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Conceptual Demo Guide

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    2013 Aspen Technology, Inc. All rights reserved

    Conceptual Solids Modelsin Aspen Plus V8.4Guide to the Demo

    Aspen Technology

    Burlington, MA

    2013

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    Conceptual Solids Models

    Conceptual models ease learning experience for new solidsusers such as process engineers

    Not necessary to have in-depth knowledge of particletechnology or the specific apparatus

    More experienced solids users can use conceptual models to

    sketch the solids processing section before adding moredetails (if necessary)

    Conceptual model can be changed to a more rigorous modelwithout reconnecting streams

    Conceptual models allow for better collaboration betweenprocess engineers and particle scientists

    Process engineer can include solids sections in the overallflowsheet using conceptual solids models

    Particle scientist can work with the process engineer to makethe model more rigorous if necessary

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    Conceptual Solids Models

    Conceptual solids models enable everybody tomodel solids without being a solids expert

    Conceptual(process engineer)

    Rigorous Equipment Model(solids expert)

    3 parameters todefine a decanter

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    Conceptual Solids Models

    Functionality of conceptual models Comminution/Formulation

    (Crusher, Granulator, Crystallizer)

    Specify outlet PSD

    Solid Separators(Centrifuge, Cyclone, ESP, Scrubber etc.)

    Specify Desired Split

    Dryers

    Specify Outlet Moisture

    Crystallizer Crusher Granulator Flash 2

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    Example:Aspen Plus Model Bisphenol A (BPA) Production

    Demo Focus: BPAPurification Section

    Large, mostly fluid process

    Includes several solids unit operations and a purificationsection at the end of the process

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    BPA Purification Section of the Process

    BPA is crystallized intoluene to remove residualphenol. The BPA crystalsare dried with nitrogen toremove toluene. The finalproduct is melted and sentto a heated storage tank

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    Open the file Conceptual Model Example

    Isolated purificationsection from the

    larger BPA Process

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    Conceptual Modeling Example

    Dryer isdescribed by a

    rigorous model

    Optimizer is used toadjust the nitrogen

    flow to reach a purityof 99.9%

    Conceptualmodel is used for

    the centrifuge

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    Conceptual Model of the Decanter

    Open the input form of centrifuge S502

    conceptual model is used for the centrifuge

    split of solids and liquid is described by split factors

    solids separation is modeled by a separation curve based onparticles settling velocity and a given separation sharpness

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    Calculation Results

    Run the example and show the results for centrifuge S502

    show the separation curve (switch to log. X-axis)

    model is more than just a splitter model, describes separationbased on settling velocity

    Tip: Change the scale ofthe X-axis to log to get abetter resolution

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    Calculation Results

    Custom tables shows

    Necessary dry gas flowrate (determine by theoptimizer)

    Power and utility costsfor the blower (K505)

    Duty and utility costsfor the nitrogen heater(E504)

    Duty and utility costsfor the exhaust heater(E503)

    Total process utility cost

    Total process utility cost in the base case are 32.30 $/hr(~283.5 K$/HR)

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    Objective

    Goals

    Necessary dry gas flow rate (determine by the optimizer)

    BPA must by purified

    reduce energy demand for the dryer and with this theprocess utility costs

    Constraints Throughput must not be changed

    Purity of the product must be minimum 99.9%

    Idea

    Investigate the influence of the moisture content from thesolids stream leaving the centrifuge on the utility costs

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    Set up a Sensitivity Analysis

    Create a sensitivity case to investigate the influence of the

    solids outlet moisture from the centrifuge on the utility costs

    Click New

    Enter ID and clickOK

    1

    23

    Position vary input form onthe left of your screen

    4Open input form of centrifuge S502 and positionthe form right on the screen

    5

    Use right click and new vertical tab.

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    Set up a Sensitivity Analysis

    6

    drag & drop

    Drag and drop thefraction of liquid toliquid outlet to themanipulatedvariable section

    7

    Varyfraction ofliquid to liquid

    outlet from 0.4 to0.6 (10 points)

    Vary

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    Set up a Sensitivity Analysis

    8

    drag & drop

    Drag and drop variables from thecustom table into the measuredvariables are- E504 Utility cost (heater before dryer)- E503 Utility costs (heater after dryer)- E505 Power costs (blower)

    Rename variables E504, E505,

    Blower in the define tab

    9

    Select tabulated variables and

    click the Fill Variables button

    Define

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    Run & Review Sensitivity Results

    Run the model andreview the results

    Reduced outlet solidsmoisture content fromthe centrifuge leads toreduced utility costs forthe heaters and the

    blower (conceptualmodel predicts a linearrelationship)

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    Objective: Gain furtherunderstanding of how theoperating conditions of thedecanter influences theutility costs of the process

    Solution: Convert the model to

    rigorous

    Conduct a sensitivitystudy using the rigorous

    model of the decanter

    Reduce Energy Costs

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    Switch to Equipment Model

    Switch the centrifuge (block S502) to the equipment model

    Not necessary to reconnect streams

    Select decanterequipment model

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    Switch to Equipment Model

    Select classification and deliquoring model

    (already pre-defined in the example)

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    Switch to Equipment Model

    Enter model and geometryparameter (already pre-defined in the example)

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    Hide Sensitivity

    Hide sensitivity case

    Only deactivating the sensitivity case will lead to an error duringinput translation since the varied variable is no longer exists

    Want to reuse the sensitivity case later on

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    Run Simulation with the rigorous model

    Run simulation and review separation efficiency curve if S502

    Tip: Change the scale ofthe X-axis to log to get abetter resolution

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    Comparison of Results from Conceptual andEquipment Model

    Equipment models predicts a slightly different separation curve

    (based on given geometry and operating conditions)leads to different dry gas flow and therefore slightly different utility costs

    Results with equipment model

    Results with conceptual model

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    Change Sensitivity Case

    Reveal the defined sensitivity task

    Use sensitivity analysis to determine how the rpm of thedecanter influence the utility costs of the process

    1

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    Change Sensitivity Case

    2Open sensitivityinput form 3

    Position vary input form on the left ofyour screen and delete defined variable

    4Open input form of centrifuge S502 and position theform right on the screen

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    Set up a Sensitivity Analysis

    5

    drag & drop

    Drag and drop thedrum rotary speedto the manipulatedvariable section

    6

    Vary drum rotaryspeed from 300 to

    1200 rpm (5 points)

    Remark: No need to make furtherchanges to the sensitivity case, sincemeasured variables etc. have beendefined already earlier

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    Sensitivity Case - Results

    Run Model &Review results

    Increased rotary speedof the decanter leadsto reduced utility costsfor the heaters and theblower (equipment

    model predicts a non-linear relationship)

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    Dryer/Centrifuge Optimization Results

    Centrifuge Rotation Residual Moisture Gas to Dryer Blower Power

    Gas Heater Duty Condenser Duty Operating Cost

    An increase of the centrifuge rotary speed from 300 rpm to 1200 rpm would: Decrease the solids outlet moisture by ~56% Decrease the drying agent flow by ~27% Decrease the process utility costs by ~215

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    Summary

    Use conceptual models togain an understanding ofwhich unit operations havethe largest impact on theenergy demand and utility

    costs of a larger process Convert those units from

    conceptual to equipmentmodels to further investigatehow design or operating

    conditions affect energydemands.

    Demo Focus: BPA Purification Section


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