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Crystal development Water jet cutting Glass glue bonding Diffusion bonding Large diameter boule...

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Crystal development Water jet cutting Glass glue bonding Diffusion bonding Large diameter boule growth Thermal stress analysis Reproducible growth of high optical quality crystals achieved. Stress fracture during fabrication arose as a new issue. 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 cm Laser polish surfaces are activated with a basic solution such as KOH Bonds are permanent, optically transparent, and can withstand temperatures up to 1000 °C “Super” polished surfaces are optically contacted and heated to allow thermal diffusion Phase errors occur in bond region – thought to be thermally stress induced. 2.7 1.35 0 2.7 1.35 0 Water based non-thermal erosion using high pressure water in a thin stream ~ 1 mm thick. Stresses frozen into crystals during growth Analysis of the stress gives optimal cutting geometry for boules Current Slabs 6.5 cm Czochralski crystals grown No bonding required for full size Mercury slabs (Central Coast Gem Lab, Inc., Santa Maria, CA) (Onyx Optics, Inc., Dublin, CA) (Material Science Dept., UC Davis) (Schott Glass Technologies, Durea, PA) (Northrup Grumman / LLNL collaboration) This work was performed under the auspices of the U. S. Department of Energy by the University of California, Lawrence Livermore National Laboratory under Contract No. W-7405-Eng-48.
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Page 1: Crystal development Water jet cutting Glass glue bonding Diffusion bonding Large diameter boule growth Thermal stress analysis Reproducible growth of high.

Crystal development

Water jet cutting

Glass glue bonding

Diffusion bonding

Large diameter boule growth

Thermal stress analysis

Reproducible growth of high optical quality crystals achieved. Stress fracture during fabrication arose as a new issue.

1 2 3 4 5 6 7 8 9 10 11 12 13 14 15cm

Laser polish surfaces are activated with a basic solution such as KOH

Bonds are permanent, optically transparent, and can withstand temperatures up to 1000 °C

“Super” polished surfaces are optically contacted and heated to allow thermal diffusion

Phase errors occur in bond region – thought to be thermally stress induced.

2.7

1.35

0

Static

2.7

1.35

0

Static

Water based non-thermal erosion using high pressure water in a thin stream ~ 1 mm thick.

Stresses frozen into crystals during growth

Analysis of the stress gives optimal cutting geometry for boules

CurrentSlabs

6.5 cm Czochralski crystals grown

No bonding required for full size Mercury slabs

(Central Coast Gem Lab, Inc., Santa Maria, CA)

(Onyx Optics, Inc., Dublin, CA)

(Material Science Dept., UC Davis)

(Schott Glass Technologies, Durea, PA)

(Northrup Grumman / LLNL collaboration)

This work was performed under the auspices of the U. S. Department of Energy by the University of California, Lawrence Livermore National Laboratory under Contract No. W-7405-Eng-48.

Page 2: Crystal development Water jet cutting Glass glue bonding Diffusion bonding Large diameter boule growth Thermal stress analysis Reproducible growth of high.

Technological advancements on the Mercury laser

Phase correction

LiquidAlcohol

Alcoholvapor

Substrate

Etchantsolution

HeNe

Capabilities: Maximum P-V modulation 7 microns Minimum feature size ~ 1 mm Plate size 30 x 30 cm2

Plate thickness > 300 m

Compensates for static phase distortions in S-FAP slabs, system optics, front end, as well as point operation thermal correction

With phasecorrector

Without phasecorrector

Front end

Far fields from amplifier alone:

Full system far fields:

With phasecorrector

Without phasecorrector

Fountain head etch tool

49% Energy in 5 TDL 7% Energy in 1 TDL

83% Energy in 5 TDL 15% Energy in 1 TDL

98% Energy in 5 TDL 15% Energy in 1 TDL

92% Energy in 5 TDL39% Energy in 1 TDL

90% Energy in 5 TDL 12% Energy in 1 TDL

Page 3: Crystal development Water jet cutting Glass glue bonding Diffusion bonding Large diameter boule growth Thermal stress analysis Reproducible growth of high.

Real time damage diagnostic

Record background image

Convert image to binary / blob analysis

Subtract background

Record shot

Shut down laser

Blob size above threshold

Blob size below threshold

Temporal Energy FarField

NearField

DarkField

Temporal Energy FarField

NearField

DarkField

a) b) c) d) f) g)

(a-f) Evolution of damage at 10 Hz and (g) the static near field (V-shaped cutouts are due to a fracture in phase plate.)

Background image Image with damage

Image with background subtracted Threshold increased

300 um spot

1 mm spot

Background image

Binary imagewith thresholding

Damage image

Damage - Background

A damage diagnostic algorithm allows automatic damage detection without user intervention.

Nearfield

w/ block

“Dark field" image

beam blockNearfield

w/ block

Nearfield

w/ block

“Dark field" image

beam blockbeam blockDark field

NearfieldNearfieldNearfield

Bright field

Dark field analysis (detects high spatial frequency damage)

Bright field analysis (detects low spatial frequency damage)

Analysis routine


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