\

LUo

DATE :

SUBJECT:

FROM :

TO :

UNITED STATES ENVIRONMENTAL PROTECTION AGENCYREGION III

ENVIRONMENTAL SCIENCE CENTER701 MAPES ROAD '

FORT MEADE, MARYLAND 20755-5350 ^

May 10, 2005

Region III Data QA Review

Khin-ChoRegion III ESAT RPO (3EA20)

Christian MattaRegional Project Manager (3HS23)

SDMS DocID 2060881

Attached is the inorganic data validation report for the Big JohnSavage - Hoult Road Site (Case. 34031; SDG#: MCOOA5, MCOOD1)completed by the Region III Environmental Services Assistance Team(ESAT) contractor under the direction of Region III EAID.

If you have any questions regarding this review, please call me at(410) 305-2743.

Attachment

cc: Tad Yancheski

TO #: 0023

(TETRA TECH)

TDF #: 0490

ANALYTICAL SERVICES AND QUALITY ASSURANCE BRANCH

Printed on 100% recycled/recyclable paper with 100% post-consumer fiber and process chlorine free.Customer Service Hotline: 1-800-438-2474

118257

Lockheed Martin Information TechnologyESAT Region 3US EPA Environmental Science Center701 Mapes Road Ft. Meade, MD 20755-5350Telephone 410-305-3037 Facsimile 410-305-3597

L O C K H E E D M A R T I N\

We never forget who we 're working for '

DATE:

FROM:

TO:

May 10,2005

SUBJECT: Inorganic Data Validation (IM2 Level)Case: 34031SDGs: MCOOA5 and MCOOD1Site: Big John Salvage - Hoult Road

Donald M. Brown ***>Inorganic Data Reviewer

IM^Mahboobeh Mecanic ™Senior Oversight Chemist

Khin-Cho ThaungESAT Region 3 Project Officer

OVERVIEW

Case 34031, Sample Delivery Groups (SDGs) MCOOA5 and MCOOD1, consisted of forty (40)soil samples analyzed for total metals and cyanide (GST) by Chemtech Consulting Group(CHEM). The sample set included three (3) field duplicate pairs. Samples were analyzed inaccordance with Contract Laboratory Program (CLP) Statement of Work (SOW) ELM05.3through Routine Analytical Services (RAS) program.

SUMMARY

All samples were successfully analyzed for all Target Analyte List (TAL) parameters. Areas ofconcern with respect to data usability are listed .below.

Data in this case have been impacted by outliers present in the laboratory blanks as well as thematrix spike, laboratory duplicate and serial dilution analyses. Details of these outliers arediscussed under "Minor Problems"; specific samples affected are outlined in "Table 1 A" andqualified analytical results for all samples are summarized on the Data Summary Forms (DSFs).

118258

6'Page 2 of 4

MINOR PROBLEMS

Continuing Calibration (CCB) and/or Preparation (PB) Blanks had reported results greater thanthe Method Detection Limits (MDLs) for the analytes listed below. Positive results reported inaffected samples which are less than or equal to five times (<5X) the blank concentrations maybe biased high and have been qualified "B" on the DSFs.

SDG Blank Affected AnalvtesMCOOA5 CCB antimony (Sb), selenium (Se), silver (Ag), sodium (Na)MCOOD1 CCB Sb, arsenic (As), chromium (Cr), cobalt (Co), Se, Ag, Na,

thallium (Tl), vanadium (V)PB CN- ,

CCBs and/or PBs had negative values greater than the absolute values of the MDLs regarding theanalytes listed below. Positive results reported in affected samples which are less than two times(<2X) the absolute value of the blank concentrations may be biased low. The "L" qualifier forthese outliers have been superseded by "J" or "B" on the DSFs. Quantitation limits in affectedsamples may be biased low and have been qualified "UL" on the DSFs.

SDG Affected AnalvtesMCOOA5 Sb, cadmium (Cd), AgMCOOD1 Sb, Cd, lead (Pb), Na, Tl ' ;

Matrix spike recoveries were high (>125%) for manganese (Mn) in both SDGs as well as for Asin SDG MCOOD1. Positive results reported for these analytes in these SDGs may be biased highand have been qualified "K" on the DSFs unless superseded by "B".

Matrix spike recoveries were low (<75% but >30%) for Sb and Tl in SDG MCOOD1. Lowrecoveries may be attributed to matrix interferences or analyte lost during the digestion process.Positive results reported for these analytes in affected samples in this SDG may be biased low.The "L" qualifier for these outliers has been superseded by "J" or "B" on the DSFs. Quantitationlimits for these analytes in affected samples in this SDG may be biased low and have beenqualified "UL" on the DSFs.

The Relative Percent Difference (RPD) for the laboratory duplicate analysis was outside controllimits (35% RPD, ±2XCRQL) for calcium (Ca) in SDG MCOOD1. Positive results reported forthis analyte in this SDG are estimated and have been qualified "J" on the DSFs.

Percent Differences (%Ds) for the ICP serial dilution analyses were outside control limits(>10%) for Cr, Co and V in both SDGs as well as for beryllium (Be), copper (Cu) and nickel (Ni)in SDG MCOOD1. Positive results reported for these analytes in these SDGs are estimated due topossible matrix interferences and have been qualified "J" on the DSFs unless superseded by "B".

118259

Page 3 of 4

NOTES

Reported results between MDLs and Contract Required Quantitation Limits (CRQLs) werequalified "J" on the DSFs unless superseded by "B".

The RPD for the laboratory duplicate analysis was outside contractual control limits (20% RPD,±CRQL) for Pb in SDG MCOOA5. However, the RPD for this analyte was within Region 3established control limits (35% RPD, ±2XCRQL) for soil analysis. No data were qualified forthis analyte in this SDG based on laboratory duplicate imprecision.

Reported results for field duplicate pair MCOOB2/MCOOC4 were within 35% RPD, ±2XCRQLfor all analytes except aluminum (Al), Cr, Cu, iron (Fe), Pb, Mn and zinc (Zn).

Reported results for field duplicate pair MCOOF9/MCOOG4 were within 35% RPD, ±2XCRQLfor all analytes.

Reported results for field duplicate pair MC0002/MCOOG2 were within 35% RPD, ±2XCRQLfor all analytes except Fe and mercury (Hg).

Post-digestion spike recoveries were low for Sb, As and Tl in SDG MCOOD1; however, data arenot qualified based on the post-digestion spike recoveries.

The following samples in SDG MCOOD1 were reanalyzed at the dilutions listed below for Hg inorder to bring concentrations within the linear range of the instrument. Results for this analyte inthese samples were reported from the diluted analyses, annotated with a "+" on the DSFs andnoted below.

Sample ID Dilution FactorMCOOE1 5.0MCOOE2 10.0MCOOE9, MCOOF3 2.0

Data for Case 34031, SDGs MCOOA5 and MCOOD1, were reviewed in accordance with NationalFunctional Guidelines for Evaluating Inorganic Analyses with Modification for use withinRegion IE.

118260

Qc

Page 1 of6

TABLE1ASUMMARY OF QUALIFIERS ON DATA SUMMARY

FORM AFTER DATA VALIDATION

Case 34031, SDG MCOOA5

ANALYTE

Sb

SAMPLESAFFECTED

MCOOA6, MCOOB7

MC0143, MC0149,

POSITIVEVALUES

B

B

NON-DETECTEDVALUES BIAS

High

High

Cd

MC0157

MC0148

All Samples ExceptMCOOA6, MCOOB7,MC0143, MC0148,MC0149,MC0157

MC0148, MC0163

MCOOA5, MCOOBO,MCOOB1,MCOOB2,MCOOB7, MCOOB8,MC0135,MC0136,MC0144

MC0149,MC0155,MC0156,MC0157

B

Cr

Co

Mn

All Samples

All Samples

All Samples

J

J

K

UL

High

Low

UL Low

UL Low

COMMENTS*

CCB (4.245 J

CCB (7.255 J jig/L)

CCB (7.255 J ng/L)CBN (-6.005 J ng/L)

PEN (-0.57 J mg/Kg)

>MDL<CRQLCBN(-1.595Jng/L)

CBN(-1.660Jng/L)

High

CBN(-1.595Jng/L)

ISD (13%)

ISD(13%)

MSH (177%)

* See explanation of comments in Table IB

118261

PageS of 6

TABLE1ASUMMARY OF QUALIFIERS ON DATA SUMMARY

FORM AFTER DATA VALIDATION

Case 34031, SDG MCOOD1

SAMPLESANALYTE AFFECTED

Sb

As

MCOOD1, MCOOF6

MCOOE1

MCOOE2

MCOOE9, MCOOF2,MCOOF3, MCOOF9,MCOOQ3

MCOOD2

MCOOD8, MCOOEO,MCOOE3, MCOOE8,MCOOF4, MC0002

MC0004, MC0006,MC0008, MC0009

MCOOEO

All Samples ExceptMCOOEO

POSITIVEVALUES

B

B

B

B

B

K

NON-DETECTEDVALUES BIAS

High

High

High

High

UL

UL

UL

Low

Low

Low

High

High

Be All Samples J

* See explanation of comments in Table IB

COMMENTS*

CCB (14.610 J jig/L)MSL (50%)

CCB (13.775 JMSL (50%)

CCB (13.775 JCBN (-9.825 J jig/L)MSL (50%)

CCB (14.610 J ng/L)CBN (-9.825 Jug/L)MSL (50%)

CBN (-12.935 J ng/L)MSL (50%)

CBN (-9.825 JMSL (50%)

MSL (50%)

CCB(6.315J|xg/L)MSH (142%)

MSH (142%)

ISD (23%)

118262

Page 5 of 6

TABLE 1ASUMMARY OF QUALIFIERS ON DATA SUMMARY

FORM AFTER DATA VALIDATION

Case 3403 1 , SDG MCOOD 1

Ag

Na

MCOOD 1,MCOOD2,MC0004, MC0006,MC0008, MC0009

MCOOD1 B

MCOOD8, MCOOEO, BMCOOE2

MCOOE8, MCOOE9 B

MCOOD1,MCOOE9, BMC0003, MC0004,MC0008

MCOOD8, MCOOE1, BMCOOE2

MCOOEO, MCOOE3 B

MCOOF2, MCOOF3, BMCOOF4, MCOOF6,MCOOF9

MCOOD2

MCOOE8, MC0002

NON-SAMPLES POSITIVE DETECTED

ANALYTE AFFECTED VALUES VALUES BIAS

Se MCOOD2

All Samples Except

B

B

High

High

UL

UL

High

High

High

High

High

High

High

Low

Low

COMMENTS*

CCB (4.210 J jig/L)

CCB (8.445 J jig/L)

CCB (5.175 J jig/L)

CCB (4.850 J jig/L)

CCB (4.710 J ng/L)

CCB (846.585 J jig/L)

CCB (439.230 J jig/L)

CCB (439.230 J jig/L)CBN (-587.245 J jig/L)

CCB (846.585 J ^g/L)CBN (-587.245 J ng/L)

CBN (-614.770 J

CBN (-587.245 J ng/L)

See explanation of comments in Table IB

118263

'«$Page 1 of 1

TABLE IBCODES USED IN COMMENTS COLUMN

CCB = Continuing calibration blanks had results >MDLs [results are in parenthesis].Reported results which are <5X the blank concentrations may be biased high.

CBN = Continuing calibration blanks had negative results with absolute values >MDLs[results are in parenthesis]. Reported results which are <2X the absolute value ofthe blank concentrations and quantitation limits may be biased low.

PBN = Preparation blanks had negative results with absolute values >MDLs [results arein parenthesis]. Reported results which are <2X the absolute value of the blankconcentrations and quantitation limits may be biased low.

>MDL = Reported results are greater than MDLs but less than CRQLs and are considered<CRQL estimated.

ISD =, Percent Differences (%Ds) for the serial dilution analyses were outside controllimits (>10%) [%Ds are in parenthesis]. Positive results reported are estimated.

MSH = Matrix spike recoveries were high (>125%) [% recoveries are in parenthesis].Positive results may be biased high.

MSL = Matrix spike recoveries were low (<75% but >30%) [% recoveries are inparenthesis]. Reported results and quantitation limits may be biased low.

DUP = The Relative Percent Difference (RPD) for the laboratory duplicate analysis wasoutside control limits (35% RPD, ±2XCRQL) [RPD is in parenthesis]. Positiveresults reported are estimated.

PB = The preparation blank had a result >MDL [result is in parenthesis]. Reportedresults which are ^5X the blank concentration may be biased high.

118264

GLOSSARY OF DATA QUALIFIER CODES (INORGANIC)

CODES RELATED TO IDENTIFICATION(confidence concerning'presence or absence of analytes):

U = Not detected. The associated number indicates approxim .te sampleconcentration necessary to be detected.

(NO CODE) = Confirmed identification.

B = Not detected substantially above the level reported in laboratory or fieldblanks.

R = Unreliable result. Analyte may or may not be present in the sample.Supporting data necessary to confirm result.

CODES RELATED TO OUANTITATION(can be used for both positive results and sample quantitation limits):

J = Analyte Present. Reported value may not be accurate or precise.

K = Analyte present. Reported value may be biased high. Actual value isexpected to be lower.

L = Analyte present. Reported value may be biased low. Actual value is expectedto be higher.

UJ = Not detected, quantitation limit may be inaccurate or imprecise.

UL = Not detected, quantitation limit is probably higher.

OTHER CODES

Q = No analytical result.

118265

Appendix B

Data Summary Forms

118266

DATA SUMMARY FORM: INORGANIC Page 1__ of _8_

Case #: 34031

Site:

Lab.:

SDG : MCOOA5

BIG JOHN SALVAGE HOULT RD

CHEM

Number of Soil Samples : 20

Number of Water Samples : 0

MCOOA5

BJS-SBK5-0405

MCOOA6

BJS-SBK6-0405

MCOOBO

BJS-SBL4-0405

MCOOB1

BJS-SBL5-0405

MCOOB2

BJS-SBL6-0405

Dup of MCOOC4

Soil

mg/Kg

4/8/2005

08:35

82.9

1.0

Soil

mg/Kg

4/8/2005

10:50

80.7

1.0

Soil

mg/Kg

4/8/2005

09:30

82.4

1.0

Soil

mg/Kg

4/8/2005

10:20

84.7

1.0

Soil

mg/Kg

4/8/2005

09:08

86.6

1.0

Sample Number:

Sampling Location:

Field QC:

Matrix:

Units:

Date Sampled:

Time Sampled:

%Solids:

Dilution Factor:

CRQL = Contract Required Quantitation Limit

To calculate sample quantitation limits: (CRQL * Dilution Factor) / (%Solids/ 100)

SEE NARRATIVE FOR CODE DEFINITIONS

Revised 09/99

118267

DATA SUMMARY FORM: INORGANIC Page_2_of_8_

Case #: 34031

Site:

Lab.:

SDG : MCOOA5

BIG JOHN SALVAGE HOULT RD

CHEM

MCOOB7

SBM5-0405

Soil

mg/Kg

4/7/2005

15:0086.01.0

MCOOB8

SBM6-0405

Soil

mg/Kg

4/8/2005

08:00

83.3

1.0

MC0135

SDMON5A2-0405

Soil

mg/Kg

4/9/2005

13:40

74.9

1.0

MC0136

SDMON5A3-0405

Soil

mg/Kg

4/9/2005

13:50

82.1

1.0

MC0143

SDMON4Y1-0405

Soil

mg/Kg

4/9/2005

11:00

76.6

1.0

Sample Number:

Sampling Location : Prefix: BJS-

Matrix:

Units:

Date Sampled:

Time Sampled:

%Solids:

Dilution Factor:

CRQL = Contract Required Quantitation Limit

To calculate sample quantitation limits: (CRQL * Dilution Factor) / (%Solids/100)

Prefix : All sample locations are prefixed BJS-

SEE NARRATIVE FOR CODE DEFINITIONS

Revised 09/99

118268

DATA SUMMARY FORM: INORGANIC Page _3_ of _8_

Case ft 34031

Site:Lab.:

SDG : MCOOA5

BIG JOHN SALVAGE HOULT RD

CHEM

Sample Number:

Sampling Location : Prefix : BJS-

Matrix :

Units:

Date Sampled :

Time Sampled :

%Solids:

Dilution Factor:

MC0144

SDMON4Y2-0405

Soil

mg/Kg

4/9/200511:1084.71.0

MC0145

SDMON4Y3-0405

Soil

mg/Kg

4/9/200511:20

57.1

1.0

MC0146

SDMON4Y4-0405

Soil

mg/Kg

4/9/2005

11:3062.6

1.0

MC0147

SDMON4Z1-0405

Soil

mg/Kg

4/9/200510:0052.0

1.0

MC0148

SDMON4Z2-0405

Soil

mg/Kg

4/9/2005

10:2055.61.0

CRQL = Contract Required Quantitation Limit

To calculate sample quantitation limits: (CRQL * Dilution Factor) / (%Solids/ 100)

Prefix : All sample locations are prefixed BJS-

SEE NARRATIVE FOR CODE DEFINITIONS

Revised 09/99

118269

DATA SUMMARY FORM: INORGANIC Page _4_ of _8__

Case #: 34031

Site:

Lab. :

SDG : MCOOA5

BIG JOHN SALVAGE HOULT RD

CHEM

| Sample Number:

Sampling Location : Prefix : BJS-

Matrix :

Units:

Date Sampled:

Time Sampled :

%Solids:

Dilution Factor:

MC0149

SDMON5A4-0405

Soil

mg/Kg

4/9/2005

14:00

81.8

1.0

MC0155

SDMON9Z1-0405

Soil

mg/Kg

4/9/2005

13:35

70.4

1.0

MC0156

SDMON9Z2-0405

Soil

mg/Kg

4/9/2005

13:55

82.3

1.0

MC0157

SDMON5A1-0405

Soil

mg/Kg

4/9/2005

13:30

73.7

1.0

MC0163

SDMON5C1-0405

Soil

mg/Kg

4/9/2005

15:30

77.2

1.0

CRQL = Contract Required Quantitation Limit

To calculate sample quantitation limits: (CRQL * Dilution Factor) / (%Solids/100)

Prefix : All sample locations are prefixed BJS-

SEE NARRATIVE FOR CODE DEFINITIONS

Revised 09/99

118270

DATA SUMMARY FORM: INORGANIC Page __5_ of _8_

Case #: 34031

Site:

Lab.:

SDG : MCOOD1

BIG JOHN SALVAGE HOULT RD

CHEM

Number of Soil Samples : 20

Number of Water Samples : 0

Sample Number:

Sampling Location:

Matrix :

Units:

Date Sampled:

Time Sampled :

%Solids:

Dilution Factor:

MCOOD1

BJS-SSD3-0405

Soil

mg/Kg

4/9/2005

11:58

73.8

1.0

MCOOD2

BJS-SSD5-0405

Soil

mg/Kg

4/9/2005

16:20

88.3

1.0

MCOOD8

BJS-SSG2-0405

Soil

mg/Kg

4/9/2005

11:07

73.6

1.0

MCOOEO

BJS-SSG6-0405

Soil

mg/Kg

4/9/2005

15:50

13.0

1.0

MCOOE1

BJS-SSH3-0405

Soil

mg/Kg

4/9/2005

13:05

82.9

1.0/5.0

MERCURY

HPOTASSIUM

CRQL = Contract Required Quantitation Limit

To calculate sample quantitation limits: (CRQL * Dilution Factor) / (%Solids/

+ = Result reported from diluted analysis.

100)SEE NARRATIVE FOR CODE DEFINITIONS

Revised 09/99

118271

DATA SUMMARY FORM: INORGANIC Page _6_ of 8

Case #: 34031

Site:

Lab.:

SDG : MCOOD1

BIG JOHN SALVAGE HOULT RD

CHEM

Sample Number:

Sampling Location:

Matrix:

Units:

Date Sampled :

Time Sampled:

%Solids:

Dilution Factor:

MCOOE3

BJS-SSI2-0405

Soil

mg/Kg

4/9/2005

10:45

82.91.0

MCOOE2

BJS-SSH5-0405

Soil

mg/Kg

4/9/2005

16:3082.7

1.0/10.0

MCOOE8

BJS-SSK2-0405

Soil

mg/Kg

4/9/2005

10:10

80.01.0

MCOOE9

BJS-SSK4-0405

Soil

mg/Kg

4/9/200513:5084.51.0/2.0

MCOOF2

BJS-SSL3-0405

Soil

mg/Kg

4/9/2005

14:50

88.0

1.0

CRQL = Contract Required Quantitation Limit

To calculate sample quantitation limits: (CRQL * Dilution Factor) / (%Solids/100)

+ = Result reported from diluted analysis.

SEE NARRATIVE FOR CODE DEFINITIONS

Revised 09/99

118272

%-DATA SUMMARY FORM: INORGANIC Page_7_of_8_

Case* 34031

Site:

Lab.:

SDG : MCOOD1

BIG JOHN SALVAGE HOULT RD

CHEM

MCOOF3

BJS-SSL5-0405

MCOOF4

BJS-SSM2-0405

MCOOF6

BJS-SSM6-0405

MCOOF9

BJS-SSN5-0405

Dup of MCOOG4

Soil

mg/Kg

4/9/200516:1078.51.0

MC0002

BJS-BSS10-0405

Dup of MCOOG2

Soil

mg/Kg

4/9/2005

11:4563.2

1.0

Soil

mg/Kg

4/9/2005

16:00

88.51.0/2.0

Soil

mg/Kg

4/9/200510:30

84.4

1.0

Soil

mg/Kg

4/9/200515:35

88.7

1.0

4010bmw£w*wiy

1170

Sample Number:

Sampling Location :

Field QC :

Matrix:

Units:

Date Sampled :

Time Sampled:

%Solids:

Dilution Factor:

CRQL = Contract Required Quantitation Limit

To calculate sample quantitation limits: (CRQL * Dilution Factor) / (%Solids/ 100)

+ = Result reported from diluted analysis.

SEE NARRATIVE FOR CODE DEFINITIONS

Revised 09/99

118273

DATA SUMMARY FORM: INORGANIC Page 8 of _8_

Case #: 34031

Site:

Lab.:

SDG : MCOOD1

BIG JOHN SALVAGE HOULT RD

CHEM

MC0009

BJS-BSS8-0405

Soil

mg/Kg

4/9/2005

11:10

70.3

1.0

MC0003

BJS-BSS2-0405

Soil

mg/Kg

4/9/2005

09:45

77.3

1.0

MC0004

BJS-BSS3-0405

Soil

mg/Kg

4/9/2005

10:00

65.0

1.0

MC0006

BJS-BSS5-0405

Soil

mg/Kg

4/11/2005

10:30

77.7

1.0

MC0008

BJS-BSS7-0405

Soil

mg/Kg

4/9/2005

13:00

80.2

1.0

Sample Number:

Sampling Location :

Matrix:

Units:

Date Sampled:

Time Sampled:

%Solids:

Dilution Factor:

CRQL = Contract Required Quantitation Limit

To calculate sample quantitation limits: (CRQL * Dilution Factor) / (%Sollds/100)

SEE NARRATIVE FOR CODE DEFINITIONS

Revised 09/99

118274

Appendix C

Chain-of-Custody Records

118275

&EPA USEPA Contract Laboratory Program Case No: -. 34031 pInorganic Traffic Report & Chain of Custody Record DAS No: IX

Region: 3

Project Code: T47121 0103Account Code: 2005T03W302DD2C .

CERCLIS ID: WVD054827944Spill ID:

Site Name/State: Big John Salvage CLP 34031 /WV

Project Leader: Tad YancheskiAction: Remedial Investigation

Sampling Co: Tetra Tech, Inc.

INORGANIC MATRIX/ CONG ANALYSIS/SAMPLE No. SAMPLER TYPE TURNAROUND

MCOOB2 Subsurface /G CN (21), TM (21)Soil/DouglasSeavey

MCOOB7 Subsurface /G CN (21), TM (21)Soil/DouglasSeavey

MCOOB8 Subsurface /G CN (21 ), TM (21 )Soil/DouglasSeavey

MCOOC4 Subsurface /G CN (21), TM (21)Soil/DouglasSeavey

MCOOC5 Subsurface /G CN (21), TM(21)Soil/DouglasSeavey

MCOOC6 Subsurface /G CN (21),TM (21)Soil/DouglasSeavey

MCOOFO Surface Soil/ /G CN (21),TM (21)DennisAnderson

MCOOF5 Surface Soil/ /G CN (21), TM(21)DennisAnderson

Date Shipped: 4/11/2005 Cham of Custody Record SamplerSignature:

Carrier Name: FertFvAirbill: ' 8489 8704 fiftfifi Relinquished By (Date /Time) Received By (Date (Time)

Shipped to: ChemTech Consulting 1

Group (CHEMED)284 Sheffield Street 2

Mountainside NJ 07092(908) 789-8900 3

4

TAGNoJ STATION SAMPLE COLLECT ORGANIC QCPRESERVATIVE Bottles LOCATION DATE/TIME SAMPLE No. T/Pe

1742 (Ice Only), 1748 (Ice BJS-SBL6-0405 8:4/8/2005 8:35 COOB2Only) (2)

1787 (Ice Only), 1793 (Ice BJS-SBM5-0405 8:4/7/2005 15:00 COOB7Only) (2)

1796 (Ice Only), 1802 (Ice BJS-SBM6-0405 8:4/8/2005 8:00 COOB8Only) (2)

1850 (Ice Only), 1856 (Ice BJS-SBP1-0405 8:4/8/2005 9:00 COOC4 Field DuplicateOnly) (2)

.• *

1859 (Ice Only), 1865 (Ice BJS-SBP2-0405 8:4/8/2005 12:20 COOC5 Field DuplicateQnly)(2)

1868 (Ice Only), 1874 (Ice BJS-SBP3-0405 8:4/8/2005 14:30 COOC6 Field DuplicateOnly) (2)

2084 (Ice Only), 2090 (Ice BJS-SSK6-0405 8:4/9/2005 15:30 COOFOOnly) (2)

2129 (Ice Only), 2135 (Ice BJS-SSM4-0405 8:4/9/2005 15:25 COOF5Only) (2)

Shipment for CaseComplete? N

Analysis Key:

CN = Cyanide, TM = CL

Sample(s) to be used for laboratory QC: Additional Sampler Signature(s):

Concentration: L = Low, M = Low/Medium. H = High Type/Designate: Composite = C, Grab = G

Chain of Custody Seal Number:

Shipment Iced?

H i AL i otai Metals

TR Number: 3-035066262-041105-0003PR provides preliminary results. Requests for preliminary results will increase analytical costs.Send Copy to: Sample Management Office. Attn: Heather Bauer, CSC, 15000 Conference Center Dr.. Chantilly, VA 20151-3819; Phone 703/818-4200; Fax F2V5.1.047 Page 2 of 2*

118276

^EPA USEPA Contract Laboratory ProgramWL-rYA inorganjc Traffic Report & Chain of Custody Record

Region:

Project Code:

Account Code:

CERCLIS ID:

Spill ID:

Site Name/State

Project Leader:

Action:

Sampling Co:

INORGANICSAMPLE No.

MC0135

MC0136

MC0143

MC0144,

MC0145

MC0146

MC0147

MC0148

MC0149

MC0155

MC0156

3

T47121.01032005T03W302DD2C

WVD054827944

= Big John Salvage SD Organics/Metals/WV

Tad YancheskiRemedial Investigation

Tetra Tech, Inc.

MATRIX/ CONC/ ANALYSIS/SAMPLER TYPE TURNAROUND

Sediment/ /G CN (21), TM (21)Tad Yancheski

Sediment/ /G CN (21), TM (21)Tad Yancheski

Sediment/ /G CN (21), TM (21)Tad Yancheski /

Sediment/ /G CN (21), TM (21)Tad Yancheski

Sediment/ /G CN (21 ), TM (21 )Tad Yancheski

Sediment/ /G CN (21), TM (21)Tad Yancheski

Sediment/ /G CN (21 ), TM (21 )Tad Yancheski

Sediment/ /G CN (21), TM (21)Tad Yancheski

Sediment/ /G CN (21 ), TM (21 )Tad Yancheski

Sediment/ /G CN (21), TM (21)Tad Yancheski

Sediment/ /G 'CN (21), TM (21)Tad Yancheski

Date Shipped: 4/1 1 /2005

Carrier Name: FedEx

Airbill: 8421 2820 5126

Shipped to: ChemTech ConsultingGroup (CHEMED)284 Sheffield StreetMountainside NJ 07092(908) 789-8900

TAG No./ STATIONPRESERVATIVE/ Bottles LOCATION

Case No: -

DAS No:

Chain of Custody Record

Relinquished By (Date / Time)

1

2

3

4

34031 Q 3

SamplerSignature:

Received By (Date / Time)

SAMPLE COLLECT ORGANIC QCDATE/TIME SAMPLE No. Type

3585 (Ice Only), 3591 (Ice BJS-SDMON5A2-0405 S: 4/9/2005 13:40 C0135Only) (2)

3593 (Ice Only), 3599 (Ice BJS-SDMON5A3-0405 S: 4/9/2005 13:50 C0136Only) (2)

3480 (Ice Only), 3486 (Ice BJS-SDMON4Y1 -0405 S: 4/9/2005 11:00 C0143Only) (2)

3488 (Ice Only), 3494 (Ice BJS-SDMON4Y2-0405 S: 4/9/2005 11:10 C0144Only) (2)

3496 (Ice Only), 3502 (Ice BJS-SDMON4Y3-0405 S: 4/9/2005 11:20 C0145Only) (2)

3504 (Ice Only), 3510 (Ice BJS-SDMON4Y4-0405 S: 4/9/2005 11:30 C0146Only) (2)

351 2 (Ice Only), 351 8 (Ice B JS-SDMON4Z1 -0405 S: 4/9/2005 10:00 C0147Only) (2)

3520 (Ice Only), 3526 (Ice BJS-SDMON4Z2-0405 S: 4/9/2005 10:20 C0148Only) (2)

3601 (Ice Only), 3607 (Ice BJS-SDMON5A4-0405 S: 4/9/2005 14:00 C0149Only) (2)

3633 (Ice Only), 3639 (Ice BJS-SDMON9Z1-0405 S: 4/9/2005 13:35 C0155Only) (2)

3641 (Ice Only), 3647 (Ice BJS-SDMON9Z2-0405 S: 4/9/2005 13:55 C0156Only) (2)

Field Duplicate

Field Duplicate

Shipment for CaseComplete? N

Analysis Key:

CN = Cyanide, TM = CL

Sample(s) to be used for laboratory QC: Additional Sampler Signature(s):

Concentration: L = LOW, M = Low/Medium, H = High Type/Designate: Composite = C, Grab = G

Chain of Custody Seal Number:

Shipment Iced?

H I AL 1 otal Metals

TR Number: 3-035066262-041105-0021PR provides preliminary results. Requests for preliminary results will increase analytical costs.Send Copy to: Sample Management Office, Attn: Heather Bauer, CSC, 15000 Conference Center Dr., Chantilly, VA 20151-3819; Phone 703/818-4200; Fax703/818-4602

F2V5.1.047 Pagel of 2118277

&EPA USEPA Contract Laboratory ProgramInorganic Traffic Report & Chain of Custody Record

Region: 3

ProjectCode: ^^ ^

Account Code: 2005T03W302DD2C

CERCLIS ID: WVD054827944Spill ID:

Site Name/State: Big John Salvage SD Organics/Metals/WV

Project Leader: Tad Yancheski

Action: Remedial Investigation

Sampling Co: Tetra Tech, Inc.

Date Shipped: 4/11/2005

Carrier Name: FedEx

Airbill: 8421 2820 5126

Shipped to: ChemTech ConsultingGroup (CHEMED)284 Sheffield StreetMountainside NJ 07092(908) 789-8900

Case No:'- 34031 ' Q

DAS No: 1^-

Chain of Custody Record

Relinquished By (Date / Time)

1

2

3

4

SamplerSignature:

Received By (Date / Time)

INORGANICSAMPLE No.

MATRIX/SAMPLER

CONC/TYPE

ANALYSIS/TURNAROUND

TAG No./PRESERVATIVE/ Bottles

STATIONLOCATION

SAMPLE COLLECTDATE/TIME

ORGANICSAMPLE No.

QCType

MC0157

MC0163

MC0164

MC0165

MC0166

MC0168

Sediment/Tad Yancheski

Sediment/Tad Yancheski

Sediment/Tad Yancheski

Sediment/Tad Yancheski

Sediment/Tad Yancheski

Sediment/Tad Yancheski

/G CN(21),TM(21)

/G CN(21),TM(21)

/G CN(21),TM(21)

/G CN(21),TM(21)

/G CN(21),TM(21)

/G CN(21), TM(21)

3585 (Ice Only) (2)

3708 (Ice Only), 3714 (IceOnly) (2)

3716 (Ice Only), 3722 (IceOnly) (2)

3724 (Ice Only), 3730 (IceOnly) (2)

3853 (Ice Only), 3859 (IceOnly) (2)

3862 (Ice Only), 3868 (IceOnly) (2)

BJS-SDMON5A1-0405 S: 4/9/2005 13:30 C0157

BJS-SDMON5C1-0405 S: 4/9/2005 15:30 C0163

BJS-SDMON5C2-0405 S: 4/9/2005 15:40 C0164

BJS-SDMON5C3-0405 S: 4/9/2005 15:50 C0165

BJS-SDMON10Z1-0405 S: 4/10/2005 12:45 C0166

BJS-SDMON10Z2-0405 S: 4/10/2005 12:55 C0168

Field Duplicate

Field Duplicate

Shipment for CaseComplete? N

Analysis Key:

CN = Cyanide, TM = CL

Sample(s) to be used for laboratory QC:

Concentration: L = Low, M = Low/Medium, H = High

K I AL I otal Metals

Additional Sampler Signature(s):

Type/Designate: Composite = C, Grab = G

Chain of Custody Seal Number:

Shipment Iced?

TR Number: 3-03506G2S2-041105-0021PR provides preliminary results. Requests for preliminary results will increase analytical costs.Send Copy to: Sample Management Office, Attn: Heather Bauer, CSC, 15000 Conference Center Dr., Chantilly, VA 20151-3819; Phone 703/818-4200; Fax F2V5.1.047 Rage

118278

&EPA USEPA Contract Laboratory ProgramInorganic Traffic Report & Chain of Custody Record

Region: 3

Project Code: T47121 0103

Account Code: 2005T03W302DD2C

CERCLIS ID: WVD054827944Spill ID:

Site Name/State: Big John Salvage CLP 34031/WV

Project Leader: -racj Yancheski

Action: Remedial Investigation

Sampling Co: Tetra Tech, Inc.

INORGANIC MATRIX/ CONC/ ANALYSIS/SAMPLE No. SAMPLER TYPE TURNAROUND

MCOOEO Surface Soil/ IG CN (21), TM (21)teessk Dennis

AndersonMCOOE1 Surface Soil/ IG CN (21), TM (21)«**SS!k Dennis

AndersonMCOOE2 Surface Soil/ IG CN (21), TM (21)'' tea. Dennis

AndersonMCOOE3 Surface Soil/ IG CN (21), TM (21)'•Ms*"- Dennis

AndersonMCOOE8 Surface Soil/ IG CN (21), TM (21)

DennisAnderson

M|£OE9 Surface Soil/ IG CN (21), TM (21)^^**fe Dennis

AndersonMCOOF2 Surface Soil/ IG CN (21), TM (21)

.DennisAnderson ,

MCOOF3 Surface Soil/ IG CN (21), TM (21)DennisAnderson

MCOOF4 Surface Soil/ IG CN (21), TM (21)DennisAnderson

MCOOF6 Surface Soil/ IG CN (21), TM (21)DennisAnderson

Date Shipped: 4/1 1/2005 Chain Of Custody

Carrier Name: FerlF*

Airbill: 84ft9 fi704 SRM Relinquished By

Shipped to: ChemTech Consulting 1

284 Sheffield Street 2

Mountainside NJ 07092(908) 789-8900 3

4 .

Case No:- 34031 T}

DAS No: «V

Record SamplerSignature:

(Date /Time) Received By (Date /Time)

TAG No./ STATION SAMPLE COLLECT ORGANIC OCPRESERVATIVE/ Bottles LOCATION DATE/TIME SAMPLE No. TVP6

1994 (Ice Only), 2000 (Ice BJS-SSG6-0405 S: 4/9/2005Only) (2)

2003 (Ice Only), 2009 (Ice BJS-SSH3-0405 S: 4/9/2005Only) (2)

2012 (Ice Only), 2018 (Ice BJS-SSH5-0405 8:4/9/2005Only) (2) (

2021 (Ice Only), 2027 (Ice BJS-SSI2-0405 S: 4/9/2005Only) (2)

2066 (Ice Only), 2072 (Ice BJS-SSK2-0405 S: 4/9/2005Only) (2)

2075 (Ice Only), 2081. (Jce BJS-SSK4-0405 8:4/9/2005Only) (2)

2102 (Ice Only), 2108 (Ice BJS-SSL3-0405 S: 4/9/2005Only) (2)

21 1 1 (Ice Only ), 21 1 7 (Ice BJS-SSL5-0405 S: 4/9/2005Only) (2)

2120 (Ice Only), 2126.(lce BJS-SSM2-0405 8:4/9/2005Only) (2)

2138 (Ice Only), 2144 (Ice BJS-SSM6-0405 S: 4/9/2005Only) (2)

15:50 COOEO

13:05 COOE1

16:30 COOE2

10:45 COOES

10:10 COOES

13:50 COOE9

14:50 COOF2

16:00 COOF3

10:30 COOF4

15:35 COOF6

Shipment for CaseComplete? N

Analysis Key:

CN = Cyanide, TM = CL

Sample(s) to be used for laboratory QC:

MC0001

Concentration: [_ = Low, M = Low/Medium, H = High

P TAL Total Metals

Additional Sampler Signature(s):

Type/Designate: Composite - C, Grab = G

Chain of Custody Seal Number:

Shipment Iced?

TR Number: 3-035066262-041105-0011PR provides preliminary results. Requests for preliminary results will increase analytical costs.Send Copy to: Sample Management Office, Attn: Heather Bauer, CSC, 15000 Conference Center Dr., Chantilly, VA 20151-3819; Phone 703/818-4200; Fax703/818-4602

F2V5.1.047 Rage 2 of 3118279

^EPA USEPA Contract Laboratory Program^ ^* Inorganic Traffic Report & Chain of Custody Record

Region: 3

Project Code: T47121 Q103Account Code: 2005T03W302DD2C

CERCLIS ID: WVD054827944

Spilt ID*

Site Name/State: Big John Salvage CLP 34031 /WV

Project Leader: Jad Yancheski

Action: Remedial Investigation

Sampling Co: Tetra Tech, Inc.

INORGANIC MATRIX/ CONG ANALYSIS/SAMPLE No. SAMPLER TYPE TURNAROUND

MC0002 Surface Soil/ /G CN (21), TM (21)^BBto' Vadim Petrov

MC0003 Surface Soil/ /G CN (21),TM (21)*^Bsffi'v Vadim Petrov

MC0004 Surface Soil/ /G CN (21), TM (21)^Btew^ Vadim Petrov

MC0006 Surface Soil/ /G CN (21), TM (21)^^BSw" Vadim Petrov

,MCOp08 Surface Soil/ ' /G CN (21), TM (21)^^aaa* Vadim Petrov

MC0009 Surface Soil/ /G CN (21),-TM (21)^™S8*K" Vadim Petrov

MCOOD1 Surface Soil/ /G CN (21), TM (21)ssssaasn. Dennis

AndersonMCOOD2 Surface Soil/ /G CN (21), TM (21)

BBBaBa!sa!!M1" DennisAnderson

MCOOE4 Surface Soil/ /G CN(21), TM(21)DennisAnderson

MCOOE6 Surface Soil/ /G CN (21), TM(21)DennisAnderson

Date Shipped: 4/11/2005 Chain of Custody

Carrier Name: FpHF*

Airbill: 8489 8704 5822 Relinquished By

Shipped to: ChemTech Consulting 1

Group (CHEMED)284 Sheffield Street 2

Mountainside NJ UYUS^(908) 789-8900 3

4

Case No: - 34031 O (

DAS No: IX

Record SamplerSignature: ,

(Date / Time) Received By (Date / Time)

TAGNoJ STATION SAMPLE COliECT ORGANIC QCPRESERVATIVE/ Bottles LOCATION DATE/TIME SAMPLE No. TVPe

724 (Ice Only), 727 (Ice BJS-BSS10-0405 S: 4/9/2005Only) (2)

728 (Ice Only), 731 (Ice BJS-BSS2-0405 S: 4/9/2005Only) (2)

732 (Ice Only), 735 (Ice BJS-BSS3-0405 S: 4/9/2005Only) (2) .

740, 743 (Ice Only) (2) BJS-BSS5-0405 8:4/11/2005

748 (Ice Only), 751 (Ice BJS-BSS7-0405 S: 4/9/2005Only) (2)

752 (Ice Only), 755 (Ice BJS-BSS8-0405 S: 4/9/2005Only) (2)

191 3 (Ice Only), 191 9 (Ice BJS-SSD3-0405 8:4/9/2005Only) (2)

1922 (Ice Only), 1928 (Ice BJS-SSD5-0405 8:4/9/2005Only) (2)

2030 (Ice Only), 2036 (Ice BJS-SSI4-0405 S: 4/9/2005Only) (2)

2048 (Ice Only), 2054 (Ice BJS-SSJ3-0405 S: 4/9/2005Only) (2)

11:45 C0002

9:45 C0003 MS/MSD

10:00 C0004

10:30 C0006

13:00 C0008

11:10 C0009

11:58 COOD1

16:20 COOD2

14:00 COOE4

13:25 COOE6

Shipment for CaseComplete? N

Analysis Key:

CN = Cyanide, TM = CL

Sample(s) to be used for laboratory QC:

MCOOOS

Additional Sampler Signature(s):

Concentration: |_ = Low, M = Low/Medium, H = High Type/Designate: Composite = C, Grab = G

Chain of Custody Seal Number:

Shipment Iced?

PTAL 'I otal Metals

TR Number: 3-035066262-041105-0012PR provides preliminary results. Requests for preliminary results will increase analytical costs.Send Copy to: Sample Management Office, Attn: Heather Bauer, CSC, 15000 Conference Center Dr.. Chantilly, VA 20151-3819; Phone 703/818-4200; Fax F2V5.1.047 Pagel of 2

118280

SEPA USEPA Contract Laboratory ProgramInorganic Traffic Report & Chain of Custody Record

Region: 3

Project Code:T47121 0103

Account Code: 2005T03W302DD2C

CERCLIS ID: WVD054827944Spill ID:

Site Name/State: Big John Salvage CLP 34031 /WV

Project Leader: -ra(j Yancheski

Action: Remedial Investigation

Sampling Co: Tetra Tech, Inc.

INORGANIC MATRIX/ CONG/ ANALYSIS/SAMPLE No. SAMPLER TYPE TURNAROUND

MC0001 Surface Soil/ /G CN (21),TM (21)Vadim Petrov

MC0005 Surface Soil/ /G CN (21 ), TM (21 )Vadim Petrov

MC0007 Surface Soil/ /G CN (21), TM (21)Vadim Petrov

MC0010 Surface Soil/ /G CN (21 ), TM (21 )Vadim Petrov

MC0085 Subsurface /G CN(21)Soil/DouglasSeavey

MCOOD3 Surface Soil/ /G CN (21), TM (21)DennisAnderson

MCOOD4 Surface Soil/ /G CN (21), TM (21)DennisAnderson

MCOOD5 Surface Soil/ /G CN (21), TM (21)DennisAnderson

MCOOD6 Surface Soil/ /G CN (21), TM (21)DennisAnderson

Mjg£p£ Surface Soil/ /G CN (21), TM (21)DennisAnderson

Date Shipped: 4/11/2005

Carrier Name: FedEx

Airbill: 8489 8704 5833

Shipped to: ChemTech ConsultingGroup (CHEMED)284 Sheffield StreetMountainside NJ 07092(908) 789-8900

TAG No J STATIONPRESERVATIVE/ Bottles LOCATION

Case No: - 34031

DAS No:

Chain of Custody Record SamplerSignature:

Relinquished By (Date / Time) Received By

1

2

3

4

SAMPLE COLLECT ORGANICDATE/TIME SAMPLE No.

720 (Ice Only), 723 (Ice BJS-BSS1-0405 8:4/9/2005 9:10 C0001Only) (2)

R(Date / Time)

QCType

MS/MSD

736 (Ice Only), 739 (Ice BJS-BSS4-0405 8:4/9/2005 10:15 C0005Only) (2)

744 (Ice Only), 747 (Ice BJS-BSS6-0405 8:4/11/2005 12:30 C0007Only) (2)

756 (Ice Only), 759 (Ice BJS-BSS9-0405 8:4/9/2005 11:10 C0010Only) (2)

1505 (Ice Only) (1) BJS-SBH2-0405 8:4/5/2005 14:00 C0085

1931 (Ice Only), 1937 (ice BJS-SSE2-0405 5:4/9/2005 11:40 COOD3Only) (2)

1940 (Ice Only), 1946 (Ice BJS-SSE4-0405 8:4/9/2005 12:20 COOD4Only) (2)

1949 (Ice Only), 1955 (Ice BJS-SSE6-0405 8:4/9/2005 16:10 COOD5Only) (2)

1958 (Ice Only), 1964 (Ice BJS-SSF3-0405 8:4/9/2005 12:40 COOD6Only) (2)

1 976 (Ice Only), 1982 (Ice \ BJS-SSG2-0405 8:4/9/2005 11:07 COOD8Only) (2)

Shipment for CaseComplete? N

Analysis Key:

CN - Cyanide, TM - CL

Sample(s) to be used for laboratory QC:

MC0001

Additional Sampler Signature(s):

Concentration: [_ = Low, M = Low/Medium, H = High Type/Designate: Composite = C, Grab = G

Chain of Custody Seal Number:

Shipment Iced?

P TAL Total Metals

TR Number: 3-035066262-041105-0011PR provides preliminary results. Requests for preliminary results will increase analytical costs.Send Copy to: Sample Management Office, Attn: Heather Bauer, CSC, 15000 Conference Center Dr., Chantilly, VA 20151-3819; Phone 703/818-4200; Fax703/818-4602

TAN -r'O^V jpF2V5.1.047 Page 1 of 3 /V

118281

"v ' *T ,

'"^

U.S EPA Region III Analytical Request FormRAS CASE #: CT3328 3 >J-O3 1Date: 3/7/2005

DAS #: NSF#:QAPP/SAP: YES Data Validation Level: M3 & IM2

Site: BIG JOHN SALVAGE — &0U/J- /£oa_£/Address: 900 HOULT RDLatitude: 39° 29' 54"Program: SUPERFUNDAccount #: 05T03jf302DD2C0371LAOOPreparer: KYLE SWARTZWELDEROSC/RPM: CHRISTIAN MATTA ^/gugSite Leader: TAD YANCHESKIEPA CO: JIM CLARK .Analytical TAT: 14 days /tf /&Ship Date From: 4/3/05Samples4613286123

J^*V-?4/IZS/.*^1414

City: FAIRMONT ' State: WVLongitude: -80° 7 12"

CERCLiS#: WVD054827944Operable Unit:Phone: 302-738-7551

f Phone:215-814-2317Phone: 302-738-7551Contract Type: RACS

Activity: RI/FS| Spill ID: 0358

Fax: 302-454-5988 E-mail: kyle.swartzwelder@tetratech.coFax: 215-814-3002 E-mail: Matta.Christian@epamail.epa.goFax: 302-454-5988 E-mail: tad.yancheski@tetratech.comPrime: TT/BV Sub:Analytical + Validation TAT: 30 daysShip Date To: 4/15/05

Method Parameter MatrixOLM04.3 LJBRTV TCL - svocs, PEST/PCBS ONLY SOIL ^^^>(^> ^. ,2-335^ILM05.3 £,#£>) ICP-AES TAL+Hg+CN SOIL ^^ J2>£* ^OLM04.3 L.IROTV TCLOLM04.3 f .SKT/ TCL

SOIL ^-"b^i G=^-AAQ ^ ^^Ih T

ILM05.3 Cc«m|- / ICP-AES TAL +HG+CN AQ ^">> 6= 0=ILM05.3 \ ICP-AES TAL +HG -]>/vv AQOLC03.2 A if. TCL AQ J2 3 ^ (** -fILM05.3 Dffmc- ICP-MS TAL+HG+CN AQ ^ 3> "3> Go^B( kl Ml 1^1 "1 =»¥=>* <7T7nrNiT7>,TT

l l ' r Vt/lYlUT../ IV^Jj • 1 1 HA.'-.,*-

m- IEM0373 " ICP-AES TAL+HU+CN SEDIMENTInstruction: See Big John Salvage - Hoult Road Site Final Ri/Fs Work Plan - February 2005, Section 4.4 (Identification Of Potential Sampling Approaches AndAppropriate Analytical Methods) For A Complete Listing Of All Proposed Analytical Methods.

Please Provide Electronic Data Deliverables For All Data

118282

Big John Salvage - Case 34031 duplicate pairs

Samples Duplicates

COO 18 / MCOO18 C0062 / MC0062C0014/MC0014 C0059 / MC0059C0033 / MC0033 C0061 / MC0061C0030 / MC0030 C0057 / MC0057C0039 / MC0039 C0058 / MC0058COOO1 / MCOOO1 COOG1 /MCOOG1C0002 / MC0002 COOG2 /MCOOG2COOF9 / MCOOF9 COOG4 /MCOOG4COOE7 / MCOOE7 COOG5 /MCOOG5COOB2 / MCOOB2 COOC4 / MCOOC4COOA1 / MCOOA1 . COOC5 / MCOOC5C0093 / MC0093 COOC6 / MCOOC6C0077 / MC0077 COOC7 / MCOOC7C0182/MC0182 COOC8/'MCOOC8C0086 / MC0086 COOC9 / MCOOC9C0066 / MC0066 COODO / MCOODOCOOL9/MCOOL9 C0155/MC0155C0111/MC0111 C0135/MC0135C0112/MC0112 • C0156/MC0156COOL1/MCOOL1 ' C0153/MC0153C0104/MC0104 C0134/MC0134C0105/MC0105 C0154/MC01.54

118283

Case #: 34031

Site:

Lab. :

DATA SUMMARY FORM: INORGANIC (Lab Results) Page. of

SDG : MCOOAO

BIG JOHN'S HOULT RD

CHEM

Number of Soil Samples : 20

.NOmber ofWater Samples : 0

/MCOOC4

BJS-SBP1-0405

Sample Number:

Sampling Location:

MCOOAO

BJS-SBJ5-0405

MCOOA1

BJS-SBJ6-0405

MCOOC6

BJS-SBP3-0405

Matrix:

Units:

Date Sampled:

Time Sampled :

%Solids:

Dilution Factor:

Soil

mg/Kg

4/8/2005

09:00

81.0

Sl.O

CRQL = Contract Required Quantitation Limit

To calculate sample quantitation limits: (CRQL * Dilution Factor) / (%Solids/100)

SEE NARRATIVE FOR CODE DEFINITIONS

Revised 09/99

118284

DATA SUMMARY FORM: INORGANIC (Lab Results) Page. of

Case #: 34031Site:Lab.:

SDG : MCOOE4

BIG JOHN'S HOULT RD

CHEM

MCOOG4 \

BJS-SSP4-0805

Sample Number:Sampling Location

MCOOGOBJS-SSO4-0405

MCOOG1

BJS-SSP1-0405MCOOG2 |BJS-SSP2-0405

MCOOG3BJS-SSP3-0405

Matrix:Units:Date Sampled:

Time Sampled:%Solids:

Dilution Factor:

Soilmg/Kg4/9/2005

15:3585.91.0

Soilmg/Kg4/9/2005

09:1576.51.0

Soil

mg/Kg4/9/2005

11:2560.0/1,0''

Soilmg/Kg4/11/2005

16:1589.91.0

MERCURY

POTASSIUM

CRQL = Contract Required Quantitation LimitTo calculate sample quantitation limits: (CRQL * Dilution Factor) / (%Solids/100)

SEE NARRATIVE FOR CODE DEFINITIONS

Revised 09/99

118285

i'CV

Appendix D

Laboratory Case Narrative

118286

CHEMTECH284 Sheffield StreetMountainside, NJ 07092

SDG NARRATIVE

USEPASDG # MCOOA5CASE #34031CONTRACT # 68-WO-2068LAB NAME: CHEMTECH CONSULTING GROUPLAB CODE: CHEMCHEMTECH PROJECT #T2302

A. Number of Samples and Date of Receipt

20 Soil Samples were delivered to the laboratory intact on 04/12/05.

B. Parameters '

Test requested for Total Metals and Cyanide.

C. Cooler Temp

Indicator Bottle: Presence/AbsenceCooler: 4°C

D. Detail Documentation (related to Sample HandlingShipping, Analytical Problem, Temp of Cooler etc):

Issue: The TR did not designate samples for laboratory QC for a few SDGs. The lab would liketo choose samples MC0141, MCOOA1, and MC0180 for this purpose.

Issue: The lab indicated that each sample received for Case 34031 consisted of 2 soil jars (1Metals, 1 Cyanide), however sample MC0085 was only sent with one Metal jar. The lab wouldlike to know if they should use the Metals jar for sample MC0085 to analyze for Metals andCyanide.

Also,

Sample < shipped to the incorrect laboratoryIssue 1: The lab received organic samples along with their inorganic shipment. The lab receivedsamples C0068-COOC1 (on 2 TR's). Please provide an address and billing information if thesamples should be trans-shipped.

Incorrect/duplicated sample numbersIssue 2: Sample MC0125 (station location: BJS-SDMON2C3-0405) was listed on the TR asC0125.

118287

( >

CHEMTECH284 Sheffield StreetMountainside, NJ 07092

Discrepancies with tags, jars, and/or TR/COCIssue 3: All of the inorganic samples were listed on the TR/COC for DM and TM, however theseare all soil samples. The sample IDs affected are MC0117, MC0118, MC0119, MC0120,MC0121, MC0122, MC0123, MC0125, MC0126, MC0217, and MC0218.

E. Corrective Action taken for above:

Following is the resolution to the issue below:Issue: The TR did not designate samples for laboratory QC for a few SDGs. The lab would liketo choose samples MC0141, MCOOA1, and MC0180 for this purpose.Resolution: In accordance with previous direction from Region 3, for both Inorganic and OrganicMulti-Media samples, the laboratory will select a sample for laboratory QC as long as the sampleis not a PE, blank, or rinsate sample. The laboratory will note the issue in the Case/SDGNarrative, notify the SMO coordinator of the sample selected for laboratory QC, and proceedwith the analysis of the samples.SMO will note that the lab chose samples MC0141, MCOOA1, and MC0180 for laboratory QC.Please indicate which SDG each of these samples is assigned to for laboratory QC.

Following is the resolution to the issue below:Issue: The lab indicated that each sample received for Case 34031 consisted of 2 soil jars (1Metals, 1 Cyanide), however sample MC0085 was only sent with one Metal jar. The lab wouldlike to know if they should use the Metals jar for sample MC0085 to analyze for Metals andCyanide.Resolution: Per Region 3, it is acceptable for the lab to analyze for Metals and Cyanide from theMetal jar for sample MC0085.

Also,

Following is an update to the Record of Communication of Case 34031. For issue 3, the sampleIDs affected are now listed.Samples shipped to the incorrect laboratoryIssue 1: The lab received organic samples along with their inorganic shipment. The lab receivedsamples C0068-COOC1 (on 2 TR's). Please provide an address and billing information if thesamples should be trans-shipped.Resolution 1: Per Region 3, the Tetra Tech air bill voucher number for the organic samplesmistakenly sent to CHEM that require transshipment is: 0191-2082-l.L The samples should besent to the following address:Liberty Analytical501 M_adison Ave.Gary, NC 27513919-379-4081

5118288

CHEMTECH284 Sheffield StreetMountainside, NJ 07092

Incorrect/duplicated sample numbersIssue 2: Sample MC0125 (station location: BJS-SDMON2C3-0405) was listed on the TR asC0125.Resolution 2: Per Region 3, the laboratory should report sample CO 125 under the new sample IDMCI AP2, note the situation in the Case/SDG Narrative, and proceed with the analysis of thesamples.Discrepancies with tags, jars, and/or TR/COCIssue 3: All of the inorganic samples were listed on the TR/COC for DM and TM, however theseare all soil samples. The sample IDs affected are MC0117, MC0118, MC0119, MC0120,MC0121, MC0122, MC0123, MC0125, MC0126, MC0217, and MC0218.Resolution 3: Per Region 3, the lab should only analyze the soil samples for total metals analysisand disregard the dissolved metals analysis. Please note this situation in the Case/SDG Narrativeand proceed with the analysis of the samples.

I * :

F. Analytical Techniques:

All analyses were based on CLP Methodology by method ILM05.3

G. Calculation:

Conversion of results from mg/L to mg/kg (Dry Weight Basis): .

Mg/Kg = (Result in mg/L) X 1000 X 100/ % Solid X Fraction of Sample Amount Taken in Prep.

G. QA/ QC

Calibrations met requirements. Interference check met requirements. Blank analyses did not indicateany presence of contamination. Laboratory Control sample was within control limits. Spike sample didmet requirements except for the Manganese. Duplicate sample did met requirements except for the Lead.Serial Dilution did met requirements except for Chromium and Cobalt.

I certify that the data package is in compliance with the terms and conditions of the contract bothtechnically and for completeness, for other than the conditions detailed above. Release of the datacontained in this hard copy data package has been authorized by the Laboratory Director or his designee,as verified by the following signature.

Name: Parveen Hasan

Title: EPA QA/QC OFFICER

118289

'Y'

CHEMTECH284 Sheffield StreetMountainside, NJ 07092

SDG NARRATIVE

USEPASDG#MCOOD1CASE #34031CONTRACT # 68-WO-2068LAB NAME: CHEMTECH CONSULTING GROUPLAB CODE: CHEMCHEMTECH PROJECT #T2299

A. Number of Samples and Date of Receipt

20 Soil Samples were delivered to the laboratory intact on 04/12/05.

B. Parameters • < <

Test requested for Total Metals and Cyanide..

C. Cooler Temp

Indicator Bottle: Presence/AbsenceCooler: 4°C

D. Detail Documentation (related to Sample HandlingShipping, Analytical Problem, Temp of Cooler etc):

Issue: The TR did not designate samples for laboratory QC for a few SDGs. The lab would liketo choose samples MC0141, MCOOA1, and MC0180 for this purpose.

Issue: The lab indicated that each sample received for Case 34031 consisted of 2 soil jars (1Metals, 1 Cyanide), however sample MC0085 was only sent with one Metal jar. The lab wouldlike to know if they should use the Metals jar for sample MC0085 to analyze for Metals andCyanide.

Also,

Samples shipped to the incorrect laboratoryIssue 1: The lab received organic samples along with their inorganic shipment. The lab receivedsamples C0068-COOC1 (on 2 TR's). Please provide an address and billing information if thesamples should be trans-shipped.

Incorrect/duplicated sample numbersIssue 2: Sample MC0125 (station location: BJS-SDMON2C3-0405) was listed on the TR asC0125.

118290

C/

CHEMTECH284 Sheffield StreetMountainside, NJ 07092

Discrepancies with tags, jars, and/or TR/COCIssue 3: All of the inorgaric samples were listed on the TR/COC for DM and TM, however theseare all soil samples. The sample IDs affected are MC0117, MC0118, MC0119, MC0120,MC0121, MC0122, MC0123, MC0125, MC0126, MC0217, and MC0218.

E. Corrective Action taken for above:

Following is the resolution to the issue below:Issue: The TR did not designate samples for laboratory QC for a few SDGs. The lab would liketo choose samples MCO141, MCOOA1, and MCO180 for this purpose.Resolution: In accordance with previous direction from Region 3, for both Inorganic and OrganicMulti-Media samples, the laboratory will select a sample for laboratory QC as long as the sampleis not a PE, blank, or rinsate sample. The laboratory will note the issue in the Case/SDGNarrative, notify the SMO coordinator of the sample selected for laboratory QC, and proceedwith the analysis of the samples.SMO will note that the lab chose samples MC0141, MCOOA1, and MC0180 for laboratory QC.Please indicate which SDG each of these samples is assigned to for laboratory QC.

Following is the resolution to the issue below:Issue: The lab indicated that each sample received for Case 34031 consisted of 2 soil jars (1Metals, 1 Cyanide), however sample MC0085 was only sent with one Metal jar. The lab wouldlike to know if they should use the Metals jar for sample MC0085 to analyze for Metals and .Cyanide.Resolution: Per Region 3, it is acceptable for the lab to analyze for Metals and Cyanide from theMetal jar for sample MC0085.

Also,

Following is an update to the Record of Communication of Case 34031. For issue 3, the sampleIDs affected are now listed.Samples shipped to the incorrect laboratoryIssue 1: The lab received organic samples along with their inorganic shipment. The lab receivedsamples C0068-COOC1 (on 2 TR's). Please provide an address and billing information if thesamples should be trans-shipped.Resolution 1: Per Region 3, the Tetra Tech air bill voucher number for the organic samplesmistakenly sent to CHEM that require transshipment is: 0191-2082-1. The samples should besent to the following address:Liberty Analytical501 Madison Ave.Gary, NC 27513919-379-4081

5118291

CHEMTECH284 Sheffield StreetMountainside, NJ 07092

Incorrect/duplicated sample numbersIssue 2: Sample MC0125 (station location: BJS-SDMON2C3-0405) was listed on the TR asC0125.Resolution 2: Per Region 3, the laboratory should report sample CO 12'j under the new sample IDMCI AP2, note the situation in the Case/SDG Narrative, and proceed with the analysis of thesamples.Discrepancies with tags, jars, and/or TR/COCIssue 3: All of the inorganic samples were listed on the TR/COC for DM and TM, however theseare all soil samples. The sample IDs affected are MC0117, MC0118, MC0119, MC0120,MC0121, MC0122, MC0123, MC0125, MC0126, MC0217, and MC0218.Resolution 3: Per Region 3, the lab should only analyze the soil samples for total metals analysisand disregard the dissolved metals analysis. Please note this situation in the Case/SDG Narrativeand proceed with the analysis of the samples.

r ' t

F. Analytical Techniques:

All analyses were based on CLP Methodology by method ILM05.3

G. Calculation:

Conversion of results from mg/L to mg/kg (Dry Weight Basis):

Mg/Kg = (Result in mg/L) X 1000 X 1007 % Solid X Fraction of Sample Amount Taken in Prep.

G. QA7 QC

Calibrations met requirements. Interference check met requirements. Blank analyses did not indicateany presence of contamination. Laboratory Control sample was within control limits. Spike sample didmet requirements except for Few Elements. Duplicate sample did met requirements except for theCalcium . Serial Dilution did met requirements except for Few Elements.

I certify that the data package is in compliance with the terms and conditions of the contract bothtechnically and for completeness, for other than the conditions detailed above. Release of the datacontained in this hard copy data package has been authorized by the Laboratory Director or his designee,as verified by the following signature.

Name: Parveen Hasan

Title: EPA QA/QC OFFICER

^^^ . • I\ ^* lx"»!S

118292

^Message Page 2 of 5

Resolution 1: Per Region 3, the Tetra Tech air bill voucher number for the organic samples mistakenlysent to CHEM. that require transshipment is: 0191 -2082-1, The samples should be sent to the followingaddress: ' . •

Liberty" Analytical . , • ' • •501 Madison Ave.Gary,-NC 27513 .919-379-4081. . '

Incorrect/duplicated sample numbersIssue 2: Sample MC0125 (station location: BJS-SDMON2C3-0405) was listed on' the TR as C0125.Resolution 2: Per Region 3, the laboratory should report sample C0125 under the new sample ID

• MCI AP2, note the situation in'the Case/SDG Narrative, and proceed with the analysis of the samples.

Discrepancies with tags. |ars. and/or TR/COCIssue 3: All of the inorganic samples were listed on the TR/COC for DM and TM, however these areall soil samples.Resolution 3: Per Region 3, the lab should only analyze the soil samples for total metals analysisand disregard the dissolved metals .analysis. Please note this situation in the Case/SDG Narrative 'andproceed with the analysis of the samples.

Please let Mike or me know if you have any questions or problems.

Michael BenhoffComputer Sciences CorporationCLP Coordinator for Regions 1, 2, and 3 •michael.benhoff@dyncorp.cpm '.Phone: (703) 818-4357;JFax: (703)818-4602

Original MessageFrom: Slizys.Dan@epamail.epa.govSent: Tuesday, April 12, 2005 6:44 AM. ' •To: Benhoff, Michael ., ' .Cc: jeffery.betty@epamail.epa.gov; kwedar.jphn@epamail.epa.gov; thaung.khin-cho@epamail.epa.govSubject: Re: NEW ISSUE - Region 3 | Case 34031 | Lab CHEM | Issue Multiple

Mike, . •

Issue 1: SMO can provide trans-shipment information to the lab.Issue 2: No, SMO should not ask the lab to change C0125 to MC0125. A memo to fl'.e from fieldpersonnel will clarify this issue. The lab will use CO 125 as sample ED when reportin {results or SMOcan provide a new CLP sample ID number.Issue 3: Yess the lab should only analyze for total metals. Disregard the dissolved metals analysis.

—^-Original Message—From: Benhoff, Michael

• Sent: Monday, April 11, 2005 3:58 PMTo: Betty Jeffery (E-mail); Dan Slizys (E-mail); John Kwedar (E-mail); Khin-Cho Thaung (E-mail)

. Subject: NEW ISSUE - Region 3 [Case 34031 | Lab CHEM | Issue Multiple

This is Carolyn Mack - Mike is out of the office, today.

4984/13/2005

118293

Message - . Page 4 of 5

i

. Subject: RE: NEW ISSUE | Case 34031 | Lab CHEM' | Issue Multiple - Trans Sh ip Information

Hi Dan -

The Tetra Tech air bill voucher number for the organic samples mistakenly sent to CHEM that require transshipment is:

0191-2082-1 •

Liberty Analytical.501 Madison Ave.Cary,NC27513919-379-4081 ' .

Memo's to file will be prepared for the other issues at a later date.

• . Please advise if you have any questions.

Regards,

TadYancheskifetraTech

. 302-738-7551

Original Message - . 'From: Sli2ys.Dan@.epamail. epa.govSent: Monday, April 11, 2005 9:46 AMTo: Benhoff, Michael; kyle.swartzwelder@tefa-atech.com: tad.yancheski@tetrateGh.coni

x Cc: jeffery.betty@epamail.epa.gov; kwedar.jobn@eparhail.epa,gov: tfaaung.kbin-oho@epamaiLepa.govSubject: Re: NEW ISSUE | Case 34031 | Lab CHEM | Issue Multiple

Mike,'

The field personnel will be contacted. The lab should proceed with the analysis of samples anddocument all issues in the ease narrative. Kyle arid Tad,

There are more issues which need your attention:Issue 1: The lab received organic samples that may have to be trans-shipped. We 'will need air bill :-voucher. ' • ' • \Issue 2: MC0125 listed on the TR/COC as sample C0125. Need a memo to file for clarification. jIssueS: Soil samples on the TR/COC are listed as for total and dissolved metals analysis. Need a memoto file/or clarification. . . •

j

Original Message ' . jFrom: Benhoff, Michael ' • • . . " ; jSent: Friday, April 08, 2005 4:45 PM . • | jTo; Betty Jeffery (E-mail); Dan Slizys-(E-mail); John Kwedar (E-mail); Khin-Cho Thaung (E-mail) . . j |

. Subject: NEW ISSUE | Case 34031 | Lab CHEM [ Issue Multiple < • • ' I IDan:. . ' • j !

! |

Please advise on the foil owing issues: • I j

Issue 1: The lab received organic samples along with their inorganic shipment. The lab received j I

50Q j4/13/2005

118294

Message Pa^e 1 of 3

Parveen Hasan

From: Benhoff, Michael [mbenhoff@fedcsc.com]

Sent: Wednesday, April 13, 2005 10:08 AM

To: Divya Mehta (E-mail); Parveen Hasan (E-mail)

Subject: Region 03 | Case 34031 | Lab CHEM | Issue Insufficient/inappropri ate designation of laboratory QC

Hi Parveen:

Following is the resolution to the issue below: - '

Issue: The TR did not designate samples for laboratory QC for a few SDGs. The lab would like to choosesamples MC0141, MCOOA1, and MCO180 for this purpose.

Resolution: In accordance with previous direction from Region 3, for both Inorganic and Organic Multi-Media samples, the laboratory will select a sample for laboratory QC as long as the sample is not a PE, blank,or rinsate sample. The laboratory will note the issue in the Case/SDG Narrative, notify the SMO coordinatorof the sample selected for laboratory QC, and proceed with the analysis of the samples.

SMO will note that the lab chose samples MC0141, MCOOA1, and MC0180 for laboratory QC. Pleaseindicate which SDG each of these samples is assigned to for laboratory QC.

thanks,Mike

Michael BenhoffComputer Sciences CorporationCLP Coordinator for Regions 1,2, and 3michael.benhofi@dyncorp.comPhone: (703) 818-4357; Fax: (703)818-4602

This is a PRIVATE message. If you are nol the intended recipient, please delete without copying and kindly advise us by e-mail ofthe mistake in delivery. NOTE: Regardless of content, this e-mail shall not operate to bind CSC to any order or other contractunless pursuant lo explicit written agreement or government initiative expressly permitting the use of e-mail for such purpose.

Original Message—-- . '• .Frorh: Parveen Hasan [mailto:parveen@Chemtech.net]Sent: Tuesday, April 12, 2005 4:57 PMTo: 'Benhoff, Michael1

Subject: RE: Region 03 | Case 34031 | Lab CHEM | Issue Insufficient volume | FINAL

Mike,

No Lab QC samples assigned for few SDGs. Lab is planning to take sample MC0141, MCOOA1 and MC0180 as LabQC, as long these are not PE and Filed Blank. Its that OK w/ the Region?

Thanks

Parveen Hasan

5024/13/2005

118295

Message - ' Page 3 of 3

From: Benhoff, MichaelSent: Tuesday, April 12, 2005 11:48 AMTo: Betty Jeffery (E-mail); Dan Slizys (E-mail); John Kwedar (E-mail); Khin-Cho Thaung (E-mail)Subject: NEW ISSUE | Case 34031 | Lab CHEM | Issue Insufficient volumeDan:

Please advise on the following issue.

Issue: The lab indicated that each sample received for Case 34031 consisted of 2 soil jars (1 Metals, 1Cyanide);, however sample MC0085 was only sent with one Metal jar. The lab would like to know ifthey should use the Metals jar for sample MC0085 to analyze for Metals and Cyanide. •

Mike

Michael BenhoffComputer Sciences CorporationCLP Coordinator for Regions 1, 2, and 3michael.benlioff@dyncorp.coniPhone: (703) 818-4357; Fax: (703)818-4602

Original Message--—From: Benhoff, MichaelSent: Thursday, April 07, 2005 1:55 PMTo: Betty Jeffery (E-mail); Dan Slizys (E-mail); John Kwedar (E-mail); Khin-Cho Thaung (E-mail)Subject: NEW ISSUE | Case 34031 | Lab CHEM | Issue Insufficient volume

Dan:

Please advise on the following issue:

Issue: The lab indicated that each sample received for Case 34031 consisted of 2 soil jars (1 Metals, 1Cyanide), however sample MC0085 was only sent with one Metal jar. The lab would like to know ifthey should use the Metals jar for sample MC0085 to analyze for Metals and Cyanide.

thanks,Mike

Michael BenhoffComputer Sciences CorporationCLP Coordinator for Regions 1,2, and 3michael.benhoff@dyncorp.comPhone: (703) 818-4357; Fax: (703)818-4602

This is a PRIVATE message. If you are not the intended recipient, please delete without copyiti.j and kindly advise us by e-niail of the mistake in delivery. NOTE: Regardless of content, this e-mail shall not operate to bind CSC to any order orother contract unless pursuant to explicit written agreement or government initiative expressly permitting the use of e-mailfor such puipose.

4/7/2005 Parveen Hasan, CHEM, contacted Mike Benhoff, SMO regarding Case 34031. The labindicated that each sample consisted of 2 soil jars (1 Metals, 1 Cyanide), however sample MC0085 wasonly sent with one Metal jar. The lab would like to know if they should use the Metals jar for sampleMC0085 to analyze for Metals and Cyanide.

504118296

v\*" < *v

'V'',

Pase2 of 2

should lose the Metals jar for sample MC0085 to analyze for Metals and Cyanide.

Mike

Michael BenhoffComputer Sciences CorporationCLP Coordinator for Regions 1, 2; and 3michael.benhofif@dyncorp.comPhone: (703) 818-4357; Fax: (703)818-4602

Original Message——Frofn: Benhoff, MichaelSent: Thursday, April 07, 2005 1:55 PMTo: Betty Jeffery (E-mail); Dan Slizys (E-mail); John Kwedar (E-mail); Khin-Cho Thaung (E-mail)Subject: NEW ISSUE | Case 34031 | Lab CHEM | Issue Insufficient volume

Dan:

Please advise on the following issue:

Issue: The lab indicated that each sample received for Case 34031 consisted of 2 soil jars (1 Metals, 1Cyanide), however sample MC0085 was only sent with one Metal jar. The lab would like to know if theyshould use the Metals jar for sample MC0085 to analyze for Metals and Cyanide.

thanks,Mike . • -

Michael Benhoff :Computer Sciences CorporationCLP Coordinator for Regions 1,2, and 3inichael.beahoff@djT3Corp.comPhone: (703) 818-4357; Fax: (703)818-4602

This is a PRIVATE message. If you are not the intended recipient, please delete without copying and kindly advise us by e-mail ofthe mistake in delivery. NOTE: Regardless of content, this e-mail shall not operate to bind CSC to any order or other contractunless pursuant to explicit written agreement or government initiative expressly permitting rhe use of e-mail for such purpose.

4/7/2005 Parveen Hasan, CHEM, contacted Mike Benhoff, SMO regarding Case 34031. The lab indicatedthat each sample consisted of 2 soil jars (1 Metal's, 1 Cyanide), however sample MC0085 was only sent withone Metal jar. The lab would like to know if they should use the Metals jar for sample MC0085 to analyze'for Metals and Cyanide.

4/1979.00^506118297

Message . Page 2 of 5

Resolution 1: Per Region 3, the Tetra Tech air bill voucher number for the organic samples mistakenlysent to CHEM that require transshipment is: 0191-2082-1, The samples should be sent to the followingaddress: '

Liberty" Analytical .501 Madison Ave.Gary, NC 27513919-379-4081

Incorrect/duplicated sample numbersIssue 2: Sample MCO125 (station location: BJS-SDMQN2C3-0405) was listed on the TR as C0125.Resolution 2: Per Region 3, the laboratory should report sample C0125 under the new sample ID

- MC1AP2, note the situation in the Case/SDG Narrative, and proceed with the analysis of the samples.

Discrepancies with tags, jars, and/or TR/COCIssue 3: All of the inorganic samples were listed on the TR/COC for DM and TM, however these areall soil samples. . .Resolution 3: Per Region 3, the lab should only analyze the soil samples for total metals analysisand disregard the dissolved metals analysis. Please note this situation in the Case/SDG Narrative andproceed with the analysis of the samples.

Please let Mike or me know if you have ariy questions or problems.

Michael BenhoffComputer Sciences CorporatioflCLP Coordinator for Regions 1,2, and 3 •michael.benhof@djTicorp.comPhone: (703) 818-4357; Fax: (703)818-4602 .

Original Message—-From: Slizys.Dan@epamail.epa.govSent: Tuesday, April 12, 2005 6:44 AM •To: Benhoff, MichaelCc: jeffery.betty@epamail.epa.gov; kwedar.john@epamail.epa.gov; thaung,khin-cho@epamail.epa.gov

. Subject: Re: NEW ISSUE - Region 3 | Case 34031 | Lab CHEM | Issue Multiple

Mike,

Issue 1: SMO can provide trans-shipment information to the lab.Issue 2: No, SMO should not ask the lab to change C0125 to MC0125. A memo to file from fieldpersonnel will clarify this issue. The lab will use CO 125 as sample ID when reporting results or SMOcan provide a new CLP sample ID number.Issue 3: Yes, the lab should only analyze for total metals. Disregard the dissolved metals analysis.

—^-Original MessageFrom: Benhoff, MichaelSent; Monday, April 11, 2005 3:58 PM "To: Betty Jeffery (E-mail); Dan Slizys (E-mail); John Kwedar (E-mail); Khin-Cho Thaung (E-mail)

. Subject: NEW ISSUE - Region 3 | Case 34031 ) Lab CHEM | Issue Multiple.

This is Carolyn Mack - Mike is out of the office, today.

508118298

Message Page 4 of 5

. Subject: RE: NEW ISSUE | Case 34031 | Lab CHEM' | Issue Multiple - Trans Sh ip Information

Hi Dan -

The Tetra Tech air bill voucher number for the organic samples mistakenly sent to CHEM that require transshipment is:

0191-2082-1 '

Liberty Analytical501 Madison Ave.Gary, NC 27513 ' '919-379-4081

Memo's to file will be prepared for the other issues at a later date.

Please advise if you have any questions.

Regards,

TadYancheskifetraTech302-738-7551 %

Original Message ., -From: Slizys.Dan@epamaii.epa.govSent: Monday, April 11,2005 9:46 AM .To: Benhoff, Michael; kyle.swart2welder@tetratech.com: tad.yanchesM(Sjtetratech.comCc: jefFery.berty@eparnaiI.epa.gov; kwedar. iohn@epamail.epa.gov; thaung.Mim-cho@epamaiLepa.govSubject: Re: NEW ISSUE | Case 34031 | Lab CHEM | Issue Multiple

Mike/ . ' '

The field personnel will be contacted. The lab should proceed with the analysis of samples anddocument all issues in the ease narrative. Kyle and Tad,

There are more issues which heed your attention:Issue 1: The lab received organic samples that may have to be trans-shipped. We will need air billvoucher. ' 'Issue 2: MC0125 listed on the TR/COC as sample CO 125. Need a memo to file for clarification.IssueS: Soil samples on the TR/COC are listed as for total and dissolve 1 metals analysis. Need a memoto file for clarification.

Original Message . -From: Benhoff, Michael • •Sent: Friday, April 08,2005 4:45 PM . •To: Betty Jeffery (E-mail); Dan Sl'izys (E-mail); John Kwedar (E-mail); Khin-Cho Thaung (E-mail)

. Subject: NEW ISSUE] Case 34031 | Lab CHEM f Issue Multiple - .Dan:. . •

Please advise on the following issues: II

Issue 1: The lab received organic samples along with their inorganic shipment. The lab received !

5104/13/2005

118299