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DUAL VIEW ICP-OES MINUS THE WAIT Introducing the Agilent 5100 ICP-OES September 23, 2015 1
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Page 1: DUAL VIEW ICP-OES MINUS THE WAIT · 2016-09-11 · DUAL VIEW ICP-OES MINUS THE WAIT Introducing the Agilent 5100 ICP-OES September 23, 2015 1. September 23, 2015 Agilent Confidential

DUAL VIEW ICP-OESMINUS THE WAITIntroducing the Agilent 5100 ICP-OES

September 23, 2015

1

Page 2: DUAL VIEW ICP-OES MINUS THE WAIT · 2016-09-11 · DUAL VIEW ICP-OES MINUS THE WAIT Introducing the Agilent 5100 ICP-OES September 23, 2015 1. September 23, 2015 Agilent Confidential

September 23, 2015

Agilent Confidential

2

Benefits. Technology & Design. Analytical Performance.

Page 3: DUAL VIEW ICP-OES MINUS THE WAIT · 2016-09-11 · DUAL VIEW ICP-OES MINUS THE WAIT Introducing the Agilent 5100 ICP-OES September 23, 2015 1. September 23, 2015 Agilent Confidential

Introducing the Agilent 5100 ICP-OES SVDV

September 23, 2015

3

• Highest throughput with highest performance

• Dichroic Spectral Combiner (DSC) technology enables

axial and radial measurements at the same time.

Page 4: DUAL VIEW ICP-OES MINUS THE WAIT · 2016-09-11 · DUAL VIEW ICP-OES MINUS THE WAIT Introducing the Agilent 5100 ICP-OES September 23, 2015 1. September 23, 2015 Agilent Confidential

How does the 5100 DSC technology work?Patented DSC technology for ICP-OES provides DV without compromise.

• Single reading of the plasma for both radial and axial.

• Vertical torch gives high matrix capability

September 23, 2015

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Dichroic

Spectral

Combiner

(DSC)

To detector

Mirror

DSCHole

Vertical

torch

5100 SVDV Pre-optics5100 SVDV Mode Selector

Page 5: DUAL VIEW ICP-OES MINUS THE WAIT · 2016-09-11 · DUAL VIEW ICP-OES MINUS THE WAIT Introducing the Agilent 5100 ICP-OES September 23, 2015 1. September 23, 2015 Agilent Confidential

Vertical Torch

• Easy-Fit

• Auto gas connected

• Auto aligned to axial preoptics

• Design enables 25% TDS

• 5 x longer life compared to

horizontal quartz torches

• High sensitivity

September 23, 2015

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Page 6: DUAL VIEW ICP-OES MINUS THE WAIT · 2016-09-11 · DUAL VIEW ICP-OES MINUS THE WAIT Introducing the Agilent 5100 ICP-OES September 23, 2015 1. September 23, 2015 Agilent Confidential

Future Proof Your Lab5100 SVDV ICP-OES is 4 instruments in 1

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2. Radial Mode 3. Axial Mode1. Synchronous VDV Mode

4. Conventional Dual View Mode

+

RAD AX

Page 7: DUAL VIEW ICP-OES MINUS THE WAIT · 2016-09-11 · DUAL VIEW ICP-OES MINUS THE WAIT Introducing the Agilent 5100 ICP-OES September 23, 2015 1. September 23, 2015 Agilent Confidential

Optics

September 23, 2015

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• Computer optimized echelle optical design

• Single entrance slit

• Single VistaChip II CCD detector

• No moving parts in polychromator

• 400mm focal length thermostatted to +35°C• CaF2 cross disperser and echelle grating

• Mass flow controlled polychromator purge (argon or nitrogen)

Page 8: DUAL VIEW ICP-OES MINUS THE WAIT · 2016-09-11 · DUAL VIEW ICP-OES MINUS THE WAIT Introducing the Agilent 5100 ICP-OES September 23, 2015 1. September 23, 2015 Agilent Confidential

September 23, 2015

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Page 9: DUAL VIEW ICP-OES MINUS THE WAIT · 2016-09-11 · DUAL VIEW ICP-OES MINUS THE WAIT Introducing the Agilent 5100 ICP-OES September 23, 2015 1. September 23, 2015 Agilent Confidential

5100 Configurations

5100 SVDV

5100 VDV

5100 RV

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Page 10: DUAL VIEW ICP-OES MINUS THE WAIT · 2016-09-11 · DUAL VIEW ICP-OES MINUS THE WAIT Introducing the Agilent 5100 ICP-OES September 23, 2015 1. September 23, 2015 Agilent Confidential

High Specification 5100 configurationsFeatures 5100 SVDV 5100 VDV 5100 RV

Dichroic Spectral Combiner (DSC) O

Vertically orientated torch

Cool Cone Interface

Robust, solid-state 27MHz RF generator

Second generation VistaChip II CCD detector

Mass flow controlled nebulizer, plasma gas, auxiliary gas

Mass Flow Controlled make-up gas for accessories like Sheath Torch

Easy-fit torch

167 to 785 nm wavelength range

Double Pass S/C, Seaspray Nebuliser, Easy Fit Torch, sample and waste pump tubes

Oxygen Addition O

5 Channel Pump O

2 & 3 port gas control O

ICP Expert 7 software

Pro Software O

HP PC, HP Monitor and HP Printer

= included

O = optional

= not included

September 23, 2015

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Page 11: DUAL VIEW ICP-OES MINUS THE WAIT · 2016-09-11 · DUAL VIEW ICP-OES MINUS THE WAIT Introducing the Agilent 5100 ICP-OES September 23, 2015 1. September 23, 2015 Agilent Confidential

Benefits of the 5100

• Fastest sample throughput of difficult samples

• Low gas consumption

Lowest cost of ownership

• Analytical performance

• System robustness and reliability

Enhanced Performance

• Hardware

• Software

Simple Operation

September 23, 2015

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Page 12: DUAL VIEW ICP-OES MINUS THE WAIT · 2016-09-11 · DUAL VIEW ICP-OES MINUS THE WAIT Introducing the Agilent 5100 ICP-OES September 23, 2015 1. September 23, 2015 Agilent Confidential

1. Lowest cost of ownership

• High throughput facilitates low Ar consumption per sample

- (a) DSC. (b) VistaChip II. (c) 80 rpm pump. (d) SVS 2+

• 50% Lower power and 50% lower exhaust requirements.

• 27MHz Solid State RF

• Robust vertical torch

• Increased self maintainability

September 23, 2015

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Ar L/sample5100

SVDV5100

VDV Vendor A Vendor B

USEPA 200.7

(min) 1 1.5 2.2 2.36

Ar L/sample 20.4 30.6 37.29 43.0228

Valve/No Valve Valve Valve Valve Valve

0

5

10

15

20

25

30

35

40

45

50

5100 SVDV 5100 VDV Vendor A Vendor B

Ar L/sample

Page 13: DUAL VIEW ICP-OES MINUS THE WAIT · 2016-09-11 · DUAL VIEW ICP-OES MINUS THE WAIT Introducing the Agilent 5100 ICP-OES September 23, 2015 1. September 23, 2015 Agilent Confidential

2. Enhanced Performance Long Term Stability

• 4Hr Long Term Stability with complex matrix

• 25% NaCl spiked with 250 ppb multi-element solution

• <2.4% RSD

0%

20%

40%

60%

80%

100%

120%

140%

0:00:00 0:28:48 0:57:36 1:26:24 1:55:12 2:24:00 2:52:48 3:21:36 3:50:24 4:19:12

% R

ead

back

Time (h:mm:ss)

As 188.980 Cd 228.802 Pb 220.353 Se 196.026

250ppb As/Se/Pb/Cd solution in 25% NaCl

September 23, 2015

13

Page 14: DUAL VIEW ICP-OES MINUS THE WAIT · 2016-09-11 · DUAL VIEW ICP-OES MINUS THE WAIT Introducing the Agilent 5100 ICP-OES September 23, 2015 1. September 23, 2015 Agilent Confidential

3. Simple Operation

• Plug-and-play torch and SIS

• Enhanced user maintainability

- Pre optic window (axial and radial)

- Optics gas filter

September 23, 2015

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Page 15: DUAL VIEW ICP-OES MINUS THE WAIT · 2016-09-11 · DUAL VIEW ICP-OES MINUS THE WAIT Introducing the Agilent 5100 ICP-OES September 23, 2015 1. September 23, 2015 Agilent Confidential

3. Simple Operation

• ICP Expert V7 software

- Intuitive workflow

- Applet methods for simple

startup

• e-Familiarization DVD videos

- Software

- Hardware

- Routine Maintenance

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Page 16: DUAL VIEW ICP-OES MINUS THE WAIT · 2016-09-11 · DUAL VIEW ICP-OES MINUS THE WAIT Introducing the Agilent 5100 ICP-OES September 23, 2015 1. September 23, 2015 Agilent Confidential

Environmental Food & Agriculture Materials Science Chemical & EnergyPharmaceuticals

Drinking and natural water Trace toxic metals in food Mining and Metals Petroleum refining Heavy metals

(USP<232>/<233>)

Soil and sediment Nutrient elements Toys and Consumer Products Alternative Energy (Biodiesel) Incoming raw material testing

Waste (solids/liquids/gases) Feed and fertilizer Semicon, Ceramics, Batteries Fine and Bulk Chemicals QA/QC of Final Product

Where can Agilent 5100 ICP-OES be used?

Performance (technology)

• Speed/low gas costs (SVDV, Vista Chip II)

• EIE interference immunity (SVDV)

• LDR (VistaChip II)

• Resolution/interference minimization

(Echelle optics, FACT/IEC, Fitted

Background Correction)

• Usability (Software, Easy Fit Torch)

Performance (technology)

• Highly stable plasma system (SSRF)

• Matrix tolerance and robust sample intro

(Vertical torch, HF resistant SIS)

• Long term stability (MFC, Thermostatted

optics)

September 23, 2015

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Page 17: DUAL VIEW ICP-OES MINUS THE WAIT · 2016-09-11 · DUAL VIEW ICP-OES MINUS THE WAIT Introducing the Agilent 5100 ICP-OES September 23, 2015 1. September 23, 2015 Agilent Confidential

Na 5100 ICP-OES SVDV mode Linear Dynamic Range

September 23, 2015

17

R² = 0.9998

0

5

10

15

20

0 500 1000 1500 2000 2500 3000

EM

ISS

ION

IN

TE

NS

ITY

X1

06

[SODIUM] PPM

Na 588.995nm

Calibrated between 0.1-2500ppm

Page 18: DUAL VIEW ICP-OES MINUS THE WAIT · 2016-09-11 · DUAL VIEW ICP-OES MINUS THE WAIT Introducing the Agilent 5100 ICP-OES September 23, 2015 1. September 23, 2015 Agilent Confidential

Agilent’s Accelerating Innovation in Atomic Spectroscopy

2009 2012 20142011

Enabling a new

level of ease of

use in ICP-MS

World’s First ICP-QQQ

Agilent MP-AES

4100

8800

7700

Agilent MP-AES

4200

7900Agilent ICP-MS

2013

Next Generation

ICP-OES

23 September 2015

18

July 2014

Page 19: DUAL VIEW ICP-OES MINUS THE WAIT · 2016-09-11 · DUAL VIEW ICP-OES MINUS THE WAIT Introducing the Agilent 5100 ICP-OES September 23, 2015 1. September 23, 2015 Agilent Confidential

Agilent 5100 ICP-OES summary

Lowest cost of ownership

Enhanced Performance

Simple Operation

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Page 20: DUAL VIEW ICP-OES MINUS THE WAIT · 2016-09-11 · DUAL VIEW ICP-OES MINUS THE WAIT Introducing the Agilent 5100 ICP-OES September 23, 2015 1. September 23, 2015 Agilent Confidential

Questions

September 23, 2015

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