106 2.74 × 106 5.23 × 106 2 Yoakum 1.27 × 106 6.78 × 106 5.80 × 106 7.43 × 106 Bryan 0.33 × 106 2.52 × 106 2.39 × 106 4.29 × 106 3 Yoakum 1.27 × 106 6.79 × 106 6.51 × 106 5.57 × 106 Bryan 0.35 × 106 2.26 × 106 2.27 × 106 3.56 × 106 4 Yoakum 1.27 × 106 4.61 × 106 4.79 × 106 5.24 × 106 Bryan 2.18 × 106 6.34 × 106 6.21 × 106 22.00 × 106 5 Yoakum ----------- ----------- ------------- -------------

Theoretical Concepts

Unlike the mechanistic-empirically based M-E Pavement Design Guide and ME

approaches, the CMSE and CM approaches were formulated on the fundamental concepts of

continuum micromechanics and energy theory, with fracture and healing as the two primary

mechanisms controlling HMAC mixture fatigue damage. The CMSE/CM approaches utilize the

fundamental HMAC mixture properties to estimate lab and/or field Nf.

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Input Data

The input data for the CMSE and CM approaches and associated laboratory tests are

comprehensive, which is necessary to sufficiently and adequately predict field Nf by considering

all relevant factors that affect HMAC fatigue performance. The CMSE and CM approaches

incorporate various material properties such as modulus, tensile strength, fracture, healing, and

anisotropy, which is not the case with the ME approach.

The input data for the M-E Pavement Design Guide is also comprehensive but can be

flexible depending on the level of analysis selected. Level 1 requires comprehensive input data in

terms of traffic, environment, and material properties, with HMAC mixture properties

characterized in terms of the |E*| values.

Laboratory Testing

The BB test for the ME approach is comparatively complex and time consuming. Note

also that the laboratory BB equipment is limited to only third-point loading HMAC beam fatigue

testing in a flexural mode. The linear kneading compactor may also be limited to rectangular

beam shaped specimens, while most of the current Superpave HMAC mixture characterization

tests use gyratory compacted cylindrical specimens.

The CMSE laboratory tests may be numerous, but they are relatively simple to run and

less time consuming (provided specimens are well aligned along the axis of loading during

testing). With the exception of SE measurements, the average test time for CMSE testing was at

most 5 hrs. Additionally, CMSE cylindrical specimens are relatively easy to fabricate and

handle. In the case of the CM approach, SE measurements (both for binder and aggregate) and

RM tests in compression are not required, thus making the CM approach even more

advantageous in terms of laboratory testing and subsequent data analysis.

However, with the CMSE uniaxial testing of the HMAC mixtures, it is imperative that

the cylindrical specimens are properly aligned along the axis of loading (tensile or compressive)

to prevent the induction of undesirable moments that can lead to erroneous results.

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DM testing for Level 1 fatigue analysis of the M-E Pavement Design Guide is relative

easy and simple to run but very time consuming in terms of temperature conditioning time for

the specimens. Since a complete DM test for a single cylindrical specimen is often conducted at

five temperatures, the minimum total conditioning time in this project was 10 hrs, i.e., a

minimum of 2 hrs for each test temperature.

BB testing with the ME approach utilizes kneading compacted beam shaped specimens

that are comparatively difficult to fabricate, time consuming to make, and require delicate

handling and storage. Improper handling and/or storage can easily induce residual stresses within

the specimen that can have a negative impact on the results.

Also, the beam shape of the specimens and the linear compaction procedure makes it

difficult to adequately control the AV content to the target level. For instance, the COV of the

AV content for the beam specimens in this project ranged between 4 to 8 percent. While this

COV range may be acceptable, it was nonetheless higher than the approximately 3 to 6 percent

COV for the cylindrical specimens utilized in the M-E Pavement Design Guide and CMSE/CM

approaches. All these factors ultimately contribute to the relatively high variability in both the

input data and final field Nf results for the ME approach.

Failure Criteria

The M-E Pavement Design Guide failure criterion is based on a percentage cracking in

the wheelpath. In this project, the research team used 50 percent as the threshold value consistent

with the TxDOT tolerable limits (61). However, the research team feels that this percent

cracking does not correlate well with the actual fatigue damage accumulation (i.e., crack growth

through the HMAC layer) or crack severity in an in situ HMAC pavement structure. For

instance, a severely cracked HMAC pavement structure with only 10 percent crack area coverage

may be considered adequate according to this criterion. Whereas a 60 percent cracked pavement

section with cracks only initiating (beginning) will be considered inadequate according to this

criterion. Therefore, there may be a need to review this failure criterion.

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In the case of the ME approach, the correlation between fatigue crack area and severity

on an in situ pavement structure and/or crack length through the HMAC layer thickness and 50

percent flexural stiffness reduction is not clear. As pointed out by Ghuzlan et al. (116), 50

percent initial stiffness reduction for constant strain BB testing is an arbitrary failure criterion

that does not correlate well to the actual damage accumulation in the HMAC material. These

researchers instead proposed the use of energy concepts. Rowe et al.’s study also suggests that

while this 50 percent stiffness reduction may work well for unmodified binders, it may not be

applicable for modified binders, and thus, results must be analyzed and interpreted cautiously

(113). Note that the Yoakum mixture with the modified binder generally exhibited higher Ln Nf

(both lab and field) variability in this project.

In addition, the ME assumption of bottom-up crack failure mode due to horizontal εt as

utilized in this project may not always be true particularly for thick, stiff or thin, flexible HMAC

pavement structures. This also applies to the M-E Pavement Design Guide approach. For the

CMSE approach, the failure criterion needs to be further reviewed to establish the adequacy of

assuming one microcrack (7.5 mm) initiating and propagating through the HMAC layer

thickness as representative of the fatigue cracking process in the entire HMAC pavement

structure. The current CMSE version is based on the generalized hypothesis that the growth of

one crack is representative of the field HAMC pavement crack size distribution. Consequently,

more data are thus required to validate this hypothesis.

Both the ME and the M-E Pavement Design Guide utilize tensile strain as the failure

load-response parameter and exhibit considerable sensitivity to this parameter (3, 4, 59). Though

still subject to review, recent research including the preliminary observation of this project has

shown that because of the anisotropic nature of HMAC, this may not always be true, particularly

for thick stiff HMAC pavement structures. Therefore, the use of εt at the bottom of the HMAC

layer may provide an under- or over-estimation of the mixture Nf, particularly for pavement

structures where εt at the bottom of the HMAC layer is not critical to fatigue performance. Based

on this theory, it appears that the ME approach may be applicable only to pavement structures

where εt at the bottom of the HMAC layer is critical to fatigue performance. Otherwise the

approach tended to over predict Nf, particularly for pavement structures with εt less than 100

microstrain in this project. Various researchers, including Nishizwa et al.(34), have also reported

infinite Nf at low strain levels less than 200 microstrain with the ME approach.

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Data Analysis

In terms of analysis, the CMSE and CM approaches are comparatively complex and

lengthy because of the comprehensive input data requirements. Inevitably, this type of analysis is

necessary to adequately model the HMAC mixture fatigue resistance by analyzing and directly

incorporating all the influencing factors. However, these numerical calculations can easily be

simplified if a simple spreadsheet analysis program is developed for the computations, as was the

case in this project. Alternatively, a CMSE/CM fatigue analysis software can be developed to

simplify and reduce the time needed for these calculations.

Nonetheless, a comprehensive sensitivity analysis of the CMSE/CM fatigue analysis

procedure is recommended to simplify the calculations by eliminating/reducing less critical

and/or redundant variables. While the CMSE/CM analysis procedure produced reasonable results

in this project, it should be noted that this is a relatively new fatigue analysis procedure and may

therefore still be subject to review and modifications in continuing research work during the

validation phase.

For the ME approach, the simplified AASHTO TP8-94 analysis procedure utilized in this

project was relatively easy and straightforward, probably because of the relatively fewer input

data required (59). For the M-E Pavement Design Guide, the fatigue analysis process is software

based but utilizes the ME concepts (3, 4).

While the ME laboratory-to-field shift factors (SF) may be environmentally specific and

require calibration to local conditions, the CMSE/CM calibration constants were developed

based on a wider environmental spectrum covering the USA (45), thus making the CMSE

approach more flexible. By contrast, the M-E Pavement Design Guide incorporates a

comprehensive climatic model that computes the shift factors based on a specific environmental

location (3, 4). The M-E Pavement Design Guide Level 1 fatigue analysis actually computes

these calibration constants based on actual climatic (current or past) data from local weather

stations. In this context, the M-E Pavement Design Guide may therefore be considered as being

more accurate and realistic in terms of simulating field environmental conditions compared to

the other fatigue analysis approaches. The M-E Pavement Design Guide software also

encompasses a comprehensive traffic analysis model that more closely simulates field traffic

loading conditions than the ME and CMSE/CM approaches (3, 4).

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Furthermore, the M-E Pavement Design Guide software incorporates a default

empirically-based Global Aging Model that takes into account the effects of aging in HMAC

mixture fatigue analysis (3, 4). By contrast, the ME and the current CMSE/CM approaches do

not directly incorporate the effects of aging in the analysis. In the case of the CMSE approach,

attempts are being made to develop shift factors due to aging (Chapters 10 and 11) in the

ongoing research and will possibly be incorporated in the final CMSE version. For the ME

approach, Miner’s hypothesis (18) can be utilized to develop and incorporate the effects of aging

in field Nf prediction, but this was beyond the scope of this study.

Additionally, the M-E Pavement Design Guide software has an added advantage of

simultaneously predicting other HMAC pavement distresses besides fatigue cracking. These

include thermal cracking, rutting, and pavement roughness expressed in terms of the

international roughness index (IRI). The CMSE approach on the other hand, has the potential to

simultaneously model HMAC moisture sensitivity through the use of surface energy data under

wet conditions (46, 47, 68, 71). In this project, however, dry conditions were assumed with no

consideration of moisture sensitivity analysis for the HMAC mixtures.

Results and Variability

Although the computed mixture field Nf results presented in Chapters 10 and 11 were

comparable, the CMSE and CM approaches exhibited relatively low variability in terms of the

COV of Ln Nf compared to both the ME and the M-E Pavement Design Guide approaches. As

highlighted in Chapter 11 (Table 11-2), the ME approach exhibited the highest statistical

variability both in terms of the COV of Ln Nf and 95 percent field Nf CI. Furthermore, the ME

field Nf predictions are significantly dependent on the selected SF value (Chapter 4), which will

obviously lead to different results if a different SF value is selected. Note that this SF value for

the ME approach was not measured in this project (Chapter 4).

Although this lower statistical variability may also indicate that the CMSE/CM test

repeatability was better than the BB and DM tests, more comprehensive statistical analyses for

the CMSE/CM approaches are required, including more laboratory HMAC mixture fatigue

characterization and field validation.

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Costs – Time Requirements for Laboratory Testing and Data Analysis

The cost comparisons in this project were evaluated in terms of billable time

requirements for laboratory testing (specimen fabrication, machine set up, and actual test running

time) and data analysis. These typical time estimates based on at least four HMAC specimens for

the ME and CMSE/CM approaches and at least two HMAC specimens for the M-E Pavement

Design Guide to obtain at least a single value of field Nf are shown in Table 12-1.

Detailed time requirements are attached as Appendix J. Note that these time estimates

were purely based on the work contained in this project, but actual time requirements for

laboratory testing and data analysis may generally vary from one person to another and from

machine to machine or computer to computer (e.g., in the case of the M-E Pavement Design

Guide).

In Table 12-1, laboratory testing time does not include aggregate pre-heating, binder

liquefying, short-term oven aging, heating for compaction, cooling after compaction, and

temperature conditioning time of the specimens prior to testing, because time for these processes

was considered equal in each approach and may often not be billable. Based on the billable time

requirements in Table 12-1, the M-E Pavement Design Guide was ranked as the cheapest

(shortest billable time requirement) followed by the CM approach.

Generally, the ME approach required more time for specimen fabrication, machine setup,

and actual testing but less time for data analysis primarily due to the simplified AASHTO

TP8-94 analysis procedure selected and the fewer input data requirements (59).

For the CMSE approach, SE values for binders and aggregates are required as input data.

Though the current test protocol for aggregates might require a test time of about 30 to 60 hrs per

aggregate, various alternate and time-efficient SE measurement methods are being investigated

in an ongoing research project (77). Despite the lengthy test time, however, SE measurements

are only performed once for any binder or aggregate type from a particular source (as long as

there are no major compositional changes). The SE data can then be utilized for numerous

analysis applications including fatigue, permanent deformation, and moisture sensitivity

modeling in HMAC pavements. Thus, SE measurements are actually efficient considering their

repeated and widespread use for binder and aggregate materials that may be utilized in different

mixture designs for different projects.

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Costs – Equipment

In terms of equipment cost, the CMSE was ranked as the most expensive approach with

an approximate total cost of $210,000 (with about $80,000 being for the SE equipment) followed

by the ME approach, based on current equipment costs. Although the SE equipment appears

costly, its versatility in terms of data measurements for HMAC mixture fatigue, permanent

deformation, and moisture sensitivity analysis may actually offset the high initial cost. This is

especially significant for numerous concurrent projects.

The equipment costs for the M-E Pavement Design Guide (≅ $130,000) and the CM (≅

$210,000 - $80,000 = $130,000) approaches are similar. However, the cost of the M-E Pavement

Design Guide software, which is not included in Table 12-1, may raise the M-E Pavement

Design Guide total cost to a value higher than that of the CM approach.

The ME equipment cost is lower than that of the CMSE, but it exceeds the M-E

Pavement Design Guide and the CM approaches by approximately $25,560 based on the current

price of the BB device (Table 12-1) (118). The limited use of the BB device for flexural fatigue

testing only also indirectly makes the ME approach more costly.

SELECTION OF FATIGUE ANALYSIS APPROACH

Table 12-2 summarizes the advantages and disadvantages of each fatigue analysis

approach as observed in this project. Table 12-3 is a summary rating based on a comprehensive

value engineering assessment including laboratory test results, statistical analysis, and relative

comparison of each analysis procedure. The assessment and rating criteria, including a TxDOT

evaluation survey questionnaire to rate the assessment factors according to their degree of

significance, are discussed in this section. A detailed rating analysis is attached as Appendix K.

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Table 12-2. Summary Comparison of the Fatigue Analysis Approaches.

Approach Advantage Disadvantage

CMSE • Utilizes fundamental HMAC mixture properties to estimate Nf • Exhibits greater flexibility & potential to incorporate material properties that are

critical to HMAC mixture fatigue performance • Utilizes shear strain as failure load-response parameter • Utilizes cylindrical specimens that are easy to fabricate & handle • Requires numerous tests that are easy & relatively less costly to run • Relates fatigue failure to damage accumulation within HMAC material • Procedures Nf results that exhibits lower statistical variability • Produces fatigue performance results as a function of microcrack growth through

HMAC layer thickness • Utilizes calibration constants that were developed nationwide • Incorporates aging, healing, & anisotropic effects in Nf analysis • Laboratory tests and resultant data are versatile in their application

• Validity & applicability • More mixture characterization • Test protocols & analysis procedure subject to

review • Lab testing – specimen alignment • Adequacy of failure criteria • Statistical analysis criteria needs more review • SE testing is lengthy & costly

CM • Same as CMSE but with no SE tests & reduced analysis

M-E Pavement Design Guide

• Ideal for pavement structures where tensile strain is critical to fatigue performance

• Incorporates global aging model • Predicts distress as a function of pavement age • Incorporates comprehensive traffic and climatic analysis models • Utilizes cylindrical specimens that are easy to fabricate & handle • Tests are easy and less costly • Failure criteria is based 50 % cracking in wheelpath • Versatility – other tests & analyses

• Empirically based • Global aging model may not be good for

modified binders • No direct incorporation of healing nor

anisotropy • Failure criteria does not clearly relate to

damage & severity • Only bottom-up cracking failure mode was

considered in this study. ME • Ideal for pavement structures where tensile strain is critical to fatigue

performance • Requires local calibration to field conditions • Failure criteria is based on 50% stiffness reduction

• Empirically based • Beam specimen are difficult to fabricate and

handle • Laboratory testing is lengthy • No direct incorporation of aging, anisotropy, &

healing effects in analysis • High variability in results • Not applicable to pavement structures where

tensile strain critical to fatigue performance • Test equipment is limited to BB testing only.

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TxDOT Evaluation Survey Questionnaire

An evaluation survey questionnaire was conducted with TxDOT personnel to ascertain

the degree of significance of the various factors to be used in evaluating and rating the four

fatigue analysis approaches consistent with the TxDOT HMAC mixture fatigue characterization

and pavement structural design for fatigue resistance. These factors include laboratory testing,

material properties, input data variability, analysis, field Nf results, and associated costs.

Appendix K is an example of the evaluation survey questionnaire and shows the sub-factors

associated with each factor. For each factor and sub-factor, the rating score was from 1 to 10,

with 10 representing the most significant factor/sub-factor and 1 being the least significant.

Figure 12-1 summarizes these rating results in a decreasing order of significance for both

the factors and sub-factors. Based on these rating scores, the averaged weighting scores out of a

total score of 100 percent were determined and are shown in parentheses in Figure 12-1.

According to these rating results, mixture field Nf results in terms of variability and tie to field

performance is the most significant factor to consider when selecting and recommending an

appropriate fatigue analysis approach to TxDOT. This factor has a weighting score of 22 percent.

Material properties were considered the least significant factor with a total weighting score of 14

percent. Within the factor “material properties,” mixture volumetrics (binder content and AV)

and modulus/stiffness were considered the most significant sub-factors with an equal weighting

score of 17 percent, while anisotropy was the least significant (9 percent). It is also worthwhile to

note that the factors “analysis” and “laboratory testing” have the same degree of importance

(with an equal weighting score of 15 percent).

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Results (22%)

Nf variability (50%) Tie to field performance (50%)

Costs (18%) Practicality of implementation (32%) Laboratory testing (hrs) (32%) Analysis (hrs) (19%) Equipment ($) (17%)

Input data (16%) Materials (36%) Traffic (34%) Environment (30%) Analysis (15%) Failure criteria (41%) Simplicity (36%) Versatility of inputs (23%) Laboratory testing (15%) Simplicity (32%) Equipment availability (29%) Equipment versatility (22%) Human resources (18%)

Material properties (14%) Mixture volumetrics (17%)

Modulus/stiffness (17%) Fracture (16%) Tensile strength (15%) Aging (14%) Healing (12%) Anisotropy (9%)

Figure 12-1. Assessment Factors/Sub-factors and Associated Weighting Scores.

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Assessment and Rating Criteria of the Fatigue Analysis Approaches

Using Tables 12-1 and 12-2, the research team assigned scores (out of 10) to each

sub-factor, as shown in Appendix L. For this analysis, the scores (with a range of 0 to 10) for

each sub-factor, e.g., those associated with the factor “results,” were defined as follows:

• Variability: 10/10 ≅ low, 5/10 ≅ low to high, and

0/10 ≅ high variability.

• Tie to field performance: 10/10 ≅ high, 5/10 ≅ low to high, and

0/10 ≅ low degree of or poor tie to field performance.

Using Figure 12-1, the weighted scores for each factor for each approach were summed

up as shown in Appendix L. Table 12-3 provides an evaluation summary of the scores and

ratings of the fatigue analysis approaches.

Table 12-3. Weighted Scores and Rating of the Fatigue Analysis Approaches.

Evaluation Score Category Weight

Guide ME CMSE CM

Results 22% 11% 9% 14% 13%

Cost 18% 12% 10% 12% 13%

Input data variability 16% 12% 8% 10% 10%

Analysis 15% 9% 9% 11% 10%

Laboratory testing 15% 12% 6% 12% 12%

Incorporation of material properties

14% 10% 8% 13% 12%

Total 100% 66% 50% 72% 70%

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Table 12-3 shows the weighting scores associated with each factor and the actual score

assigned for each approach. “Results,” for instance, has a total weighted score of 22 percent. For

this factor, the CMSE approach scored the highest score (14 percent) and would be ranked first

based on this factor. In terms of laboratory testing, while all the other approaches have the same

ranking based on equal scores (12 percent), the ME approach would be ranked last with a score

of 6 percent out of a weighted total of 15 percent. In terms of the overall scores (out of a total of

100 percent), the order of ranking is CMSE (72 percent), CM (70 percent), M-E Pavement

Design Guide (66 percent), and ME (50 percent).

The Selected Fatigue Analysis Approach – The CMSE Approach

Based on this value engineering assessment, as shown in Table 12-3, and considering the

test conditions in this project, the CMSE fatigue analysis approach with the highest score (75

percent) is recommended for predicting HMAC mixture fatigue life. With the possibility of

establishing a SE database in the future from various ongoing TxDOT projects, the CMSE

approach will become a reality both in terms of further validation and practical implementation.

Furthermore, a sensitivity analysis with more HMAC mixture characterization to streamline the

CMSE procedure will make the approach simple and practical to implement.

Based on the score ranking, the CM is recommended as the second alternative approach

in lieu of the CMSE approach to be utilized particularly in the absence of SE data. Note,

however, that the CM analysis models were modified in this project based on the CMSE results.

Consequently, more independent HMAC mixtures need to be characterized for fatigue resistance

to validate this correlation between the CMSE and the CM approaches. With further validation

through additional HMAC mixture characterization, CM is a potentially promising fatigue

analysis approach to be recommended over CMSE possibly at the end of this project.

Although the CMSE fatigue analysis approach is recommended in this project, it should

be noted that any fatigue design approach can produce desired results provided it is well

calibrated to the environmental and traffic loading conditions of interest and that all relevant

factors affecting performance are appropriately taken into consideration.

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Incorporation of Aging Effects in Field Nf Prediction

With further research and more binder and HMAC mixture fatigue characterization, a

shift factor due to aging (SFag or SFaging) will possibly be incorporated in the CMSE fatigue

analysis model, as illustrated in Chapters 10 and 11. While some aging shift factors were

developed in this project (SFag in Chapter 10 and SFaging in Chapter 11), validation of these

concepts is still required through testing of additional binders and HMAC mixtures. In contrast

to the simplicity adopted in these concepts, HMAC aging should possibly be modeled as a

function of three processes: binder oxidation, binder hardening, and field Nf reduction.

Additionally, the SFag (or SFaging) should be able to account for mix-design

characteristics, traffic loading, and environmental conditions. As pointed out in Chapter 10, field

HMAC aging is a relatively complex process involving fluctuating traffic loading and

environmental conditions. Note, however, that traffic (in terms of design ESALs) and

environmental effects (in terms of temperature) are also taken into account by the SFh (Chapter

5) in this CMSE approach. In addition, the rate of aging or response to binder oxidation and

hardening and subsequent reduction in fatigue resistance may differ from mixture to mixture

depending on the material type and mix-design characteristics. Most importantly, the SFag (or

SFaging) must be derived as a function of time so that Nf at any pavement age can be predicted.

Once these SFag have been developed and validated for a group of similar HMAC mixtures,

laboratory testing of aged HMAC mixtures may be unnecessary.

Recommendations on a Surrogate Fatigue Test and Analysis Protocol

The fatigue analysis approaches discussed in this report and the selected CMSE approach

incorporate stress-strain analysis that depends on both pavement structure and environmental

location. This is because stress and/or strain are required as an input parameter in these analyses.

Unlike other distresses, such as rutting or permanent deformation, fatigue cracking in the HMAC

layer depends on the entire pavement structure and its response to both traffic loading and the

environment. Consequently, a surrogate fatigue test and analysis protocol that is independent of

the pavement structure and environment cannot be recommended based on the fatigue analysis

approaches and results presented in this report. However, investigation of surrogate fatigue test

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protocols based on CMSE testing for use in mix design and HMAC mixture screening without

prediction of Nf is reported in Research Report 0-4468-3.

In the absence of a fatigue analysis model that is independent of stress and/or strain as

input parameters, the research team proposes establishing a database of a range of design stress

and/or strain levels for typical TxDOT HMAC pavement structures and the Texas environment.

Establishment of such a database to be used in conjunction with these fatigue analysis

approaches will facilitate an easier and quicker way of characterizing the fatigue resistance of

HMAC mixtures using some of the tests described in this report as surrogate tests. This will also

eliminate the need to conduct an extensive stress-strain analysis every time a HMAC mixture is

to be characterized for fatigue resistance.

SUMMARY

Key points from a comparison and selection of the fatigue analysis approaches are

summarized as follows:

• The four fatigue analysis approaches (ME, CMSE, CM, and M-E Pavement Design Guide)

were comparatively analyzed in terms of the following factors: theoretical concepts, input

data, laboratory testing, failure criteria, data analysis, results and variability, and associated

costs.

• Selection of the fatigue analysis approach was based on field Nf results, costs, input data

variability, analysis, laboratory testing, and incorporation of material properties consistent

with the TxDOT level of significance of each parameter. Based on this value engineering

assessment criteria and considering the test conditions in this project, the CMSE fatigue

analysis approach was selected and recommended for predicting HMAC mixture field Nf.

• Although the CMSE fatigue analysis approach was selected in this project, any fatigue

analysis approach can produce desired results provided it is well calibrated to the

environmental and traffic loading conditions of interest and that all relevant factors affecting

fatigue performance are appropriately taken into account.

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CHAPTER 13 CONCLUSIONS, RECOMMENDATIONS,

AND FUTURE WORK

From the data presented and analyzed in this interim report, the following conclusions,

recommendations, and future work plans are presented.

CONCLUSIONS

The selected fatigue analysis approach, a comparison of mixture field Nf, the effects of

binder oxidative aging and other input variables, binder and binder-mixture results are

summarized in this section.

Selected Fatigue Analysis Approach – CMSE

(1) Based on a value engineering assessment including laboratory testing, input data, statistical

analysis, costs, and the analysis procedure of each approach, the CMSE fatigue analysis

approach is recommended for predicting HMAC mixture fatigue life.

(2) In comparison to other approaches that were evaluated and for the test conditions considered

in this project, the CMSE approach exhibited better mixture field Nf prediction capability:

• It utilizes fundamental mixture properties to estimate field Nf, and incorporates the

continuum micromechanics-energy theories of fracture and healing in the fatigue analysis

of HMAC mixtures.

• It exhibits greater flexibility and the potential to account for most of the fundamental

HMAC material properties that affect HMAC pavement fatigue performance. These

properties include fracture, binder aging effects, healing, visco-elasticity, anisotropy,

crack initiation, and crack propagation.

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• With the exception of SE measurements, the CMSE laboratory tests are less costly both

in terms of billable time requirements and equipment. Laboratory testing for this

approach utilizes gyratory compacted specimens that are relatively easy to fabricate and

handle compared to beam specimens for the ME approach.

• The failure criterion of a 7.5 mm (0.3 inches) microcrack initiation, growth, and

propagation through the HMAC layer thickness closely correlates with actual fracture

damage accumulation in an in situ HMAC pavement structure compared to the failure

criteria of the other approaches, the M-E Pavement Design Guide and the ME approach.

• The CMSE mixture results exhibited lower variability in terms of the COV of Ln Nf.

• Has the potential to simultaneously model HMAC moisture sensitivity through the use of

surface energy data under wet conditions.

(3) Although the SE measurements for the CMSE analysis are lengthy in terms of test time, the

tests are performed only once for any binder or aggregate type from a particular source (as

long as there are no major compositional changes). The SE data can then be utilized for

numerous analysis applications including fatigue, permanent deformation, and moisture

sensitivity modeling in HMAC pavements. Thus, SE measurements are actually efficient

considering their repeated and widespread use for binder and aggregate materials that may be

utilized in different mixture designs in different projects.

(4) In the absence of SE data, the CM approach can be utilized in lieu of the CMSE approach.

The fundamental concepts, failure criteria, and analysis procedure are basically similar,

except for the following:

• SE laboratory measurements (both for binders and aggregates) and RM tests in

compression are not required in the CM approach.

• SE input data for both the binder and aggregate are not required in the CM approach.

Instead, the CM approach utilizes empirical relationships that were calibrated to the

CMSE approach to compute SFh and Paris’ Law fracture coefficients that are dependent

on RM (compression) and SE data in the CMSE approach.

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Comparison of Mixture Field Nf

(1) The Yoakum mixture exhibited better fatigue resistance in terms of the field Nf values for all

aging and environmental conditions and for all pavement structures considered in this project

compared to the Bryan mixture. This finding was observed in all the fatigue analysis

approaches. Also, the Yoakum mixture exhibited less susceptibility to aging compared to the

Bryan mixture. The research team hypothesizes that the Yoakum mixture’s improved fatigue

performance may be due to the following factors:

• The higher binder content for the Yoakum mixture (5.6 percent by weight of aggregate)

probably increased its fatigue resistance compared to the Bryan mixture, which was a 4.6

percent binder content by weight of aggregate.

• The effect of the SBS modifier and the 1 percent hydrated lime in the mixture could have

possibly decreased the Yoakum mixture’s susceptibility to oxidative hardening. In their

study, Wisneski et al. made similar observations that hydrated lime tended to improve the

performance of recycled asphalt (114). However, this phenomenon is yet to be explored

in greater depth.

• The binder-aggregate bond strength, as exhibited by the SE results, indicated a relatively

better bond compatibility for the Yoakum mixture (PG 76-22 plus gravel aggregate) than

for the Bryan mixture (PG 64-22 plus limestone aggregate).

(2) For the field Nf results, the Yoakum mixture exhibited higher variability in terms of the COV

of Ln Nf and 95 percent CI range.

Effects of Binder Oxidative Aging and Other Variables

(1) Binder aging reduces HMAC mixture resistance to fracture and ability to heal. Generally, all

mixtures exhibited a declining field Nf with aging.

(2) Both binders and mixtures stiffen with aging, and these changes quantitatively correlated

with each other.

(3) HMAC mixture field Nf performance depends on both pavement structure and environmental

conditions.

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(4) The computed temperature shift factors (aT) for the HMAC mixtures based on

time-temperature superposition principles using the Arrhenius model exhibited a linear

relationship with temperature. While these aT showed some sensitivity to mixture type, they

were by and large insensitive to binder oxidative aging effects.

Binder-Mixture Characterization

(1) Mixtures stiffen significantly in response to binder oxidative aging.

(2) For a given mixture specimen, mixture stiffening correlates directly to binder stiffening.

(3) The change in mixture stiffness for different mixtures relates differently to binder stiffness.

The Bryan mixture has a softer binder but a stiffer mixture compared to the Yoakum mixture.

(4) Mixture fatigue life declines significantly when the binder stiffens due to oxidative aging.

The amount of decline for a given amount of binder stiffening can vary significantly from

one mixture to the next.

(5) The decline in fatigue life with binder hardening appears to have a dramatic effect on

pavement service life. Thus, differences between mixtures and the impact of binder aging

on fatigue life can have a very significant impact on pavement life-cycle cost.

(6) From the binder-mixture relationships, aging shift factors (SFag) based on the binder

visco-elastic properties were developed for each mixture type, and a relationship was

developed between binder properties and mixture field Nf values. With more HMAC fatigue

characterization, development of a single set of SFag coefficients for a different group of

similar mixtures will inevitably allow for prediction of Nf at any pavement age without the

need to test aged mixtures.

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RECOMMENDATIONS

From the findings of this project, the following recommendations were made.

(1) More HMAC mixture laboratory fatigue characterization is recommended to:

• provide confidence and validation in the selected CMSE approach. The CMSE laboratory

test protocol, failure criteria, and analysis procedure should be reviewed and if needed,

modified accordingly. For instance, the 7.5 mm (0.3 inches) microcrack threshold should

be reviewed to establish its adequacy as representative of the fatigue cracking process in

the entire HMAC pavement structure. The current CMSE version is based on the

generalized hypothesis that the growth of one crack is representative of the field

pavement crack size distribution.

• populate the field Nf database of commonly used TxDOT rut resistant mixtures.

• provide additional data so as to adequately model and incorporate the effects of binder

oxidative aging.

(2) A numerical analysis software for the CMSE (and CM) fatigue analysis approach(es) should

be developed based on the analysis procedure described in this report. Such a program will

among others lead to the following benefits:

• simplify and reduce the time required for the CMSE/CM fatigue analysis process.

• minimize human associated errors resulting from manual calculations.

• facilitate a faster methodology of conducting a sensitivity analysis on the CMSE/CM

approach so as to reduce/eliminate redundant variables in CMSE/CM analysis models.

• facilitate a quicker and convenient way to validate and, if need be, modify the CMSE/CM

approach based on more laboratory HMAC mixture characterization.

(3) Because of the apparent importance of fatigue decline with oxidative binder stiffening, more

work is needed to understand this phenomenon and the essential features of mixture design

that impact this decline. This effect is believed to be as much a mixture as a binder property

and, if so, can only be established and understood through additional, carefully designed

combined mixture-binder studies.

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244

(4) For CMSE uniaxial laboratory testing, it is strongly recommended that the specimens must

always be properly aligned along the central axis of loading to minimize the induction of

undesirable moments that can lead to erroneous results.

CLOSURE

The CMSE/CM approaches described in this interim report are relatively new analysis

procedures for fatigue characterization of HMAC mixtures and therefore still may be subject to

review and/or modifications. These approaches predict Nf and recognize the dependence of

fatigue cracking on the entire pavement structure when subjected to traffic loading. Investigation

of surrogate fatigue test protocols based on CMSE testing for use in mix design and HMAC

mixture screening is reported in Research Report 0-4468-3.

CURRENT AND FUTURE FY05 WORK

In the modified project, the research team plans to expand on the materials characterized

in this interim report. This laboratory characterization of more HMAC mixtures will increase the

TxDOT field Nf database, validate and provide more confidence in the selected CMSE/CM

approach and, if need be, provide guidance on any necessary modifications. The third year will

also provide more data for understanding the important phenomenon of binder oxidative aging

and its influence on HMAC mixture fatigue resistance as well as developing shift factors to

account for binder oxidative aging when estimating mixture field Nf.

Based on the limited timeframe and budget for the third year, mixture design for the

FY05 mixtures will be limited to Superpave mixes only, with gravel as the only aggregate to be

used. PG 64-22 and PG 76-22 binders will be used with two modifiers (SBS and tire rubber

(TR)). In line with the prime objective and title of the overall project, the emphasis of the third

year work plan is to characterize more rut resistant mixtures and compare the subsequent

findings to the Yoakum mixture as well as to further investigate the effect of binder oxidative

aging on the mixture fatigue resistance. Consequently, the focus of the modified project will be

on modified binders, which provide rut resistant mixtures.

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245

Two binder content levels, optimum and optimum plus 0.5 percent, consistent with

TxDOT recommendations, will be utilized to investigate the effect of binder content on the

fatigue resistance of the rut resistant mixtures. In terms of aging conditions, only two (0 and 6

months at 60 °C [140 °F]) will be addressed to supplement the 0, 3, and 6 months aging

conditions.

Table 13-1 summarizes the possible FY05 mixtures based on a comprehensive factorial

experimental design that can estimate all the main factors (binder type-modifier type (BTMT),

binder content (BC), and aging) considered in the third year and the two-way interactions

(BC*aging, BTMT*aging, and BTMT*BC).

Table 13-1. Example of a Factorial Experimental Design for FY05.

Run/Mixture Binder Type-Modifier Type

Binder Content Aging Condition (Months)

1 PG 76-22_SBS Optimum 02 PG 76-22_TR Optimum 0

3 PG 76-22_SBS Optimum + 0.5% 04 PG 76-22_TR Optimum + 0.5% 05 PG 64-22 Optimum 06 PG 64-22 Optimum + 0.5% 0

7 PG 76-22_SBS Optimum 6

8 PG 76-22_TR Optimum 6

9 PG 76-22_SBS Optimum + 0.5% 6

10 PG 64-22 Optimum 611 PG 64-22 Optimum + 0.5% 6

12 PG 76-22_TR Optimum + 0.5% 6

Note that the mixtures in Italics (Runs # 1 and 7) in Table 13-1 are the rut resistant

mixtures already characterized in Phase I and presented in this interim report. At the end of the

project in the third year modification, the following will be addressed:

• validation and provision of more confidence in the selected and recommended CMSE

approach through utilization of more HMAC mixtures,

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246

• a database of mixture field Nf results based on the CMSE approach,

• a better understanding and quantification of the binder-mixture relationships and effects of

binder oxidative aging,

• development of a shift factor due to aging to be incorporated in the CMSE approach,

• investigation of the effects of binder content and modification on mixture field Nf and aging,

• development of a fatigue design check criteria for the CMSE fatigue analysis approach, and

• investigation of the possibility of establishing a surrogate fatigue test protocol based on

CMSE testing (TS, RM, or RDT) for use only in mix design and HMAC mixture screening

without prediction of Nf

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247

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100. Davison, R.R., et al., Size Exclusion Chromatography of Asphalts. Chromatographic

Science Series, pp. 211-247 (1995).

101. ASTM D 113 – 86. “Standard Test Method for Ductility of Bituminous Materials,”

Annual Book of ASTM Standards, 04.03, ASTM, Easton, Maryland, 23 (1994)

102. Jemison, H.B., et al., Application and Use of the ATR, FTIR Method to Asphalt Aging

Studies. Preprints - American Chemical Society, Division of Petroleum Chemistry,

pp. 490-495 (1990).

103. Liu, M., et al., Oxygen Uptake as Correlated to Carbonyl Growth in Aged Asphalts and

Asphalt Corbett Fractions. Industrial & Engineering Chemistry Research, pp. 466-467

(1998).

104. Ferry, J. D. Viscoelastic Properties of Polymers, Wiley, New York (1980).

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260

105. Williams, D.J., Polymer science and engineering. Prentice-Hall International Series in the

Physical and Chemical Engineering Sciences, Prentice-Hall, New Jersey (1971).

106. Huang, Y.H., Pavement Analysis and Design. Prentice Hall, New Jersey (1993).

107. Kandhal, P.S., Low-Temperature Ductility in Relation to Pavement Performance. In

ASTM STP 628: Low-Temperature Properties of Bituminous Materials and Compacted

Bituminous Paving Mixtures, C.R. Marek (Ed.), American Society for Testing and

Materials, PP. 95-106 (1977).

108. Schapery, R.A., A Theory of Crack Growth in Viscoelastic Media, Technical Report No.

2, Mechanics & Materials Research Center, Texas A&M University, College Station,

Texas (1973).

109. Christensen, R.M., and D.A. Anderson, ‘Interpretation of Dynamic Mechanical Test Data

for Paving Grade Asphalt Cements.” Journal of the Association of Asphalt Paving

Technologists, Vol. 61, pp. 67-98 (1992).

110. Medani, T.O., Huurman, M., and A.A.A. Molenaar, “On the Computation of Master

Curves for Bituminous Mixes.” EuroBitumen (2004).

111. Aparicio Ramos, S I., “Study of the Asphalt Pavement Damage through Non-Destructive

Testing on Overweight Truck Routes,” Masters Thesis, Texas A&M University, College

Station, Texas (2003).

112. Oh, Jeong-Ho, “Field Monitoring and Modeling of Pavement Response and Service Life

Consumption Due to Overweight Truck Traffic,” PhD Dissertation, Texas A&M

University, College Station, Texas (2004).

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261

113. Rowe, G.M., and M. G. Bouldin, “Improved Techniques to Evaluate the Fatigue

Resistance of Asphaltic Mixtures”. 2nd Euroaphalt and Eurobitumen Congress, Book 1,

pp. 754-763, Barcelona, Spain, September (2000).

114. Wisneski, M.L., J.M. Chaffin, R.R. Davison, J.A. Bullin, and C.J. Glover, Use of Lime in

Recycling Asphalt. Transportation Research Board No. 1535, pp. 117-123 (1996).

115. Juvinall, R.C., and K.M. Marshek, Fundamentals of Machine Component Design.

John Wiley & Sons (2000).

116. Coons, R.F., and P.H. Wright, An Investigation of the Hardening of Asphalt Recovered

from Pavements of Various Ages. Journal of the Association of Asphalt Paving

Technologists, pp. 510-528 (1968).

117. Ghuzlan, K., and S. Carpenter, “Energy-Derived, Damage-Based Failure Criterion for

Fatigue Testing,” Transportation Research Board, Vol. 1723, National Academy Press,

Washington D.C. (2000).

118. James Cox & Sons, Inc., 2004 Price List, Model CS7600 4-pt Bending Fixture, Colfax,

California (2004).

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263

APPENDICES

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APPENDIX A: EVALUATION FIELD SURVEY QUESTIONAIRE (FOR GOVERNMENT AGENCIES AND THE INDUSTRY)

TxDOT PROJECT 0-4468 FATIGUE RESISTANT MIXES AND DESIGN METHODOLOGY SURVEY

This survey is conducted as part of the Texas Department of Transportation (TxDOT) research Project No. 0-4468, Evaluation of the

Fatigue Resistance of Rut Resistant Mixes, under the supervision of Gregory Cleveland (512-506-5830). The primary goal of this project is to

develop and recommend the process for incorporating fatigue analysis and testing into TxDOT's pavement design and mixture design process.

TxDOT already has the means to screen out mixtures that are susceptible to rutting; mixtures with stiffer binders greatly decrease the risk of

premature failure due to rutting. However, there are concerns that some of the mixtures that are highly resistant to rutting may be more prone to

fatigue failure. To identify, document, and compare several materials, mixtures, and pavement structure types in terms of fatigue resistance, we

are sending out this survey to several government agencies and industry representatives in order to create a complete knowledge database.

We would appreciate your participation. If there are any questions concerning this survey or this project, please contact Dr. Amy Epps

Martin (979-862-1750) of the Texas Transportation Institute. Once again we appreciate your time and assistance.

Agency Name: __________________________________ Contact Name: ____________________________________

Phone: ( ____ ___ ) - ____________ - __________ Fax: ( ________ ) - ____________ - __________

_____________________________________________________________________________________________________________________

1. Do you utilize any methodology or approach to design and/or check for fatigue resistance?

YES __________ please proceed to question 2. NO __________ please stop.

2. What mix design methodology(ies) or approach(es) do you follow? _____________________________________________

3. List literature references you have found useful to approach fatigue resistance designs.

____________________________________________________________________________________________________________

4. List the laboratory tests, and corresponding standards, performed as part of the fatigue resistance approach(es) you use.

____________________________________________________________________________________________________________

5. What type(s) of aggregate(s) and binder(s) grades do 6. What pavement structure(s) do you commonly use for you use for fatigue resistant mixes? fatigue resistant pavement design?

Aggregate Type Binder Grade

Layer Thickness Elastic

Modulus

7. What type and amount of resources (time, persons, equipment, etc.) do you require to perform a fatigue resistant mix and pavement design?

Thank you for your time and effort in completing this survey. The results will aid us to identify, document, and compare several materials, mixtures, and pavement structure types in terms of fatigue resistance.

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APPENDIX A (CONTINUED): SUMMARY RESULTS OF EVALUATION FIELD SURVEY

QUESTIONAIRE

(FROM GOVERNMENT AGENCIES AND THE INDUSTRY)

TxDOT PROJECT 0-4468: FATIGUE RESISTANT MIXES AND DESIGN METHODOLOGY SURVEY

Table A1. Summary of Respondent Questionnaire Survey Details.

Materials Pavement Structures No. Agency Contact Fatigue

Methodology Laboratory

Tests Aggregate Binder Layer Thickness Modulus Resources Standards/

References

1

Advanced Asphalt Technologies, LLC

D W. Christensen 814-278 1991

Continuum damage analysis (NCHRP 9-25 and 9-31)

Uniaxial fatigue testing

9.5 – 12 mm, dense gradation

- - - -

-16 hrs -Compactor, ovens, molds, saw, coring rig, MTS system

AAPT papers on Continuum Damage modeling & analysis

2 Abatech G.Rowe 215 – 215 258

Superpave Bending beam and SHRP IDT - - - - - ≥ $40,000 Various paper

publications

3 Louisiana DOTD

C.Abadie 225-767 9109

Superpave

Modified T-283, Moisture sensitivity & retained ITS

Various PG 76-22 Modified - -

Use SN criteria, i.e. 0.44 to 0.48 for HMAC

No special design procedure for fatigue

Superpave

4 North Carolina State University

Y.R. Kim 619-515 7758

Visco-elastic continuum damage model

Uniaxial tension & indirect tension

Granite PG 64-22 - - - MTS & graduate students

-

5 Minnesota DOT

S. Dai 651-779 5218

Superpave & MnPave

No fatigue tests - - Mechanistic-empirically based One

researcher Superpave

6 UCB, Berkeley

M.O. Bejarano 510-231-5746

Caltrans & Asphalt Institute

Bending beam, AASHTO TP-8

Crushed stone, dense graded

AR 4000 AR 8000 AC 150 mm 1000 to

8 000 MPa

-2-3 wks -4 people -bending beam device (Cox & Sons)

-NCHRP 39 -Various publications

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APPENDIX B : HMAC ANISOTROPIC ADJUSTMENT FACTORS

Table B1. Example of Determination of Anisotropic Adjustment Factors (ai). HMAC Elastic Modulus

(MPa) Under Unconfined Conditions

HAMC Elastic Modulus (MPa) Under Confined

Conditions

Test#

Ex(u) Ez(u) Ex(c) Ez(c)

ax = Ex(c)/Ex(u)

az =

1/(Ez(c)/Ex(u))

1 1789 3399 1940 4450 1.08 0.76

2 1569 2980 1785 3927 1.14 0.76

3 1678 3188 1963 4320 1.17 0.74

4 1589 3219 1900 4180 1.20 0.77

5 1498 2846 1760 3972 1.17 0.71

Mean 1625 3127 1870 4170 1.15 0.75

Stdev 112 216 92 223 0.04 0.02

COV 6.90% 6.91% 4.91% 5.35% 3.76% 2.96%

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268

APPENDIX B (CONTINUED):

THE UNIVERSAL SORPTION DEVICE

Table B2. Summary of the Testing and Analysis Procedure for Determining the Surface Energy of Aggregates Using the USD Method.

Step Action

1 The aggregate sample is prepared from the fraction passing the No.4 (4.75mm) sieve, retained on

the No.8 (2.36mm) sieve.

• Wet sieve approximately 150 g of each type of aggregate. • Wash the samples again using distilled water and dry in a 120 °C (248 °F) oven for at least

8 hrs. • Move the samples into a vacuum desiccator at about 1 torr and 120 °C (248 °F) for at least

24 hrs to de-gas. • Wash the aggregate sample holder with distilled water and acetone and then dry in a 120°C

(248 °F) oven for 1 hr. 2 Place the weighed aggregate in the container and proceed with chamber conditioning:

• Connect the temperature control circulator with the high-pressure steel chamber. • Activate and calibrate the Magnetic Suspension Balance. • Use the vacuum pump to evacuate the chamber to below 1 torr for one day while it is

heated up to 60 °C (140 °F). • Reduce and maintain the chamber temperature at 25°C (77 °F) under the vacuum of below

1 torr for 8 hrs. 3 Proceed with testing using the selected solvents: n-hexane (apolar), methyl-propyl-ketone (mono-

polar) and water (bipolar):

• Initiate the computer program to control testing and control data capturing and enter 8 to 10 predetermined pressure steps based on the saturation vapor pressure of the solvents used. The following two steps are then controlled automatically and is included for completeness of process description.

• Solvent vapor is injected into the system until the first predetermined value is reached by using the macro-adjustment valve. After the steady-state adsorption mass is reached and measured by the system, the pressure is changed to the next setting point.

• Last step is repeated while the computer records the absorbed mass and vapor pressure until the saturated vapor pressure of solvent is reached.

4 Use the specific amount of solvent adsorbed on the surface of the adsorbent and vapor pressure at

the surface of the asphalt or aggregate to do surface energy calculations:

• Calculate the specific surface area of the aggregate using the BET equation. • Calculate the spreading pressure at saturation vapor pressure for each solvent using Gibbs

adsorption equation. • Calculate the three unknown components of surface energy utilizing the equilibrium

spreading pressure of adsorbed vapor on the solid surface and known surface energies of the a polar, mono-polar, and bipolar solvents.

5 Using SE results from step 4, calculate the total surface energy of the aggregate.

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APPENDIX C: BENDING BEAM LABORATORY TEST DATA FOR THE MECHANISTIC EMPIRICAL APPROACH

Table C1. ME Mixture N Data for 0, 3, and 6 Months Aging Conditions. Rows Micro

Strain Nf LabBryan-

0M

Nf Lab Bryan-

3M

Nf Lab Yoakum-

0M

Nf Lab Yoakum-

3M

Nf Lab Yoakum-

6M 1 374 131000 71400 246580 170000 76600 2 374 120000 90600 201000 191000 138000 3 374 130000 78560 . 155500 110000 4 468 55000 47000 95200 68200 40450 5 468 51000 32000 115500 90000 46000 6 468 46000 40500 . 100300 55000 7 157 . . . . . 8 278.96 . . . . . 9 273.21 . . . . . 10 289.47 . . . . . 11 (US290)

98.97 . . . . .

Table C2. Example of ME Log-Transformation of Table B1 Data.

Rows Log Micro Strain

Log Nf Lab

Bryan-0M

Log Nf Lab

Bryan-3M

Log Nf Lab

Yoakum-0M

Log Nf Lab

Yoakum-3M

Log Nf Lab

Yoakum-6M

1 5.92 11.78 11.18 12.42 12.04 11.25 2 5.92 11.70 11.41 12.21 12.16 11.84 3 5.92 11.78 11.27 . 11.95 11.61 4 6.15 10.92 10.76 11.46 11.13 10.61 5 6.15 10.84 10.37 11.66 11.41 10.74 6 6.15 10.74 10.61 . 11.52 10.92 7 5.06 . . . . . 8 5.63 . . . . . 9 5.61 . . . . . 10 5.67 . . . . . 11 (US290)

4.59 . . . . .

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APPENDIX C (CONTINUED): BB LABORATORY TEST DATA

Table C3. Example of ME 95 Percent Prediction Interval Estimates of Log Nf

(Bryan Mixture). Rows Log

Micro Strain

Predicted Log Nf

Bryan-0M (Yhat_B0)

Lower 95%

prediction interval

for Yhat_B0

Upper 95%

prediction interval

for Yhat_B0

Predicted Log Nf

Bryan-3M(Yhat_B3)

Lower 95%

prediction interval

for Yhat_B3

Upper 95%

prediction interval

for Yhat_B3

1 5.92 11.75 11.52 11.98 11.29 10.77 11.802 5.92 11.75 11.52 11.98 11.29 10.77 11.803 5.92 11.75 11.52 11.98 11.29 10.77 11.804 6.15 10.83 10.60 11.06 10.58 10.06 11.105 6.15 10.83 10.60 11.06 10.58 10.06 11.106 6.15 10.83 10.60 11.06 10.58 10.06 11.107 5.06 15.32 14.57 16.06 14.02 12.36 15.698 5.63 12.96 12.59 13.32 12.21 11.39 13.039 5.61 13.04 12.66 13.42 12.28 11.43 13.1210 5.67 12.80 12.46 13.15 12.10 11.32 12.8711 (US290) 4.59 17.21 16.14 18.28 15.48 13.08 17.88

Table C4. Example of ME 95 Percent Prediction Interval Estimates of Log Nf

(Yoakum Mixture). Rows Log

Micro Strain

Predicted Log Nf

Yoakum-0M

(Yhat_Y0)

Lower 95%

prediction interval

for Yhat_Y0

Upper 95%

prediction interval

for Yhat_Y0

Predicted Log Nf

Yoakum-3M

(Yhat_Y3)

Lower 95%

prediction interval

for Yhat_Y3

Upper 95%

prediction interval

for Yhat_Y3

1 5.92 12.31 11.57 13.05 12.05 11.54 12.562 5.92 12.31 11.57 13.05 12.05 11.54 12.563 5.92 12.31 11.57 13.05 12.05 11.54 12.564 6.15 11.56 10.82 12.30 11.35 10.84 11.865 6.15 11.56 10.82 12.30 11.35 10.84 11.866 6.15 11.56 10.82 12.30 11.35 10.84 11.867 5.06 15.23 12.50 17.96 14.77 13.13 16.418 5.63 13.30 12.01 14.58 12.97 12.17 13.779 5.61 13.37 12.03 14.70 13.04 12.20 13.8710 5.67 13.17 11.97 14.38 12.85 12.10 13.61

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APPENDIX D: DYNAMIC MODULUS LABORATORY TEST DATA FOR THE M-E PAVEMENT DESIGN GUIDE

Table D1. Summary of DM Values for

Bryan Mixture: Basic TxDOT Type C Mixture [PG 64-22 + Limestone].

Specimen # BDM0001, AV =6.56 Percent Temperature Dynamic Modulus, psi

oC oF 0.1 Hz 0.5 Hz 1.0 Hz 5.0 Hz 10 Hz 25 Hz -10 14 2,833,936 3,359,219 3,512,016 3,959,646 4,093,719 4,340,675 4.4 40 1,362,920 1,742,570 1,922,417 2,313,526 2,529,980 2,753,048

21.1 70 471,605 680,590 808,919 1,125,797 1,300,089 1,599,810 37.8 100 152,623 247,913 297,864 490,257 622,778 878,987 54.4 130 68,023 92,476 106,168 175,264 230,189 366,307

Specimen # BDM0002, AV =7.50 Percent

Temperature Dynamic Modulus, psi oC oF 0.1 Hz 0.5 Hz 1.0 Hz 5.0 Hz 10 Hz 25 Hz

-10 14 2,120,104 2,497,956 2,645,111 3,008,257 3,159,546 3,359,538 4.4 40 1,109,930 1,483,373 1,657,332 2,085,121 2,303,968 2,614,421

21.1 70 418,492 630,972 753,195 1,080,343 1,276,608 1,604,175 37.8 100 172,696 266,202 311,860 531,505 659,501 948,953 54.4 130 52,025 74,158 84,804 138,163 188,041 283,114

Specimen # BDM0003, AV =6.90 Percent Temperature Dynamic Modulus, psi

oC oF 0.1 Hz 0.5 Hz 1.0 Hz 5.0 Hz 10 Hz 25 Hz -10 14 2,316,644 2,778,531 2,950,198 3,420,947 3,601,258 3,895,873 4.4 40 1,269,660 1,634,343 1,813,320 2,221,456 2,431,326 2,738,008

21.1 70 445,048 655,781 781,057 1,103,070 1,288,348 1,601,993 37.8 100 125,313 193,466 226,085 369,658 478,044 645,244 54.4 130 72,983 95,478 104,862 165,952 215,831 338,576

Binder Content = 4.6 percent by weight of aggregate VMA = 14 percent at maximum density

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APPENDIX D (CONTINUED): DM LABORATORY TEST DATA

Table D2. Summary of DM Values for Yoakum Mixture: Rut Resistant 12.5 mm Superpave Mixture [PG 76-22 + Gravel].

Specimen # YDM0001, AV =6.80 Percent

Temperature Dynamic Modulus, psi oC oF 0.1 Hz 0.5 Hz 1.0 Hz 5.0 Hz 10 Hz 25 Hz

-10 14 1,823,472 2,389,410 2,612,666 3,241,115 3,485,344 3,899,108 4.4 40 1,124,434 1,558,590 1,759,177 2,291,190 2,525,325 2,890,051

21.1 70 269,944 504,934 638,616 1,011,870 1,223,640 1,607,120 37.8 100 71,852 124,239 152,333 283,839 388,353 641,603 54.4 130 32,996 46,862 52,547 95,116 135,030 251,495

Specimen # YDM0002, AV =6.90 Percent

Temperature Dynamic Modulus, psi oC oF 0.1 Hz 0.5 Hz 1.0 Hz 5.0 Hz 10 Hz 25 Hz

-10 14 1,102, 693 1,520,779 1,742,483 2,348,088 2,615,828 2,924,933 4.4 40 1,062,343 1,513,991 1,693,229 2,166,255 2,380,446 2,607,213

21.1 70 294,499 513,564 657,877 1,082,518 1,325,065 1,634,097 37.8 100 72,852 119,526 148,635 281,170 383,001 619,616 54.4 130 50,502 63,033 69,038 133,174 187,041 327,597

Specimen # YDM0003, AV =7.30 Percent

Temperature Dynamic Modulus, psi oC oF 0.1 Hz 0.5 Hz 1.0 Hz 5.0 Hz 10 Hz 25 Hz

-10 14 1,131,831 1,576,792 1,770,302 2,275,236 2,518,580 2,810,991 4.4 40 710,395 1,028,477 1,187,351 1,600,694 1,763,615 2,005,712

21.1 70 177,758 325,262 419,899 695,877 863,178 1,057,511 37.8 100 45,933 71,214 88,633 156,858 216,353 342,956 54.4 130 29,530 38,116 41,060 64,324 84,238 127,865

Binder Content = 5.6 percent by weight of aggregate VMA = 15.9 percent at maximum density

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APPENDIX E: EXAMPLE OF PERCENTAGE CRACKING ANALYSIS FROM THE M-E PAVEMENT DESIGN GUIDE SOFTWARE

Table E1. Example of the M-E Pavement Design Guide Software Analysis

for Bryan Mixture based on a 20-Year Design Life (WW Environment). Pavement Structure

HMAC Specimen Traffic ESALs (Millions)

Percent Cracking in Wheelpath (Output from Software)

BDM0001 2.50 26.80 BDM0002 2.50 38.3 BDM0003 2.50 31.80 BDM0001 5.00 45.60 BDM0002 5.00 59.90

PS1

BDM0003 5.00 51.60 BDM0001 2.50 21.9 BDM0002 2.50 36.80 BDM0003 2.50 28.60 BDM0001 5.00 53.90 BDM0002 5.00 71.50

PS2

BDM0003 5.00 63.20 BDM0001 1.25 29.90 BDM0002 1.25 40.10 BDM0003 1.25 36.60 BDM0001 2.50 61 BDM0002 2.50 70.00 BDM0003 2.50 67.20 BDM0001 5.00 78.10 BDM0002 5.00 89.80

PS3

BDM0003 5.00 87.40 BDM0001 1.25 26.60 BDM0002 1.25 43.80 BDM0003 1.25 32.30 BDM0001 2.50 58 BDM0002 2.50 70.10 BDM0003 2.50 64.30 BDM0001 5.00 85.50 BDM0002 5.00 96.25

PS4

BDM0003 5.00 88.30 BDM0001 2.50 7.85 BDM0002 2.50 13.51 BDM0003 2.50 9.02 BDM0001 5.00 15 BDM0002 5.00 20.40 BDM0003 5.00 18.10 BDM0001 25 55.10 BDM0002 25 70.40

PS5

BDM0003 25 63.89

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APPENDIX E (CONTINUED): EXAMPLE OF PERCENTAGE CRACKING ANALYSIS FROM THE M-E PAVEMENT DESIGN GUIDE SOFTWARE

Table E2. Example of the M-E Pavement Design Guide Software Analysis

for Bryan Mixture based on a 20-Year Design Life (DC Environment).

Pavement Structure

HMAC Specimen Traffic ESALs (Millions)

Percent Cracking in Wheelpath (Output from Software)

BDM0001 2.50 18.40 BDM0002 2.50 31.60 BDM0003 2.50 23.70 BDM0001 5.00 40.00 BDM0002 5.00 53.90

PS2

BDM0003 5.00 49.70 BDM0001 2.50 18.40 BDM0002 2.50 27.90 BDM0003 2.50 32.60 BDM0001 5.00 48.50 BDM0002 5.00 72.10

PS3

BDM0003 5.00 57.6 BDM0001 2.50 30.50 BDM0002 2.50 48.80 BDM0003 2.50 36.50 BDM0001 5.00 62.80 BDM0002 5.00 73.00

PS4

BDM0003 5.00 60.40

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APPENDIX F: ME MIXTURE LAB Nf RESULTS Mixture Lab Nf Prediction: ME Approach = 50 Percent Reduction in Flexural Stiffness

Table F1. Example of ME Lab Nf for Bryan Mixture for Wet-Warm (WW) Environment.

0 Months 3 Months 6 Months

95% Lab Nf Prediction Interval

95% Lab Nf Prediction Interval

95% Lab Nf Prediction Interval

Pavement Structure

(PS#) Lab Nf

Lower Upper

Lab Nf

Upper Lower

Lab Nf

Lower Upper

1 4,483,670 2,124,669 9,461,849 1,232,934 232,469 6,539,046 755,762 13,829 31,095,112

2 423,048 293,301 610,190 201,184 88,761 456,001 123,017 19,976 757,585

3 460,826 315,567 672,950 214,843 92,205 500,598 130,707 19,828 861,609

4 363,435 257,421 513,108 179,035 82,856 386,855 110,460 20,190 604,323

5 29,828,466 10,197,087 87,254,077 5,284,069 480,383 58,123,166 2,512,795 9,467 66,694,421

Table F2. Example of ME Lab Nf for Yoakum Mixture for Wet-Warm (WW) Environment.

0 Months 3 Months 6 Months

95% Lab Nf Prediction Interval

95% Lab Nf Prediction Interval

95% Lab Nf Prediction Interval

Pavement Structure

(PS#) Lab Nf

Lower Upper

Lab Nf

Upper Lower

Lab Nf

Lower Upper

1 4,105,724 267,604 62,992,098 2,592,589 502,685 13,371,222 2,420,257 208,917 28,038,084

2 595,841 164,629 2,156,527 429,285 192,011 959,764 303,309 91,221 1,008,496

3 639,003 168,256 2,426,800 458,188 199,448 1,052,585 327,014 94,442 1,132,320

4 526,257 158,105 1,751,663 382,383 179,264 815,650 265,371 85,614 822,545

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APPENDIX F (CONTINUED): ME MIXTURE LAB Nf RESULTS Mixture LAB Nf Prediction: ME Approach = 50 Percent Reduction in Flexural Stiffness

Table F3. Example of Variance Estimates for Predicted Log ME Lan Nf (Bryan Mixture, WW Conditions).

Micro Strain Log (Micro Strain)

Var(Log(Log Nf))_Bryan-0M

Var(Log(Lab Nf)))_Bryan-3M

157 5.06 0.272 0.602

278.96 5.63 0.132 0.292

273.21 5.61 0.142 0.302

289.47 5.67 0.122 0.282

98.97 4.59 0.392 0.862

Table F4. Example of Variance Estimates for Predicted Log ME Nf (Yoakum Mixture, WW Conditions).

Micro Strain Log (Micro Strain)

Var(Log(Lab Nf)))_Yaokum-0M

Var(Log(Log Nf)))_Yaokum-3M

Var(Log(Log Nf)))_Yaokum-6M

157 5.06 0.632 0.592 0.882 278.96 5.63 0.302 0.292 0.432 273.21 5.61 0.312 0.302 0.452 289.47 5.67 0.282 0.272 0.412 98.97 4.59 - - -

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APPENDIX G: CMSE MIXTURE LAB Nf RESULTS Mixture Lab Nf Prediction: CMSE Approach = 7.5 mm Crack Growth & Propagation through HMAC

Layer

Table G1. Example of Bryan Mixture for Wet-Warm (WW) Environment.

0 Months 3 Months 6 Months

95% Lab Nf Prediction Interval

95% Lab Nf Prediction Interval

95% Lab Nf Prediction Interval

PS#

Lab Nf

Lower Upper

Lab Nf

Upper Lower

Lab Nf

Lower Upper

1 6,310,031 5,891,450 7,896,612 2,419,856 2,175,875 3,181,037 940,447 820,866 1,258,028

2 4,310,723 4,008,142 4,613,304 2,311,781 1,809,200 2,814,362 1,001,560 798,979 1,204,141

3 4,425,803 4,120,250 4,728,412 2,428,810 1,926,329 2,931,491 1,211,403 1,008,822 1,413,984

4 3,960,542 3,955,200 4,005,620 2,189,413 1,686,832 2,691,994 1,309,518 1,106,937 1,512,099

5 11,123,548 9,820,967 13, 118,456 8,600,514 7,397,933 9,803,095 5,081,720 4,279,139 5,884,301

Table G2. Example of Yoakum Mixture for Wet-Warm (WW) Environment.

0 Months 3 Months 6 Months

95% Lab Nf Prediction Interval

95% Lab Nf Prediction Interval

95% Lab Nf Prediction Interval

PS#

Lab Nf

Lower Upper

Lab Nf

Upper Lower

Lab Nf

Lower Upper

1 7,879,929 6,315,948 8,921,110 4,954,378 3,733,797 5,334,959 3,229,895 2,179,244 3,980,406

2 5,893,480 4,590,899 7,196,061 3,057,842 2,257,261 3,858,423 2,115,169 1,214,568 3,015,750

3 5,899,598 4,597,017 7,202,179 3,118,460 2,317,879 3,919,041 2,009,481 1,108,900 2,910,062

4 4,001,831 3,979,250 4,041,412 3,057,181 2,156,600 3,957,762 1,980,815 1,080,234 2,881,396

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APPENDIX H: CM MIXTURE LAB Nf RESULTS

Mixture Lab Nf Prediction: CM Approach = 7.5 mm Crack Growth & Propagation through HMAC Layer

Table H1. Example of Bryan Mixture for Wet-Warm (WW) Environment.

0 Months 3 Months 6 Months

95% Lab Nf Prediction Interval

95% Lab Nf Prediction Interval

95% Lab Nf Prediction Interval

PS#

Lab Nf

Lower Upper

Lab Nf

Upper Lower

Lab Nf

Lower Upper

1 6,290,861 5,825,280 7,626,442 2,313,584 1,651,003 3,452,165 914 ,861 612,480 1,413,442

2 4,811,422 3,910,841 5,712,003 2,011,781 2,011,781 2,912,362 989,795 589,214 1,390,376

3 4,181,312 3,980,731 4,381,893 2,611,912 2,611,912 3,512,493 1,009,215 808,634 1,209,796

4 3,980,182 3,959,601 4,000,763 2,204,315 2,204,315 3,104,896 995,850 895,264 1,096,431

5 10,891,433 9,690,852 12,092,014 8,401,515 8,401,515 9,902,096 4,890,253 3,889,672 5,890,834

Table H2. Example of Yoakum Mixture for Wet-Warm (WW) Environment.

0 Months 3 Months 6 Months

95% Lab Nf Prediction Interval

95% Lab Nf Prediction Interval

95% Lab Nf Prediction Interval

PS#

Lab Nf

Lower Upper

Lab Nf

Upper Lower

Lab Nf

Lower Upper

1 7,281,594 6,121,013 7,922,175 5,169,851 3,960,670 5,761,832 3,132,561 2,633,980 3,335,142

2 4,989,845 4,089,264 5,890,420 3,000,221 2,699,640 3,300,802 2,542,506 2,161,925 2,923,087

3 5,600,125 5,0995,544 6,100,706 2,986,420 2,689,839 3,287,001 1,998,652 1,718,071 2,279,233

4 4,121,458 4,000,877 4,224,039 3,116,108 2,765,527 3,466,689 1,500,824 1,260,243 1,741,405

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APPENDIX I: MIXTURE FIELD Nf RESULTS

ME Approach = 50 Percent Reduction in Flexural Stiffness

Table I1. Example of ME Field Nf (Field Nf = SF × Lab Nf): Bryan Mixture, WW Environment.

0 Months 3 Months 6 Months

95% Field Nf Prediction Interval

95% Field Nf Prediction Interval

95% Field Nf Prediction Interval

Pavement Structure

(PS#) Field Nf

Lower Upper

Field Nf

Upper Lower

Field Nf

Lower Upper

1 8.519E+07 4.037E+07 1.798E+08 2.343E+07 4.417E+06 1.242E+08 1.436E+07 2.628E+05 5.908E+08

2 8.038E+06 5.573E+06 1.159E+07 3.822E+06 1.686E+06 8.664E+06 2.337E+06 3.795E+05 1.439E+07

3 8.756E+06 5.996E+06 1.279E+07 4.082E+06 1.752E+06 9.511E+06 2.483E+06 3.767E+05 1.637E+07

4 6.905E+06 4.891E+06 9.749E+06 3.402E+06 1.574E+06 7.350E+06 2.099E+06 3.836E+05 1.148E+07

5 5.667E+08 1.937E+08 1.658E+09 1.004E+08 9.127E+06 1.104E+09 4.774E+07 1.799E+05 1.267E+09

Table I2. Example of ME Field Nf (Field Nf = SF × Lab Nf): Yoakum Mixture, WW Environment.

0 Months 3 Months 6 Months

95% Field Nf Prediction Interval

95% Field Nf Prediction Interval

95% Field Nf Prediction Interval

Pavement Structure

(PS#) Field Nf

Lower Upper

Field Nf

Upper Lower

Field Nf

Lower Upper

1 7.801E+07 5.084E+06 1.197E+09 4.926E+07 9.551E+06 2.541E+08 4.598E+07 3.969E+06 5.327E+08

2 1.132E+07 3.128E+06 4.097E+07 8.156E+06 3.648E+06 1.824E+07 5.763E+06 1.733E+06 1.916E+07

3 1.214E+07 3.197E+06 4.611E+07 8.706E+06 3.790E+06 2.000E+07 6.213E+06 1.794E+06 2.151E+07

4 9.999E+06 3.004E+06 3.328E+07 7.265E+06 3.406E+06 1.550E+07 5.042E+06 1.627E+06 1.563E+07

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APPENDIX I (CONTINUED): MIXTURE FIELD Nf RESULTS

CMSE Approach = 7.5 mm Crack Growth and Propagation through HMAC Layer

Table I3. Example of CMSE Field Nf (Field Nf = [SFa × SFh] × Lab Nf): Bryan Mixture, WW Environment.

0 Months 3 Months 6 Months

95% Field Nf Prediction Interval

95% Field Nf Prediction Interval

95% Field Nf Prediction Interval

Pavement Structure

(PS#) Field Nf

Lower Upper

Field Nf

Upper Lower

Field Nf

Lower Upper

1 6.922E+07 6.463E+07 8.663E+07 1.893E+07 1.702E+07 2.488E+07 6.034E+06 5.267E+06 8.072E+06

2 4.729E+07 4.397E+07 5.061E+07 1.808E+07 1.415E+07 2.201E+07 6.426E+06 5.126E+06 7.726E+06

3 4.855E+07 4.520E+07 5.187E+07 1.900E+07 1.507E+07 2.293E+07 7.773E+06 6.473E+06 9.073E+06

4 4.345E+07 4.339E+07 4.394E+07 1.712E+07 1.319E+07 2.105E+07 8.402E+06 7.102E+06 9.702E+06

5 1.220E+08 1.077E+08 1.439E+08 6.726E+07 5.786E+07 7.667E+07 3.261E+07 2.746E+07 3.776E+07

Table I4. Example of CMSE Field Nf (Field Nf = [SFa × SFh] × Lab Nf): Yoakum Mixture, WW Environment.

0 Months 3 Months 6 Months

95% Field Nf Prediction Interval

95% Field Nf Prediction Interval

95% Field Nf Prediction Interval

Pavement Structure

(PS#) Field Nf

Lower Upper

Field Nf

Upper Lower

Field Nf

Lower Upper

1 1.201E+08 9.629E+07 1.360E+08 4.905E+07 3.697E+07 5.282E+07 2.953E+07 1.993E+07 3.640E+07

2 8.985E+07 6.999E+07 1.097E+08 3.028E+07 2.235E+07 3.820E+07 1.934E+07 1.111E+07 2.758E+07

3 8.995E+07 7.009E+07 1.098E+08 3.088E+07 2.295E+07 3.880E+07 1.837E+07 1.014E+07 2.661E+07

4 6.101E+07 6.067E+07 6.162E+07 3.027E+07 2.135E+07 3.919E+07 1.811E+07 9.878E+06 2.635E+07

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APPENDIX I (CONTINUED): MIXTURE FIELD Nf RESULTS

CM Approach = 7.5 mm Crack Growth and Propagation through HMAC Layer

Table I5. Example of CM Field Nf (Field Nf = [SFa × SFh] × Lab Nf): Bryan Mixture, WW Environment.

0 Months 3 Months 6 Months

95% Field Nf Prediction Interval

95% Field Nf Prediction Interval

95% Field Nf Prediction Interval

Pavement Structure

(PS#) Field Nf

Lower Upper

Field Nf

Upper Lower

Field Nf

Lower Upper

1 6.901E+07 6.390E+07 8.366E+07 1.809E+07 1.291E+07 2.700E+07 5.870E+06 3.930E+06 9.069E+06

2 5.278E+07 4.290E+07 6.266E+07 1.573E+07 1.573E+07 2.278E+07 6.351E+06 3.781E+06 8.921E+06

3 4.587E+07 4.367E+07 4.807E+07 2.043E+07 2.043E+07 2.747E+07 6.475E+06 5.188E+06 7.762E+06

4 4.366E+07 4.344E+07 4.389E+07 1.724E+07 1.724E+07 2.428E+07 6.390E+06 5.744E+06 7.035E+06

5 1.195E+08 1.063E+08 1.326E+08 6.571E+07 6.571E+07 7.744E+07 3.138E+07 2.496E+07 3.780E+07

Table I6. Example of CM Field Nf (Field Nf = [SFa × SFh] × Lab Nf): Yoakum Mixture, WW Environment.

0 Months 3 Months 6 Months

95% Field Nf Prediction Interval

95% Field Nf Prediction Interval

95% Field Nf Prediction Interval

Pavement Structure

(PS#) Field Nf

Lower Upper

Field Nf

Upper Lower

Field Nf

Lower Upper

1 1.110E+08 9.332E+07 1.208E+08 5.119E+07 3.921E+07 5.705E+07 2.864E+07 2.409E+07 3.050E+07

2 7.608E+07 6.234E+07 8.981E+07 2.970E+07 2.673E+07 3.268E+07 2.325E+07 1.977E+07 2.673E+07

3 8.538E+07 7.775E+08 9.301E+07 2.957E+07 2.663E+07 3.254E+07 1.828E+07 1.571E+07 2.084E+07

4 6.284E+07 6.100E+07 6.440E+07 3.085E+07 2.738E+07 3.432E+07 1.372E+07 1.152E+07 1.592E+07

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APPENDIX I (CONTINUED): MIXTURE FIELD Nf RESULTS

The M-E Pavement Design Guide = 50 Percent Cracking in Wheelpath

Table I7. Example of 0 Months Results with Global Aging Model Analysis based on a 20-Year Design Life (WW Environment).

Bryan Mixture Yoakum Mixture

95% Field Nf Prediction Interval

95% Field Nf Prediction Interval

PS#

Field Nf

Lower Upper

Field Nf Lower

Lower Upper

1 4.705E+06 1.927E+06 9.737E+06 6.210E+06 2.037E+06 1.534E+07

2 4.047E+06 1.996E+06 6.354E+06 5.750E+06 2.348E+06 1.054E+07

3 1.932E+06 0.000E+00 3.737E+06 3.410E+06 1.345E+05 7.771E+06

4 2.018E+06 2.802E+05 3.563E+06 2.970E+06 3.491E+05 6.000E+06

5 1.929E+07 1.420E+07 2.483E+07 - - -

Table I8. Example of 0 Months Results with Global Aging Model Analysis based on a 20-Year Design Life

(DC Environment). Bryan Mixture

95% Field Nf Prediction Interval

PS#

Field Nf Lower Upper

2 5.229E+06 2.948E+06 9.924E+06

3 4.290E+06 1.646E+06 7.836E+06

4 3.563E+06 2.639E+05 6.530E+06

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APPENDIX I (CONTINUED): MIXTURE FIELD Nf RESULTS

Example of CMSE and CM Field Nf Prediction at Year 20 (PS# 1, WW Environment)

Table I9. Example of CMSE Field Nf Prediction at Year 20 (PS# 1, WW Environment)

HMAC Mixture SFag @ SFa SFh [Ni + Np] Nf = [SFag ]× [SFa × SFh] ×[Ni + Np]

Bryan 0.045 1.63 6.73 6.31E+06 3.11E+06 Yoakum 0.070 2.10 7.26 7.88E+06 8.40E+06

Table I10. Example of CM Field Nf Prediction at Year 20 (PS# 1, WW Environment)

HMAC Mixture SFag @ SFa SFh [Ni + Np] Nf = [SFag ]× [SFa × SFh] ×[Ni + Np]

Bryan 0.045 1.63 6.73 6.29E+06 3.10E+06 Yoakum 0.070 2.10 7.26 7.28E+06 7.77E+06

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APPENDIX I (CONTINUED): MIXTURE FIELD Nf RESULTS

Example of ME Field Nf Prediction at Year 20 (PS# 1, WW Environment)

1.0E+05

1.0E+06

1.0E+07

0 5 10 15 20 25

Pavement Age (Years)

Mea

sure

d La

b N

f

Bryan Yoakum

Figure I1. Example of Lab Nf Trend with Pavement Age (0 months ≅ 0 years, 3 months ≅ 6 years, and 6 months ≅12 years).

Approximate Lab Nf values at year 20 based on extrapolations in Figure I1 are approximately:

Bryan mixture: Lab Nf = 0.20 E+06

Yoakum mixture: Lab Nf = 1.56 E+06

Using the following ME equation (Chapter 4) with SF = 19, M = 3.57, and TCF = 1, the field Nf

values at year 20 are approximately predicted as follows:

( )[ ]TCFM

NLabSFTCFM

kSFFieldN f

kti

f ×

×=

×=

− 2ε

Bryan mixture: Field Nf ≅ 19* 0.20E+06/(3.57*1) ≅ 1.03 E+06

Yoakum mixture: Field Nf ≅19*1.56E+06/(3.57*1) ≅ 8.30 E+06

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APPENDIX J: RESOURCE REQUIREMENTS

Table J1. Approximate Time (hrs) Requirement to Produce at Least One Mixture Nf Result.

Task 2002 Guide ME CMSE CM

Specimen fabrication 43.75 hrs 45.5 hrs 43.75 hrs 43.75 hrs

Specimen temperature conditioning 20 hrs 4 hrs 15 hrs 11 hrs Lab testing (including set-up) 5 hrs 30 hrs 70 hrs 5 hrs Data analysis 4.5 hrs 3 hrs 6 hrs 5 hrs

Total 72.25 hrs 82.5 hrs 134.75 hrs 64.75 hrs

Note: For the CMSE approach, about 65 hrs lab testing is for surface energy measurements. SE values for asphalts and aggregates are required as CMSE input. Though the current SE test protocol for aggregates might require a test time of about 30 to 60 hrs per aggregate, various alternate and time efficient SE measurement methods are being investigated in other ongoing research projects. Despite the lengthy test time, SE measurements are only performed once for any asphalt or aggregate type from a particular source (as long as there are no major compositional changes). The SE data can then be utilized for numerous analysis applications including fatigue, permanent deformation, and moisture sensitivity modeling in HMAC pavements. Thus, SE measurements are actually efficient considering their repeated and widespread use for asphalt and aggregate materials that may be utilized in different mixture designs.

Table J2. Typical Equipment Requirements.

Task 2002 Guide ME CMSE CM

Binder-Aggregate Mixing Electric mixer Electric mixer Electric mixer Electric mixer

Compacting SGC Linear kneading SGC SGC

Testing MTS LVDTs Control unit

MTS LVDT Control unit BB device

MTS LVDTs Control unit Whilmey Plate USD device

MTS LVDTs Control unit

Data acquisition Automated computer system

Automated computer system

Automated computer system

Automated computer system

Temperature control unit Thermocouples Thermocouples Thermocouples Thermocouples

Other test accessories Attachment plates Attachment plates

Data analysis 2002 Software Excel/manual Excel/manual Excel/manual

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APPENDIX J (CONTINUED): RESOURCE REQUIREMENTS

Table J3. Approximate Time (hrs) Requirements for a Single Specimen Fabrication.

# Task ME

(Beam Specimen) CMSE, CM, & M-E Pavement

Design Guide (Cylindrical Specimen)

1 Aggregate batching 0.5 hrs 0.5 hrs

2 Aggregate pre-heating (minimum ≅ 4 hrs)

12 hrs (overnight)

12 hrs (overnight)

3 Binder liquefying (heating) 0.5 hrs 0.5 hrs

4 Binder aggregate mixing 0.25 hrs 0.25 hrs

5 PP2 Short-Term Oven Aging @ 135 °C (275 °F) 4 hrs 4 hrs

6 Heating for compaction 0.5 hrs 0.5 hrs 7

Compaction 0.25 0.25 hrs

8 Specimen cooling 12 hrs (overnight)

12 hrs (overnight)

9 Sawing & coring (with water) 2 hrs 0.5 hrs

10 Drying after sawing/coring 12 hrs (overnight)

12 hrs (overnight)

11 AV measurements 0.75 hrs 0.25 hrs 12 Cleaning up 1 hrs 1 hrs Total 45.75 hrs 43.75 hrs

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APPENDIX K: TxDOT EVALUATION SURVEY QUESTIONNAIRE

Evaluation & Weighting of Factors for the Selection of Appropriate Fatigue Analysis Approach.

Factor Rating: 1-10

(1 = least important) (10 = most important)

Sub-factor Rating: 1 – 10 (1 = least important) (10 = most important)

Simplicity Equipment availability Equipment versatility

Laboratory testing

Human resources Traffic Materials

Input variability

Environment (temperature & moisture)

Mixture volumetrics Modulus/stiffness Tensile strength Aging Healing Fracture

Incorporation of material properties in analysis

Anisotropy Simplicity Versatility of inputs

Analysis

Definition of failure criteria Nf variability Results Tie to field validation Lab testing (hrs) Equipment ($) Analysis (hrs) -Lab data reduction -Nf computation

Cost

Practicality of implementation

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APPENDIX L: RATING CRITERIA OF THE FATIGUE ANALYSIS APPROACHES

ME CMSE CM 2002 GUIDE CATEGORY WEIGHT (1)

ITEM WEIGHT(2) SCORE EVALUATION SCORE EVALUATION SCORE EVALUATION SCORE EVALUATION

COMMENT

Nf variability 50% 3/10 3.30% 8/10 8.80% 7/10 7.70% 5/10 5.50%Tie to field validation 50% 5/10 5.50% 5/10 5.50% 5/10 5.50% 5/10 5.50%

Results 22%

100% 40% 9% 65% 14% 60% 13 50% 11% CMSE

Practicality 32% 6/10 3.46% 6/10 3.5% 6/10 3.5% 6/10 3.5%

Testing (hrs) 32% 4/10 2.30% 7/10 4% 8/10 4.6% 7/10 4%Analysis (hrs) 19% 8/10 2.74% 6/10 2.05% 6/10 2.05% 6/10 2.05%

Equipment ($) 17% 6/10 1.84% 8.5/10 2.6% 8/10 2.45% 8/10 2.45%

Cost 18%

100% 57% 10% 65% 12% 70% 13% 67% 12%

CM

Materials 36% 5/10 3% 8/10 5% 8/10 5% 6/10 3%Traffic 34% 5/10 3% 5/10 3% 5/10 3% 9/10 5%

Environment 29% 5/10 2% 5/10 2% 5/10 2% 8/10 4%

Input variability

16%

100% 50% 8% 60% 10% 60% 10% 75% 12%

2002 GUIDE

Failure criteria 41% 5/10 3% 8/10 5% 7/10 4% 5/10 3.1%Simplicity 36% 8.5/10 5% 5/10 3% 6/10 3% 6/10 3.2%Versatility of inputs 23% 4/10 1% 10 3% 8/10 3% 7/10 2.4%

Analysis 15%

100% 60% 9% 74% 11% 69% 10% 58% 9%

CMSE

Simplicity 32% 5/10 2.4% 8/10 3.84% 9/10 4.3% 9/10 4.32%

Equipment availability 29% 3/10 1.3% 7/10 3.05% 7/10 3.0% 7/10 3.05%Equipment versatility 22% 2/10 0.7% 10/10 3.30% 8/10 2.3% 8/10 2.64%Human resources 18% 5/10 1.4% 8/10 2.16% 8/10 2.2% 8/10 2.16%

Lab testing 15%

100% 38% 6% 82% 12% 81% 12% 81% 12%

CMSE

Mixture volumetrics 17% 6/10 1.4% 9/10 2.1% 9/10 2.1% 10/10 2.4%Modulus/stiffness 17% 8/10 1.9% 9/10 2.1% 9/10 2.1% 10/10 2.4%

Fracture 16% 5/10 1.1% 10/10 2.2% 8/10 1.8% 5/10 1.1%

Tensile strength 15% 5/10 1.1% 10/10 2.1% 1/100 2.1% 5/10 1.1%

Aging 14% 5/10 1.0% 9/10 1.8% 9/10 1.8% 8.5/10 1.8%Healing 12% 5/10 0.8% 9/10 1.5% 7.5/10 1.3% 5/10 0.8%

Anisotropy 9% 5/10 0.6% 9/10 1.1% 9/10 1.1% 5/10 0.6%

Incorporation of Material Properties

14%

100% 57% 8% 93% 13% 88% 12% 73% 10%

CMSE

Total 100% 50% 72% 70% 66% CMSE Example of Score and Evaluation Calculations: Evaluation = [Score × Weight (1) × Weight (2)], Score sub-total = ∑[Score ×Weight (2)], and Total scores = ∑[Evaluation]

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