Al Shaheen Crude Oil 2018

Crude Assay Report

on

Crude sample marked

Date:

Company details :

For the Attention of :

Sample(s) received from : Qatar

Sample(s) submitted as : Al Shaheen Crude Oil 2018

Description(s) on Label(s) : Al Shaheen Crude Oil 2018

Seals on Sample(s) : Nil

Sample(s) received on :

Logistics Base within Gulf Warehousing Company

Al Ghuwairiya Street

Street No. 512

West Side Support Service Area

Outside RLIC Khalifa Gate (Gate no. 2)

Ras Laffan - Qatar

AUTHORIZED SIGNATURE

George Idicula Laboratory Manager,O&P Laboratory

Bureau Veritas

Technopark – Plot 010407

Jebel Ali, Dubai, U.A.E

Please refer attached sheets for analysis report.

LABORATORY REPORT NO. IDL 5579/2018

December 21, 2018

The above sample(s) was/were examined and the following results obtained:

NORTH OIL COMPANY

21 November, 2018

Sl.No. Page No.

1 Front Cover 1

2 Title 2

3 Index 3

4 Main Assay Properties 4

5 True Boiling Point Distillation Data 5

6 True Boiling Point Distillation data - Graph 6

7 Summary of Product / Residue cut points & Yield 7

8 Summary of True Boiling Point Distillation Cuts - Graph 8

9 Whole Crude Analysis 9

10 Naphtha Cuts - Light Naphtha [IBP/C5/15-70°C] 10

11 Naphtha Cuts - Light Reformer Naphtha [70-165°C] 11

12 Naphtha Cuts - Reformer & Heavy Naphtha [165-195°C] 12

13 Kerosene Cut - Kerosene [195-235°C] 13

14 Vacuum Gas Oil Cuts - Light Gas Oil [235-325°C] 14

15 Vacuum Gas Oil Cuts - Gas Oil [325-370°C] 15

16 Vacuum Gas Oil Cuts - Gas Oil 1[370 - 540°C] 16

17 Vacuum Gas Oil Cuts - Heavy Vacuum Gas Oil [370 - 548°C] 17

18 Residue Cuts - Atmospheric Residue [+370°C] 18

19 Residue Cuts -  Vacuum Residue [+548°C] 19

INDEX

Description

LABORATORY REPORT NO. IDL 5579/2018

Al Shaheen Crude Oil 2018

Page No: 3

Al Shaheen Crude Oil 2018

LABORATORY REPORT NO. IDL 5579/2018

Kerosene Cut

Lig

ht

Na

ph

tha

Lig

ht

Re

form

e

r

Na

ph

tha

Re

form

e

r &

He

av

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Na

ph

tha

Ke

rose

n

e

Lig

ht

Ga

s O

il

Ga

s O

il

Ga

s O

il 1

He

av

y

Va

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um

Ga

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il

Atm

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Re

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 Va

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ue

CUTS, YIELDS AND DISTILLATIONS 1 2 3 4 5 6 7 8 9 10

Initial BP °C IBP /C5/15 70 165 195 235 325 370 370 370 + 548 +

Final BP °C 70 165 195 235 325 370 540 548

Yield % Wt.ASTM D5236/

ASTM D28923.27 9.58 5.10 5.52 17.65 7.51 22.71 24.79 49.50 24.65

Yield % Vol.ASTM D5236/

ASTM D28924.43 11.35 5.63 5.92 18.14 7.41 21.57 23.55 44.77 21.23

Density @ 15°C kg/LASTM D5002 / D4052 /

D25980.6481 0.7415 0.7951 0.8190 0.8546 0.8909 0.9229 0.9251 0.9713 1.0199

Specific Gravity @ 60/60° F Conversion 0.8790 0.6482 0.7417 0.7954 0.8194 0.8551 0.8914 0.9234 0.9256 0.9718 1.0206

API Gravity @ 60° F ° API Calculated 29.5 86.8 59.3 46.4 41.2 34.0 27.2 21.7 21.4 14.1 7.2

Sulphur Content % Wt. IP 336 / ASTM D4294 2.31 0.0274 0.0897 0.1930 0.304 1.08 2.25 2.49 2.55 3.70 4.87

Mercaptan Sulphur ppm Wt. UOP 163 322 243 356 380 354 69 52

Hydrogen Sulphide ppm Wt. UOP 163 <1 <1 <1

Total Nitrogen ppm Wt. ASTM D4629 / D5762 900 0.3 0.4 0.6 0.9 36 220 639 680 1823 2800

Basic Nitrogen % Wt UOP 269 0.0225 0.0017 0.0063 0.0179 0.0186 0.0484 0.0728

Vapour Pressure psi ASTM D323 / D5191 6.20 14.67 1.81

PIONA  Analysis

Total Paraffins 93.0 59.0 62.7

n-Paraffins 34.8 8.3 7.5

iso-Paraffins 58.2 50.7 55.2

Total Olefins <0.1 <0.1 0.5

Total Napthenes 6.9 36.4 15.7

Total Aromatics <0.1 4.6 21.1

Unidentified <0.1 <0.1 <0.1

Research Octane Number (Clear) * ASTM D2699 70.0(2*) 55.0

Pour Point ° C IP 15 / ASTM D97 <-18 <-36 <-36 <-36 +6 +30 +33 +24 +39

Cold Filter Plugging Point ° C IP 309 <-51 -44 -16 +8

Cloud Point ° C IP 219 / ASTM D2500 <-42 <-42 -14 +8

Freeze Point ° C IP 16 /ASTM D2386 -81.5 -53.5

Cetane Index calc. IP 380 /ASTM D976 48.0 45.6

UOP K Factor calc. UOP 375 11.6 11.7 11.6 11.4

Kinematic Viscosity @ 15° C 31.88

Kinematic Viscosity @ 25° C 21.00

Kinematic Viscosity @ 35° C 13.31

Kinematic Viscosity @ 40° C 10.88 0.9690 1.517 3.338 8.472 55.97 62.50 1212 266400*

Kinematic Viscosity @ 55° C 7.203

Kinematic Viscosity @ 100° C 2.957 0.5520 0.7310 1.289 2.300 7.068 7.573 46.62 1131

Kinematic Viscosity @ 135° C ASTM D2170 3.575 3.754 15.90 188.1

Smoke Point mm IP 57 / ASTM D1322 26.0 25.0

Copper corrosion test @ 40° C, 3 hours IP 154 /ASTM D 130 2C 2C 3A 1A

Aniline Point ° C IP 2 / ASTM D 611 53.6 59.0 68.2 71.4 83.6 81.0

Hydrocarbon types by FIA

FIA-Aromatic 20.3 23.8

FIA-Olefins 0.7 2.1

FIA-Saturates 79.0 74.1

Organic Chloride mg/kg ASTM D4929B 1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0

Conradson carbon residue % Wt. ASTM D189 4.84 <0.10 <0.10 0.25 0.40 9.30 19.5

Total Acid Number mgKOH/g IP 177 / ASTM D664 0.20 0.24 0.08 0.12 0.18 0.21 0.16 0.19 0.25

Refractive Index @ 70°C ASTM D1218 1.4557 1.4770 1.4945 1.4959

Naphthalene Content %Wt / %Vol ASTM D1840 0.18 1.95

Wax Content % Wt. UOP 46 <5(1.8) <5(1.9) <5(3.5) 19.2 20.1 5.4 2.2

Metals

Nickel 7 <1 <1 15 29

Vanadium 26 <1 <1 49 94

Sodium <1 <1 3 5

Softening Point ASTM D36 NA(1*) 35.2

Penetration @ 25°C ASTM D5 NA(1*) 248.0

Asphaltene % Wt. IP 143 1.7 3.9 7.6

Ash Content % Wt. IP 4 / ASTM D482 0.008 0.013 0.027

Salt Content mg/kg IP 265 / ASTM D3230 15

B.S. & Water % Vol. ASTM D4007 0.025

Water Content % Vol. IP 74 / ASTM D95 <0.05

Flash Point ° C IP170 / ASTM D93 <40.0 <40.0 <40.0 <40.0 80.0 124.0 178.0

Distillation - - - - - - -

IBP ° C 27.7 83.2 161.1 202.8 250.9 311.8

10% Evaporated/Recovered ° C 37.6 99.3 170.5 210.8 264.3 334.3

20% Evaporated/Recovered ° C 39.9 104.7 173.5 212.2 267.2 333.8

30% Evaporated/Recovered ° C 41.9 109.5 175.8 213.3 270.2 334.8

40% Evaporated/Recovered ° C 44.1 115.3 177.6 214.5 274.0 336.4

50% Evaporated/Recovered ° C 46.4 121.1 179.7 216.2 278.3 338.3

60% Evaporated/Recovered ° C 49.1 128.3 181.8 217.2 283.2 340.3

70% Evaporated/Recovered ° C 52.5 135.2 184.2 219.1 289.6 342.6

80% Evaporated/Recovered ° C 57.1 142.4 187.3 221.7 297.1 345.5

90% Evaporated/Recovered ° C 63.1 151.4 191.4 225.2 307.5 349.7

95% Evaporated/Recovered ° C 66.6 157.0 195.2 228.5 315.8 353.4

FBP ° C 73.0 166.1 201.0 232.7 327.9 357.7

Residue % Vol. 0.9 0.7 0.7 1.2 1.0 0.8

Loss % Vol. 0.8 0.5 0.6 1.0 0.8 0.5

Composition (C1-C5) -

Methane % Wt. <0.01

Ethane % Wt. 0.02

Propane % Wt. 0.26

I-butane % Wt. 0.27

n-butane % Wt. 0.85

IP 501

Residue Cuts

TEST

% VolGC (ASTM D6839/

ASTM D6730)

cStIP 71 / D 445

Vacuum Gas Oil Cuts

ASTM D86

IP344 / IP 601

Remark(s): 1. Unable to test due to sample nature. 2. Results is calculated and only as indicative –

precision parameters are not applicable.

UNIT METHOD

Wh

ole

Cru

de Naphtha Cuts

% Vol. IP 156

mg/kg

Page No: 4

Sample Descriptions / Label : Al Shaheen Crude Oil 2018

Sl. No. % Mass % Volume

1 1.38 2.16

2 3.27 4.43

3 9.58 11.35

4 5.10 5.63

5 5.52 5.92

6 17.65 18.14

7 7.51 7.41

9 24.79 23.55

10 24.65 21.23

LPG 1.38

Heavy Vacuum Gas Oil

(370-548C)74.80 78.59

LABORATORY REPORT NO. IDL 5579/2018

Vapour Temperature °C

19.33 23.57

TRUE BOILING POINT DISTILLATION DATA

(ASTM D 2892/D5236)

Cumulative %

Mass

Light Reformer Naphtha

(70-165C)

Cumulative %

Volume

17.94

Reformer & Heavy Naphtha

(165 - 195C)

Vacuum Residue

(548+C)

Light Naphtha

(C5-70C)4.65 6.59

14.23

99.45 99.82

2.16

Kerosene

(195- 235C)

Light Gas Oil

(235 - 325C)

29.49

47.63

55.04Gas Oil

(325-370C)

24.85

42.50

50.01

Page No: 5

Page No: 6

15

70

165

195

235

325

370

548

0

20

40

60

80

100

120

140

160

180

200

220

240

260

280

300

320

340

360

380

400

420

440

460

480

500

520

540

560

0.0 10.0 20.0 30.0 40.0 50.0 60.0 70.0 80.0

Te

mp

era

ture

°C

Recovery %

% Mass

% Volume

TRUE BOILING POINT DISTILLATION CURVE(ASTM D 2892 & ASTM D 5236)

LABORATORY REPORT NO. IDL 5579/2018

AL Shaheen Crude Assay Report 2018

Sample Descriptions / Label:

% mass Volume %

1.38 2.16

3.27 4.43

9.58 11.35

5.10 5.63

5.52 5.92

17.65 18.14

7.51 7.41

49.50 44.70

22.71 21.57

24.79 23.55

24.65 21.23

LABORATORY REPORT NO. IDL 5579/2018

370+ Res

370-548

Al Shaheen Crude Oil 2018

Yield %

Al Shaheen Crude Oil 2018

165-195

Cut Points

(° C)

SUMMARY OF PRODUCT / RESIDUE CUT POINTS AND YIELDS

195-235

370-540

0-15

15-70

70-165

548+ Res

235-325

325-370

Page No: 7

Page N

o: 8

0.0

0

5.0

0

10

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15

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20

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25

.00

30

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35

.00

40

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45

.00

50

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55

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60

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65

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70

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75

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80

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85

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90

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95

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-70

70

-165

16

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95

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35

23

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25

32

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70

37

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37

0-5

40

37

0-5

48

54

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% Yield

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Sample Descriptions / Label :

Specific Gravity @ 60/60° F ASTM D5002 - 0.8790

API Gravity @ 60° F Calculated ° API 29.5

Sulphur Content ASTM D4294 % Wt. 2.31

Mercaptan Sulphur UOP 163 ppm Wt. 322

Hydrogen Sulphide UOP 163 ppm Wt. <1

Total Nitrogen ASTM D5762 ppm Wt. 900

Basic Nitrogen UOP 269 % Wt 0.0225

Vapour Pressure ASTM D323 psi 6.20

Pour Point ASTM D97 ° C <-18

Kinematic Viscosity @ 15° C 31.88

Kinematic Viscosity @ 25° C 21.00

Kinematic Viscosity @ 35° C 13.31

Kinematic Viscosity @ 40° C 10.88

Kinematic Viscosity @ 55° C 7.203

Kinematic Viscosity @ 100° C 2.957

Organic Chloride ASTM D4929B mg/kg 1.0

Conradson carbon residue ASTM D189 % Wt. 4.84

Total Acid Number ASTM D664 mgKOH/g 0.20

Wax Content UOP 46 % Wt. <5(1.8)

Nickel IP 501 mg/kg 7

Vanadium IP 501 mg/kg 26

Asphaltene IP 143 % Wt. 1.7

Ash Content ASTM D482 % Wt. 0.008

Salt Content ASTM D3230 mg/kg 15

B.S. & Water ASTM D4007 % Vol. 0.025

Water Content ASTM D95 % Vol. <0.05

Flash Point ASTM D93 ° C <40.0

Composition (C1-C5) -

Methane <0.01

Ethane 0.02

Propane 0.26

I-butane 0.27

n-butane 0.85

Al Shaheen Crude Oil 2018

LABORATORY REPORT NO. IDL 5579/2018

WHOLE CRUDE PROPERTIES

TESTTEST METHOD UNIT RESULT

ASTM D445 cSt

IP 601 % Wt.

Page No: 9

Sample Descriptions / Label :

Yield ASTM D2892 / D5236 % Wt. 3.27

Yield ASTM D2892 / D5236 % Vol. 4.43

Density @ 15°C ASTM D4052 kg/L 0.6481

Specific Gravity @ 60/60° F Conversion - 0.6482

API Gravity @ 60° F Calculated ° API 86.8

Sulphur Content ASTM D 5453 % Wt. 0.0274

Mercaptan Sulphur UOP 163 ppm Wt. 243

Total Nitrogen ASTM D4629 ppm Wt. 0.3

Vapour Pressure ASTM D5191 psi 14.7

PIONA  Analysis % Vol -

Total Paraffins % Vol 93.0

n-Paraffins % Vol 34.8

iso-Paraffins % Vol 58.2

Total Olefins % Vol <0.1

Total Napthenes % Vol 6.9

Total Aromatics % Vol <0.1

Unidentified % Vol <0.1

Research Octane Number (Clear) * ASTM D2699/ GC Cal 70.0(*)

Organic Chloride ASTM D4929 mg/kg <1.0

Flash Point ASTM D93 ° C <40.0

Distillation - -

IBP ° C 27.7

10% Evaporated/Recovered ° C 37.6

20% Evaporated/Recovered ° C 39.9

30% Evaporated/Recovered ° C 41.9

40% Evaporated/Recovered ° C 44.1

50% Evaporated/Recovered ° C 46.4

60% Evaporated/Recovered ° C 49.1

70% Evaporated/Recovered ° C 52.5

80% Evaporated/Recovered ° C 57.1

90% Evaporated/Recovered ° C 63.1

95% Evaporated/Recovered ° C 66.6

FBP ° C 73.0

Residue % Vol. 0.9

Loss % Vol. 0.8

ASTM D6839

ASTM D86

LABORATORY REPORT NO. IDL 5579/2018

Light Naphtha [IBP/C5 - 70° C]

Al Shaheen Crude Oil 2018

TEST METHOD UNIT RESULT

Page No: 10

Sample Descriptions / Label :

Yield ASTM D2892 / D5236 % Wt. 9.58

Yield ASTM D2892 / D5236 % Vol. 11.35

Density @ 15°C ASTM D4052 kg/L 0.7415

Specific Gravity @ 60/60° F Conversion - 0.7417

API Gravity @ 60° F Calculated ° API 59.3

Sulphur Content ASTM D5453 % Wt. 0.0897

Mercaptan Sulphur UOP 163 ppm Wt. 356

Total Nitrogen ASTM D4629 ppm Wt. 0.4

Vapour Pressure ASTM D5191 psi 1.81

PIONA  Analysis % Vol -

Total Paraffins % Vol 59

n-Paraffins % Vol 8.3

iso-Paraffins % Vol 50.7

Total Olefins % Vol <0.1

Total Napthenes % Vol 36.4

Total Aromatics % Vol 4.6

Unidentified % Vol <0.1

Research Octane Number (Clear) ASTM D2699/ GC Cal - 55

Copper corrosion test @ 40° C, 3 hours ASTM D130 - 2C

Organic Chloride ASTM D4929 mg/kg <1.0

Flash Point ASTM D93 ° C <40.0

Distillation ° C -

IBP ° C 83.2

10% Evaporated/Recovered ° C 99.3

20% Evaporated/Recovered ° C 104.7

30% Evaporated/Recovered ° C 109.5

40% Evaporated/Recovered ° C 115.3

50% Evaporated/Recovered ° C 121.1

60% Evaporated/Recovered ° C 128.3

70% Evaporated/Recovered ° C 135.2

80% Evaporated/Recovered ° C 142.4

90% Evaporated/Recovered ° C 151.4

95% Evaporated/Recovered ° C 157.0

FBP ° C 166.1

Residue % Vol. 0.7

Loss % Vol. 0.5

LABORATORY REPORT NO. IDL 5579/2018

ASTM D6839

ASTM D86

RESULT

Al Shaheen Crude Oil 2018

TEST METHOD UNIT

Light Reformer Naphtha [70 - 165° C]

Page No: 11

Sample Descriptions / Label :

Yield ASTM D2892 / D5236 % Wt. 5.10

Yield ASTM D2892 / D5236 % Vol. 5.63

Density @ 15°C ASTM D4052 kg/L 0.7951

Specific Gravity @ 60/60° F Conversion - 0.7954

API Gravity @ 60° F Calculated ° API 46.4

Sulphur Content ASTM D5453 % Wt. 0.193

Mercaptan Sulphur UOP 163 ppm Wt. 380

Total Nitrogen ASTM D4629 ppm Wt. 0.6

PIONA  Analysis % Vol -

Total Paraffins % Vol 62.7

n-Paraffins % Vol 7.5

iso-Paraffins % Vol 55.2

Total Olefins % Vol 0.5

Total Napthenes % Vol 15.7

Total Aromatics % Vol 21.1

Unidentified % Vol <0.1

Pour Point ASTM D97 ° C <-36

Cold Filter Plugging Point IP 309 ° C <-51

Cloud Point ASTM D2500 ° C <-42

Freeze Point ASTM D2386 ° C -81.5

Kinematic Viscosity @ 40° C ASTM D445 cSt 0.969

Kinematic Viscosity @ 100° C ASTM D445 cSt 0.552

Smoke Point ASTM D1322 mm 26.0

Copper corrosion test @ 40° C, 3 hours ASTM D130 - 2C

Aniline Point ASTM D611 ° C 53.6

Hydrocarbon types by FIA - -

FIA-Aromatic % Vol. 20.3

FIA-Olefins % Vol. 0.7

FIA-Saturates % Vol. 79

Organic Chloride ASTM D4929 mg/kg <1.0

Flash Point ASTM D93 ° C <40.0

Distillation ° C -

IBP ° C 161.1

10% Evaporated/Recovered ° C 170.5

20% Evaporated/Recovered ° C 173.5

30% Evaporated/Recovered ° C 175.8

40% Evaporated/Recovered ° C 177.6

50% Evaporated/Recovered ° C 179.7

60% Evaporated/Recovered ° C 181.8

70% Evaporated/Recovered ° C 184.2

80% Evaporated/Recovered ° C 187.3

90% Evaporated/Recovered ° C 191.4

95% Evaporated/Recovered ° C 195.2

FBP ° C 201

Residue % Vol. 0.7

Loss % Vol. 0.6

LABORATORY REPORT NO. IDL 5579/2018

Reformer & Heavy Naphtha [165 - 195° C]

ASTM D6839

ASTM D86

IP 156

RESULT

Al Shaheen Crude Oil 2018

TEST METHOD UNIT

Page No: 12

Sample Descriptions / Label :

Yield ASTM D 2892 / D5236 % Wt. 5.52

Yield ASTM D 2892 / D5236 % Vol. 5.92

Density @ 15°C ASTM D4052 kg/L 0.8190

Specific Gravity @ 60/60° F Conversion 0.8194

API Gravity @ 60° F Calculated ° API 41.2

Sulphur Content ASTM D 4294 % Wt. 0.304

Mercaptan Sulphur UOP 163 ppm Wt. 354

Total Nitrogen ASTM D4629 ppm Wt. 0.9

Pour Point ASTM D97 ° C <-36

Cold Filter Plugging Point IP 309 ° C -44

Cloud Point ASTM D2500 ° C <-42

Freeze Point ASTM D2386 ° C -53.5

Kinematic Viscosity @ 40° C ASTM D445 cSt 1.517

Kinematic Viscosity @ 100° C ASTM D445 cSt 0.7310

Smoke Point IP 57 / ASTM D1322 mm 25.0

Copper corrosion test @ 40° C, 3 hours ASTM D130 3A

Aniline Point ASTM D611 (Proc. A) ° C 59.0

Hydrocarbon types by FIA - -

FIA-Aromatic % Vol. 23.8

FIA-Olefins % Vol. 2.1

FIA-Saturates % Vol. 74.1

Organic Chloride ASTM D4929B mg/kg <1.0

Total Acid Number ASTM D664 mgKOH/g 0.08

Naphthalene Content ASTM D1840 %Wt / %Vol 1.95

Flash Point ASTM D93 ° C >70.0

Distillation - -

IBP ° C 202.8

10% Evaporated/Recovered ° C 210.8

20% Evaporated/Recovered ° C 212.2

30% Evaporated/Recovered ° C 213.3

40% Evaporated/Recovered ° C 214.5

50% Evaporated/Recovered ° C 216.2

60% Evaporated/Recovered ° C 217.2

70% Evaporated/Recovered ° C 219.1

80% Evaporated/Recovered ° C 221.7

90% Evaporated/Recovered ° C 225.2

95% Evaporated/Recovered ° C 228.5

FBP ° C 232.7

Residue % Vol. 1.2

Loss % Vol. 1.0

LABORATORY REPORT NO. IDL 5579/2018

Kerosene [195 - 235° C]

IP 156

ASTM D86

RESULT

Al Shaheen Crude Oil 2018

TEST METHOD UNIT

Page No: 13

Sample Descriptions / Label :

Yield ASTM D2892 / D5236 % Wt. 17.65

Yield ASTM D2892 / D5236 % Vol. 18.14

Density @ 15°C ASTM D4052 kg/L 0.8546

Specific Gravity @ 60/60° F Conversion 0.8551

API Gravity @ 60° F Calculated ° API 34.0

Sulphur Content ASTM D4294 % Wt. 1.080

Total Nitrogen ASTM D4629 ppm Wt. 36

Basic Nitrogen UOP 269 % Wt 0.0017

Pour Point ASTM D97 ° C <-36

Cold Filter Plugging Point IP 309 ° C -16

Cloud Point ASTM D2500 ° C -14

Cetane Index ASTM D976 calc. 48.0

Kinematic Viscosity @ 40° C ASTM D445 cSt 3.338

Kinematic Viscosity @ 100° C ASTM D445 cSt 1.289

Copper corrosion test @ 40° C, 3 hours ASTM D130 - 1A

Aniline Point ASTM D611 (Proc. A) ° C 68.2

Organic Chloride ASTM D4929 mg/kg <1.0

Conradson carbon residue ASTM D189 % Wt. <0.10

Total Acid Number ASTM D664 mgKOH/g 0.12

Refractive Index @ 70°C ASTM D1218 1.4557

Wax Content UOP 46 % Wt. <5(1.9)

Flash Point ASTM D93 ° C 124.0

Distillation - -

IBP ° C 250.9

10% Evaporated/Recovered ° C 264.3

20% Evaporated/Recovered ° C 267.2

30% Evaporated/Recovered ° C 270.2

40% Evaporated/Recovered ° C 274.0

50% Evaporated/Recovered ° C 278.3

60% Evaporated/Recovered ° C 283.2

70% Evaporated/Recovered ° C 289.6

80% Evaporated/Recovered ° C 297.1

90% Evaporated/Recovered ° C 307.5

95% Evaporated/Recovered ° C 315.8

FBP ° C 327.9

Residue % Vol. 1.0

Loss % Vol. 0.8

LABORATORY REPORT NO. IDL 5579/2018

Light Gas Oil [235 - 325° C]

ASTM D86

RESULT

Al Shaheen Crude Oil 2018

TEST METHOD UNIT

Page No: 14

Sample Descriptions / Label :

Yield ASTM D2892 % Wt. 7.51

Yield ASTM D2892 % Vol. 7.41

Density @ 15°C ASTM D4052 kg/L 0.8909

Specific Gravity @ 60/60° F Conversion 0.8914

API Gravity @ 60° F Calculated ° API 27.2

Sulphur Content ASTM D4294 % Wt. 2.25

Total Nitrogen ASTM D4629 ppm Wt. 220

Basic Nitrogen UOP 269 % Wt 0.0063

Pour Point ASTM D97 ° C +6

Cold Filter Plugging Point IP 309 ° C +8

Cloud Point ASTM D2500 ° C +8

Cetane Index ASTM D976 calc. 45.6

UOP K Factor UOP 375 calc. 11.6

Kinematic Viscosity @ 40° C ASTM D445 cSt 8.472

Kinematic Viscosity @ 100° C ASTM D445 cSt 2.300

Aniline Point ASTM D611 (Proc. A) ° C 71.40

Organic Chloride ASTM D4929 mg/kg <1.0

Conradson carbon residue ASTM D189 % Wt. <0.10

Total Acid Number ASTM D664 mgKOH/g 0.18

Refractive Index @ 70°C ASTM D1218 1.4770

Wax Content UOP 46 % Wt. <5(3.5)

Flash Point ASTM D93 ° C 178.0

Distillation - -

IBP ° C 311.8

10% Evaporated/Recovered ° C 334.3

20% Evaporated/Recovered ° C 333.8

30% Evaporated/Recovered ° C 334.8

40% Evaporated/Recovered ° C 336.4

50% Evaporated/Recovered ° C 338.3

60% Evaporated/Recovered ° C 340.3

70% Evaporated/Recovered ° C 342.6

80% Evaporated/Recovered ° C 345.5

90% Evaporated/Recovered ° C 349.7

95% Evaporated/Recovered ° C 353.4

FBP ° C 357.7

Residue % Vol. 0.8

Loss % Vol. 0.5

LABORATORY REPORT NO. IDL 5579/2018

Gas Oil [325 - 370° C]

RESULT

ASTM D86

Al Shaheen Crude Oil 2018

TEST METHOD UNIT

Page No: 15

Sample Descriptions / Label :

Yield ASTM D2892/ D5236 % Wt. 22.71

Yield ASTM D2892/ D5236 % Vol. 21.57

Density @ 15°C ASTM D4052 kg/L 0.9229

Specific Gravity @ 60/60° F Conversion 0.9234

API Gravity @ 60° F Calculated ° API 21.7

Sulphur Content ASTM D 4294 % Wt. 2.49

Total Nitrogen ASTM D 4629 ppm Wt. 639

Basic Nitrogen UOP 269 % Wt 0.0179

Pour Point ASTM D97 ° C +30

UOP K Factor UOP 375 calc. 11.7

Kinematic Viscosity @ 40° C ASTM D445 cSt 55.97

Kinematic Viscosity @ 100° C ASTM D445 cSt 7.068

Kinematic Viscosity @ 135° C ASTM D2170 cSt 3.575

Aniline Point ASTM D611 (Proc. A) ° C 83.6

Conradson carbon residue ASTM D189 % Wt. 0.25

Total Acid Number ASTM D664 mgKOH/g 0.21

Refractive Index @ 70°C ASTM D1218 1.4945

Wax Content UOP 46 % Wt. 19.2

Metals - -

Nickel mg/kg <1

Vanadium mg/kg <1

Sodium mg/kg <1

LABORATORY REPORT NO. IDL 5579/2018

Vacuum Gas Oil 1 [370 - 540°C]

RESULT

IP 501

Al Shaheen Crude Oil 2018

TEST METHOD UNIT

Page No: 16

Sample Descriptions / Label :

Yield ASTM D2892 / D5236 % Wt. 24.79

Yield ASTM D2892 / D5236 % Vol. 23.55

Density @ 15°C ASTM D4052 kg/L 0.9251

Specific Gravity @ 60/60° F Conversion 0.9256

API Gravity @ 60° F Calculated ° API 21.4

Sulphur Content ASTM D4294 % Wt. 2.55

Total Nitrogen ASTM D4629 ppm Wt. 680

Basic Nitrogen UOP 269 % Wt 0.0186

Pour Point ASTM D97 ° C +33

UOP K Factor UOP 375 calc. 11.6

Kinematic Viscosity @ 40° C ASTM D445 cSt 62.50

Kinematic Viscosity @ 100° C ASTM D445 cSt 7.573

Kinematic Viscosity @ 135° C ASTM D2170 cSt 3.754

Aniline Point ASTM D611 (Proc. A) ° C 81.0

Conradson carbon residue ASTM D189 % Wt. 0.40

Total Acid Number ASTM D664 mgKOH/g 0.16

Refractive Index @ 70°C ASTM D1218 1.4959

Wax Content UOP 46 % Wt. 20.1

Metals - -

Nickel mg/kg <1

Vanadium mg/kg <1

Sodium mg/kg <1

LABORATORY REPORT NO. IDL 5579/2018

Heavy Vacuum Gas Oil [370 - 548°C]

RESULT

IP 501

Al Shaheen Crude Oil 2018

TEST METHOD UNIT

Page No: 17

Sample Descriptions / Label :

Yield ASTM D2892 / D5236 % Wt. 49.50

Yield ASTM D2892 / D5236 % Vol. 44.77

Density @ 15°C IP 365 kg/L 0.9713

Specific Gravity @ 60/60° F Conversion 0.9718

API Gravity @ 60° F Calculated ° API 14.1

Sulphur Content ASTM D 4294 % Wt. 3.70

Mercaptan Sulphur UOP 163 ppm Wt. 69

Hydrogen Sulphide UOP 163 ppm Wt. <1

Total Nitrogen ASTM D4629 ppm Wt. 1823

Basic Nitrogen UOP 269 % Wt 0.0484

Pour Point ASTM D97 ° C +24

Kinematic Viscosity @ 40° C ASTM D445 cSt 1212

Kinematic Viscosity @ 100° C ASTM D445 cSt 46.62

Kinematic Viscosity @ 135° C ASTM D2170 cSt 15.90

Conradson carbon residue ASTM D189 % Wt. 9.30

Total Acid Number ASTM D664 mgKOH/g 0.19

Asphaltene IP 143 % Wt. 3.9

Wax Content UOP 46 % Wt. 5.4

Metals - -

Nickel mg/kg 15

Vanadium mg/kg 49

Sodium mg/kg 3

Atmospheric Residue [370°C+]

LABORATORY REPORT NO. IDL 5579/2018

IP 501

RESULT

Al Shaheen Crude Oil 2018

TEST METHOD UNIT

Page No: 18

Sample Descriptions / Label :

Yield ASTM D2892 / D5236 % Wt. 24.65

Yield ASTM D2892 / D5236 % Vol. 21.23

Density @ 15°C ASTM D70 kg/L 1.0199

Specific Gravity @ 60/60° F Conversion - 1.0206

API Gravity @ 60° F Calculated ° API 7.2

Sulphur Content ASTM D4294 % Wt. 4.87

Mercaptan Sulphur UOP 163 ppm Wt. 52

Hydrogen Sulphide UOP 163 ppm Wt. <1

Total Nitrogen ASTM D4629 ppm Wt. 2800

Basic Nitrogen UOP 269 % Wt 0.0728

Pour Point ASTM D97 ° C +39

UOP K Factor UOP 375 calc. 11.4

Kinematic Viscosity @ 40° C ASTM D445 cSt 266400*

Kinematic Viscosity @ 100° C ASTM D445 cSt 1131

Kinematic Viscosity @ 135° C ASTM D2170 cSt 188.1

Conradson carbon residue ASTM D189 % Wt. 19.5

Total Acid Number ASTM D664 mgKOH/g 0.25

Wax Content UOP 46 % Wt. 2.2

Softening Point D 36 ° C 35.2

Penetration @ 25°C ASTM D5 mm 248.0

Asphaltene IP 143 % Wt. 7.6

Ash Content IP 4 / ASTM D482 % Wt. 0.027

Metals - -

Nickel mg/kg 29

Vanadium mg/kg 94

Sodium mg/kg 5

Al Shaheen Crude Oil 2018

TEST METHOD

LABORATORY REPORT NO. IDL 5579/2018

Vacuum Residue [548°C+]

Remark(s): Results is calculated and only as indicative – precision parameters are not applicable.

UNIT RESULT

IP 501

Page No: 19