DAMES & MOORE - SUBSURFACE SOIL INVESTIGATION OF …purpose of this investigation was to...

9'JO 90:

SUBSURFACE SOIL INVESTIGATIONNORTHWEST AND SOUTHWEST QUADRANTS

CAM-OR SITEWESTVILLE, INDIANA

Prepared for

CAM-OR PRPTECHNICAL COMMITTEE

Dames & Moore Job No. 13704-020-045February 25, 1991

TABLE OF CONTENTS

1.0 INTRODUCTION

2.0 FIELD OBSERVATIONS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 22.1 Field Methods . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 22.2 Northwest Area . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 22.3 Southwest Area . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3

3.0 SAMPLING AND ANALYSIS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 43.1 Sampling Methods . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 43.2 Sample Analyses . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5

4.0 VOLUME OF BURIED SLUDGE . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 74.1 Northwest Area . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 74.2 Southwest Area . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 74.3 Assumptions for Volume Computations . . . . . . . . . . . . . . . . . . . . . . 7

5.0 CONCLUSIONS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8

FIGURES

Figure 1 - Borehole Location Map

TABLES

Table 1 - Summary of Laboratory AnalysesTable 2 - Sludge Zone Thicknesses

APPENDICES

Appendix A - Boring LogsAppendix B - Chain-of-Custody FormAppendix C - Laboratory Report

1.0 INTRODUCTION

A borehole investigation was conducted b. Dames & Moore within the northwest andsouthwest portions of the CAM-OR Site, Westville, Indiana from November 19-21, 1990. Thepurpose of this investigation was to characterize and determine the approximate volume and

extent of process-derived subsurface sludge and discolored soils in this area. The sludge isvisible at the surface in several small mounds which seem to have resulted from sludge

outcroppings beneath the soil in the northwest quadrant of the property.

A total of twenty-five (25) borings were drilled; the total footage of these borings was

453.5 feet. Depths of the borings varied from eight (8) to twenty-nine (29) feet. All but two

(2) of the borings were arranged in a grid pattern on approximately 75-foot centers (Figure 1)to determine the thickness, depth and lateral extent of the black sludge or discolored soils.These twenty-three (23) borings were logged in detail. Two (2) additional borings (Borings B-24and B-25) were advanced to take laboratory samples in order to characterize the black sludgeand discolored soils.

This report presents Dames & Moore's f indings concerning the characteristics, thickness

and lateral extent of the black sludge and discolored soils. These findings are based solely onthe following:

1. The observations of Dames & Moore personnel2. Analytical data

2.0 FIELD OBSERVATIONS

2.1 Field Methods

Drilling was performed by D&G Drilling Company of New Lenox, Illinois. A CME-55ATV (all terrain vehicle) was utilized during this effort to negotiate the soft ground surface.

Drilling was accomplished using a 4-inch solid stem auger. Continuous sampling wasinitially performed by driving a 2-inch diameter, 2-foot long split spoon with a 140 poundhammer. The 4-inch solid stem auger was used to ream the borehole when necessary in orderto drive the split spoon to greater depths. This method was used for the first eight (8) borings.Although discrete soil samples were not retained for laboratory analysis, they were closelyexamined for evidence of discoloration.

We continued to sample using just the solid stem auger (auger probe method). The splitspoon was used to obtain samples for laboratory analysis from Borings B-24 and B-25. Theauger was driven approximately five (5) feet at a time and pulled out of the hole at which timethe outer coating of material on the lead auger stem was removed and the remaining materialwas logged.

The augers were decontaminated between borings by washing with a steam cleaner. Thesplit spoon, when used on the first eight (8) borings, was thoroughly rinsed off between samples.(Sampling and decontamination procedures used for collection of laboratory samples in BoringsB-24 and B-25 are described later.) After the completion of this effort, the borings were

backfilled with cuttings and nearby surface materials.

2.2 Northwest Area

The northwest area is a triangular area bordered to the north and west by the propertyfence line. The southeast boundary extends from just west of the lagoon area (where

remediation is currently taking place) to just south of the large leaning tank. Hardened black

sludge outcroppings were evident in this region of the site. Borings B-l though B-19 wereadvanced in this area to define thickness and lateral extent of the black sludge and other

discolored soils. Samples were taken from Boring B-25 to characterize this material in the

northwest area.

Detailed logs of all borings are attached (See Appendix A). The soil column was notalways consistent from one boring to the next in the northwest area. Contacts between soil types

were hard to distinguish when masked by black sludge or oil stains. Generally, the upper five(5) to fifteen (15) feet consisted of silty clay with minor sand and gravel. Below this silty clay

a layer of fine sand with minor silt was encountered. The repetition of this lower fine sand uni t

at deeper intervals indicates it is likely native soil, but its upper boundary is highly variable and

has probably been disturbed by past site excavations.

Black sludge-like materials or discolored soils were generally encountered at depths ofless than two (2) feet below the surface. In Boring B-12, however, there was six (6) feet of siltyclay overlying the black sludge. The discolored soils zone generally consisted of black sludge

or sludge-like materials and oil-stained soil interbedded with visually clean soil.

2.3 Southwest Area

The southwest area is rectangular in shape and is much smaller in area than the northwestportion of the site. It includes the flat, low-lying area which is bounded to the west and south

by the property fence line, to the east by several tanks and buildings, and to the north by the

leaning tank. Borings B-20 through B-23 were advanced in this area to define thickness and

lateral extent of the discolored soils or sludge zone. Samples were taken from Boring B-24 to

characterize this zone in the southwest area.

The soil column was fairly consistent in the southwest area. Generally, sandy and siltyclay with minor gravel was encountered from zero (0) to five (5) feet. Below this a fine sandunit was encountered.

The upper zone was observed to consist of black sludge or oil-stained seams interbeddedwith the silty clay or the fine sand. At depths from 4.5 to 10.5 feet, we encountered the top ofa more continuous sludge zone consisting of black oily sludge interbedded with a fine sand uni t .The proportion of sludge or oil in the sand decreased gradually with depth. The black sludge-like material encountered in the southwest area was generally more fluid in nature than thesludge and discolored soils in the northwest area.

3.0 SAMPLING AND ANALYSIS

3.1 Sampling Methods

Soil/sludge samples were taken from Borings B-24 and B-25. The borings were advancedusing the CME-55 ATV drilling rig. Continuous samples were obtained by driving a 2-inchdiameter, 2-foot long split spoon with a 140-pound hammer. When necessary, the hole wasreamed with a 4-inch solid stem auger.

Prior to drilling Boring 2-24 and between Borings B-24 and B-25, the entire back of thedrilling rig was steam cleaned along with the augers and split spoons. Between samples, thesplit spoon was cleaned with a mixture of Alconox and water and then rinsed with tap water.

During sample collection the samplers wore sterile latex gloves. Tongue depressors wereused to transfer samples from the split spoon to the sample jars. A discrete sample was takenfor TCLP VOAs (volatile organics) from each of two (2) locations (Borings B-24 and B-25):One in the upper soil region and one from deeper soils. Care was taken to transfer this samplequickly and to displace all air space in the sample jar with the soil/sludge. Composite samples

were taken from each of two (2) intervals from Borings B-24 and B-25 and analyzed for TCLPparameters including semi-volatile organics and metals as wells as PCBs, pesticides, herbicides,

pH, flashpoint and percent solids (see Table 2). Due to the fact that samples collected at theseboreholes were among the most visually discolored and odorous (similar to fuel oil) of all soils

encountered during the drilling, they were submitted for laboratory analysis.

All samples were immediately placed in a closed cooler with ice for temporary storage.These samples were later taped shut, sealed in plastic bags, and placed with ice in a plastic

cooler to be shipped by Federal Express to EMS Heritage Laboratory in Darien, Ill inois. Thesamples were accompanied by a chain-of-custody form (see Appendix B).

3.2 Sample Analyses

The following EPA methods were used for these laboratory analyses: SW846-8240 for

TCLP volatile organics; SW846-8270 for TCLP semi-volatile organics; SW7.3.3.2 for cyanide;SW7.3.4.1 for sulfide; SW846-7080 for barium; SW846-3010 for cadmium; SW846-7190 for

chromium; SW846-7420 for lead; SW846-7760 for silver; SW846-7060 for arsenic; SW846-7740 for selenium; SW-846-7470 for mercury; SW846-8080 for PCBs and TCLP organochlorine

pesticides; SW846-8150 for TCLP chlorinated herbicides; SW846-9045 for pH; ASTM D-92

for flashpoint; and EPA 160.3 for total solids. Methods for extractions, digestion, leachate andother preparatory procedures are outlined in the laboratory report (Appendix C).

A summary of results for the previously described parameters is attached (Table 1).Laboratory analytical data sheets are also provided in Appendix C. As these results indicate,

all organic constituents were well below the i r respective TCLP l i m i t s . The only volatile (VGA)

TCLP constituents detected were benzene, tetrachloroethylene, and trichloroethylene. The VGA

constituents for both samples collected from Boring B-25 at the northwest portion of site were

below their respective detectable limits (i.e. below the method quantitation limits). With theexception of benzene, all VGA constituents for both samples collected from Boring B-24 werealso below their respective detectable l imi t s . The average benzene concentration for th i s

borehole is 0.058 mg/L, which is only slightly above its detectable limit. (This assumes thatthe benzene concentration for the sample collected at the 13.5- to 14-foot interval is equal to its

method quantitation limit of 0.05 mg/L. This is a conservative evaluation and assumes the worst

case.)

With regard to TCLP semi-volatile constituents, all were well below their respective

detectable limits.

TCLP herbicides and pesticides were not detected in any of the samples collected at thenorthwest and southwest portions of the facility. PCBs (polychlorinated biphenyls) were also

not detected in any of the samples collected in these areas. With the exception of the 4.4 mg/kg(or parts per millions) of sulfides detected in Sample B-24 at the 4 to 10-foot depth interval, all

other cyanide/sulfide levels were below detection limits, and, consequently indicate that thismaterial is not hazardous via RCRA reactivity criteria. Flashpoints for samples at the northwestand southwest portions of the site were greater than 180°F in all cases, which indicates that thematerial could not be considered RCRA ignitable.

The pH for all samples collected fell within the range of 5.4 to 6.7 standard units.

With regard to TCLP metals, only arsenic, barium and lead were detected. Althoughthese constituents are present at both the northwest and southwest portions of the Site, theaverage concentration for all three (3) constituents were below their respective RCRA TCLPl imi ts in Borings B-24 and B-25. The average concentrations for arsenic, barium and lead for

Boring B-24 (i.e. the average of the composite collected at 4 to 10 feet and the composite from12 to 22 feet) are 0.033 mg/L, 0.865 mg/L, and 0.595 mg/L, respectively. The averageconcentrations for arsenic, barium and lead for Boring B-25 (i.e. the average of the composite

collected at 2 to 12 feet and the composite from 12.5 to 18 feet) are 0.012 mg/L, 1.69 mg/L and4.7 mg/L, respectively.

4.0 VOLUME OF BURIED SLUDGE

4.1 Northwest Area

The volume of buried sludge and discolored soils in the northwest area was estimatedby considering this entire area as one (1) unit. The average thickness of suspect soils is jus tunder thirteen (13) feet from Borings B-l though B-19 (Table 2). Generally, the northwest arearesembles a right triangle, with legs of approximately 525 feet and 550 feet in length. To findthe area, we multiply (l/2)(525 feet)(550 feet) to get 144,375 square feet. To get the volume,we multiply the area (144,375 square feet) by average thickness (13 feet) to get 1,876,875 cubicfeet. Dividing by 27 cubic feet per cubic yard, we get 69,514 cubic yards.

4.2 Southwest Area

Borings in the southwest area indicated a much more homogenous sludge zone. Weestimated an average thickness of material at 25.75 feet. The southwest area of subsurfacesludge comprises a rectangle approximately 150 feet by 275 feet. Multiplying (150 feet)(25.75feet)(275 feet) and then dividing by 27 cubic feet/cubic yard, we get 39,340 cubic yards ofmaterial.

The resulting total from both areas on the site is estimated to be approximately 110,000cubic yards.

4.3 Assumptions for Volume Computations

The lateral extent of sludge and discolored soils was assumed to extend to the north, westand south to the property fence line. The northwest area was assumed to extend east toward thelagoon and southeast toward existing tanks and structures. The southwest area was assumed toextend east to existing tanks and structures.

The values provided for the thickness of sludge include the interval from ground surfaceto the lowest level where oil-stained materials were detected. In most of the borings, sludge wasencountered at depths of two (2) feet or less. Should soil excavation be required, any overlyingclean material would likewise be excavated; therefore, the total volume of soils would includethe interval from the ground surface to the bottom extent of sludge and discolored soils.

5.0 CONCLUSIONS

Dames & Moore has completed an investigation of the process-derived sludge anddiscolored soils in the northwest and southwest quadrants of the CAM-OR site, Westville,Indiana. This investigation involved the following activities:

• Drilling of twenty-five (25) borings

• Laboratory analyses of two (2) samples from each of two (2)borings for TCLP volatile and semi-volatile organics, TCLPmetals, TCLP herbicides and pesticides, pH values, and PCBs.

Based on the results and findings from this investigation, the following conclusions havebeen reached:

• There are approximately 110,000 cubic yards of sludge anddiscolored soils and cover material within the boundaries of theareas referred to in this report as the northwest and southwestareas.

• The laboratory analytical data indicates that, with regard to TCLPorganics and metals, the sludge and discolored soils do not exhibithazardous waste characteristics.

The pH values for samples collected were all within the range of5 to 7.

['91 cam-or:soilinvs.rpt]

FIGURE

NORTH FENCEN/

)

UJ2LUU.

cnLLJ

s/

s\/

|B-1 |B-2"T" "T

|B-6 _|B"7 IB-B( T -T "T

[ B- 1 i IB-12 IB- 13

1 /TV '0<±) B-25

• (B -15 [B-16~T I

WATER TREATAENTTANK

/\ s\

x

LAGOONS /( cur r e n t

I B-9 I B-10 rened io t ion— — — — eff or t s )

IB-H / \

'

|B-17 N

-.18

B-19LEANING"TANK

1-21ee-"BOREHOLE

BOREHOLE ( taboroiorysamples taken)

i B-22 i BB-23

Scale in Feet

FIGURE 1BOREHOLE LOCATIONS

c a pproxI not e)CAM-OR

WESTVILLE. INDIANA

SOUTH FENCEPl ,-.,— .•,.- ». It

TABLES

Table 1Summary of Laboratory Analyses

Volatile Oraanlcs (VOAs):BenzeneTelrachloroethyteneThchloroelhyleneALL Other VOAs

Semi-VolatileOraanlcs (Seml-VOAs):2-Methyl Phenol4 -Methyl PhenolPhenol

ALL Other Seml-VOAs

HerbicidesPesticidesPCDsFlashpoint (Degrees F)pllCyanide (T)Sullides (T)Percent Solids

Mcials:ArsenicBariumLeadALL Other Metals(Cd. Cr, Ag. Se. and Hg)

SAMPLE B-24Southwest Portion ol Site

4-10 ft.

• 0.058 mg/L' 0.094 mg/L• 0.061 mg/LBDL

BDLBDLBDL>1806.0BDL4.4 mg/kg87%

0.045 mg/L1.3 mg/L0.99 mg/LBDL

5.5-6 ft.

0.066 mg/L* 0.025 mg/L* 0.033 mg/LBDL

13.5-14 ft.

BDLBDLBDLBDL

12-22 ft.

BDLBDLBDLBDL

BDLBDLBDL>1806.2BDLBDL90%

0.021 mg/L0.43 mg/LBDLBDL

SAMPLE B-25Northwest Portion of Site

3.5-4 ft.

BDLBDL *BDLBDL

2-12 ft.

BDLBDLBDLBDL


0.01 4 mg/l2.5 mg/L8.9 mg/LBDL

12.5-13 ft.

BDL* 0.026 mg/LBDLBDL

12.5-1 8 ft.

BDLBDLBDLBDL


BDL0.88 mg/L0.50 mg/LBDL

• - Estimated values: below method of quantltatlon limit

Table 2Sludge ZoneThicknesses

Boring

B-1

B-2

B-3

B-4

B-5

B-6

B-7

B-6

B-9

B-10

B-11

B-12

B-13

B-14

B-15

B-16

B-17

B-18

B-1 9

B-20

B-21

B-22

B-23

Surfaceelevation

(feet)

809.5

811.5

810.3

806.9

803.8

810.1

810.6

808.1

797.1

801.6

809.9

809.4

798.3

795.5

809.4

804.5

795.5

801.9

795.6

793.3

792.2

792.2

792.4

Elevationbottom of sludge

zone (feet)

791

794.1

790.8

795.9

788.8

790.1

793.6

797.1

785.6

787.1

789.9

785.4

782.3

794.5

796.9

796

794

...

788.1

768.8

763.2

767.2

767.9

Total thicknesssludge zone

(feet)

18.5

17.5

19.5

11

15

20

17

11

11.5

14.5

20

24

16

1

12.5

8.5

1.5

0

7.5

24.5

29

25

24.5

APPENDIX A

BORING LOG

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WATER LEVEL

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DATE

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SHEET

1 « \

START

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DATE

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DATUM ELEVATION


l l l t IX /I/

DRILLING METHOD

4"

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WATER LEVEL

TIME

DATE

CASING DEPTH

BORING NO

B-7SHEET

DRILLING

START

TIME

DATE

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JOa NO CLIENT LOCATION

O«ILUNG METHOD:

S/MPLINC METHOD:

(A- P

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DATE

CASING DEPTH

BORINC NO

SHEET

DRILUNG

START

TIME

l/r,OATE

FINISH

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5

DATUM ELEVATION


DRILLING METHOD:

SAMPLING METHOD

WATER LEVEL

TIME

DATE

CASING DEPTH

BOWING NO

B-SHEET

\ ~ IDRILLING

START

TIME

DATE

FINISH

TIME

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SA

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5"


DATUM ELEVATION

JOB MO. CLIENT LOCATION

OR.LUNG METHOD

SAMPLING METHOD:

^ !fW4* C'APj

WATER LEVEL

DATE

CASING DEPTH

•ONINC NO

SHEET

) » 1

DRILLING

START

T1ME

DATE

n-zj-^t

FINISH

TIME

DATE

SA

MP

LTY

PE

DE

PT

H O

FC

AS

ING

NU

MB

ER

RIN

GS

D N

SO

ILG

RA

PH

SURFACE CONDITIONS:

•"f

fr?

M

<V

o

\

2

3

4

5

6

7

8

9

0

1

2

3

4

5

6

7

B

9 -

»- .S"'0-4.5-

> H

/

\~L-

Dames & Moore

J

t

S*

1B

j

11-

0

_

LOCATION OF BOWING

DATUM ELEVATION

1SA

MP

LE

RTY

PE

w

>c?

^

A?

%/%///%*////y/////%////

DE

PT

H O

FC

AS

ING

** /A*/ 5°

/\/

///^////"*/f////^////

BL

OW

VF

TS

AM

PL

ER

1

BE

RO

FN

GS

3<r2

DE

PT

HIN

FE

ET

0

1

2

3

4

5

6

7

8

9

l o

1

2

3

4

1 5

6

7

8

9

-

-

SO

ILG

RA

PH

CL

S.

JOB NO CLIENT LOCATIONI^T9L|~0|t C-ir^-Of.. U)C.k-f\/[ II e I A/

DRILLING MCTHOO:

S« / ri. s Jc_ ^ " AT * D — 1 \SHEET

SAMPLING MCTHOO: ' OF \

7T ^V" lj^'k-4. OKILUNGSTART FINISH

WATER LEVEL TIME TIME

TIME T » 0 P M * * ^

DATE DATE OATE

CASING DEPTH It-IP-*

SURFACE CONDITIONS.

—— k^*-**- -y v*-^ >>lt /Crky ————————————————

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&i-{0i Bl^ck c (^^jj.•"

|0 - M ' f>(^c^ r/^JU

— iT^n — ^^ 4-> ^b —— T^J — —————I 1 /

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J H ~ \ T " ' U*Jy oil 1-fxrv.i ^ si Iv CUV/ i f

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1

DATUM ELEVATION

JOB NO

- G l f eCLIENT LOCATION

DRILLING METHOD

SAMPLING METHOD:

*f*- Y^ I It /L —— _

WATER LEVEL

TIME

DATE

CASING DEPTH

BORING NO

SHEET

I C-D"'LUNC

START

TIME

DATE

FINISH

TIME"

DATE

SA

MP

TY

P

DE

PT

H O

CA

SIN

G

BL

OW

S/F

TS

AM

PL

ER

NU

MB

ER

OF

RIN

GS

D INSURFACE CONDITIONS:

55

Ji VV

Si

Si

Si

Ji

/*

,

S 16

A

c

i

3

4

5

6

7

8

9

I 0

1

2

3

4

1 5

6

7

8

9

CL.

H

_ P

3 ' f r ' J

4- -v/ M. s:

6 - * '

-•?. ^S -

- 10 ~ i—^ ^; if f

^}I P -<i. IQ' <Vfr"J

Li^jv. ai'l ii'w-J- It.- >3

t l - 'M A 1>XJL S^-s. ilj nrIM- 1 t,

Vi^.

u.I t-.J

^ i .4-1 . . / . . * •

Dames & MooreLOCATION Of BORING

DATUM ELEVATION

JOB NO CUENT LOCATION

DRILUNG MCTHOO:

SAMPLING MfThOO:•V*

WATER LEVEL

T.ME

DATE

CASING DEPTH

SHEET

2-DRILLING

START

TIME

DATE

FINISH

TIMI:

OATE

SA

MP

LTY

PE

DE

PT

H O

CA

SIN

G

BL

OW

S/

SA

MP

LE

NU

MB

ER

RIN

GS 5!r "i"

0 Z SO

ILG

RA

PH

SURFACE CONDITIONS

SiLM

3

4

2.5

6

7 -

8 -

9

0

1

2

3

4

5

6

T . O - - L I . S - (.;/srs


DATUM ELEVATION

JOB NO. CUENT

DRILLING METHOD

-5«^-^r

SAMPLING METHOD:

^'»'•«•It < ———— ,~

WATER LEVEL

TIME

DATE

CASING DEPTH

BORING NO

"B- 13SHEET

DNILUNG

START

TIME

DATE

FINISH

TIME

DATE

DE

PT

H O

CA

SIN

G

BL

OW

S/F

TS

AM

PL

ER

NU

MB

ER

OF

RIN

GS

DE

PIN

F SO

ILG

RA

PH

SURFACE CONDITIONS:

. i^x :,;(.(.

S3

s s

SJ

Si

lo

n.

\\

o

i

i

3

4

5

6

7

8

9

lo

1

1

3

4

I S

6

7

8 -

9 -

CL

0- J—— J?

J

~i o 14- L — 4U *~-J? -i

10-10. i ** — <-

10. 5- -P-*

.Wl/o^4^

^ t~.y

IM-U1

Ac. A.-A-C

._il=ÂoL__' v.i«-i.

Dames & Moore

DATUM ELEVATION

JOB NO. CUCNT LOCATION

DKILUNC MCTMOO:

SAMPLING METHOD:

A —— **.-

WATER LEVEL

DATE

CASING DEPTH

•OftING NO.

B - 14OF

START

T)ME

DATE

I-it-Id

FINISH

T1ME

DATE

SA

MP

LE

TY

PE

DE

PTH

OC

AS

ING

BL

OW

S/F

TS

AM

PL

ER

NU

MB

ER

RIN

GS

DE

PT

HIN

FE

E

SO

ILG

RA

PH

SURFACE CONDITIONS

ss /ft

si

SJ

~A

o

i

i

3

4

5

6

7

a

9

0

1

2

3

4

5

6

7

8

9 -

(- L

J/c

frTt*^ ««k-

4-r

l-i- uw


DATUM ELEVATION


ORILUNG METHOD

P^N*. i l t t -pit If i,I, '' '

SAMPLING METHOD:

Y*"*" • ——WATER LEVEL

DATE

CAS,NG DEPTH

•OMINC

6-SHEET

I -or /OMILUNC

STAKT FINISH

DATE °*TE

SA

MP

LTY

PE

ss

SS

09Q

"71

DE

PT

H O

FC

AS

ING

-

-*'

*»/u

LO

WS

/FT

SA

MP

LE

R

NU

MB

ER

OF

RIN

GS

DE

PT

HN

FE

E

0

1

2

3

4

5

6

7

8

9

I 0

1

2

3

4

6

7

8 -

9 -

SO

ILG

RA

PH

)-X'CL

SURFACE CONDITIONS:

:\

6 - S 1 oi l -7. 6-V. o

ev A ^ If - l o P-1.5

• v, C<<Y7,./o6

n-1^Lb_i, «•««-


DATUM ELEVATION

JOB NO. CUENT LOCATION

DRILLING METHOD

SAMPLING METHOD:

WATER LEVEL

TIME

DATE

CASING DEPTH

SOWING NO

DRILL'NG

START

TIME

DATE

-i vit

FINISH

TIME

DATE

l\-n~°rt>

SA

MP

LTY

PE

DE

PTH

OC

AS

ING

BL

OW

S/F

TS

AM

PL

ER

NUM

BER

OFR

ING

S

DE

PT

HIN

FE

E

SO

ILG

RA

PH

SURFACE CONDITIONS:

Si

x 0

1

2

3

4

5

6

7

8

9

10

1 -

2 -

3

4

I 5

6

7 -

a

9

2.Q

o-x

CLfc^y.

»"vi_ a.«S l^_U

H- t ' c _ ^_ 0H~M.r '^

s-r>» fi \

^ , J~ P .

10

Dames & MooreLOCATION Of BOWING

IDATUM ELEVATION

JOB NO CUCNT LOCATION

DRILLING METHOD

tf"SAMPLING METHOD:

•y** I Ho

WATER LEVEL

TIME

DATE

CASING DEPTH

BONING NO.

SHEET

I ' crOR.LUNG

STARTTIME

DATE

FINISHTIME

DATE

DE

PTH

OC

AS

ING

BL

CW

S/F

TS

AM

PL

ER

NU

MB

ER

OF

RIN

GS

t u

t"-O Z S

OIL

GR

AP

H

SURFACE CONDITIONS:

X~>>r

IS

5S

1

2

3

4

5

6

7

8

9

1°

1

2

3

4

5

6

cu (o-t," j) ^r A

"Z.-3

? - M ' 1 5 H -

CL

— C

«-^^ ' j*.- \\ ~ c)Vv/

0/A,\t J J/?^>4.

8 ~ i o '

0 ' o 2)


}1 -.

DATUM ELEVATION


DRILLING METHOD.

SAMPLING METHOD:

WATER LEVEL

DATE

CASING DEPTH

•OWING NO

SHEET

START

TIME

DATE

FINISH

TIME

DATE

f

DE

PT

H O

FC

AS

INO

BL

OW

VF

TS

AM

PL

ER

NU

MB

ER

OF

RIN

GS

PT

HFE

E

SO

ILG

RA

PH

SURFACE CONDITIONS:

SI

Si

Si

ao

u

o

1 -

4

I 5

6

7

8

9

, ' I VCu

1- H C . ' I - V

_uSi

CL 5 I Ji -V-

ML

- \~Lf» ^vs

Z£

Dames & MooreLOCATION OF BONING

DATUM ELEVATION


DKILUNG METHOD:

SAMPLING METHOD

WATER LEVEL

TIME

DATE

CASING DEPTH

•OAING NO.

SHEET

0,

ORILUNG

START

TIME

DATE

FINISH

TIME

DATE

SA

MP

LTY

PE

DE

PT

H O

CA

SIN

G

LO

WS

/FT

AM

PL

ER

NU

MB

ER

OF

RIN

GS z

5=oz SO

ILG

RA

PH

SURFACE CONDITIONS

; H- FILL

J.S o

S J

SJ

ss ?ft

Si

aaiczo

Q

f

O

71

\

A

1

2

3

4

5

6

7

8

9

l o

1

2

3

4

1 5

6

7

8

CL

1-1. o\ \

f'.V* lw<i

-PM- t> '

t - t f '

M

10' ^


DATUM ELEVATION

JOB NO. CLIENT LOCATION

OMILUN6 METHOD:

SAMPLE C MCTMOO:

WATER LEVEL

TIME

DATE

CASING DEPTH

•°"'NG N°

SHEET

I 'DHILUNG

START

T1ME

DATE

FINISH

nME

DATE

SA

MP

LE

TYPE

BL

OW

S/F

TS

AM

PL

ER

NU

MB

ER

RIN

GS

Q Z

SO

ILG

RA

PH

SURFACE CONDITIONS:

4^- ^V

/v?

\rt

A?

M

9 -r-

D-H.4* U- > « \il4>,

-s .o

If i .U


DATUM ELEVATION


OH.LUNO METHOD:

H "

SAMPLING METHOD:

WATER LEVEL

TIME

DATE

CASING DEPTH

BORING NO.

B- 2.0SHEET

2~-OF2_

START

DATE

FINISH

DATE

/l-io-fii

1SA

MP

LE

RT

YP

E

DE

PTH

OF

CA

SIN

G

LO

WV

FT

SA

MP

LE

R

NU

MB

ER

OF

RIN

GS

Q Z SO

ILG

RA

PH

SURFACE CONDITIONS:

rV?

mQX

u

Ks

1-0

}

1

4

2-5

6

7

fro

1

2

3

4

5

6

7

8

9 -

M.JL «_ l.r 4, -2:. f<-l.~Ao 2-*f--S"

a-f UJWu -v ft i


DATUM ELEVATION


v'.ll.

ORILUNC MCTHOO:

SAMPLING MCTHOO:

WATER LEVEL

TIME

DATE

CASING DEPTH

•OWING NO

R-Z.1SHEET

0, -

ORILUNG

START

TIME

DATE

FINISH

TIME

DATE

SA

MP

LT

YP

E

DE

PC

A

LO

WV

FT

SA

MP

LE

R fc<r fuOO 2ZiZ

D N

SGM

LG

RA

PH

SURFACE CONDITIONS:

X?

Art o

A-tTo-

1

2

3

4

5

6

7

8

9

(0

1

4

Is

6

7

8 H

CL

'M

0 - 4 -r

*-»«'« I.«*<.*****-.

f- 11/7«" *f " •«•<- L-

0^, \-. 14 v. . f..j—^:«-

4'S ! ) V

^-10.

1 —— *

17.- 14

/^'J'y^'

*^^^T^^^^^


DATUM ELEVATION

JOB NO.

1370M-CUCUCNT

CAfA-OfLLOCATION

XMORILUNG METHOD:

SAMPLING METHOD:

WATER LEVEL

DATE

CASING DEPTH

•°"WB "°-

SHEET

•2. OF

OH.LUNG

START

TIME

DATE

FINISH

TIME

DATE

Vfl

DE

PTH

OF

CA

SIN

G

NU

MB

ER

RIN

GS

SO

ILG

RA

PH

SURFACE CONDITIONS

A-?

/v?

0

o'•*.

r*\

0

2.0

1

2

3

4

2.5

6

7

8

4

5

6H

7

8

9

0

r>~ urUo^

1*1-7. H* > l ^ ) 0 0

\ooo


DATUM ELEVATION


D..LUNG METHOD:

SAMPLING METHOD:

WATER LEVEL

DATE

CASING DEPTH

•°"ING NO

SHEET

START

TIME

OATE

FINISH

OATE

P DE

PT

H O

CA

SIN

G

LO

WS

/FT

AM

PL

ER

B S

0 zSiz

Q Z SO

ILG

RA

PH

SURFACE CONDITIONS:

A?

oro

A-?

A

4

5

6

7

8

9

0

1 (-4

4

15

6H

9 -

0- -s i — o

10 - | 0.

SfA

- «


DATUM ELEVATION

JOB NO. CUCNT LOCATION

DRILLING METHOD

SAMP'JNC METHOD:

WATER LEVEL

T.ME

DATE

CASING DEPTH

BORING NO

SHEET

•2-0,*-START

*"**

DATE

FINISH

1 l~

SA

MP

LE

TYP

E

DE

PT

H O

CA

SIN

G

BL

OW

S/F

TS

AM

PL

ER &t <nSo

0)2S E3Z

DE

PT

HIN

FE

E

OI A

SURFACE CONDITIONS.

I/c

rV?

BDXXu

OroI

0

to

6

7

8

9

I

> 0

1

2

3

4

5

6

7

8

9

0 M

J f l

•Vv


DATUM ELEVATION


DR.LLING METHOD:

SAMPLING METHOD:

WATER LEVEL

DATE

CASING DEPTH

•°"1NG NO

SHEET

2_DRILLJNG

START

TIME

I I

DATE

U-zc-'io

FINISH

T1ME

OATE

MP

LT

YP

E

DE

PT

H O

CA

SIN

G

BL

OW

S/F

TS

AM

PL

ER

NU

MB

ER

RIN

GS

DE

PT

HIN

F

EE

SO

ILG

WA

PH

SURFACE CONDITIONS

/v?

I BOieIu

uI

.s

T~7T

9

f 0

1

1

3

4

I s

6

O-M.

CL

tV-J U* t- 4 " 1 •» - *Jl* (• .'

11.S~ 9 — -UiÂi. < !>-• w C

-i- U^

o. i - >H. •!_;*• Ut

h

ill I "IV II 101 PATT M'XP ~^ 0 run n BV_

CO

NJ »

T~I I

r*inTTT

oo%

SAMPLERTYPE

DEPTH OFCASING

lAWPlI• O

BLOWS/FTSAMPLER

NUMBER OFRINGS

DEPTHIN FEET

SOtLGRAPH

I«i

o5r

I

n

8

ow>

(D

IIo

Dames & Moore

o-«f>

of o

s »i s

o70

-4-5. 8

U.1 , u (j Ct

APPENDIX BCHAIN-OF-CUSTODY FORM

JLEMS

... VI ^ ,1 il. W*- *V

8205 SOUTH CASS AVENUE SUITt 106DARIEN, II 60559 (708)969-9030

CHAIN OF CUSTODY RECORD AND ANALYSIS REQUEST FORMCo. Name: n • '

DftfiiS f JflAOfi L. • •PfojeclName; -/\/t •Ouoio N<\: PONo.: ' "•.ENVIRONMENTAL PROGRAM:

CWA NPDES JWP (SLUDGE/ ^RCRA

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MW SW DISPOSAL

CERCLA/SUPERFUND OTHEft

Sampled by:

Samplo10:

0-J1B-JCJR-J^R - A VG-* v.

0-AsrCJ-AJ!

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fr. £**:f *nt> _ & \ lit.Aim: T6m c.dt/.'a j\Plwno: ^/q - 75A~a^"99Accelerated liurnaiouno Requested ___

{SubjOCl io Addiboiul CKir i}

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APPENDIX C

LABORATORY REPORT

' . C E R T I F I C A T E

Service LocationMS HERITAGE LABORATORIES, INC.

8205 S. CASS AVE. SUITE 106HARIEN, IL 60559708)969-9030

O F A N A L Y S I S

Received Lab ID21-NOV-90 C126588

Complete PO Number

18- DEC-90 ...... .............Frinted Sampled

19-DEC-90 20-NOV-90

Report To -•:.

DAMES AND MOORE DAMES 5 MOORECHARLIE BEST1550 NORTHWEST HIGHWAY JAN 7 IQQfPARK RIDGE, IL 60068 IJ31

Bill To

DAMES AND MOORE

1550 NW HIGHWAY, SUITE 220PARK RIDGE, IL 60068

Sample DescriptionDESCRIPTION: CAM-OR - B-24 13.5'-14.0'

1 J HEADSPACE EXTRACTION (TCLP) SW846-1311•nalyst: C. EDWARDS Analysis Date: 03-DEC-90 Test: P108.1. 0

ParameterIUTAL SAMPLE WEIGHT1 IQUID -PORTION :«; -™^ Y :: " Y-K - - • • • • . '••

QUID FRACTION (GRAMS)_«TRACTED SAMPLE3.5 MM SIEVE TEST

.5% SOLIDS :.v:;,:2:.:.:-:^:.v,':.<.-^^, • " ' . ' , ; . ' . - . . . : ' , - / / - . • • .IITIAL PH

ADJUSTED PH"IFFER SOLUTION PH

1LUME BUFFERED SOLUTIONvULUME EXTRACT FILTEREDTOTAL VOLUME FILTRATE ; /

IITIAL TIME .............................................................. ........

Result Oct. Limit24.92

24.92

4.9650080804021.64039.1

UnitsGramsmLGramsGramsPassedPercentStd. UnitsStd. UnitsStd. UnitsmLmLmLHoursHours

'CLP VOLATILE ORGAN I CS (TOXICITY CHARACTERISTIC) SW846-8240nalyst: S. BUSSEY Analysis Date: 12-DEC-90 Instrument: CC/HS VGA Test: 0513.3. 0Prep: ZERO HEADSPACE EXTRACTION (TCLP) SW846-1311

Corrected DetectionParameter Result Limit

itNZEKE , 5 0 uERECTED RESULT " . ' - • ' - " . :. '/:-Z^3-'L'.,::- :" T:.- .

tBON TETRACHLORIOE SO u

iRECTEO RESULT ; ..-.•]...-.:... . - . • " .:

:HLOROflEMZEME . 5 0 uiHECTED RESULT '•'-.:'. '•'•".' '"":'.• '"-..': ''...'• ;

.OROFORN SO U3RRECTED RESULT :' ?-OICHLOROETHAJ(E 50 u

'RECTED RESULT

'.1-DICHLOROETHYLENE 50 u:CRRECTED RESULT

THYL ETHYL KETOHE 100 (.«RECTEO RESULT

fETRACHLOROETHYLENE 50 (.

Observed Matrix Spike Sample *Units Result True Value Spike

g/L BOLBOL

g/L BOLBOL

g/L BOLBOL

g/L BOLBOL

ig/L BOLBOL

ig/L BOLBOL

ig/L BOLBOL

g/L BOL

Matrix SpikeX Recovery

Page 1

EMS'HERITAGE LABORATORIES, INC. Lab Sample ID: C126588r

Parameter

CORRECTED RESULTTR1CHLOROETHYLENE :CORRECTED RESULT

V1MTL CHLORIDE : -w:

1 CORRECTED RESULT'.:-,: ...:-•-- . . . - . : • • ... •;•;•'•'.'.•""•'•' •::"•'•:•:••'.

SURROGATE RECOVERY

D1CHLOROETHANE-D4

TOLUENE-08 : :'.'./ ••'• '•: /: .'.'.. BROHOFLUOR08EN2ENE

CorrectedResult

• • . - : . " • ? • • : • . , !

...:.".-.

DetectionUnit

:'. ' 'v-,:.:-. ':^0

::<^-x€:7:^100

Units

U8/L

:-:.uo/L. ••••;••- ':':-.

X Rec: X Rec

X Rec

ObservedResult

SOLBOLBOL

.; MLBOL

10310392

Matrix SpikeTrue Value

Sample *Spike


'

BDL Below Detection LimitSample Carments

Qua l i t y Assurance Off icer : Last Page 2

C E R T I F I C A T E O F A N A L Y S I S

Service Location Received

EMS HERITAGE LABORATORIES, INC. 21-NOV-908205 S. CASS AVE. SUITE 106 completeDARIEN, IL 60559 17-DEC-90(708)969-9030 Printed

18-DEC-90

Lab 10

C126586PO Nun*>er

Samp.ed20-NOV-90

Report To ' Bill To

DAMES AND MOORE DAMES AND MOORECHARLIE BEST1550 NORTHWEST HIGHWAY 1550 NW HIGHWAY, SUITE 220PARK RIDGE, IL 60068 PARK RIDGE, IL 60068

Swple DescriptionDESCRIPTION: CAM-OR - B-24 4.0'-10.0' COMPOSITE

,OTAL SOLIDS EPA 160.3Analyst: D. RIHELLA-SIEKERMAM Analysis Date: 27-NOV-90

. Parameter ResultSOLIDS 87

Test: C401.7. 0

Det. Limit Units0.1 Percent

OPENAnalyst

FLASH

CUP FLASH: F. FLORES,

POINT

POINTJR.

- SOLIDS

Parameter

(ASTMAnalysis

D-92Date:

MODIFIED)28-HOV-90

ASTM D-92Test

Result> 180

Det.

: G515.1. 0

Limit UnitsDecrees F

II PH S/S/SAnalyst: D.

II PH

SW846-9045RINELLA-S1EKERMAM Analysis Date: 26-NOV-90 Test

Parameter Result6.0

Det.

: G624.

Limit0.

0. 0

1Units

Std. Units

IhCYANIDE

alyst: D

CYANIDE

TOTAL AVAILABLE. RINELLA-SIEKERMAN

sw 7.3.3.2Analysis Date: 30-MOV-90 Instrument: AUTO-ANALYZER Test

ParameterBDL

Result Det.

: G115.

Limit0.

3. 0

5Units

ma/ka

TOTALAnalyst:

AVAILABLEL. DIA2

INITIAL WEIGHTFINAL VOLUME

SULFIDE EXTRACTION SW 7.Analysis Date:

3.4.126-NOV-90 Test: P116.2. 0

ParameterOR VOLUME

Result11.05250

Det. Limit UnitsGramsmL

SULFIDE SW846-9030 |Analyst: L. OIA2 Analysis Date: 26-NOV-90 Test: QUO. 4. 0 I

Prep: TOTAL AVAILABLE SULFIDE EXTRACTION SW 7.3.4.1 j

SULFIDEParameter Result

4.4Oet. Limit

2.3Units |

ma/ka '

PCB SONICATION EXTRACTION SW846-3550 1Analyst: C. SARKAN Analysis Date: 29-HOV-90 Test: P231.1. 0 !

ParameterINITIAL WEIGHT OR VOLUMEFINAL VOLUME

Result5.44100

Det. Limit Units !Grams \mL ;

Page 1

Lab Sample ID: C126586

POLYCHLORINATED BIPHENYLS (PCBS) SW846-8080Analyst: C. SARKAN Analysis Date: OJ-OEC-90 Instruntnt: CC/ECO Test: 0301.2. 0

Prep: PCB SONICATION EXTRACTION SW846-3550Parameter

PCB AROCHLOR 1016rto AKULHLUK \.LL\PCB AROCHLOR 1232PCB AROCHLOR 1 242 1 -PCB AROCHLOR 1248PCB AROCHLOR 1254PCB AROCHLOR 1260PCB AROCHLOR 1262

ResultBDLBDLBDLBDLBDLBDLBDLBDL

Oct. Limit1.05.01.01.01.01.01.01.0

Unitsmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgtnq/kq

TOX CHAR LEACHING PROCEDURE (TCLP W/ORG+PEST+HERBS) SW846-1311Analyst: S. HUMAN Analysis Date: 29-HOV-90 Test: P107.2. 0

ParameterTOTAL SAMPLE WEIGHTLIQUID FRACTION (GRAMS)"XTRACTED SAMPLEoOLIDS ,•• :- : : ; : : • : : • • : : : . , : : - -;,•::;'•.",. ' , ' '' ;.. ;,. . •9.5 MM SIEVE TESTINITIAL PH :.^^;./:V-:-::^:;:v.>v-:v:: • r^ : ••-^. ';' "• . . /ADJUSTED PHBUFFER SOLUTION PH ;iFINAL PHVOLUME BUFFERED SOLUTIONVOLUME EXTRACT FILTEREDLIQUID FRACTIONTOTAL VOLUME FILTRATEINITIAL TIME :FINAL TIME

Result100090100

5.591.694.924.9418001800018006825.46843.5

Det. Limit UnitsGramsGramsGramsPercentPassedStd. UnitsStd. Units!Std. Units;Std. Units:mLmLmLmLHRSHRS

FAA OR ICP ACID DIGESTION OF LEACHATE SAMPLES SW846-3010Analyst: J. WARE Analysis Date: 05-DEC-90 Test: P130.B. 0

Prep: TOX CHAR LEACHING PROCEDURE (TCLP W/ORG+PEST+HERBS) SW846-1311Parameter

INITIAL WEIGHT OR VOLUMEFINAL WEIGHT OR VOLUME •-•^•>w^;m : -

Result100100

Det. Limit UnitsmLmL

BARIUM FAA (1 POINT MSA) SW846-7080Analyst: S. STRUEyiNC Analysis Date: M-OEC-90 Instrument: FAAPrep: FAA OR ICP ACID DIGESTION OF LEACHATE SAMPLES SW846-3010Prep: TOX CHAR LEACHING PROCEDURE (TCLP W/ORG+PEST+HERBS) SW846-1311

Test: M604.5. 0

ParameterBARIUMADDITION 1 -SAMPLESAMPLE + ADD 1DILUTION

Result1.32.501.343.971

Det. Limit0.20

i

Units img/L jmg/L ;Cone !Cone j

Page 2

trio ntiwinuc. Lôuivni UIMC.O, inv». i.au jamy i c lu. v,ii.D300

CADMIUM FAA (1 POINT MSA) SW846-7130 |Analyst: A. STOCKBURGER Analysis Date: OA-DEC-90 Inatrunent: FAA Test: M608.5. 0 !

Prep: FAA OR ICP ACID DIGESTION OF LEACHATE SAMPLES SW846-3010 1Prep: TOX CHAR LEACHING PROCEDURE (TCLP W/ORG+PEST+HERBS) SW846-1311

ParameterCADMIUMADDITION l^Ti^m^/Z;, :---^c ,• ;. :SAMPLESAMPLE + ADD '•l^^^-^,.-:^/:-DILUTION

ResultBDL0.500.010.481

Det. Limit0.02

Units >mg/Lmg/L ;Cone !Cone

CHROMIUM FAA (1 POINT MSA) SW846-7190Analyst: A. STOCKBURCER Analysis Date: 06-DEC-90 Instrunent: FAA Test: M610.5. 0

Prep: FAA OR ICP ACID DIGESTION OF LEACHATE SAMPLES SW846-3010Prep: TOX CHAR LEACHING PROCEDURE (TCLP W/ORG+PEST+HERBS) SW846-1311

ParameterCHROMIUM

'ADDITION :i:;::^^:M^-::^vx.,s :::••:•;;::>>••;,•::,••:.•:;••;.. . • . , .SAMPLESAMPLE + ADD i":: :;.J /^p'-" : •;JlLUTION

ResultBDL1.000.011.0710

Det. Limit0.50

Unitsmg/Lmg/LConeCone

LEAD FAA (1 POINT HSA) SW846-7420Analyst: A. STOCKBURGER Analysis Date: 06-DEC-90 Instrunent: FAA Test: M616.5. 0

Prep: FAA OR ICP ACID DIGESTION OF LEACHATE SAMPLES SW846-3010Prep: TOX CHAR LEACHING PROCEDURE (TCLP W/ORG+PEST+HERBS) SW846r1311

ParameterLEADADDITION l/^:-:^.:.-:-::S::.^:^.-.-:\.--:/\ : .SAMPLESAMPLE + ADD 1 .:^m^X:^K^-' -: \^: • ,- ,DILUTION

Result0.995.000.995.731

Oct. Limit0.20


SILVER FAA (1 POINT MSA) SW846-7760Analyst: A. STOCKBURCER ' : Analysis Date: 06-OEC-90 Instrunent: FAA Test: M630.S. 0


ParameterSILVERADDITION 1 •^m:mzmm£:£:m^K:::: .::• 'SAMPLESAMPLE + ADD l-^:^^:^}mKs.^^---: ' •DILUTION


Det. Limit0.04


GFAA ACID DIGESTION OF LEACHATE SAMPLES SW846-3020Analyst- J WARE Analysis Date: 05-DEC-90 Test: P130.9. 0


INITIAL WEIGHT OR VOLUMEFINAL WEIGHT OR VOLUME

Result5050

Det. Limiti

Units

mLmL

Page 3

EMS HERITAGE LABORATORIES, INC. Lab Sample ID: C126586ARSENIC GFAA (1 POINT HSA) SW846-7060 ?Analyst: K. KEHOE Analysit Date: 07-DEC-90 Instrument: GFAA Test: M603.6. 0 !

, Prep: GFAA ACID DIGESTION OF LEACHATE SAMPLES SW846-3020 1| Prep: TOX CHAR LEACHING PROCEDURE (TCLP W/ORG+PEST+HERBS) SW846-1311 {

Parameter„ ARSENIC

ADDITION 1 ; s: ; ; :SAMPLESAMPLE + ADD 1 > b^^:/lJ\JB---. •{/.2::[-.-: . . . .'DILUTION

Result0.0450.01UO0.0450.0662

Det. Limit0.010

Units Img/Lmg/LConeCone

SELENIUM GFAA (1 POINT MSA) SW846-7740 1Analyst: K. ICE HOE Analysis Date: 10 -DEC -90 Instrument: CFAA Test: M628.6. 0 I

Prep: GFAA ACID DIGESTION OF LEACHATE SAMPLES SW846-3020 I" Prep: TOX CHAR LEACHING PROCEDURE (TCLP W/ORG+PEST+HERBS) SW846-1311

ParameterII SELENIUM"ADDITION i : > : m - :::

SAMPLE•WPLE + ADD 1

uRUTION

ResultBDL0.01000.0000.0435

Oct. Limit0.025

Uni ts

mg/Lmg/LConeCone

., CVAA ACID DIGESTION OF LEACHATE SAMPLES SW846-7470Analyst: M. SCROGHAH Analysis Date: 05-OEC-90 Test: P131.9. 0

11 Prep: TOX CHAR LEACHING PROCEDURE (TCLP W/ORG+PEST+HERBS) SW846-1311Parameter

|| INITIAL WEIGHT OR VOLUME'! FINAL VOLUME

Result10100

Oct. Limit Units

mLmL

i MERCURY CVAA (1 POINT MSA) SW846-7470Analyst: H. SCROGKAM Analysis Date: 06-OEC-90 Instrument: CVAAPrep: CVAA ACID DIGESTION OF LEACHATE SAMPLES SW846-7470Prep: TOX CHAR LEACHING PROCEDURE (TCLP W/ORG+PEST+HERBS) SW846-1311

Test: H620.6. 0

MERCURYADDITION i mmz.

\MPLESAMPLE + ADD 1 iDILUTION

Parameter ResultBDL0.001000.0000.000921

Oct. Limit0.005


GC/MS SEPARATORYAnalyst: C. CIESIELSICI

Prep: TOX CHAR

INITIAL WEIGHT ORFINAL VOLUME

FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510Analysis Date: 30-HOV-90 Test: P233.4. 0

LEACHING PROCEDURE (TCLP W/ORG+PEST+HERBS) SW846-1311Parameter

VOLUMEResult

2001

Oct. Limit Units

mLmL

TCLP SEMIVOLATILE ORGANICS (TOXICITY CHARACTERISTIC) SW846-8270Analyst: A. BRADBURN Analysis Date: 02-DEC-90 Instrument: CC/HS SVOAPrep: GC/MS SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510Prep: TOX CHAR LEACHING PROCEDURE (TCLP W/ORG+PEST+HERBS) SW846-1311

Test: 05H.3. 0

Parameter1,t-DICHLOROBENZENE2.4-OIMITROTOLUENEHEXACHLOR08EMZENEHEXACKLOROBUT AD I ENEHEXACXLOROETHANE

CorrectedResult

DetectionLimit

5050505050

Unitsug/Lug/Lug/Lug/Lug/L

ObservedResult

BDLBOLBOLBOLBDL


Sample *Spike


Page 4

EMS HERITAGE LABORATORIES, INC. Lab Sample ID: C126586

ParameterNITROBENZENEPYRID1NErRESYLIC ACIDJ-METHYL PHENOL. : ; ' '•3-METHYL PHENOL

;-METHYLPHENOL : X : : :'ENTACHLOROPHENOL

I PHENOL ''::::.'V.VP!::-''X:::'-X : : . . • ' . ' - X '"'.'..'1 TETRACHLOROPHENOL

2 . < , 5- TR I CHLOROPHENOL X v1 2,4,6-TRICHLOROPHENOL

v •••-:•:;,- ••••:, I-:-:.-:-:-- -:;,.--v • ' • v " " . :"-:':-| - - • V -.. .,., - V V . - . - . V . -

SURROCATE RECOVERY

I 2-FLUOROPHENOL" PHENOL-D5 • / : - : : : .v : I ./ Xf • ..;.::.' -.;, .'• ';-X

NITROBENZENE-DSII UOROBIPHENYLII 2,<»,6-TRIBROMOPHENOL

TERPHENYL-D14

CorrectedResult

''.....

DetectionLimit

50250120120120120250120120120120

. .-••

Unitsug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L

X RecX RecX RecX RecX RecX Rec

ObservedResult

BDLBOLBOLEST 58BDLEST 94BOLEST 61BDLBOLBOL

423271695858


Sample *Spike

Matr ix Spike !X Recovery

r

1I

^Results not corrected for spike recovery.**3-and 4-Methyl Phenol coelute so identification is tentative.

GC SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510Analyst: B. UOOO Analysis Date: 05-DEC-90 Test: P233.1. 0


INITIAL WEIGHT OR VOLUMEFINAL VOLUME •• : : . " : : .> '- :>-. ; ; , . : . .- :- . :-- . ; : :>/- ' -" : :- ' : ' : ' "" :" "

Result20010'

Det. Limit UnitsmLml

TCLP ORGANOCHLORINE PESTICIDES BY GC:ECD SW846-8080Analyst: J. HOUAT Analysis Date: 11-OEC-90 Instrument: CC/ECOPrep: GC SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510

Test: 0164.7. 0

Prep: TOX CHAR LEACHING PROCEDURE (TCLP W/ORG+PESI+HEKBb) bW84o-l,JII

ParameterGAMMA-BHC (LINOANE)

HEPTACHLOR

HEPTACHLOR EPOXIDEENORIN •-: .-. : . • • • : > : . : > . . . : : . ; . . . • • : : : : 'HETHOXYCHLOR

CHLORDANETOXAPHENE

CorrectedResult

DetectionLimit

0.000250.000250.000250.00050.00250.00250.005

Unitsng/Lng/Lng/L•g/L•g/Lng/Lmg/L

ObservedResult

BOLBOLBOLBDL

BDLBDLBDL


Sample »Spike


DIAZOMETHANE HERBICIDE DERIVATIZATION SW846-8150Analyst: L. DOBBINS Analysis Date: 06- DEC -90 Test: P201.4. 0

Prep: TOX CHAR LEACHING PROCEDURE (TCLP W/ORG-t-PEST-t-HERBS) SW846-1311Parameter

INITIAL WEIGHT OR VOLUMEFINAL VOLUME

Result25010

Oct. Limit Unitsmlml

Page 5

EMS HERITAGE LABORATORIES, INC. Lab Sample ID: C126586 1TCLP CHLORINATED HERBICIDES SW846-8150Analyst: A. HOACLAND Analysis Date: 13-OEC-90 Instrument: GC/ECD Test: 0253.7. 0

Prep: DIAZOMETHANE HERBICIDE DERIVATIZATION SW846-8150Prep: TOX CHAR LEACHING PROCEDURE (TCLP H/ORG+PEST+HERBS) SW846-1311

Parameter2,4-DICHLOROPHENOXYACETIC ACIDSILVEX

Result Oct. limit UnitsBDL O . O J mg/LBDL 0.001 mo/L

> Greater Than Upper Detection LBDL Below Detection LimitE5T Estimated Value

Sample Cementsimit

Quality Assurance Officer: \ G Last Page 6

C E R T I F I C A T E O F A N A

Service Location

EMS HERITAGE LABORATORIES, INC.8205 S. CASS AVE. SUITE 106DARIEN, IL 60f59(708)969-9030

L Y S I S

Received21-NOV-90

Complete

17-DEC-90Printed

18-DEC-90

lab 10

C126589PO Ncmocr i

Sampled \

20-NOV-90 !

Report To

DAMES AND MOORECHARLIE BEST1550 NORTHWEST HIGHWAYPARK RIDGE, IL 60068

Bill To

DAMES AND MOORE


Sample DescriptionDESCRIPTION: CAM-OR - B-24 12'-22' COMPOSITE

• oFALAnalyst:

SOLIDS

SOLIDS EPA 160.3D. RINELLA-S1EKERMAN Analysis Date: 27-NOV-90 Test

Parameter Result90

Det.

: GAOL

Limit0.

7. 0

1Units

Percent

OPENAnalyst

FLASH


POINT

POINTJR.

- SOLIDS

Parameter

(ASTMAnalysis

D-92Date:

MODIFIED)28-NOV-90

ASTM D-92Test

Result> 180

Det.

: G515.1. 0

Limit UnitsDeqrees F

PH S/S/SAnalyst: D.

PH

SH846-9045RINELLA-SIEKERMAN Analysis Date: 26-NOV-90 Test

Parameter Result6.2

Det.

: G624

Limit0

.0. 0

1Units

Std. Uni

i

its:

CYANIDEi lyst: D

CYANIDE

TOTAL AVAILABLE. RINELLA-SIEKERHAN

SW 7 .3.3.2Analysis Date: 30 -MOV -90 Instrument: AUTO-ANALYZER Test

ParameterBDL

Result Det.: G115.

Limit0.

3. 0 1

5Units i

mq/kq 1

TOTAL AVAILABLEAnalyst: L. DIAZ

INITIAL WEIGHT1 FINAL VOLUME


3.26

4.1-NOV-90 Test: P116.2. 0

ParameterOR VOLUME

Result11.66250


SULFIDE SW846-9030Analyst: L. OlAZ Analysis Date: 26-NOV-90 Test: G110.4. 0 1

Prep: TOTAL AVAILABLE SULFIDE EXTRACTION SW 7.3.4.1 ' iParameter

SULFIDEResult

BDLDet. Limit Units ;

2.1 mq/ka ';

PCB SONICATION EXTRACTION SW846-3550Analyst: C. SARKAM Analysis Date: 29-NOV-90 Test: P231.1. 0

ParameterINITIAL WEIGHT OR VOLUME

i FINAL VOLUME

Result5.33100


Page 1


POLYCHLORINATED BIPHENYLS (PCBS) SW846-8080 jAnalyst: C. SARKAN Analysis Oat*: 03-DEC-90 Irwtruwnt: CC/ECO Ttst: 0301.2. 0 :

I Prep: PCB SONICATION EXTRACTION SW846-3550Parrneter

PCB AROCHLOR 10161 PCB AROCHLOR 12211 PCB AROCHLOR 1232

PCB AROCHLOR 1242 •: .-...-., PCB AROCHLOR 1248

PCB AROCHLOR 1254PCB AROCHLOR 1260PCB AROCHLOR 1262


Oet. Limit1.05.01.01.01.01.01.01.0

Unitsmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmq/kq

1 TOX CHAR LEACHING PROCEDURE (TCLP W/ORG+PEST+HERBS) SW846-1311Analyst: S. HUMAN Analysis Date: 29-NOV-90 Test: P107.2. 0

1 Parameter1 TOTAL SAMPLE WEIGHT

LIQUID FRACTION (GRAMS)EXTRACTED SAMPLE

)LIDS . . : • . : : : , • : : • , • , : , • • : . ::: ' ;.,.... .; .

9.5 MM SIEVE TESTINITIAL PH ; : :ADJUSTED PHBUFFER SOLUTION PH :FINAL PHVOLUME BUFFERED SOLUTIONVOLUME EXTRACT FILTEREDLIQUID FRACTIONTOTAL VOLUME FILTRATEINITIAL TIMEFINAL TIME

Result100090100

5.851.664.924.94180018000180012370.512388.6

Det. Limit UnitsGramsGramsGramsPercentPassedStd. UnitsStd. Units:Std. Units:Std. Units.mLmLmLmLMRSMRS

FAA OR ICP ACID DIGESTION OF LEACHATE SAMPLES SW846-3010Analyst: J. WARE Analysis Date: 05 -DEC -90 Test: P130.8. 0


iNITIAL WEIGHT OR VOLUMEFINAL WEIGHT OR VOLUME •

Result100100


BARIUM FAA (1 POINT MSA) SW846-7080Analyst: S. STRUEU1NG Analysis Date: 06-DEC-90 Instrument: FAAPrep: FAA OR ICP ACID DIGESTION OF LEACHATE SAMPLES SW846-3010Prep: TOX CHAR LEACHING PROCEDURE (TCLP W/ORG+PEST+HERBS) SW846-1311

Test: H604.5. 0

ParameterBARIUMADDITION 1 : • , . . : .SAMPLESAMPLE + ADD 1 ; ;DILUTION

Result0.432.500.432.941

Oct. Limit0.2


Page 2

.EMS HERITAGE LABORATORIES, INC. Lab Sample ID: C126589CADMIUM FAA (1 POINT MSA) SW846-7130Analyst: A. STXKBURGER Analysis Date: 06-DEC-90 Instrunent: FAA T«st: M60«.5. 0


ParameterCADMIUMADDITION 1SAMPLESAMPLE + ADD .1 •:• :.^ZC;^;;-'^--':v •:,DILUTION


Det. Limit0.02

Units 1mg/Lmg/LConeCone

CHROMIUM FAA (1 POINT MSA) SW846-7190 iAnalyst: A. STOCCTURGER Analysis Date: 06-DEC-90 Instrunent: FAA Test: M610.5. 0


ParameterCHROMIUMADDITION 1 :SAMPLE"AMPLE + ADD IOILUTION


Oet. Limit0.05


LEAD FAA (1 POINT MSA) SW846-7420Analyst: A. STOCKBURGER Analysis Date: 06-DEC-90 Instrunent: FAAPrep: FAA OR ICP ACID DIGESTION OF LEACHATE SAMPLES SW846-3010Prep: TOX CHAR LEACHING PROCEDURE (TCLP W/ORG+PEST+HERBS) SW846-1311

Test: H616.5. Q

ParameterLEADADDITION 1SAMPLESAMPLE + ADD 1 ; :DILUTION


Det. Limit0.2

Units

mg/Lmg/LConeCone

SILVER FAA (1 POINT MSA) SW846-7760Analyst: A. STOCKBURGER Analysis Date: 06-DEC-90 Instrunent: FAAPrep: FAA OR ICP ACID DIGESTION OF LEACHATE SAMPLES SW846-3010Prep: TOX CHAR LEACHING PROCEDURE (TCLP W/ORG+PEST+HERBS) SW846-1311

Test: H630.5. 0

ParameterSILVERADDITION i •;:SAMPLESAMPLE + ADD 1DILUTION


Det. Limit0.04


6FAA ACID DIGESTION OF LEACHATE SAMPLES SW846-3020Analyst: J. WARE Analysis Date: OS-DEC-90 Test: P130.9. 0



Result5050

Det. Limit Units

mLmL

Page 3

EHS HERITAGE LABORATORIES, INC. Lab Sample ID: C1265891 ARSENIC GFAA (I POINT NSA) SW846-7060

Analyst: t. KEHOE Analysis Date: 07-OEC-90 Instrument: GFAA Test: H603.6. 0, Prep: GFAA ACID DIGESTION OF LEACHATE SAMPLES SW846-30201 Prep: TOX CHAR LEACHING PROCEDURE (TCLP W/ORG+PEST+HERBS) SW846-1311

ParameterARSENIC

I ADDITION i ;: ?: : :11 SAMPLE

SAMPLE + ADD 'l^t:&^^.-y- .-.-,-.• , , , , • . ; . - , . . • . . . ; • ..;. ,1 DILUTION

Res Jit0.0210.01000.0210.0442

Det. Limit0.010


SELENIUM GFAA (1 POINT MSA) SW846-7740Analyst: K. ICEKO? Analysis Date: 10-OEC-90 Instrunent: CFAA Test: M628.6. 0Prep: GFAA ACID DIGESTION OF LEACHATE SAMPLES SW846-3020

" Prep: TOX CHAR LEACHING PROCEDURE (TCLP W/ORG+PEST+HERBS) SW846-1311Parameter

I SELENIUM"ADDITION r:AM^m^>;y:. : - v:..-; '.:.. ••••••-•''....

SAMPLEH MPLE + ADD i : • ::: ::::>::I uiLUTION

ResultBDL0.01000.0000.00671

Oet. Limit0.005

Un i : smg/Lmg/LConeCone

CVAA ACID DIGESTION OF LEACHATE SAMPLES SW846-7470Analyst: M. SCJtOGHAM Analysis Date: 05-OEC-90 Test: P131.9. 0

11 Prep: TOX CHAR LEACHING PROCEDURE (TCLP W/ORG+PEST+HERBS) SW846-1311Parameter

II INITIAL WEIGHT OR VOLUME11 FINAL VOLUME :

; : : ; :

Result10100

Oct. Limit UnitsmLmL

1 MERCURY CVAA (1 POINT MSA) SW846-7470R Analyst: M. SCROGHAH Analysis Date: 06-DEC-90 Instrument: CVAA Test: K620.6. 0

Prep: CVAA ACID DIGESTION OF LEACHATE SAMPLES SW846-7470Prep: TOX CHAR LEACHING PROCEDURE (TCLP W/ORG+PEST+HERBS) SW846-1311

1 Parameter1 MERCURY

EDITION i . • ; : . •••L:v;Sl?z^ ;• ; . . : '•••••' .\ -1PLEI SAMPLE + ADD i: ::

DILUTION

ResultBDL0.00100-0.0000.001101

Det. Limit0.005


i

| GC/MS SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510Analyst: C. CIESIELSKI Analysis Datt: 30-MOV-90 Test: P233.4. 0

Prep: TOX CHAR LEACHING PROCEDURE (TCLP W/ORG+PEST+HERBS) SW846-13111 Parameter1 INITIAL WEIGHT OR VOLUME

FINAL VOLUME -

Result2001

Det. Limit UnitsmLtnL

TCLP SEMIVOLATILE ORGANICS (TOXICITY CHARACTERISTIC) SW846-8270Analyst: A. BRAOBURN Analysis Date: 02-OEC-90 Instrunent: GC/MS SVOAPrep: GC/MS SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510Prep: TOX CHAR LEACHING PROCEDURE (TCLP W/ORG+PEST+HERBS) SW846-1311

Test: 05H.3. 0

Parameter1.4-DICHLOS08ENZENE2.4-OIHITROTOLUENEHEXACHLORC«ENZENEHEXACHLOROBUTAOIENEHEXACHLOHOETHAME

CorrectedResult

DetectionLimit

50SOSOSO50

Unitsug/Lug/LU9/LU9/Lug/L

ObservedResultBOLBOLBDL80 LBOL


Sample *Spike


Page 4

•vFU ll*_l\A I rÛL •V^WwiX^ 1 V

1Parameter

1 NITROBENZENE

IPYRIDINECRESYL1C ACID2-METHYL PHENOL

1 3-METHYL PHENOL

' 4-METHYLPHENOLPENTACHLOROPHEMOL

I PHENOL '.•• - • • • • '

[ TETRACHLOROPHENOL2.4,5-TRICHLOROPHENOL

, 2,4,6-TRICHLOfiOPHENOL. . . . , - . . . ; , . , . .. :•:-•-..

SURROGATE RECOVERY

2-FLUOROPHENOLPHENOL-05 •.•:'.-,. • • > ; • . . ; . :-;:y- ; '••^•/^•NITROBENZENE-05

FLUOROBIPHENYL.,4,6-TRIBROMOPHENOL

TERPHENYL-D14'Results not corrected

M LJ | 1I1L. •

CorrectedResult

x

for spike

DetectionLimit

50250120120120120250120120120120

recovery.

Unitsug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L


ObservedResult

BOLBDLBOLBOLBOLBOLBOLBDL

BOLBOLBDL

4231&4606275

uai


4 •jaui^r i « i k

Sample *Spike

* • U i cOw97

Mat r i x Spike |X Reccvery |

I

ii1

1ii1i

i

!

i

ii

GC SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510 ;Analyst: B. WOOD Analysis Date: 05-DEC-90 Test: P 233.1. 0 '

Prep: TOX CHAR LEACHING PROCEDURE (TCLP W/ORG+PEST+HERBS) SW846-1311


ParameterOR VOLUME

Result20010

Oct. Limit Units

mLmL

TCLP ORGANOCHLORINE PESTICIDES BY GC:ECD SW846-8080Analyst: J. MOUAT Analysis Date: 11-OEC-90 Instrument: CC/ECOPrep: GC SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510Prep: TOX CHAR LEACHING PROCEDURE (TCLP W/ORG+PEST+HERBS} SW846-1311

Test: 0164.7. 0

ParameterGAMMA-BHC (LINDAME)

HEPTACHLOR : . . . : . :HEPTACHLOR EPOXIOEENORIM . :;:METHOXYCHLOR

CHLOROANE , ..-'-.; ' • . ' "•--.:{:••-.'••.TOXAPHENE

CorrectedResult

DetectionLimit

0.000250.000250.000250.00050.00250.00250.005

Units«g/L•g/Lng/L•g/L•g/L•g/L»g/L

ObservedResult

BOLBOLBOLBOLBOLBOLBOL


Sample +Spike


DIAZOMETHANE HERBICIDE DERIVATIZATION SW846-8150Analyst: L. DOBBINS Analysis Date: 06-DEC-90 Test: P201.4. 0



Result25010

Oct. Linit UnitsmLmL

Page 5

EMS HERITAGE LABORATORIES, INC. Lab Sample ID: C126589TCLP CHLORINATED HERBICIDES SW846-8150Analyst: A. HOAGLANO Analysis Date: 13-DEC-90 Instrument: GC/ECO

Prep: DIAZOHETHANE HERBICIDE DERIVATIZATION SW846-8150Prep: TOX CHAR LEACHING PROCEDURE (TCLP W/ORG+PEST+HERBS) SW846-1311

Test: 0253.7. 0

Parameter2,4-DF.HLOROf'HENOXYAC-:TIC ACIDSILVEX

ResultBDLBDL

Det. Limit0.01

0.001

Unitsmg/Lmq/L

> Greater Than Upper Detection LimitBDL Below Detection Limit

Sample Comments

Quality Assurance Off icer: N Last Page 6


Service Location

EMS HERITAGE LABORATORIES, INC.8205 S. CASS AVE. SUITE 106DARIEN, IL 60559(708)969-9030

Received

21-NOV-90Complete

17-DEC-90Printed

18-DEC-90

Lab ID I

C126593PO Numoer

Sampled

20-NOV-90

Report To


B i l l To

DAMES AND MOORE«


Simple DescriptionDESCRIPTION: CAM-OR - B-25 12.5'-18' COMPOSITE

! .uTAL SOLIDS EPA 160.3Analyst: D. R1NEILA-SIEKERMAN Analysis Date: 27-NOV-90 Test: GA01.7. 0

ParameterSOLIDS

Result89

Det. Limit0.1

Units iPercent •

OPENAnalyst

FLASH


POINT

POINTJR.

- SOLIDS

Parameter

(ASTMAnalysis

D-92Date:

MODIFIED) ASTM D-9228 - HO V- 90 Test

Result> 180

Oct.

: G515.1. 0

Limit UnitsDeqrees F

PH S/S/SAnalyst: 0.

PH

SW846-9045RINELLA-SIEKERMAN Analysis Date: 26-NOV-90 ' Test

Parameter Result6.7

Det.

: G624.

Limit0.

0. 0

1Units

Std. Units

CYANIDE^

lyst: D

CYANIDE

TOTAL. RINELLA

AVAILABLE•SIEKERHAN

SW 7 .3.3.2Analysis Date: 30-NOV-90 Instrument: AUTO-ANALYZER Test

ParameterBDL

Result Det.

: G115.Limit

0.

3. 0

5Units |

ma/ka

1 TOTALAnalyst

AVAILABLE: L. OIAZ

1 INITIAL WEIGHTFINAL VOLUME

SULFIDE

ParanOR VOLUME

EXTRACTION SW 7.. Analysis Date:

Kter

3.4.126-NOV-90 Test: P116.2. 0

Result10.87250


I SULFIDE SW846-9030I Analyst: L. DIAZ Analysis Date: 26-NOV-90

Prep: TOTAL AVAILABLE SULFIDE EXTRACTION SW 7.3.4.1Test: C110.4. 0

1 SULFIDEParameter

BDLResult Det. Limit

2.3Units

ma/ka

PCS SONICATION EXTRACTIONAnalyst: C. SARKAN

SW846-3550Analysis Date: 29-MOV-90 Test: P231.1. 0


Result5.69100

Det. Limit Uni tsGramsmL

Page 1

EMS HERITAGE LABORATORIES, INC. Lab Sample ID: C126S93 :

POLYCHLORINATED BIPHENYLS (PCBS) SW846-8080Analyst: C. SARKAN Analysis Date: 03-DEC-90

Prep: PCB SONICATION EXTRACTION SW846-3550Parameter

PCB AROCHLOR 10161 PCB AROCHLOR 1221 • SKM1 PCB AROCHLOR 1232

PCB AROCHLOR 1 242 '••'mmî ' >• PCB AROCHLOR 1248

PCB AROCHLOR 1254PCB AROCHLOR 1260PCB AROCHLOR 1262 -

Instrument: CC/ECO


Test: 0301.2.

Oct. Limit1.05.01.01.01.01.01.01.0

0

Units jrig/ kg 'mg/kgmg/kg jmg/kgmg/kgmg/kgmg/kgma/ka

TOX CHAR LEACHING PROCEDURE (TCLP W/ORG+PEST+HERBS) SW846-1311Analyst: S. T1LLHAN Analysis Date: 29-NOV-90 Test: P107.2. 0

ParameterTOTAL SAMPLE WEIGHTLIQUID FRACTION (GRAMS)EXTRACTED SAMPLELIDS . ••"••-..:-•• •":•;,;,:•,•,: ' . . • • .

9.5 MM SIEVE TESTINITIAL PH <^"I^m^,' ' , :>:v-. •-.ADJUSTED PHBUFFER SOLUTION PH ! iiFINAL PHVOLUME BUFFERED SOLUTION •VOLUME EXTRACT FILTEREDLIQUID FRACTION ••:--v ^ :>;-::::;y •;:••;> -v:v^,--: •TOTAL VOLUME FILTRATEINITIAL TIME : . ; ; : • : • : : : • ; ;FINAL TIME

Result100090100

7.251.854.925.05180018000180012370.512388.6

Det. Limit UnitsGramsGramsGramsPercentPassedStd. Units!Std. Units;Std. UnitsStd. UnitsmL jmLmLmLHRSHRS

FAA OR ICP ACID DIGESTION OF LEACHATE SAMPLES SW846-3010Analyst: J. WARE Analysis Date: 05-DEC-90 Test: P130.8. 0


1 .HITIAL WEIGHT OR VOLUMEFINAL WEIGHT OR VOLUME

Result100100

Oct. Limit Units

mLmL

BARIUM FAA (1 POINT USA) SW846-7080Analyst: S. STRUEWIMG Analysis Date: W-OEC-90 Instrument: FAA Test: M604.5. 0


ParameterBARIUMADDITION 1 i^ ;SAMPLESAMPLE + ADD 1 . ;DILUTION

Result0.882.500.883.291

Dec. Limit2.0

i


Page 2

EMS HERITAGE LABORATORIES, INC. Lab Sample ID: C126593CADMIUM FAA (1 POINT MSA) SW846-7130Analyst: A. STOCKBURGER Analysis Date: 06-DEC-90 Instrument: FAAPrep: FAA OR ICP ACID DIGESTION OF LEACHATE SAMPLES SW846-3010Prep: TOX CHAR LEACHING PROCEDURE (TCLP W/ORG+PEST+HERBS) SW846-1311

Test: H608.5. 0

ParameterCADMIUM

(ADDITION 1 x1 SAMPLE

SAMPLE + ADD 1 ^: ^: '.i DILUTION


Det. Limit0.02

Units !mg/Lmg/LConeCone

CHROMIUM FAA (1 POINT MSA) SW846-7190Analyst: A. STOCKBURGER Analysis Date: M-DEC-90 Instrument: FAAPrep: FAA OR ICP ACID DIGESTION OF LEACHATE SAMPLES SW846-3010Prep: TOX CHAR LEACHING PROCEDURE (TCLP W/ORG+PEST+HERBS) SW846-1311

Test: H610.5. 0

ParameterII CHROMIUM'I ADDITION 1 ::.";m>v:vV:., - . . . • : .

SAMPLE„ 'AMPLE + ADD I :1! LUTION


Det. Limit0.05


LEAD FAA (1 POINT MSA) SW846-7420Analyst: A. STOCKBURGER Analysis Date: 06-DEC-90 Instrument: FAAPrep: FAA OR ICP ACID DIGESTION OF LEACHATE SAMPLES SW846-3010Prep: TOX CHAR LEACHING PROCEDURE (TCLP W/ORG+PEST+HERBS) SW846-1311

Test: M616.5. 0

ParameterLEAD

SAMPLESAMPLE + ADD 1 : : :DILUTION

Result0.505.000.505.211

Det. Limit0.20

Units 1mg/L !mg/L iCone iCone

SILVER FAA (1 POINT MSA) SW846-7760Analyst: A. STOCKBURGER Analysis Date: 06-OEC-90 Instrunent: FAAPrep: FAA OR ICP ACID DIGESTION OF LEACHATE SAMPLES SW846-3010Prep: TOX CHAR LEACHING PROCEDURE (TCLP W/ORG+PEST+HERBS) SW846-1311

Test: M630.5. 0

—————————————————————————————————————————Parameter

SILVERADDITION l " :M^v":; . / • • ' . . :.:.:•::..: : ; .. .SAMPLESAMPLE + ADD 1 : : : :DILUTION

ResultBOL0.500.000.511

O't. Limit0.04


GFAA ACID DIGESTION OF LEACHATE SAMPLES SW846-3020Analyst: J. WARE : Analysis Date: 05-DEC-90 Test: P130.9. 0



Result5050


Page 3

EMS HERITAGE LABORATORIES, INC. Lab Sample ID: C126593ARSENIC GFAA (I POINT HSA) SW846-7060Analyst: K. KEHOE Analysis Date: 07-DEC-90 Instrument: CFAAPrep: GFAA ACID DIGESTION OF LEACHATE SAMPLES SW846-3020Prep: TOX CHAR LEACHING PROCEDURE (TCLP W/ORG+PEST+HERBS) SW846-1311

Test: M603.6. 0

ParameterARSENIC

1 ADDITION 1 ; V1 SAMPLE

SAMPLE + ADD 1 : v ; -1 DILUTION

Result0.00720.01000.00720.0181

Det. Limit0.005


>.t

i1i

1SELENIUM GFAA (1 POINT MSA) SW846-7740Analyst: K. KEHOE Analysis Date: 10-DEC-90 Instrunent: CFAA Test: M628.6. 0Prep: GFAA ACID DIGESTION OF LEACHATE SAMPLES SW846-3020Prep: TOX CHAR LEACHING PROCEDURE (TCLP W/ORG+PEST+HERBS) SW846-1311

ParameterSELENIUMADDITION 1SAMPLESAMPLE + ADD 1

.LUTION

ResultBDL0.01000.0000.00811

Det. Limit0.005

Units

mg/Lmg/LConeCone

i

ii

I

CVAA ACID DIGESTION OF LEACHATE SAMPLESAnalyst: H. SCROGHAM Analysis Date:

Prep: TOX CHAR LEACHING PROCEDURE (TCLP

SW846-747005-DEC-90W/ORG+PEST+HERBS)

ParameterINITIAL WEIGHT OR VOLUMEFINAL VOLUME : : - : : :;:;: - :: : ; : : -

10100

Test: P131.9. 0SW846-1311

Result Oct. Limit Units ImLmL

MERCURY CVAA (1 POINT MSA) SW846-7470Analyst: H. SCROGHAM : Analysis Date: 06-DEC-90 Instrunent: CVAAPrep: CVAA ACID DIGESTION OF LEACHATE SAMPLES SW846-7470Prep: TOX CHAR LEACHING PROCEDURE (TCLP W/ORG+PEST+HERBS) SW846-1311

Test: K620.6. 0

MERCURYADDITION:!~<\MPLE-AMPLE + ADD 1DILUTION

Parameter ResultBDL0.00100-0.0000.000921

Det. Limit0.005

Units img/L img/L iCone ;Cone |

GC/MS SEPARATORYAnalyst: C. CIESIELSXI

Prep: TOX CHAR


FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510 j: Analysis Date: 03-DEC-90 Test: P233.4. 0 1

LEACHING PROCEDURE (TCLP W/ORG+PEST+HERBS) SW846-1311 !Parameter

VOLUMEResult

2001

Det. Limit Units imL imL :

TCLP SEMIVOLATILE ORGANICS (TOXICITY CHARACTERISTIC) SW846-8270Analyst: A. BRAOBURN Analysis Date: 05-DEC-90 Instrunent: GC/MS SVOAPrep: GC/MS SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510Prep: TOX CHAR LEACHING PROCEDURE (TCLP W/ORG+PEST+HERBS) SW846-1311

Test: 05U.3. 0

Parameter1,4-DICm.OROBENZENE2,4-DIMITROTOUIEMENEXACHLOROBEHZENENEXACHLOROBUTAOtENEHEXACHLOROETHANE

CorrectedResult

DetectionLimit

50SO505050


ObservedResult80 LBOL80 LBOLBDL


Sample »Spike

Mitrix Spike ,X Recovery

:

Page 4

EMS HERITAGE LABORATORIES, INC. Lab Sample ID: C126593 i

ParameterNITROBENZENEOYRIDINEIfESYLIC ACID<!-METHYL PHENOL3-METHYL PHENOLi-METHYLPHENOL'ENTACHLOROPHENOL2,4,5-TRICHLOROPHENOL•>,4.6-TRICHLC*OPHENOL

SURROGATE RECOVERY

2-FLUOROPHENOLPHENOL-D5 ;NITROBENZENE-OS2-FLUOROBIPHENYL2,4,6-TRIBROMOPHENOL' -OHENYL-D14

CorrectedResult

DetectionLimit

50250120120120120250120120

Unitsug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L


ObservedResultBDLBOLBOLBOLBOLBDLBOLBOLBDL

543998816877


Sample »Spike

Matrix Spike |X Recovery

j

'

.esults not corrected for spike recovery.

GC SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510Analyst: B. WOOD Analysis Date: 06-OEC-90 Test: P233.1. 0Prep: TOX CHAR LEACHING PROCEDURE (TCLP W/ORG+PEST+HERBS) SW846-1311


Result20010

Oet. Limit Unitsmlml

TCLP ORGANOCHLORINE PESTICIDES BY GC:ECD SW846-8080Analyst: J. MOWAT Analysis Date: 11-DEC-90 Instrument: GC/ECD Test: 0164.7. 0

, Prep: GC SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510Prep: TOX CHAR LEACHING PROCEDURE (TCLP W/ORG+PEST+HERBS) SW846-1311

ParameterMA-BHC (L1NDANE)

HEPTACHLOR

HEPTACHLOR EPOXIDEENDRINMETHOXYCHLOR

CHLORDANE

TOXAPHENE

CorrectedResult

DetectionLimit

.00025

.00025

.00025.0005.0025.0025

.005

Unitsng/Lng/Lng/L»g/Lng/Lng/Lmg/L

ObservedResult

BOLBOLBOLBDLBOLBOLBDL


Sample »Spike

Matrix SpikeX Recovery :

i

DIAZOHETHANE HERBICIDE DERIVATIZATION SW846-8150Analyst: L. DOBBINS Analysis Dtte: 06-DEC-90

iTest: P201.4. 0



Result25010

Oet. Limit Units

mlml

Page 5

EMS HERITAGE LABORATORIES, INC. Lab Sample ID: C126593TCLP CHLORINATED HERBICIDES SW846-8150Analyst: A. HOAGUND Analysis Date: 13-DEC-90 Instrument: GC/ECOPrep: DIAZOMETHANE HERBICIDE DERIVATIZATION SW846-8150Prep: TOX CHAR LEACHING PROCEDURE (TCLP W/ORG+PEST+HERBS) SW846-1311

Test: 0253.7. 0

P»r«neter2, 4-DICHLO.WPHENOXY ACETIC ACIDSILVEX

ResultBDLBDL

Oct. Limit0.01

0.001

Units 1mg/Lmq/L

> Greater Than Upper Detection LimitBDL Below Detection Limit

S*npl* Comnents

Quality Assurance Officer: < "/. Last Page 6


Service Location Received Lab 10 ;

EMS HERITAGE LABORATORIES, INC. 21-NOV-90 C126587 i8205 S. CASS AVE. SUITE 106 Conplete PO HimwrDARIEN, IL 60559 19-DEC-90 ...............(/UB)9b9-yGjU Printed Sampled

20-DEC-90 20-UOV-90 I

Report To - Bill To

DAMES AND MOORE DAMES AND MOORECHARLIE BEST1550 NORTHWEST HIGHWAY 1550 NW HIGHWAY, SUITE 220PARK RIDGE, IL 60068 PARK RIDGE, IL 60068

1 Sample DescriptionDESCRIPTION: CAM-OR - B-24 5.5 ' -6 .0 '

7ERO HEADSPACE EXTRACTION (TCLP) SW846-1311.talyst: G. EOUAROS Analysis Date: 03-DEC-90 Test: P108.1. 0

Parameter Result Oct. LimitTOTAL SAMPLE WEIGHT 25.04

1 LIQUID PORTIONLIQUID FRACTION (GRAMS)

1 EXTRACTED SAMPLE 25.041 9.5 MM SIEVE TEST

> .5% SOLIDSI INITIAL PH| ADJUSTED PH :

BUFFER SOLUTION PH 4.96VOLUME BUFFERED SOLUTION 500

1 VOLUME EXTRACT FILTERED 801 TOTAL VOLUME FILTRATE 80

INITIAL TIME 4021.61 FINAL TIME 4039.1 -

UnitsGramsmLGrams iGramsPassedPercentStd. UnitsStd. Units;Std. Units;mLmLmLHoursHours

TCLP VOLATILE ORGANICS (TOXICITY CHARACTERISTIC) SW846-8240Analyst: S. SHARP Analysis Date: U-OEC-90 Instrument: GC/MS VGA Test: 0513.3. 0

Corrected Detection Observed Matrix Spike Sample *Parameter Result Limit Units Result True Value Spike

BENZENE 50 ug/L 66CARBON TETRACHLOR IDE :: 50 ug/L BOLCML0808EHZENE 50 ug/L BOLCHLOROFORM 50 ug/L BOL1.2-DICMLOROETNANE 50 ug/L BOLM-OICHLOROETHYLENE 50 ug/L BOLMETHYL ETHYL KETONE 100 ug/L BOLTETRACHIOR06THYLENE 50 ug/L EST 25TRICHLOROETKYLENE 50 ug/L EST 33VINYL CHLORIDE 100 ug/L BOL

SURROGATE RECOVERY

OICHLOROETHANE-D4 X Rec 102TOLUENE-08 X Rec 109

.MpMOFLUOHOBENZENE X Rec 99


Page 1

1

i

, EMS HERITAGE LABORATORIES, INC. Lab Sample ID: C126587*Satnple results are not corrected for spike recovery.

Sample GarmentsBDL Below Detection LimitEST Estimated Value

-. CO,Quality Assurance Officer: ( •VA /. U :Li >LJL. v^\w/-. ^ Last Page 2t *


Service Location

EMS HERITAGE LABORATORIES, INC.8205 S. CASS AVE. SUITE 106IARIEN, IL 60559.708)969-9030

Received Lab ID

21-NOV-90 C126590Complete PO Number

19-DEC-90 ....................Printed Sampled

20-DEC-90 20-NOV-90

Report To


Bill To

DAMES AND MOORE


Simple DescriptionDESCRIPTION: CAM-OR - B-25 3.5'-4.0'

' ^0 HEADSPACE EXTRACTION (TCLP) SW846-1311<. -,yst: C. EDWARDS Analysis Date: 04-OEC-90

ParameterTOTAL SAMPLE WEIGHT

IQUID PORTIONIQUID FRACTION (GRAMS)

EXTRACTED SAMPLE".5 MM SIEVE TEST

.5% SOLIDSINITIAL PHADJUSTED PH

UFFER SOLUTION PH,OLUME BUFFERED SOLUTIONVOLUME EXTRACT FILTERED

OTAL. VOLUME FILTRATENITIAL TIME

FINAL TIME

Test: P108.1. 0

Result Oct. Limit24.89

24.89

4.95£00 .80804039.14056.8

UnitsGramsmLGramsGramsPassedPercentStd. UnitsStd. UnitsStd. UnitsmLmLmLHoursHours

TCLP VOLATILE ORGANICS (TOXICITY CHARACTERISTIC) SW846-8240Analyst: S. SHARP Analysis Date: U-DEC-90 Instrument: CC/MS VOA Test: 0513.3. 0

Prep: ZERO HEADSPACE EXTRACTION (TCLP) SW846-1311Corrected

Parameter ResultBENZENE

ARBOM TETRACHLORIDEHIOROBENZEME

CHLOROFORM',2-DICHLOROETHANE

,1-DICHLOROETHYLENEMETHYL ETHYL KETONETETBACHLOROETHYLENE

RICHLOROETHYLENE

.1NYL CHLORIDE

URROGATE RECOVERY

OICHLOROETHANE-04

' TOLUENE-D8

Detection Observed Matrix Spike Sample »Limit Units Result True Value Spike

50 ug/L 80 L50 ug/L 10 L50 ug/L BO ISO ug/L BOLSO ug/L BDL50 ug/L BOL

100 ug/L BOL50 vg/L BOL50 ug/L BOL

100 ug/L BOL

X Rec 110X Rec 111


Page 1

'EMS HERITAGE LABORATORIES, INC. Lab Sample ID: C126590Corrected

Parameter ResultBROMOFIUOROBENZEME

DetectionLimit Units

X Rec

ObservedResult

99


Sample *Spike

——— • —————— i 'Matrix SpikeX Recovery

*Sample results are not corrected for spike recovery.

BDL Below Detection Limit -Sanpl* Carmen ts

Quality Assurance Off icer: .s 8 Last Page 2


Service Location

EMS HERITAGE LABORATORIES, INC.8205 S. CASS AVE. SUITE 106DARIEN, IL 60559(703)969-9030

Received

21-NOV-90Complete

19-DEC-90Printed

20-OEC-90

Lab ID

C126592PO Mincer

Sampled

20-NOV-90

Report To


Bill To

DAMES AND MOORE


DESCRIPTION: CAM-OR - B-25Sample Description

12.5'-13.0'

7ERO HEADSPACE EXTRACTION (TCLP) SW846-1311analyst: C. EDUAROS Analysis Date: 04-DEC-90

ParameterTOTAL SAMPLE WEIGHTLIQUID PORTIONLIQUID FRACTION (GRAMS)EXTRACTED SAMPLE9.5 MM SIEVE TEST> .5% SOLIDSINITIAL PHADJUSTED PHBUFFER SOLUTION PHVOLUME BUFFERED SOLUTIONVOLUME EXTRACT FILTEREDTOTAL VOLUME FILTRATEINITIAL TIMEFINAL TIME

Result24.99

24.99

4.9550080804039.14056.8

Test: P108.1.

Det. Limit

0

UnitsGrams !mL !GramsGramsPassedPercentStd. UnitsStd. UnitsStd. UnitsmLmLmLHoursHours

TCLP VOLATILE ORGANICS (TOXICITY CHARACTERISTIC) SW846-8240Analyst: S. SHARP Analysis Date: K-OEC-90 Instrument: GC/HS VOAPrep: ZERO HEADSPACE EXTRACTION (TCLP) SW846-1311

Test: 0513.3. 0

ParameterBENZENECARBON TETRACHLORIOECHLOftOBENZENECHLOROFORM1,2-DICHLOKOETHANE1,1-OICHLOROETHTLENEHETHYl ETHYL KETONETETRACHLOROETHYLEWETRICHLOROETHYLENEVIMTL CHLORIDE

SURROGATE RECOVERY

OICHLOROETHANE-DtTOLUENE-08

CorrectedResult

DetectionLimit

50505050505010050SO100

Unitsug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L

X Rec1 Rec

ObservedResultBOLBDLBOLBDLBDLBDLBOLEST 26BOLBOL

9998


Sample *Spike


Page 1

IMS HERITAGE LABORATORIES, INC. Lab Sample ID: C126592

ParameterICMOFLUOR08ENZENE

CorrectedResult

DetectionLimit Units

X Rec

ObservedResult

105


Sample »Spike

Hatru spike ,X Recovery i

1;

*Sample results are not corrected for spike recovery. ;

IDL BeToH Detection Limit:ST Estimated Value

Sample Comments

Quality Assurance Officer: ^ Last Page 2


Service LocationEMS HERITAGE LABORATORIES, INC.8205 S. CASS AVE. SUITE 106DARIEN, II. 60559(708)969-9030

Received21-NOV-90

Complete17-DEC-9J

Printed18-DEC-90

Lab 10

C126591PO Number

Samplet20-NOV-90

Report To


B i l l To

DAMES AND MOORE


DescriptionDESCRIPTION: CAM-OR - B-25 2'-12' COMPOSITE

^TAL. -*lyst:

SOLIDS

SOLIDS EPA 160.D. RINELLA-SIEKERMAN

3Analysis Date: 27-NOV-90 Test

Parameter Result89

Det.

: C401.

Limit0.

7. 0

1Units

Percent

OPEN CUP FLASHAnalyst: F. FLORES,

FLASH POINT

POINTJR.

- SOLIDS

Parameter

(ASTMAnalysis

D-92Date:

MODIFIED)28-NOV-90

ASTM D-92Test

Result> 180

Det.

: G515.1. 0

Limit UnitsDegrees F

PH S/S/S SW846-9045Analyst: 0. RINELLA-SIEICERHAN Analysis Date: 26-NOV-90 Test: C624.0. 0

ParameterPH

Result5.4

Det. Limit0.1

UnitsStd. Unitsi

CYANIDE TOTAL AVAILABLE SWAnalyst: 0. RINELLA-SIEKERHAM

7.3.3.2Analysis Date: 30-NOV-90 Instrument: AUTO-ANALYZER Test: G115.3. 0

ParameterCYANIDE BDL

Result Det. Limit0.5

Unitsmg/ka

1 TOTALAnalyst:

AVAILABLEL. DIAZ

1 INITIAL WEIGHT ORFINAL VOLUME


3.26

4.1•NOV-90 Test: P116.2. 0

ParameterVOLUME

Result10.31250


SULFIDE SW846-9030Analyst: L. DIAZ

Prep:

SULFIDE

TOTAL AVAILABLEPan

Analysis Data: 26SULFIDE EXTRACTION

meter

-NOV-90 Test: G110.SW 7.3.4.1

ResultBDL

Det. Limit2.

4.

4

0

Unitsma/ka

PCS SONICATIONAnalyst: C. SARKAN


EXTRACTION SW846-3550Analysis Date: 29-NOV-90 Test: P231.1. 0

ParameterOR VOLUME

Result5.32100

Det. Limit Units

GramsmL

Page 1


POLYCHLORINATED BIPHENYLS (PCBS) SW846-8080Analyst: C. SARKAN Analysis D»t«: 03-DEC-90 Instrument: CC/ECD Test: 0301.2. 0

Prep: PCB SONICATION EXTRACTION SW846-3550 jParameter

PCB AROCHLOR 1016PCB AROCHLOR 1221 , ;;;PCB AROCHLOR 1232PCB AROCHLOR 1242 -^^L :.;. ;MS&.rPCB AROCHLOR 1248PCB AROCHLOR 1254PCB AROCHLOR 1260PCB AROCHLOR 1262 ::


Oct. Limit1.05.01.0; i.o1.01.01.01.0

Units :

mg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmq/kq

TOX CHAR LEACHING PROCEDURE (TCLP W/ORG+PEST+HERBS) SW846-1311Analyst: S. TILLHAN Analysis Date: 29 -MOV -90 Test: P107.2. 0

ParameterTOTAL SAMPLE WEIGHTLIQUID FRACTION (GRAMS)EXTRACTED SAMPLE

OLIOS' ' ' -:V:::>"vX,V;;ê^n;/:"-.:-'^:- '9.5 MM SIEVE TESTINITIAL- PH •M:-.-;mx:m-^':i;^ •• • •:• •-ADJUSTED PHBUFFER SOLUTION PH xFINAL PHVOLUME BUFFERED SOLUTIONVOLUME EXTRACT FILTEREDLIQUID FRACTION i

-TOTAL VOLUME FILTRATEINITIAL TIME. ,::v^ ::;;;.:;. ;:-.;FINAL TIME

Result100090100

5.641.674.924.89180018000180012370.512388.6

Det. Limit UnitsGramsGramsGramsPercentPassedStd. UnitsStd. UnitsStd. Units:Std. Units;mLmLmLmlHRS ;HRS

FAA OR ICP ACID DIGESTION OF LEACHATE SAMPLES SW846-3010Analyst: J. WARE Analysis Date: 05-DEC-90 Test: P130.8. 0


, INITIAL WEIGHT OR VOLUMEFINAL WEIGHT OR VOLUME : ; .

Result100100


BARIUM FAA (1 POINT MSA) SW846-7080Analyst: S. STRUEUIMC Analysis Date: 06-OEC-90 Instrunent: FAAPrep: FAA OR ICP ACID DIGESTION OF LEACHATE SAMPLES SW846-3010Prep: TOX CHAR LEACHING PROCEDURE (TCLP W/ORG+PEST-rHERBS) SW846-1311

Test: K604.5. 0

ParameterBARIUMADDITION 1 •••^'••^:-^^m-^ •::••:.••'. ••• '"•'•• ' .SAMPLESAMPLE + ADD 1 •- -^':^ '^, -••',•DILUTION

Result2.52.502.504.911

Det. Limit0.2

\

Unitsmg/Lmg/LConeCone '

1

Page 2

EMS HERITAGE LABORATORIES, INC. Lab Sample ID: C126591CADMIUM FAA (1 POINT MSA) SW846-7130Analyst: A. STOCKBURGER Analytic Oat*: OA-DEC-90 Instrument: FAA Tttt: M608.5. 0


ParameterCADMIUMADDITION i : : : ; : : : ; : ; > : : .SAMPLESAMPLE' -r ADD 'l::-.7^Mmm.:-'^ ,'::..., -A. • '••• 'DILUTION


Oct. Limit0.02

Units

nig/1.mg/LConeCone

i

ii'i

)iii

CHROMIUM FAA (1 POINT MSA) SW846-7190Analyst: A. STOCKBURGER Analysis Date: 06-DEC-90 Instrunent: FAA Test: H610.5. 0


ParameterCHROMIUMADDITION i : : •..•'.: :7£:^J- : •SAMPLESAMPLE + ADD 1 : ::

1LUTION


Oct. Limit0.05

Units

mg/Lmg/LConeCone

LEAD FAA (1 POINT MSA) SW846-7420Analyst: A. STOCKBURGER Analysis Date: 06-OEC-90 Instrunent: FAAPrep: FAA OR ICP ACID DIGESTION OF LEACHATE SAMPLES SW846-3010Prep: TOX CHAR LEACHING PROCEDURE (TCLP W/ORG+PEST+HERBS) SW846-1311

Test: H616.5. 0

. ParameterLEADADDITION 1 : :SAMPLESAMPLE + ADD 1 :DILUTION

Result8.95.000.896.0210

Oct. Limit2.0


SILVER FAA (1 POINT MSA) SW846-7760Analyst: A. STOCKBURGER Analysis Date: 06-DEC-90 Instrument: FAA Test: M630.S. 0


ParameterSILVERADDITION 1 ••V^^^:^;^^^;;>;;^;;-;;-:: ,^{- •• • :•• • '.SAMPLESAMPLE + ADDT:V:vr:::^:^^^^DILUTION


Det. Limit0.04

Units !mg/L ' img/L |Cone jCone !

GFAA ACID DIGESTION OF LEACHATE SAMPLES SW846-3020 !Analyst: J. WARE Analysis Date: 05-OEC-90 Test: P130.9. 0

Prep: TOX CHAR LEACHING PROCEDURE (TCLP W/ORG+PEST+HERBS) SW846-1311 '<Parameter


Result5050

Oct. Limit Units

mLml ;

Page 3

EMS HERITAGE LABORATORIES, INC. Lab Sample ID: C126591ARSENIC GFAA (1 POINT HSA) SW846-7060 ]Analyst: K. KHOE Analysis Oatt: 07-DEC-90 Instrunent: GFAA Ttst: M603.6. 0

, Prep: GFAA ACID DIGESTION OF LEACHATE SAMPLES SW846-30201 Prep: TOX CHAR LEACHING PROCEDURE (TCLP W/ORG+PEST+HERBS) SW846-1311

ParameterARSENICADDITION l-^ÎPm^.'" V^.V;;::V^ • • • • • .SAMPLESAMPLE'"*'1 ADD 1 ; l. S • : ••:. . : : " ... .: '.'..'. ..••/• ••-,'.. '; •••• : • • ; : .DILUTION

Resulto.on0.01000.0140.0241

Det. Limit0.005

Units img/Lmg/LConeCone

SELENIUM GFAA (1 POINT MSA) SW846-7740Analyst: 1. KEHOE Analysis Date: 10-OEC-90 Instrunent: GFAA Test : H628.6. 0

Prep: GFAA ACID DIGESTION OF LEACHATE SAMPLES SW846-3020Prep: TOX CHAR LEACHING PROCEDURE (TCLP W/ORG+PEST+HERBS) SW846-1311

ParameterSELENIUMADDITION 1 •:': ^1:I;;-;'V v ' : • • • ; • • > , : V;:::;SAMPLESAMPLE + ADD 1 -^^î.:/:''.

ILUTION

ResultBDL0.01000.0000.00641

Det. Limit0.005


CVAA ACID DIGESTION OF LEACHATE SAMPLES SW846-7470 IAnalyst: M. SCROGHAM Analysis Date: 05-DEC-90 Test: P131.9. 0 iPrep: TOX CHAR LEACHING PROCEDURE (TCLP W/ORG+PEST+HERBS) SW846-1311 I


10100

Result Det. Limit Units ;mL |mL '.

Instrument: CVAAMERCURY CVAA (1 POINT MSA) SW846-7470Analyst: H. SCROGHAM Analysis Date: 06-OEC-90Prep: CVAA ACID DIGESTION OF LEACHATE SAMPLES SW846-7470Prep: TOX CHAR LEACHING PROCEDURE (TCLP W/ORG+PEST+HERBS) SW846-1311

Test: M62Q.6. 0

MERCURYADDITION i:^::i:;s:SAMPLESAMPLE + ADD 1 . -

Parameter

DILUTION

ResultBDL0.0000-0.0000.000951

Det. Limit0.005


GC/MS SEPARATORYAnalyst: C. CIESIELSKI

Prep: TOX CHAR


FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510::'-;• Analysis Date: 03-DEC-9Q Test: P233.4. 0

LEACHING PROCEDURE (TCLP W/ORG+PEST+HERBS) SW846-1311Parameter

VOLUMEResult

2001


TCLP SEMIVOLATILE ORGANICS (TOXICITY CHARACTERISTIC) SW846-8270Analyst: A. IRAD8URN Analysis Date: OS-OEC-90 Instrunent: GC/MS SVGAPrep: GC/MS SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510Prep: TOX CHAR LEACHING PROCEDURE (TCLP W/ORG+PEST+HERBS) SW846-1311

Test: 05U.3. 0

Parameter1.&-DICHLOROBEN2ENE2.4-DIMITROTOLUENEHEXACHLOROBEMZENEHEXACHLOR08UTADIEMEHEXACHLOROETHAME

CorrectedResult

DetectionLimit

500SOO500500500


ObservedResultBOLBOLBOLBOLBDL


Sample *Spike

Matrix SpueX Recovery

Page 4


ParameterNITROBENZENEPYR1DINECRESYLIC ACID2-METHYL PHENOL3-METHYL PHENOL4-METHYLPHENOLPENTACHLOROPHENOL2,4,5-TRlCHLOROPHENOL2.4,6-TRICHLOROPHENOL

SURROGATE RECOVERY

2-FLUOROPHENOLPHENOL-D5NITROBENZENE-052-FLUOROBIPHENYL :• : :2,4,6-TRlBROMOPHENOLT<;RPHEHYL-OU

CorrectedResult

' . " " . .

DetectionLimit

500250012001200120012002500

.12001200

Unitsug/Lug/Lug/LU9/Lug/LU9/Lug/Lug/Lug/L


ObservedResultBOLIOLBOLBtLBOLBOLBOI-BOLBOL

••**•• .


Sample *Spike

Matrix spikeX Recovery '.

I

Surrogates diluted out. Dilution necessary due to matrix of sample.*Results not corrected for spike recovery.

GC SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510Analyst: B. WOOD Analysis Date: 05-DEC-90Prep: TOX CHAR LEACHING PROCEDURE (TCLP W/ORG+PEST+HERBS) SW846-1311

Test: P233.1. 0


Result20010


TCLP ORGANOCHLORINE PESTICIDES BY GC:ECD SW846-8080Analyst: J. MOWAT Analysis Date: 11-DEC-90 Inscrument: GC/ECOPrep: GC SEPARATORY FUNNEL LIQUID-LIQUID EXTRACTION SW846-3510Prep: TOX CHAR LEACHING PROCEDURE (TCLP W/ORG+PEST+HERBS) SW846-1311

Test: 0164.7. 0

ParameterGAMMA- BMC (L1NDANE)HEPTACHLOR : ^ . ,'"..:....:"...HEPTACHLOR EPOXIDEEHORIN - •• . . • : • • , ; - • ' • • • •••::'•:•':.METHOXYCHLORCHLOROAHE : ; .: : :TOXAPHENE

CorrectedResult

DetectionLimit

.00025

.00025

.00025.:;;;,, .0005

.0025••'::LI:.0025

.005

Units•g/L•9/Lmg/L•g/L«g/L•g/L .mg/L

ObservedResult

BOLBOLBOLBOLBOLBOLBOL


Sample +Spike


DIAZOMETHANE HERBICIDE DERIVATIZATION SH846-8150Analyst: L. DOBBINS Analysis Date: 06-DEC-90 Test: P201.4. 0



Result25010

Oct. Limit UnitsmLml

Page 5

EMS HERITAGE LABORATORIES, INC. Lab Sample ID: C126591TCLP CHLORINATED HERBICIDES SW846-8150Analyst: A. HOAGUKD An»lysil 0»te: 13-OEC-90 Instruct: CC/ECOPrep: DIAZOMETHANE HERBICIDE DERIVATIZATION SW846-8150Prep: TOX CHAR LEACHING PROCEDURE (TCLP W/ORG+PEST+HERBS) SW846-1311

Test: 0253.7. 0

Par— «, 2,4-DICHLOROPHENOXYACETIC

SILVEX

terACID

Resul tBDLBDL

Det LimitO.Oi

0.001

Unitsmg/Lmq/L

* 5ee Hote for Parameter> Greater Than Upper Detection LimitBDL Below Detection Limit

Sample Comments

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