JOL Mr. Fred Lindeman Director, Power Plant Construction Interstate Power Company 1000 Main Street P.O. Box. 769 Dubuque, Iowa 52004-0769 Dear Mr. Lindeman: I99/ RE: Mason City Coal Gas Site, Mason City, Iowa Enclosed is the Data Transmittal of split samples for ground water sampling activities conducted at the Mason City Coal Gas site during May 1997. This information is forwarded to you in accordance with provisions of Section 3007 (a) of the Resource Conservation and Recovery Act (RCRA) of 1980, as amended, and Section 104 (e) of the Comprehensive Environmental Response, Compensation and Liability Act (CERCLA) of 1980, as amended. If you have any questions or comments, you may contact me (913) 551-7746. at Sincerely, Diana L. Engeman Remedial Project Manager Iowa/Nebraska Remedial Branch Superfund Division Enclosure cc: Johanshir Golchin, Iowa Department of Natural Resources Randy Kroneman, Montgomery Watson SUPR:IANE:Engeman:dulmer G:\user\share\iane\datagw2.mc 7/31/97 IANE IANE • '; Engeman Curt is ,-, .............. . \n/\ i_^^^" " ~~—— "••mil HIM S00105885 SUPERFUND RECORDS 7?
Transcript
JOL
Mr. Fred LindemanDirector, Power Plant ConstructionInterstate Power Company1000 Main StreetP.O. Box. 769Dubuque, Iowa 52004-0769
Dear Mr. Lindeman:
I99/
RE: Mason City Coal Gas Site, Mason City, Iowa
Enclosed is the Data Transmittal of split samples for groundwater sampling activities conducted at the Mason City Coal Gassite during May 1997. This information is forwarded to you inaccordance with provisions of Section 3007 (a) of the ResourceConservation and Recovery Act (RCRA) of 1980, as amended, andSection 104 (e) of the Comprehensive Environmental Response,Compensation and Liability Act (CERCLA) of 1980, as amended.
If you have any questions or comments, you may contact me(913) 551-7746.
at
Sincerely,
Diana L. EngemanRemedial Project ManagerIowa/Nebraska Remedial BranchSuperfund Division
Enclosure
cc: Johanshir Golchin, Iowa Department of Natural ResourcesRandy Kroneman, Montgomery Watson
Mr. Fred Lindemar.Director, Power Plant ConstructionInterstate Power Company1000 Main StreetP.O. Box 769Dubuque, Iowa 52004-0769
Dear Mr. Lindeman:
RE: Mason City Coal Gas Site, Mason City, Iowa
Enclosed is the Data Transmittal of split samples for groundwater sampling activities conducted at the Mason City Coal Gassite during May 1997. This information is forwarded to you inaccordance with provisions of Section 3007 (a) of the ResourceConservation and Recovery Act (RCRA) of 1980, as amended, andSection 104 (e) of the Comprehensive Environmental Response,Compensation and Liability Act (CERCLA) of 1980, as amended.
If you have any questions or comments, you may contact me at(913) 551-7746.
Sincerely,
J&J-
Diana L. EngemjanRemedial Project ManagerIowa/Nebraska Remedial BranchSuperfund Division
Enclosure
cc: Johanshir Golchin, Iowa Department of Natural ResourcesRandy Kroneman, Montgomery Watson
RECYCLE
.aez, UNITED S T A T E S ENVIRONMENTAL PROTECTION AGENCYREGION '
:' FUNSTCN ROADK A N S A S C I T Y ^ A N S A S 6
DATE: JUL .-*•>' 1997
SUBJECT: Data Transmittal for Activity #:Site Description: \~\ &
FROM: Andrea Jirka, Program Manager JRegional Laboratory, Environmental/ S^r/vices Division
TO:f
Attached is the data transmittal for the above-referenced
site. The data contained in this transmittal have been
approved by the Regional Laboratory. This should be considered a
____ Partial or /K Complete data transmittal (completes
1 1 °\transmittal of Tne Project Leader should notify
the Regional Laboratory with 14 days of any changes in the LAST
analytical database. If you have any questions, comments, or
data changes, please contact Dee Simmons at 551-5129.
Attachment
cc: Analytical Data File
RECYCLE
DRAFT FIELD SHEETU.S. ENVIRONMENTAL PROTECTION AGENCY, REGION VII
ACTIVITY DES: MASON CITY COAL GAS REF LATITUDE: _ _LOCATION: MASON CITY IA PROJECT NUM: L30 PT: LONGITUDE:
SAMPLE DES: EXISTING SHALLOW MONITORING WELL MW-19 DATE TIME FROM REF PTLOCATION: PHa <m Q.4-sy IA BEG: 5 /& II/77o'i^p EAST:: met'CASE/BATCH/SMO:STORET/AIRS NO:
JIT.
ANALYSIS REQUESTED:CONTAINER PRESERVATIVE
1 L CUBITAINER 1:1 HN03
LAB:
MGPW47W15W15WM30
END:DOWN:
NAMEBTEX (LDL)PAHS BY HPLCPAHS BY HPLCLEAD, TOTAL, BY AA
COMMENTS: FOR SUPERFUND ONLY
S..w-O4 t
SUBSITE IDENTIFIER: OPERABLE UNIT;
(CLM
G ,
f
O."7
H r
Q
SAMPLE COLLECTED BY : *<v
DRAFT FIELD SHEETU.S. ENVIRONMENTAL PROTECTION AGENCY, REGION VII
\CTIVITY DES: MASON CITY COAL GAS REF LATITUDE: _ _^OCATION: MASON CITY IA PROJECT NUM: L30 PT: LONGITUDE:
SAMPLE DES: EXISTING JDEEP MONITORING WELL MW-25OCATION: H Cf .- TTN ,- S IA BEG:
/ /' LAB: __ END:CASE/BATCH/SMO;STORET/AIRS NO:
DATE TIME FROM REF PT7 _|b :t/£' EAST: ___
/5e/9J L : 3 NORTH: ___DOWN:
.ANALYSIS REQUESTED:CONTAINER PRESERVATIVE
1 L CUBITAINER 1:1 HN03
MGP NAMEW47 BTEX (LDL)W15 PAHS BY HPLCW15 PAHS BY HPLCWM30 LEAD, TOTAL, BY AA
COMMENTS: FOR SUPERFUND ONLY: SUBSITE IDENTIFIER: OPERABLE UNIT:
m VX
u
SAMPLE COLLECTED BY
CHAIN OF CUSTODY RECORDENVIRONMENTAL PROTECTION AGENCY REGION VII
>CIJVITK.
NAME OF SURVEY OR ACTIVITY DATE QF
DAYIPION<n
WONTH vEAR Of
CONTENTS OF SHIPMENT
SAMPLENUMBER
vn» Sf •1 vi»i$ (
SfMABKS O'MfR icond'tioi o' umcx« upon tfcno'
jtrier si^aie -lumcws f'c i
7-
7-777
-ool £
-oo 1 '
-f-T
^
^F
XLtiil
\\
\
DESCRIPTION OF SHIPMENT MODE OF SHIPMENT
C E ' S ' f/)MSlST:V, , / •
CHEST S. ;,IMER _
:z:COMMERCIAL CARRIER
SAMPLER C O N V E Y E D
^
(SHIPPING DOCUVENT NjMBE«
PERSONNEL C ' J S T O D Y R E C O R DBY
SEALED UNSE •XL ED |—
TIME RECEIVED BY
SEALED
•>(9
UNSE^-ED ["
REASON FOR CHANC.f OF CUSTODY
RELINUUISHf D BY D A T E TIME
~~1 SEALED JNSEALED|
RECEIVED BY
[SEALED
I C1CJ V
UNSEALEDRELINQUISHED BY
' f PA
DATE TIME RECEIVED BY REASON FOR CHANGE OF CUS1
UNSEAL! D "[SEALED UNSEALED^
E N G E R M A N , D I A N A
A N A L Y S I S REQUEST REPORT
FOR A C T I V I T Y : BS26B
07/28/97 17:24:55
V A L I D A T E D D A T A
A L L R E A L S A M P L E S A N D F I E L D O . C .
* FINAL REPORT
FY: 97 A C T I V I T Y : BS26E DESCRIPTION: MASON CITY COAL GAS LOCATION: MASON CITY
STATUS: ACTIVE TYPE: SAMPLING - IN HOUSE ANALYSIS PROJECT:
LABO DUE DATE IS 6/21/S7. REPORT DUE D A T E IS 7/20/97.
INSPECTION DATE: 5/21/97 ALL SAMPLES R E C E I V E D DATE: 05/22/97
ALL DATA APPROVED BY LAEO DATE: 07/25/97 F I N A L REPORT TRANSMITTED DATE: 07/28/97
E X P E C T E D LABO T U R N A R O U N D T I M E IS 30 DAYS E X P E C T E D REPORT T U R N A R O U N D T I M E IS 60 DAYS
A C T U A L LABO TURNAROUND T I M E IS 64 DAYS A C T U A L REPORT TURNAROUND TIME IS 68 DAYS
SITE CODE: 6B SITE: COAL G A S I F I C A T I O N PLANT SITE
10UA
L30
AIRS/SAMP .NO. QCC M
001002002003004005
CESCRIPTION
EXISTING I N T E R M E D I A T E ZONE WELL MU-10EXISTING SHA1LOU MONITORING UELL MU-19 1DUPLICATE OF BS26B-002F I E L D / T R I P B I A N KE X I S T I N G SHAILOU MONITORING UELL MU23REXIST I N G DEEP MONITORING UELL HU-25
SAMPLE aSTATUS
10-19
23R
111111
MASONMASONMASONMASONMASONMASON
CITY
CITYCITYCITYCITYCITYCITY
STORET LAY- BEG.STATE LOC NO SECT ER DATE
IOUAIOWAIOUAIOUAIOUAIOUA
05/21/9705/21/9705/21/9705/19/9705/21/9705/20/97
BEG.TIME
110909
0818
:12:20:20
•31:45
END .DATE
05/21/9705/21/9705/21/97
/ /05/21/9705/20/97
END .T I M E
1 10909:
08^18:
:29:42:42
: 48: 49
E X P L A N A T I O N OF CODES AND I N F O R M A T I O N ON ANALYSIS REQUEST D E T A I L REPORT
S A M P L E I N F O R M A T I O N :
SAMP. NO.
QCC
SAHPLE I D E N T I F I C A T I O N NUMBER (A 3-DIGIT NUMBERWHICH IN COMBINATION WITH THE ACTIVITY NUMBERAND QCC, PRO V I D E S AN UNIQUE N U M B E R FOR EACH SAMPLEFOI 1 D E N T I I I CATION PURPOSES)QUALITY CONTROL CODE (A ONE-LETTER CODE USED TOD E S I G N A T E S P E C I F I C Q C S A M P L E S . THIS F I E L D U I L L B EBLANK FOR ALL NON-OC Of) A C T U A L SAMPLES):BDFGHKLMNPRSTUYZ123A567M E D I A
CAL I N C R E A S E D C O N C E N T R A T I O N FOR A LAB S P I K E D DUP S A M P L EM E A S U R E D V A L U E F O R F I E L D D U P L I C A T E S A M P L EM E A S U R E D V A L U E F O R F I E L D B L A N KM E A S U R E D V A L U E F O R METHOD S T A N D A R DT R U E V A L U E F O R M E T H O D S T A N D A R DC A L I N C R E A S E D C O N C E N T R A T I O N F O R F I E L D S P I K E D D U P S A M P L EM E A S U R E D V A L U E F O R A L A B D U P L I C A T E S A M P L EM E A S U R E D V A L U E F O R L A B B L A N KM E A S U R E D CONCENTRATION OF F I E L D SPIKED DUPLICATEM E A S U R E D VALUE FOR P E R F O R M A N C E STANDARDC A L I N C R E A S E D C O N C E N T R A T I O N R E S U L T I N G F R O M L A B SPIKEM E A S U R E D CONCENTRATION OF LAB SPIKED SAMPLETRUE V / L U E OF P E R F O R M A N C E S T A N D A R DM E A S U R I D C O N C E N T R A T I O N OF LAB SPIKED D U P L I C A T EM E A S U R I D C O N C E N T R A T I O N OF F I E L D SPIKED SAMPLECAL I N I R E A S E D C O N C E N T R A T I O N R E S U L T I N G FROM FIELD SPIKEM E A S U R I D V A L U E O F F I R S T S P I K E D R E P L I C A T E
SECOND SPIKED R E P L I C A T ETHIRD SPIKED R E P L I C A T EFOURTH SPIKED REPLICATEF I F T H S P I K E D R E P L I C A T E
M E A S U R E D VALUE OF SIXTH SPIKED REPLICATEM E A S U R E D VALUE OF SEVENTH SPIKED REPLICATE
(A O N E - L E T T E R C O D E D E S I G N A T I N G T HE M E D I A
M E A S U R E D V A L U E OFM E A S U R E D V A L U E OFM E A S U R E D V A L U E OFM E A S U R E D V A L U E OF
CODEOF THE SAMfLE):A = AIR M « HAZARDOUS WASTE/OTHERS = SOLID (SOIL, SEDIMENT, SLUDGE)T > T I S S U E ( P L A N T B A N I M A L )W = W A T E R (GROUND WATER, S U R F A C E W A T E R , WASTE WATER,
D R I N K I N G W A T E R )D E S C R I P T I O N = A S H O RT D E S C R I P T I O N OF THE L O C A T I O N W H E R E S A M P L E WAS
COLLECTEDAIRS/STORET LOC. NO. = THE S P E C I F I C LOCATION ID NUMBER OF EITHER OF
THESE N A T I O N A L D A T A B A S E SYSTEMS, AS APPROPRIATED A T E / T I M E I N F O R M A T I O N = S P E C I F I C I N F O R M A T I O N R E G A R D I N G W H E N T H E S A M P L E
WAS COLLECTEDBEG. D A T E = D A T E S A M P L I N G W A S S T A R T E DBEG. T I M E = T I M E S A M P L I N G WAS S T A R T E DE N D D A T E = D A T E S A M P L I N G W A S C O M P L E T E DE N D T I M E - T I M E S A M P L I N G W A S C O M P L E T E DM O T E : A G R A B S A M P L E W I L L C O N T A I N O N L Y BEG.
D A T E / T I M EA TIMED COMPOSITE SAMPLE UILL CONTAINBOTH BEG AND END DATE/TIME TO DESIGNATEDURATION OF SAMPLE COLLECTION
OTHER CODESV - V A L I D A 1 E D
A N A L Y T I C A L R E S U L T S / M E A S U R E M E N T S I N F O R M A T I O N :
COMPOUND = MGP ( M E D I A - G R O U P - P A R A M E T E R ) CODE AND N A M E OFTHE MEASURED CONSTITUENT OR C H A R A C T E R I S T I COF E A C H SAMPLE
UNITS = S P E C I F I C UNITS IN UHICH R E S U L T S ARE R E P O R T E D :C = C E N T I G R A D E (CELSIUS) D E G R E E SCFS = CUBIC FEET PER SECONDGPM GALLONS PER MINUTEIN INCHES1.0. SPECIES I D E N T I F I C A T I O NKG KILOGRAML LITERLB = POUNDSMG = M I L L I G R A M S (1 X 10-3 G R A M S )MGD = M I L L I O N G A L L O N S PER DAYHPH = M I L E S PER HOURMV = M I L L I V O L TM / F = M A L E / F E M A L EM2 = S Q U A R E M E T E RM3 = C U B I C M E T E RNA = NOT A P P L I C A B L ENG = N A N O G R A M S (1 X 10-9 G R A M S )N T U = N E P H E L O M E T R I C T U R B I D I T Y U N I T SPC/L = P I C O (1 X 10-12) C U R R I E S PER L I T E RPG = P I C O G R A M S (1 X 10-12 G R A M S )P / C M 2 P I C O G R A M S P E R S Q U A R E C E N T I M E T E RSCM S T A N D A R D CUBIC M E T E R (1 A T M , 25 C)SQ FT S Q U A R E F E E TSU S T A N D A R D U N I T S (PH)UG H I C R O G R A M S (1 X 10-6 G R A M S )UNHOS HICROHHOS/CH ( C O N D U C T I V I T Y U N I T S )U/CC2 H I C R O G R A N S P E R 1 0 0 S Q U A R E C E N T I M E T E R SU/CH2 N I C R O G R A N S P E R S Q U A R E C E N T I M E T E R1000G 1000 G A L L O N S+/- P O S I T I V E / N E G A T I V E» = N U M B E R
D A T A Q U A L I F I E R S = S P E C I F I C C O D E S U S E D I N C O N J U N C T I O N W I T HDATA V A L U E S TO PROVIDE A D D I T I O N A L I N F O R M A T I O NON THE R E P O R T E D R E S U L T S , OR USED TO E X P L A I NTHE A B S E N C E OF A S P E C I F I C V A L U E :B L A N K « IF F I E L D IS B L A N K , NO R E M A R K S OR
Q U A L I F I E R S A R E P E R T I N E N T . F O R F I N A LR E P O R T E D D A T A , THIS M E A N S T H A T T H EV A L U E S H A V E B E E N R E V I E W E D A N D F O U N DTO BE A C C E P T A B L E FOR U S E .
I = I N V A L I D S A M P L E / D A T A - V A L U E NOT R E P O R T E DJ - D A T A R E P O R T E D BUT NOT V A L I D BY A P P R O V E D
QC P R O C E D U R E SK = A C T U A L V A L U E OF S A M P L E IS < V A L U E R E P O R T E DL = A C T U A L V A L U E OF S A M P L E IS > V A L U E R E P O R T E DM = D E T E C T E D BUT B E L O W THE L E V E L OF R E P O R T E D
VALUE FOR A C C U R A T E Q U A N T I F I C A T I O N0 = PARAMETER NOT ANALYZEDU = ACTUAL VA L U E OF SAMPLE IS < THE M E A S U R E M E N T
DETECTION LIMIT (REPORTED VALUE)
CONFOUND
A N A L Y S I S REQUEST DETAIL R E P O R T A C T I V I T Y : 7-BS26B
U N I T S 001 002 002 0 003 F
V A L I D A T E D D A T A
004
UF01 TEMPERATURE, UATER
UF05 PH, F I E L D
UF10 CONDUCTIVITY (FIELD)
UM14 LEAD, TOTAL, BY ICAP
UT35 NAPHTHALENE, BY HPLC
UT36 A C E N A P H T H Y L E N E , BY >-PLC
UT37 A C E N A P H T H E N E , BY H P I C
UT38 F L U O R E N E , BY HPLC
WT39 P H E N A N T H R E N E , BY H P I C
UT40 A N T H R A C E N E , BY HPLC
UT41 F L U O R A N T H E N E , BY H P I C
UT42 PYRENE, BY HPLC
UT43 A N T H R A C E N E , BENZO(A), BY HPLC
UT44 CHRYSENE, BY HPLC
UT45 FLUORANTHENE, BENZO(B), BY HPLC
UT46 FLUORANTHENE, BENZO(K), BY HPLC
UT47 PYRENE, BENZO(A), B1 HPLC
UT48 A N T H R A C E N E , D IBENZO ( A , H ) , BY HPLC
UT49 P E R Y L E N E , BENZO (G , H , I ) , BY HPLC
UT50 PYRENE, INDENOM ,2,3-CD), BY HPLC
UW54 BENZENE, BY GC/MS LCL
UU61 TOLUENE, BY GC/MS LDL
UU64 ETHYLBENZENE, BY GC/HS LDL
UU71 XYLENES, TOTAL, BY GC/MS LDL
ZZ01 SAMPLE NUMBER
ZZ02 A C T I V I T Y CODE
: ' C
: SU
:UMHOS
:UG/L
•UG/L
:UG/L
:UG/L
:UG/L
•UG/L
:UG/L
•UG/L
•UG/L
•UG/L
•UG/L
•UG/L
•UG/L
•UG/L
•UG/L
•UG/L
•UG/L
•UG/L
•UG/L
•UG/L
•UG/L
:NA
:NA
:12.2
:7.17
:0.69
:45.5
•0.020
:0.022
:0.011
•0.045
•0.038
•0.00048
•0.030
•0.00067
•0.0029
•0.0033
:0.0059
•0.0024
•0.0018
•0.0019
•0.0057
•0.022
•0.1
•0.5
•0.3
•0.8
•001
•BS26B
:9.7
:7.07
:0.66
:55.5
U :0.020
U :0.022
U :0.011U :0.045
U :0.038
U : 0.00048
U -0.030
U :0. 00067
U -0.0029
U -0.0033
U :0.0059
U :0.0024
U -0.0018
U -0.0019
U -0.0057
U :0.022
U :0.1
U :0.5
U :0.3
U :0.8
•002
•BS26B
:9.7
-.7.07
:0.66
:29.9
U :0.020
U :0.022
U :0.011
U :0.045
U -0.038
U :0. 00048
U :0.030
U :0. 00067
U -0.0029
U -0.0033
U :0.0059
U : 0.0024
U -0.0018
U -0.0019
U -0.0057
U -0.022
U :0.1
U :0.5
U :0.3
U -0.8
!002
•BS26B
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
0.1 u0.5 U
0.3 U
0.8 U
003
BS26B
10.0
6.92
1 .7
68.2
0.60
38.8
62.4
2.25 U
26. 6
7.19
1.50 U
4 .00 U
0.295 U
0.165 U
0.12 U
0.043 U
0.113
0.095 U
0.048
1.10 U
21
0.9
11
14
004
BS26B
A N A L Y S I S REQUEST DETAIL R E P O R T A C T I V I T Y : 7-BS26B V A L I D A T E D D A T A
COMPOUND UNITS 005
UF01 T E M P E R A T U R E , UATER
UF05 PH, FIELD
UF10 CONDUCTIVITY (FIELD)
UM14 LEAD, TOTAL, BY ICAP
UT35 NAPHTHALENE, BY HPLC
UT36 A C E N A P H T H Y L E N E , BY hPLC
UT37 A C E N A P H T H E N E , BY HPIC
UT38 F L U O R E N E , BY HPLC
UTJ9 P H E N A N T H R E N E , BY H P I C
UT40 A N T H R A C E N E , BY HPLC
UT41 FLUORANTHENE, BY HPIC
UT42 PYRENE, BY HPLC
UT43 ANTHRACENE, BENZO(A), BY HPLC
WT44 CHRYSENE, BY HPLC
WT45 FLUORANTHENE, BENZO(B), BY HPLC
UT46 F L U O R A N T H E N E , BENZO(K), BY HPLC
UT47 PYRENE, BENZO(A), BY HPLC
UT48 A N T H R A C E N E , D IBENZO ( A , H ) , BY HPLC
UT49 PERYLENE, BEN ZO(G , H , I ) , BY HPLC
UT50 PYRENE, INOENOC1 ,2, 3-CD), BY HPLC
UU54 BENZENE, BY GC/MS Lt>L
UU61 TOLUENE, BY GC/MS LUL
UU64 ETHYLBENZENE, BY GC/MS LDL
UU71 XYLENES, TOTAL, BY dC/MS LDL
ZZ01 SAMPLE NUMBER
ZZ02 ACTIVITY CODE
: 'C -11.8
:SU :7.04
:UMHOS:0.9A
•UG/L :39.9
•UG/L :0.020
•UG/L :0.022
•UG/L :0.011
•UG/L :O.OA5
:UG/L :0.038
•UG/L :0.024
•UG/L :0.030
•UG/L -0.038
•UG/L '0.0029
•UG/L -0.0033
•UG/L -0.0059
•UG/L -0.0024
•UG/L -0.0018
:UG/L :0.0019
•UG/L -0.0057
:UG/L :0.022
:UG/L :0.1
•UG/L :0.5
•UG/L :0.3
:UG/L :0.8
:NA :005
:NA :BS26B
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
A C T I V I T Y BS26B N A S O N C I T Y COAL G A S
THE P R O J E C T LEADER SHOULD C I R C L E ONE - STORET, AIRS, OR ARCHIVE.
C I R C L E ONE: STORl;T A I R S A R C H I V E
DATA A P P R O V E D BY LABO FOR TRANSMISSION TO P R O J E C T LEADER ON 07/25/97 18:22:16 BY ^TJ
