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COMMONWEALTH OF PENNSYLVANIA DEPARTMENT OF ENVIRONMENTAL PROTECTION BUREAU OF LABORATORIES LABORATORY ACCREDITATION PROGRAM Having duly met the requirement of The act of June 29, 2002 (P.L. 596, No. 90) dealing with Environmental Laboratories Accreditation (27 Pa. C.S. §§4104-4113) and the National Environmental Laboratory Accreditation Program Standard is hereby approved as an Accredited Laboratory to conduct analysis within the fields of accreditations more fully described in the attached Scope of Accreditation Certifies That 36-00037 Eurofins Lancaster Laboratories Environmental LLC 2425 New Holland Pike, Lancaster, PA 17601-5994 Expiration Date: 01/31/2018 Certificate Number: 016 Continued accreditation status depends on successful ongoing participation in the program Certificate not transferable Surrender upon revocation To be conspicuously displayed at the Laboratory Not valid unless accompanied by a valid Scope of Accreditation Shall not be used to imply endorsement by the Commonwealth of Pennsylvania Customers are urged to verify the laboratory's current accreditation status PA DEP is a NELAP recognized accreditation body Aaren S. Alger, Chief Laboratory Accreditation Program Bureau of Laboratories
Transcript

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~ pennsylvania ~ DEPARTMENT OF ENVIRONMENTAL

PROTECTION Laboratory Scope of Accreditation

~••<o~\

/-~~ ........ . ' ' ... ..t "'··,. ~--'

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes should be used only when associated with a valid certificate of accreditation.

DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TN102128 (717) 656-2300 PADWIS ID: 36037

Eurofins Lancaster Laboratories Environmental LLC 2425 New Holland Pike Lancaster, PA 17601-5994

Matrix: Drinking Water

Method Revision Analyte Accreditation Type Primary Effecµve Date EPA 110.2 Color NE LAP PA 4/4/2005 EPA 150.1 pH NE LAP PA 2/28/2002 EPA 1613 B Dioxin NE LAP PA 10/5/2010 EPA 1664 A Oil and grease NE LAP PA 5124/2011 EPA 1664 B Oil and grease NE LAP PA 1127/2014 EPA 180.1 Turbidity NE LAP PA 4/4/2005 EPA200.7 4.4 Barium NE LAP PA 1122/2001 EPA200.7 4.4 Beryllium NE LAP PA 6/2/2004 EPA200.7 4.4 Cadmium NE LAP PA 1122/2001 EPA200.7 4.4 Calcium NE LAP PA 11128/2001 EPA200.7 4.4 Chromium NE LAP PA 1/22/2001 EPA200.7 4.4 Cobalt NELAP PA 10/16/2008 EPA200.7 4.4 Copper NE LAP PA 1122/2001 EPA 200.7 4.4 Iron NE LAP PA 4/4/2005 EPA200.7 4.4 Lithium NE LAP PA 11113/2012 EPA200.7 4.4 Magnesium NE LAP PA 12/412007 EPA200.7 4.4 Manganese NE LAP PA 4/4/2005 EPA200.7 4.4 Nickel NE LAP PA 1/22/2001 EPA 200.7 4.4 Potassium NE LAP PA 5/24/2011 EPA200.7 4.4 Silver NE LAP PA 1126/2001 EPA200.7 4.4 Sodium NE LAP PA 1122/2001 EPA200.7 4.4 Strontium NE LAP PA 5/24/2011 EPA200.7 4.4 Sulfur NE LAP PA 11/9/2012 EPA200.7 4.4 Tin NE LAP PA 11/3/2008 EPA200.7 4.4 Vanadium NE LAP PA 10/16/2008 EPA200.7 4.4 Zinc NE LAP PA 4/4/2005 EPA200.8 5.4 Antimony NE LAP PA 2/10/2005 EPA200.8 5.4 Arsenic NE LAP PA 2/10/2005 EPA 200.8 5.4 Barium NE LAP PA 11/16/2011 EPA200.8 5.4 Beryllium NE LAP PA 2/10/2005 EPA200.8 5.4 Cadmium NE LAP PA 211012005 EPA200.8 5.4 Calcium NE LAP PA 1111612011 EPA 200.8 5.4 Chromium NE LAP PA 2/10/2005 EPA 200.8 5.4 Copper NE LAP PA 3/9/2007 EPA 200.8 5.4 Iron NE LAP PA 1112/2012 EPA200.8 5.4 Lead NE LAP PA 2/10/2005 EPA200.8 5.4 Magnesium NE LAP PA 11/2/2012 EPA200.8 5.4 Manganese NE LAP PA 11116/2011 EPA200.8 5.4 Nickel NE LAP PA 2/10/2005

~~ The Pennsylvania Department of Environmental Protection Laboratory Accreditation Program is a NELAP recognized

Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing. Page 1of57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania tAif DEPARTMENT OF ENVIRONMENTAL PROTECTION Laboratory Scope of Accreditation

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes should be used only when associated with a valid certificate of accreditation.

DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TNI02128 (717) 656-2300 PADWIS ID: 36037

Matrix: Drinking Water Method Revision Analyte Accreditation Type Primary Effective Date

EPA200.8 5.4 Potassium NELAP PA 11/16/2011 EPA200.8 5.4 Selenium NE LAP PA 2/10/2005 EPA200.8 5.4 Sodium NE LAP PA 11/16/2011 EPA200.8 5.4 . Strontium NE LAP PA 11/16/2011 EPA200.8 5.4 Thallium NE LAP PA 2/10/2005 EPA200.8 5.4 Zinc NE LAP PA 11/16/2011 EPA 245.1 3.0 Mercury NELAP PA 8/29/2001 EPA300.0 2.1 Bromide NELAP PA 11/9/2012 EPA300.0 2.1 Chloride NELAP PA 511-7/2005 EPA300.0 2.1 Fluoride NELAP PA 1/22/2004 EPA300.0 2.1 Nitrate asN NELAP PA 10/31/2002 EPA300.0 2.1 NitriteasN NELAP PA 10/31/2002 EPA 300.0 2.1 Sulfate NELAP PA 717/2003 EPA335.4 Cyanide NELAP PA 7/11/2006 EPA353.2 Nitrate as N NELAP PA 2/28/2002 EPA353.2 Nitrite as N NELAP PA 2/28/2002 EPA353.2 Total nitrate-nitrite NE LAP PA 5/24/2011 EPA 504.1 1.1 l,2-Dibromo-3-chloropropane (DBCP, NE LAP PA 2/28/2002

Dibromochloropropane) EPA504.l 1.1 1,2-Dibromoethane (EDB, Ethylene NELAP PA 1/26/2001

dibromide) EPA524.2 4.1 1, 1, 1,2-Tetrachloroethane NELAP PA 10/31/2002 EPA 524.2 4.1 1,1,1-Trichloroethane NELAP PA 10/31/2002 EPA524.2 4.1 1, 1,2,2-Tetrachloroethane NE LAP PA 10/31/2002 EPA524.2 4.1 1,1,2-Trichloroethane NELAP PA 10/31/2002 EPA 524.2 4.1 l,l-Dichloro-2-propanone (1,1- NELAP PA 5/17/2005

Dichloropropanone) EPA 524.2 4.1 1,1-Dichloroethane NELAP PA 10/31/2002 EPA524.2 4.1 1,1-Dichloroethene (1,1-Dichloroethylene) NELAP PA 10/31/2002 EPA524.2 4.1 1,1-Dichloropropene NELAP PA 10/31/2002 EPA 524.2 4.1 1,2,3-Trichlorobenzene NELAP PA 4/4/2005 EPA524.2 4.1 1,2,3-Trichloropropane (1,2,3-TCP) NELAP PA 10/31/2002 EPA 524.2 4.1 1,2,4-Trichlorobenzene NE LAP PA 10/31/2002 EPA524.2 4.1 1,2,4-Trimethylbenzene NELAP PA 4/4/2005 EPA524.2 4.1 1,2-Dichlorobenzene ( o-Dichlorobenzene) NELAP PA 10/31/2002 EPA 524.2 4.1 1,2-Dichloroethane NELAP PA 10/31/2002 EPA524.2 4.1 1,2-D ichloropropane NE LAP PA 10/31/2002 EPA524.2 4.1 1,3,5-Trimethylbenzene NELAP PA 5117/2005 EPA524.2 4.1 1,3-Dichlorobenzene (m-Dichlorobenzene) NE LAP PA 10/31/2002 EPA524.2 4.1 1,3-Dichloropropane NE LAP PA 10/31/2002 EPA524.2 4.1 1,4-Dichlorobenzene (p-Dichlorobenzene) NE LAP PA 10/31/2002 EPA524.2 4.1 1-Chlorobutane NELAP PA 5/24/2007 EPA 524.2 4.1 2,2-Dichloropropane NE LAP PA 10/31/2002 EPA524.2 4.1 2-Butanone (Methyl ethyl ketone, MEK) NE LAP PA 5/24/2007 EPA524.2 4.1 2-Chlorotoluene NELAP PA 10/31/2002 EPA 524.2 4.1 2-Hexanone NE LAP PA 5/24/2007

~~ The Pennsylvania Department of Environmental Protection Laboratory Accreditation Program is a NELAP recognized

Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing. Page 2 of 57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania !~ DEPARTMENT OF ENVIRONMENTAL

PROTECTION Laboratory Scope of Accreditation

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes should be used only when associated with a valid certificate of accreditation.

DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TNI02128 (717) 656-2300 PADWIS ID: 36037

Matrix: Drinking Water

Method Revision Analyte Accreditation Type Primary Effective Date EPA524.2 4.1 2-Nitropropane NE LAP PA 5/24/2007 EPA 524.2 4.1 4-Chlorotoluene NE LAP PA 10/31/2002 EPA 524.2 4.1 4-Methyl-2-pentanone (MIBK) NE LAP PA 5/24/2007 EPA524.2 4.1 Acetone NELAP PA 5/24/2007 EPA524.2 4.1 Acrylonitrile NELAP PA 5/24/2007 EPA524.2 4.1 Ally! chloride (3-Chloropropene) NELAP PA 7/3/2007 EPA524.2 4.1 Benzene NELAP PA 10/3112002 EPA 524.2 4.1 Bromobenzene NE LAP PA 10/3112002 EPA 524.2 4.1 Bromochloromethane NE LAP PA 4/4/2005 EPA524.2 4.1 Bromodichloromethane NELAP PA 11/3/2016 EPA524.2 4.1 Bromoform NELAP PA 11/3/2016 EPA524.2 4.1 Carbon disulfide NE LAP PA 5/24/2007 EPA524.2 4.1 Carbon tetrachloride NE LAP PA 10/31/2002 EPA 524.2 4.1 Chloroacetonitrile NE LAP PA 5/24/2007 EPA524.2 4.1 Chlorobenzene NE LAP PA 10/31/2002 EPA524.2 4.1 Chloroethane NE LAP PA 10/3112002 EPA524.2 4.1 Chloroform NELAP PA 11/3/2016 EPA524.2 4.1 Dibromochloromethane NE LAP PA 11/3/2016 EPA 524.2 4.1 Dibromomethane NE LAP PA 10/3112002 EPA524.2 4.1 Dichlorodifluoromethane (Freon 12) NE LAP PA 4/4/2005 EPA 524.2 4.1 Diethyl ether (Ethyl ether) NELAP PA 5/24/2007 EPA 524.2 4.1 Diisopropyl ether (DIPE) NE LAP PA 117/2010 EPA 524.2 4.1 Ethyl methacrylate NE LAP PA 5/24/2007 EPA 524.2 4.1 Ethyl tert-butyl ether (ETBE) NE LAP PA 1124/2007 EPA 524.2 4.1 Ethylbenzene NE LAP PA 10/31/2002 EPA524.2 4.1 Hexachlorobutadiene (1,3- NE LAP PA 4/4/2005

Hexachlorobutadiene) EPA 524.2 4.1 Hexachloroethane NE LAP PA 5/24/2007 EPA 524.2 4.1 Isopropylbenzene (Cumene) NE LAP PA 4/4/2005 EPA 524.2 4.1 Methacrylonitrile NE LAP PA 5/24/2007 EPA524.2 4.1 Methyl bromide (Bromomethane) NE LAP PA 10/3112002 EPA524.2 4.1 Methyl chloride (Chloromethane) NE LAP PA 10/3112002 EPA524.2 4.1 Methyl iodide (Iodomethane) NE LAP PA 5/24/2007 EPA 524.2 4.1 Methyl tert-butyl ether (MTBE) NE LAP PA 4/4/2005 EPA524.2 4.1 Methylacrylate NE LAP PA 5/24/2007 EPA 524.2 4.1 Methylene chloride (Dichloromethane) NE LAP PA 10/3112002 EPA 524.2 4.1 Methylmethacrylate NE LAP PA 5/24/2007 EPA 524.2 4.1 Naphthalene NE LAP PA 5/17/2005 EPA524.2 4.1 Nitrobenzene NE LAP PA 5/17/2005 EPA524.2 4.1 Pentachloroethane NELAP PA 5/24/2007 EPA524.2 4.1 Propionitrile (Ethyl cyanide) NELAP PA 5/24/2007 EPA524.2 4.1 Styrene NELAP PA 10/31/2002 EPA 524.2 4.1 Tetrachloroethene (PCE, Perchloroethylene) NE LAP PA 10/3112002 EPA 524.2 4.1 Tetrahydrofuran (THF) NE LAP PA 5/24/2007 EPA524.2 4.1 Toluene NE LAP PA 10/31/2002 EPA524.2 4.1 Total trihalomethanes (TTHMs) NE LAP PA 10/3112002

~~ The Pennsylvania Department of Environmental Protection Laboratory Accreditation Program is a NELAP recognized

Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing. Page 3 of57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania ~ DEPARTMENT OF ENVIRONMENTAL

PROTECTION Laboratory Scope of Accreditation I

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes

should be used only when associated with a valid certificate of accreditation. DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TNI02128 (717) 656-2300 . PADWIS ID: 36037

Matrix: Drinking Water

Method Revision Analyte Accreditation Type Primary Effective Date EPA 524.2 4.1 Trichloroethene (TCE, Trichloroethylene) NE LAP PA 10/31/2002 EPA 524.2 4.1 Trichlorofluoromethane (Freon 11) NE LAP PA 4/4/2005 EPA524.2 4.1 Vinyl chloride (Chloroethene) NE LAP PA 10/31/2002 EPA524.2 4.1 Xylenes, total NE LAP PA 10/31/2002 EPA 524.2 4.1 cis-1,2-Dichloroethene NELAP PA 10/31/2002 EPA 524.2 4.1 cis-1,3-Dichloropropene NE LAP PA 10/31/2002 EPA524.2 4.1 m+p-Xylene NE LAP PA 12/8/2014 EPA 524.2 4.1 n-Butylbenzene NE LAP PA 4/4/2005 EPA 524.2 4.1 n-Propylbenzene NE LAP PA 5/17/2005 EPA 524.2 4.1 o-Xylene NE LAP PA 12/8/2014 EPA524.2 4.1 p-Isopropyltoluene ( 4-Isopropyltoluene) NELAP PA 5/17/2005 EPA524.2 4.1 sec-Butylbenzene NELAP PA· 4/4/2005 EPA524.2 4.1 tert-Amyl methyl ether (TAME) NE LAP PA 1/24/2007 EPA 524.2 4.1 tert-Butyl alcohol (2-Methyl-2-propanol) NE LAP PA 5/24/2007 EPA524.2 4.1 tert-Butylbenzene NE LAP PA 4/4/2005 EPA524.2 4.1 trans-1,2-Dichloroethene NE LAP PA 10/31/2002 EPA 524.2 4.1 trans-l ,3-Dichloropropene NELAP PA 10/31/2002 EPA524.2 4.1 trans-1,4-Dichloro-2-butene NE LAP PA 5/24/2007 EPA525.2 2.0 2,3-Dichlorobiphenyl (BZ 5) NE LAP PA 5/17/2005 EPA 525.2 2.0 Acenaphthene NE LAP PA 5/25/2007 EPA 525.2 2.0 Ac~naphthylene NE LAP PA 4/28/2010 EPA525.2 2.0 Alachlor (Lasso) NE LAP PA 2/28/2002 EPA 525.2 2.0 Aldrin (HHDN) NE LAP PA 10/9/2013 EPA525.2 2.0 Anthracene NELAP PA 5/25/2007 EPA525.2 2.0 Atrazine NE LAP PA 1/3/2002 EPA 525.2 2.0 Benzo[ a]anthracene NELAP PA 5/25/2007 EPA 525.2 2.0 Benzo[ a]pyrene NE LAP PA 1124/2001 EPA525.2 2.0 Benzo[b ]fluoranthene NE LAP PA 6/4/2007 EPA 525.2 2.0 Benzo[ghi]perylene NELAP PA 7/3/2007 EPA525.2 2.0 Benzo[k ]fluoranthene NE LAP PA 6/4/2007 EPA525.2 2.0 Benzyl butyl phthalate (Butyl benzyl NE LAP PA 5/25/2007

phthalate) EPA525.2 2.0 Butachlor NELAP PA 12/19/2002 EPA525.2 2.0 Chrysene (Benzo[a]phenanthrene) NELAP PA 5/25/2007 EPA525.2 2.0 Di-n-butyl phthalate NE LAP PA 5/25/2007 EPA525.2 2.0 Dibenzo[ a,h ]anthracene NE LAP PA 5/25/2007 EPA525.2 2.0 Dieldrin NE LAP PA 5/1712005 EPA 525.2 2.0 Diethyl phthalate NE LAP PA 5/25/2007 EPA525.2 2.0 Dimethyl phthalate NELAP PA 5/25/2007 EPA525.2 2.0 Endrin NE LAP PA 5/17/2005 EPA525.2 2.0 Fluoranthene NE LAP PA 317/2012 EPA 525.2 2.0 Fluorene NE LAP PA 217/2012 EPA 525.2 2.0 Heptachlor NE LAP PA 5/17/2005 EPA525.2 2.0 Heptachlor epoxide NE LAP PA 5/17/2005 EPA525.2 2.0 Hexachlorobenzene NE LAP PA 2/11/2005 EPA 525.2 2.0 Hexachlorocyclopentadiene NE LAP PA 1/24/2001

~~ The Pennsylvania Department of Environmental Protection Laboratory Accreditation Program is a NELAP recognized

Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing. Page 4 of 57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania ,.... DEPARTMENT OF ENVIRONMENTAL

PROTECTION Laboratory Scope of Accreditation

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes

should be used only when associated with a valid certificate of accreditation. DEP Laboratocy ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TNI02128 (717) 656-2300

PADWIS ID: 36037

Matrix: Drinking Water

Method Revision Analyte Accreditation Type Primary Effective Date EPA 525.2 2.0 Indeno( 1,2,3-cd)pyrene NE LAP PA 217/2012 EPA 525.2 2.0 Methoxychlor NE LAP PA 1/24/2001 EPA 525.2 2.0 Metolachlor NE LAP PA 12/19/2002 EPA525.2 2.0 Metribuzin NELAP PA 12/19/2002 EPA 525.2 2.0 Phenanthrene NE LAP PA 5/25/2007 EPA 525.2 2.0 Propachlor (Ramrod) NE LAP PA 1/24/2001 EPA 525.2 2.0 Pyrene NELAP PA 5/25/2007 EPA 525.2 2.0 Sirnazine NE LAP PA 1/3/2002 EPA 525.2 2.0 bis(2-Ethylhexyl) adipate (di(2-Ethylhexyl) NE LAP PA 1/24/2001

adipate) EPA 525.2 2.0 bis(2-Ethylhexyl) phthalate (DEHP) NE LAP PA 1/24/2001 EPA 525.2 2.0 garnrna-BHC (Lindane, gamma- NE LAP PA 1/24/2001

Hexachlorocyclohexane) EPA 531.1 3.1 3-Hydroxycarbofuran NE LAP PA 1117/2006 EPA 531.1 3.1 Aldicarb (Temik) NE LAP PA 4/14/2015 EPA 531.1 3.1 Aldicarb sulfone NE LAP PA 1124/2001 EPA 531.1 3.1 Aldicarb sulfoxide NE LAP PA 1124/2001 EPA 531.1 3.1 Carbary) (Sevin) NE LAP PA 10/9/2002 EPA 531.1 3.1 Carbofuran (Furaden) NE LAP PA 1124/2001 EPA 531.1 3.1 Methomyl (Lannate) NELAP PA 1124/2001 EPA 531.1 3.1 Oxamyl (Vydate) NE LAP PA 1/24/2001 EPA 537 Modified Perfluorobutanesulfonic acid (PFBS) NE LAP PA 5/24/2017 EPA 537 Modified Perfluorodecanoic acid (PFDA) NE LAP PA 5/24/2017 EPA 537 Modified Perfluorododecanoic acid (PFDoA) NELAP PA 5/24/2017 EPA 537 Modified Perfluoroheptanoic acid (PFHpA) NELAP PA 5/24/2017 EPA 537 Modified Perfluorohexanesulfonic acid (PFHxS) NE LAP PA 5/24/2017 EPA 537 Modified Perfluorohexanoic acid (PFHxA) NE LAP PA 5/24/2017 EPA 537 Modified Perfluorononanoic acid (PFNA) NE LAP PA 5/24/2017 EPA 537 Modified Perfluorooctanesulfonic acid (PFOS) NE LAP PA 5/24/2017 EPA 537 Modified Perfluorooctanoic acid (PFOA) NE LAP PA 5/24/2017 EPA 537 Modified Perfluorotetradecanoic acid (PFT A) NELAP PA 5/24/2017 EPA 537 Modified Perfluorotridecanoic acid (PFTrDA) NE LAP PA 5/24/2017 EPA 537 Modified Perfluoroundecanoic acid (PFUnA) NE LAP PA 5/24/2017 EPA 8015 Ethane NE LAP PA 5/24/2011 EPA 8015 Methane NE LAP PA 5/24/2011 EPA 8015 Propane NE LAP PA 1119/2012 RSK-175 Acetylene (Ethyne) NELAP PA 11/19/2015 RSK-175 Carbon dioxide NE LAP PA 11/19/2015 RSK-175 Ethane NE LAP PA 11/19/2015 RSK-175 Ethene NE LAP PA 11119/2015 RSK-175 Isobutane (2-Methylpropane) NE LAP PA 11/19/2015 RSK-175 Methane NELAP PA 11/19/2015 RSK-175 n-Butane NE LAP PA 11/19/2015 SM2120B Color NE LAP PA 512512005 SM2130B Turbidity NELAP PA 5117/2005 SM2320B Alkalinity as CaC03 NE LAP PA 1/24/2001

~~ The Pennsylvania Department of Environmental Protection Laboratocy Accreditation Program is a NELAP recognized

Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing. Page 5 of57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania t...if DEPARTMENT OF ENVIRONMENTAL PROTECTION Laboratory Scope of Accreditation

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes should be used only when associated with a valid certificate of accreditation.

DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TN102128 P ADWIS ID: 36037

Matrix: Drinking Water Method Revision

SM2340C SM2510B SM2540C SM2540D SM2550B SM4500-ClF SM4500-F-C SM4500-H+B SM4500-PE SM 4500-Si02 C 20-22 SM5310 C SM5540C SM 9215 B SM 9223 Colilert

Matrix: Non-Potable Water Method

AK-101 AK-102 ASTMD7511-09 EPA 1010 EPA 130.2 EPA 1311

EPA 1312

EPA 160.1 EPA 160.4 EPA 1613

EPA 1613

EPA 1613

EPA 1613

EPA 1613

EPA 1613

EPA 1613

EPA 1613

EPA 1613

Revision

B

B

B

B

B

B

B

B

B

Analyte Accreditation Type Primary Total hardness as CaC03 NE LAP PA Conductivity NE LAP PA Total dissolved solids (TDS) NE LAP PA Residue, nonfilterable (TSS) NE LAP PA Temperature, deg. C NE LAP PA Total residual chlorine NE LAP PA Fluoride NE LAP PA pH NE LAP PA Orthophosphate as P NE LAP PA Silica, dissolved NELAP PA Total organic carbon (TOC) NE LAP PA Surfactants as MBAS NELAP PA Heterotrophic bacteria (Enumeration) NELAP PA Total coliform & E.coli (PIA) NE LAP PA

Analyte Accreditation Type Primary Gasoline-range organics (ORO) NELAP PA Diesel-range organics (DRO) NE LAP PA Total cyanide NE LAP PA Ignitability NE LAP PA Hardness NELAP PA Toxicity characteristic leaching procedure NELAP PA (TCLP) Synthetic precipitation leaching procedure NE LAP PA (SPLP) Residue, filterable (TDS) NE LAP PA Residue, volatile NE LAP PA 1,2,3 ,4,6, 7 ,8,9-0ctachlorodibenzo-p-dioxin NE LAP PA (OCDD) 1,2,3,4,6,7 ,8,9-0ctachlorodibenzofuran NE LAP PA (OCDF) 1,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin NE LAP PA (1,2,3,4,6, 7 ,8-hpcdd) 1,2,3 ,4,6, 7 ,8-Heptachlorodibenzofuran NE LAP PA (1,2,3,4,6, 7 ,8-hpcdf) 1,2,3,4,7,8,9-Heptachlorodibenzofuran NE LAP PA (1,2,3,4,7,8,9-hpcdf) 1,2,3 ,4, 7 ,8-Hexachlorodibenzo-p-dioxin NE LAP PA (HxCDD) 1,2,3 ,4, 7 ,8-Hexachlorodibenzofuran NE LAP PA (HxCDF) 1,2,3,6, 7,8-Hexachlorodibenzo-p-dioxin NELAP PA (HxCDD) 1,2,3 ,6, 7 ,8-Hexachlorodibenzofuran NE LAP PA (HxCDF)

~~

(717) 656-2300

Effective Date 5/24/2011 5/17/2005

61212004 5/24/2011 4/4/2005

5/24/2011 10/15/2003 5/16/2007 6/12/2007 5/24/2007 4/18/2013 5/24/2007 2/5/2003

1/26/2001

Effective Date 12/12/2005 12/12/2005 2/15/2013

12/12/2005 1/19/2005

12/12/2005

12/12/2005

1/19/2005 1/19/2005 6/30/2010

6/30/2010

6/30/2010

6/30/2010

6/30/2010

6/30/2010

6/30/2010

6/30/2010

6/30/2010

The Pennsylvania Department of Environmental Protection Laboratory Accreditation Program is a NELAP recognized Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing.

Page 6 of57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania t1 DEPARTMENT OF ENVIRONMENTAL PROTECTION Laboratory Scope of Accreditation

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes

should be used only when associated with a valid certificate of accreditation.

DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TNI02128 (717) 656-2300

PADWIS ID: 36037

Matrix: Non-Potable Water

Method Revision Analyte Accreditation Type Primary Effective Date EPA 1613 B 1,2,3,7,8,9-Hexachlorodibenzo-p-dioxin NE LAP PA

(HxCDD) EPA 1613 B 1,2,3, 7 ,8,9-Hexachlorodibenzofuran NELAP PA

(HxCDF) EPA 1613 B 1,2,3, 7,8-Pentachlorodibenzo-p-dioxin NE LAP PA

(PeCDD) EPA 1613 B 1,2,3, 7 ,8-Pentachlorodibenzofuran (PeCDF) NE LAP PA EPA 1613 B 2,3,4,6,7,8-Hexachlorodibenzofuran NELAP PA

(HxCDF) EPA 1613 B 2,3,4, 7 ,8-Pentachlorodibenzofuran (PeCDF) NE LAP PA EPA 1613 B 2,3, 7 ,8-Tetrachlorodibenzo-p-dioxin NE LAP PA

(2,3, 7 ,8-TCDD)(Dioxin) EPA 1613 B 2,3, 7 ,8-Tetrachlorodibenzofuran (TCDF) NELAP PA EPA 1613 B Total heptachlorodibenzo-p-dioxin NELAP PA

(HpCDD)

EPA 1613 B Total heptachlorodibenzofuran (HpCDF) NELAP PA

EPA 1613 B Total hexachlorodibenzo-p-dioxin (HxCDD) NE LAP PA EPA 1613 B Total hexachlorodibenzofuran (HxCDF) NE LAP PA EPA 1613 B Total pentachlorodibenzo-p-dioxin (PeCDD) NE LAP PA EPA 1613 B Total pentachlorodibenzofuran (PeCDF) NELAP PA EPA 1613 B Total tetrachlorodibenzo-p-dioxin (TCDD) NELAP PA

EPA 1613 B Total tetrachlorodibenzofuran (TCDF) NE LAP PA EPA 1625 c N-Nitrosodimethylamine NE LAP PA EPA 1631 E Mercury NELAP PA EPA 1664 A Oil and grease NELAP PA EPA 1664 B Oil and grease NE LAP PA EPA 1666 A 4-Methyl-2-pentanone (MIBK) NE LAP PA EPA 1666 A Diisopropyl ether (DIPE) NELAP PA EPA 1666 A Ethyl acetate NELAP PA EPA 1666 A Isobutyraldehyde NE LAP PA EPA 1666 A Isopropyl acetate NE LAP PA

EPA 1666 A Isopropyl alcohol (2-Propanol) NE LAP PA EPA 1666 A Methyl formate NE LAP PA EPA 1666 A Tetrahydrofuran (THF) NE LAP PA EPA 1666 A Xylenes, total NE LAP PA EPA 1666 A n-Amyl acetate (n-Pentyl acetate) NELAP PA EPA 1666 A n-Amyl alcohol (1-Pentanol) NELAP PA EPA 1666 A n-Butyl acetate NELAP PA EPA 1666 A n-Heptane NE LAP PA EPA 1666 A n-Hexane NE LAP PA EPA 1666 A tert-Butyl alcohol (2-Methyl-2-propanol) NE LAP PA EPA 1668 2,2',3,3',4,4',5,5',6-Nonachlorobiphenyl (BZ NELAP PA

206) EPA 1668 2,2',3,3',4,4',5,5'-0ctachlorobiphenyl (BZ NELAP PA

194) EPA 1668 2,2',3,3',4,4',5,6'-0ctachlorobiphenyl (BZ NELAP PA

196)

~~ The Pennsylvania Department of Environmental Protection Laboratory Accreditation Program is a NELAP recognized

Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing.

6/30/2010

6/3012010

6/30/2010

6/30/2010 6/30/2010

6/30/2010 6/30/2010

6/30/2010 8/6/2010

8/6/2010 8/6/2010 8/612010 8/6/2010 8/612010 81614010 8/6/2010

11/2312010 10/16/2014

1/1912005 1/27/2014

12/12/2005 1/19/2005 1/19/2005 111912005 111912005 12/2/2009 1119/2005 111912005 1/19/2005 4/4/2005 4/4/2005 4/4/2005

1/19/2005 1119/2005 4/4/2005 2/1/2013

12117/2012

12117/2012

Page 7 of 57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania M DEPARTMENT OF ENVIRONMENTAL PROTECTION Laboratory Scope of Accreditation

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes should be used only when associated with a valid certificate of accreditation.

DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TNI02128 (717) 656-2300 PADWIS ID: 36037

Matrix: Non-Potable Water Method Revision Analyte Accreditation Type Primary Effective Date

EPA 1668 2,2',3,3',4,4',5,6,6'-Nonachlorobiphenyl (BZ NELAP PA 207)

EPA 1668 2,2',3,3',4,4',5,6-0ctachlorobiphenyl (BZ NELAP PA 195)

EPA 1668 2,2',3,3',4,4',5-Heptachlorobiphenyl (BZ NELAP PA 170)

EPA 1668 2,2',3,3',4,4',6,6'-0ctachlorobiphenyl (BZ NELAP PA 197)

EPA 1668 2,2',3,3',4,4',6-Heptachlorobiphenyl (BZ NELAP PA 171)

EPA 1668 2,2',3,3',4,4'-Hexachlorobiphenyl (BZ 128) NELAP PA EPA 1668 2,2',3,3',4,5',6'-Heptachlorobiphenyl (BZ NELAP PA

177) EPA 1668 2,2',3,3',4,5',6,6'-0ctachlorobiphenyl (BZ NELAP PA

201) EPA 1668 2,2',3,3',4,5',6-Heptachlorobiphenyl (BZ NELAP PA

175) ' EPA 1668 2,2',3,3',4,5'-Hexachlorobiphenyl (BZ 130) NELAP PA EPA 1668 2,2',3,3',4,5,5',6'-0ctachlorobiphenyl (BZ NELAP PA

199) EPA 1668 2,2',3,3',4,5,5',6,6'-Nonachlorobiphenyl (BZ NELAP. PA

208) EPA 1668 2,2',3,3',4,5,5',6-0ctachlorobiphenyl (BZ NELAP PA

198) EPA 1668 2,2',3,3',4,5,5'-Heptachlorobiphenyl (BZ NELAP PA

172) EPA 1668 2,2',3,3',4,5,6'-Heptachlorobiphenyl (BZ NELAP PA

174) EPA 1668 2,2',3,3',4,5,6,6'-0ctachlorobiphenyl (BZ NELAP PA

200) EPA 1668 2,2',3,3',4,5,6-Heptachlorobiphenyl (BZ NELAP PA

173) EPA 1668 2,2',3,3',4,5-Hexachlorobiphenyl (BZ 129) NE LAP PA EPA 1668 2,2',3,3',4,6'-Hexachlorobiphenyl (BZ 132) NELAP PA EPA 1668 2,2',3,3',4,6,6'-Heptachlorobiphenyl (BZ NELAP PA

176) EPA 1668 2,2',3,3',4,6-Hexachlorobiphenyl (BZ 131) NELAP PA EPA 1668 2,2',3,3',4-Pentachlorobiphenyl (BZ 82) NELAP PA EPA 1668 2,2',3,3',5,5',6,6'-0ctachlorobiphenyl (BZ NELAP PA

202) EPA 1668 2,2',3,3',5,5',6-Heptachlorobiphenyl (BZ NELAP PA

178) EPA 1668 2,2',3,3',5,5'-Hexachlorobiphenyl (BZ 133) NELAP PA EPA 1668 2,2',3,3',5,6'-Hexachlorobiphenyl (BZ 135) NELAP PA EPA 1668 2,2',3,3',5,6,6'-Heptachlorobiphenyl (BZ NELAP PA

179) EPA 1668 2,2',3,3',5,6-Hexachlorobiphenyl (BZ 134) NELAP PA EPA 1668 2,2',3,3',5-Pentachlorobiphenyl (BZ 83) NELAP PA EPA 1668 2,2',3,3',6,6'-Hexachlorobiphenyl (BZ 136) NELAP PA

~~ The Pennsylvania Department of Environmental Protection Laboratory Accreditation Program is a NELAP recognized

Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing.

12/17/2012

12/17/2012

12/17/2012

12/17/2012

12117/2012

12/17/2012 12/17/2012

12/17/2012

12/17/2012

12/17/2012 12117/2012

12/17/2012

12/17/2012

12117/2012

12/17/2012

12/17/2012

12/17/2012

12/17/2012 12/17/2012 12/17/2012

12117/2012 12/17/2012

2/112013

12/17/2012

12/17/2012 12/17/2012 12/17/2012

12/17/2012 12/17/2012 12/17/2012

Page 8 of57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania t1 DEPARTMENT OF ENVIRONMENTAL PROTECTION Laboratory Scope of Accreditation

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes should be used only when associated with a valid certificate of accreditation.

DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TN102128 (717) 656-2300 PADWIS ID: 36037

Matrix: Non-Potable Water

Method Revision Analyte Accreditation Type Primary Effective Date EPA 1668 2,2',3,3',6-Pentachlorobiphenyl (BZ 84) NE LAP PA 12/17/2012 EPA 1668 2,2',3,3'-Tetrachlorobiphenyl (BZ 40) NE LAP PA 12/17/2012

EPA 1668 2,2',3,4',5',6-Hexachlorobiphenyl (BZ 149) NELAP PA 12/17/2012 EPA 1668 2,2',3,4',5'-Pentachlorobiphenyl (BZ 97) NELAP PA 12/17/2012

EPA 1668 2,2',3,4',5,5',6-Heptachlorobiphenyl (BZ NELAP PA 12/17/2012 187)

EPA 1668 2,2',3,4',5,5'-Hexachlorobiphenyl (BZ 146) NE LAP PA 12/17/2012

EPA 1668 2,2',3,4',5,6'-Hexachlorobiphenyl (BZ 148) NE LAP PA 12117/2012 EPA 1668 2,2',3,4',5,6,6'-Heptachlorobiphenyl (BZ NELAP PA 2/1/2013

188) EPA 1668 2,2',3,4',5,6-Hexachlorobiphenyl (BZ 147) NE LAP PA 12/17/2012 EPA 1668 2,2',3,4',5-Pentachlorobiphenyl (BZ 90) NE LAP PA 12/17/2012 EPA 1668 2,2',3,4',6'-Pentachlorobiphenyl (BZ 98) NE LAP PA 12/17/2012 EPA 1668 2,2',3,4',6,6'-Hexachlorobiphenyl (BZ 150) NE LAP PA 12/17/2012

EPA 1668 2,2',3,4',6-Pentachlorobiphenyl (BZ 91) NE LAP PA 12/17/2012

EPA 1668 2,2',3,4'-Tetrachlorobiphenyl (BZ 42) NE LAP PA 12/17/2012

EPA 1668 2,2',3,4,4',5',6-Heptachlorobiphenyl (BZ NE LAP PA 12/17/2012 183)

EPA 1668 2,2',3,4,4',5'-Hexachlorobiphenyl (BZ 138) NELAP PA 12/17/2012 EPA 1668 2,2',3,4,4',5,5',6-0ctachlorobiphenyl (BZ NE LAP PA 12/17/2012

203) EPA 1668 2,2',3,4,4',5,5'-Heptachlorobiphenyl (BZ NELAP PA 12/17/2012

180) EPA 1668 2,2',3,4,4',5,6'-Heptachlorobiphenyl (BZ NE LAP PA 12/17/2012

182) EPA 1668 2,2',3,4,4',5,6,6'-0ctachlorobiphenyl (BZ NELAP PA 12/17/2012

204) EPA 1668 2,2',3,4,4',5,6-Heptachlorobiphenyl (BZ NE LAP PA 12117/2012

181) EPA 1668 2,2',3,4,4',5-Hexachlorobiphenyl (BZ 137) NE LAP PA 12/17/2012 EPA 1668 2,2',3,4,4',6'-Hexachlorobiphenyl (BZ 140) NELAP PA 12/17/2012 EPA 1668 2,2',3,4,4',6,6'-Heptachlorobiphenyl (BZ NELAP PA 12/17/2012

184) EPA 1668 2,2',3,4,4',6-Hexachlorobiphenyl (BZ 139) NELAP PA 12/17/2012 EPA 1668 2,2',3,4,4'-Pentachlorobiphenyl (BZ 85) NELAP PA 12/17/2012 EPA 1668 2,2',3,4,5',6-Hexachlorobiphenyl (BZ 144) NELAP PA 12/17/2012 EPA 1668 2,2',3,4,5'-Pentachlorobiphenyl (BZ 87) NE LAP PA 12/17/2012 EPA 1668 2,2',3,4,5,5',6-Heptachlorobiphenyl (BZ NE LAP PA 12/17/2012

185) EPA 1668 2,2',3,4,5,5'-Hexachlorobiphenyl (BZ 141) NELAP PA 12/17/2012 EPA 1668 2,2',3,4,5,6'-Hexachlorobiphenyl (BZ 143) NELAP PA 12/17/2012 EPA 1668 2,2',3,4,5,6,6'-Heptachlorobiphenyl (BZ NELAP PA 12/17/2012

186) EPA 1668 2,2',3,4,5,6-Hexachlorobiphenyl (BZ 142) NELAP PA 12/17/2012 EPA 1668 2,2',3,4,5-Pentachlorobiphenyl (BZ 86) NE LAP PA 12/17/2012 EPA 1668 2,2',3,4,6'-Pentachlorobiphenyl (BZ 89) NELAP PA 12/17/2012 EPA 1668 2,2',3,4,6,6'-Hexachlorobiphenyl (BZ 145) NELAP PA 12/17/2012 EPA 1668 2,2',3,4,6-Pentachlorobiphenyl (BZ 88) NELAP PA 12/17/2012

~~ The Pennsylvania Deparbnent of Environmental Protection Laboratory Accreditation Program is a NELAP recognized

Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing. Page 9 of57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania !1 DEPARTMENT OF ENVIRONMENTAL PROTECTION Laboratory Scope of Accreditation

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes should be used only when associated with a valid certificate of accreditation.

DEP Laboratory ID: 36-00037. EPA Lab Code: PA00009 TNI Code: TNI02128 (717) 656-2300 PADWIS ID: 36037

Matrix: Non-Potable Water Method Revision Analyte Accreditation Type Primary Effective Date

EPA 1668 2,2',3,4-Tetrachlorobiphenyl (BZ 41) NE LAP PA EPA 1668 2,2',3,5',6-Pentachlorobiphenyl (BZ 95) NE LAP PA EPA 1668 2,2',3,5'-Tetrachlorobiphenyl (BZ 44) NE LAP PA EPA 1668 2,2',3,5,5',6-Hexachlorobiphenyl (BZ 151) NELAP PA EPA 1668 2,2',3,5,5'-Pentachlorobiphenyl (BZ 92) NELAP PA EPA 1668 2,2',3,5,6'-Pentachlorobiphenyl (BZ 94) NE LAP PA EPA 1668 2,2',3,5,6,6'-Hexachlorobiphenyl (BZ 152) NE LAP PA EPA 1668 2,2',3,5,6-Pentachlorobiphenyl (BZ 93) NELAP PA EPA 1668 2,2',3,5-Tetrachlorobiphenyl (BZ 43) NE LAP PA EPA 1668 2,2',3,6'-Tetrachlorobiphenyl (BZ 46) NE LAP PA EPA 1668 2,2',3,6,6'-Pentachlorobiphenyl (BZ 96) NE LAP PA EPA 1668 2,2',3,6-Tetrachlorobiphenyl (BZ 45) NELAP PA EPA 1668 2,2',3-Trichlorobiphenyl (BZ 16) NE LAP PA EPA 1668 2,2',4,4',5,5'-Hexachlorobiphenyl (BZ 153) NELAP PA EPA 1668 2,2',4,4',5,6'-Hexachlorobiphenyl (BZ 154) NE LAP PA EPA 1668 2,2',4,4',5-Pentachlorobiphenyl (BZ 99) NELAP PA EPA 1668 2,2',4,4',6,6'-Hexachlorobiphenyl (BZ 155) NE LAP PA EPA 1668 2,2',4,4',6-Pentachlorobiphenyl (BZ 100) NELAP PA EPA 1668 2,2',4,4'-Tetrachlorobiphenyl (BZ 47) NELAP PA EPA 1668 2,2',4,5',6-Pentachlorobiphenyl (BZ 103) NELAP PA EPA 1668 2,2',4,5'-Tetrachlorobiphenyl (BZ 49) NE LAP PA EPA 1668 2,2',4,5,5'-Pentachlorobiphenyl (BZ 101) NE LAP PA EPA 1668 2,2',4,5,6'-Pentachlorobiphenyl (BZ 102) NE LAP PA EPA 1668 2,2',4,5-Tetrachlorobiphenyl (BZ 48) NELAP PA EPA 1668 2,2',4,6'-Tetrachlorobiphenyl (BZ 51) NE LAP PA EPA 1668 2,2',4,6,6'-Pentachlorobiphenyl (BZ 104) NE LAP PA EPA 1668 2,2',4,6-Tetrachlorobiphenyl (BZ 50) NE LAP PA EPA 1668 2,2',4-Trichlorobiphenyl (BZ 17) NELAP PA EPA 1668 2,2',5,5'-Tetrachlorobiphenyl (BZ 52) NE LAP PA EPA 1668 2,2',5,6'-Tetrachlorobiphenyl (BZ 53) NE LAP PA EPA 1668 2,2',5-Trichlorobiphenyl (BZ 18) NELAP PA EPA 1668 2,2',6,6'-Tetrachlorobiphenyl (BZ 54) NE LAP PA EPA 1668 2,2',6-Trichlorobiphenyl (BZ 19) NELAP PA EPA 1668 2,2'-Dichlorobiphenyl (BZ 4) NE LAP PA EPA 1668 2,3',4',5',6-Pentachlorobiphenyl (BZ 125) NELAP PA EPA 1668 2,3',4',5'-Tetrachlorobiphenyl (BZ 76) NE LAP PA EPA 1668 2,3',4',5,5'-Pentachlorobiphenyl (BZ 124) NELAP PA EPA 1668 2,3',4',5-Tetrachlorobiphenyl (BZ 70) NELAP PA EPA 1668 2,3',4',6-Tetrachlorobiphenyl (BZ 71) NELAP PA EPA 1668 2,3',4'-Trichlorobiphenyl (BZ 33) NELAP PA EPA 1668 2,3',4,4',5',6-Hexachlorobiphenyl (BZ 168) NELAP PA EPA 1668 2,3' ,4,4',5'-Pentachlorobiphenyl (BZ 123) NELAP PA EPA 1668 2,3',4,4',5,5'-Hexachlorobiphenyl (BZ 167) NE LAP PA EPA 1668 2,3',4,4',5-Pentachlorobiphenyl (BZ 118) NE LAP PA EPA 1668 2,3',4,4',6-Pentachlorobiphenyl (BZ 119) NE LAP PA

~~ The Pennsylvania Department of Environmental Protection Laboratory Accreditation Program is a NELAP recognized

Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing.

12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012

2/1/2013 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012

Page 10 of57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania ~ DEPARTMENT OF ENVIRONMENTAL

PROTECTION Laboratory Scope of Accreditation

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes

should be used only when associated with a valid certificate of accreditation.

DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TNI02128 (717) 656-2300

PADWIS ID: 36037

Matrix: Non-Potable Water

Method Revision Analyte Accreditation Type Primary Effective Date EPA 1668 2,3',4,4'-Tetrachlorobiphenyl (BZ 66) NE LAP PA

EPA 1668 2,3',4,5',6-Pentachlorobiphenyl (BZ 121) NE LAP PA

EPA 1668 2,3',4,5'-Tetrachlorobiphenyl (BZ 68) NE LAP PA

EPA 1668 2,3',4,5,5'-Pentachlorobiphenyl (BZ 120) NE LAP PA

EPA 1668 2,3',4,5-Tetrachlorobiphenyl (BZ 67) NELAP PA

EPA 1668 2,3',4,6-Tetrachlorobiphenyl (BZ 69) NELAP PA

EPA 1668 2,3',4-Trichlorobiphenyl (BZ 25) NE LAP PA

EPA 1668 2,3',5',6-Tetrachlorobiphenyl (BZ 73) NE LAP PA

EPA 1668 2,3',5'-Trichlorobiphenyl (BZ 34) NELAP PA

EPA 1668 2,3',5,5'-Tetrachlorobiphenyl (BZ 72) NE LAP PA

EPA 1668 2,3',5-Trichlorobiphenyl (BZ 26) NE LAP PA

EPA 1668 2,3',6-Trichlorobiphenyl (BZ 27) NE LAP PA

EPA 1668 2,3'-Dichlorobiphenyl (BZ 6) NE LAP PA

EPA 1668 2,3,3',4',5',6-Hexachlorobiphenyl (BZ 164) NELAP PA

EPA 1668 2,3,3',4',5'-Pentachlorobiphenyl (BZ 122) NE LAP PA

EPA 1668 2,3,3',4',5,5',6-Heptachlorobiphenyl (BZ NELAP PA 193)

EPA 1668 2,3,3',4',5,5'-Hexachlorobiphenyl (BZ 162) NE LAP PA

EPA 1668 2,3,3',4',5,6-Hexachlorobiphenyl (BZ 163) NELAP PA

EPA 1668 2,3,3',4',5-Pentachlorobiphenyl (BZ I 07) NELAP PA

EPA 1668 2,3,3',4',6-Pentachlorobiphenyl (BZ 110) NE LAP PA

EPA 1668 2,3,3',4'-Tetrachlorobiphenyl (BZ 56) NE LAP PA

EPA 1668 2,3,3',4,4',5',6-Heptachlorobiphenyl (BZ NELAP PA 191)

EPA 1668 2,3,3',4,4',5'-Hexachlorobiphenyl (BZ 157) NE LAP PA

EPA 1668 2,3,3',4,4',5,5',6-0ctachlorobiphenyl (BZ NE LAP PA 205)

EPA 1668 2,3,3',4,4',5,5'-Heptachlorobiphenyl (BZ NE LAP PA 189)

EPA 1668 2,3,3',4,4',5,6-Heptachlorobiphenyl (BZ NE LAP PA 190)

EPA 1668 2,3,3',4,4',5-Hexachlorobiphenyl (BZ 156) NE LAP PA

EPA 1668 2,3,3',4,4',6-Hexachlorobiphenyl (BZ 158) NE LAP PA

EPA 1668 2,3,3',4,4'-Pentachlorobiphenyl (BZ 105) NE LAP PA

EPA 1668 2,3,3',4,5',6-Hexachlorobiphenyl (BZ 161) NE LAP PA

EPA 1668 2,3,3',4,5'-Pentachlorobiphenyl (BZ 108) NELAP PA

EPA 1668 2,3,3',4,5,5',6-Heptachlorobiphenyl (BZ NELAP PA 192)

EPA 1668 2,3,3',4,5,5'-Hexachlorobiphenyl (BZ 159) NE LAP PA

EPA 1668 2,3,3',4,5,6-Hexachlorobiphenyl (BZ 160) NELAP PA

EPA 1668 2,3,3',4,5-Pentachlorobiphenyl (BZ 106) NE LAP PA

EPA 1668 2,3,3',4,6-Pentachlorobiphenyl (BZ 109) NE LAP PA

EPA 1668 2,3,3',4-Tetrachlorobiphenyl (BZ 55) NE LAP PA

EPA 1668 2,3,3',5',6-Pentachlorobiphenyl (BZ 113) NELAP PA

EPA 1668 2,3,3',5'-Tetrachlorobiphenyl (BZ 58) NELAP PA

EPA 1668 2,3,3',5,5',6-Hexachlorobiphenyl (BZ 165) NE LAP PA

EPA 1668 2,3,3',5,5'-Pentachlorobiphenyl (BZ 111) NELAP PA

~~ The Pennsylvania Department of Environmental Protection Laboratory Accreditation Program is a NELAP recognized

Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing.

12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012

12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012

12/17/2012 2/1/2013

12117/2012

12/17/2012

12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012

12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012

Page 11 of 57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania It DEPARTMENT. OF ENVIRONMENTAL PROTECTION Laboratory Scope of Accreditation

._,.v•<<<>~

·51··,..~· ;' ~·r

·, ' '·· ,'

'~· ,, '.. . ",,,. ,.·

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes should be used only when associated with a valid certificate of accreditation.

DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TNI02128 (717) 656-2300 P ADWIS ID: 36037

Matrix: Non-Potable Water .Method Revision Analyte Accreditation Type Primary Effective Date

EPA 1668 2,3,3',5,6-Pentachlorobiphenyl (BZ 112) NE LAP PA 12/17/2012 EPA 1668 2,3,3',5-Tetrachlorobiphenyl (BZ 57) NELAP PA 12/17/2012 EPA 1668 2,3,3',6-Tetrachlorobiphenyl (BZ 59) NE LAP PA 12/17/2012 EPA 1668 2,3,3'-Trichlorobiphenyl (BZ 20) NE LAP PA 12/17/2012 EPA 1668 2,3,4',5,6-Pentachlorobiphenyl (BZ 117) NE LAP PA 12/17/2012 EPA 1668 2,3,4',5-Tetrachlorobiphenyl (BZ 63) NE LAP PA 12/17/2012 EPA 1668 2,3,4',6-Tetrachlorobiphenyl (BZ 64) NELAP PA 12/17/2012 EPA 1668 2,3,4'-Trichlorobiphenyl (BZ 22) NELAP PA 12/17/2012 EPA 1668 2,3,4,4',5,6-Hexachlorobiphenyl (BZ 166) NELAP PA 12/17/2012 EPA 1668 2,3,4,4',5-Pentachlorobiphenyl (BZ 114) NE LAP PA 12/17/2012 EPA 1668 2,3,4,4',6-Pentachlorobiphenyl (BZ 115) NELAP PA 12/1712012 EPA 1668 2,3,4,4'-Tetrachlorobiphenyl (BZ 60) NELAP PA 12/17/2012 EPA 1668 2,3,4,5,6-Pentachlorobiphenyl (BZ 116) NE LAP PA 12/17/2012 EPA 1668 2,3,4,5-Tetrachlorobiphenyl (BZ 61) NELAP PA 12/17/2012 EPA 1668 2,3,4,6-Tetrachlorobiphenyl (BZ 62) NE LAP PA 12/17/2012 EPA 1668 2,3,4-Trichlorobiphenyl (BZ 21) NE LAP PA 12/17/2012 EPA 1668 2,3,5,6-Tetrachlorobiphenyl (BZ 65) NE LAP PA 12/17/2012 EPA 1668 2,3,5-Trichlorobiphenyl (BZ 23) NELAP PA 12/17/2012 EPA 1668 2,3,6-Trichlorobiphenyl (BZ 24) NE LAP PA 12/17/2012 EPA 1668 2,3-Dichlorobiphenyl (BZ 5) NE LAP PA 12/17/2012 EPA 1668 2,4',5-Trichlorobiphenyl (BZ 31) NE LAP PA 12/17/2012 EPA 1668 2,4',6-Trichlorobiphenyl (BZ 32) NE LAP PA 12/17/2012 EPA 1668 2,4'-Dichlorobiphenyl (BZ 8) NELAP PA 12117/2012 EPA 1668 2,4,4',5-Tetrachlorobiphenyl (BZ 74) NE LAP PA 12/17/2012 EPA 1668 2,4,4',6-Tetrachlorobiphenyl (BZ 75) NE LAP PA 12/17/2012 EPA 1668 2,4,4'-Trichlorobiphenyl (BZ 28) NELAP PA 12/17/2012 EPA 1668 2,4,5-Trichlorobiphenyl (BZ 29) NE LAP PA 12/17/2012 EPA 1668 2,4,6-Trichlorobiphenyl (BZ 30) NE LAP PA 12/17/2012 EPA 1668 2,4-Dichlorobiphenyl (BZ 7) NE LAP PA 12/17/2012 EPA 1668 2,5-Dichlorobiphenyl (BZ 9) NELAP PA 12/17/2012 EPA 1668 2,6-Dichlorobiphenyl (BZ 10) NE LAP PA 12/17/2012 EPA 1668 2-Chlorobiphenyl (BZ 1) NE LAP PA 12/17/2012 EPA 1668 3,3',4,4',5,5'-Hexachlorobiphenyl (BZ 169) NELAP PA 12/17/2012 EPA 1668 3,3',4,4',5-Pentachlorobiphenyl (BZ 126) NE LAP PA 12/17/2012 EPA 1668 3,3',4,4'-Tetrachlorobiphenyl (BZ 77) NE LAP PA 12/17/2012 EPA 1668 3,3',4,5'-Tetrachlorobiphenyl (BZ 79) NELAP PA 12/17/2012 EPA 1668 3,3',4,5,5'-Pentachlorobiphenyl (BZ 127) NELAP PA 12/17/2012 EPA 1668 3,3',4,5-Tetrachlorobiphenyl (BZ 78) NELAP PA 12/17/2012 EPA 1668 3,3',4-Trichlorobiphenyl (BZ 35) NE LAP PA 12/17/2012 EPA 1668 3,3',5,5'-Tetrachlorobiphenyl (BZ 80) NELAP PA 12/17/2012 EPA 1668 3,3',5-Trichlorobiphenyl (BZ 36) NELAP PA 12/17/2012 EPA 1668 3,3'-Dichlorobiphenyl (BZ 11) NE LAP PA 12/17/2012 EPA 1668 3,4',5-Trichlorobiphenyl (BZ 39) NE LAP PA 12/17/2012 EPA 1668 3,4'-Dichlorobiphenyl (BZ 13) NE LAP PA 12/17/2012 EPA 1668 3,4,4',5-Tetrachlorobiphenyl (BZ 81) NE LAP PA 12/17/2012

~~ The Pennsylvania Department of Environmental Protection Laboratory Accreditation Program is a NELAP recognized

Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing. Page 12 of57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania t~ DEPARTMENT OF ENVIRONMENTAL

PROTECTION Laboratory Scope of Accreditation

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes should be used only when associated with a valid certificate of accreditation.

DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TN102128 (717) 656-2300

PADWIS ID: 36037

Ma1rix.: Non-Potable Water

Method Revision Analyte Accreditation Type Primary Effective Date EPA 1668 3,4,4'-Trichlorobiphenyl (BZ 37) NE LAP PA 12/17/2012

EPA 1668 3,4,5-Trichlorobiphenyl (BZ 38) NELAP PA 12/17/2012

EPA 1668 3,4-Dichlorobiphenyl (BZ 12) NE LAP PA 1211712012

EPA 1668 3,5-Dichlorobiphenyl (BZ 14) NE LAP PA 12117/2012

EPA 1668 3-Chlorobiphenyl (BZ 2) NELAP PA 12/17/2012

EPA 1668 4,4'-Dichlorobiphenyl (BZ 15) NELAP PA 12/1712012

EPA 1668 4-Chlorobiphenyl (BZ 3) NE LAP PA 12117/2012

EPA 1668 Decachlorobiphenyl NE LAP PA 2/1/2013

EPA 1668 c PCBs as congeners by HRGC/HRMS NE LAP PA 3/4/2015

EPA 1668 A PCBs as congeners by HRGC/HRMS NELAP PA 3/4/2015

EPA 1671 A Acetonitrile NELAP PA 1/1912005

EPA 1671 A Diethylamine NE LAP PA 1/19/2005

EPA 1671 A Dimethyl sulfoxide · NE LAP PA 1/19/2005

EPA 1671 A Ethanol NELAP PA 1/19/2005

EPA 1671 A Methanol NE LAP PA 1/19/2005

EPA 1671 A Methyl cellosolve (2-Methoxyethanol) NE LAP PA 1119/2005

EPA 1671 A Triethylamine NELAP PA 1/19/2005

EPA 1671 A n-Propanol (1-Propanol) NELAP PA 1119/2005

EPA 170.1 Temperature, deg. C NELAP PA 4/4/2005

EPA 180.1 Turbidity NE LAP PA 1119/2005

EPA200.2 Metals sample preparation NE LAP PA 1124/2007

EPA 200.7 4.4 Aluminum NE LAP PA 1119/2005

EPA200.7 4.4 Antimony NE LAP PA 1119/2005

EPA 200.7 4.4 Arsenic NE LAP PA 1119/2005

EPA 200.7 4.4 Barium NE LAP PA 1/19/2005

EPA200.7 4.4 Beryllium NELAP PA 1/1912005

EPA 200.7 4.4 Boron NELAP PA 1119/2005

EPA 200.7 4.4 Cadmium NELAP PA 1/19/2005

EPA200.7 4.4 Calcium NELAP PA 1/19/2005

EPA200.7 4.4 Chromium NELAP PA 1/19/2005

EPA200.7 4.4 Cobalt NELAP PA 1/19/2005

EPA200.7 4.4 Copper NELAP PA 1/19/2005

EPA 200.7 4.4 Iron NELAP PA 1/19/2005

EPA 200.7 4.4 Lead NELAP PA 1/19/2005

EPA200.7 4.4 Lithium NELAP PA 217/2012

EPA 200.7 4.4 Magnesium NE LAP PA 1/19/2005

EPA 200.7 4.4 Manganese NE LAP PA 1/19/2005

EPA200.7 4.4 Molybdenum NELAP PA 1/19/2005

EPA 200.7 4.4 Nickel NELAP PA 1/19/2005

EPA 200.7 4.4 Potassium NE LAP PA 1/19/2005

EPA 200.7 4.4 Selenium NE LAP PA 1119/2005

EPA 200.7 4.4 Silver NE LAP PA 41412005 EPA200.7 4.4 Sodium NE LAP PA 1/19/2005

EPA200.7 4.4 Strontium NE LAP PA 5/24/2011

EPA200.7 4.4 Tellurium NELAP PA 2/4/2016

~~ The Pennsylvania Department of Environmental Protection Laboratory Accreditation Program is a NELAP recognized

Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing. Page 13 of57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania M DEPARTMENT OF ENVIRONMENTAL PROTECTION Laboratory Scope of Accreditation

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes should be used only when associated with a valid certificate of accreditation.

DEP Labomtocy ID: 36-00037 EPA Lab Code: PA00009 1NI Code: 1NI02128 (717) 656-2300 PADWIS ID: 36037

Matrix: Non-Potable Water Method Revision Analyte Accreditation Type Primacy Effective Date

EPA 200.7 4.4 Thallium NELAP PA 1119/2005 EPA200.7 4.4 Thorium NELAP PA 11119/2015 EPA200.7 4.4 Tin NE LAP PA 1119/2005 EPA200.7 4.4 Titanium NELAP PA 1/19/2005 EPA200.7 4.4 Tungsten NELAP PA 11119/2015 EPA200.7 4.4 Vanadium NE LAP PA 1119/2005 EPA 200.7 4.4 Zinc NELAP PA 1/19/2005 EPA200.7 4.4 Zirconium NE LAP PA 7/29/2015 EPA 200.8 5.4 Aluminum NE LAP PA 11712010 EPA 200.8 5.4 Antimony NELAP PA 41412005 EPA200.8 5.4 Arsenic NE LAP PA 41412005 EPA200.8 5.4 Barium NE LAP PA 41412005 EPA200.8 5.4 Beryllium NELAP PA 41412005 EPA200.8 5.4 Boron NE LAP PA 111112012 EPA200.8 5.4 Cadmium NE LAP PA 41412005 EPA200.8 5.4 Calcium NELAP PA 11712010 EPA200.8 5.4 Chromium NELAP PA 41412005 EPA 200.8 5.4 Cobalt NE LAP PA 11/23/2010 EPA200.8 5.4 Copper NELAP PA 41412005 EPA200.8 5.4 Iron NE LAP PA 11123/2010 EPA200.8 5.4 Lead NELAP PA 41412005 EPA200.8 5.4 Magnesium NELAP PA 11712010 EPA200.8 5.4 Manganese NE LAP PA 11/23/2010 EPA200.8 5.4 Molybdenum NELAP PA 11712010 EPA 200.8 5.4 Nickel NELAP PA 41412005 EPA200.8 5.4 Potassium NE LAP PA 11712010 EPA200.8 5.4 Selenium NELAP PA 12/12/2005 EPA 200.8 5.4 Silver NE LAP PA 11212007 EPA200.8 5.4 Sodium NE LAP PA 11712010 EPA200.8 5.4 Strontium NELAP PA 11712010 EPA 200.8 5.4 Thallium NE LAP PA 5/3112006 EPA200.8 5.4 Tin NE LAP PA 11712010 EPA200.8 5.4 Titanium NELAP PA 11712010 EPA200.8 5.4 Uranium, total NE LAP PA 11119/2015 EPA 200.8 5.4 Vanadium NE LAP PA 11712010 EPA 200.8 5.4 Zinc NE LAP PA 1118/2011 EPA218.6 Chromium VI NE LAP PA 41412005 EPA 245.1 3.0 Mercury NE LAP PA 1/19/2005 EPA 300.0 2.1 Bromide NE LAP PA 41412005 EPA300.0 2.1 Chloride NE LAP PA 1/19/2005 EPA 300.0 2.1 Fluoride NE LAP PA 512512005 EPA 300.0 2.1 Nitrate as N NE LAP PA 1119/2005 EPA300.0 2.1 Nitrite as N NELAP PA 1/19/2005 EPA 300.0 2.1 Sulfate NE LAP PA 1119/2005 EPA3005 A Preconcentration under acid NE LAP PA 12/12/2005

~~ The Pennsylvania Deparbnent of Environmental Protection Labomtocy Accreditation Program is a NELAP recognized

Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing. Page 14 of57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania t1 DEPARTMENT OF ENVIRONMENTAL PROTECTION Laboratory Scope of Accreditation

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes

should be used only when associated with a valid certificate of accreditation.

DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TNI02128 (717) 656-2300

PADWIS ID: 36037

Matrix: Non-Potable Water

Method Revision Analyte Accreditation Type Primary Effective Date EPA 3010 A Hot plate acid digestion (HN03 + HCI) NELAP PA 12/12/2005

EPA 3020 A Hot plate acid digestion (HN03 only) NELAP PA 12/12/2005

EPA 305.2 Acidity as CaC03 NE LAP PA 1/24/2007

EPA 3060 A Alkaline digestion of Cr(VI) NE LAP PA 1124/2007

EPA 310.1 Alkalinity as CaC03 NE LAP PA 11/19/2015

EPA 335.4 Total cyanide NE LAP PA 1/19/2005

EPA 350.1 AmmoniaasN NELAP PA 10/9/2013

EPA 350.3 AmmoniaasN NE LAP PA 1/19/2016

EPA351.2 Kjeldahl nitrogen, total (TKN) NE LAP PA 1/19/2005

EPA3510 c Separatory funnel liquid-liquid extraction NE LAP PA 12/12/2005

EPA3511 Organic compounds in water by NE LAP PA 317/2012 microextraction

EPA 3520 c Continuous liquid-liquid extraction NE LAP PA 12/12/2005

EPA353.2 NitrateasN NE LAP PA 1/19/2005

EPA353.2 Nitrite as N NE LAP PA 1/19/2005

EPA353.2 Total nitrate-nitrite NE LAP PA 4/4/2005

EPA3620 B Florisil cleanup NE LAP PA 12/12/2005

EPA3630 c Silica gel cleanup NE LAP PA 12/12/2005

EPA 3640 A Gel permeation cleanup (GPC) NELAP PA 12/12/2005

EPA365.l Phosphorus, total NELAP PA 4/4/2005

EPA365.3 Orthophosphate as P NE LAP PA 1/19/2005

EPA 3660 .B Sulfur cleanup NE LAP PA 12/12/2005

EPA370.l Silica, dissolved NE LAP PA 11/19/2015

EPA 375.4 Sulfate NE LAP PA 4/4/2005

EPA410.4 Chemical oxygen demand (COD) NE LAP PA 4/1/2005

EPA 415.l Total organic carbon (TOC) NE LAP PA 1/19/2005

EPA 420.4 Total phenolics NE LAP PA 4/17/2007

EPA425.l Surfactants as MBAS NE LAP PA 1/19/2005

EPA 5030 c Aqueous-phase purge-and-trap NE LAP PA 1/27/2014

EPA5030 B Aqueous-phase purge-and-trap NE LAP PA 12/12/2005

EPA 524.2 4.1 1,2-Dichlorobenzene ( o-Dichlorobenzene) NE LAP PA 1/18/2011

EPA524.2 4.1 1,2-Dichloroethane NE LAP PA 1/18/2011

EPA524.2 4.1 4-Methyl-2-pentanone (MIBK) NE LAP PA 5/24/2011

EPA 524.2 4.1 Acetone NE LAP PA 1/18/2011

EPA524.2 4.1 Acrolein (Propenal) NE LAP PA 11/19/2015

EPA 524.2 4.1 Benzene NE LAP PA 1/18/2011

EPA524.2 4.1 Chlorobenzene NE LAP PA 1/18/2011

EPA524.2 4.1 Chloroform NE LAP PA 1/18/2011

EPA524.2 4.1 Dichlorodifluoromethane (Freon 12) NE LAP PA 11/19/2015

EPA524.2 4.1 Diisopropyl ether (DIPE) NELAP PA 11/19/2015

EPA524.2 4.1 Ethyl tert-butyl ether (ETBE) NE LAP PA 11/19/2015

EPA 524.2 4.1 Methylene chloride (Dichloromethane) NE LAP PA 5/24/2011

EPA524.2 4.1 Tetrahydrofuran (THF) NE LAP PA 5/24/2011

EPA524.2 4.1 Toluene NE LAP PA 1/18/2011

EPA524.2 4.1 m+p-Xylene NE LAP PA 7/25/2011

EPA524.2 4.1 n-Hexane NELAP PA 11/19/2015

~~ The Pennsylvania Department of Environmental Protection Laboratory Accreditation Program is a NELAP recognized

Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing.

Page 15 of 57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania t...if DEPARTMENT OF ENVIRONMENTAL PROTECTION Laboratory Scope of Accreditation

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes should be used only when associated with a valid certificate of accreditation.

DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TNI02128 (717) 656-2300 PADWIS ID: 36037

Matrix: Non-Potable Water Method Revision Analyte Accreditation Type Primary Effective Date

EPA524.2 4.1 o-Xylene NE LAP PA 5/24/2011 EPA524.2 4.1 tert-Arnyl methyl ether (TAME) NELAP PA 11/19/2015 EPA 531.1 3.1 3-Hydroxycarbofuran NE LAP PA 11/19/2015 EPA 531.1 3.1 Aldicarb (Temik) NE LAP PA 11119/2015 EPA 531.1 3.1 Aldicarb sulfone NELAP PA 11119/2015 EPA 531.1 3.1 Aldicarb sulfoxide NELAP PA 11/19/2015 EPA 531.1 3.1 Methiocarb (Mesurol) NELAP PA 11119/2015 EPA 531.1 3.1 Methomyl (Lannate) NE LAP PA 11119/2015 EPA 531.1 3.1 Propoxur(Baygon) NELAP PA 11119/2015 EPA 537 Modified Perfluorobutanesulfonic acid (PFBS) NELAP PA 5/24/2017 EPA 537 Modified Perfluorodecanoic acid (PFDA) NE LAP PA 5/24/2017 EPA 537 Modified Perfluorododecanoic acid (PFDoA) NE LAP PA 5/24/2017 EPA 537 Modified Perfluoroheptanoic acid (PFHpA) NELAP PA 5/24/2017 EPA 537 Modified Perfluorohexanesulfonic acid (PFHxS) NELAP PA 5/24/2017 EPA 537 Modified Perfluorohexanoic acid (PFHxA) NE LAP PA 5/24/2017 EPA 537 Modified Perfluorononanoic acid (PFNA) NE LAP PA 5/24/2017 EPA 537 Modified Perfluorooctanesulfonic acid (PFOS) NE LAP PA 5/24/2017 EPA 537 Modified Perfluorooctanoic acid (PFOA) NELAP PA 5/24/2017 EPA 537 Modified Perfluorotetradecanoic acid (PFT A) NE LAP PA 5/24/2017 EPA 537 Modified Perfluorotridecanoic acid (PFTrDA) NE LAP PA 5/24/2017 EPA 537 Modified Perfluoroundecanoic acid (PFUnA) NELAP PA 5/24/2017 EPA 6010 Aluminum NE LAP PA 12/12/2005 EPA 6010 Antimony NE LAP PA 12/12/2005 EPA 6010 Arsenic NELAP PA 12/12/2005 EPA6010 Barium NELAP PA 12112/2005 EPA 6010 Beryllium NE LAP PA 12/12/2005 EPA 6010 Boron NELAP PA 12/12/2005 EPA 6010 Cadmium NE LAP PA 12/12/2005 EPA6010 Calcium NE LAP PA 12/12/2005 EPA6010 Chromium NELAP PA 12/12/2005 EPA 6010 Cobalt NE LAP PA 12112/2005 EPA6010 Copper NELAP PA 12/12/2005 EPA 6010 Iron NELAP PA 12/12/2005 EPA6010 Lead NE LAP PA 12/12/2005 EPA 6010 Lithium NELAP PA 1/18/2011 EPA6010 Magnesium NE LAP PA 12112/2005 EPA 6010 Manganese NE LAP PA 12112/2005 EPA 6010 B Metals by ICP/AES NELAP PA 3/26/2012 EPA6010 c Metals by ICP/AES NE LAP PA 3/26/2012 EPA 6010 Molybdenum NELAP PA 12/12/2005 EPA 6010 Nickel NE LAP PA 12/12/2005 EPA 6010 Potassium NE LAP PA 12/12/2005 EPA 6010 Selenium NE LAP PA 12112/2005 EPA 6010 Silver NELAP PA 12/12/2005 EPA 6010 Sodium NELAP PA 12/12/2005

~~ The Pennsylvania Department of Environmental Protection Laboratory Accreditation Program. is a NELAP recognized

Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing. Page 16 of 57 www.dep.state.pa.us Issue Date: 09/28/2017

·~ pennsylvania ,... DEPARTMENT OF ENVIRONMENTAL

PROTECTION Laboratory Scope of Accreditation

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes

should be used only when associated with a valid certificate of accreditation.

DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TNI02128 (717) 656-2300

PADWIS ID: 36037

Matrix: Non-Potable Water

Method Revision Analyte Accreditation Type Primary Effective Date EPA 6010 Strontium NE LAP PA 12/12/2005

EPA 6010 Sulfur NE LAP PA 12/19/2011

EPA 6010 Tellurium NE LAP PA 2/4/2016

EPA 6010 Thallium NE LAP PA 12/12/2005

EPA 6010 Thorium NE LAP PA 11/19/2015

EPA6010 Tin NE LAP PA 12/12/2005

EPA 6010 Titanium NE LAP PA 12/12/2005

EPA6010 Tungsten NE LAP PA 11/19/2015

EPA 6010 Vanadium NE LAP PA 12/12/2005

EPA6010 Zinc NE LAP PA 12/12/2005

EPA 6010 Zirconium NE LAP PA 7/29/2015

EPA602 Benzene NE LAP PA 1119/2005

EPA 602 Ethylbenzene NE LAP PA 1/19/2005

EPA602 Methyl tert-butyl ether (MTBE) NE LAP PA 1119/2005

EPA 602 Naphthalene NE LAP PA 1118/2011

EPA602 Styrene NE LAP PA 6/24/2008

EPA602 Toluene NE LAP PA 1/19/2005

EPA602 Xylenes, total NE LAP PA 1/19/2005

EPA602 m+p-Xylene NE LAP PA 1/18/2011

EPA 602 o-Xylene NE LAP PA 1118/2011

EPA6020 Aluminum NE LAP PA 117/2010

EPA6020 Antimony NE LAP PA 1211212005

EPA6020 Arsenic NE LAP PA 1211212005

EPA6020 Barium NE LAP PA 12/12/2005

EPA6020 Beryllium NE LAP PA 12/12/2005

EPA6020 Boron NE LAP PA 1111/2012

EPA6020 Cadmium NE LAP PA 12/12/2005

EPA6020 Calcium NE LAP PA 117/2010

EPA6020 Chromium NE LAP PA 12/12/2005

EPA6020 Cobalt NE LAP PA 11123/2010

EPA6020 Copper NE LAP PA 12/12/2005

EPA 6020 Iron NE LAP PA 11123/2010

EPA6020 Lead NE LAP PA 12/12/2005

EPA6020 Magnesium NE LAP PA 117/2010

EPA6020 Manganese NE LAP PA 11/23/2010

EPA6020 A Metals by ICP/MS NE LAP PA 3/26/2012

EPA6020 Molybdenum NE LAP PA 117/2010

EPA6020 Nickel NE LAP PA 7/23/2008

EPA6020 Potassium NE LAP PA 117/2010

EPA6020 Selenium NE LAP PA 12/12/2005

EPA6020 Silver NE LAP PA 1/12/2007

EPA6020 Sodium NE LAP PA' 117/2010

EPA 6020 Strontium NE LAP PA 117/2010

EPA 6020 Thallium NE LAP PA 12/12/2005

EPA6020 Tin NE LAP PA 117/2010

~~ The Pennsylvania Department of Environmental Protection Laboratory Accreditation Program is a NELAP recognized

Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing.

Page 17 of57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania u DEPARTMENT OF ENVIRONMENTAL PROTECTION Laboratory Scope of Accreditation

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes should be used only when associated with a valid certificate of accreditation.

DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TNI02128 (717) 656-2300 PADWIS ID: 36037

Matrix: Non-Potable Water Method Revision Analyte Accreditation Type Primary Effective Date

EPA 6020 Titanium NELAP PA 11712010 EPA6020 Uranium, total NE LAP PA 11/19/2015 EPA 6020 Vanadium NELAP PA 11712010 EPA6020 Zinc NELAP PA 1118/2011 EPA608 4,4'-DDD NE LAP PA 111912005 EPA608 4,4'-DDE NE LAP PA 111912005 EPA608 4,4'-DDT NE LAP PA 111912005 EPA608 Aldrin (HHDN) NE LAP PA 111912005 EPA608 Aroclor-1016 (PCB-1016) NELAP PA 1211112006 EPA608 Aroclor-1221 (PCB-1221) NE LAP PA 1211112006 EPA608 Aroclor-1232 (PCB-1232) NE LAP PA 1211112006 EPA608 Aroclor-1242 (PCB-1242) NELAP PA 1211112006 EPA 608 Aroclor-1248 (PCB-1248) NE LAP PA 12/11/2006 EPA608 Aroclor-1254 (PCB-1254) NE LAP PA 1211112006 EPA608 Aroclor-1260 (PCB-1260) NELAP PA 1211112006 EPA 608 Aroclor-1262 (PCB-1262) NELAP PA 1119/2016 EPA608 Aroclor-1268 (PCB-1268) NELAP PA 11/13/2012 EPA 608 Chlordane (tech.) · NELAP PA 111912005 EPA608 Dieldrin NELAP PA 111912005 EPA608 Endosulfan I NELAP PA 111912005 EPA608 Endosulfan II NELAP PA 111912005 EPA608 Endosulfan sulfate NE LAP PA 111912005 EPA608 Endrin NELAP PA 1/19/2005 EPA608 Endrin aldehyde NE LAP PA 1119/2005 EPA608 Heptachlor NE LAP PA 1119/2005 EPA608 Heptachlor epoxide NE LAP PA 111912005 EPA608 Methoxychlor NELAP PA 51212006 EPA608 Mirex NE LAP PA 11/13/2012 EPA608 Toxaphene (Chlorinated camphene) NE LAP PA 111912005 EPA608 alpha-BHC (alpha-Hexachlorocyclohexane) NE LAP PA 111912005 EPA608 beta-BHC (beta-Hexachlorocyclohexane) NELAP PA 111912005 EPA608 delta-BHC ( delta-Hexachlorocyclohexane) NE LAP PA 111912005 EPA608 gamma-BHC (Lindane, gamma- NELAP PA 111912005

Rexach lorocyclohexane) EPA622 Azinphos-methyl (Guthion) NELAP PA 6/15/2009 EPA622 Bolstar (Sulprofos) NELAP PA 611512009 EPA622 Carbophenothion (Trithion) NE LAP PA 4/28/2010 EPA622 Chlorpyrifos NELAP PA 611512009 EPA622 Coumaphos NE LAP PA 611512009 EPA622 Demeton-0 NE LAP PA 611512009 EPA622 Demeton-S NE LAP PA 611512009 EPA622 Diazinon (Spectracide) NE LAP PA 611512009 EPA622 Dichlorovos (DDVP, Dichlorvos) NELAP PA 611512009 EPA622 Disulfoton NELAP PA 611512009 EPA622 EPN (Santox) NE LAP PA 611512009 EPA622 Ethion NELAP PA 611512009

~~ The Pennsylvania Department of Environmental Protection Laboratory Accreditation Program is a NELAP recognized

Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing. Page 18of57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania R DEPARTMENT OF ENVIRONMENTAL PROTECTION Laboratory Scope of Accreditation

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes

should be used only when associated with a valid certificate of accreditation.

DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TNI02128 (717) 656-2300

PADWIS ID: 36037

Matrix: Non-Potable Water

Method Revision Analyte Accreditation Type Primary Effective Date

EPA622 Ethoprop (Prophos) NE LAP PA 6/15/2009

EPA622 Famphur NE LAP PA 6/15/2009

EPA622 Fensulfothion NE LAP PA 6/15/2009

EPA 622 Fenthion NELAP PA 6/15/2009

EPA622 Malathion NE LAP PA 6/15/2009

EPA622 Merphos NE LAP PA 6/15/2009

EPA622 Methyl parathion (Parathion, methyl) NE LAP PA 6/15/2009

EPA622 Mevinphos NE LAP PA 6/15/2009

EPA 622 Naled NE LAP PA 6/15/2009

EPA622 Parathion, ethyl (Ethyl parathion, Parathion) NE LAP PA 6/15/2009

EPA622 Phorate (Thimet) NE LAP PA 6/15/2009

EPA622 Ronne! NE LAP PA 6/15/2009

EPA622 Stirophos (Tetrachlorovinphos) NE LAP PA 6/15/2009

EPA622 Tokuthion (Prothiophos) NELAP PA 6/15/2009

EPA622 Trichloronate NE LAP PA 6/15/2009

EPA624 1, 1, 1,2-Tetrachloroethane NELAP PA 1/19/2005

EPA624 1, 1, 1-Trichloroethane NE LAP PA 1/19/2005

EPA624 1,1,2,2-Tetrachloroethane NELAP PA 1/19/2005

EPA624 1, 1,2-Trichloro-1,2,2-trifluoroethane (Freon NE LAP PA 7/3/2007

113)

EPA624 1,1,2-Trichloroethane NE LAP PA 1/19/2005

EPA624 1, 1-Dich loroethane NE LAP PA 1/19/2005

EPA624 1, 1-Dichloroethene ( 1, 1-Dichloroethylene) NE LAP PA 1/19/2005

EPA624 1,1-Dichloropropene NELAP PA 7/3/2007

EPA624 1,2, 3-Trichlorobenzene NE LAP PA 7/3/2007

EPA624 1,2,3-Trichloropropane (1,2,3-TCP) NE LAP PA 7/3/2007

EPA624 1,2,3-Trimethylbenzene NELAP PA 7/3/2007

EPA 624 1,2,4-Trichlorobenzene NE LAP PA 7/3/2007

EPA624, 1,2,4-Trimethylbenzene NELAP PA 7/3/2007

EPA624 1,2-Dibromo-3-chloropropane (DBCP, NE LAP PA 7/3/2007 Dibromochloropropane)

EPA624 1,2-Dibromoethane (EDB, Ethylene NE LAP PA 7/3/2007 dibromide)

EPA624 1,2-Dichlorobenzene (o-Dichlorobenzene) NE LAP PA 1119/2005

EPA624 1,2-Dichloroethane NELAP PA 1/19/2005

EPA624 1,2-Dichloropropane NE LAP PA 1/19/2005

EPA624 1,3,5-Trimethylbenzene NE LAP PA 7/3/2007 .

EPA624 1,3-Dichlorobenzene (m-Dichlorobenzene) NE LAP PA 1/19/2005

EPA624 1,3-Dichloropropane NELAP PA 7/3/2007

EPA624 1,4-Dichlorobenzene (p-Dichlorobenzene) NE LAP PA 1/19/2005

EPA624 1,4-Dioxane (1,4-Diethyleneoxide) NE LAP PA 7/3/2007

EPA624 2,2-Dichloropropane NE LAP PA 7/3/2007

EPA624 . 2,4,4-Trimethyl-1-pentene (Diisobutylene) NE LAP PA 1/19/2016

EPA624 2,4,4-Trimethyl-2-pentene NE LAP PA 1119/2016

EPA624 2-Butanone (Methyl ethyl ketone, MEK) NE LAP PA 7/3/2007

EPA624 2-Chloroethyl vinyl ether NELAP PA 1/19/2005

~~ The Pennsylvania Department of Environmental Protection Laboratory Accreditation Program is a NELAP recognized

Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing.

Page 19 of57 www.dep.state.pa.us Issue Date: 09/28/2017

... ;,.v•«o~ .. ;,. .•. ,,"'t;

; -) ·,''·., , ..... ,, .. :

~ pennsylvania !1 DEPARTMENT OF ENVIRONMENTAL PROTECTION Laboratory Scope of Accreditation

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes should be used only when associated with a valid certificate of accreditation.

DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TNI02128 (717) 656-2300 PADWIS ID: 36037

Matrix: Non-Potable Water Method Revision Analyte Accreditation Type Primary Effective Date

EPA624 2-Chlorotoluene NELAP PA 7/3/2007 EPA624 2-Hexanone NE LAP PA 7/3/2007 EPA624 4-Chloro-2-nitrophenol NE LAP PA 7/3/2007 EPA624 4-Chlorotoluene NE LAP PA 7/3/2007 EPA624 4-Methyl-2-pentanone (MIBK) NE LAP PA 51212006 EPA624 Acetone NE LAP PA 71312007 EPA 624 Acetonitrile NELAP PA 7/3/2007 EPA624 Acrolein (Propenal) NE LAP PA 1/19/2005 EPA624 Acrylonitrile .NELAP PA 1/19/2005 EPA 624 Ally! chloride (3-Chloropropene) NE LAP PA 7/3/2007 EPA 624 Benzene NE LAP PA 1/19/2005 EPA624 Benzyl chloride NE LAP PA 11/19/2015 EPA624 Bromobenzene NELAP PA 7/3/2007 EPA624 Bromochloromethane NE LAP PA 51212006 EPA624 Bromodichloromethane NE LAP PA 111912005 EPA624 Bromoform NE LAP PA 1/19/2005 EPA624 Carbon disulfide NE LAP PA 7/3/2007 EPA624 Carbon tetrachloride NELAP PA 1/19/2005 EPA 624 Chlorobenzene NELAP PA 111912005 EPA624 Chloroethane NE LAP PA 111912005 EPA624 Chloroform NE LAP PA 1/19/2005 EPA624 Chloroprene (2-Chloro-1,3-butadiene) NE LAP PA 6/12/2009 EPA624 Cyclohexane NE LAP PA 7/3/2007 EPA 624 Dibromochloromethane NE LAP PA 41412005 EPA 624 Dibromomethane NELAP PA 7/3/2007 EPA624 Dichlorodifluoromethane (Freon 12) NE LAP PA 7/3/2007 EPA624 Diisopropyl ether (DIPE) NELAP PA 51212006 EPA624 Ethyl acetate NE LAP PA 1/20/2012 EPA624 Ethyl methacrylate NE LAP PA 7/3/2007 EPA624 Ethylbenzene NE LAP PA 1/19/2005 EPA624 Freon 113 (l,1,2-Trichloro-1,2,2- NELAP PA 2/1/2011 trifluoroethane) EPA624 Freon-123A NE LAP PA 2/1/2011 EPA 624 Heptane NE LAP PA 11/19/2015 EPA624 Hexachlorobutadiene (1,3- NE LAP PA 1/19/2016 Hexachlorobutadiene) EPA 624 Isobutyl alcohol (2-Methyl-1-propanol) NE LAP PA 7/3/2007 EPA624 Isopropyl acetate NELAP PA 111912016 EPA624 Isopropyl alcohol (2-Propanol) NE LAP PA 11/19/2015 EPA624 Isopropylbenzene (Cumene) NE LAP PA 51212006 EPA624 Methacrylonitrile NELAP PA 7/3/2007 EPA624 Methyl bromide (Bromomethane) NELAP PA 1/19/2005 EPA624 Methyl chloride (Chloromethane) NE LAP PA 111912005 EPA624 Methyl iodide (Iodomethane) NELAP PA 7/3/2007 EPA624 Methyl tert-butyl ether (MTBE) NE LAP PA 12/12/2005 EPA624 Methylene chloride (Dichloromethane) NELAP PA 111912005

~~ The Pennsylvania Deparbnent of Environmental Protection Laboratory Accreditation Program is a NELAP recognized

Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing. Page 20 of 57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania ,,., DEPARTMENT OF ENVIRONMENTAL

PROTECTION Laboratory Scope of Accreditation

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited aoalytes should be used only when associated with a valid certificate of accreditation.

DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TNI02128 (717) 656-2300 PADWIS ID: 36037

Matrix: Non-Potable Water

Method Revision Analyte Accreditation· Type Primary Effective Date EPA624 Methylmethacrylate NE LAP PA EPA 624 Naphthalene NE LAP PA EPA624 Pentachloroethane NELAP PA EPA624 Propionitrile (Ethyl cyanide) NE LAP PA EPA624 Styrene NE LAP PA EPA624 Tetrachloroethene (PCE, Perchloroethylene) NELAP PA EPA624 Tetrahydrofuran (THF) NELAP PA EPA624 Toluene NE LAP PA EPA624 Trichloroethene (TCE, Trichloroethylene) NE LAP PA EPA624 Trichlorofluoromethane (Freon 11) NE LAP PA EPA624 Vinyl acetate NELAP PA EPA624 Vinyl chloride (Chloroethene) NELAP PA EPA624 Xylt<nes, total NE LAP PA EPA624 cis-1,2-Dichloroethene NE LAP PA EPA624 cis-1,3-Dichloropropene NE LAP PA EPA624 m+p-Xylene NE LAP PA EPA624 n-Butyl acetate NE LAP PA EPA624 n-Butylbenzene NE LAP PA EPA624 n-Heptane NE LAP PA EPA624 n-Hexane NE LAP PA EPA624 n-Propyl acetate NE LAP PA EPA624 n-Propylbenzene NE LAP PA EPA624 o-Xylene NELAP PA EPA624 p-Isopropyltoluene ( 4-Isopropyltoluene) NELAP PA EPA624 sec-Butylbenzene NE LAP PA EPA 624 tert-Amyl methyl ether (TAME) NE LAP PA EPA624 tert-Butyl alcohol (2-Methyl-2-propanol) NE LAP PA EPA624 tert-Butyl ethyl ether NELAP PA EPA624 tert-Butylbenzene NELAP PA EPA624 trans-1,2-Dichloroethene NE LAP PA EPA624 trans-1,3-Dichloropropene NELAP PA EPA624 trans-1,4-Dichloro-2-butene NE LAP PA EPA625 1,1 '-Biphenyl (Biphenyl, Lemonene) NE LAP PA EPA625 1,2,4,5-Tetrachlorobenzene NE LAP PA EPA625 1,2,4-Trichlorobenzene NE LAP PA EPA625 1,2-Dichlorobenzene ( o-Dichlorobenzene) NELAP PA EPA625 1,2-Diphenylhydrazine NE LAP PA EPA625 1,3-Dichlorobenzene (m-Dichlorobenzene) NE LAP PA EPA 625 1,4-Dichlorobenzene (p-Dichlorobenzene) NE LAP PA EPA625 1,4-Dioxane (1,4-Diethyleneoxi~e) NELAP PA EPA625 1-Methylnaphthalene NE LAP PA EPA625 1-Methylphenanthrene NE LAP PA EPA625 2,2'-0xybis( 1-chloropropane) (bis(2-Chloro- NELAP PA

1-methylethyl) ether) EPA625 2,2'-oxybis(l-Chloropropane) NELAP PA EPA625 2,3,4,6-Tetrachlorophenol NE LAP PA

~~ The Pennsylvania Department of Environmental Protection Laboratory Accreditation Program is a NELAP recognized

Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing.

7/3/2007 7/3/2007 7/3/2007 7/3/2007 5/2/2006

1/19/2005 7/3/2007

1/19/2005 1/19/2005 1/19/2005 7/3/2007

1/19/2005 1/19/2005 6/12/2009 1/19/2005 1/19/2016 1/19/2016 7/3/2007 7/3/2007 7/3/2007

1/19/2016 7/3/2007

1/19/2016 7/3/2007 7/3/2007 512/2006 5/2/2006 5/2/2006 7/3/2007

1/19/2005 1/19/2005 1/19/2016 7/3/2007 5/2/2006

1/19/2005 1/19/2005 5/2/2006

1/19/2005 1/19/2005 7/3/2007

1/19/2016 5/2/2006

1/19/2016

1/19/2005 7/3/2007

Page 21 of 57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania g DEPARTMENT OF ENVIRONMENTAL PROTECTION Laboratory Scope of Accreditation

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes should be used only when associated with a valid certificate of accreditation.

DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TN102128 (717) 656-2300 PADWIS ID: 36037

Matrix: Non-Potable Water Method Revision Analyte Accreditation Type Primary Effective Date

EPA625 2,3-Dichloroaniline NELAP PA EPA625 2,3-Dinitrotoluene NE LAP PA EPA625 2,4,5-Trichlorophenol NE LAP PA EPA625 2,4,6-Trichlorophenol NELAP PA EPA 625 2,4-Dichlorophenol NE LAP PA EPA625 2,4-Dimethylphenol NE LAP PA EPA625 2,4-Dinitrophenol NE LAP PA EPA625 2,4-Dinitrotolue_ne (2,4-DNT) NE LAP PA EPA625 2,6-Dichlorophenol NE LAP PA EPA625 2,6-Dinitrotoluene (2,6-DNT) NE LAP PA EPA625 2-Chloronaphthalene NE LAP PA EPA625 2-Chlorophenol NE LAP PA EPA625 2-Methyl-4,6-dinitrophenol (4,6-Dinitro-2- NELAP PA

methylphenol) EPA625 2-Methylnaphthalene NELAP PA EPA 625 2-Methylphenol (o-Cresol) NELAP PA EPA625 2-Nitroaniline NE LAP PA EPA625 2-Nitrophenol NE LAP PA EPA625 3+4-Methylphenol (m+p-Cresol) NE LAP PA EPA625 3,3'-Dichlorobenzidine NE LAP PA EPA625 3-Nitroaniline NE LAP PA EPA625 4-Bromophenyl phenyl ether NE LAP PA EPA625 4-Chloro-3-methylphenol NE LAP PA EPA625 4-Chloroaniline NE LAP PA EPA625 4-Chlorophenyl phenyl ether NE LAP PA EPA625 4-Nitroaniline NELAP PA EPA625 4-Nitrophenol NE LAP PA EPA625 Acenaphthene NE LAP PA EPA625 Acenaphthylene NELAP PA EPA625 Acetophenone NE LAP PA EPA625 Aniline NE LAP PA EPA625 Anthracene NE LAP PA EPA625 Benzidine NELAP PA EPA625 Benzo[ a ]anthracene NE LAP PA EPA 625 Benzo[ a ]pyrene NELAP PA EPA625 Benzo[b ]fluoranthene NELAP PA EPA625 Benzo[ghi]perylene NE LAP PA EPA625 Benzo[k]fluoranthene NE LAP PA EPA625 Benzoic acid NELAP PA EPA625 Benzyl alcohol NELAP PA EPA625 Butyl benzyl phthalate (Benzyl butyl NE LAP PA

phthalate) EPA625 Carbazole NE LAP PA EPA625 Chrysene (Benzo[a]phenanthrene) NE LAP PA EPA625 Di-n-butyl phthalate NE LAP PA EPA625 Di-n-octyl phthalate NE LAP PA

~~ The Pennsylvania Department of Environmental Protection Laboratory Accreditation Program is a NELAP recognized

Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing.

5/2/2006 7/3/2007 7/3/2007

1/19/2005 1/19/2005 1/19/2005 1/19/2005 1/19/2005 7/3/2007

1/19/2005 1/19/2005 1/19/2005 1/19/2005

7/3/2007 7/3/2007 7/3/2007

1/19/2005 7/3/2007

1/19/2005 7/3/2007

1/19/2005 1/19/2005 7/3/2007

1/19/2005 7/3/2007

1/19/2005 1/19/2005 1/19/2005 5/2/2006 5/2/2006 4/4/2005

1/19/2005 1/19/2005 1/19/2005 1/19/2005 1/19/2005 1/19/2005 51212006 7/3/2007

1/19/2005

5/2/2006 1/19/2005 1/19/2005 1/19/2005

Page 22 of 57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania t..df DEPARTMENT OF ENVIRONMENTAL PROTECTION Laboratory Scope of Accreditation

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes

should be used only when associated with a valid certificate of accreditation.

DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TNI02128 (717) 656-2300

PADWIS ID: 36037

Matrix: Non-Potable Water

Method Revision Analyte Accreditation Type Primary Effective Date EPA625 Dibenzo[ a,h ]anthracene NE LAP PA

EPA625 Dibenzofuran NE LAP PA

EPA625 Diethyl phthalate NE LAP PA

EPA625 Dimethyl phthalate NE LAP PA

EPA625 Diphenyl ether NE LAP PA

EPA625 Fluoranthene NE LAP PA

EPA625 Fluorene NE LAP PA

EPA 625 Hexachlorobenzene NE LAP PA

EPA625 Hexachlorobutadiene (1,3- NE LAP PA Hexachlorobutadiene)

EPA625 Hexachlorocyclopentadiene NE LAP PA

EPA625 Hexachloroethane NE LAP PA

EPA 625 Indeno( 1,2,3-cd)pyrene NE LAP PA

EPA625 Isophorone NELAP PA

EPA625 N-Nitrosodi-n-butylamine NE LAP PA

EPA625 N-Nitrosodi-n-propylamine NE LAP PA

EPA 625 N-Nitrosodiethylamine NE LAP PA

EPA625 N-Nitrosodimethylamine NELAP PA

EPA625 N-Nitrosodiphenylamine NELAP PA

EPA 625 N-Nitrosopyrrolidine NE LAP PA

EPA625 Naphthalene NE LAP PA

EPA625 Nitro benzene NE LAP PA

EPA625 Pentachlorobenzene NELAP PA

EPA625 Pentachlorophenol (PCP) NELAP PA

EPA625 Phenanthrene NE LAP PA

EPA625 Phenol NE LAP PA

EPA625 Pyrene NELAP PA

EPA625 Pyridine NELAP PA

EPA625 alpha-Terpineol NELAP PA

EPA625 bis(2-Chloroethoxy)methane NE LAP PA

EPA625 bis(2-Chloroethyl) ether NELAP PA

EPA 625 bis(2-Ethylhexyl) phthalate (DEHP) NE LAP PA

EPA625 n-Decane NE LAP PA

EPA625 n-Docosane NE LAP PA

EPA625 n-Dodecane NELAP PA

EPA625 n-Eicosane NE LAP PA

EPA625 n-Hexadecane NELAP PA

EPA625 n-Octadecane NELAP PA

EPA625 n-Tetradecane NELAP PA

EPA625 o-Toluidine (2-Toluidine, 2-Methylaniline) NELAP PA

EPA680 Decachlorobiphenyl NELAP PA

EPA 680 Dichlorobiphenyls NE LAP PA

EPA680 Heptachlorobiphenyls NE LAP PA

EPA 680 Hexachlorbiphenyls NE LAP PA

EPA680 Monochlorobiphenyls · NELAP PA

EPA680 Nonachlorobiphenyls NE LAP PA

~~ The Pennsylvania Department of Environmental Protection Laboratory Accreditation Program is a NELAP recognized

Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing.

1/1912005 7/3/2007

1/1912005 1/19/2005 71312007

1/19/2005 1/19/2005 1/19/2005 1/19/2005

1/19/2005 1/1912005 1/19/2005 1/19/2005 5/2/2006

1/19/2005 51212006

1/19/2005 1/19/2005 51212006

1/19/2005 1/19/2005 7/3/2007

1/19/2005 1/19/2005 1/19/2005 1/19/2005 51212006 51212006

1/19/2005 1/19/2005 1/19/2005 51212006 51212006 51212006 51212006 51212006 51212006 51212006 7/3/2007

1/19/2016 l/19/2016 1/1912016 1/19/2016 1/19/2016 1/19/2016

Page 23 of 57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania ~ DEPARTMENT OF ENVIRONMENTAL

PROTECTION Laboratory Scope of Accreditation

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes , should be used only when associated with a valid certificate of accreditation.

DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TNI02128 (717) 656-2300 PADWIS ID: 36037

Matrix: Non-Potable Water Method Revision Analyte Accreditation Type Primary Effective Date

EPA680 Octachlorobiphenyls NELAP PA 1119/2016 EPA 680 Pentachlorobiphenyls NELAP PA 1119/2016 EPA680 Tetrachlorobiphenyls NELAP PA 1119/2016 EPA680 Trichlorobiphenyls NELAP PA 1119/2016 EPA6850 Perchlorate NELAP PA 1/19/2011 EPA 7196 A Chromium VI NELAP PA 4/6/2006 EPA 7199 Chromium VI NELAP PA 1/4/2006 EPA 7470 Mercury NELAP PA 11/21/2005 EPA8011 1,2-Dibromo-3-chloropropane (DBCP, NELAP PA 5/2/2006

Dibromochloropropane) EPA8011 1,2-Dibromoethane (EDB, Ethylene NELAP PA 12/12/2005

di bromide) EPA 8015 Diesel-range organics (DRO) NELAP PA 12/12/2005 EPA 8015 Diethylene glycol NE LAP PA 1/20/2012 EPA 8015 Ethane NELAP PA 12/4/2007 EPA 8015 Ethanol NELAP PA 12/4/2007 EPA 8015 Ethene NELAP PA 12/4/2007 EPA 8015 Ethylene glycol NELAP PA 12/4/2007 EPA 8015 Gasoline-range organics (GRO) NELAP PA 12/12/2005 EPA8015 Isobutyl alcohol (2-Methyl-1-propanol) NELAP PA 217/2012 EPA 8015 Isopropyl alcohol (2-Propanol) NELAP PA 12/4/2007 EPA 8015 Methane NELAP PA 12/4/2007 EPA 8015 Methanol NELAP PA 12/4/2007 EPA 8015 D Nonhalogenated organics by GC/FID NELAP PA 7/29/2015 EPA 8015 c Nonhalogenated organics by GC/FID NELAP PA 3/26/2012 EPA8015 B Nonhalogenated organics by GC/FID NELAP PA 3/26/2012 EPA 8015 Propane NELAP PA 12/4/2007 EPA 8015 Propylene glycol NELAP PA 1/20/2012 EPA 8015 Tetraethylene glycol NELAP PA 1/20/2012 EPA 8015 Total petroleum hydrocarbons (TPH) NELAP PA 1/24/2007 EPA 8015 Triethylene glycol NELAP PA 1/20/2012 EPA 8015 n-Butyl alcohol (n-Butanol, 1-Butanol) NELAP PA 217/2012 EPA 8015 n-Propanol (1-Propanol) NELAP PA 217/2012 EPA 8021 Benzene NELAP PA 12112/2005 EPA 8021 Ethyl benzene NELAP PA 12/12/2005 EPA 8021 Isopropylbenzene (Cumene) NE LAP PA 12/12/2005 EPA 8021 Methyl tert-butyl ether (MTBE) NELAP PA 2/11/2011 EPA 8021 Naphthalene NELAP PA 6/24/2008 EPA 8021 Toluene NELAP PA 12/12/2005 EPA 8021 B voes by GC/PID/ELCD NELAP PA 3/26/2012 EPA 8021 Xylenes, total NELAP PA 12/12/2005 EPA 8021 m-Xylene NELAP PA 11/23/2009 EPA 8021 o-Xylene NELAP PA 11/2312009 EPA 8021 p-Xylene NELAP PA 11/23/2009 EPA 8081 2,4'-DDD NELAP PA 11119/2015 EPA 8081 2,4'-DDE NELAP PA 11/19/2015

~~ The Pennsylvania Department of Environmental Protection Laboratory Accreditation Program is a NELAP recognized

Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing. Page 24 of57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania t~ DEPARTMENT OF ENVIRONMENTAL

PROTECTION Laboratory Scope of Accreditation

:.'9".'""~ ', 'til' ~·. ;. ,-- ·_

' ' ' .-..t -. .. ,,, .. n&1>r··

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes should be used only when associated with a valid certificate of accreditation.

DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TNI02128 (717) '656-2300

PADWIS ID: 36037

Matrix: Non-Potable Water

Method Revision Analyte Accreditation Type Primary Effective Date EPA 8081 2,4'-DDT NE LAP PA 11119/2015

EPA 8081 4,4'-DDD NE LAP PA 2/10/2006

EPA 8081 4,4'-DDE NE LAP PA 12/1212005

EPA 8081 4,4'-DDT NE LAP PA 12/12/2005

EPA8081 Aldrin (HHDN) NE LAP PA 12/12/2005

EPA 8081 Chlordane (tech.) NE LAP PA 12/12/2005

EPA 8081 Dieldrin NE LAP PA 12/12/2005

EPA 8081 Endosulfan I NE LAP PA 2/10/2006

EPA 8081 Endosulfan II NE LAP PA 12/12/2005

EPA8081 Endosulfan sulfate NE LAP PA 12/12/2005

EPA 8081 Endrin NE LAP PA 12/12/2005

EPA 8081 Endrin aldehyde NE LAP PA 12/12/2005

EPA8081 Endrin ketone NE LAP PA 2/10/2006

EPA 8081 Heptachlor NE LAP PA 12/12/2005

EPA 8081 Heptachlor epoxide NE LAP PA 12/12/2005

EPA 8081 Kepone NE LAP PA 51212006

EPA 8081 Methoxychlor NE LAP PA 12/12/2005

EPA 8081 Mirex NE LAP PA 12/12/2005

EPA8081 A Organochlorine pesticides by GC/ECD NE LAP PA 3/26/2012

EPA8081 B Organochlorine pesticides by GC/ECD NE LAP PA 11112013

EPA 8081 Toxaphene (Chlorinated camphene) NE LAP PA 12/12/2005

EPA 8081 alpha-BHC (alpha-Hexachlorocyclohexane) NE LAP PA 2/10/2006

EPA8081 alpha-Chlordane NE LAP PA 2/10/2006

EPA 8081 beta-BHC (beta-Hexachlorocyclohexane) NE LAP PA 211012006

EPA 8081 delta-BHC ( delta-Hexachlorocyclohexane) NE LAP PA 2/10/2006

EPA 8081 gamma-BHC (Lindane, gamma- NE LAP PA 2/10/2006 Rexach lorocyclohexane)

EPA8081 gamma-Chlordane NE LAP PA 2/10/2006

EPA 8082 Aroclor-1016 (PCB-1016) NE LAP PA 12/11/2006

EPA8082 Aroclor-1221 (PCB-1221) NE LAP PA 12/11/2006

EPA8082 Aroclor-1232 (PCB-1232) NE LAP PA 12/11/2006

EPA8082 Aroclor-1242 (PCB-1242) NE LAP PA 12/11/2006

EPA 8082 Aroclor-1248 (PCB-1248) NE LAP PA 12/11/2006

EPA 8082 Aroclor-1254 (PCB-1254) NE LAP PA 12/1112006

EPA 8082 Aroclor-1260 (PCB-1260) NE LAP PA 12/11/2006

EPA 8082 Aroclor-1262 (PCB-1262) NE LAP PA 7/23/2008

EPA8082 Aroclor-1268 (PCB-1268) NE LAP PA 7/23/2008

EPA8082 Decachlorobiphenyl NE LAP PA 12/17/2012

EPA 8082 A PCBs by GC/ECD NE LAP PA 3/26/2012

EPA8141 Alachlor (Lasso) NE LAP PA 1/21/2009

EPA8141 Atrazine NE LAP PA 12/12/2005

EPA 8141 Azinphos-methyl (Guthion) NE LAP PA 12/12/2005

EPA 8141 Bolstar (Sulprofos) NE LAP PA 12/12/2005

EPA8141 Carbophenothion (Trithion) NE LAP PA 11/9/2012

EPA 8141 Chlorpyrifos NE LAP PA 12/12/2005

EPA8141 Coumaphos NE LAP PA 12/12/2005

~~ The Pennsylvania Department of Environmental Protection Laboratory Accreditation Program is a NELAP recognized

Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing.

Page 25 of57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania u DEPARTMENT OF ENVIRONMENTAL PROTECTION Laboratory Scope of Accreditation

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes should be used only when associated with a valid certificate of accreditation.

DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TNI02128 (717) 656-2300 PADWIS ID: 36037

Matrix: Non-Potable Water Method Revision Analyte Accreditation Type Primary Effective Date

EPA8141 Demeton-0 NELAP PA 12/12/2005 EPA 8141 Demeton-S NELAP PA 12/12/2005 EPA8141 Diazinon (Spectracide) NE LAP PA 12/12/2005 EPA 8141 Dichlorovos (DDVP, Dichlorvos) NE LAP PA 12/12/2005 EPA 8141 Disulfoton NE LAP PA 12/12/2005 EPA8141 EPN (Santox) NE LAP PA 12/12/2005 EPA 8141 Ethion NELAP PA 12/12/2005 EPA8141 Ethoprop (Prophos) NE LAP PA 12/12/2005 EPA8141 Famphur NE LAP PA 12/12/2005 EPA 8141 Fensulfothion NELAP PA 12/12/2005 EPA8141 Fenthion NE LAP PA 12/12/2005 EPA8141 Malathion NELAP PA 12/12/2005 EPA 8141 Merphos NELAP PA 12/12/2005 EPA8141 Methyl parathion (Parathion, methyl) NELAP PA 12/12/2005 EPA8141 Metolachlor NE LAP PA 1124/2007 EPA 8141 Mevinphos NELAP PA 12/12/2005 EPA8141 Naled NELAP PA 12112/2005 EPA8141 B Organophosphorus compounds by GC/NPD NELAP PA 3/26/2012 EPA 8141 A Organophosphorus compounds by GC/NPD NELAP PA 3/26/2012 EPA8141 Parathion, ethyl (Ethyl parathion, Parathion) NELAP PA 12/12/2005 EPA8141 Phorate (Thimet) NE LAP PA 12/12/2005 EPA 8141 Ronne! NE LAP PA 12/12/2005 EPA8141 Simazine NE LAP PA 12/12/2005 EPA8141 Stirophos (Tetrachlorovinphos) NE LAP PA 51212006 EPA 8141 Tokuthion (Prothiophos) NELAP PA 12/12/2005 EPA8141 Trichloronate NE LAP PA 51212006 EPA 8151 2,4,5-T NELAP PA 12/12/2005 EPA 8151 2,4,5-TP (Silvex) NE LAP PA 12/12/2005 EPA 8151 2,4-D NE LAP PA 12/12/2005 EPA 8151 2,4-DB (Butoxon) NE LAP PA 1211212005 EPA 8151 A Chlorinated herbicides by GC/ECD NELAP PA 3/26/2012 EPA 8151 Dalapon (2,2-Dichloropropionic acid) NE LAP PA 12/12/2005 EPA 8151 Dicamba NE LAP PA 12/12/2005 EPA 8151 Dichloroprop (Dichlorprop) NE LAP PA 112412007 EPA 8151 Dinoseb (2-sec-Butyl-4,6-dinitrophenol, NELAP PA 12/12/2005

DNBP) EPA8151 MCPA NE LAP PA 1211212005 EPA 8151 MCPP (Mecoprop) NELAP PA 12/12/2005 EPA 8151 Pentachlorophenol (PCP) NE LAP PA 12/12/2005 EPA 8151 Picloram (4-Amino-3,5,6-trichloro-2- NE LAP PA 12/12/2005

pyridinecarboxylic acid) EPA 8260 1,1,1,2-Tetrachloroethane NELAP PA 12/12/2005 EPA8260 I, I, I-Trichloroethane NELAP PA 12/12/2005 EPA 8260 I, 1,2,2-Tetrachloroethane NE LAP PA 12/12/2005 EPA8260 I, l ,2-Trichloro-1,2,2-trifluoroethane (Freon NELAP PA 12/12/2005

113)

~~ The Pennsylvania Department of Environmental Protection Laboratory Accreditation Program is a NELAP recognized

Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing. Page 26 of57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania ,,., DEPARTMENT OF ENVIRONMENTAL

PROTECTION Laboratory Scope of Accreditation

.. :J-0~.Cc,~·· ..

~--,· (~. ;) ··~.·

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes

should be used only when associated with a valid certificate of accreditation.

DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TNI02128 (717) 656-2300

PADWIS ID: 36037

Matrix: Non-Potable Water

Method Revision Analyte Accreditation Type Primary Effective Date EPA 8260 1,1,2-Trichloroethane NE LAP PA 12/12/2005

EPA 8260 1, 1-Dichloroethane NE LAP PA 12/12/2005

EPA8260 1, 1-Dichloroethene ( 1, 1-Dichloroethylene) NELAP PA 12/12/2005

EPA 8260 1, 1-Dichloropropene NELAP PA 12112/2005

EPA8260 1,2,3-Trichlorobenzene NE LAP PA 12112/2005

EPA 8260 1,2,3-Trichloropropane ( 1,2,3-TCP) NE LAP PA 12/12/2005

EPA 8260 1,2,3-Trimethylbenzene NE LAP PA 1/19/2016

EPA 8260 1,2,4-Trichlorobenzene NELAP PA 12112/2005

EPA 8260 1,2,4-Trimethy !benzene NE LAP PA 12112/2005

EPA 8260 l,2-Dibromo-3-chloropropane (DBCP, NE LAP PA 1211212005 Dibromochloropropane)

EPA 8260 1,2-Dibromoethane (EDB, Ethylene NELAP PA 1211212005 dibromide)

EPA 8260 1,2-Dichloro-l, 1,2-trifluoroethane NE LAP PA 3/19/2015

EPA8260 1,2-Dichlorobenzene (o-Dichlorobenzene) NELAP PA 12/12/2005

EPA8260 1,2-Dichloroethane NE LAP PA 12/12/2005

EPA 8260 1,2-Dichloropropane NELAP PA 12112/2005

EPA8260 1,2-Diethylbenzene NELAP PA 1119/2016

EPA 8260 1,3,5-Trichlorobenzene NE LAP PA 1119/2016

EPA8260 1,3,5-Trimethylbenzene NE LAP PA 12/12/2005

EPA 8260 1,3-Butadiene (Divinyl) NE LAP PA 1119/2016

EPA 8260 1,3-Dichloro-2-butene NE LAP PA 1119/2016

EPA8260 1,3-Dichlorobenzene (m-Dichlorobenzene) NE LAP PA 12/12/2005

EPA8260 1,3-Dichloropropane NE LAP PA 12/12/2005

EPA8260 1,3-Diethylbenzene NE LAP PA 1/19/2016

EPA8260 1,4-Dichlorobenzene (p-Dichlorobenzene) NELAP PA 12/12/2005

EPA 8260 1,4-Dioxane (1,4-Diethyleneoxide) NE LAP PA 12/12/2005

EPA 8260 2,2-Dichloropropane NELAP. PA 51212006 EPA 8260 2-Butanone (Methyl ethyl ketone, MEK) NE LAP PA 51212006 EPA 8260 2-Chloroethyl vinyl ether NE LAP PA 12/12/2005

EPA 8260 2-Chlorotoluene NE LAP PA 12/12/2005

EPA 8260 2-Hexanone NELAP PA 12/12/2005

EPA 8260 2-Nitropropane NE LAP PA 1/19/2011

EPA8260 3,3'-Dimethyl-1-butanol NE LAP PA 4/17/2009

EPA 8260 4-Chlorotoluene NE LAP PA 12/12/2005

EPA8260 4-Methyl-2-pentanone (MIBK) NE LAP PA 12112/2005

EPA 8260 Acetone NELAP PA 12/12/2005

EPA 8260 Acetonitrile NE LAP PA 12/12/2005

EPA 8260 Acrolein (Propenal) NE LAP PA 12/12/2005 EPA8260 Acrylonitrile NE LAP PA 12/12/2005 EPA 8260 Ally! chloride (3-Chloropropene) NE LAP PA 12/12/2005

EPA8260 Benzene NE LAP PA 12/12/2005

EPA 8260 Benzyl chloride NE LAP PA 7/3/2007

EPA 8260 Bromobenzene NE LAP PA 12/12/2005

EPA 8260 Bromochloromethane NELAP PA 12/12/2005

EPA 8260 Bromodichloromethane NELAP PA 12/12/2005

~~ The Pennsylvania Department of Environmental Protection Laboratory Accreditation Program is a NELAP recognized

Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing. Page 27 of57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania u DEPARTMENT OF ENVIRONMENTAL PROTECTION Laboratory Scope of Accreditation

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes should be used onlY: when associated with a valid certificate of accreditation.

DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TNI02128 (717) 656-2300 PADWIS ID: 36037

Matrix: Non-Potable Water Method Revision Analyte Accreditation Type Primary Effective Date

EPA 8260 Bromoform NE LAP PA 12/12/2005 EPA8260 Carbon disulfide NE LAP PA 12/12/2005 EPA 8260 Carbon tetrachloride NELAP PA 12/12/2005 EPA8260 Chlorobenzene NE LAP PA 12/12/2005 EPA8260 Chloroethane NE LAP PA 12/12/2005 EPA 8260 Chloroform NE LAP PA 12/12/2005 EPA 8260 Chloroprene (2-Chloro-1,3-butadiene) NE LAP PA 7/3/2007 EPA8260 Crotonaldehyde NE LAP PA 10/30/2014 EPA 8260 Cyclohexane NELAP PA 7/3/2007 EPA 8260 Cyclohexanone NE LAP PA 617/2012 EPA8260 Dibromochloromethane NE LAP PA 12/12/2005 EPA8260 Dibromomethane NE LAP PA 51212006 EPA 8260 Dichloroditluoromethane (Freon 12) NELAP PA 12/12/2005 EPA8260 Diethyl ether (Ethyl ether) NELAP PA 2/1/2011 EPA 8260 Diisopropyl ether (DIPE) NELAP PA 7/3/2007 EPA8260 Dimethyl ether NE LAP PA 617/2012 EPA 8260 Epichlorohydrin (l-Chloro-2,3- NELAP PA 4/17/2009

epoxypropane) EPA 8260 Ethanol NELAP PA 1/24/2007 EPA 8260 Ethyl acetate NE LAP PA 1/24/2007 EPA8260 Ethyl methacrylate NELAP PA 1/24/2007 EPA 8260 Ethyl tert-butyl ether (ETBE) NE LAP PA 1/24/2007 EPA8260 Ethylbenzene NE LAP PA 12/12/2005 EPA8260 Ethylene oxide NELAP PA 10/30/2014 EPA8260 Freon 113 (1,1,2-Trichloro-1,2,2- NELAP PA 3/4/2015

tritluoroethane) EPA 8260 Gasoline-range organics (GRO) NELAP PA 6/8/2006 EPA 8260 Heptane NE LAP PA 1/20/2012 EPA 8260 Hexachlorobutadiene ( 1,3- NELAP PA 12/12/2005

Hexachlorobutadiene) EPA 8260 Hexachloroethane NE LAP PA 5/23/2012 EPA 8260 Isobutyl alcohol (2-Methyl-1-propanol) NELAP PA 7/3/2007 EPA8260 Isopropyl alcohol (2-Propanol) NELAP PA 1/18/2011 EPA 8260 Isopropylbenzene (Cumene) NE LAP PA 51212006 EPA8260 Methacrylonitrile NELAP PA 7/3/2007 EPA 8260 Methyl acetate NELAP PA 1/24/2007 EPA8260 Methyl bromide (Bromomethane) NE LAP PA 12/12/2005 EPA 8260 Methyl chloride (Chloromethane) NELAP PA 12/12/2005 EPA 8260 Methyl iodide (Iodomethane) NELAP PA 512512007 EPA 8260 Methyl tert-butyl ether (MTBE) NE LAP PA 12/12/2005 EPA 8260 Methylcyclohexane NE LAP PA 1/21/2009 EPA8260 Methylene chloride (Dichloromethane) NE LAP PA 12/12/2005 EPA8260 Methylmethacrylate NELAP PA 5/25/2007 EPA 8260 Naphthalene NELAP PA 12/12/2005 EPA8260 Pentachloroethane NELAP PA 1/24/2007 EPA8260 Propionitrile (Ethyl cyanide) NELAP PA 12/12/2005

~~ The Pennsylvania Department of Environmental Protection Laboratory Accreditation Program is a NELAP recognized

Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing. Page 28 of57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania t1 DEPARTMENT OF ENVIRONMENTAL PROTECTION Laboratory Scope of Accreditation

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes

should be used only when associated with a valid certificate of accreditation. DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TNI02128 (717) 656-2300

PADWIS ID: 36037

Matrix: Non-Potable Water

Method Revision Analyte Accreditation Type Primary Effective Date EPA 8260 EPA 8260 EPA 8260 EPA8260 EPA 8260 EPA8260 EPA 8260 EPA 8260 EPA 8260 EPA8260 EPA8260 EPA 8260 EPA8260 EPA 8260 EPA 8260 EPA 8260 EPA8260 EPA8260 EPA 8260 EPA 8260 EPA 8260 EPA 8260 EPA 8260 EPA8260 EPA 8260 EPA8260 EPA 8260 EPA 8260 EPA8260 EPA 8260 EPA 8260 EPA 8260 SIM EPA 8270 EPA 8270 EPA 8270 EPA8270 EPA8270 EPA 8270 EPA 8270 EPA 8270 EPA 8270 EPA 8270 EPA 8270 EPA8270 EPA8270

c B

Styrene NE LAP Tetrachloroethene (PCB, Perchloroethylene) NE LAP Tetrahydrofuran (THF) NE LAP Toluene NE LAP Trichloroethene (TCE, Trichloroethylene) NE LAP Trichlorofluoromethane (Freon 11) NE LAP voes by GC/MS NE LAP voes by GC/MS NE LAP Vinyl acetate NE LAP Vinyl chloride (Chloroethene) NE LAP Xylenes, total NE LAP cis-1,2-Dichloroethene NE LAP cis-1,3-Dichloropropene NE LAP m+p-Xylene NE LAP n-Butyl acetate NE LAP n-Butyl alcohol (n-Butanol, 1-Butanol) NE LAP n-Butylbenzene NE LAP n-Hexane NE LAP n-Propylamine NELAP n-Propylbenzene NE LAP o-Xylene NE LAP p-Isopropyltoluene (4-Isopropyltoluene) NE LAP sec-Butylbenzene NE LAP tert-Amyl alcohol (2-Methyl-2-butanol) NE LAP tert-Amyl methyl ether (TAME) NE LAP tert-Butyl alcohol (2-Methyl-2-propanol) NE LAP tert-Butyl formate NE LAP tert-Butylbenzene NE LAP trans-1,2-Dichloroethene NE LAP trans-1,3-Dichloropropene NE LAP trans-1,4-Dichloro-2-butene NELAP 1,4-Dioxane (1,4-Diethyleneoxide) NE LAP 1,1 '-Biphenyl (Biphenyl, Lemonene) NE LAP 1,2,3,4-Tetrachlorobenzene NE LAP 1,2,3 ,4-Tetrahydronaphthalene NE LAP 1,2,3,5-Tetrachlorobenzene NE LAP 1,2,4,5-Tetrachlorobenzene NE LAP 1,2,4-Trichlorobenzene NE LAP 1,2-Dichlorobenzene ( o-Dichlorobenzene) NE LAP 1,2-Diphenylhydrazine NE LAP 1,3,5-Trinitrobenzene (1,3,5-TNB) NE LAP 1,3-Dichlorobenzene (m-Dichlorobenzene) NE LAP 1,3-Dinitrobenzene (1,3-DNB) NE LAP 1,4-Dichlorobenzene (p-Dichlorobenzene) NE LAP 1,4-Dinitrobenzene (1,4-DNB) NE LAP

~~

PA PA PA PA PA PA PA PA PA PA PA PA PA PA PA PA PA PA PA PA PA PA PA PA PA PA PA PA PA PA PA PA PA PA PA PA PA PA PA PA PA PA PA PA PA

The Pennsylvania Department of Environmental Protection Laboratory Accreditation Program is a NELAP recognized Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing.

12/12/2005 12/12/2005

1/18/2011 12/12/2005 12112/2005 12/12/2005 3126/2012 3/26/2012

12/12/2005 12/12/2005 12/12/2005 12112/2005 12/12/2005 4117/2009 1119/2016 4/17/2009

12/12/2005 1120/2012

12112/2005 1124/2007 4/17/2009 1124/2007

12112/2005 411712009 1124/2007

12112/2005 4/17/2009

12/12/2005 12/12/2005 1.2/12/2005

7/3/2007 12/4/2007 4/1712009

7/3/2007 4117/2009

7/3/2007 12/12/2005 12/12/2005 12/12/2005 12/12/2005 12/1212005 12/12/2005 12/12/2005 12/12/2005 4/1712009

Page 29 of57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania t....tf DEPARTMENT OF ENVIRONMENTAL PROTECTION Laboratory Scope of Accreditation

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes should be used only when associated with a valid certificate of accreditation.

DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TN102128 (717) 656-2300 PADWIS ID: 36037

Matrix: Non-Potable Water

Method Revision Analyte Accreditation Type Primary Effective Date EPA 8270 1,4-Dioxane (1,4-Diethyleneoxide) NELAP PA 4/17/2009 EPA 8270 1,4-Naphthoquinone NE LAP PA 12/12/2005 EPA8270 1,4-Phenylenediamine NE LAP PA 12/12/2005 EPA8270 1-Chloronaphthalene NE LAP PA 12/12/2005 EPA 8270 1-Methylnaphthalene NELAP PA 4/17/2009 EPA 8270 1-Naphthylamine (alpha-Naphthylamine) NELAP PA 12/12/2005 EPA 8270 2,2 '-Oxybis(l-chloropropane) (bis(2-Chloro- NELAP PA 1/19/2011

1-methylethyl) ether) EPA8270 2,2'-oxybis(l-Chloropropane) NE LAP PA 12/12/2005 EPA 8270 2,3,4,6-Tetrachlorophenol NE LAP PA 12/12/2005 EPA 8270 2,4,5-Trichlorophenol NE LAP PA 12/12/2005 EPA8270 2,4,6-Trichlorophenol NE LAP PA 12/12/2005 EPA8270 2,4-Dichlorophenol NE LAP PA 12/12/2005 EPA 8270 2,4-Dimethylphenol NE LAP PA 12/12/2005 EPA 8270 2,4-Dinitrophenol NE LAP PA 12/12/2005 EPA 8270 2,4-Dinitrotoluene (2,4-DNT) NELAP PA 12/12/2005 EPA8270 2,6-Dichlorophenol NELAP PA 12/12/2005 EPA8270 2,6-Dinitrotoluene (2,6-DNT) NE LAP PA 12/12/2005 EPA8270 2-Acetylaminotluorene NE LAP PA 12/12/2005 EPA 8270 2-Butoxyethanol NE LAP PA 21712012 EPA8270 2-Chloronaphthalene NELAP PA 12/12/2005 EPA 8270 2-Chlorophenol NE LAP PA 12/12/2005 EPA 8270 2-Methyl-4,6-dinitrophenol ( 4,6-Dinitro-2- NE LAP PA 12/12/2005

methylphenol) EPA 8270 2-Methylnaphthalene NELAP PA 12/12/2005 EPA 8270 2-Methylphenol (o-Cresol) NE LAP PA 12/12/2005 EPA 8270 2-Naphthylamine (beta-Naphthylamine) NE LAP PA 12/12/2005 EPA 8270 2-Nitroaniline NE LAP PA 12/12/2005 EPA8270 2-Nitrophenol NELAP PA 12/12/2005 EPA 8270 2-Picoline (2-Methylpyridine) NE LAP PA 51212006 EPA 8270 3+4-Methylphenol (m+p-Cresol) NE LAP PA 12/12/2005 EPA8270 3,3'-Dichlorobenzidine NE LAP PA 12/12/2005 EPA 8270 3,3'-Dimethylbenzidine NE LAP PA 7/3/2007 EPA 8270 3-Methylcholanthrene NE LAP PA 12/12/2005 EPA8270 3-Nitroaniline NE LAP PA 12/12/2005 EPA 8270 4,4'-Methylenebis(2-chloroaniline) NELAP PA 12/12/2005 EPA 8270 4-Aminobiphenyl NE LAP PA 12/12/2005 EPA 8270 4-Bromophenyl phenyl ether NELAP PA 12/12/2005 EPA8270 4-Chloro-3-methylphenol NE LAP PA 12/12/2005 EPA 8270 4-Chloroaniline NELAP PA 12/12/2005 EPA 8270 4-Chlorophenyl phenyl ether NELAP PA 12/12/2005 EPA 8270 4-Nitroaniline NELAP PA 12/12/2005 EPA 8270 4-Nitrophenol NELAP PA 12/12/2005 EPA 8270. 4-Nitroquinoline-1-oxide NE LAP PA 7/3/2007 EPA 8270 5-Nitro-o-toluidine NE LAP PA 12/12/2005 EPA 8270 6-Methylchrysene NE LAP PA 1/19/2011

~~ The Pennsylvania Department of Environmental Protection Laboratory Accreditation Program is a NELAP recognized

Accreditation Body. Customers are wged to verify the laboratory's current accreditation standing. Page 30 of57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania ,.. DEPARTMENT OF ENVIRONMENTAL

PROTECTION Laboratory Scope of Accreditation

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes

should be used only when associated with a valid certificate of accreditation.

DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TNI02128 (717) 656-2300

PADWIS ID: 36037

Matrix: Non-Potable Water

Method Revision Analyte Accreditation Type Primary Effective Date EPA 8270 7, 12-Dimethylbenz( a)anthracene NE LAP PA 12/12/2005

EPA 8270 Acenaphthene NE LAP PA 12/12/2005

EPA 8270 Acenaphthylene NE LAP PA 12/12/2005

EPA 8270 Acetophenonl;l NE LAP PA 12/12/2005

EPA 8270 Aniline NE LAP PA q11212005

EPA 8270 Anthracene NE LAP PA 12/12/2005

EPA 8270 Aramite NE LAP PA 12/12/2005

EPA 8270 Atrazine NE LAP PA 1122/2007

EPA8270 Benzaldehyde NE LAP PA 4/17/2009

EPA 8270 Benzenethiol NE LAP PA 4/17/2009

EPA 8270 Benzidine NE LAP PA 12/12/2005

EPA 8270 Benzo[ a]anthracene NE LAP PA 12/12/2005

EPA 8270 Benzo[ a ]pyrene NE LAP PA 12/12/2005

EPA 8270 Benzo[b ]fluoranthene NE LAP PA 12/12/2005

EPA 8270 Benzo[ghi]perylene NE LAP PA 12/12/2005

EPA 8270 Benzo[k ]fluoranthene NE LAP PA 12/12/2005

EPA 8270 Benzoic acid NE LAP PA 12/12/2005

EPA8270 Benzyl alcohol NE LAP PA 12/12/2005

EPA8270 Butyl benzyl phthalate (Benzyl butyl NE LAP PA 12/12/2005 phthalate)

EPA8270 Caprolactam NE LAP PA 4/17/2009

EPA 8270 Carbazole NE LAP PA 12/12/2005

EPA 8270 Chlorobenzilate NE LAP PA 12/12/2005

EPA 8270 Chrysene (Benzo[ a ]phenanthrene) NE LAP PA 12/12/2005

EPA 8270 Di-n-butyl phthalate NELAP PA 12/12/2005

EPA 8270 Di-n-octyl phthalate NE LAP PA 12/12/2005

EPA8270 Diallate ( cis or trans) NE LAP PA 12/12/2005

EPA8270 Dibenz[ a,h ]acridine NE LAP PA 4/17/2009

EPA 8270 Dibenz[ aj]acridine NE LAP PA 12/12/2005

EPA 8270 Dibenzo[ a,h ]anthracene NE LAP PA 12/12/2005

EPA 8270 Dibenzofuran NE LAP PA 12/12/2005

EPA 8270 Diethyl phthalate NE LAP PA 12/12/2005

EPA 8270 Dimethoate NE LAP PA 12/12/2005

EPA 8270 Dimethyl phthalate NE LAP PA 12/12/2005

EPA 8270 Dimethylaminoazobenzene ( 4- NELAP PA 5/2/2006 Dimethylaminoazobenzene)

EPA 8270 Dinoseb (2-sec-Butyl-4,6-dinitrophenol, NE LAP PA 12/12/2005 DNBP)

EPA 8270 Diphenylamine NE LAP PA 12/12/2005

EPA 8270 Disulfoton NE LAP PA 12112/2005

EPA 8270 Ethyl methanesulfonate NE LAP PA 12112/2005

EPA8270 Famphur NE LAP PA 12/12/2005

EPA8270 Fluoranthene NE LAP PA 12/12/2005

EPA8270 Fluorene NE LAP PA 12/12/2005 EPA8270 Hexachlorobenzene NE LAP PA 12/12/2005

The Pennsylvania Department of Environmental Protection Laboratory Accreditation Program is a NELAP recognized

Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing. Page 31 of57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania M DEPARTMENT OF ENVIRONMENTAL PROTECTION Laboratory Scope of Accreditation

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes should be used only when associated with a valid certificate of accreditation.

DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TNI02128 (717) 656-2300 P ADWIS ID: 36037

Matrix: Non-Potable Water Method Revision Analyte Accreditation Type Primary Effective Date

EPA 8270 Hexachlorobutadiene (1,3- NELAP PA 12/12/2005 Hexachlorobutadiene)

EPA 8270 Hexachlorocyclopentadiene NE LAP PA 12/12/2005 EPA 8270 Hexachloroethane NE LAP PA 12112/2005 EPA 8270 Hexachloropropene NE LAP PA 12/12/2005 EPA8270 Indene NE LAP PA 4/17/2009 EPA8270 Indeno( 1,2,3-cd)pyrene NELAP PA 12/12/2005 EPA 8270 Isodrin NE LAP PA 12/12/2005 EPA 8270 Isophorone NE LAP PA 12/12/2005 EPA8270 Isosafrole NELAP PA 12/12/2005 EPA 8270 Kepone NELAP PA 12/12/2005 EPA8270 Methapyrilene NE LAP PA 12/12/2005 EPA8270 Methyl methanesulfonate NE LAP PA 12/12/2005 EPA8270 Methyl parathion (Parathion, methyl) NE LAP PA 5/25/2007 EPA8270 N,N-Dimethylacetamide NELAP PA 4/17/2009 EPA8270 N,N-Dimethylformamide NE LAP PA 4/17/2009 EPA 8270 N-Nitrosodi-n-butylamine NE LAP PA 12/12/2005 EPA8270 N-Nitrosodi-n-propylamine NELAP PA 12/12/2005 EPA 8270 N-Nitrosodiethylamine NE LAP PA 12/12/2005 EPA8270 N-Nitrosodimethylamine NE LAP PA 12/12/2005 EPA 8270 N-Nitrosodiphenylamine NELAP PA 12/12/2005 EPA 8270 N-Nitrosomethylethylamine NELAP PA 12/12/2005 EPA 8270 N-Nitrosomorpholine NELAP PA 12/1212005 EPA8270 N-Nitrosopiperidine NELAP PA 12/12/2005 EPA 8270 N-Nitrosopyrrolidine NE LAP PA 12/12/2005 EPA 8270 Naphthalene NE LAP PA 12/1212005 EPA 8270 Nitrobenzene NE LAP PA 12/12/2005 EPA8270 0,0,0-Triethyl phosphorothioate NELAP PA 12/12/2005 EPA 8270 Parathion, ethyl (Ethyl parathion, Parathion) NELAP PA 512512007 EPA 8270 Pentachlorobenzene NELAP PA 12/12/2005 EPA 8270 Pentachloronitrobenzene (PCNB) NE LAP PA 12/12/2005 EPA8270 Pentachlorophenol (PCP) NE LAP PA 12/12/2005 EPA 8270 Phenacetin NE LAP PA 12/12/2005 EPA 8270 Phenanthrene NE LAP PA 12/12/2005 EPA8270 Phenol NELAP PA 12/12/2005 EPA8270 Phorate (Thimet) NELAP PA 12/12/2005 EPA 8270 Phthalic anhydride NELAP PA 1/21/2009 EPA 8270 Pronamide (Kerb) NE LAP PA 12/12/2005 EPA8270 Pyrene NE LAP PA 12/12/2005 EPA 8270 Pyridine NE LAP PA 12/12/2005 EPA8270 Quinoline NE LAP PA '4117/2009 EPA8270 D SOCs by GC/MS NE LAP PA 3/26/2012 EPA 8270 c SOCs by GC/MS NELAP PA 3/26/2012 EPA 8270 Safrole NELAP PA 12/12/2005 EPA8270 Sulfotepp (Tetraethyl dithiopyrophosphate) NE LAP PA 4/1712009 EPA 8270 Tetraethyl lead NE LAP PA 317/2012

~~ The Pennsylvania Department of Environmental Protection Laboratory Accreditation Program is a NELAP recognized

Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing. Page 32 of 57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania ~ DEPARTMENT OF ENVIRONMENTAL

PROTECTION Laboratory Scope of Accreditation

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes

should be used only when associated with a valid certificate of accreditation.

DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TNI02128 . (717) 656-2300

PADWIS ID: 36037

Matrix: Non-Potable Water

Method Revision Analyte Accreditation Type Primary Effective Date EPA 8270 Thionazine (Thionazin, Zinophos) NE LAP PA 12/12/2005

EPA 8270 a,a-Dimethylphenethylamine (Phentennine) NE LAP PA 12/12/2005

EPA 8270 a-Methylstyrene NELAP PA 411712009

EPA 8270 bis(2-Chloroethoxy)methane NELAP PA 12/12/2005

EPA8270 bis(2-Chloroethyl) ether NELAP PA 12/1212005

EPA 8270 bis(2-Chloromethyl) ether NELAP PA 1/2112009

EPA8270 bis(2-Ethylhexyl) phthalate (DEHP) NE LAP PA 1211212005

EPA8270 o-Toluidine (2-Toluidine, 2-Methylaniline) NE LAP PA 12/1212005

EPA8270 p-(Dimethylamino)azobenzene NE LAP PA 411712009 EPA8270 tris-(2,3-Dibromopropyl) phosphate (tris- NE LAP PA 411712009

BP) EPA 8270 SIM 1-Methylnaphthalene NE LAP PA 712512011

EPA8270 SIM 2-Methylnaphthalene NE LAP PA 5/23/2012

EPA8270 SIM Acenaphthene NELAP PA 121412007

EPA8270 SIM Acenaphthylene NE LAP PA 12/4/2007

EPA 8270 SIM Anthracene NELAP PA 121412007 EPA 8270 SIM Benzo[ a ]anthracene NE LAP PA 12/4/2007

EPA8270 SIM Benzo[a)pyrene NE LAP PA 12/4/2007

EPA8270 SIM Benzo[b ]fluoranthene NE LAP PA 12/4/2007

EPA 8270 SIM Benzo[ghi]perylene NE LAP PA 12/4/2007

EPA8270 SIM Benzo[k ]fluoranthene NELAP PA 121412007 EPA8270 SIM Chrysene (Benzo[a]phenanthrene) NE LAP PA 121412007 EPA8270 SIM Dibenzo[ a,h ]anthracene NE LAP PA 12/4/2007

EPA8270 SIM Fluoranthene NE LAP PA 12/4/2007

EPA8270 SIM Fluorene NE LAP PA 12/4/2007

EPA8270 SIM Indeno( 1,2,3-cd)pyrene NE LAP PA 12/4/2007

EPA8270 SIM Naphthalene NE LAP PA 121412007

EPA 8270 SIM Phenanthrene NE LAP PA 12/412007

EPA 8270SIM Pyrene NELAP PA 12/4/2007

EPA 8290 1,2,3,4,6, 7 ,8,9-0ctachlorodibenzo-p-dioxin NELAP PA 6/30/2010 (OCDD)

EPA 8290 1,2 ,3 ,4,6, 7 ,8,9-0ctachlorodibenzofuran NE LAP PA 6/30/2010 (OCDF)

EPA 8290 1,2,3,4,6, 7 ,8-Heptachlorodibenzo-p-dioxin NE LAP PA 6/30/2010 ( 1,2,3,4,6, 7,8-hpcdd)

EPA8290 1,2,3 ,4,6, 7 ,8-Heptachlorodibenzofuran NELAP PA 6/30/2010 ( 1,2,3,4,6,7 ,8-hpcdf)

EPA8290 1,2,3,4,7,8,9-Heptachlorodibenzofuran NE LAP PA 6/30/2010 (1,2,3,4,7 ,8,9-hpcdf)

EPA8290 1,2,3,4,7 ,8-Hexachlorodibenzo-p-dioxin NE LAP PA 6/30/2010 (HxCDD)

EPA 8290 1,2,3 ,4, 7 ,8-Hexachlorodibenzofuran NELAP PA 8/6/2010 (HxCDF)

EPA8290 1,2,3,6,7,8-Hexachlorodibenzo-p-dioxin NE LAP PA 6/30/2010 (HxCDD)

EPA 8290 1,2,3,6, 7 ,8-Hexachlorodibenzofuran NE LAP PA 6/30/2010 (HxCDF)

~~ The Pennsylvania Department of Environmental Protection Laboratory Accreditation Program is a NELAP recognized

Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing.

Page 33 of 57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania M DEPARTMENT OF ENVIRONMENTAL PROTECTION Laboratory Scope of Accreditation

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes should be used only when associated with a valid certificate of accreditation.

DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TNI02128 (711) 656-2300 PADWIS ID: 36037

Matrix: Non-Potable Water Method Revision Analyte Accreditation Type Primary Effective Date

EPA8290 1,2,3, 7,8,9-Hexachlorodibenzo-p-dioxin NELAP PA (HxCDD)

EPA8290 1,2,3, 7 ,8 ,9-Hexachlorodibenzofuran NE LAP PA (HxCDF)

EPA8290 1,2,3, 7,8-Pentachlorodibenzo-p-dioxin NELAP PA (PeCDD)

EPA 8290 1,2,3, 7,8-Pentachlorodibenzofuran (PeCDF) NE LAP PA EPA8290 2,3,4,6, 7,8-Hexachlorodibenzofuran NELAP PA

(HxCDF) EPA 8290 2,3,4, 7 ,8-Pentachlorodibenzofuran (PeCDF) NE LAP PA EPA 8290 2,3, 7,8-Tetrachlorodibenzo-p-dioxin NE LAP PA

(2,3,7,8-TCDD)(Dioxin) EPA 8290 2 ,3, 7 ,8-Tetrachlorodibenzofuran (TCD F) NELAP PA EPA 8290 PCDDs and PCDFs by HRGC-HRMS NELAP PA EPA 8290 A PCDDs and PCDFs by HRGC-HRMS NE LAP PA EPA8290 Total TCDD NELAP PA EPA8290 Total TCDF NE LAP PA EPA 8290 Total heptachlorodibenzo-p-dioxin NE LAP PA

(HpCDD) EPA 8290 Total heptachlorodibenzofuran (HpCDF) NE LAP PA EPA 8290 Total hexachlorodibenzo-p-dioxin (HxCDD) NE LAP PA EPA 8290 Total hexachlorodibenzofuran (HxCDF) NE LAP PA EPA 8290 Total pentachlorodibenzo-p-dioxin (PeCDD) NELAP PA EPA 8290 Total pentachlorodibenzofuran (PeCDF) NE LAP PA EPA8315 2,5-Dimethylbenzaldehyde NELAP PA EPA 8315 Acetaldehyde NE LAP PA EPA 8315 Benzaldehyde NE LAP PA EPA8315 Butanal (Butyraldehyde) NE LAP PA EPA 8315 A Carbonyl compounds by HPLC NE LAP PA EPA8315 Crotonaldehyde NE LAP PA EPA8315 Formaldehyde NE LAP PA EPA 8315 Hexanal (Hexaldehyde) NE LAP PA EPA 8315 Isovaleraldehyde NE LAP PA EPA8315 Pentanal (Valeraldehyde) NE LAP PA EPA 8315 Propanal (Propionaldehyde) NE LAP PA EPA 8315 m-Tolualdehyde (1,3-Tolualdehyde) NE LAP PA EPA8315 o-Tolualdehyde (1,2-Tolualdehyde) NELAP PA EPA 8315 p-Tolualdehyde (1,4-Tolualdehyde) NE LAP PA EPA 8330 1,3,5-Trinitrobenzene (1,3,5-TNB) NELAP PA EPA 8330 1,3-Dinitrobenzene (1,3-DNB) NELAP PA EPA8330 2,4,6-Trinitrotoluene (2,4,6-TNT) NE LAP PA EPA 8330 2,4-Diamino-6-nitrotoluene NELAP PA EPA 8330 2,4-Dinitrotoluene (2,4-DNT) NE LAP PA EPA 8330 2,6-Diamino-4-nitrotoluene NELAP PA EPA8330 2,6-Dinitrotoluene (2,6-DNT) NE LAP PA EPA8330 2-Amino-4,6-dinitrotoluene (2-Am-DNT) NE LAP PA EPA8330 2-Nitrotoluene NE LAP PA

~~ The Pennsylvania Department of Environmental Protection Laboratory Accreditation Program is a NELAP recognized

Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing.

6/30/2010

6/30/2010

6/30/2010

6/30/2010 6/30/2010

8/6/2010 6/30/2010

6/30/2010 3/26/2012 3/4/2015

6/30/2010 6/30/2010 6/30/2010

6/30/2010 6/30/2010 6/30/2010 6/30/2010 6/30/2010

12/12/2005 12/12/2005 12/12/2005

5/2/2006 3/26/2012

12/12/2005 12/12/2005 1/21/2009

12/12/2005 12/12/2005

1/21/2009 5/2/2006

1/24/2007 1124/2007

12/12/2005 12/12/2005 12/12/2005 7129/2015 6/11/2007 7/29/2015 6/11/2007

12/12/2005 12112/2005

Page 34 of57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania ,..., DEPARTMENT OF ENVIRONMENTAL

PROTECTION Laboratory Scope of Accreditation

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes

should be used only when associated with a valid certificate of accreditation. DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TNI02128 (717) 656-2300

PADWIS ID: 36037

Matrix: Non-Potable Water

Method Revision Analyte Accreditation Type Primacy Effective Date EPA 8330 3,5-Dinitroaniline NE LAP PA 7/29/2015 EPA 8330 3-Nitrotoluene NE LAP PA 12/12/2005 EPA8330 4-Amino-2,6-dinitrotoluene ( 4-Am-DNT) NE LAP PA 12/12/2005 EPA8330 4-Nitrotoluene NE LAP PA 12/12/2005 EPA8330 Methyl-2,4,6-trinitrophenylnitramine NE LAP PA 12/12/2005

(Tetryl) EPA 8330 A Nitroaromatics and nitramines by HPLC/UV NE LAP PA 3/26/2012 EPA 8330 B Nitroaromatics and nitramines by HPLC/UV NE LAP PA 7/29/2015 EPA 8330 Nitroaromatics and nitramines by HPLC/UV NE LAP PA 3/26/2012 EPA8330 Nitrobenzene NE LAP PA 6/11/2007 EPA8330 Nitroglycerin NE LAP PA 1/24/2007 EPA8330 Octahydro-1,3,5, 7-tetranitro-1,3,5, 7- NE LAP PA 12/12/2005

tetrazocine (HMX) EPA8330 Pentaerythritol tetranitrate (PETN) NE LAP PA 5/2/2006 EPA 8330 RDX (Hexahydro-l,3,5-trinitro-1,3,5- NE LAP PA 12/12/2005

triazine) EPA9012 Total cyanide NE LAP PA 12/12/2005 EPA 9040 pH NE LAP PA 12/12/2005 EPA9050 Conductivity NE LAP PA 12/12/2005 EPA9050 A Conductivity NELAP PA 1/27/2014 EPA9056 A Anions by IC NE LAP PA 3/19/2015 EPA9056 Bromide NE LAP PA 12/12/2005 EPA 9056 Chloride NE LAP PA 12/12/2005 EPA 9056 Fluoride NE LAP PA 12/12/2005 EPA 9056 Nitrate as N NE LAP PA 12/12/2005 EPA 9056 Nitrite as N NE LAP PA 1/19/2005 EPA 9056 Sulfate NELAP PA 12/12/2005 EPA 9060 Total organic carbon (TOC) NE LAP PA 12/12/2005 EPA9066 Total phenolics NE LAP PA 12/12/2005 FL-PRO Total petroleum hydrocarbons (TPH) NE LAP PA 12/12/2005 MADEPEPH I.I Cl l-C22 Aromatics NE LAP PA 7/15/2013 MADEPEPH I.I Cl9-C36 Aliphatics NE LAP PA 7/15/2013 MADEPEPH I.I C9-Cl8 Aliphatics NE LAP PA 7/15/2013 MADEPVPH I.I C5-C8 Aliphatics NE LAP PA 7/15/2013 MADEPVPH I.I C9-Cl0 Aromatics NE LAP PA 7/29/2015 MADEPVPH 1.1 C9-Cl2 Aliphatics NELAP PA 7/15/2013 NWTPH-Dx Diesel-range organics (DRO) NE LAP PA 12/12/2005 NWTPH-Gx Gasoline-range organics (GRO) NE LAP PA 12/12/2005 OJA 1677 Available cyanide NE LAP PA 10/9/2013 OJA 1677 Free cyanide NE LAP PA 10/9/2013 RSK-175 Acetylene (Ethyne) NE LAP PA 1/20/2012 RSK-175 Carbon dioxide NE LAP PA 11/19/2015 RSK-175 Ethane NE LAP PA 6/29/2010 RSK-175 Ethene NELAP PA 612912010 RSK-175 Isobutane (2-Methylpropane) NE LAP PA 11/19/2015 RSK-175 Methane NE LAP PA 6/29/2010

~~ The Pennsylvania Department of Environmental Protection Laboratory Accreditation Program is a NELAP recognized

Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing. Page 35 of57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania g DEPARTMENT OF ENVIRONMENTAL PROTECTION Laboratory Scope of Accreditation

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes should be used only when ass0ciated with a valid certificate of accreditation.

DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TNI02128 (717) 656-2300 PADWIS ID: 36037

Matrix: Non-Potable Water

Method Revision Analyte Accreditation Type Primary Effective Date RSK-175 Propane NE LAP PA RSK-175 n-Butane NE LAP PA SM2120B Color NELAP PA SM2310B Acidity as CaC03 NELAP PA SM2320B Alkalinity as CaC03 NE LAP PA SM2340C Total hardness as CaC03 NE LAP PA SM2510 B Conductivity NE LAP PA SM2540B Residue, total NE LAP PA SM2540 C Residue, filterable (TDS) NE LAP PA SM2540D Residue, nonfilterable (TSS) NE LAP PA SM2540F Residue, settleable NE LAP PA SM2580B Oxidation-reduction potential NE LAP PA SM3500-CrB 20-22 Chromium VI NELAP PA SM3500-FeB 20/21 Ferrous iron NE LAP PA SM 4500-CN- G Amenable cyanide NELAP PA SM4500-ClF Total residual chlorine NELAP PA SM 4500-Cl- C Chloride NE LAP PA SM4500-F-B Preliminary distillation of fluoride NE LAP PA SM4500-F-C Fluoride NELAP PA SM.4500-H+ B pH NE LAP PA SM 4500-NH3 B Ammonia distillation NE LAP PA SM 4500-NH3 D AmmoniaasN NELAP PA SM4500-0G Oxygen (dissolved) NE LAP PA SM4500-P B Preliminary treatment of phosphate samples NE LAP PA SM4500-P E Orthophosphate as P NELAP PA SM4500-P F Phosphorus, total NE LAP PA SM4500-S D Sulfide NE LAP PA SM4500-S F Sulfide NE LAP PA SM 4500-S03 B Sulfite, S03 NE LAP PA SM 4500-Si02 C 20-22 Silica, as Si02 NE LAP PA SM 4500-Si02 C 20-22 Silica, dissolved NELAP PA SM5210B Biochemical oxygen demand (BOD) NE LAP PA SM5210B Carbonaceous BOD (CBOD) NE LAP PA SM5310C Total organic carbon (TOC) NE LAP PA SM 5540 C Surfactants as MBAS NE LAP PA TXI005 (TNRCC) Total petroleum hydrocarbons (TPH) NE LAP PA TX1006 (TNRCC) Total petroleum hydrocarbons (TPH) NE LAP PA WA-EPH Diesel-range organics (DRO) NE LAP PA WA-VPH Gasoline-range organics (GRO) NE LAP PA WI-DRO Diesel-range organics (DRO) NE LAP PA WI-GRO Gasoline-range organics (GRO) NE LAP PA

The Pennsylvania Deparbnent of Environmental Protection Laboratory Accreditation Program is a NELAP recognized Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing.

6/29/2010 12/22/2011 4/17/2007 4/17/2007 111912005 4/17/2007

12/12/2005 4/17/2007 4/17/2007 4/17/2007 4/17/2007

3/4/2015 5/24/2007 611512009 5/24/2007 1/11/2012 4/17/2007 4/28/2010 1/19/2005 4/17/2007 4/17/2007 4/17/2007 4/17/2007 4/28/2010

12/12/2005 4/28/2010 4/17/2007 4/17/2007 4/17/2007 5/25/2007 5/24/2007

41412005 111912005 5/24/2007 4/17/2007

12/12/2005 12/12/2005 12/12/2005 1211212005 12/12/2005 12/12/2005

Page 36 of 57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania t-1 DEPARTMENT OF ENVIRONMENTAL PROTECTION Laboratory Scope of Accreditation

Attached to Certificate of Accreditation 016-006 expiration date Januacy 31, 2018. This listing of accredited analytes should be used only when associated with a valid certificate of accreditation.

DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TN1 Code: TN102128 ,(717) 656-2300 PADWISID: 36037

Matrix: Solid and Chemical Materials

Method Revision Analyte Accreditation Type Primary Effective Date AK-101 Gasoline-range organics (GRO) NELAP PA 12/12/2005 AK-102 Diesel-range organics (DRO) NE LAP PA 12/12/2005 AK-103 Residual-range organics (RRO) NE LAP PA 3/19/2015 ASTM D3987-85 Shake extraction of solid waste with water NE LAP PA 7/21/2017 EPA 1010 A Ignitahility NE LAP PA 11/19/2015 EPA 1010 lgnitability NE LAP PA 111912005 EPA 1311 Toxicity characteristic leaching.procedure NE LAP PA 12/12/2005

(TCLP) EPA 1312 Synthetic precipitation leaching procedure NE LAP PA 12/12/2005

(SPLP) EPA 1668 2,2',3,3',4,4',5,5',6-Nonachlorobiphenyl (BZ NE LAP PA 12/17/2012

206) EPA 1668 2,2',3,3',4,4',5,5'-0ctachlorobiphenyl (BZ NELAP PA 12/17/2012

194) EPA 1668 2,2',3,3',4,4',5,6'-0ctachlorobiphenyl (BZ NE LAP PA 12/17/2012

196) EPA 1668 2,2',3,3',4,4',5,6,6'-Nonachlorobiphenyl (BZ NE LAP PA 12/17/2012

207) EPA 1668 2,2',3,3',4,4',5,6-0ctachlorobiphenyl (BZ NE LAP PA 12/17/2012

195) EPA 1668 2,2',3,3',4,4',5-Heptachlorobiphenyl (BZ NE LAP PA 12/17/2012

170) EPA 1668 2,2',3,3',4,4',6,6'-0ctachlorobiphenyl (BZ NE LAP PA 12/17/2012

197) EPA 1668 2,2',3,3',4,4',6-Heptachlorobiphenyl (BZ NE LAP PA 12/17/2012

171) EPA 1668 2,2',3,3',4,4'-Hexachlorobiphenyl (BZ 128) NE LAP PA 12/17/2012 EPA 1668 2,2',3,3',4,5',6'-Heptachlorobiphenyl (BZ NELAP PA 12/17/2012

177) EPA 1668 2,2',3,3',4,5',6,6'-0ctachlorobiphenyl (BZ NE LAP PA 12/17/2012

201) EPA 1668 2,2',3,3',4,5',6-Heptachlorobiphenyl (BZ NE LAP PA 12/17/2012

175) EPA 1668 2,2',3,3',4,5'-Hexachlorobiphenyl (BZ 130) NE LAP PA 12/17/2012 EPA 1668 2,2',3,3',4,5,5',6'-0ctachlorobiphenyl (BZ NE LAP PA 12/17/2012

199) EPA 1668 2,2',3,3',4,5,5',6,6'-Nonachlorobiphenyl (BZ NE LAP PA 12/17/2012

208) EPA 1668 2,2',3,3',4,5,5',6-0ctachlorobiphenyl (BZ NE LAP PA 12/17/2012

198) EPA 1668 2,2',3,3',4,5,5'-Heptachlorobiphenyl (BZ NE LAP PA 12/17/2012

172) EPA 1668 2,2',3,3',4,5,6'-Heptachlorobiphenyl (BZ NE LAP PA 12/17/2012

174) EPA 1668 2,2',3,3',4,5,6,6'-0ctachlorobiphenyl (BZ NELAP PA 12/17/2012

200) EPA 1668 2,2',3,3',4,5,6-Heptachlorobiphenyl (BZ NE LAP PA 12/17/2012

173) EPA 1668 2,2',3,3',4,5-Hexachlorobiphenyl (BZ 129) NE LAP PA 12/17/2012

The Pennsylvania Department of Environmental Protection Laboratory Accreditation Program is a NELAP recognized Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing.

Page 37 of57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania u· DEPARTMENT OF ENVIRONMENTAL PROTECTION Laboratory Scope of Accreditation

:..J9•''"""""'"

,-···~· ., I : ;,

\_, . ./ ...... ' .. , ... _ ..... -:·,''

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes should be used only when associated with a valid certificate of accreditation.

DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TNI02128 (717) 656-2300 PADWIS ID: 36037

Matrix: Solid and Chemical Materials

Method Revision Analyte Accreditation Type Primacy Effective Date EPA 1668 2,2',3,3',4,6'-Hexachlorobiphenyl (BZ 132) NE LAP PA 12/17/2012 EPA 1668 2,2',3,3',4,6,6'-Heptachlorobiphenyl (BZ NE LAP PA 12/17/2012

176) EPA 1668 2,2',3,3',4,6-Hexachlorobiphenyl (BZ 131) NE LAP PA 12/17/2012 EPA 1668 2,2',3,3',4-Pentachlorobiphenyl (BZ 82) NE LAP PA 12/17/2012 EPA 1668 2,2',3,3',5,5',6,6'-0ctachlorobiphenyl (BZ NE LAP PA 12/17/2012

202) EPA 1668 2,2',3,3',5,5',6-Heptachlorobiphenyl (BZ NE LAP PA 12/17/2012

178) EPA 1668 2,2',3,3',5,5'-Hexachlorobiphenyl (BZ 133) NE LAP PA 12/17/2012 EPA 1668 2,2',3,3',5,6'-Hexachlorobiphenyl (BZ 135) NE LAP PA 12/17/2012 EPA 1668 2,2',3,3',5,6,6'-Heptachlorobiphenyl (BZ NELAP PA 12/17/2012

179) EPA 1668 2,2',3,3',5,6-Hexachlorobiphenyl (BZ 134) NE LAP PA 12/17/2012 EPA 1668 2,2',3,3',5-Pentachlorobiphenyl (BZ 83) NE LAP PA 12/17/2012 EPA 1668 2,2',3,3',6,6'-Hexachlorobiphenyl (BZ 136) NE LAP PA 12/17/2012 EPA 1668 2,2',3,3',6-Pentachlorobiphenyl (BZ 84) NE LAP PA 12/17/2012 EPA 1668 2,2',3,3'-Tetrachlorobiphenyl (BZ 40) NE LAP PA 12/17/2012 EPA 1668 2,2',3,4',5',6-Hexachlorobiphenyl (BZ 149) NE LAP PA 12/17/2012 EPA 1668 2,2',3,4',5'-Pentachlorobiphenyl (BZ 97) NE LAP PA 12/17/2012 EPA 1668 2,2',3,4',5,5',6-Heptachlorobiphenyl (BZ NELAP PA 12/17/2012

187) EPA 1668 2,2',3,4',5,5'-Hexachlorobiphenyl (BZ 146) NELAP PA 12/17/2012 EPA 1668 2,2',3,4',5,6'-Hexachlorobiphenyl (BZ 148) NELAP PA 12117/2012 EPA 1668 2,2',3,4',5,6,6'-Heptachlorobiphenyl (BZ NE LAP PA 12/17/2012

188) EPA 1668 2,2',3,4',5,6-Hexachlorobiphenyl (BZ 147) NELAP PA 12/17/2012 EPA 1668 2,2',3,4',5-Pentachlorobiphenyl (BZ 90) NE LAP PA 12/17/2012 EPA 1668 2,2',3,4',6'-Pentachlorobiphenyl (BZ 98) NE LAP PA 12/17/2012 EPA 1668 2,2',3,4',6,6'-Hexachlorobiphenyl (BZ 150) NE LAP PA 12/17/2012 EPA 1668 2,2',3,4',6-Pentachlorobiphenyl (BZ 91) NE LAP PA 12117/2012 EPA 1668 2,2',3,4'-Tetrachlorobiphenyl (BZ 42) NELAP PA 12117/2012 EPA 1668 2,2',3,4,4',5',6-Heptachlorobiphenyl (BZ NE LAP PA 12/17/2012

183) EPA 1668 2,2',3,4,4',5'-Hexachlorobiphenyl (BZ 138) NELAP PA 12/17/2012 EPA 1668 2,2',3,4,4',5,5',6-0ctachlorobiphenyl (BZ NE LAP PA 12/17/2012

203) EPA 1668 2,2',3,4,4',5,5'-Heptachlorobiphenyl (BZ NE LAP PA 12117/2012

180) EPA 1668 2,2',3,4,4',5,6'-Heptachlorobiphenyl (BZ NE LAP PA 12/17/2012

182) EPA 1668 2,2',3,4,4',5,6,6'-0ctachlorobiphenyl (BZ NE LAP PA 12/17/2012

204) EPA 1668 2,2' ,3 ,4,4' ,5 ,6-Heptachlorobiphenyl (BZ NELAP PA 12/1712012

181) EPA 1668 2,2',3,4,4',5-Hexachlorobiphenyl (BZ 137) NE LAP PA 12/17/2012 EPA 1668 2,2',3,4,4',6'-Hexachlorobiphenyl (BZ 140) NE LAP PA 12/17/2012

The Pennsylvania Department of Environmental Protection Laboratory Accreditation Program is a NELAP recognized Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing.

Page 38 of57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania t-1 DEPARTMENT OF ENVIRONMENTAL PROTECTION Laboratory Scope of Accreditation

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes

should be used only when associated with a valid certificate of accreditation. DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TNI02128 (717) 656-2300

PADWIS ID: 36037

Matrix: Solid and Chemical Materials

Method Revision Analyte Accreditation Type Primary Effective Date EPA 1668 2,2',3,4,4',6,6'-Heptachlorobiphenyl (BZ NE LAP PA

184) EPA 1668 2,2',3,4,4',6-Hexachlorobiphenyl (BZ 139) NE LAP PA EPA 1668 2,2',3,4,4'-Pentachlorobiphenyl (BZ 85) NE LAP PA EPA 1668 2,2',3,4,5',6-Hexachlorobiphenyl (BZ 144) NE LAP PA EPA 1668 2,2',3,4,5'-Pentachlorobiphenyl (BZ 87) NELAP PA EPA 1668 2,2',3,4,5,5',6-Heptachlorobiphenyl (BZ NE LAP PA

185) EPA 1668 2,2',3,4,5,5'-Hexachlorobiphenyl (BZ 141) NE LAP PA EPA 1668 2,2',3,4,5,6'-Hexachlorobiphenyl (BZ 143) NE LAP PA EPA 1668 2,2',3,4,5,6,6'-Heptachlorobiphenyl (BZ NE LAP PA

186) EPA 1668 2,2',3,4,5,6-Hexachlorobiphenyl (BZ 142) NE LAP PA EPA 1668 2,2',3,4,5-Pentachlorobiphenyl (BZ 86) NE LAP PA EPA 1668 2,2',3,4,6'-Pentachlorobiphenyl (BZ 89) NE LAP PA EPA 1668 2,2',3,4,6,6'-Hexachlorobiphenyl (BZ 145) NE LAP PA EPA 1668 2,2',3,4,6-Pentachlorobiphenyl (BZ 88) NELAP PA EPA 1668 2,2',3,4-Tetrachlorobiphenyl (BZ 41) NE LAP PA EPA 1668 2,2',3,5',6-Pentachlorobiphenyl (BZ 95) NE LAP PA EPA 1668 2,2',3,5'-Tetrachlorobiphenyl (BZ 44) NE LAP PA EPA 1668 2,2',3,5,5',6-Hexachlorobiphenyl (BZ 151) NE LAP PA EPA 1668 2,2',3,5,5'-Pentachlorobiphenyl (BZ 92) NE LAP PA EPA 1668 2,2',3,5,6'-Pentachlorobiphenyl (BZ 94) NE LAP PA EPA 1668 2,2',3,5,6,6'-Hexachlorobiphenyl (BZ 152) NE LAP PA EPA 1668 2,2',3,5,6-Pentachlorobiphenyl (BZ 93) NELAP PA EPA 1668 2,2',3,5-Tetrachlorobiphenyl (BZ 43) NE LAP PA EPA 1668 2,2',3,6'-Tetrachlorobiphenyl (BZ 46) NE LAP PA EPA 1668 2,2',3,6,6'-Pentachlorobiphenyl (BZ 96) NE LAP PA EPA 1668 2,2',3,6-Tetrachlorobiphenyl (BZ 45) NE LAP PA EPA 1668 2,2',3-Trichlorobiphenyl (BZ 16) NE LAP PA EPA 1668 2,2',4,4',5,5'-Hexachlorobiphenyl (BZ 153) NE LAP PA EPA 1668 2,2',4,4',5,6'-Hexachlorobiphenyl (BZ 154) NELAP PA EPA 1668 2,2',4,4',5-Pentachlorobiphenyl (BZ 99) NELAP PA EPA 1668 2,2',4,4',6,6'-Hexachlorobiphenyl (BZ 155) NELAP PA EPA 1668 2,2',4,4',6-Pentachlorobiphenyl (BZ 100) NELAP. PA EPA 1668 2,2',4,4'-Tetrachlorobiphenyl (BZ 47) NELAP PA EPA 1668 2,2',4,5',6-Pentachlorobiphenyl (BZ 103) NELAP PA EPA 1668 2,2',4,5'-Tetrachlorobiphenyl (BZ 49) NE LAP PA EPA 1668 2,2',4,5,5'-Pentachlorobiphenyl (BZ 101) NE LAP PA EPA 1668 2,2',4,5,6'-Pentachlorobiphenyl (BZ 102) NE LAP PA EPA 1668 2,2',4,5-Tetrachlorobiphenyl (BZ 48) NE LAP PA EPA 1668 2,2',4,6'-Tetrachlorobiphenyl (BZ 51) NELAP PA EPA 1668 2,2',4,6,6'-Pentachlorobiphenyl (BZ 104) NE LAP PA EPA 1668 2,2',4,6-Tetrachlorobiphenyl (BZ 50) NE LAP PA EPA 1668 2,2',4-Trichlorobiphenyl (BZ I 7) NELAP PA EPA 1668 2,2',5,5'-Tetrachlorobiphenyl (BZ 52) NE LAP PA

~~ The Pennsylvania Department ofEnviromnental Protection Laboratory Accreditation Program is a NELAP recognized

Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing.

12/17/2012

12/17/2012 12/1712012 12/17/2012 12/17/2012 12/17/2012

12/17/2012 12/17/2012 12/17/2012

12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12117/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12117/2012 12/17/2012 12/1712012 12/1712012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12117/2012 12117/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012

Page 39 of57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania t-1 DEPARTMENT OF ENVIRONMENTAL PROTECTION Laboratory Scope of Accreditation

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes should be used only when associated with a valid certificate of accreditation.

DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TNI02128 (717) 656-2300 PADWIS ID: 36037

Matrix: Solid and Chemical Materials

Method Revision Analyte Accreditation Type Primary Effective Date EPA 1668 2,2',5,6'-Tetrachlorobiphenyl (BZ 53) NELAP PA EPA 1668 2,2',5-Trich\orobiphenyl (BZ 18) NELAP PA EPA 1668 2,2',6,6'-Tetrachlorobiphenyl (BZ 54) NE LAP PA EPA 1668 2,2',6-Trichlorobiphenyl (BZ 19) NE LAP PA EPA 1668 2,2'-Dichlorobiphenyl (BZ 4) NE LAP PA EPA 1668 2,3',4',5',6-Pentachlorobiphenyl (BZ 125) NE LAP PA EPA 1668 2,3',4',5'-Tetrachlorobiphenyl (BZ 76) NE LAP PA EPA 1668 2,3',4',5,5'-Pentachlorobiphenyl (BZ 124) NE LAP PA EPA 1668 2,3',4',5-Tetrachlorobiphenyl (BZ 70) NELAP PA EPA 1668 2,3',4',6-Tetrach\orobiphenyl (BZ 71) NELAP PA EPA 1668 2,3',4'-Trichlorobiphenyl (BZ 33) NELAP PA EPA 1668 2,3',4,4',5',6-Hexachlorobiphenyl (BZ 168) NELAP PA EPA 1668 2,3',4,4',5'-Pentachlorobiphenyl (BZ 123) NELAP PA EPA 1668 2,3',4,4',5,5'-Hexachlorobiphenyl (BZ 167) NE LAP PA EPA 1668 2,3',4,4',5-Pentachlorobiphenyl (BZ 118) NELAP PA EPA 1668 2,3',4,4',6-Pentachlorobiphenyl (BZ 119) NELAP PA EPA 1668 2,3',4,4'-Tetrachlorobiphenyl (BZ 66) NELAP PA EPA 1668 2,3',4,5',6-Pentachlorobiphenyl (BZ 121) NE LAP PA EPA 1668 2,3',4,5'-Tetrachlorobiphenyl (BZ 68) NELAP PA EPA 1668 2,3',4,5,5'-Pentach\orobiphenyl (BZ 120) NE LAP PA EPA 1668 2,3',4,5-Tetrachlorobiphenyl (BZ 67) NE LAP PA EPA 1668 2,3',4,6-Tetrachlorobiphenyl (BZ 69) NELAP PA EPA 1668 2,3',4-Trichlorobiphenyl (BZ 25) NELAP PA EPA 1668 2,3',5',6-Tetrachlorobiphenyl (BZ 73) NE LAP PA EPA 1668 2,3',5'-Trichlorobiphenyl (BZ 34) NE LAP PA EPA 1668 2,3',5,5'-Tetrachlorobiphenyl (BZ 72) NE LAP PA EPA 1668 2,3 ',5-Trichlorobiphenyl (BZ 26) NE LAP PA EPA 1668 2,3',6-Trichlorobiphenyl (BZ 27) NE LAP PA EPA 1668 2,3'-Dichlorobiphenyl (BZ 6) NE LAP PA EPA 1668 2,3,3',4',5',6-Hexachlorobiphenyl (BZ 164) NELAP PA EPA 1668 2,3,3',4',5'-Pentachlorobiphenyl (BZ 122) NELAP PA EPA 1668 2,3,3',4',5,5',6-Heptachlorobiphenyl (BZ NELAP PA

193) EPA 1668 2,3,3',4',5,5'-Hexachlorobiphenyl (BZ 162) NELAP PA EPA 1668 2,3,3',4',5,6-Hexachlorobiphenyl (BZ 163) NELAP PA EPA 1668 2,3,3',4',5-Pentachlorobiphenyl (BZ 107) NE LAP PA EPA 1668 2,3,3',4',6-Pentach\orobiphenyl (BZ llO) NELAP PA EPA 1668 2,3,3',4'-Tetrachlorobiphenyl (BZ 56) NELAP PA EPA 1668 2,3,3',4,4',5',6-Heptachlorobiphenyl (BZ NELAP PA

191) EPA 1668 2,3,3',4,4',5'-Hexachlorobiphenyl (BZ 157) NE LAP PA EPA 1668 2,3,3',4,4',5,5',6-0ctachlorobiphenyl (BZ NELAP PA

205) EPA 1668 2,3,3',4,4',5,5'-Heptachlorobiphenyl (BZ NE LAP PA

189)

The Pennsylvania Department of Environmental Protection Laboratory Accreditation Program is a NELAP recognized Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing.

12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012

12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012

12/17/2012 12117/2012

12/17/2012

Page 40 of57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania · lit DEPARTMENT OF ENVIRONMENTAL PROTECTION Laboratory Scope of Accreditation

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes

should be used only when associated with a valid certificate of accreditation.

DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TN102128 (717) 656-2300

PADWIS ID: 36037

Matrix: Solid and Chemical Materials

Method Revision Analyte Accreditation Type Primmy Effective Date EPA 1668 2,3,3',4,4',5,6-Heptachlorobiphenyl (BZ NE LAP PA

190) EPA 1668 2,3,3',4,4',5-Hexachlorobiphenyl (BZ 156) NE LAP PA EPA 1668 2,3,3';4,4',6-Hexachlorobiphenyl (BZ 158) NE LAP PA EPA 1668 2,3,3',4,4'-Pentachlorobiphenyl (BZ I 05) NE LAP PA EPA 1668 2,3,3',4,5',6-Hexachlorobiphenyl (BZ 161) NELAP PA EPA 1668 2,3,3',4,5'-Pentachlorobiphenyl (BZ 108) NE LAP PA EPA 1668 2,3,3',4,5,5',6-Heptachlorobiphenyl (BZ NE LAP PA

192) EPA 1668 2,3,3',4,5,5'-Hexachlorobiphenyl (BZ 159) NE LAP PA EPA 1668 2,3,3',4,5,6-Hexachlorobiphenyl (BZ 160) NE LAP PA EPA 166.8 2,3,3',4,5-Pentachlorobiphenyl (BZ 106) NE LAP PA EPA 1668 2,3,3',4,6-Pentachlorobiphenyl (BZ 109) NE LAP PA EPA 1668 2,3,3',4-Tetrachlorobiphenyl (BZ 55) NE LAP PA EPA 1668 2,3,3',5',6-Pentachlorobiphenyl (BZ 113) NE LAP PA EPA 1668 2,3,3',5'-Tetrachlorobiphenyl (BZ 58) NE LAP PA EPA 1668 2,3,3',5,5',6-Hexachlorobiphenyl (BZ 165) NE LAP PA EPA 1668 2,3,3',5,5'-Pentachlorobiphenyl (BZ 111) NE LAP PA EPA 1668 2,3,3',5,6-Pentachlorobiphenyl (BZ 112) NE LAP PA EPA 1668 2,3,3',5-Tetrachlorobiphenyl (BZ 57) NE LAP PA EPA 1668 2,3,3',6-Tetrachlorobiphenyl (BZ 59) NE LAP PA EPA 1668 2,3,3'-Trichlorobiphenyl (BZ 20) NE LAP PA EPA 1668 2,3,4',5,6-Pentachlorobiphenyl (BZ 117) NE LAP PA EPA 1668 2,3,4',5-Tetrachlorobiphenyl (BZ 63) NE LAP PA EPA 1668 2,3,4',6-Tetrachlorobiphenyl (BZ 64) NE LAP PA EPA 1668 2,3,4'-Trichlorobiphenyl (BZ 22) NE LAP PA EPA 1668 2,3,4,4',5,6-Hexachlorobiphenyl (BZ 166) NE LAP PA EPA 1668 2,3,4,4',5-Pentachlorobiphenyl (BZ 114) NE LAP PA EPA 1668 2,3,4,4',6-Pentachlorobiphenyl (BZ 115) NE LAP PA EPA 1668 2,3,4,4'-Tetrachlorobiphenyl (BZ 60) NE LAP PA EPA 1668 2,3,4,5,6-Pentachlorobiphenyl (BZ 116) NELAP PA EPA 1668 2,3,4,5-Tetrachlorobiphenyl (BZ 61) NE LAP PA EPA 1668 2,3,4,6-Tetrachlorobiphenyl (BZ 62) NE LAP PA EPA 1668 2,3,4-Trichlorobiphenyl (BZ 21) NE LAP PA EPA 1668 2,3,5,6-Tetrachlorobiphenyl (BZ 65) NE LAP PA EPA 1668 2,3,5-Trichlorobiphenyl (BZ 23) NE LAP PA EPA 1668 2,3,6-Trichlorobiphenyl (BZ 24) NE LAP PA EPA 1668 2,3-Dichlorobiphenyl (BZ 5) NE LAP PA EPA 1668 2,4',5-Trichlorobiphenyl (BZ 31) NE LAP PA EPA 1668 2,4',6-Trichlorobiphenyl (BZ 32) NELAP PA EPA 1668 2,4'-Dichlorobiphenyl (BZ 8) NE LAP PA EPA 1668 2,4,4',5-Tetrachlorobiphenyl (BZ 74) NE LAP PA EPA 1668 2,4,4',6-Tetrachlorobiphenyl (BZ 75) NE LAP PA EPA 1668 2,4,4'-Trichlorobiphenyl (BZ 28) NE LAP PA EPA 1668 2,4,5-Trichlorobiphenyl (BZ 29) NE LAP PA EPA 1668 2,4,6-Trichlorobiphenyl (BZ 30) NE LAP PA

~~ The Pennsylvania Department of Environmental Protection Laboratory Accreditation Program is a NELAP recognized

Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing.

12117/2012

12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012

12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12117/2012 12/17/2012 12/17/2012 12/17/2012 12117/2012 12/17/2012 12117/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012 12117/2012 12/17/2012 12/17/2012 12/17/2012 12/17/2012

Page41 of57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania g DEPARTMENT OF ENVIRONMENTAL PROTECTION Laboratory Scope of Accreditation

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes should be used only when associated with a valid certificate of accreditation.

DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TN102128 (717) 656-2300 PADWIS ID: 36037

Matrix: Solid and Chemical Materials

Method Revision Analyte Accreditation Type Primary Effective Date EPA 1668 2,4-Dich\orobiphenyl (BZ 7) NELAP PA 12/17/2012 EPA 1668 2,5-Dichlorobiphenyl (BZ 9) NELAP PA 12/17/2012 EPA 1668 2,6-Dichlorobiphenyl (BZ 10) NELAP PA 12/17/2012 EPA 1668 2-Chlorobiphenyl (BZ 1) NELAP PA 12/17/2012 EPA 1668 3,3',4,4',5,5'-Hexachlorobiphenyl (BZ 169) NELAP PA 12/17/2012 EPA 1668 3,3',4,4',5-Pentachlorobiphenyl (BZ 126) NE LAP PA 12/17/2012 EPA 1668 3,3',4,4'-Tetrachlorobiphenyl (BZ 77) NE LAP PA 12/17/2012 EPA 1668 3,3',4,5'-Tetrachlorobiphenyl (BZ 79) NE LAP PA 12/17/2012 EPA 1668 3,3',4,5,5'-Pentachlorobiphenyl (BZ 127) NELAP PA 12/17/2012 EPA 1668 3,3',4,5-Tetrachlorobiphenyl (BZ 78) NELAP PA 12/17/2012 EPA 1668 3,3',4-Trichlorobiphenyl (BZ 35) NELAP PA 12/17/2012 EPA 1668 3,3',5,5'-Tetrachlorobiphenyl (BZ 80) NE LAP PA 12/17/2012 EPA 1668 3,3',5-Trichlorobiphenyl (BZ 36) NE LAP PA 12/17/2012 EPA 1668 3,3'-Dichlorobiphenyl (BZ 11) NELAP PA 12/17/2012 EPA 1668 3,4',5-Trichlorobiphenyl (BZ 39) NE LAP PA 12/17/2012 EPA 1668 3,4'-Dichlorobiphenyl (BZ 13) NELAP PA 12/17/2012 EPA 1668 3,4,4',5-Tetrachlorobiphenyl (BZ 81) NE LAP PA 12117/2012 EPA 1668 3,4,4'-Trich\orobiphenyl (BZ 37) NELAP PA 12/17/2012 EPA 1668 3,4,5-Trichlorobiphenyl (BZ 38) NELAP PA 12/17/2012 EPA 1668 3,4-Dichlorobiphenyl (BZ 12) NELAP PA 12/17/2012 EPA 1668 3,5-Dichlorobiphenyl (BZ 14) NELAP PA 12/17/2012 EPA 1668 3-Chlorobiphenyl (BZ 2) NELAP PA 12/17/2012 EPA 1668 4,4'-Dichlorobiphenyl (BZ 15) NELAP PA 12/17/2012 EPA 1668 4-Chlorobiphenyl (BZ 3) NE LAP PA 12/17/2012 EPA 1668 Decach\orobiphenyl NE LAP PA 12/17/2012 EPA 1668 c PCBs as congeners by HRGCIHRMS NELAP PA 3/4/2015 EPA 1668 A PCBs as congeners by HRGCIHRMS NELAP PA 3/4/2015 EPA 300.0 2.1 Bromide NELAP PA 3/9/2016 EPA 300.0 2.1 Chloride NELAP PA 10/30/2014 EPA 300.0 2.1 Fluoride NE LAP PA 10/16/2012 EPA 300.0 2.1 NitrateasN NE LAP PA 10/16/2012 EPA 300.0 2.1 Nitrite as N NELAP PA 10/16/2012 EPA 300.0 2.1 Sulfate NELAP PA 10/16/2012 EPA3050 B Acid digestion of solids NELAP PA 4/4/2005 EPA3060 A Alkaline digestion ofCr(VI) NE LAP PA 4/4/2005 EPA350.3 AmmoniaasN NE LAP PA 12/8/2014 EPA3510 c Separatory funnel liquid-liquid extraction NE LAP PA 4/4/2005 EPA3540 c Soxhlet extraction NE LAP PA 4/4/2005 EPA3546 Microwave extraction NELAP PA 9/25/2009 EPA3550 Ultrasonic extraction NE LAP PA 41412005 EPA3550 c Ultrasonic extraction NE LAP PA 3/4/2015 EPA3620 B Florisi\ cleanup NE LAP PA 4/4/2005 EPA3630 c Silica gel cleanup NE LAP PA 4/4/2005 EPA 3640 A Gel permeation cleanup (GPC) NELAP PA 4/4/2005 EPA365.l Phosphorus, total NELAP PA 11/19/2015

~~ The Pennsylvania Department of Environmental Protection Laboratory Accreditation Program is a NELAP recognized

Accreditation Body. Customers are lll'ged to verify the laboratory's current accreditation standing. Page 42 of 57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania t-1 DEPARTMENT OF ENVIRONMENTAL PROTECTION Laboratory Scope of Accreditation

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes should be used only when associated with a valid certificate of accreditation.

DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TNI02128 (717) 656-2300 PADWIS ID: 36037

Matrix: Solid and Chemical Materials

Method Revision Analyte Accreditation Type Primary Effective Date EPA3660 B Sulfur cleanup NE LAP PA 4/4/2005 EPA3665 A Sulfuric acid/permanganate clean-up NELAP PA 41412005 EPA5030 Bulk purge-and-trap (methanol) NE LAP PA 12/4/2007 EPA5035 Closed-system purge-and-trap (bisulfate NE LAP PA 12/12/2005

option) EPA5035 Closed-system purge-and-trap (methanol NE LAP PA 41412005

option) EPA5035 Closed-system purge-and-trap (unpreserved) NELAP PA 41412005 EPA 537 Modified Perfluorobutanesulfonic acid (PFBS) NE LAP PA 5/24/2017 EPA 537 Modified Perfluorodecanoic acid (PFDA) NE LAP PA 5/24/2017 EPA 537 Modified Perfluorododecanoic acid (PFDoA) NE LAP PA 5/24/2017 EPA 537 Modified Perfluoroheptanoic acid (PFHpA) NE LAP PA 5/24/2017 EPA 537 Modified Perfluorohexanesulfonic acid (PFHxS) NE LAP PA 5/24/2017 EPA 537 Modified Perfluorohexanoic acid (PFHxA) NE LAP PA 5/2412017 EPA 537 Modified Perfluorononanoic acid (PFNA) NE LAP PA 5/24/2017 EPA 537 Modified Perfluorooctanesulfonic acid (PFOS) NE LAP PA 512412017 EPA 537 Modified Perfluorooctanoic acid (PFOA) NELAP PA 512412017 EPA 537 Modified Perfluorotetradecanoic acid (PFTA) NELAP PA 5/24/2017 EPA 537 Modified Perfluorotridecanoic acid (PFTrDA) NELAP PA 5/24/2017 EPA 537 Modified Perfluoroundecanoic acid (PFUnA) NE LAP PA 5/24/2017 EPA 6010 Aluminum NE LAP PA 111912005 EPA 6010 J\ntimony NE LAP PA 111912005 EPA 6010 Arsenic NE LAP PA 111912005 EPA 6010 Barium NE LAP PA 1119/2005 EPA 6010 Beryllium NE LAP PA 111912005 EPA 6010 Boron NELAP PA 111912005 EPA6010 Cadmium NELAP PA 1/19/2005 EPA6010 Calcium NE LAP PA 111912005 EPA 6010 Chromium NE LAP PA 111912005 EPA6010 Cobalt NE LAP PA 1/19/2005 EPA 6010 Copper NE LAP PA 1/19/2005 EPA 6010 Iron NELAP PA 1/19/2005 EPA 6010 Lead NE LAP PA 1/19/2005 EPA 6010 Lithium NELAP PA 1/20/2012 EPA 6010 Magnesium NELAP PA 111912005 EPA6010 Manganese NE LAP PA 1119/2005 EPA6010 B Metals by ICP/AES NE LAP PA 3126/2012 EPA6010 c Metals by ICP/AES NE LAP PA 3/26/2012 EPA 6010 Molybdenum NE LAP PA 111912005 EPA 6010 Nickel NELAP PA 1/19/2005 EPA 6010 Potassium NE LAP PA 1/19/2005 EPA6010 Selenium NE LAP PA 1/19/2005 EPA 6010 Silica, as Si02 NE LAP PA 1/20/2012 EPA 6010 Silver NELAP PA 1/19/2005 EPA6010 Sodium NELAP PA 1/19/2005 EPA6010 Strontium NE LAP PA 111912005

~~ The Pennsylvania Department of Environmental Protection Laboratory Accreditation Program is a NELAP recognized

Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing. Page 43 of57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania M DEPARTMENT OF ENVIRONMENTAL PROTECTION Laboratory Scope of Accreditation

Attachedto Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes should be used only when associated with a valid certificate of accreditation.

DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TNI02128 (717) 656-2300 PADWIS ID: 36037

Matrix: Solid and Chemical Materials

Method Revision Analyte Accreditation Type Primary Effective Date EPA6010 Sulfur NE LAP PA 12/19/2011 EPA 6010 Tellurium NELAP PA 2/4/2016 EPA 6010 Thallium NELAP PA 1/19/2005 EPA 6010 Thorium NE LAP PA 11/19/2015 EPA 6010 Tin NE LAP PA 1/19/2005 EPA6010 Titanium NE LAP PA 1/19/2005 EPA 6010 Tungsten NE LAP PA 11/19/2015 EPA6010 Vanadium NE LAP PA 1/19/2005 EPA 6010 Zinc NE LAP PA 1/19/2005 EPA 6010 Zirconium NE LAP PA 7/29/2015 EPA 6020 Aluminum NE LAP PA 4/29/2010 EPA 6020 Antimony NELAP PA 1/19/2005 EPA 6020 Arsenic NELAP PA 1/19/2005 EPA 6020 Barium NELAP PA 1/20/2012 EPA 6020 Beryllium NE LAP PA 1/19/2005 EPA6020 Boron NE LAP PA 4/29/2010 EPA6020 Cadmium NE LAP PA 1/19/2005 EPA6020 Calcium NELAP PA 4/29/2010 EPA6020 Chromium NELAP PA 1/19/2005 EPA6020 Cobalt NELAP PA 4/29/2010 EPA6020 Copper NE LAP PA 1/19/2005 EPA6020 Iron NE LAP PA 4/29/2010 EPA6020 Lead NE LAP PA 1/19/2005 EPA6020 Magnesium NELAP PA 4/29/2010 EPA 6020 Manganese NELAP PA 4/29/2010 EPA6020 A Metals by ICP/MS NE LAP PA 3/26/2012 EPA6020 Molybdenum NE LAP PA 7/25/2011 EPA6020 Nickel NE LAP PA 4/4/2005 EPA 6020 Potassium NE LAP PA 4/29/2010 EPA6020 Selenium NE LAP PA 41412005 EPA6020 Silver NELAP PA 2/23/2010 EPA6020 Sodium NE LAP PA 4/29/2010 EPA6020 Strontium NE LAP PA 4/29/2010 EPA6020 Thallium NE LAP PA 1/19/2005 EPA6020 Tin NE LAP PA 4/29/2010 EPA6020 Titanium NELAP PA 4/29/2010 EPA6020 Uranium, total NE LAP PA 11/19/2015 EPA 6020 Vanadium NE LAP PA 117/2010 EPA 6020 Zinc NE LAP PA 2/1/2011 EPA680 Decachlorobiphenyl NE LAP PA 1/19/2016 EPA680 Dichlorobiphenyls NE LAP PA 1/19/2016 EPA 680 Heptachlorobiphenyls NE LAP PA 1/19/2016 EPA680 Hexachlorbiphenyls NE LAP PA 1/19/2016 EPA680 Monochlorobiphenyls NE LAP PA 1/19/2016 EPA680 Nonachlorobiphenyls NE LAP PA 1/19/2016

~~ The Pennsylvania Department of Environmental Protection Laboratory Accreditation Program is a NELAP recognized

Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing. Page 44 of57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania gjif DEPARTMENT OF ENVIRONMENTAL PROTECTION Laboratory Scope of Accreditation

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes should be used only when associated with a valid certificate of accreditation.

DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TN102128 (717) 656-2300 PADWIS ID: 36037

Matrix: Solid and Chemical Materials

Method Revision Analyte Accreditation Type Primary Effective Date EPA680 Octachlorobiphenyls NE LAP PA EPA680 Pentachlorobiphenyls NELAP PA EPA680 Tetrachlorobiphenyls NELAP PA EPA 680 Trichlorobiphenyls NELAP PA EPA 6850 Perchlorate NE LAP PA EPA 7.3.3.2 Reactive cyanide NE LAP PA EPA 7.3.4.2 Reactive sulfide NE LAP PA EPA 7196 Chromium VI NE LAP PA EPA 7199 Chromium VI NE LAP PA EPA 7471 Mercury NE LAP PA EPA8015 Diesel-range organics (DRO) NE LAP PA EPA8015 Ethanol NE LAP PA EPA8015 Ethylene glycol NELAP PA EPA8015 Gasoline-range organics (GRO) NE LAP PA EPA 8015 Isopropyl alcohol (2-Propanol) NE LAP PA EPA8015 Methanol NE LAP PA EPA8015 D Nonhalogenated organics by GC/FID NE LAP PA EPA 8015 c Nonhalogenated organics by GC/FID NE LAP PA EPA8015 B Nonha\ogenated organics by.GC/FID NE LAP PA EPA8021 Benzene NELAP PA EPA 8021 Ethylbenzene NELAP PA EPA 8021 Isopropylbenzene (Cumene) NE LAP PA EPA8021 Methyl tert-butyl ether (MTBE) NE LAP PA EPA 8021 Naphthalene NE LAP PA EPA8021 Toluene NE LAP PA EPA 8021 B voes by GCIPID/ELCD NELAP PA EPA 8021 Xylenes, total NE LAP PA EPA8021 m-Xylene NE LAP PA EPA8021 o-Xylene NE LAP PA EPA 8021 p-Xylene NE LAP PA EPA 8081 2,4'-DDD NE LAP PA EPA 8081 2,4'-DDE NE LAP PA EPA 8081 2,4'-DDT NE LAP PA EPA 8081 4,4'-DDD NE LAP PA EPA 8081 4,4'-DDE NE LAP PA EPA 8081 4,4'-DDT NE LAP PA EPA 8081 Aldrin (HHDN) NE LAP PA EPA 8081 Chlordane (tech.) NELAP PA EPA 8081 Dieldrin NELAP PA EPA 8081 Endosulfan I NELAP PA EPA8081 Endosulfan II NELAP PA EPA 8081 Endosulfan sulfate NELAP PA EPA 8081 Endrin NE LAP PA EPA 8081 Endrin aldehyde NE LAP PA EPA 8081 Endrin ketone NE LAP PA

~~ The Pennsylvania Deparbnent of Environmental Protection Laboratory Accreditation Program is a NELAP recognized

Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing.

1/19/2016 1/19/2016 1/19/2016 1/19/2016 1/19/2011

12/12/2005 12/12/2005

1119/2005 51212006

10/17/2007 4/4/2005

1/19/2005 12/4/2007 4/4/2005

12/4/2007 1/19/2005 7/29/2015 3/26/2012 3/26/2012 1119/2005 1/19/2005 1/24/2007 5/2/2006

12/4/2007 1119/2005 3/26/2012 1/19/2005 1/24/2007 1/24/2007 1/24/2007

11/19/2015 11/19/2015 11119/2015

1/19/2005 1119/2005 1/19/2005 1/19/2005 1119/2005 1/19/2005 1/19/2005 111912005 1119/2005 1/19/2005 1/19/2005 1/19/2005

Page 45 of57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania gJf DEPARTMENT OF ENVIRONMENTAL PROTECTION Laboratory Scope of .Accreditation

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes should be used only when associated with a valid certificate of accreditation.

DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TN102128 (717) 656-2300 PADWIS ID: 36037

Matrix: Solid and Chemical Materials Method Revision Analyte Accreditation Type Primary Effective Date

EPA 8081 Heptach\or NELAP PA 1/19/2005 EPA 8081 Heptachlor epoxide NE LAP PA 1/19/2005 EPA8081 Kepone NE LAP PA 1/19/2005 EPA 8081 Methoxychlor NELAP PA 1/19/2005 EPA 8081 Mirex NE LAP PA 1/19/2005 EPA 8081 A Organochlorine pesticides by GC/ECD NE LAP PA 3/26/2012 EPA 8081 B Organochlorine pesticides by GC/ECD NELAP PA 1/1/2013 EPA 8081 Toxaphene (Chlorinated camphene) NE LAP PA 1/19/2005 EPA 8081 alpha-BHC (alpha-Hexachlorocyclohexane) NE LAP PA 1/19/2005 EPA 8081 alpha-Chlordane NELAP PA 41412005 EPA 8081 beta-BHC (beta-Hexachlorocyclohexane) NE LAP PA 1/19/2005 EPA 8081 delta-BHC ( delta-Hexachlorocyclohexane) NE LAP PA 1/19/2005 EPA 8081 gamma-BHC (Lindane, gamma- NE LAP PA 1/19/2005

Hexach\orocyclohexane) EPA 8081 gamma-Chlordane NELAP PA 4/4/2005 EPA 8082 Aroclor-1016 (PCB-1016) NELAP PA 1/2/2007 EPA 8082 Aroclor-1016 (in oil) NELAP PA 5/24/2011 EPA 8082 Aroclor-1221 (PCB-1221) NELAP PA 1/2/2007 EPA8082 Aroclor-1221 (in oil) NELAP PA 5/24/2011 EPA8082 Aroclor-1232 (PCB-1232) NELAP PA 1/2/2007 EPA 8082 Aroclor-1232 (in oil) NE LAP PA 5/24/2011 EPA 8082 Aroclor-1242 (PCB-1242) NE LAP PA 1/2/2007 EPA8082 Aroclor-1242 (in oil) NE LAP PA 5/24/2011 EPA 8082 Aroclor-1248 (PCB-1248) NE LAP PA 1/2/2007 EPA 8082 Aroclor-1248 (in oil) NE LAP PA 5/24/2011 EPA 8082 Aroc\or-1254 (PCB-1254) NELAP PA 1/2/2007 EPA 8082 Aroclor-1254 (in oil) NELAP PA 5/24/2011 EPA 8082 Aroclor-1260 (PCB-1260) NELAP PA 1/2/2007 EPA 8082 Aroclor-1260 (in oil) NELAP PA 5/24/2011 EPA8082 Aroclor-1262 (PCB-1262) NELAP PA 7/23/2008 EPA8082 Aroclor-1268 (PCB-1268) NELAP PA 7/23/2008 EPA 8082 Decachlorobiphenyl NELAP PA 12/17/2012 EPA8082 A PCBs by GC/ECD NE LAP PA 3/26/2012 EPA8141 Alachlor (Lasso) NE LAP PA 1/21/2009 EPA 8141 Atrazine NELAP PA 1/19/2005 EPA8141 Azinphos-methyl (Guthion) NELAP PA 41412005 EPA8141 Bolstar (Sulprofos) NE LAP PA 1/19/2005 EPA 8141 Carbophenothion (Trithion) NELAP PA 11/9/2012 EPA8141 Chlorpyrifos NE LAP PA 41412005 EPA8141 Coumaphos NELAP PA 1/19/2005 EPA8141 Demeton-0 NELAP PA 1/19/2005 EPA 8141 Demeton-S NELAP PA 1/19/2005 EPA 8141 Diazinon (Spectracide) NE LAP PA 1/19/2005 EPA8141 Dichlorovos (DDVP, Dichlorvos) NE LAP PA 1/19/2005 EPA 8141 Disulfoton NELAP PA 1/19/2005 EPA 8141 EPN (Santox) NELAP PA 1/19/2005

~~ The Pennsylvania Department of Environmental Protection Laboratory Accreditation Program is a NELAP recognized

Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing. Page 46 of57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania M DEPARTMENT OF ENVIRONMENTAL PROTECTION Laboratory Scope of Accreditation

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes should be used only when associated with a valid certificate of accreditation.

DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TN102128 (717) 656-2300 PADWIS ID: 36037

Matrix: Solid and Chemical Materials

Method Revision Analyte Accreditation Type Primary Effective Date EPA8141 Et hi on NE LAP PA 1/19/2005 EPA8141 Ethoprop (Prophos) NELAP PA 1119/2005 EPA8141 Famphur NE LAP PA 1119/2005 EPA8141 Fensulfothion NE LAP PA 1119/2005 EPA8141 Fenthion . NELAP PA 4/4/2005 EPA8141 Malathion NE LAP PA 1119/2005 EPA8141 Merphos NE LAP PA 1119/2005 EPA 8141 Methyl parathion (Parathion, methyl) NE LAP PA 5/25/2005 EPA8141 Mevinphos NE LAP PA 1119/2005 EPA8141 Na led NE LAP PA 1119/2005 EPA8141 A Organophosphorus compounds by GCINPD NE LAP PA 3/26/2012 EPA 8141 B Organophosphorus compounds by GCINPD NE LAP PA 3/26/2012 EPA8141 Parathion, ethyl (Ethyl parathion, Parathion) NE LAP PA 1119/2005 EPA8141 Phorate (Thimet) NELAP PA 1119/2005 EPA 8141 Ronne! NE LAP PA 1119/2005 EPA8141 Simazine NE LAP PA 11412006 EPA8141 Stirophos (Tetrachlorovinphos) NE LAP PA 111912005 EPA 8141 Tokuthion (Prothiophos) NE LAP PA 1/19/2005 EPA8141 Trichloronate NE LAP PA 1/19/2005 EPA8151 2,4,5-T NE LAP PA 1/19/2005 EPA 8151 2,4,5-TP (Silvex) NELAP. PA 1119/2005 EPA8151 2,4-D NE LAP PA 1119/2005 EPA 8151 2,4-DB (Butoxon) NE LAP PA 4/4/2005 EPA 8151 A Chlorinated herbicides by GC/ECD NE LAP PA 3/26/2012 EPA8151 Dalapon (2,2-Dichloropropionic acid) NE LAP PA 1119/2005 EPA8151 Dicamba NELAP PA 1119/2005 EPA8151 Dichloroprop (Dichlorprop) NE LAP PA 1119/2005 EPA 8151 Dinoseb (2-sec-Butyl-4,6-dinitrophenol, NE LAP PA 1119/2005

DNBP) EPA 8151 MCPA NE LAP PA 1119/2005 EPA 8151 MCPP (Mecoprop) NE LAP PA 5/2/2006 EPA8151 Pentachlorophenol (PCP) NE LAP PA 1/1912005 EPA 8151 Picloram ( 4-Amino-3,5,6-trichloro-2- NE LAP PA 1/1912005

pyridinecarboxylic acid) EPA 8260 I, 1, 1,2-Tetrachloroethane NE LAP PA 1/1912005 EPA 8260 1, 1, I-Trichloroethane NE LAP PA 1/1912005 EPA8260 1, 1,2,2-Tetrachloroethane NE LAP PA 1/1912005 EPA8260 1, 1,2-Trichloro-1,2,2-trifluoroethane (Freon NE LAP PA 5/212006

113) EPA8260 I, 1,2-Trichloroethane NE LAP PA 1119/2005 EPA 8260 1, 1-Dichloroethane NE LAP PA 1119/2005 EPA 8260 1, 1-Dichloroethene ( 1,1-Dichloroethylene) NE LAP PA 1119/2005 EPA8260 1, 1-Dichloropropene NE LAP PA 1119/2005 EPA8260 1,2,3-Trichlorobenzene NE LAP PA 1119/2005 EPA 8260 1,2,3-Trichloropropane ( 1,2,3-TCP) NE LAP PA 1119/2005 EPA 8260 1,2,4-Trichlorobenzene NE LAP PA 1119/2005

~~ The Pennsylvania Department of Environmental Protection Laboratory Accreditation Program is a NELAP recognized

Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing. Page 47 of57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania u DEPARTMENT OF ENVIRONMENTAL PROTECTION Laboratory Scope of Accreditation

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes should be used only when associated with a valid certificate of accreditation.

DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TNI02128 (717) 656-2300 PADWIS ID: 36037

Matrix: Solid and Chemical Materials Method Revision Analyte Accreditation Type Primary Effective Date

EPA8260 1,2,4-Trimethylbenzene NE LAP PA EPA 8260 l ,2-Dibromo-3-chloropropane (DBCP, NELAP PA

Dibromochloropropane) EPA8260 1,2-Dibromoethane (EDB, Ethylene NE LAP PA

di bromide) EPA 8260 1,2-Dichlorobenzene ( o-Dichlorobenzene) NE LAP PA EPA8260 1,2-Dichloroethane NE LAP PA EPA 8260 1,2-Dichloropropane NE LAP PA EPA 8260 1,3,5-Trimethylbenzene NE LAP PA EPA8260 1,3-Dichlorobenzene (m-Dichlorobenzene) NELAP PA EPA 8260 1,3-Dichloropropane NELAP PA EPA 8260 1,4-Dichlorobenzene (p-Dichlorobenzene) NELAP PA EPA8260 1,4-Dioxane ( 1,4-Diethyleneoxide) NE LAP PA EPA 8260 2,2-Dichloropropane NELAP PA EPA8260 2-Butanone (Methyl ethyl ketone, MEK) NE LAP PA EPA8260 2-Chloroethyl vinyl ether NE LAP PA EPA 8260 2-Chlorotoluene NELAP PA EPA8260 2-Hexanone NELAP PA EPA8260 2-Nitropropane NE LAP PA EPA 8260 3,3'-Dimethyl-l-butanol NE LAP PA EPA8260 4-Chloro-2-nitrophenol NE LAP PA EPA8260 4-Chlorotoluene NE LAP PA EPA 8260 4-Methyl-2-pentanone (MIBK) NE LAP PA EPA8260 Acetone NE LAP PA EPA8260 Acetonitrile NELAP PA EPA 8260 Acrolein (Propenal) NE LAP PA EPA 8260 Acrylonitrile NE LAP PA EPA 8260 Ally! chloride (3-Chloropropene) NE LAP PA EPA 8260 Benzene NE LAP PA EPA8260 Benzyl chloride NE LAP PA EPA 8260 Bromobenzene NE LAP PA EPA 8260 Bromochloromethane NELAP PA EPA8260 Bromodichloromethane NE LAP PA EPA 8260 Bromoform NE LAP PA EPA 8260 Carbon disulfide NE LAP PA EPA8260 Carbon tetrachloride NE LAP PA EPA8260 Chlorobenzene NE LAP PA EPA 8260 Chloroethane NE LAP PA EPA8260 Chloroform NE LAP PA EPA 8260 Chloroprene (2-Chloro-1,3-butadiene) NELAP PA EPA 8260 Crotonaldehyde NELAP PA EPA 8260 Cyclohexane NE LAP PA EPA 8260 Cyclohexanone NE LAP PA EPA8260 Dibromochloromethane NE LAP PA EPA8260 Dibromomethane NE LAP PA EPA 8260 Dichlorodifluoromethane (Freon 12) NE LAP PA

~~ The Pennsylvania Department of Environmental Protection Laboratory Accreditation Program is a NELAP recognized

Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing.

1119/2005 1/19/2005

1/19/2005

1119/2005 111912005 1/19/2005 1/19/2005 111912005 1/19/2005 1/19/2005 1/19/2005 111912005 1/19/2005 1/19/2005 51212006

111912005 12/17/2012 4/17/2009

5/2/2006 111912005 111912005 111912005

11412006 111912005 1/19/2005 1/19/2005 111912005

11412006 1/19/2005 1/19/2005 1/19/2005 1/19/2005 1119/2005 111912005 111912005 1/19/2005 1119/2005 4/17/2009

10/30/2014 6/29/2010

7/3/2007 111912005 1/19/2005 1/19/2005

Page 48 of57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania !1 DEPARTMENT OF ENVIRONMENTAL PROTECTION . Laboratory Scope of Accreditation

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes should be used only when associated with a valid certificate of accreditation.

DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TN102128 (717) 656-2300 P ADWIS ID: 36037

Matrix: Solid and Chemical Materials

Method Revision Analyte Accreditation Type Primary Effective Date EPA8260 Diisopropyl ether (DIPE) NE LAP PA 7/3/2007 EPA8260 Epichlorohydrin (l-Chloro-2,3- NE LAP PA 11412006

epoxypropane) EPA 8260 Ethanol NE LAP PA 1/4/2006 EPA8260 Ethyl acetate NELAP PA 1/4/2006 EPA 8260 Ethyl methacrylate NE LAP PA 1/4/2006 EPA8260 Ethyl tert-butyl ether (ETBE) NE LAP PA 7/3/2007 EPA8260 Ethyl benzene NELAP PA 1/19/2005 EPA 8260 Ethylene oxide NE LAP PA 10/30/2014 EPA8260 Gasoline-range organics (GRO) NE LAP PA 6/8/2006 EPA 8260 Hexachlorobutadiene (1,3- NE LAP PA 1/19/2005

Hexachlorobutadiene) EPA8260 lsobutyl alcohol (2-Methyl-1-propanol) NE LAP PA 7/3/2007 EPA 8260 lsopropyl alcohol (2-Propanol) NE LAP PA 1/19/2005 EPA8260 Isopropylbenzene (Cumene) NE LAP PA 817/2005 EPA8260 Methacrylonitrile NE LAP PA 1/24/2007 EPA8260 Methyl acetate NELAP PA 6/29/2010 EPA 8260 Methyl bromide (Bromomethane) NELAP PA 1/19/2005 EPA 8260 Methyl chloride (Chloromethane) NE LAP PA 1/19/2005 EPA8260 Methyl iodide (Iodomethane) NE LAP PA 5/2/2006 EPA8260 Methyl tert-butyl ether (MTBE) NE LAP PA 1/19/2005 EPA 8260 Methylcyclohexane NE LAP PA 1/21/2009 EPA 8260 Methylene chloride (Dichloromethane) NE LAP PA 1/19/2005 EPA8260 Methylmethacrylate NE LAP PA 5/2/2006 EPA8260 Naphthalene NE LAP PA 1/19/2005 EPA 8260 Pentachloroethane NE LAP PA 1/24/2007 EPA 8260 Propionitrile (Ethyl cyanide) NE LAP PA 1/24/2007 EPA8260 Styrene NE LAP PA 1/19/2005 EPA8260 Tetrachloroethene (PCB, Perchloroethylene) NE LAP PA 1/19/2005 EPA 8260 Tetrahydrofuran (THF) NE LAP PA 617/2012 EPA 8260 Toluene NE LAP PA 1/19/2005 EPA 8260 Trichloroethene (TCE, Trichloroethylene) NE LAP PA 1/19/2005 EPA8260 Trichlorofluoromethane (Freon 11) NE LAP PA 1/19/2005 EPA8260 B voes by GC/MS NE LAP PA 3/26/2012 EPA8260 c voes by Ge/Ms NE LAP PA 3/26/2012 EPA8260 Vinyl acetate NE LAP PA 1/19/2005 EPA 8260 Vinyl chloride (Chloroethene) NE LAP PA 111912005 EPA 8260 Xylenes, total NE LAP PA 1119/2005 EPA 8260 cis-1,2-Dichloroethene NE LAP PA 111912005 EPA8260 cis-1,3-Dichloropropene NE LAP PA 1/19/2005 EPA 8260 m+p-Xylene NE LAP PA 1/24/2007 EPA8260 n-Butyl acetate NE LAP PA 1/19/2016 EPA 8260 n-Butyl alcohol (n-Butanol, 1-Butanol) NE LAP PA 1/19/2005 EPA8260 n-Butylbenzene NE LAP PA 1/19/2005 EPA8260 n-Propylbenzene NE LAP PA 1/4/2006 EPA8260 o-Xylene NE LAP PA 1/24/2007

~~ The Pennsylvania Department of Environmental Protection Laboratory Accreditation Program is a NELAP recognized

Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing. Page49 of57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania ~ DEPARTMENT OF ENVIRONMENTAL

PROTECTION Laboratory Scope of Accreditation

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes should be used only when associated with a valid certificate of accreditation.

DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TNI02128 (717) 656-2300 P ADWIS ID: 36037

Matrix: Solid and Chemical Materials Method Revision Analyte Accreditation Type Primary Effective Date

EPA 8260 p-Isopropyltoluene (4-Isopropyltoluene) NE LAP PA EPA8260 sec-Butylbenzene NE LAP PA EPA8260 tert-Amyl alcohol (2-Methyl-2-butanol) NELAP PA EPA 8260 tert-Amyl methyl ether (TAME) NELAP PA EPA8260 tert-Butyl alcohol (2-Methyl-2-propanol) NELAP PA EPA 8260 tert-Butyl ethyl ether NELAP PA EPA 8260 tert-Butyl formate NELAP PA EPA 8260 tert-Butylbenzene NE LAP PA EPA 8260 trans-1,2-Dichloroethene NE LAP PA EPA 8260 trans-1,3-Dichloropropene NE LAP PA EPA 8260 trans-1,4-Dichloro-2-butene NE LAP PA EPA8260 SIM 1,4-Dioxane (1,4-Diethyleneoxide) NE LAP PA EPA8270 1,1 '-Biphenyl (Biphenyl, Lemonene) NELAP PA EPA8270 1,2,3 ,4-Tetrachlorobenzene NELAP PA EPA 8270 1,2,3 ,4-Tetrahydronaphthalene NE LAP PA EPA 8270 1,2,3,5-Tetrachlorobenzene NE LAP PA EPA8270 1,2,4,5-Tetrachlorobenzene NE LAP PA EPA8270 1,2,4-Trichlorobenzene NE LAP PA EPA8270 1,2-Dichlorobenzene ( o-Dichlorobenzene) NELAP PA EPA 8270 1,2-Dinitrobenzene (1,2-DNB) NELAP PA EPA 8270 1,2-Diphenylhydrazine NELAP PA EPA8270 1,3,5-Trinitrobenzene (1,3,5-TNB) NE LAP PA EPA8270 1,3-Dichlorobenzene (m-Dichlorobenzene) NE LAP PA EPA 8270 1,3-Dinitrobenzene (1,3-DNB) NELAP PA EPA 8270 1,4-Dichlorobenzene (p-Dichlorobenzene) NELAP PA EPA 8270 1,4-Dinitrobenzene ( 1,4-DNB) NE LAP PA EPA 8270 1,4-Dioxane (1,4-Diethyleneoxide) NELAP PA EPA8270 1,4-Naphthoquinone NE LAP PA EPA8270 1,4-Phenylenediamine NE LAP PA EPA8270 1-Chloronaphthalene NE LAP PA EPA8270 1-Methylnaphthalene NE LAP PA EPA 8270 1-Naphthylamine (alpha-Naphthylamine) NELAP PA EPA 8270 2,2'-0xybis( 1-chloropropane) (bis(2-Chloro- NE LAP PA

1-methylethyl) ether) EPA 8270 2,2' -oxybis( 1-Chloropropane) NE LAP PA EPA 8270 2,3,4,6-Tetrachlorophenol NE LAP PA EPA 8270 2,4,5-Trichlorophenol NE LAP PA EPA 8270 2,4,6-Trichlorophenol NELAP PA EPA 8270 2,4-Dichlorophenol NELAP PA EPA8270 2,4-Dimethylphenol NE LAP PA EPA 8270 2,4-Dinitrophenol NELAP PA EPA 8270 2,4-Dinitrotoluene (2,4-DNT) NELAP PA EPA8270 2,6-Dichlorophenol NELAP PA EPA8270 2,6-Dinitrotoluene (2,6-DNT) NE LAP PA EPA 8270 2-Acetylaminofluorene NE LAP PA EPA 8270 2-Chloronaphthalene NELAP PA

~~ The Pennsylvania Department of Environmental Protection Laboratory Accreditation Program is a NELAP recognized

Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing.

112412007 111912005 4/17/2009

7/3/2007 111912005 512512007 411712009 111912005 111912005 111912005 7/3/2007

4/17/2009 12/4/2007 7/3/2007

12/4/2007 7/3/2007 41412005

1119/2005 1119/2005 1119/2005 51212006 11412006

111912005 111912005 1/19/2005 51212006

121412007 1/19/2005 111912005

11412006 121412007 41412005

10/30/2014

11412006 111912005 111912005 111912005 111912005 111912005 111912005 111912005 111912005 111912005 111912005 1/19/2005

Page 50 of 57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania ~ DEPARTMENT OF ENVIRONMENTAL

PROTECTION Laboratory Scope of Accreditation

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes should be used only when associated with a valid certificate of accreditation.

DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TNI02128 (717) 656-2300 PADWIS ID: 36037

Matrix: Solid and Chemical Materials

Method Revision Analyte Accreditation Type Primary Effective Date EPA 8270 2-Chlorophenol NE LAP PA EPA8270 2-Methyl-4,6-dinitrophenol ( 4,6-Dinitro-2- NE LAP PA

methylphenol) EPA8270 2-Methylnaphthalene NELAP PA EPA8270 2-Methylphenol (o-Cresol) NE LAP PA EPA 8270 2-Naphthylamine (beta-Naphthylamine) NE LAP PA EPA8270 2-Nitroaniline NE LAP PA EPA8270 2-Nitrophenol NE LAP PA EPA8270 2-Picoline (2-Methylpyridine) NELAP PA EPA8270 3+4-Methylphenol (m+p-Cresol) ,NELAP PA EPA8270 3,3'-Dichlorobenzidine NELAP PA EPA 8270 3,3'-Dimethoxybenzidine NELAP PA EPA 8270 3,3'-Dimethylbenzidine NE LAP PA EPA 8270 3-Methylcholanthrene NE LAP PA EPA8270 3-Nitroaniline NELAP PA EPA8270 4,4'-Methylenebis(2-chloroaniline) NE LAP PA EPA8270 4-Aminobiphenyl NE LAP PA EPA8270 4-Bromophenyl phenyl ether NE LAP PA EPA 8270 4-Chloro-3-methylphenol NE LAP PA EPA 8270 4-Chloroaniline NELAP PA EPA 8270 4-Chlorophenyl phenyl ether NELAP PA EPA8270 4-Nitroaniline NE LAP PA EPA8270 4-Nitrophenol NE LAP PA EPA8270 4-Nitroquinoline-1-oxide NE LAP PA EPA 8270 5-Nitro-o-toluidine NE LAP PA EPA8270 6-Methylchrysene NE LAP PA EPA 8270 7, 12-Dimethylbenz(a)anthracene NE LAP PA EPA8270 Acenaphthene NE LAP PA EPA8270 Acenaphthylene NELAP PA EPA 8270 Acetophenone NELAP PA EPA 8270 Acrylamide NE LAP PA EPA 8270 Aniline NELAP PA EPA 8270 Anthracene NELAP PA EPA 8270 Aramite NE LAP PA EPA 8270 Atrazine NE LAP PA EPA8270 Benzaldehyde NE LAP PA EPA8270 Benzenethiol NE LAP PA EPA8270 Benzidine NE LAP PA EPA8270 Benzo[ a ]anthracene NE LAP PA EPA 8270 Benzo[ a ]pyrene NE LAP PA EPA 8270 Benzo[b ]fluoranthene NE LAP PA EPA 8270 Benzo[ghi]perylene NE LAP PA EPA8270 Benzo[k ]fluoranthene NE LAP PA EPA 8270 Benzoic acid NE LAP PA EPA8270 Benzyl alcohol NE LAP PA

~~ The Pennsylvania Department of Environmental Protection Laboratory Accreditation Program is a NELAP recognized

Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing.

111912005 111912005

111912005 111912005 511712005

4/4/2005 111912005 111912005 111912005 111912005 4/17/2009 111912005 111912005 111912005 111912005 1119/2005 111912005 111912005 111912005 111912005 4/412005

111912005 7/3/2007 4/4/2005

12/4/2007 111912005 111912005 111912005 111912005 112112009 111912005 111912005 511712005 111212007 12/4/2007 12/4/2007 111912005 111912005 111912005 111912005 111912005 111912005 111912005 111912005

Page 51 of57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania ~ DEPARTMENT OF EN,VIRONMENTAL

PROTECTION Laboratory Scope of Accreditation

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes should be used only when associated with a valid certificate of accreditation.

DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TNI02128 (717) 656-2300 PADWIS ID: 36037

Matrix: Solid and Chemical Materials Method Revision Analyte Accreditation Type Primary Effective Date

EPA 8270 Butyl benzyl phthalate (Benzyl butyl NELAP PA phthalate)

EPA8270 Caprolactam NELAP PA EPA 8270 Carbazole NELAP PA EPA 8270 Chlorobenzilate NE LAP PA EPA 8270 Chrysene (Benzo[ a ]phenanthrene) NE LAP PA EPA 8270 Di-n-butyl phthalate NELAP PA EPA 8270 Di-n-octyl phthalate NELAP PA EPA 8270 Diallate ( cis or trans) NELAP PA EPA 8270 Dibenz[ a,h ]acridine NELAP PA EPA 8270 Dibenz[aJ]acridine NELAP PA EPA 8270 Dibenzo[ a,h ]anthracene NE LAP PA EPA8270 Dibenzofuran NELAP PA EPA 8270 Diethyl phthalate NE LAP PA EPA 8270 Dimethoate NELAP PA EPA 8270 Dimethyl phthalate NELAP PA EPA8270 Diphenylamine NELAP PA EPA8270 Disulfoton NELAP PA EPA 8270 Ethyl methanesulfonate NELAP PA EPA8270 Famphur NE LAP PA EPA 8270 Fluoranthene NE LAP PA EPA8270 Fluorene NE LAP PA EPA 8270 Hexachlorobenzene NELAP PA EPA 8270 Hexachlorobutadiene (1,3- NELAP PA

Hexachlorobutadiene) EPA8270 Hexachlorocyclopentadiene NE LAP PA EPA 8270 Hexachloroethane NELAP PA EPA8270 Hexachloropropene NELAP PA EPA 8270 Indene NELAP PA EPA 8270 Indeno( 1,2,3-cd)pyrene NELAP PA EPA 8270 Isodrin NELAP PA EPA8270 Isophorone NELAP PA EPA 8270 Isosafrole NE LAP PA EPA8270 Kepone NE LAP PA EPA8270 Malononitrile NE LAP PA EPA 8270 Methapyrilene NELAP PA EPA 8270 Methyl methanesulfonate NELAP PA EPA8270 Methyl parathion (Parathion, methyl) NELAP PA EPA 8270 N,N-Dimethylacetamide NELAP PA EPA 8270 N,N-Dimethylformamide NELAP PA EPA 8270 N-Nitrosodi-n-butylamine NELAP PA EPA 8270 N-Nitrosodi-n-propylamine NE LAP PA EPA 8270 N-Nitrosodiethylamine NE LAP PA EPA8270 N-Nitrosodimethylamine NE LAP PA EPA8270 N-Nitrosodiphenylamine NE LAP PA EPA8270 N-Nitrosomethylethylamine NELAP PA

~~ The Pennsylvania Department of Environmental Protection Laboratory Accreditation Program is a NELAP recognized

Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing.

5/17/2005

12/4/2007 1/19/2005 5/2/2006

1119/2005 1119/2005 1/19/2005 5/2/2006

12/4/2007 5/17/2005 1/19/2005 1/19/2005 1/19/2005 5/2/2006

1/19/2005 5/2/2006 7/1/2007

1/19/2005 5/2/2006

1/19/2005 1/19/2005 1119/2005 1/19/2005

1/19/2005 1/19/2005 1/19/2005 12/4/2007 1/19/2005 5/2/2006

1119/2005 1119/2005 5/2/2006

5/23/2013 1/19/2005 1/19/2005 5/25/2007 12/4/2007 12/4/2007 1/19/2005 1/19/2005 1119/2005 1/1912005 1/19/2005 1/19/2005

Page 52 of 57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania !.if DEPARTMENT OF ENVIRONMENTAL PROTECTION Laboratory Scope of Accreditation

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes should be used only when associated with a valid certificate of accreditation.

DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TNI02128 (717) 656-2300 PADWIS ID: 36037

Matrix: Solid and Chemical Materials

Method Revision Analyte Accreditation Type Primary Effective Date EPA 8270 N-Nitrosomorpholine NE LAP PA EPA 8270 N-Nitrosopiperidine NE LAP PA EPA 8270 N-Nitrosopyrrolidine NE LAP PA EPA8270 Naphthalene NELAP PA EPA8270 Nitrobenzene NE LAP PA EPA8270 0,0,0-Triethyl phosphorothioate NE LAP PA EPA 8270 Parathion, ethyl (Ethyl parathion, Parathion) NE LAP PA EPA8270 Pentach\orobenzene NE LAP PA EPA 8270 Pentachloronitrobenzene (PCNB) NE LAP PA EPA8270 Pentachlorophenol (PCP) NE LAP PA EPA 8270 Phenacetin NE LAP PA EPA 8270 Phenanthrene NE LAP PA EPA 8270 Phenol NE LAP PA EPA8270 Phorate (Thimet) NE LAP PA EPA8270 Phthalic anhydride NE LAP PA EPA 8270 Pronamide (Kerb) NE LAP PA EPA 8270 Pyrene NE LAP PA EPA8270 Pyridine NELAP PA EPA8270 Quinoline NE LAP PA EPA 8270 D SOCs by GC/MS NE LAP PA EPA8270 c SOCs by GC/MS NE LAP PA EPA8270 Safrole NE LAP PA EPA 8270 Sulfotepp (Tetraethyl dithiopyrophosphate) NE LAP PA EPA 8270 Tetraethyl lead NE LAP PA EPA 8270 Thionazine (Thionazin, Zinophos) NE LAP PA EPA 8270 a,a-Dimethylphenethylamine (Phenterrnine) NE LAP PA EPA 8270 bis(2-Chloroethoxy)methane NE LAP PA EPA 8270 bis(2-Chloroethyl) ether NE LAP PA EPA8270 bis(2-Chloromethyl) ether NE LAP PA EPA 8270 bis(2-Ethylhexyl) adipate (di(2-Ethylhexyl) NE LAP PA

adipate) EPA8270 bis(2-Ethylhexyl) phthalate (DEHP) NE LAP PA EPA8270 o-Toluidine (2-Toluidine, 2-Methylaniline) NE LAP PA EPA 8270 p-(Dimethylamino )azobenzene NE LAP PA EPA 8270 p-Chloronitrobenzene NE LAP PA EPA 8270 tris-(2,3-Dibromopropyl) phosphate (tris- NELAP PA

BP) EPA8270 SIM 1-Methylnaphthalene NE LAP PA EPA 8270 SIM 2-Methylnaphthalene NE LAP PA EPA 8270 SIM Acenaphthene NE LAP PA EPA 8270 SIM Acenaphthylene NE LAP PA EPA 8270 SIM Anthracene NE LAP PA EPA 8270 SIM Benzo[ a ]anthracene NE LAP PA EPA8270 SIM Benzo[a]pyrene NE LAP PA EPA8270 SIM Benzo[b ]fluoranthene NE LAP PA EPA8270 SIM Benzo[ghi]perylene NE LAP PA

~~ The Pennsylvania Department of Environmental Protection Laboratory Accreditation Program is a NELAP recognized

Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing.

1/19/2005 1/19/2005 1/19/2005 1/19/2005

1/4/2006 5/2/2006

5/25/2007 1/19/2005 1/19/2005 1/19/2005 1/19/2005 1/19/2005 1/19/2005 5/2/2006

1/21/2009 1/19/2005 1/19/2005 4/4/2005

12/412007 3/26/2012 3/26/2012 1/19/2005 12/4/2007 317/2012 5/2/2006 5/2/2006

1/19/2005 1/19/2005 1/21/2009 1/21/2009

1/19/2005 1/19/2005 5/2/2006

1/21/2009 12/4/2007

7/25/2011 5/2312012 12/4/2007 12/4/2007 12/4/2007 12/4/2007 12/4/2007 12/4/2007 12/4/2007

Page 53 of 57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania u DEPARTMENT OF ENVIRONMENTAL PROTECTION Laboratory Scope of Accreditation

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes should be used only when associated with a valid certificate of accreditation.

DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TN102128 (717) 656-2300 PADWIS ID: 36037

Matrix: Solid and Chemical Materials Method Revision Analyte Accreditation Type Primary Effective Date

EPA 8270 SIM Benzo[k ]fluoranthene NE LAP PA 12/4/2007 EPA8270 SIM Chrysene (Benzo[a]phenanthrene) NE LAP PA 12/4/2007 EPA8270 SIM Dibenzo[ a,h]anthracene NE LAP PA 12/4/2007 EPA 8270 SIM Fluoranthene NELAP PA 12/4/2007 EPA8270 SIM Fluorene NELAP PA 12/4/2007 EPA8270 SIM Indeno(l ,2,3-cd)pyrene NELAP PA 12/4/2007 EPA8270 SIM Naphthalene NE LAP PA 12/4/2007 EPA 8270 SIM Phenanthrene NE LAP PA 12/4/2007 EPA8270 SIM Pyrene NELAP PA 12/4/2007 EPA 8290 1,2,3 ,4,6,7 ,8,9-0ctachlorodibenzo-p-dioxin NELAP PA 6/30/2010

(OCDD) EPA 8290 l,2,3,4,6,7,8,9-0ctachlorodibenzofuran NELAP PA 6/30/2010

(OCDF) EPA8290 1,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin NELAP PA 6/30/2010

(1,2,3,4,6, 7 ,8-hpcdd) EPA 8290 1,2,3 ,4,6, 7 ,8-Heptachlorodibenzofuran NE LAP PA 6/30/2010

(1,2,3,4,6,7,8-hpcdt) EPA 8290 1,2,3,4, 7 ,8,9-Heptachlorodibenzofuran NELAP PA 6/30/2010

(1,2,3,4, 7 ,8,9-hpcdt) EPA 8290 1,2,3 ,4, 7 ,8-Hexachlorodibenzo-p-dioxin NELAP PA 6/30/2010

(HxCDD) EPA8290 1,2,3 ,4, 7 ,8-Hexachlorodibenzofuran NE LAP PA 8/6/2010

(HxCDF) EPA8290 1,2,3,6, 7 ,8-Hexachlorodibenzo-p-dioxin NELAP PA 6/30/2010

(HxCDD) EPA8290 1,2,3 ,6, 7 ,8-Hexachlorodibenzofuran NELAP PA 6/30/2010

(HxCDF) EPA 8290 1,2,3, 7 ,8,9-Hexachlorodibenzo-p-dioxin NE LAP PA 6/30/2010

(HxCDD) EPA 8290 1,2,3, 7,8, 9-Hexachlorodibenzofuran NELAP PA 613012010

(HxCDF) EPA8290 1,2,3, 7 ,8-Pentachlorodi benzo-p-dioxin NELAP PA 6/30/2010

(PeCDD) EPA 8290 1,2,3, 7 ,8-Pentachlorodibenzofuran (PeCDF) NELAP PA 6/30/2010 EPA8290 2,3,4,6, 7 ,8-Hexachlorodibenzofuran NE LAP PA 6/30/2010

(HxCDF) EPA8290 2,3,4,7,8-Pentachlorodibenzofuran (PeCDF) NELAP PA 8/6/2010 EPA 8290 2,3,7 ,8-Tetrachlorodibenzo-p-dioxin NELAP PA 6/30/2010

(2,3, 7,8-TCDD)(Dioxin) EPA 8290 2,3, 7 ,8-Tetrachlorodibenzofuran (TCDF) NELAP PA 6/30/2010 EPA 8290 PCDDs and PCDFs by HRGC-HRMS NELAP PA 3/26/2012 EPA 8290 A PCDDs and PCDFs by HRGC-HRMS NE LAP PA 3/4/2015 EPA 8290 Total TCDD NELAP PA 6/30/2010 EPA 8290 Total TCDF NE LAP PA 6/30/2010 EPA8290 Total heptachlorodibenzo-p-dioxin NE LAP PA 6/30/2010

(HpCDD) EPA 8290 Total heptachlorodibenzofuran (HpCDF) NELAP PA 6/30/2010 EPA 8290 Total hexachlorodibenzo-p-dioxin (HxCDD) NE LAP PA 6/30/2010

~~ The Pennsylvania Department of Environmental Protection Laboratory Accreditation Program is a NELAP recognized

Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing. Page 54 of 57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania t...df DEPARTMENT OF ENVIRONMENTAL PROTECTION Laboratory Scope of Accreditation

·Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes should be used only when associated with a valid certificate of accreditation.

DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TN102128 (717) 656-2300 PADWIS ID: 36037

Matrix: Solid and Chemical Materials

Method Revision Analyte Accreditation Type Primary Effective Date EPA 8290 Total hexachlorodibenzofuran (HxCDF) NE LAP PA 6/30/2010 EPA8290 Total pentachlorodibenzo-p-dioxin (PeCDD) NE LAP PA 6/30/2010 EPA8290 Total pentachlorodibenzofuran (PeCDF) NE LAP PA 6/30/2010 EPA8315 2,5-Dimethylbenzaldehyde NE LAP PA 112112009 EPA8315 Acetaldehyde NELAP PA 112112009 EPA 8315 Benzaldehyde NE LAP PA 112112009 EPA 8315 Butanal (Butyraldehyde) NE LAP PA 1121/2009 EPA 8315 A Carbonyl compounds by HPLC NE LAP PA 312612012 EPA8315 Crotonaldehyde NELAP PA 112112009 EPA 8315 Formaldehyde NE LAP PA 111912005 EPA 8315 Hexanal (Hexaldehyde) NE LAP PA 1/21/2009 EPA 8315 lsovaleraldehyde NE LAP PA 1/21/2009 EPA8315 Pentanal (Valeraldehyde) NELAP PA 112112009 EPA 8315 Propanal (Propionaldehyde) NELAP PA 112112009 EPA 8315 m-Tolualdehyde ( 1,3-Tolualdehyde) NE LAP PA 1/2112009 EPA 8315 o-Tolualdehyde (1,2-Tolualdehyde) NELAP PA 112112009 EPA8315 p-Tolualdehyde (1,4-Tolualdehyde) NE LAP PA 1/21/2009 EPA8318 3-Hydroxycarbofuran NE LAP PA 4/4/2005 EPA 8318 Aldicarb (Temik) NE LAP PA 41412005 EPA 8318 Aldicarb sulfone NELAP PA 41412005 EPA8318 Aldicarb sulfoxide NE LAP PA 12/12/2005 EPA8318 Carbary! (Sevin) NE LAP PA 41412005 EPA 8318 Carbofuran (Furaden) NE LAP PA 41412005 EPA 8318 Methiocarb (Mesurol) NELAP PA 41412005 EPA 8318 Methomyl (Lannate) NELAP PA 41412005 EPA 8318 A N-Methylcarbamates by HPLC NE LAP PA 10/15/2012 EPA8318 Oxamyl (Vydate) NE LAP PA 1211212005 EPA8318 Propoxur (Baygon) NE LAP PA 41412005 EPA 8330 1,3,5-Trinitrobenzene (1,3,5-TNB) NE LAP PA 111912005 EPA8330 1,3-Dinitrobenzene (1,3-DNB) NE LAP PA 1119/2005 EPA8330 2,4,6-Trinitrotoluene (2,4,6-TNT) NE LAP PA 1/19/2005 EPA8330 2,4-Diamino-6-nitrotoluene NE LAP PA 712912015 EPA 8330 2,4-Dinitrotoluene (2,4-DNT) NELAP PA 111912005 EPA 8330 2,6-Diamino-4-nitrotoluene NE LAP PA 7/29/2015 EPA8330 2,6-Dinitrotoluene (2,6-DNT) NE LAP PA 1/19/2005 EPA8330 2-Amino-4,6-dinitrotoluene (2-Am-DNT) NE LAP PA 111912005 EPA8330 2-Nitrotoluene NELAP PA 111912005 EPA 8330 3,5-Dinitroaniline NE LAP PA 712912015 EPA8330 3-Nitrotoluene NE LAP PA 111912005 EPA8330 4-Amino-2,6-dinitrotoluene (4-Am-DNT) NE LAP PA 1/19/2005 EPA 8330 4-Nitrotoluene NELAP PA 111912005 EPA 8330 Methyl-2,4,6-trinitrophenylnitramine NELAP PA 111912005

(Tetryl) EPA8330 B Nitroaromatics and nitramines by HPLCIUV NE LAP PA 7/29/2015 EPA 8330 Nitroaromatics and nitramines by HPLCIUV NE LAP PA 312612012 EPA 8330 A Nitroaromatics and nitramines by HPLCIUV NE LAP PA 312612012

~~ The Pennsylvania Department of Environmental Protection Laboratory Accreditation Program is a NELAP recognized

Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing. Page 55 of57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania t-1 DEPARTMENT OF ENVIRONMENTAL PROTECTION Laboratory Scope of Accreditation

·. ~o•co;\,f • " . ,·/

"··· ··"'

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes should be used only when associated with a valid certificate of accreditation.

DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TNI02128 (717) 656-2300 P ADWIS ID: 36037

Matrix: Solid and Chemical Materials

Method Revision Analyte Accreditation Type Primary Effective Date EPA8330 Nitro benzene NELAP PA 1/19/2005 EPA8330 Nitroglycerin NE LAP PA 10/9/2013 EPA8330 Octahydro-1,3,5, 7-tetranitro-1,3,5, 7- NE LAP PA 1/24/2006

tetrazocine (HMX) EPA 8330 Pentaerythritol tetranitrate (PETN) NE LAP PA 11/2112005 EPA 8330 RDX (Hexahydro-1,3,5-trinitro-l,3,5- NE LAP PA 1/19/2005

triazine) EPA9012 Total cyanide NE LAP PA 4/18/2013 EPA 9045 pH NE LAP PA 11/19/2008 EPA9050 A Conductivity NE LAP PA 1/27/2014 EPA9050 Conductivity NE LAP PA 5/17/2005 EPA9060 Total organic carbon (TOC) NE LAP PA 1/19/2005 EPA9066 Total phenolics NE LAP PA 4/4/2005 EPA 9071 B Oil and grease NE LAP PA 1/19/2005 EPA 9071 B Total petroleum hydrocarbons (TPH) NE LAP PA 11/19/2015 EPA 9081 Cation exchange capacity of soils NE LAP PA 5/25/2005

(Ammonium acetate) EPA9095 B Paint filter liquids test NE LAP PA 11/19/2015 EPA9095 A Paint filter liquids test NE LAP PA 1/24/2007 EPA Lloyd Kahn Method Total organic carbon (TOC) NELAP PA 10/9/2013 FL-PRO Total petroleum hydrocarbons (TPH) NELAP PA 12/12/2005 MADEPEPH I.I Cll-C22 Aromatics NELAP PA 7/15/2013 MADEPEPH I.I Cl9-C36 Aliphatics NE LAP PA 7/15/2013 MADEPEPH I.I C9-C18 Aliphatics NE LAP PA 7/15/2013 MADEPVPH I.I C5-C8 Aliphatics NE LAP PA 7/15/2013 MADEPVPH I.I C9-Cl0 Aromatics NE LAP PA 7/15/2013 MADEPVPH I.I C9-Cl2 Aliphatics NE LAP PA 7/15/2013 NWTPH-Dx Diesel-range organics (DRO) NELAP PA 12/12/2005 NWTPH-Gx Gasoline-range organics (GRO) NE LAP PA 12/12/2005 SM2540E Fixed suspended solids NE LAP PA 1/19/2016 SM2540E Residue, volatile NELAP PA 1/19/2016 SM2540E Volatile dissolved solids NE LAP PA 1/19/2016 SM2540E Volatile suspended solids NE LAP PA 1119/2016 SM2540G Percent moisture in soil NELAP PA 11/19/2015 SM2540G Residue, total NELAP PA 2/25/2014 SM2540G Residue, volatile NELAP PA 11/19/2015 SM2540G Total, fixed, and volatile residue NELAP PA 3/19/2015 'SM5310B Total organic carbon (TOC) NE LAP PA 10/9/2013 TXJ005 (TNRCC) Total petroleum hydrocarbons (TPH) NE LAP PA 12/12/2005 TX1006 (TNRCC) Total petroleum hydrocarbons (TPH) NELAP PA 12/12/2005 WA-EPH Diesel-range organics (DRO) NE LAP PA 12/12/2005 WA-VPH Gasoline-range organics (GRO) NELAP PA 12/12/2005 WI-DRO Diesel-range organics (DRO) NELAP PA 12/12/2005 WI-GRO Gasoline-range organics (GRO) NELAP PA 12/12/2005

The Pennsylvania Department of Environmental Protection Laboratory Accreditation Program is ~ NE~AP recognized Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing.

Page 56 of 57 www.dep.state.pa.us Issue Date: 09/28/2017

~ pennsylvania ~ DEPARTMENT OF ENVIRONMENTAL

PROTECTION Laboratory Scope of Accreditation

Attached to Certificate of Accreditation 016-006 expiration date January 31, 2018. This listing of accredited analytes

should be used only when associated with a valid certificate of accreditation. DEP Laboratory ID: 36-00037 EPA Lab Code: PA00009 TNI Code: TNI02128 (717) 656-2300

PADWIS ID: 36037

The Pennsylvania Department of Environmental Protection Laboratory Accreditation Program is a NELAP recognized Accreditation Body. Customers are urged to verify the laboratory's current accreditation standing.

Page 57 of57 www.dep.state.pa.us Issue Date: 09/28/2017


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