Contamination Fundamentals
Types of Contamination
SOLIDS
LIQUIDS
GASES
Particle Size Diameter Comparison
Human Hair = 80 micron
1 µm = 0.001 mm = 0.000039”
Particle 5 micron
Particle 15 micron
The human eye can only see particles sized down to 40 microns.
ISO 4406: 1999 (E) - ISO Contamination Code
Number of Particles per 100 ml
Scale Number
More Than Up To and Including
28 130,000,000 250,000,000
27 64,000,000 130,000,000
26 32,000,000 64,000,000
25 16,000,000 32,000,000
24 8,000,000 16,000,000
23 4,000,000 8,000,000
22 2,000,000 4,000,000
21 1,000,000 2,000,000
20 500,000 1,000,000
19 250,000 500,000
18 130,000 250,000
17 64,000 130,000
16 32,000 64,000
15 16,000 32,000
Structure of ISO-Code max. amount of dirt particles ISO Code: 22/18/13 in 100 ml > given size
Chart cont…
Scale Number
More Than Up To and Including
14 8,000 16,000
13 4,000 8,000
12 2,000 4,000
11 1,000 2,000
10 500 1,000
9 250 500
8 130 250
7 64 130
6 32 64
5 16 32
4 8 16
3 4 8
2 2 4
1 1 2
0 0.5 1
Structure of ISO-Code: amount of dirt particles in a 100 ml sample larger than these specified sizes: 4µmc / 6µmc / 14µmc
Example: larger than 4µmc = 2,234,000 larger than 6µmc = 195,000 larger than 14µmc = 4,250
ISO Code = / /
22
22
18
18
13
13
How do we measure fluid contamination?
4µmc / 6µmc / 14µmc
Structure of ISO-Code: amount of dirt particles in a 100 ml sample larger than these specified sizes: 4µmc / 6µmc / 14µmc
Example: larger than 4µmc = 2,234,000
ISO Code = / /
22
22
How do we measure fluid contamination?
Structure of ISO-Code: amount of dirt particles in a 100 ml sample larger than these specified sizes: 4µmc / 6µmc / 14µmc
Example: larger than 4µmc = 2,234,000 larger than 6µmc = 195,000
ISO Code = / /
22
22
18
18
How do we measure fluid contamination?
Structure of ISO-Code: amount of dirt particles in a 100 ml sample larger than these specified sizes: 4µmc / 6µmc / 14µmc
Example: larger than 4µmc = 2,234,000 larger than 6µmc = 195,000 larger than 14µmc = 4,250
ISO Code = / /
22
22
18
18
13
13
How do we measure fluid contamination?
max. amount of dirt particles in 100ml at given size
Class 2-5 µm 5-15 µm 15-25 µm >25 µm
00 125 22 4 1
0 250 44 8 2
1 500 89 16 3
2 1000 178 32 6
3 2000 356 63 11
4 4000 712 126 22
5 8000 1425 253 45
6 16000 2850 506 90
7 32000 5700 1012 180
8 64000 11400 2025 360
9 128000 22800 4050 720
10 256000 45600 8100 1440
11 51200 91200 16200 2880
12 1024000 182400 32400 5760
Structure of NAS Codes
How do we measure fluid contamination?
Cumulative Particles per 100 ml Differential Particles per 100 ml Code Designation
Code Designation
> 1 um > 5 um > 15 um 5 to 15 um 15 to 25 um 25 to 50 um 50 to 100 um > 100 um
SAE AS 4059
Equivalent ISO 4406
Class
> 4 um(c) >6 um(c) >14 um(c)
6 to 14 um(c)
14 to 21 um(c) 21 to 38 um(c) 38 to 70 um(c)
> 70 um(c)
Size Code A
Size Code B
Size Code C
--- --- --- --- ---
195 76 14 --- --- --- --- --- 000 8/7/4
390 152 27 125 22 4 1 0 00 9/8/5
780 304 54 250 44 8 2 0 0 10/9/6
1,560 609 109 500 89 16 3 1 1 11/10/7
3,120 1,217 217 1,000 178 32 6 1 2 12/11/8
6,250 2,432 432 2,000 356 63 11 2 3 13/12/9
12,500 4,864 864 4,000 712 126 22 4 4 14/13/10
25,000 9,731 1,731 8,000 1,425 256 45 8 5 15/14/11
50,000 19,462 3,462 16,000 2,850 506 90 16 6 16/14/12
100,000 38,924 6,924 32,000 5,700 1,012 180 32 7 17/16/13
200,000 77,849 13,849 64,000 11,400 2,025 360 64 8 18/17/14
400,000 155,698 27,698 128,000 22,800 4,050 720 128 9 19/18/15
800,000 311,396 55,396 256,000 45,600 8,100 1,440 256 10 20/19/16
1,600,000 622,792 110,792 512,000 91,200 16,200 2,880 512 11 21/20/17
3,200,000 1,245,584 221,584 1,024,000 182,400 32,400 5,760 1,024 12 22/21/18
Cleanliness Code Conversion: SAE AS 4059 – Equivalent ISO 4406 Class Based on ISO 4406: 1999 and SAE AS 4059 Revised 2005-05: Rev E 8/29/07
SAE AS 4059
servo valve J1: 1 - 4µm J2: 100 - 450µm J3: 20 - 80µm
valve J1: 1 - 25µm
piston pump J1: 5 - 40µm J2: 0.5 - 1µm J3: 20 - 40µm J4: 1 - 25µm vane pump
J1: 0.5 - 5µm J2: 5 - 20µm J3: 30 - 40µm
gear pump J1: 0.5 - 5µm J2: 0.5 - 5µm
Hydraulic Component Clearances Are Critical and therefore require strategic filtration designs to remove the
sized particles that will attack the most critical components of the hydraulic system
Abrasion Wear
5µ 8 µ
Surface fatigue Wear - Bearings 1. Initiation particle
trapped and crushed 2. Surface dented – fault Created – crack initiated
3. After “X” fatigue cycles further micro cracks
propagate.
4. Surface fails, spall created & Particles release and enter flow
Sources of Contamination
New Oil - Photomicrographs
ISO 16/14/11 Demanded by Modern Hydraulic Systems
ISO 17/15/13 New Oil as Delivered in Mini-container
ISO 20/18/15 New Oil as Delivered in Tanker
ISO 23/21/18 New Oil as Delivered in Barrels
1 class => 21=2X
4 classes => 24=16X 7 classes => 27=128X
CAN EFFECTS OF CONTAMINATION BE STOPPED? Effects of Contamination
Air
Gaseous
Water
Liquid
Laminated FabricFibers
Seal AbrasionRubber Hose Particles
Iron, SteelBrass, Bronze
Aluminum
EmeryMetal Scale
Rust Particles
Solid
Type of Contamination
Basics of Fluid Contamination
MinimalDamage
Damaging
ExtremelyDamaging
Effects
Chemicals Gases
Basic principle light obscuration
Light source is an LED light • Durability • Holds calibration for 2 years • Does not saturate when
reading high contamination levels
How do we measure fluid contamination?
The number of pulses equals the number of particles.
Size of Particles
Number of Particles = Number of Pulses
4 micron
6 micron
14 micron
How do we measure fluid contamination?
Classification of oil / water mixtures
H H O
Dissolved Water: Homogenous mixture of oil and water. The water molecules are discrete and thoroughly mixed with the oil molecules. Free Water Bulk Water: Above the saturation point, water molecules are aggregated into separate drops (clumps of water). The mixture is no longer homogenous. Emulsified Water: Is a special form of free water. Tiny droplets (1-10 micron size) of water stay suspended in oil and form a hazy or cloudy mixture in the oil.
Contamination Issues caused by available water: FREE WATER ISSUES: • Corrosion caused by free water contamination – corrosion pits, rough surfaces, and release of abrasive flakes into the fluid – rust and aluminum oxide. • Microbial colonization caused by free water – odors, acids, slime, and health problems. • Loss of lubricity caused by free water entering contact loading zones, allowing opposing surfaces to crash together – results in high friction, wear and seizure. • Additive depletion caused by free water retaining polar additives DISSOLVED WATER ISSUES: • Faster oil oxidation caused by dissolved water accelerating this form of oil degradation – leads to oil acidity, thickening, varnishes, sludge & resins • Reduced Fatigue life caused by dissolved water promoting propagation of fatigue cracks in metals • Demolition of Ester-based fluids and additives caused by dissolved water reacting with esters – hydrolysis - results in formation of acids, gels, and loss of additives
Taking a sample from pressure header
Taking a sample from stagnant fluid
SYRINGE VACUUM BOTTLE
RESERVOIRS
THROTTLE VALVE
Sources of Error Possible Sample Locations
PRESSURE HEADER
Definitions:
Saturation Point: • max. amount of water that can be dissolved in the
fluid at a specific temperature • measured in ppm – max level is fluid dependent
Saturation Level: • the percentage of water dissolved in the fluid
relative to the saturation point • measured in % - max level should be less than or
equal to 50%.
Example: Reservoir Extraction with auxiliary pump
suction hose near surface
suction hose near bottom
Example: Reservoir Extraction with Auxiliary Pump
Point at which suction hose was lowered slowly to the bottom of the tank.
ISO CLASS INCREASE FROM 15 TO 20 IS EQUIVALENT TO AN INCREASE IN PARTICLE COUNT OF 32 TIMES!
Sources of Error-Reservoir sampling
Sources of Error Point of Extraction - Test Connection Arrangement
Point of Extraction - Where in the System is the best representation of system fluid cleanliness?
TEST POINT SHOULD BE LOCATED IMMEDIATELY DOWN STREAM OF
HYDRAULIC OR LUBE PUMP, BEFORE FILTRATION, BEFORE
CONTROL AND BEFORE ACTUATION.
HPU
IDEAL SAMPLE POINT-GEAR LUBE SYSTEM
IDEAL SAMPLE POINT LOCATION
• Leaving sample bottles open too long
• Using previously contaminated bottles
• Being unaware of system operation immediately before sampling – possibly resulting in inaccurate analysis and conclusions from sample report data.
• Improper handling of sample causing contamination from hands, atmosphere, chemicals and water.
• Failure to flush sampling ports and lines before sampling results in readings that include built up deposits of dirt and sludge in lines.
Note: Such errors are likely to result in higher contamination readings than actual.
Sources of Error Sampling Errors caused by:
Element Technology
Hydraulic Power Unit Cylinder actuator
Control Valve
Pressure filter
Main Hydraulic Pump
Reservior
Single Pressure filtration strategy
• COST OF FACILITY PREP • COST OF DESIGN AND ACQUISITION • COST OF MACHINE • COST OF UTILITIES • COST OF INSTALLATION & STARTUP • COST OF RUNNING MACHINE • COST OF MAINTAINANCE • COST OF DECOMMISSIONING • COST OF REMOVAL/DISPOSAL
$$$$
Cost of single standard filtration
Strategy
Loss of component efficiency due to wear
(non-efficient operation)- System performance degradation
System downtime costs resulting from component failures-
Can not produce product
Decrease in product quality resulting
from poor control and operation – higher
rejection rates
Equipment & component repair and
Replacement – labor & component costs
Contamination Control
Pressure filter
Reservoir
Return filter
Kidney loop filter
Main Hydraulic Pump
SERVO
Cylinder actuator
Hydraulic Power Unit Comprehensive and/or Balanced Filtration Strategy
Cost of a comprehensive balanced filtration system
System downtime Costs resulting from Component failures
Decrease in product Quality resulting from
Poor control and operation
Equipment & component repair and
replacement
Small investment for comprehensive filtration results in shrinking entire maintenance, quality, and manufacturing budget.
Loss of component Efficiency due to wear
(non-efficient operation)
Hydraulic Power Unit Investment:
5X 4X 3X 2X Life Ext. Factor
14/12/8 14/12/9 15/13/10 16/14/11 19/17/14
14/12/9 15/13/10 16/14/11 17/15/12 20/18/15
15/13/10 16/14/11 17/15/12 18/16/13 21/19/16
16/14/11 17/15/12 18/16/13 19/17/14 22/20/17
17/15/12 18/16/13 19/17/14 20/18/15 23/21/18
18/16/13 19/17/14 20/18/15 21/19/16 24/22/19
Target Target Target Target Current
Cleanliness
Required New Machine Cleanliness Fluid Cleanliness vs. Service Life
Cleanup 5 ISO Codes (32 times cleaner) yields a life extension factor of 4 times
5 ISO CLASS IMPROVEMENT
Machinery Life Extension Factor
Curre
nt M
achi
ne C
leanl
ines
s (IS
O Co
de)
Hydraulics and Diesel Engines
Rolling Element Bearing
Journal Bearing and Turbo Machinery
Gear Boxes and Other
Ref. Noria Corporation
Features of a High Quality Element
BETAMICRON 4 Features optimization of all element performance characteristics
• High ßx-values (efficiency)
• High ßx-value stability
• High dirt holding capacity
• Low long term pressure drop
• High collapse stability
• High flow fatigue stability
• Wide fluid compatibility
• Structrual pleat support with resilience and
memory
BETAMICRON 4 ABSOLUTE NON-WOVEN SYNTHETIC
Nickel or (Tin) Coated End Caps and Support Tubes
- Nickel (Tin) Coating Allows the Use of One Standard Element for ALL Application Needs.
High BETA Efficiency
High BETA Stability in severe dynamic fluid conditions over element life
High Dirt holding capacity
High degree of pleat stability & support due to high quality structrual design
What Data is Obtained? Best performance comparison regarding
below parameters • Beta Ratios • Beta Stability • Dirt Holding Capacity How is test completed? • ISO Medium Test Dust (ISO MTD) • Mil-5606 Hydraulic Fluid • Constant Viscosity • Constant Temperature at 40 degrees Centigrade • Constant Flow rate through filter • Constant rate of dirt injection • Continuous measurement of particle counts upstream vs. down stream. • Continuous measurement of pressures upstream & down.
Multi-Pass Testing ISO 16889: 1999
The Test Lab Real Life
• Steady Flow • No Fatigue Cycles • Constant Dirt • “Ingression Rate” to Filter • Single Fluid Used • Temperature 100°F • ISO Medium Test Dust • Accelerated Element Life
• Continuous Variations • Millions of Fatigue Cycles • Always Changing • Wide Variety • -40°F to 210°F • Debris, Water, Air • Months
What is Dynamic Filter Performance? Filters that Perform in REAL LIFE!
Multi-Pass Testing ISO 16889: 1999 (ISO Standard for Performing Multi-Pass Test)
FOR EVERY 1000 PARTICLES SIZED 5 micron OR GREATER THAT ENTER THE FILTER, ONE GOES THROUGH WHEN THE BETA 5 IS = 1000
Beta Values Versus Efficiency Beta Value Efficiency Particles ≥ Beta() Micron Upstream Particles Downstream
Beta X 2 50.0000% 100,000 50,000
Beta X 4 75.0000% 100,000 25,000
Beta X 10 90.0000% 100,000 10,000
Beta X 20 95.0000% 100,000 5,000
Beta X 40 97.5000% 100,000 2,500
Beta X 60 98.3333% 100,000 1,667
Beta X 75 98.6667% 100,000 1,333
Beta X 100 99.0000% 100,000 1,000
Beta X 125 99.2000% 100,000 800
Beta X 150 99.3333% 100,000 667
Beta X 200 99.5000% 100,000 500
Beta X 300 99.6667% 100,000 333
Beta X 500 99.8000% 100,000 200
Beta X 1,000 99.9000% 100,000 100
Beta X 2,000 99.9500% 100,000 50
Beta X 4,000 99.9750% 100,000 25
Beta X 5,000 99.9800% 100,000 20
Beta X 10,000 99.9900% 100,000 10
Beta X 20,000 99.9950% 100,000 5
Beta X 50,000 99.9980% 100,000 2
Beta Values Versus Efficiency Beta Value Efficiency Particles ≥ Beta() Micron Upstream Particles Downstream
Beta X 2 50.0000% 100,000 50,000
Beta X 4 75.0000% 100,000 25,000
Beta X 10 90.0000% 100,000 10,000
Beta X 20 95.0000% 100,000 5,000
Beta X 40 97.5000% 100,000 2,500
Beta X 60 98.3333% 100,000 1,667
Beta X 75 98.6667% 100,000 1,333
Beta X 100 99.0000% 100,000 1,000
Beta X 125 99.2000% 100,000 800
Beta X 150 99.3333% 100,000 667
Beta X 200 99.5000% 100,000 500
Beta X 300 99.6667% 100,000 333
Beta X 500 99.8000% 100,000 200
Beta X 1,000 99.9000% 100,000 100
Beta X 2,000 99.9500% 100,000 50
Beta X 4,000 99.9750% 100,000 25
Beta X 5,000 99.9800% 100,000 20
Beta X 10,000 99.9900% 100,000 10
Beta X 20,000 99.9950% 100,000 5
Beta X 50,000 99.9980% 100,000 2
Beta Ratio remains at a relatively constant level at high pressure drops beyond normal element operating ranges with high beta stability.
Beta 100 Stability = 210 psi means that: Beta Ratio at the rated micron will not drop below Beta Ratio = 100 until 210 PSID
Beta Stability ISO 16889: 1999
Point of element failure
High ßx-Values / High ßx-Value Stability
Element 1
Element 2
10000
1000
100
Poor Beta Stability Causes a loss of adequate protection from the point that Beta drops below manufacturer’s published beta specification
before the end of element life.
• Significant loss of filter efficiency before the end of element life
• Loss of equipment through loss of protection • Increased wear and component failures • Increased downtime • Decrease in Customer Satisfaction
• Decrease in downtime when indicator is utilized for change-out indication (Less Element Changes)
• Decrease in replacement element costs
(longer lasting-utilizing full element capacity) • Decrease in maintenance/labor costs
High Dirt Holding Capacity ISO 16889: 1999
DHC - Dirt Holding Capacity DHC Measured at Terminal Pressure / Indicator Setting
72
INDICATOR TRIP POINT Element Terminal Pressure
Superior Element Life Pressure Drop Over Element Life Comparison
High efficiency element has higher D/P than a low efficiency element HYDAC designs elements to increase D/P at a slower rate than others