201079

Lockheed Martin Technology Services Environmental Services REAC 2890 Woodbridge Avenue Building 209 Annex Edison, NJ 08837-3679 Telephone 732-321-4200 Facsimile 732-494-4021

ADC2.8439

1Zy\y \\ lo

LOCKHEED A HTT~H~^

FINAL DATE: September 29, 2006

TO: Jeff Catanzarita, U.S. EPA/ERT

THROUGH: Jeffrey Bradstreet, REAC Air Response Section Leader

FROM: Michael Gemelli, REAC Task Leade; e

SUBJECT: AMERICAN DRIVE-IN CLEANERS SITE, LEVITTOWN, NY WORK ASSIGNMENT #EAC00114 - TRIP REPORT

BACKGROUND

The American Drive-In Cleaners (ADC) Site encompasses approximately 16,000 square feet (sf) or 0.37 acres of land located at 3801 Hempstead Turnpike, Levittown, Nassau County, New York. The site includes a single masonry block structure, approximately 4,800 sf in size. Currently, the building is occupied by a number of tenants including- ADC (west side ofthe building), Urban Speed Outfitters, Christine's Alteration Shop, Robert's Barber Shop, and Blimpie Subs (east side of building). '

Chainlink fences are located at the property boundary to the west and to the north. A building (Beverage Discount Center) is located near the east boundary of the property and the right-of-way of Hempstead Turnpike is alone the southern boundary ofthe property. The areas immediately adjacent to the on-site building include unpaved areas to the east, west, and north. A parking area, approximately 8,000 sf, is located south of the on-site buildine alnno A Hempstead Turnpike. ^ 8 m e

The New York State Department of Environmental Conservation (NYSDEC) had an interim soil vapor extraction (SVE) system installed in the rear ofthe ADC Site to treat contaminated soil. The SVE system was installed by the NYSDEC contractor as part of an emergency remediation program for the Site. Piping for the SVE treatment system extends from the rear ofthe ADC Site to the recovery wells located on the east, north, and south side ofthe Site. While indoor a' quality has improved with the implementation of the NYSDEC SVE system, it has not consistently been below the New York State Department of Health (NYSDOH) 1,000 microgram per cubic meter (u.g/m3) volatile organic compounds (VOCs) guideline. This is due to limitations ofthe discharge air treatment system in which the vacuum has been throttled back to prevent rapid breakthrough of the carbon.

On June 6,2006 REAC personnel, at the request of the EPA/Environmental Response Team (ERT), traveled to the ADC Site in Levittown, NY to install sub-slab sampling ports. Upon arrival the Work Assignment Manager (WAM) decided to sample from existing ports on the sub-slab ventilation system. Indoor and ambient air samples were also collected

OBSERVATIONS AND ACTIVITIES

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ADC2.8441

Mobilizations

On July 21, 2006 REAC personnel, at the request of the EPA/Environmental Response Team (ERT), traveled to the ADC Site in Levittown, NY to sample from existing ports on the sub-slab ventilation and the SVE systems. Indoor and ambient air samples were also collected.

Air Sampling Procedures

REAC personnel collected a 24-hour indoor air sample from each ofthe five tenant areas listed above at the ADC Site as well as, one from the Beverage Discount Center located immediately to the west ofthe Site. An additional collocated 24-hour indoor air sample was also collected from Christine's Alterations Shop. Six sub-slab grab samples were collected from the existing sub-slab ventilation system onsite. Seven grab samples were collected from the existing SVE system. Two ambient 24-hour samples were taken near the Northwest and Northeast comers ofthe ADC site. All samples were collected using a 6-liter (L) SUMMA® canister in accordance with REAC SOP #1704, SUMMA* Canister Sampling. The samples collected in SUMMA® canisters were properly documented and shipped to an outside laboratory for analysis. The laboratory analysis was performed in accordance with EPA Method TO-15, Determination of Volatile Organic Compounds (VOCs) in Air Collected in Specially-Prepared Canisters and Analyzed by Gas Chromatography/Mass Spectrometry (GC/MS). The Target Compound List (TCL) included Chloromethane, Vinyl Chloride, 1,1-Dichloroethene, trans-1,2-Dichloroethene, cis-1,2-Dichloroethene, 1,1,1-Trichloroethane, Carbon Tetrachloride, Trichloroethene (TCE), Tetrachloroethene (PCE), Dichlorodifluoromethane, Chloroethane, 1,1 -Dichloroethane, Methy tert-Butyl Ether, Methy Ethyl Ketone, 1,2-Dichloroethane. Detection Limits (DLs) for VOCs were set at 0.1 parts per billion by volume (ppbv) for all contaminants. Results were reported in both ppbv and micrograms per cubic meter (/ig/m3). A total of seven indoor air, six sub-slab and two ambient air samples were collected and sent for VOC analysis.

RESULTS

Six of the seven samples taken from the SVE system had detectable levels of both TCE and PCE, sample# 44738 taken from S VE-5 was the only sample with no detectable levels of TCE and PCE. Sample #44737 taken from SVE-6 had the highest levels of both TCE (98.9 ppbv, 531 ug/m3) and PCE (4760 ppbv, 3200 ug/m3).

Both ambient samples had no detectable levels of TCE and PCE.

All of the indoor samples had detectble levels of PCE and were non-detect for TCE except for sample#44746(ID-Barb) which had detectable levels of TCE and was non-detect for PCE.

All ofthe sub-slab samples had detectable levels of PCE with the highest concentration 146 ppbv, 990 ug/m3) measured in sample #44755(SS-Ba-US colocated). Four of the seven sub-slab samples had detectable levels of TCE with the highest concentration(7.39 ppbv, 39.7 ug/m3) found in sample #44752(SS-Ba-US).

A summary of TCE and PCE results for all samples can be found in Table 1, SUMMA* Canister Results.

A map of the sample locations can be found in Figure EJJMMA* Cannister Locations. Appendix A contains the REAC analytical report

FUTURE ACTIVITIES

Future activities will be determined by ERT and Region II personnel based on the results obtained from the initial sub-slab sampling event.

cc: Central File(w/attachments) Electronic File: I:/Archive/REAC4/0114/ Dennis Miller, REAC Program Manager (cover page only)

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ADC2.8443

Table 1 SUMMA* Canister Results

American Drive-In Cleaners Superfund Site Levittown, NY

July 2006

Location / Sample Number Trichloroethene ppbv / ftg/m3

Tetrachloroethene ppbv / ug/m3

44733 / SVE-7 4.78/25.7 49.9 / 338

44734 / SVE-2 18.7/100 1320/8950

44735 / SVE-1 28.5/153 935 / 6340

44736 / SVE-4 2.12/11.4 186/ 1260

44737 / SVE-6 98.9/531 4760/32300

44738 / SVE-5 U / U U / U

44739 / SVE-3 84.7/455 2255 / 15300

44740 / Ambient East U / U U / U

44741 / Ambient West U / U U / U

44742 / ID-ADI U / U 0.81/5.49

44743 / ID-US U / U 1.18/8.00

44744 / ID-Chris U / U 0.589/3.99

44745 / ID-Chris-Co U / U 1.53 / 10.4

44746 / ID-Barb 0.454 / 2.44 U / U

44747 / ID-Blimp U / U 0.451/3.06

44748 / ID-Bev U / U 0.245/ 1.66

44749 / SS-FR-ADI 5.02 / 27.0 87.0/590

44750 / SS-Ba-ADI U / U 3.33/22.6

44751 / SS-Fr-US 1.11/5.96 38.5/261

44752 / SS-Ba-US 7.39 / 39.7 127/861

44753 / SS-Ba-Chris U / U 3.47 / 23.5

44754 / SS-Blimp U / U 5.11/34.6

44755/SS-Ba-US 7.17/38.5 146 / 990

44756 / Trip Blank U / U U / U

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a u'l o

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111 J-

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a.

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ADC2.8447

APPENDIX A SUMMA* Analytical Report

American Drive-In Cleaners Superfund Site Levittown, NY

July 2006

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ADC2.8449

Lockheed Martin Technology Services Environmental Services REAC 2890 Woodbridge Avenue Building 209 Anna Edison, NJ 08837-3679 Telephone 732-321-4200 Facsimile 732-494-4021 LOCKHEED MARTIN

DATE: 22 September 2006

TO: R. Singhvi EPA/ERTC

FROM: V. Kansal Analytical Section Leader

SUBJECT: DOCUMENT TRANSMITTAL UNDER WORK ASSIGNMENT #0-114

Attached please find the following document prepared under this work assignment:

American Drive In - Analytical Report

Central File WA # 0-114 (w/attachment) J. Catanzarita Work Assignment Manager (w/attachment) M. Gemelli Task Leader (w/attachment) J. Soroka Data Validation and Report Writing

Group Leader (w/o attachment)

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ANALYTICAL REPORT

Prepared by LOCKHEED MARTIN, Inc.

American Drive In Levittown, NY

September 2006

EPA Work Assignment No. 0-114 LOCKHEED MARTIN Work Order EAC00114

EPA Contract No. EP-C-04-032

ADC2.8451

V;, .Kansal 'najytical Section Leader

r o l l e r Program Manager 1

Submitted to J. Catanzarita

EPA-ERTC

(7CG

MM Date'

Analysis by: REAC

Prepared by: A. LoSurdo

Reviewed by: J. Soroka

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ADC2.8453

Table of Contents

Topic

Introduction Case Narrative Summary of Abbreviations

Section I

Results of the Analysis for VOC in Air (ppbv) Results of the Analysis for VOC in Air (ug/m3)

Section II

Results of the LCS Analysis for VOC in Air Results of the MS/MSD Analysis for VOC in Air Results of the Replicate Analysis for VOC in Air

Table 1.1a Table 1.1b

Table 2.1 Table 2.2 Table 2.3

Section III

Chains of Custody

Appendix A Data for VOC in Air

Appendices will be furnished on request.

Page R 355 001

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Introduction

REAC personnel in response to WA 0-114, provided analytical support for environmental samples collected from the American Drive In Site, located in Levittown, NY as described in the following table. The support also included QA/QC, data review, and preparation of an analytical report containing a summary of the analytical methods, the results, and the QA/QC results.

The samples were treated with procedures consistent with those specified in SOP #1008.

coc# 0-114-07/21/

Number of

Samples

Sampling . Date

Date Received

Matrix Analysis/ Method

Laboratory1 Data Package

06-0005 2 07/19/06 07/24/06 SUMMA/ Air

VOA/ TO-15

REAC R355

06-0006 2 07/19/06 07/24/06 SUMMA/ Air

VOA/ TO-15

REAC R355

06-0007 2 07/19/06 07/24/06 SUMMA/ Air

VOA/ TO-15

REAC R355

06-0015 1 1

07/19/06 07/20/06

07/24/06 07/24/06

SUMMA/ Air

VOA/ TO-15

REAC R355

06-0016 2 07/19/06 07/24/06 SUMMA/ Air

VOA/ TO-15

REAC R355

06-0008 2 07/19/06 07/24/06 SUMMA/ Air

VOA/ TO-15

REAC R355

06-0009 2 07/19/06 07/24/06 SUMMA/ Air

VOAV TO-15

REAC R355

06-0010 2 07/19/06 07/24/06 SUMMA/ Air

VOA/ TO-15

REAC R355

06-0011 2 07/19/06 07/24/06 SUMMA/ Air

VOA/ TO-15

REAC R355

06-0012 2 07/19/06 07/24/06 SUMMA/ Air

VOA/ TO-15

REAC R355

06-0013 2 07/19/06 07/24/06 SUMMA/ Air

VOA/ TO-15

REAC R355

06-0014 2 07/19/06 07/24/06 SUMMA/ Air

VOA/ TO-15

REAC R355

0114-DAR-092206 01

1 REAC Analytical Laboratory is NELAC certified.

Case Narrative

The data in this report have been validated to three significant figures. Any other representation of the data is the responsibility ofthe user. Values less than the reporting limits for organic analyses have not been reported

VOC In Air TO-1S Package R 355

Data have been validated for the following compounds: dichlorodifluoromethane, chloromethane, vinyl chloride, chloroethane, 1,1-dichloroethene, trans-1,2-dichloroethene, 1.1-dichloroethane, methyl tertiary butyl ether (MTBE), 1,2-dichloroethane, 1,1,1-trichloroethane, carbon tetrachloride, trichloroethene (TCE) and tetrachloroethene (PCE). Samples were analyzed by a modified EPA Method TO-15 using selective ion monitoring (SIM). As per the request of the work assignment manager RLs for the subslab and SVE samples were 1 00 ppbv. Results below the RLs are not reported.

The reanalysis of tetrachloroethene (PCE), for sample 44736. 44739, 44752 and 44755 and trichloroethene (TCE), for samples 44736 and 44739, exceeded the holding time . For these associated samples the respective concentration of PCE and TCE is estimated "J".

For sample 44741, the percent recovery of PCE was exceeded in the matrix spike duplicate.The PCE result for sample 44741 is estimated "J".

For sample 44749, the percent recovery of TCE was exceeded in the matrix spike duplicate.The concentration of TCE for sample 44749 is estimated "J".

Reanalysis of sample 44738 for the confirmation of chloromethane and PCE indicated a possible carry­over of PCE in the original analysis. Chloromethane concentration was confirmed at 1.1 ppbv. Therefore, for sample 44738, the concentration of PCE is not detected and the reporting limit for this compound is based on the original sample concentration of PCE.

For sample 44742, the concentration of chloromethane exceeded the linear calibration range. Chloromethane concentration is estimated ("E") for sample 44742.

0114-DAR-092206 02

ADC2.8457

Summary of Abbreviations

B 8FB C cont. D

Dioxin

CLP COC C CRDL CRQL DFTPP DL E EMPC ICAP IS J LCS LCSD MDL MS (BS) MSD (BSD MW NA NC NR NS %D % REC PAL PQL QA/QC QL RL RPD RSD SIM SURR TCLP U m 3

L mL ML

Analyte was found in the blank Bromofluorobenzehe Centigrade Continued (Surrogate Table) value is from a diluted sample and was not calculated (Result Table) result was obtained from a diluted sample denotes Polychlorinated Dibenzo-p-dioxins (PCDD) and Polychlorinated Dibenzofurans and/or PCDD and PCDF Contract Laboratory Procedure Chain of Custody Concentration Contract Required Detection Limit Contract Required Quantitation Limit Decafluorotriphenylphosphine Detection Limit Value is greater than the highest linear standard and is estimated Estimated maximum possible concentration Inductively Coupled Argon Plasma Internal Standard Value is estimated Laboratory Control Sample Laboratory Control Sample Duplicate Method Detection Limit Matrix Spike (Blank Spike) Matrix Spike Duplicate (Blank Spike Duplicate) Molecular Weight either Not Applicable or Not Available Not Calculated Not Requested Not Spiked Percent Difference Percent Recovery Permissible Acceptance Limit Practical Quantitation Limit Quality Assurance/Quality Control Quantitation Limit Reporting Limit Relative Percent Difference Relative Standard Deviation Selected Ion Monitoring Surrogate Toxic Characteristics Leaching Procedure Not detected cubic meter kg kilogram ug microgram liter g gram pg picogram milliliter mg milligram ng nanogram microliter Value exceeds the acceptable QC limit

Revision 6/21/05

0114-DAR-092206 03

ADC2.8458

r Table 1.1a Results crt the Analysis lor VOC in Air (ppbv)

WA# 0-114 America Drive In

Method SOP 1614 Sample Number Sample Location

Compound

DlchbroeSnuorornethane Chtwomemane Vinyl Chloride Chtoroethane

1.1-Oicnloroe»ierva (1.1-OCE) trani-1,2-0icNoro«n«ne 1,1-Olchioroeth»ne (1.1-0CA) MethyMer.eutyl Ether (MTBE) as-1.2-Oichloroeihene 1 J^ i chkxoe thene 1,1,1-Tricnloraethane (TCA) Car ton Tetrachloride Trichloroethene (TCE) Tetrachloroethene (PCE) Methyl Ethyl Ketone

Method Blank 060731-1

R e m * ppbv

RL cobv

44756 Trip Blank

Result ppbv

RL PPbv

44745 tO-Chris-Co

Resut pobv

RL _£pbv_

4474E lD-8art>

Resut ppbv

RL ppbv

Page 44747

ID-Blimp

Resut

PP°V

U U U U U U U U U

u u u u u u

0.050 0.050 0.OS0 0.050 0.050

o.oso 0.050 0.050 0.050 0.050 0 050 0.060 0.050 0.050 0.050

U U U U U U U U U U U

u u u u

0.050 0.050 0.050 0.050 0.050 0.050

aoso 0.050 0.050 0.050 0.050

aoso 0.050 0.050 0.050

0.563 u 0 u u u u u u u u

0.11 u

1.53 u

0.100 0.100 0.100 0.100 0.100 0.100 0.100 0.100 0.100 0100 0.100 O.100 0.100 0.100 0.100

0.617 u u u u u u u u u

O220 0 1 0 5 0 4 5 4

U . U

0.100 0.100 0.100 0.100 0.100 0.100 0.100 0.100 0.100 0.100 0.100 0.100 0.100

0.100 0.100

0.693 1.44

U U U U U U U u u

0.107 U

0.451 U

RL ppbv

0.100 0.100 0.100 0.100 0.100 0.100 0.100 0.100 0.100 0.100 0.100 O.10O 0.100 0.100 0.100

c

0114-DAR-092206 04

ADC2.8459

Taole * la Icon*) Results ot the Analysis for VOC in Ait (ppbv) / WAX 0-114 Amenca Orive In

Metnoa: SOP 1814 Pafl« 2 of 6 Sample Number 44748 44740 44742 44743 44744 Sample Location ID-Bev Ambient East IO-AOI ID-US ID-Chris

Result RL Result RL Result R l Result RL Result RL Compound PPbv ppbv ppbv PPbv PPbv oobv PPbv PPbv PObv PPbv

Dicrtlorodirluorometnane 0683 0.100 0.215 0.0667 0.320 0.150 0.603 0.300 0.337 0.100 Chloromethane U 0.100 0.310 0.0667 13.6 E 0.150 U 0.300 U 0.100 Vinyl Chloride U 0.100 U 0.0667 U 0.150 U 0.300 U 0.100 CMoroethane U 0.100 U 0.0667 U 0.150 U 0.300 U 0100 1.1-0khloroetnene (1.1-OCE) U 0.100 U 0 0867 U 0.150 U 0.300 U 0.100 tran»-1,2-DicWoroelhene U 0.100 U 0.0667 U 0.150 U 0.300 U a 100 1.1-Oichtoroethane (1.1-DCA) U 0 100 U 0.0667 U 0.150 U 0300 U o too Melhyl-ler-eutyl Ether (MTBE] U 0.100 U 0.0667 U 0.150 U 0.300 U 0.100 cis-1,2-Dichloroethene U 0.100 u 0.0667 U 0.1S0 U 0.300 U aioo 1.2-Okntoroathana U 0.100 u 0.0667 U 0 150 O 0 300 U O.IOO 1,t.1-Trichloroelhane (TCA) U 0.100 u 0.0667 U 0.150 U 0.300 U O.IOO Carbon Tenachlorioe U 0.100 u 0.0667 U 0.150 U 0300 U O1O0 TrichloroMhene (TCE) U o.ioo u 0.0667 U 0160 U 0.300 U 0.100 Telrachloroelhene (PCE) 0.245 0.100 u 0.0667 0.61 0.150 vie O.3O0 0 539 0.100 Melhyl Ethyl Ketone U 0100 u 0.0667 U 0.150 u 0.300 U 0100

0114-DAR-092206 05

ADC2.8460

r Meihocr. SOP 1814 Sample Number SemplG Location

Compound

D'ichjorodflimomethane Chioroniethane Vnyt Chloride Chloroethane 1.1-0ichloroelhene (i.l-OCE) trans-1,2-Oichloroelhene 1.1- Dichloroethane (1,1-OCA) Methyl-let-Butyl Ether (MTBE) cis-1.24iiehloroetnene 1.2- Dichloroethane 1.1,1-Tfichlotoelhane (TCA) Carbon Tetrachloride Trichloroethene (TCE) Tetrachloroethene (PCE) Methyl Ethyl Ketone

Table t I a toont.) Results of the Analysis lor VOC in Air (ppbv) WAS 0-114 AmeriCB Drive In

tnoo Blank 44741 44750 44733

160801. 1 Ambient West SS-Ba-ADI SVE-7

Result RL Resuk Rl Result RL Result RL

PObv PPbv PCPV EfiSS ppbv oobv Pf"

U 0.050 0.678 0.200 U 1.00 U 1.00

U O.OSO 0.617 a200 l l 1.00 1.21 1.00

U 0 050 U 0.200 U 1.00 U 1.00

U 0.050 U 0.200 U 1.00 U 1.00

U 0.050 U 0.200 U 1.00 U 1.00

U O.OSO U 0.200 U 1.00 U 1.00

U 0.050 U 0.200 U 1.00 U 1 00

U 0.050 U 0.200 U 1 00 U 1.00

U 0.050 U 0.200 U 1 00 U 1.00

U 0.050 U 0.200 L) 1.00 U 1.00

U 0.050 U 0200 U 1.00 U 1.00

U 0.050 U 0.200 U 1.00 U 1.00

U 0050 U 0.200 U 1.00 4.78 1.00

U 0050 U J 0.200 3.33 1.00 49.9 100

U 0.050 U 0.200 U 1.00 U 1.00

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G

0114-DAR-092206 06

ADC2.8461

Table 1,1a {ecru,) Resutts of trie Analysis for VOC in Air (ppbv] WAtf 0 -1H America Drive tn

Method: SOP 1814 Sample Number Sample Location

Compound

44755 SS-Ba-US

Result PPbv

RL ppbv

44753, SS-BaOvis

Result PObv

RL PObv

44754 SS-6limp

Result ppbv

RL PObv

44751 SS-FMJS

Result ppbv

RL PPbv

Page 44752

SS-Ba-US

Result PObv

4 0 ( 6

RL PObv

Oichtorodifluorometnane U 1.00 U 1.00 U 1.00 u 1.00 U 1.00 Chtoromethane U 1.00 U 1.00 U 1.00 u 1.00 U 1.00 Vinyl Chloride U 1.00 U 1.00 U 1.00 U 1.00 U 1.00 ChtooMfhane U 1.00 U 1.00 U 1.00 u 1.00 U 1.00 1.1-OioWoroethene (1,1-DCE) U 1.00 U 1.00 U 1.00 u 1.00 U 1.00 trai»-1.2-Dicnioroetheno U 1.00 U 1.00 U 1.00 u 1.00 U 1.00 l . ta j i iMoroetnane (1.1-OCA) U 1.00 U 1.00 U 1.00 u 1.00 U 1.00 MethyHer-Butyl Ether (MTBE) U 1.00 U 1.00 U 1.00 u 1.00 U 1.00 oa-l^-OichtoroeUiene U 1.00 U 1.00 U 1.00 u 1.00 1.02 1.00 1.2-Oichloroethane U 1.00 U 1.00 U 1.00 u 1.00 U 1.00 1.1.1-Trichkxoelhane (TCA) U 1.00 U 1.00 U 1.00 u 1.00 U 1.00 Carbon Tetrachloride U 1.00 U 1.00 U 1.00 u 1.00 U 1.00 Ttichkxoelhene (TCE) 717 1.00 U 1.00 U 1.00 1.11 1.00 7.39 1.00 Tetrachloroethene (PCE) 146 J 5.00 3.47 1.00 5.11 1.00 38.5 1.00 127 J 5 00 Methyl Ethyl Ketone U 1.00 U 1.00 U 1.00 U 1.00 U 1.00

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ADC2. 8462

r Tabts 1.1a(conl.) Results cl the Analysis for VOC in Air (ppbv) WA# 0-114 America Drive In

Method: SOP 1814 Sample Number Sample Location

Compound

DicMorodilluoiomethane Chtoromethane Vinyl Chloride Cnlofoelhane

1,14J«cntorcW«» (1.1-DCE) trans-1.2-OKrtoroMheoe 1.l-Oicraoroetnane (1.1-OCA) Methyl-t*r43utyt Ether (MTBE) cis-1 i-Dichloroethene 1 ^-Oichtoroethane 1,1.1-Ticworoemane (TCA) Carbon Tettactitoride Trichloroethene (TCE) Tetrachloroethene (PCE) Methyl Ethyl Ketone

44738 SVE-5

ResuB ppbv

RL oebv

44739 SVE-3

Result PPbv

Method Blank. 060815-2

RL QPbv

ResuH _ p p b y _

RL ppbv

44736 SVE-4

Result _ £ p b y _

RL

Page 44737 SVE 45

Result ppbv

RL CCfav

U 1.07

l l u u u u u u u u u u u u

1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 3.17 1.00

u u u u u u u u

27.6 u u u

64.7 22S5

U

1.O0 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 60.0 50.0 1.00

U U u u u u u u u u u u u u u

1.00 1 00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1 00 1.00 1.00

1.03 u u u u u

I . 17 u u u

I I . 3 1.64 2 1 2 1B6 U

1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 100 1.00

u u u u u u u u

4.20 u u u

96.9 4760

U

1.00 1.00 1.00 1.00 1.00 100 1.00 1.00 1.00 1.00 1.00 1.00 25.0 1000 1.00

0114-DAR-0922C6 08

ADC2.8463

Method: SOP 1814 Sample Number Sample Location

Compound

DicWoroifluoromethane Chloromethane Vinyl Chloride Chloroethane 1 J-Cichloroethene (1.1-OCE) trans-1.2-Dkrtoroelhene 1.1- Dtchkxoethene 11.1-OCA) Melhyl-ter-Butyl Ether (MTBE) crt-1,2-Oichloroethene 1.2- 0'ichloroethane 1,1.1-Trichloroethane (TCA) Carbon Tetrachloride Trichloroethene (TCE) Tetracnloroelhene (PCE) Methyl Ethyl Ketone

Table L i e (cent.) Results of the Analysis lor VOC in Air (ppbv) WA# 0-114 America Drive m

RL PPbv

44734 44735 44749 SVE-2 SVE-1 SS-FR-AD

Result RL Result RL Result ppbv • PP°" ppbv

U 1.00 U 1.00 U U 1 00 U 1 00 11.6 U 1.00 U 1 00 U U 1.00 U 1.00 U U 1.00 U 1.00 U U 1.00 U 1.00 U U 1 00 U 1.00 U U 100 U 1.00 U

8.30 1.00 4.06 1.00 U U 1.00 U 1.00 U u 1.00 U 1.00 U u 1.00 U 1.00 u

18.7 1.00 28.5 1.00 5.02 1320 5O.0 835 25.0 87.0

U 1.00 U 1.00 129

Page

1.00 1.00 1.00 l.OO 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 10.0 1.00

0114-DAR-092206 09

ADC2.8464

r Table 1.1b Results of Ihe Analysis lor VOC in Air (ug/m3)

WA# 0-114 America Drive In

Metttod: SOP 1614 Sample Number Sample Location

Compound

Page 1 o<6 Method Blank 44756 44745 44746 44747

060731-1 Trip Blank IO-Chtis-Co ID-Barb ID-Blimp

Result RL Result RL Result RL Result RL Result RL

uq/m3 uq/m3 uqAn3 uo/m3 uq/m3 uo/m3 ua/m3 UQ/m3 ucym3 ug/m3

U 0.247 U 0.247 2.78 0.494 3.05 0.494 - 3.43 0.494

U 0.103 U 0.103 U 0.206 U 0.206 2.97 0.206

U 0.128 U 0.128 U 0.256 U 0.256 U 0.256

U 0132 U 0.132 U 0.284 U 0.264 U 0.264

U 0.198 U 0.198 U 0.396 U 0.396 U 0.396

U 0.198 U 0.198 U 0.396 U 0.396 U 0.396

U 0.202 U 0.202 U 0.405 U 0.405 U 0.40S

U 0.180 U 0.180 U 0.360 U 0.360 U 0.360

U 0.198 U 0.198 U 0.396 U 0.396 U 0.396

U 0.202 U 0.202 U 0.405 U 0.405 U 0.405

U 0.273 U 0.273 U 0.545 1,20 0.545 U 0.545

U 0.314 U 0.314 0.692 0.629 0.66 0.629 0.673 0.629

U 0.269 U 0.269 U 0.537 2.44 0.537 U 0.537

U 0.339 U 0.339 10.4 0.678 U 0.678 3.06 0.678

U 0.147 u 0.147 U 0.29S u 0.295 U 0.295

Oichlorodtnuorometharie Chioromethane Vinyl Chloride Chloroethane 1,1-Oichloroetherie (1.1-OCE) trans-1,2-Oichloroethene 1.1- Olchloroethane (1,1-OCA) Methyl-ter-Butyl Ether (MTBE) cis-1,2-Dichloroetnene 1.2- Dichloroethane 1,1,1-Trichloroemane (TCA) Carbon Tetrachloride Trichloroethene (TCE) Tetrachlwoethene (PCE) Methyl Ethyl Ketone

0114-DAR-G92206 010

ADC2.8465

Table l .10 (cont.) Results of tne Analysis for VOC in Air (ug/m3) WA# 0-114 America Drive In

Method: SOP 1814 Page 2 of 6

Sample Number 44748 44740 44742 44743 44744

Sample Location ID-86V Ambient East 10-AOI ID-US ID-Chris

Result RL Result RL Result RL Result RL Result RL

Compound uq/m3 uoVm3 UQ/m3 uq/m3 uqfm3 uQ/m3 uq/m3 ug/m3 uqi'm3 uQ/m.3

Dichlorodrnuoromeihane 3.38 0.494 1.06 0.330 1.580 0.741 2.98 1.483 1.67 0.494

Chloromethane U 0.206 0.640 0.138 28.1 E 0.310 U 0.619 U 0.206

Vinyl Chloride U 0.256 U 0.170 U 0.383 U 0.767 U 0.256

Chloroethane u 0.264 U 0.176 U 0.396 U 0.791 U 0.264 1,1-Dichloroethene (1,1-DCE) u 0.396 U 0.264 U 0.595 U 1.189 U 0.396 trans-1,2-Dichloroether.e u 0.396 U 0.264 U 0.594 U 1.189 U 0.396 1,1-Dichloroethane (1,1-DCA) u 0.405 U 0.270 U 0.607 U 1.214 U 0.405 Methyl-ter-Butyl Ether (MTBE) u 0.360 U 0.240 U 0.541 U 1 081 U 0.360 cis-1,2-Dichloroethene u 0.396 U 0.264 U 0.594 U 1.189 U 0.396 1,2-Dichloroethane u 0.405 U 0.270 U 0.607 U 1.214 U 0.405 1,1.1 -Trichloroethane (TCA) u 0.545 U 0.364 U 0.818 U 1.636 U 0.S45 Carbon Tetrachloride u 0.629 U 0.419 U 0.943 U 1.887 U 0.629 Trichloroethene (TCE) u 0.537 U 0.358 U 0.806 U 1.611 U 0.537 Tetra chloroe thene (PCE) 1.86 0678 0 0.452 5.49 1.017 8.00 2.034 3.99 0.678 Methyl Ethyl Ketone u 0.295 U 0.197 U 0.442 U 0.884 U 0.295

0114-DAR-092206 on

ADC2.8466

C Method: SOP 1614 Sample Number Sample Location

Compound

Table 1.1 b (cont.) Results of the Analysis (or VOC in Ait (ug/m3) WA* 0-114 America Drive In

Method Blank 060801-1

DirAlorodifiuoromethane Chloromethane Vinyl Chloride Chloroethane 1,1-Dichloroetrierie (1,1-DCE) lrans-1.2-Dichl oroethene 1.1- Dichloroethane (1.1-DCA) Melhyl-ter-Butyl Ether (MTBE) cis-1,2-OichtoroethBne 1.2- 0ichloroethane 1.1.1-Trichloroethane (TCA) Carbon Tetrachloride Trichloroethene (TCE) Tetrachloroethene (PCE) Methyl Ethyl Ketone

Page 3 o(6

44741 Ambient West

44750 SS-Ba-ADI

esult d/m3

RL Result RL Result RL esult d/m3 uq/m3 ua/m3 uovm3 uq/m3 uq/m3

U 0.247 3.35 0.989 U 4.94

U 0.103 1.68 0.413 U 2.06

U 0.128 U 0.511 U 2.56

U 0.132 U 0.528 U 2.64

U 0.198 U 0.793 U 3.96

U 0.198 U 0.793 U 3.96

u 0.202 U 0.809 U 4.05

u 0.180 U 0.721 U 3.60

u 0.198 U 0.793 U 3.96

u 0.202 U 0.809 u 4.05

u 0.273 U 1.091 u 5.45

u 0.314 U 1.258 u 6.29

u 0.269 U 1.074 . u 5.37

u 0.339 U J 1.356 22.6 6.78

u 0.147 U 0.590 U 2.95

44733 SVE-7

Result RL ugfm3

U 2.5 U U U U U U U U U U

25.7 338 U

4.94 2.06 2.56 2.64 3.96 3.96 4.05 3.60 396 4.05 5.45 6.29 5.37 6.78 2.95

c

C114-DAR-092206 012

ADC2.8467

Table 1.16 (cont) Results ot the Analysis (or VOC in Air (ug/m3) WA» 0-114 America Drive In

Method: SOP 1814 Page 4 of 6 Sample Number 44755 44753 44754 44751 44752 Sample Location SS-Ba-US SS-Ba-Chris SS-Blimp SS-Fr-US SS-Ba-US

Result RL Result RL Result RL Result RL Result RL Compound un/m3 ua/m3 uo/m3 uq/m3 ug/m3 uQ/m3 uo/m3 uQ/m3 ug/m3 uq/m3

Dichlorodifluoromethane U 4.94 U 4.94 U 4.94 U 4.94 U 4.94 Chloromethane U 2.08 U 206 U 2.06 U 2.06 U 2.06 Vinyl Chloride U 2.56 U 256 U 256 U 2.56 U 2.56 Chloroethane 0 2.64 u 2.64 U 2.64 U 2.64 U 2.64 1,1-Dichloroethene (1,1-DCE) U 3.96 U 3.96 U 3.96 U 3.96 u 3.96 trans-1,2-Dichloroethene U 3.96 u 3.96 U 3.96 U 3.96 u 3.96 1,1-Dichloroethane (1,1-DCA) U 4.05 u 4.05 U 4.05 U 4.05 u 4.05 MethyMer-Butyl Ether (MTBE) U 3.60 u 3.60 U 3.60 U 3.60 u 3.60 cis-1.2-Dichloroethene U 3.96 u 3.96 U 3.96 U 3.96 4.04 3.96 1,2-Dichloroethane U 4.05 u 4.05 U 4.05 U 4.05 u 4.05 1,1,1-Trichloroethane (TCA) U 5.45 u 5.45 U 5.45 U 5.45 u 5.45 Carbon Tetrachloride U 6.29 u - 6.29 U 6.29 U 6.29 u 6.29 Trichloroethene (TCE) 38.5 5.37 u 5.37 U 5.37 5.96 5.37 39.7 5.37 Tetrachloroethene (PCE) 990 J 33.9 23.5 6.78 34.6 6.78 261 6.78 861 J 33.9 Methyl Ethyl Ketone U 2.95 U 2.95 U 2.95 U 2.95 U 2.95

0114-DAR-092206 013

ADC2.8468

C v.

Table L i b (conl) Results of the Analysis for VOC in Air (ug/m3) WA* 0-114 America Drive In

Method: SOP 1B14 Sample Number Sample Location

Compound

Dichtorodifluorornelhane Chloromethane Vinyl Chloride Chloroethane 1.1-Dichloroethene (1.1-OCE) trans-1,2-Dichloroethene 1.1- Dtahloroethane (1,1-DCA) Methyl-ter-Butyl Ether (MTBE) cis-1,2-Dichloroethene 1.2- Dichloroethane 1.1,1 -Trichloroethane (TCA) Carbon Tetrachloride Trichloroethene (TCE) Tetrachloroethene (PCE) Methyl Ethyl Ketone

44738 SVES

Result uQ/m3

U 2.21

U U U U U U U U U U U U U

RL uq/m.3

44739 SVE-3

Result uq/m3

RL uq/m3

Method Blank 06081 S-2

Result uo/m3

44736 SVE-4

Page 44737 SVE-6

4.94 2.06 2.56 2.64 3.96 3.96 4.05 3.60 3.96 4.05 5.45 6.29 5.37 21.5 2.95

U U U U U U U U

109 U U U'

455 15300

U

4.94 2.06 2.56 2.64 3.98 3.96 4.05 3.60 3.96 4.05 5.45 6.29 269 339 2.95

U U U U U U U U U U U U U U U

S Of 6

RL Result RL Result RL

iQ/m3 uoVms u<j/m3 uo/m3 uq/m3

4.94 5.09 4.94 U 4.94

2.06 U 2.06 U 2.06

2.56 U 2.56 U 2.56

2.64 U 2.64 U 2.64

3.96 U 3.96 U 3 96

3.96 U 3.96 U 3.96

4.05 4.73 4.05 U 4.05

3.60 U 3.60 U 3.60

3.96 U 3.96 16.60 3.96

4.05 U 4.05 U 4.05

5.45 61.6 S.45 U 5.45

6.29 10.3 6.29 U 6.29 5.37 11.4 J 5.37 531 134 8.78 1260 J 678 32300 6780

2.95 U 2.95 U 2.95

0114-DAR-092206 014

ADC2.8469

TaWe1.1b(conq Results of the Analysis for VOC in Air (u9/m3) {'• WA* 0-114 America Drive In

Ivlethod: SOP 1814 P a 9 e

Sample Number 44734 44735 44749 Sample Location SVE-2 SVE-1 SS-FR-ADI

Result RL Result RL Result RL

Compound ua/m3 ua/m3 uq/m3 uo/m3 PPbv ppbv

Dichlorodifluoromethane U 4.94 U 4.94 U 4.94

Chloromethane U 2.08 U 2.06 23.9 2.06

Vinyl Chloride U 2.56 U 2.56 U 2.58

Chloroethane U 2.64 U 2.64 U 2.64 1,1-Dichloroethene (1.1-DCE) U 3.96 U 3.98 U 3.96 frans-1.2-Dichloroethene U 3.96 U 3.96 U 3.96 1.1.Dichloroethane (1.1-DCA) U 4.05 U 4.05 U 4.05 Methyl-ter-Butyl Ether (MTBE) U 3.60 U 3.60 U 3.60 cis-1,2-Dichloroethene 21.00 3.96 16.1 3.96 u 3.96 1,2-Dichloroethane U 4.05 U 4.05 u 4.05 1,1,1-Trichloroethane (TCA) U 5.45 U 5.45 u 5.45 Carbon Tetrachloride U 6.29 ' U 6.29 u 6.29 Trichloroethene (TCE) 100 5.37 153 5.37 27.0 J 5.37 Tetrachloroethene (PCE) 8950 339 6340 169 590 67.8 Methyl Ethyl Ketone U 2.95 U 2.95 3.80 2.95

0114-DAR-092206 015

ADC2.8470

Cmpound

Table 2.1 Results of the LCS Analysis for VOC in Air WA* 0-114 American Drive In

LCS-AT-27 LCS-AT-28 Added Recovered Added Recovered Amount Amount Amount Amount QC Limits

pptv ppfv %Rec pptv pptv %Rec %

Dichlorodifluoromethane Chloromethane Vinyl Chloride Chloroethane 1,1-Dichloroethene (1.1-DCE) trans-1,2-Dichloroethene 1.1- Dichloroethane (1,1-DCA) Methyl-ter-Butyl Ether (MTBE) cis-1,2-Oichloroethene 1.2- Dichloroethane 1,1,1-Trichloroethane (TCA) Carbon Tetrachloride Trichloroethene (TCE) Tetrachloroethene (PCE)

105 112.62 107 105 115.62 110 70 - 130

103 115.53 112 103 118.85 115 70 - 130

103 114.88 112 103 118.53 115 70 - 130

105 115.97 110 105 119.22 114 70 - 130

105 114.25 109 105 117.68 112 70 - 130

105 89.79 86 105 123.28 117 70 - 130

105 129.67 123 105 134.63 128 70 - 130

105 117.51 112 105 120.9 115 70 - 130

105 118.96 113 105 122.87 117 70 - 130

105 117.81 112 105 121.03 115 70 - 130

105 124.26 118 105 127.29 121 70 - 130 104 122.53 118 104 124.38 120 70 - 130 104 118.25 114 104 122.18 117 70 - 130 104 120.1 115 104 123.02 118 70 - 130

0114-DAR-092206 016

ADC2.8471

Table 2.2 Results of the MS/MSD Analysis foi VOC in Air WA# 0-114 American Drive In

Sample: 44749 MS MS MSD MSD Sample: 44749 Added Sample Recovered Added Recovered Amount Amount Amount Amounl Amount QC Limits

Cmpound ppbv ppbv ppbv %Rec. ppbv ppbv %Rec. RPD %

Dichlorodifluoromelhane 10.5 U 13.43 128 10.5 10.85 103 21 75 135 Chloromethane 10.3 11.6 13.28 NC 10.3 10.42 NC NC 75 135 Vinyl Chloride 10.3 U 12.73 124 10.3 10.06 97.7 23 75 135 Chloroethane 10.5 U 12.64 120 10.5 10.07 95.9 23 75 135 1,1-Dichloroethene (1,1-DCE) 10.5 U 12.45 119 10.5 9.86 93.9 23 75 135 trans-1,2-Dichloroethene 10.5 U 12.6 120 10.5 9.94 94.7 24 75 135 1,1-Dichloroethane (1,1-DCA) 10.5 U 13.11 125 10.5 10.51 100 22 75 135 MethyMer-Butyl Ether (MTBE) 10.5 U 13.04 124 10.5 10.56 101 21 75 135 cis-1,2-Dichloroethene 10.5 U 13.25 126 10.5 10.75 102 21 75 135 1.2-Dichloroethane 10.5 U 13.06 124 10.5 10.46 100 22 75 135 1.1.1-Trichloroethane (TCA) 10.5 U 13.4 128 10.5 10.8 103 21 75 • 135 Carbon Tetrachloride 10.4 U 13.15 126 10.4 10.42 100 23 75 135 Trichloroethene (TCE) 10.4 5.02 14.94 95.4 10.4 12.26 69.6 30 75 135 Tetrachloroethene (PCE) 10.4 87 91.7 NC 10.4 87.2 NC NC 75 135

Table 2.2 (Cont.) Results of the MS/MSD Analysis for VOC in Air WA# 0-114 American Drive In

Sample: 44741 MS MS MSD MSD Added Sample Recovered Added Recovered Amount Amount Amount Amount Amounl QC Limits

Cmpound ppbv ppbv ppbv %Rec. ppbv ppbv %Rec. RPD %

Dichlorodifluoromethane 2.10 0.678 2.81 102 2.10 2.82 102 0 75 - 135 Chloromethane 2.06 0.817 2.99 105 2.06 3.01 107 1 75 - 135 Vinyl Chloride 2.06 0 2.26 110 2.06 2.26 110 0 75 - 135 Chloroethane 2.06 U 2.3 110 2.06 2.29 109 1 75 - 135 1.1-Dichloroethene (1,1-DCE) 2.10 U 2.26 108 2.10 2.24 107 1 75 - 135 Irans-1,2-Dichloroethene 2.10 U 2.45 117 2.10 2.44 116 0 75 - 135 1,1-Dichloroethane (1,1-DCA) 2.10 U 2.62 125 2.10 2.61 124 0 75 - 135 MelhyMer-Butyl Ether (MTBE) 2.10 U 2.36 112 2.10 2.36 113 0 75 - 1 3 5 cis-1.2-Dichloroethene 2.10 U 2.44 116 2.10 2.44 116 0 75 - 135 1.2-Dichloroethane 2.10 U 2.39 114 2.10 2.37 113 1 75 - 135 1.1,1-Trichloroethane (TCA) 2.10 U 2.53 120 2.10 2.54 121 1 75 - 135 Carbon Tetrachloride 2.08 U 2.54 122 2.08 2.56 123 1 75 - 135 Trichloroethene (TCE) 2.08 U 2.47 119 2.08 2.48 119 0 75 - 135 Tetrachloroethene (PCE) 2.08 U 2.47 119 2.08 3.15 151 * 24 75 - 135

14-DAR-G92206 017

ADC2.8472

Table 2.3 Results ol the Replicate Analysis for VOC in Air WA# 0-114 American Drive In

Sample

Compound

Dichlorodifluoromethane -Chloromethane Vinyl Chloride Chloroethane 1,1-Dichloroethene (1,1-DCE) trans-1.2-Oichlo/oethene 1.1- Dichloroethane (1,1-DCA) MethyMer-Butyl Ether (MTBE) cis-12-Dichloroethene 1.2- Dichloroethane 1.1.1-Trichloroethane (TCA) Carbon Telrachloride Trichloroethene (TCE) Tetrachloroethene (PCE)

44735 44735 DUP

44744 44744 DUP QC

Cone. Cone. Cone. Cone. Limit

ppbv ppbv RPD ppbv ppbv RPD RPD

U U NC 0.337 0.319 5 25

U U NC U U NC 25

U U NC U U NC 25

U U NC U U NC 25

U U NC U U NC 25

U U NC U U NC 25

U U NC U U NC 25

U U NC U U NC 25

4.06 2.38 52 U U NC 25

U U NC U U NC 25

U U NC U U NC 25

U U NC U U NC 25

28.5 32.2 12 U U NC 25

934 623 E 40 0.589 0.587 0 25

Table 2.3 (Cont.) Results of the Replicate Analysis for VOC in Air WA# 0-114 American Drive In

Sample

Compound

Dichlorodifluoromethane Chloromethane Vinyl Chloride Chloroethane 1,1 -Dichloroethene (1,1 -DCE) trans-1.2-Oichloroethene 1.1- Dichloroethane (1,1-DCA) MethyMer-Butyl Ether (MTBE) cis-1,2-Dichlor oethene 1.2- Dichloroethane 1,1,1 -Trichloroethane (TCA) Carbon Tetrachloride Trichloroethene (TCE) Tetrachloroethene (PCE)

44737 44737 DUP QC

Cone. Cone. Limit ppbv ppbv RPD RPD

U U NC 25

U U NC 25 U U NC 25

U U NC 25

U U NC 25 U U NC 25

U U NC 25

U U NC 25 4.20 • 4.20 0 25

U U NC 25 U U NC 25 U U NC 25

98.9 60.9 E 48 25 4760 4940 4 25

0114-DAR-092206 018

t \

¥ ERT

f> REAC, Edison, NJ

5 EPA Contract Number: EP-C-04-032

o

CHAIN OF CUSTODY RECORD

Site #: 0-114

Contact Name: John Johnson

Contact Phone: 732-321-4248

No: 0-114-07/21/06-0005

Lab: REAC

Lab#

.U2SQ.

H3S1

o T O

Sample #•

44734

44735

'— Location Analyses Matrix Collected Numb

Cont Container Preservativ

• Sample_Remark s

MS/MSD '—

C \ / C 4

TO-15 Low Level Air 7/19/2006 1 Summa Canister

high ppb

oVfc-1 TO-15 Low Level Air 7/19/2006 1 Summa Canister

high ppb

• • — • • — - • • • — • • — -- ... - _

— - i

. ... .

- . — —

• . ..

— .... ,. —

. ..

Special instructions. PCEPR= PCE PREVIOUS RESULTS, HIGH PPB-SUSPECT PCE CONC RANGE SAMPLES TRANSFERRED FROM

CHAIN OF CUSTODY #

Items/Reason Relinquished by Date Received by Date Time

JIL45.

Items/Reason Relinquished By Date Received by Date Tim

> o n t o bo J>

r: ERT

*» REAC. Edison, NJ

§ EPA Contract Number: EP-C-04-032 I

o co

g L a b * s a m p l e * Location

CHAIN OF CUSTODY RECORD

Site*: 0-114 Contact Name: John Johnson Contact Phone: 732-321-4248

N o : 0 -114-07 /21 /06-0006

Lab: REAC

o to bo J> —i 4 ^

U3S3

D O

Sample #

"44736

44737

SVE-4

SVE-6

Analyses

TO-15 Low Level

TO-15 Low Level

Matrix

Air

Air

Collected

7/19/2006

7/19/2006

Numb Cent

Container

Summa Canister

Summa Canister

Preservativ e

Sample_Remark | MS/MSD s

high ppb

high ppb

Special Instructions: PCEPR= PCE PREVIOUS RESULTS, HIGH PPB*SUSPECT PCE CONC RANGE SAMPLES TRANSFERRED FROM .

CHAIN OF CUSTODY *

Items/Reason Relinquished by Oate Received by Dale Time Items/Reason Relinquished By Date Received by Date Tim

T f

j

2 ERT

• f REAC. Edison, NJ

> EPA Contract Number: EP-C-04-032

o CO

u

n CHAIN OF CUSTODY RECORD

Site #: 0-114

Contact Name: John Johnson

Contact Phone: 732-321-4248 S>Lab#

IJ35H 11355

©

Sample U

44738""

44739

Location

~SvE>5 ~

SVE-3

Analyse

TO-15 Low Level

TO-15 Low Level

Matrix

Air

Air

Collected

7/19/2006

7/19/2006

No: 0-114-07/21/06-0007

Lab: REAC

Numb Cont

Container

Summa Canister

Summa Canister

Preservativ e

Sample_Remark s

high ppb

high ppb

MS/MSD

Special instructions: PCEPR= PCE PREVIOUS RESULTS, HIGH PPB=SUSPECT PCE CONC RANGE

Relinquished by

SAMPLES TRANSFERRED FROM

CHAIN OF CUSTODY #

Hems/Reason

Att-

Date Received by Date Time Items/Reason Relinquished By Date Received by Dale Tim

o to bo J>

2 ERT

7s REAC, Edison, NJ

> EPA Contract Number: EP-C-04-032 <° o CO N r\' C i

CHAIN OF CUSTODY RECORD

- Site*: 0-114 Contact Name: John Johnson Contact Phone: 732-321-4248

Lab*

11341

B... o

Sample #

44733

44755

Location

SVE-7

SS-Ba-US

Analyses

TO-15 Low Level

TO-15 Low Level

Matrix

Air

Air

Collected

7/19/2006

7/20/2006

No: 0-114-07/21/06-0015

Lab: REAC

Numb Cont

Container

Summa Canister Summa Canister

Preservativ e

Sample_Remark s

high ppb

PCEPW-Tfbw" ppb

MS/MSD

o t o bo J >

Special Instructions: PCEPR- PCE PREVIOUS RESULTS. HIGH PPB=SUSPECT PCE CONC RANGE SAMPLES TRANSFERRED FROM

CHAIN OF CUSTODY #

Items/Reason Relinquished by

2 ERT

7̂ REAC. Edison, NJ

> EPA Contract Number EP-C-04-032 73

i o t o ro r\ '

CHAIN OF CUSTODY RECORD

Site #: 0-114

Contact Name: John Johnson

Contact Phone: 732-321-»24B

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No: 0-114-07/21/06-0016

Lab: REAC

g Lab# a

)I3S7

o

Sample U

44740

44756

Location Analyses Matrix Collected Numb Cont

Container Preservativ e

Sampie_Remark s

MS/MSD

Ambient East " TO-15 Low Level Air 7/20/2006 1 Summa Canister

PCEPR- 0.036 ppb

inp TO-1S Low Level Air 7/20/2006 1 Summa Canister

. _

. ..

-— _

.. ... ...

....

. .. .

Special Instructions: PCEPR* PCE PREVIOUS RESULTS. HIGH PPB=SUSPECT PCE CONC RANGE SAMPLES TRANSFERRED FROM

CHAIN OF CUSTODY #

Hems/Reason Relinquished by Date Received by Date Time Items/Reason Relinquished By Date Received by . Dale Tim

O'/'.iO

Dale Tim

O'/'.iO

,

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> EPA Contract Number: EP-C-04-032 73 • o CD t o

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CHAIN OF CUSTODY RECORD

Site*: 0-114

Contact Name: John Johnson

Contact Phone: 732-321-4248

No: 0-114-07/21/06-0008

Lab: REAC

o to

Sample «

44741

'44742

Ambient West

ID-ADI

Analyses

TO-15 Low Level

TO-15 Low Level

Matrix

Air

Air

Collected

7/20/2006

7/20/2006

Numb Cont

Container

Summa Canister Summa Canister

Preservativ e

Sample_Remark s

PCEPR- 0.060 ppb

PCEPR- 0.60 ppb

MS/MSD

Special Instructions: PCEPR* PCE PREVIOUS RESULTS, HIGH PPB=SUSPECT PCE CONC RANGE 6AMPLES TRANSFERRED FROM CHAIN OF CUSTODY*

Items/Reason Relinquished by

> o o t o bo J> -o 00

2 ERT

J> REAC, Edison, NJ

• 5 E p A Contract Number; EP-C-04-032 50 o 10

c 1 Lab# Sample U

44743

44744

Location

ID-US

ID-Chris

Analyses

TO-15 Low Level

TO-15 Low Level

CHAIN OF CUSTODY RECORD

Site #: 0-114

Contact Name: John Johnson Contact Phone: 732-321-4248

Matrix

Air

Air

Collected

7/2072006

7/20/2006

Numb Cont

Container

Summa Canister

Summa Canister

rS

N o : 0-114-07/21/06-0009

Lab: REAC

Preservativ e

Sample_Remark c

PCEPR- 0.54 ppb

PCEPR- 0.31 ppb

MS/MSD

Speaal InstrucUons. P C EPR= PCE PREVIOUS RESULTS, HIGH PPB-SUSPECT PCE CONC RANGE

SAMPLES TRANSFERRED FROM

CHAIN OF CUSTODY #

Items/Reason Relinquished by Dale Received by Date Time Items/Reason

All/An*ly<i\

Relinquished By Date Received by Date Tim

> o o to bo <i

2 E R T

S REAC. Edison. NJ

O EPA Contract Number: EP-C-04-032

o CD t o is: c a

CHAIN OF CUSTODY RECORD

Site #: 0-114

Contact Name: John Johnson

Contact Phone: 732-321-4246

No: 0-114-O7/21/06-0010

Lab: REAC

Lab U

1)3 &3

Sample U

44745

44746

Location

lLVChrts~-Co~

lO-Barb

Analyses

TO-15 Low LaveT

TO-15 Low Level

Matrix

Air

Air

Collected

7/20/2006

7/2072006

Numb Cont

Container

Summa Canister

Summa Canister

Preservativ e

Sample_Remark s

PCEPR- 0.31 ppb

PCEPR- 0.63 ppb

MS/MSD

Special Instructions: PCEPR= PCE PREVIOUS RESULTS. HIGH PPB=SUSPECT PCE CONC RANGE SAMPLES TRANSFERRED FROM

CHAIN OF CUSTODY #

Items/Reason Relinquished by Date Received by Date Time Items/Reason Relinquished By Date Received by Date Tim

J

o t o bo oo o

2 ERT

4> REAC. Edison. NJ

^ EPA Contract Number: EP-C-04-032 JO i o CD ro o aampte* Location"

CHAIN OF CUSTODY RECORD

Site* 0-114

Contact Name: John Johnson

Contact Phone: 732-321-4248

No: 0-114-07/21/06-0011

Lab: REAC

Lab*

nits

© o

Sample *

44747

44748

ID-Blimp

7D-Bev~

Analytes

TO-15 Low Level

TO-15 Low Level

Matrix

Air

Air

Collected

7/20/2006

7/20/2006

Numb Cont

Container

Summa Canister

Summa Canister

Preservativ Sample_Remark s

PCEPR- 1.0 ppb

PCEPR- 1.1 ppb

MS/MSD

Special instructions: PCEPR* PCE PREVIOUS RESULTS. HIGH PPB-SUSPECT PCE CONC RANGE SAMPLES TRANSFERRED FROM

CHAIN OF CUSTOO~Y*

Items/Reason Relinquished by Date Received by Date Time Items/Reason Relinquished By Date Received by Date Tim

n ro bo 00

2 ERT

£ REAC. Edison. NJ

•O EPA Contract Number: EP-C-04-032 70 • a io to, g Lab* CD

11167

o o

Sample #

44749

44750

Location

SS-FR-ADI

SS-Ba-ADI

CHAIN OF CUSTODY RECORD

Site ft 0-114

Contact Name: John Johnson

Contact Rhone: 732-321-4248

Analyses

TO-15 Low Level

TO-15 Low Level

Matrix

Air

Air

Collected

7/20/2006

7/20/2006

Numb Cont

Container

Summa Canister Summa Canister

No: 0-114-07/21/06-0012

Lab: REAC

Preservativ e

Sample_Remark s

PCEPR- 340 ppb

PCEPR- 41 ppb

MS/MSO

>

o bo J> oo t o

Specal Instructions: PCEPR= PCE PREVIOUS RESULTS. HIGH PPB=SUSPECT PCE CONC RANGE SAMPLES TRANSFERRED FROM

CHAIN OF CUSTODY #

Items/Reason Relinquished by Date

7/zj//>b

Received by Date

Ml/06

Time Items/Reason Relinquished By Dale Received by Date Tim

2 ERT

REAC. Ed/son. NJ

> EPA Contract Number: EP-C-04-032

Lab#

o IO

Sample H~

44751

44752"

Location

SS-Fr-US~

SS-Ba-US

i- '

CHAIN OF CUSTODY RECORD

Site #: 0-114

Contact Name: John Johnson Contact Phone: 732-321-4248

No: 0-114-07/21/06-0013

Lab: REAC

Analytes

TO-15 Low Level

TO-15 Low Level

Matrix

Air

Air

Collected

7/20/2006

7/20/2006

Numb Cont

Container

Summa Canister Summa Canister

Preservativ a

Sample_RemanV s

PCEPR-120 ppb

PCEPR- 11000 ppb

MS/MSD

Special Instructions: P C E P R = PCE PREVIOUS RESULTS. HIGH PPB=SUSPECT PCE CONC RANGE

Items/Reason Relinquished by

o t o bo oo

2 ERT

REAC. Edison. NJ

^ EPA Contracl Number: EP-C-04-032 <° o ID to

L a b * O K

CHAIN OF CUSTODY RECORD

Site #: 0-114

Contact Name: John Johnson Contact Phone: 732-321-4248

No: 0-114-07/21/06-0014

Lab: REAC

1971

o w ©

Sample *

44753

44754

Location

SS-Ba-Chris

SS-Blimp

Analyses

TO-15 Low Level

TO-15 Low Level

Matrix

Air

Air

Collected

7/2072006

7/2072006

Numb Cont

Container

Summa Canister Summa Canister

Preservativ e

Sample.Remaric s

PCEPR- 22 ppb

PCEPR- 5.7 ppb

MS/MSD

Special Instructions: PCEPR= PCE PREVIOUS RESULTS. HIGH PPB=SUSPECT PCE CONC RANGE SAMPLES TRANSFERRED FROM

CHAIN OF CUSTODY*

Items/Reason Relinquished by Data Received by Date Time Items/Reason Relinquished By Date

7&m

Received by

r/Ji<ff& \&tu

> o o l-O bo J>. 00 J>