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Continuous On-line Concentration and Density Measurement via … · 2020. 7. 22. · 4 µ - ICC...

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Continuous On-line Concentration and Density Measurement via Microwave Technology pro | M | tec Theisen GmbH Pforzheimer Str. 162 D-76275 Ettlingen + 49 7243 5306 - 0 + 49 7243 5306 - 11 [email protected]
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Page 1: Continuous On-line Concentration and Density Measurement via … · 2020. 7. 22. · 4 µ - ICC 2.45 pro /M /tectec LOCK wz2 Kristallisation A1 % Trockensubstanzgehalt-23.9 dB 223.3

Continuous On-line

Concentration and Density Measurement

via Microwave Technology

pro | M | tec Theisen GmbHPforzheimer Str. 162

D-76275 Ettlingen

+ 49 7243 5306 - 0

+ 49 7243 5306 - 11

[email protected]

Page 2: Continuous On-line Concentration and Density Measurement via … · 2020. 7. 22. · 4 µ - ICC 2.45 pro /M /tectec LOCK wz2 Kristallisation A1 % Trockensubstanzgehalt-23.9 dB 223.3

… before we show the technology:

Some words about pro/M/tec:

Page 3: Continuous On-line Concentration and Density Measurement via … · 2020. 7. 22. · 4 µ - ICC 2.45 pro /M /tectec LOCK wz2 Kristallisation A1 % Trockensubstanzgehalt-23.9 dB 223.3

pro/M/tec is located in the South-West of Germany, in the Black Forest.

Page 4: Continuous On-line Concentration and Density Measurement via … · 2020. 7. 22. · 4 µ - ICC 2.45 pro /M /tectec LOCK wz2 Kristallisation A1 % Trockensubstanzgehalt-23.9 dB 223.3

Company was formed in 1996 and intro-duced the microwave technology to control the sugar crystallisation.

International business. By 2005 over 1.500 instruments have been placed all over the world. You find pro/M/tec-installtions in all continents.

Market activity only for industrial process control:originally for the SUGAR INDUSTRY.

Focussing to microwave measurement technology for the online determination of density and concentration in liquids:

Inline Concentration Control µ-ICC 2.45

Page 5: Continuous On-line Concentration and Density Measurement via … · 2020. 7. 22. · 4 µ - ICC 2.45 pro /M /tectec LOCK wz2 Kristallisation A1 % Trockensubstanzgehalt-23.9 dB 223.3

Microwave signalbefore transmission

Microwave signal afterradiated through

PHASE SHIFT

Radiated micro-waves suffer a

phase shift

ATTENUATIONWhile radiating

through themedium themirowavessuffer an

attenuation

… basic principles of the microwave technology

Page 6: Continuous On-line Concentration and Density Measurement via … · 2020. 7. 22. · 4 µ - ICC 2.45 pro /M /tectec LOCK wz2 Kristallisation A1 % Trockensubstanzgehalt-23.9 dB 223.3

… basic principles of the microwave technology

Page 7: Continuous On-line Concentration and Density Measurement via … · 2020. 7. 22. · 4 µ - ICC 2.45 pro /M /tectec LOCK wz2 Kristallisation A1 % Trockensubstanzgehalt-23.9 dB 223.3

… typical installation for pan application:

sealing

insertion length 148

insulating

14

M 1

2

Ø 1

30

Ø 1

00

pan wall

45

microvawemeasuring field

MICROWAVE

pro/M/tec

CONCENTRATION/-DENSITY - SENSOR

LAB

µ-ICC 2.45

RUN

PLL OPERATINGTR

MODEL NO. µ-ICC 2.45 MODULE

MADE IN GERMANY

DATA - LINEDC - POWER

ext.

TEM

P.

PT

100

/ 0

externalO

PTION

pro/M/tec THEISEN GmbH Pforzheimer Str. 162 D - 76275 Ettlingen www. pro-m-tec.de

SERIAL NO.

ON

RUN

CONTRAST

F2

F3

F4

µ - IC C 2 .45

pro Mtec//pro Mtec//LOCK

wz2 Kristallisation A1

%Trocke nsubs ta nzgeh alt

-23.9 dB 223.3 °

17.25:5906.09.00Sensor 1

Fehlerstatus : 10 90

5.5 86verfügbarer Messbereich %

Skala %

- +

F1

70.9 °C D : Temp. Prod. : P :

Mikrowellen-KonzentrationsmessungMicrowave-Concentration-Measurement

ISOLATED OUTPUTS4x 0/4 - 20 mA

MODEM DATA - LINERS 232/485 µW-SENSOR

AC: 90-270V ~ 45-68 Hz 70WDC: 18-36V 2A

pro/M/tec THEISEN GmbH Pforzheimer Str. 162 D - 76275 Ettlingen www. pro-m-tec.deMADE IN GERMANY

MODEL NO. µ-ICC 2.45

SERIAL NO.

AC 90-270V~or DC 18-36V

output0/4 - 20 mA

max

. 150

m

50 ΩBNC-plug

coaxial cable RG 58

mic

row

ave-

mod

ule

evaluation unit

Ø 1

60

Page 8: Continuous On-line Concentration and Density Measurement via … · 2020. 7. 22. · 4 µ - ICC 2.45 pro /M /tectec LOCK wz2 Kristallisation A1 % Trockensubstanzgehalt-23.9 dB 223.3

… basic principles of the microwave technology

MICROWAVE PHASE SHIFT AND ATTENUATIONCORRELATES WITH THE WATER CONTENT OFTHE MEDIUM.

WATER CONTENT CORRELATES WITH THE DRYMATTER CONTENT.

THE BEST AND SENSITIVE SIGNAL IS THEPHASE SHIFT.

MICROWAVE PHASE SHIFT MEASURES THECONCENTRATION, DENSITY, DRY MATTER ORWATER CONTENT OF THE MEDIUM.

Page 9: Continuous On-line Concentration and Density Measurement via … · 2020. 7. 22. · 4 µ - ICC 2.45 pro /M /tectec LOCK wz2 Kristallisation A1 % Trockensubstanzgehalt-23.9 dB 223.3

1. MICROWAVE SENSOR

4. MEMORY CHIP

2. MICROWAVE MODULE

Max 3 m

3. EVALUATION UNIT

Max 150 m

… typical components that make up a system:

or

Page 10: Continuous On-line Concentration and Density Measurement via … · 2020. 7. 22. · 4 µ - ICC 2.45 pro /M /tectec LOCK wz2 Kristallisation A1 % Trockensubstanzgehalt-23.9 dB 223.3

Microwave evaluation unit µ-ICC 2.45and the compact microwave module

Page 11: Continuous On-line Concentration and Density Measurement via … · 2020. 7. 22. · 4 µ - ICC 2.45 pro /M /tectec LOCK wz2 Kristallisation A1 % Trockensubstanzgehalt-23.9 dB 223.3

Microwave evaluation unit µ-ICC 2.45and the microwave sensor for pans

Page 12: Continuous On-line Concentration and Density Measurement via … · 2020. 7. 22. · 4 µ - ICC 2.45 pro /M /tectec LOCK wz2 Kristallisation A1 % Trockensubstanzgehalt-23.9 dB 223.3

Microwave measurementsystem µ-ICC 2.45 forpipeline

MODULAR EXTENSION

FOR UP TO 4 UNITS ON

ONLY ONE CONTROLLER.

Page 13: Continuous On-line Concentration and Density Measurement via … · 2020. 7. 22. · 4 µ - ICC 2.45 pro /M /tectec LOCK wz2 Kristallisation A1 % Trockensubstanzgehalt-23.9 dB 223.3

Multiple installation of µ-ICC 2.45 controllers

Page 14: Continuous On-line Concentration and Density Measurement via … · 2020. 7. 22. · 4 µ - ICC 2.45 pro /M /tectec LOCK wz2 Kristallisation A1 % Trockensubstanzgehalt-23.9 dB 223.3

Process Value

Details des Microwavesignal: Phase, Attenuation and Producttemperature, and Range

Softkeys

Date, Time, Measurementpoint Description

… all relevant, important measurement informationin the main displaypage

Page 15: Continuous On-line Concentration and Density Measurement via … · 2020. 7. 22. · 4 µ - ICC 2.45 pro /M /tectec LOCK wz2 Kristallisation A1 % Trockensubstanzgehalt-23.9 dB 223.3

Sensors- typical installation

Rod SensorsDirect mounting in a boiler

Inline-SectionDN40-DN150

Insertion SensorsInstallation below a pan

Flat Sensors in a pipe

Page 16: Continuous On-line Concentration and Density Measurement via … · 2020. 7. 22. · 4 µ - ICC 2.45 pro /M /tectec LOCK wz2 Kristallisation A1 % Trockensubstanzgehalt-23.9 dB 223.3

… advantages of the microwave technology:

THE MEASUREMENT IS INSTALLED INLINETO THE PROCESS. NO BYPASS.

MICROWAVE TRANSMISSION OF REPRESENTATIVECROSS-SECTION WILL MEASURE THE PRODUCTSTREAM CORRECTLY. IT MEASURES WHAT COUNTS.

MICROWAVE MEASUREMENT DOES NOT REQUIREOPTICAL TRANSPARENCY OF THE PRODUCT.THEREFORE IT IS ALMOST INDEPENDENT OFCONTAMINATION AND DEPOSITS ON THE SENSOR.

Page 17: Continuous On-line Concentration and Density Measurement via … · 2020. 7. 22. · 4 µ - ICC 2.45 pro /M /tectec LOCK wz2 Kristallisation A1 % Trockensubstanzgehalt-23.9 dB 223.3

Where do we use it in the sugar factory ?

Page 18: Continuous On-line Concentration and Density Measurement via … · 2020. 7. 22. · 4 µ - ICC 2.45 pro /M /tectec LOCK wz2 Kristallisation A1 % Trockensubstanzgehalt-23.9 dB 223.3

Inline Concentration Control µ-ICC 2.45Applications in the sugar industry:

• Crystallization pan control:all typs of the crystallization processfor product and seed magma pans in discontinuous (batch) and continuous technologyinstalled vertical, horizontal or in a cascade.Also use for cooling crystallization.

Page 19: Continuous On-line Concentration and Density Measurement via … · 2020. 7. 22. · 4 µ - ICC 2.45 pro /M /tectec LOCK wz2 Kristallisation A1 % Trockensubstanzgehalt-23.9 dB 223.3

Inline Concentration Control µ-ICC 2.45Applications in the sugar industry:

• Evaporator and concentrator control:thinjuice and thickjuice control to optimizeevaporator work in each step.Thickjuice conditioning to stabilize standardliquor dry substance content.Thinjuice control to compensate thickjuiceirregularities what my cause instabilities in thecrystallization.Thickjuice, syrup and feed syrup control to in-crease dry substance content in order to minimizethe amount of water introduced to the sugar houseto save energy consumption.

Page 20: Continuous On-line Concentration and Density Measurement via … · 2020. 7. 22. · 4 µ - ICC 2.45 pro /M /tectec LOCK wz2 Kristallisation A1 % Trockensubstanzgehalt-23.9 dB 223.3

Inline Concentration Control µ-ICC 2.45Applications in the sugar industry:

• Any installation on pans, tanks, vessels, mixersor pipelines to control any liquid, massecuite,syrup and crystal suspensionfor the inline process control.

Page 21: Continuous On-line Concentration and Density Measurement via … · 2020. 7. 22. · 4 µ - ICC 2.45 pro /M /tectec LOCK wz2 Kristallisation A1 % Trockensubstanzgehalt-23.9 dB 223.3

80

82

84

86

88

90

92

94

96

0 20 40 60 80 100 120 140 160 180 200

Sample

wD

S (%

)

0

10

20

30

40

50

60

70

80

90

100

Leve

l (%

)white sugar crystallization

Lab

µ-wave

level

… main application: batch crystallizers

Page 22: Continuous On-line Concentration and Density Measurement via … · 2020. 7. 22. · 4 µ - ICC 2.45 pro /M /tectec LOCK wz2 Kristallisation A1 % Trockensubstanzgehalt-23.9 dB 223.3

BEST INSTALLATION POINT IS ALWAYS BELOW CALANDRIA

IN CYLINDER PART

OR CONE AREA.

Best results will be expected for pans with stirrer.

… typical installation in batch pans:

Page 23: Continuous On-line Concentration and Density Measurement via … · 2020. 7. 22. · 4 µ - ICC 2.45 pro /M /tectec LOCK wz2 Kristallisation A1 % Trockensubstanzgehalt-23.9 dB 223.3

Thick juice pipeline

69,0

69,5

70,0

70,5

71,0

71,5

1 2 3 4 5 6 7 8 9 10 11 12 13 14 15

Samples

wD

S (%

)

laboratoryµ-waverefractometer

… inline application for thick juice control

Page 24: Continuous On-line Concentration and Density Measurement via … · 2020. 7. 22. · 4 µ - ICC 2.45 pro /M /tectec LOCK wz2 Kristallisation A1 % Trockensubstanzgehalt-23.9 dB 223.3

y = x - 0,0006R2 = 0,994

69

70

71

72

73

74

75

76

77

78

79

69 71 73 75 77 79

Lab

µ-w

ave

standard deviation ± 0,2 Bx

Thick juice pipeline DN 150

… inline application for thick juice control

Page 25: Continuous On-line Concentration and Density Measurement via … · 2020. 7. 22. · 4 µ - ICC 2.45 pro /M /tectec LOCK wz2 Kristallisation A1 % Trockensubstanzgehalt-23.9 dB 223.3

… inline application for thick juice control

Page 26: Continuous On-line Concentration and Density Measurement via … · 2020. 7. 22. · 4 µ - ICC 2.45 pro /M /tectec LOCK wz2 Kristallisation A1 % Trockensubstanzgehalt-23.9 dB 223.3

Conti pan

80

82

84

86

88

90

92

94

96

98

100

0 20 40 60 80 100 120 140 160 180 200

time (min)

w D

s (%

)

chamber 4chamber 2

… application for continuous pan boiling

Page 27: Continuous On-line Concentration and Density Measurement via … · 2020. 7. 22. · 4 µ - ICC 2.45 pro /M /tectec LOCK wz2 Kristallisation A1 % Trockensubstanzgehalt-23.9 dB 223.3

… installation directly into mixer wall

Page 28: Continuous On-line Concentration and Density Measurement via … · 2020. 7. 22. · 4 µ - ICC 2.45 pro /M /tectec LOCK wz2 Kristallisation A1 % Trockensubstanzgehalt-23.9 dB 223.3

Application Span

• Concentration and Density of almost all Mixtures, Suspensions, Solutions, Emulsions, Dispersions, Slurries IN WATER

• Boiling • Mixing• Concentrating / Diluting• Evaporating• Quality Control

Page 29: Continuous On-line Concentration and Density Measurement via … · 2020. 7. 22. · 4 µ - ICC 2.45 pro /M /tectec LOCK wz2 Kristallisation A1 % Trockensubstanzgehalt-23.9 dB 223.3

Danke / Thank you !


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