expt 380 - aspen screen shotseng-web1.eng.famu.fsu.edu/~schreiber/LM08_lab_library/... · 2013. 9....

Absorption: An Aspen Plus® Tutorial 03September2013

Absorption: Aspen Plus® Tutorial

by

Loren B. Schreiber

O v e r v i e w Aspen Plus® is a powerful, world-class computer program that can simulate diverse chemical unit operations. This tutorial provides a step-by-step guide to students who (1) are presently conducting studying gas absorption and (2) have had no prior experience using Aspen Plus®. The specific physical application in this tutorial is absorption of carbon dioxide from an air stream into a water stream using a packed-bed column. Chemical engineering textbooks commonly examine this problem, or ones similar. Students may thus compare the numerical solution generated by Aspen Plus® with predictions using spreadsheets based upon elementary textbook methods. Having completed this tutorial, students will be able to examine what-if scenarios in gas absorption. In addition, students, on their own, will be able to start to play with the Aspen Plus® package to explore its extensive features.

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Table of Contents

Overview 1

Problem Statement 3

Tips 3

Spreadsheet Calculation for Stream Setup 5

Screen shots

Create Aspen Plus® file 7

Simulation ≫ Main Flowsheet tab 14 Simulation ≫ Setup 18 Properties ≫ Components ≫ Specifications 26 Properties ≫ Components ≫ Henry Comps 29 Properties ≫ Method 31 Simulation ≫ Streams 33 Simulation ≫ Blocks ≫ B1 ≫ Specifications 36 Simulation ≫ Blocks ≫ B1 ≫ Sizing and Rating 39 Stream Table 42

Create Report 43

Simulation Report 46

N o t e

This tutorial was developed using Aspen Plus® version 8.2.

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Problem Statement Predict the performance of an absorption column in a unit operations laboratory. The column has an inside diameter of 80 mm. The packed section has a length of 1.27 m and consists of dumped glass Raschig-style rings. The dimensions of the rings are: an ID of 8 mm, an OD of 10 mm, and a height of 9 mm. Carbon dioxide gas, at a flow rate of 3.466 SLPM, is mixed with dry air, at a flow rate of 39.87 SLPM. The gas mixture is fed to the bottom of the column at a temperature of 22.07 °C and a pressure of 103184 Pa. Standard conditions are 25 °C and 101325 Pa, according the specifications of the flow meter. Water is fed to the top of the column at a mass flow rate of 4 kg/min, at a temperature of 20.21 °C and at a pressure of 101931 Pa. Characterize the performance in terms of the flow rate, temperature, pressure, and composition of the gas outlet stream at the top of the column and liquid outlet stream at the bottom of the column. Tips Several issues may baffle students in applying Aspen Plus® to this particular problem. Here are some tips. The tutorial presents step-by-step screen shots. Tip 1 – Henry's components The user of process software must specify the model to characterize vapor-liquid equilibrium. Carbon dioxide and air have low solubility in water. Henry's Law provides a good description. In Aspen Plus®, the user must explicitly specify i to treat carbon dioxide and air as Henry's components. The software fails to deduce this on its own. Another idiosyncrasy is that this software cannot apply Henry's Law to air. This tutorial therefore approximates air as a mixture of oxygen (0.21 mole fraction), carbon dioxide (0.0004 mole fraction), and the balance nitrogen. Tip 2 – Gas feed stream The instruments in the unit operations laboratory display readings for gas flow rate in the unit SLPM (standard liters per minute). Some students have misinterpreted this unit and inputted incorrect data into Aspen Plus® leading to huge errors in the predictions. This tutorial presents a small spreadsheet to convert SLPM to the unit mol/min for the carbon dioxide and air streams. It then computes the composition of the gas fed to the column.

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Tip 3 – Flowsheet The flowsheet icon for the absorption column should show an inlet arrow at the top of the column and an inlet arrow at the bottom of the column. The RadFrac icon on the flowsheet, however, initially displays only one feed point for the column and it is located in the middle of the column. The user just needs to be persistent. First, connect one feed stream (e.g. the gas stream) to the inlet arrow in the middle of the column. Second, drag the feed arrow to the desired location on the column (e.g., the bottom of the column). A new feed arrow then appears in the middle of the column, which the user can connect to another stream and move it to the desired location (e.g., the top of the column). Tip 4 – Stage numbers The RadFrac model requires a minimum of two stages. Because inlets and outlets are located only at the ends of the columns, there is no need for more than two stages. Tip 5 – Rate-based model Students commonly use equilibrium models. The screen shots of this tutorial show the user where to select a rate-based model. Tip 6 – Report file The tutorial shows the user how to create a complete report as a text file. Just press CTRL + ALT + R and then select Simulation from the drop-down menu. Such a report is included at the end of the tutorial as an example Tip 7 – Dry gas-outlet stream In the unit operations laboratory, an instrument measures the content of carbon dioxide in the outlet gas stream. Water droplets striking the sensor will irrevocably damage the instrument.1 A silica gel filter, installed at the inlet of the instrument, protects the sensor. In addition to removing water droplets, the filter also removes water vapor. The content for the outlet gas stream from the RadFrac model contains water vapor. A simple spreadsheet calculation adjusts the RadFrac results to predict the carbon dioxide content of the outlet gas stream on a dry basis. The user may then compare this prediction to the measured result.

1 A student convincingly demonstrated this phenomenon in 2004.

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Expt 380 AbsorptionSetup for stream input (and output) to (and from) Aspen Plus ®

Trial ID 1a

Trial symbol + +

Property Unit Other Stream Stream Stream Stream Stream Stream

Values Air In CO2 In Gas In Water In Gas Out Dry Gas Out

Temp C 22.07 20.21

Pressure Pa 103184 101931

Molal flows

Total gas mol/min 1.6296 0.1417 1.7713 222.0372

Carbon dioxide mol/min 0.0007 0.1417 0.1423 0.0000

Nitrogen mol/min 1.2868 0.0000 1.2868 0.0000

Oxygen mol/min 0.3422 0.0000 0.3422 0.0000

Water mol/min 0.0000 0.0000 0.0000 222.0372Data from Derived from

Composition Aspen Aspen

Carbon dioxide mol fr 0.0004 1.000 0.0803 0.000 0.0736 0.0754

Nitrogen mol fr 0.7896 0.000 0.7264 0.000 0.7138 0.7306

Oxygen mol fr 0.2100 0.000 0.1932 0.000 0.1896 0.1940

Water mol fr 0.0000 0.000 0.0000 1.000 0.0230 0.0000

Sum 1.0000 1.0000 1.0000 1.0000 1.0000 1.0000

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Property Unit Other Stream Stream Stream Stream Stream Stream

Values Air In CO2 In Gas In Water In Gas Out Dry Gas Out

Other flows

Air inlet SL/min 39.87

Air inlet Sm3/min 0.03987

CO2 inlet SL/min 3.466

CO2 inlet Sm3/min 0.003466

Water inlet kg/min 4

Constants for gas flow meters

Standard pressure psia 14.696

Standard pressure Pa 101325

Standard temperature C 25

Standard temperature K 298.15

Standard molar volume m3 / mol 0.02446543

Other constants

Gas law contant R Pa m3 / mol K 8.314472

Molar mass water kg/mol 0.018015

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Initial screen in Aspen Plus.

Next step: Click on File on the menu bar at the top of the screen.

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Next step: Click New.

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Next step: Create a Blank Simulation

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Next step: Click on Simulation at the bottom of the Navigation Pane. Note: The Navigation Pane is the area on the left side of the screen listing various links in a tree structure.

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Next step: Select from the Model Palette at the bottom of the screen Columns >> Radfrac.

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Next step: Select the icon for the packed absorber. Paste it into the main flowsheet.

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Next step: After clicking on the Material stream icon in the Model Palette, move the cursor to the main flowsheet.

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Next step: Add a stream for the gas inlet. Connect the stream to the single feed arrow in the middle of the absorber icon.

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Next step Move the arrow on the absorber icon from the middle to the bottom. Click on Align on the ribbon to straighten the line, if needed.

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Next step: Add a stream for the liquid inlet. A feed arrow will appear in the middle of the absorber icon. Connect a stream to the feed arrow. Then move it to the top of the absorber icon. Click on Align on the ribbon to straighten the line, if needed.

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Next step: Add streams for the gas outlet and the liquid outlet.

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Next step: Click on Setup in the Navigation Pane on the left side of the screen. Enter the description Expt 380 - Trial 1a (++) in the Title box.

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Next step: Click on Simulation ≫ Setup ≫ Unit Sets in the Navigation Pane. Then click on the New button.

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Next step: Enter UOL as the ID for the user set of units.

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Next step: Adjust the Aspen Plus® units to be friendly with instrument readings for this trial.

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Next step: Click on Simulation ≫ Setup ≫ Specifications. Enter UOL set as the Global Unit Set.

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Next step: Click on Simulation ≫ Setup ≫ Report Options. Select all checkboxes in the General tab.

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Next step: On the Stream tab, select checkboxes for Mole and Mass for both the Flow basis and the Fraction basis.

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Next step: On the Property tab, select the checkboxes for all the options to include in the report file.

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Next step: Click on Properties at the bottom of the Navigation Pane.

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Next step: Using the Find button in the Selection tab, search for carbon dioxide.

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Next step: Click on CARBON-DIOXIDE in the list to add it to the model. Then add nitrogen, oxygen, and water.

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Next step: Click on Properties ≫ Components ≫ Henry Comps in the Navigation Pane. Click on the New button to create a set of components modeled by Henry’s Law.

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Next step: Click OK. Then select carbon dioxide, nitrogen, and oxygen.

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Next step: Click on Properties ≫ Methods in the Navigation Pane. Enter IDEAL for the base method. Enter HC-1 for Henry Components.

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Next step: Click Properties ≫ Methods ≫ Parameters ≫ Binary Interaction ≫ HENRY-1. Inspect the chart to confirm that parameters are available for all three components.

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Next step: Return to the Simulation in the Navigation Pane. Click on Simulation ≫ Streams ≫ 1 ≫ Input. Note: The numeral 1 refers to the stream number on the flow sheet. The data entry here defines it as the gas inlet),

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Next step: Consult the Excel spreadsheet, constructed earlier, for the gas inlet stream and enter the appropriate values for: -- temperature -- pressure -- total flow rate -- and composition.

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Next step: Enter the values for stream 2 (the water inlet).

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Next step: Click on Simulation ≫ Blocks ≫ B1 ≫ Specifications ≫ Setup Enter values for the absorber block on the Configuration tab. For Calculation type, enter Rate-based (not Equilibrium).

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Next step: Enter column entry points of the feeds on the Streams tab. The top stage in Aspen Plus® is always number 1. So in this case, the inlet water stage enters above stage 1.

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Next step: Enter the operating pressures for each stage on the Pressure tab.

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Next step: Click on Simulation ≫ Blocks ≫ B1 ≫ Sizing and Rating ≫ Packing Rating. Click on the New button.

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Next step: Click OK. Enter the data from the equipment data sheets.

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Next step: Click on Simulation ≫ Blocks ≫ B1 ≫ Sizing and Rating ≫ Packing Rating ≫ Rate-based. Then mark the checkbox for Rate-based calculations.

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Next step: Click the Run icon on the Ribbon. Allow the calculations to complete. Click on Stream Summary on the Ribbon.

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Next step: Copy the composition of the outlet gas stream into the Excel data sheet. Adjust the composition in the Excel sheet to a dry basis (water is eliminated) to find a carbon dioxide content of 0.0754 mole fraction in the outlet stream. Click on Report in the Ribbon and then select Simulation.

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Next step: Click OK

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Next step: Save the simulation report file. Format this text file, as needed, to furnish a neat display. This typically requires margins of 0.5" on all four sides. THE END

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ASPEN PLUS PLAT: WINDOWS VER: 28.0 09/01/2013 PAGE 1 EXPT 380 - TRIAL 1A (++) RUN CONTROL SECTION RUN CONTROL INFORMATION ----------------------- THIS COPY OF ASPEN PLUS LICENSED TO TYPE OF RUN: NEW INPUT FILE NAME: _3754lxp.inm OUTPUT PROBLEM DATA FILE NAME: _3754lxp LOCATED IN: PDF SIZE USED FOR INPUT TRANSLATION: NUMBER OF FILE RECORDS (PSIZE) = 0 NUMBER OF IN-CORE RECORDS = 256 PSIZE NEEDED FOR SIMULATION = 256 CALLING PROGRAM NAME: apmain LOCATED IN: C:\PROGRA~2\ASPENT~1\ASPENP~1.2\Engine\\xeq SIMULATION REQUESTED FOR ENTIRE FLOWSHEET

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ASPEN PLUS PLAT: WINDOWS VER: 28.0 09/01/2013 PAGE 2 EXPT 380 - TRIAL 1A (++) INPUT SECTION INPUT FILE(S) ------------- ; ;Input file created by Aspen Plus Rel. 28.0 at 22:00:44 Sun Sep 1, 2013 ;Directory C:\Users\schreiber\AppData\Local\Aspentech\Aspen Plus V8.2 Runid _A2 ; TITLE 'EXPT 380 - TRIAL 1A (++)' IN-UNITS SI FLOW='KG/MIN' MASS-FLOW='KG/MIN' MOLE-FLOW='MOL/MIN' & PRESSURE=PA TEMPERATURE=C DELTA-T=C PDROP=PA DEF-STREAMS CONVEN ALL MODEL-OPTION DATABANKS 'APV82 PURE28' / 'APV82 AQUEOUS' / 'APV82 SOLIDS' / & 'APV82 INORGANIC' / NOASPENPCD PROP-SOURCES 'APV82 PURE28' / 'APV82 AQUEOUS' / 'APV82 SOLIDS' & / 'APV82 INORGANIC' COMPONENTS CARBO-01 CO2 / NITRO-01 N2 / OXYGE-01 O2 / WATER H2O HENRY-COMPS HC-1 CARBO-01 NITRO-01 OXYGE-01 SOLVE RUN-MODE MODE=SIM FLOWSHEET BLOCK B1 IN=1 2 OUT=3 4 PROPERTIES IDEAL HENRY-COMPS=HC-1 PROP-DATA HENRY-1 IN-UNITS SI FLOW='KG/MIN' MASS-FLOW='KG/MIN' & MOLE-FLOW='MOL/MIN' PRESSURE=PA TEMPERATURE=C DELTA-T=C & PDROP=PA PROP-LIST HENRY BPVAL CARBO-01 WATER 171.3780000 -8741.550000 -21.66900000 & 1.10259000E-3 -.1500000000 79.85000000 0.0 BPVAL NITRO-01 WATER 176.5070000 -8432.770000 -21.55800000 & -8.4362400E-3 -.1500000000 72.85000000 0.0 BPVAL OXYGE-01 WATER 155.9210000 -7775.060000 -18.39740000 & -9.4435400E-3 .8500000000 74.85000000 0.0 STREAM 1 SUBSTREAM MIXED TEMP=22.07 PRES=103184. MOLE-FLOW=1.7713 MOLE-FRAC CARBO-01 0.1423 / NITRO-01 1.2868 / OXYGE-01 &

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ASPEN PLUS PLAT: WINDOWS VER: 28.0 09/01/2013 PAGE 3 EXPT 380 - TRIAL 1A (++) INPUT SECTION INPUT FILE(S) (CONTINUED) 0.3422 STREAM 2 SUBSTREAM MIXED TEMP=20.21 PRES=101931. MASS-FLOW=4. MASS-FRAC WATER 1. BLOCK B1 RADFRAC PARAM NSTAGE=2 ALGORITHM=STANDARD MAXOL=25 DAMPING=NONE COL-CONFIG CONDENSER=NONE REBOILER=NONE RATESEP-ENAB CALC-MODE=RIG-RATE FEEDS 1 2 ON-STAGE / 2 1 PRODUCTS 3 1 V / 4 2 L P-SPEC 1 101931. / 2 103184. COL-SPECS PACK-RATE 1 1 2 RASCHIG VENDOR=GENERIC PACK-MAT=CERAMIC & PACK-SIZE="0.375-IN" PACK-HT=1.27 DIAM=80. & P-UPDATE=NO PACK-RATE2 1 RATE-BASED=YES MTRFC-CORR=ONDA-68 & INTFA-CORR=ONDA-68 EO-CONV-OPTI REPORT INPUT STREAM-REPOR MOLEFLOW MASSFLOW MOLEFRAC MASSFRAC PROPERTY-REP PARAMS PCES PARAM-PLUS ; ; ; ; ;

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ASPEN PLUS PLAT: WINDOWS VER: 28.0 09/01/2013 PAGE 4 EXPT 380 - TRIAL 1A (++) FLOWSHEET SECTION FLOWSHEET CONNECTIVITY BY STREAMS --------------------------------- STREAM SOURCE DEST STREAM SOURCE DEST 2 ---- B1 1 ---- B1 3 B1 ---- 4 B1 ---- FLOWSHEET CONNECTIVITY BY BLOCKS -------------------------------- BLOCK INLETS OUTLETS B1 1 2 3 4 COMPUTATIONAL SEQUENCE ---------------------- SEQUENCE USED WAS: B1 OVERALL FLOWSHEET BALANCE ------------------------- *** MASS AND ENERGY BALANCE *** IN OUT RELATIVE DIFF. CONVENTIONAL COMPONENTS (MOL/MIN ) CARBO-01 0.142300 0.142300 0.165582E-10 NITRO-01 1.28680 1.28680 -0.674693E-12 OXYGE-01 0.342200 0.342200 -0.402302E-12 WATER 222.034 222.034 -0.601629E-14 TOTAL BALANCE MOLE(MOL/MIN ) 223.805 223.805 0.126993E-15 MASS(KG/MIN ) 4.05326 4.05326 0.122711E-13 ENTHALPY(WATT ) -0.105987E+07 -0.105987E+07 -0.192338E-08 *** CO2 EQUIVALENT SUMMARY *** FEED STREAMS CO2E 0.626259E-02 KG/MIN PRODUCT STREAMS CO2E 0.626259E-02 KG/MIN NET STREAMS CO2E PRODUCTION 0.00000 KG/MIN UTILITIES CO2E PRODUCTION 0.00000 KG/MIN TOTAL CO2E PRODUCTION 0.00000 KG/MIN

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ASPEN PLUS PLAT: WINDOWS VER: 28.0 09/01/2013 PAGE 5 EXPT 380 - TRIAL 1A (++) PHYSICAL PROPERTIES SECTION COMPONENTS ---------- ID TYPE ALIAS NAME CARBO-01 C CO2 CARBON-DIOXIDE NITRO-01 C N2 NITROGEN OXYGE-01 C O2 OXYGEN WATER C H2O WATER LISTID SUPERCRITICAL COMPONENT LIST HC-1 CARBO-01 NITRO-01 OXYGE-01 PARAMETER VALUES ---------------- CONVENTIONAL COMPONENT - UNARY PARAMETER TABLE PARAMETER COMPONENTS NAME/SET/EL CARBO-01 NITRO-01 OXYGE-01 WATER ZC 1 2.74000-01 2.89000-01 2.88000-01 2.29000-01 TC 1 3.04210+02 1.26200+02 1.54580+02 6.47096+02 PC 1 7.38300+06 3.40000+06 5.04300+06 2.20640+07 MW 1 4.40098+01 2.80135+01 3.19988+01 1.80153+01 PLXANT 1 1 1.40540+02 5.82820+01 5.12450+01 7.36490+01 2 -4.73500+03 -1.08410+03 -1.20020+03 -7.25820+03 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 -2.12680+01 -8.31440 00 -6.43610 00 -7.30370 00 6 4.09090-02 4.41270-02 2.84050-02 4.16530-06 7 1.00000 00 1.00000 00 1.00000 00 2.00000 00 8 2.16580+02 6.31500+01 5.43600+01 2.73160+02 9 3.04210+02 1.26200+02 1.54580+02 6.47100+02 TB 1 1.94700+02 7.73440+01 9.01880+01 3.73150+02 CPIG 1 1 1.97952+04 MISSING MISSING MISSING 2 7.34365+01 0.0 0.0 0.0 3 -5.60194-02 0.0 0.0 0.0 4 1.71533-05 0.0 0.0 0.0 5 0.0 0.0 0.0 0.0 6 0.0 0.0 0.0 0.0 7 3.00000+02 0.0 0.0 0.0 8 1.08860+03 1.00000+03 1.00000+03 1.00000+03 9 2.90990+04 MISSING MISSING MISSING 10 7.18760-01 MISSING MISSING MISSING 11 1.63680 00 MISSING MISSING MISSING DHVLWT 1 1 MISSING MISSING MISSING MISSING 2 MISSING MISSING MISSING MISSING 3 3.80000-01 3.80000-01 3.80000-01 3.80000-01 4 0.0 0.0 0.0 0.0 5 0.0 0.0 0.0 0.0 OMEGA 1 2.23621-01 3.77215-02 2.21798-02 3.44861-01 DHFORM 1 -3.93510+08 0.0 0.0 -2.41818+08 DGFORM 1 -3.94370+08 0.0 0.0 -2.28572+08 VLSTD 1 5.35578-02 5.35578-02 5.35578-02 1.80500-02 SG 1 3.00000-01 3.00000-01 3.00000-01 1.00000 00 API 1 3.40000+02 3.40000+02 3.40000+02 1.00000+01 WATSOL 1 1 -5.30000 00 -5.30000 00 -5.30000 00 1.76832 00

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ASPEN PLUS PLAT: WINDOWS VER: 28.0 09/01/2013 PAGE 6 EXPT 380 - TRIAL 1A (++) PHYSICAL PROPERTIES SECTION PARAMETER VALUES (CONTINUED) 2 -5.00000+02 -5.00000+02 -5.00000+02 -2.28298+03 3 0.0 0.0 0.0 0.0 4 2.00000+02 2.00000+02 2.00000+02 0.0 5 3.73000+02 3.73000+02 3.73000+02 9.24913+02 CHARGE 1 0.0 0.0 0.0 0.0 HIGPY 1 1 MISSING MISSING MISSING MISSING 2 0.0 0.0 0.0 0.0 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 0.0 0.0 0.0 0.0 6 0.0 0.0 0.0 0.0 7 0.0 0.0 0.0 0.0 8 0.0 0.0 0.0 0.0 9 0.0 0.0 0.0 0.0 10 1.00000+03 1.00000+03 1.00000+03 1.00000+03 PSEUDO 1 MISSING MISSING MISSING MISSING CPIGDP 1 1 2.93700+04 2.91050+04 2.91030+04 3.33630+04 2 3.45400+04 8.61490+03 1.00400+04 2.67900+04 3 1.42800+03 1.70160+03 2.52650+03 2.61050+03 4 2.64000+04 1.03470+02 9.35600+03 8.89600+03 5 5.88000+02 9.09790+02 1.15380+03 1.16900+03 6 5.00000+01 5.00000+01 5.00000+01 1.00000+02 7 5.00000+03 1.50000+03 1.50000+03 2.27315+03 ATOMNO 1 1 6.00000 00 7.00000 00 8.00000 00 1.00000 00 2 8.00000 00 0.0 0.0 8.00000 00 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 0.0 0.0 0.0 0.0 6 0.0 0.0 0.0 0.0 7 0.0 0.0 0.0 0.0 8 0.0 0.0 0.0 0.0 9 0.0 0.0 0.0 0.0 10 0.0 0.0 0.0 0.0 NOATOM 1 1 1.00000 00 2.00000 00 2.00000 00 2.00000 00 2 2.00000 00 0.0 0.0 1.00000 00 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 0.0 0.0 0.0 0.0 6 0.0 0.0 0.0 0.0 7 0.0 0.0 0.0 0.0 8 0.0 0.0 0.0 0.0 9 0.0 0.0 0.0 0.0 10 0.0 0.0 0.0 0.0 CPIXP1 1 1 2.98150+02 2.98150+02 2.98150+02 2.98150+02 2 1.00000+03 1.00000+03 1.00000+03 1.20000+03 3 -4.05519+08 -6.55614+06 -3.46467+06 -2.52304+08 4 2.08205+05 1.68923+05 9.71783+04 2.68010+05 5 -2.93419+04 -2.53171+04 -1.32017+04 -3.32484+04 6 -2.24028+01 -1.10356 00 -2.27567+01 2.37049-01 7 4.04634-03 -1.70199-03 5.72448-03 -2.17949-03 8 -4.10886-07 4.53696-07 -8.14234-07 3.66987-07 9 2.83617+08 -2.42771+08 -4.19015+08 1.17992+08 10 -1.25450+10 1.35946+10 1.77957+10 -9.24171+09 CPIXP2 1 1 1.00000+03 1.00000+03 1.00000+03 1.20000+03 2 3.00000+03 5.00000+03 3.00000+03 2.50000+03

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ASPEN PLUS PLAT: WINDOWS VER: 28.0 09/01/2013 PAGE 7 EXPT 380 - TRIAL 1A (++) PHYSICAL PROPERTIES SECTION PARAMETER VALUES (CONTINUED) 3 -4.29051+08 -2.20569+07 -1.82818+07 -2.80324+08 4 4.13593+05 2.57745+05 2.68238+05 3.67548+05 5 -5.88099+04 -3.67817+04 -3.88584+04 -4.46634+04 6 -1.63155 00 -2.86246-01 1.45889 00 -3.70790 00 7 1.51679-04 1.70355-05 -3.10073-04 1.85761-04 8 -8.83643-09 -7.51771-10 2.04865-08 -2.79906-09 9 5.30058+09 4.20149+09 1.68355+09 1.16931+10 10 -6.06527+11 -6.39852+11 -1.13530+11 -2.30214+12 CPIXP3 1 1 MISSING MISSING 3.00000+03 2.50000+03 2 MISSING MISSING 5.00000+03 5.00000+03 3 MISSING MISSING -5.77657+07 -2.66964+08 4 0.0 0.0 2.97323+05 3.34868+05 5 0.0 0.0 -4.05502+04 -4.07975+04 6 0.0 0.0 -1.99026 00 -4.39824 00 7 0.0 0.0 1.85450-04 2.47266-04 8 0.0 0.0 -8.49773-09 -7.91235-09 9 0.0 0.0 4.83512+10 4.83595+08 10 0.0 0.0 -2.42056+13 2.44832+12 TFP 1 MISSING MISSING MISSING MISSING S025E 1 2.10887+05 1.91609+05 2.05147+05 0.0 WAGNER 1 1 MISSING MISSING MISSING MISSING 2 0.0 0.0 0.0 0.0 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 0.0 0.0 0.0 0.0 6 1.00000+03 1.00000+03 1.00000+03 1.00000+03 DHVLDS 1 1 MISSING MISSING MISSING MISSING 2 0.0 0.0 0.0 0.0 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 0.0 0.0 0.0 0.0 6 0.0 0.0 0.0 0.0 7 1.00000+03 1.00000+03 1.00000+03 1.00000+03 CPIGDS 1 1 MISSING MISSING MISSING MISSING 2 0.0 0.0 0.0 0.0 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 0.0 0.0 0.0 0.0 6 0.0 0.0 0.0 0.0 7 0.0 0.0 0.0 0.0 8 0.0 0.0 0.0 0.0 9 0.0 0.0 0.0 0.0 10 3.00000+03 3.00000+03 3.00000+03 3.00000+03 CPIGYM 1 1 MISSING MISSING MISSING MISSING 2 0.0 0.0 0.0 0.0 3 0.0 0.0 0.0 0.0 4 1.00000 00 1.00000 00 1.00000 00 1.00000 00 5 0.0 0.0 0.0 0.0 6 2.00000+03 2.00000+03 2.00000+03 2.00000+03 PDSNEL 1 1 MISSING MISSING MISSING MISSING 2 MISSING MISSING MISSING MISSING 3 MISSING MISSING MISSING MISSING HCTYPE 1 0.0 0.0 0.0 0.0 VC 1 9.40000-02 8.92100-02 7.34000-02 5.59472-02 HCSOL 1 1 MISSING MISSING MISSING MISSING

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ASPEN PLUS PLAT: WINDOWS VER: 28.0 09/01/2013 PAGE 8 EXPT 380 - TRIAL 1A (++) PHYSICAL PROPERTIES SECTION PARAMETER VALUES (CONTINUED) 2 MISSING MISSING MISSING MISSING 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 1.00000+03 1.00000+03 1.00000+03 1.00000+03 FREEZEPT 1 2.16580+02 6.31490+01 5.43610+01 2.73150+02 CPIAPI 1 1 MISSING MISSING MISSING MISSING 2 0.0 0.0 0.0 0.0 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 0.0 0.0 0.0 0.0 CPIGPO 1 1 MISSING MISSING MISSING MISSING 2 0.0 0.0 0.0 0.0 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 0.0 0.0 0.0 0.0 6 0.0 0.0 0.0 0.0 7 0.0 0.0 0.0 0.0 8 0.0 0.0 0.0 0.0 9 0.0 0.0 0.0 0.0 10 0.0 0.0 0.0 0.0 11 0.0 0.0 0.0 0.0 12 1.00000+03 1.00000+03 1.00000+03 1.00000+03 CPIALEE 1 1 MISSING MISSING MISSING MISSING 2 0.0 0.0 0.0 0.0 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 0.0 0.0 0.0 0.0 6 0.0 0.0 0.0 0.0 7 8.31447 00 8.31447 00 8.31447 00 8.31447 00 8 0.0 0.0 0.0 0.0 9 1.00000+03 1.00000+03 1.00000+03 1.00000+03 CPITMLPO 1 1 MISSING MISSING MISSING MISSING 2 0.0 0.0 0.0 0.0 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 0.0 0.0 0.0 0.0 6 0.0 0.0 0.0 0.0 7 6.00000 00 6.00000 00 6.00000 00 6.00000 00 8 0.0 0.0 0.0 0.0 9 1.00000+03 1.00000+03 1.00000+03 1.00000+03 CPIWEOS 1 1 MISSING MISSING MISSING MISSING 2 0.0 0.0 0.0 0.0 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 0.0 0.0 0.0 0.0 6 0.0 0.0 0.0 0.0 7 0.0 0.0 0.0 0.0 8 0.0 0.0 0.0 0.0 9 0.0 0.0 0.0 0.0 10 0.0 0.0 0.0 0.0 11 8.31447 00 8.31447 00 8.31447 00 8.31447 00 12 1.00000 00 1.00000 00 1.00000 00 1.00000 00 13 1.00000+03 1.00000+03 1.00000+03 1.00000+03 CMPCLASS 1 1.10000+02 1.00000+02 1.00000+02 1.00000+02 ZWITTER 1 0.0 0.0 0.0 0.0

53

ASPEN PLUS PLAT: WINDOWS VER: 28.0 09/01/2013 PAGE 9 EXPT 380 - TRIAL 1A (++) PHYSICAL PROPERTIES SECTION PARAMETER VALUES (CONTINUED) RKTZRA 1 2.72560-01 2.89970-01 2.89240-01 2.43172-01 VCRKT 1 9.40000-02 8.92100-02 7.34000-02 5.59472-02 RACKET 1 1 3.42585-01 3.08608-01 2.54854-01 2.43844-01 2 2.72560-01 2.89970-01 2.89240-01 2.43172-01 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 1.00000+03 1.00000+03 1.00000+03 1.00000+03 MULAND 1 1 MISSING MISSING MISSING MISSING 2 0.0 0.0 0.0 0.0 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 5.00000+02 5.00000+02 5.00000+02 5.00000+02 MULDIP 1 1 1.87750+01 1.60040+01 -4.14760 00 -5.28430+01 2 -4.02920+02 -1.81610+02 9.40400+01 3.70360+03 3 -4.68540 00 -5.15510 00 -1.20700 00 5.86600 00 4 -6.91710-26 0.0 0.0 -5.87900-29 5 1.00000+01 0.0 0.0 1.00000+01 6 2.16580+02 6.31500+01 5.43600+01 2.73160+02 7 3.03150+02 1.24000+02 1.50000+02 6.46150+02 TRNSWT 1 1 1.01000+02 1.01000+02 1.01000+02 1.01000+02 2 1.02000+02 1.02000+02 1.02000+02 1.02000+02 3 1.00000+02 1.00000+02 1.00000+02 1.00000+02 4 1.02000+02 1.02000+02 1.02000+02 1.02000+02 5 1.06000+02 1.06000+02 1.06000+02 1.06000+02 MULPDS 1 1 MISSING MISSING MISSING MISSING 2 0.0 0.0 0.0 0.0 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 MISSING MISSING MISSING MISSING 6 0.0 0.0 0.0 0.0 7 1.00000+03 1.00000+03 1.00000+03 1.00000+03 MULIKC 1 1 MISSING MISSING MISSING MISSING 2 0.0 0.0 0.0 0.0 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 1.00000+03 1.00000+03 1.00000+03 1.00000+03 MULPO 1 1 MISSING MISSING MISSING MISSING 2 0.0 0.0 0.0 0.0 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 0.0 0.0 0.0 0.0 6 0.0 0.0 0.0 0.0 7 0.0 0.0 0.0 0.0 8 0.0 0.0 0.0 0.0 9 0.0 0.0 0.0 0.0 10 0.0 0.0 0.0 0.0 11 0.0 0.0 0.0 0.0 12 1.00000+03 1.00000+03 1.00000+03 1.00000+03 MULNVE 1 1 MISSING MISSING MISSING MISSING 2 0.0 0.0 0.0 0.0 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 0.0 0.0 0.0 0.0 6 1.00000+03 1.00000+03 1.00000+03 1.00000+03 MULPPDS9 1 1 MISSING MISSING MISSING MISSING

54

ASPEN PLUS PLAT: WINDOWS VER: 28.0 09/01/2013 PAGE 10 EXPT 380 - TRIAL 1A (++) PHYSICAL PROPERTIES SECTION PARAMETER VALUES (CONTINUED) 2 0.0 0.0 0.0 0.0 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 0.0 0.0 0.0 0.0 6 0.0 0.0 0.0 0.0 7 1.00000+03 1.00000+03 1.00000+03 1.00000+03 KLDIP 1 1 4.40600-01 2.65400-01 2.74100-01 -4.32000-01 2 -1.21750-03 -1.67700-03 -1.38000-03 5.72550-03 3 0.0 0.0 0.0 -8.07800-06 4 0.0 0.0 0.0 1.86100-09 5 0.0 0.0 0.0 0.0 6 2.16580+02 6.31500+01 6.00000+01 2.73160+02 7 3.00000+02 1.24000+02 1.50000+02 6.33150+02 KLPDS 1 1 MISSING MISSING MISSING MISSING 2 0.0 0.0 0.0 0.0 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 0.0 0.0 0.0 0.0 6 1.00000+03 1.00000+03 1.00000+03 1.00000+03 KLPO 1 1 MISSING MISSING MISSING MISSING 2 0.0 0.0 0.0 0.0 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 0.0 0.0 0.0 0.0 6 0.0 0.0 0.0 0.0 7 0.0 0.0 0.0 0.0 8 0.0 0.0 0.0 0.0 9 0.0 0.0 0.0 0.0 10 0.0 0.0 0.0 0.0 11 0.0 0.0 0.0 0.0 12 1.00000+03 1.00000+03 1.00000+03 1.00000+03 KLTMLPO 1 1 MISSING MISSING MISSING MISSING 2 0.0 0.0 0.0 0.0 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 4.00000 00 4.00000 00 4.00000 00 4.00000 00 6 0.0 0.0 0.0 0.0 7 1.00000+03 1.00000+03 1.00000+03 1.00000+03 KLPPDS8 1 1 MISSING MISSING MISSING MISSING 2 0.0 0.0 0.0 0.0 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 0.0 0.0 0.0 0.0 6 0.0 0.0 0.0 0.0 7 0.0 0.0 0.0 0.0 8 MISSING MISSING MISSING MISSING 9 7.00000 00 7.00000 00 7.00000 00 7.00000 00 10 0.0 0.0 0.0 0.0 11 1.00000+03 1.00000+03 1.00000+03 1.00000+03 VB 1 3.50189-02 3.46723-02 2.80225-02 1.88311-02 MUP 1 0.0 0.0 0.0 5.84934-25 LJPAR 1 1 2.52299+02 1.00693+02 1.22931+02 MISSING 2 3.76074-10 3.65722-10 3.43317-10 MISSING STKPAR 1 1 2.29746+02 9.12659+01 1.06422+02 9.51082+02 2 3.81456-10 3.80193-10 3.54143-10 2.39967-10

55

ASPEN PLUS PLAT: WINDOWS VER: 28.0 09/01/2013 PAGE 11 EXPT 380 - TRIAL 1A (++) PHYSICAL PROPERTIES SECTION PARAMETER VALUES (CONTINUED) DVBLNC 1 1.00000 00 1.00000 00 1.00000 00 1.00000 00 DLWC 1 1.00000 00 1.00000 00 1.00000 00 1.00000 00 CHI 1 0.0 0.0 0.0 0.0 SIGDIP 1 1 8.07100-02 2.90100-02 3.80660-02 1.77660-01 2 1.26620 00 1.24850 00 1.21360 00 2.56700 00 3 0.0 0.0 0.0 -3.33770 00 4 0.0 0.0 0.0 1.96990 00 5 0.0 0.0 0.0 0.0 6 2.16580+02 6.31500+01 5.43500+01 2.73160+02 7 3.04210+02 1.26200+02 1.54580+02 6.47100+02 SIGPDS 1 1 MISSING MISSING MISSING MISSING 2 0.0 0.0 0.0 0.0 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 1.00000+03 1.00000+03 1.00000+03 1.00000+03 SIGPO 1 1 MISSING MISSING MISSING MISSING 2 0.0 0.0 0.0 0.0 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 0.0 0.0 0.0 0.0 6 0.0 0.0 0.0 0.0 7 0.0 0.0 0.0 0.0 8 0.0 0.0 0.0 0.0 9 0.0 0.0 0.0 0.0 10 0.0 0.0 0.0 0.0 11 0.0 0.0 0.0 0.0 12 1.00000+03 1.00000+03 1.00000+03 1.00000+03 SIGISTE 1 1 MISSING MISSING MISSING MISSING 2 0.0 0.0 0.0 0.0 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 MISSING MISSING MISSING MISSING 6 4.00000 00 4.00000 00 4.00000 00 4.00000 00 7 0.0 0.0 0.0 0.0 8 1.00000+03 1.00000+03 1.00000+03 1.00000+03 SIGPDS14 1 1 MISSING MISSING MISSING MISSING 2 0.0 0.0 0.0 0.0 3 0.0 0.0 0.0 0.0 4 MISSING MISSING MISSING MISSING 5 0.0 0.0 0.0 0.0 6 1.00000+03 1.00000+03 1.00000+03 1.00000+03 SIGTDEW 1 1 MISSING MISSING MISSING MISSING 2 0.0 0.0 0.0 0.0 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 MISSING MISSING MISSING MISSING 6 4.00000 00 4.00000 00 4.00000 00 4.00000 00 7 0.0 0.0 0.0 0.0 8 1.00000+03 1.00000+03 1.00000+03 1.00000+03 VKGRP 1 1 MISSING MISSING MISSING MISSING 2 MISSING MISSING MISSING MISSING 3 MISSING MISSING MISSING MISSING 4 MISSING MISSING MISSING MISSING 5 MISSING MISSING MISSING MISSING 6 MISSING MISSING MISSING MISSING

56

ASPEN PLUS PLAT: WINDOWS VER: 28.0 09/01/2013 PAGE 12 EXPT 380 - TRIAL 1A (++) PHYSICAL PROPERTIES SECTION PARAMETER VALUES (CONTINUED) 7 MISSING MISSING MISSING MISSING 8 MISSING MISSING MISSING MISSING 9 MISSING MISSING MISSING MISSING 10 MISSING MISSING MISSING MISSING 11 MISSING MISSING MISSING MISSING 12 MISSING MISSING MISSING MISSING 13 MISSING MISSING MISSING MISSING 14 MISSING MISSING MISSING MISSING 15 MISSING MISSING MISSING MISSING 16 MISSING MISSING MISSING MISSING 17 MISSING MISSING MISSING MISSING 18 MISSING MISSING MISSING MISSING 19 MISSING MISSING MISSING MISSING 20 MISSING MISSING MISSING MISSING 21 MISSING MISSING MISSING MISSING 22 MISSING MISSING MISSING MISSING 23 MISSING MISSING MISSING MISSING 24 MISSING MISSING MISSING MISSING DHFVK 1 MISSING MISSING MISSING MISSING DGFVK 1 MISSING MISSING MISSING MISSING DHFVKM 1 MISSING MISSING MISSING MISSING DGFVKM 1 MISSING MISSING MISSING MISSING DGCON 1 MISSING MISSING MISSING MISSING DGCONM 1 MISSING MISSING MISSING MISSING DHCON 1 MISSING MISSING MISSING MISSING DHCONM 1 MISSING MISSING MISSING MISSING DGSUB 1 MISSING MISSING MISSING MISSING DGSUBM 1 MISSING MISSING MISSING MISSING DHSUB 1 MISSING MISSING MISSING MISSING DHSUBM 1 MISSING MISSING MISSING MISSING THRSWT 1 1 1.00000+02 1.00000+02 1.00000+02 1.00000+02 2 1.05000+02 1.05000+02 1.05000+02 1.16000+02 3 1.01000+02 1.01000+02 1.01000+02 1.01000+02 4 1.06000+02 1.06000+02 1.06000+02 1.06000+02 5 1.00000+02 1.00000+02 1.00000+02 1.00000+02 6 1.00000+02 1.00000+02 1.00000+02 1.00000+02 7 1.07000+02 1.07000+02 1.07000+02 1.07000+02 8 1.04000+02 1.04000+02 1.04000+02 1.04000+02 NATOM 1 1 1.00000 00 0.0 0.0 0.0 2 0.0 0.0 0.0 2.00000 00 3 2.00000 00 0.0 2.00000 00 1.00000 00 4 0.0 2.00000 00 0.0 0.0 5 0.0 0.0 0.0 0.0 6 0.0 0.0 0.0 0.0 7 0.0 0.0 0.0 0.0 8 0.0 0.0 0.0 0.0 9 0.0 0.0 0.0 0.0 10 0.0 0.0 0.0 0.0 11 0.0 0.0 0.0 0.0 DHAQFM 1 -4.13800+08 0.0 -1.17000+07 0.0 HCOM 1 0.0 0.0 0.0 0.0 CPLXP1 1 1 MISSING MISSING MISSING MISSING 2 MISSING MISSING MISSING MISSING 3 MISSING MISSING MISSING MISSING 4 0.0 0.0 0.0 0.0

57

ASPEN PLUS PLAT: WINDOWS VER: 28.0 09/01/2013 PAGE 13 EXPT 380 - TRIAL 1A (++) PHYSICAL PROPERTIES SECTION PARAMETER VALUES (CONTINUED) 5 0.0 0.0 0.0 0.0 6 0.0 0.0 0.0 0.0 7 0.0 0.0 0.0 0.0 8 0.0 0.0 0.0 0.0 9 0.0 0.0 0.0 0.0 10 0.0 0.0 0.0 0.0 CPLXP2 1 1 MISSING MISSING MISSING MISSING 2 MISSING MISSING MISSING MISSING 3 MISSING MISSING MISSING MISSING 4 0.0 0.0 0.0 0.0 5 0.0 0.0 0.0 0.0 6 0.0 0.0 0.0 0.0 7 0.0 0.0 0.0 0.0 8 0.0 0.0 0.0 0.0 9 0.0 0.0 0.0 0.0 10 0.0 0.0 0.0 0.0 PLPO 1 1 MISSING MISSING MISSING MISSING 2 0.0 0.0 0.0 0.0 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 0.0 0.0 0.0 0.0 6 0.0 0.0 0.0 0.0 7 0.0 0.0 0.0 0.0 8 0.0 0.0 0.0 0.0 9 0.0 0.0 0.0 0.0 10 0.0 0.0 0.0 0.0 11 0.0 0.0 0.0 0.0 12 1.00000+03 1.00000+03 1.00000+03 1.00000+03 LNVPEQ 1 1 MISSING MISSING MISSING MISSING 2 MISSING MISSING MISSING MISSING 3 MISSING MISSING MISSING MISSING LNVP1 1 1 MISSING MISSING MISSING MISSING 2 0.0 0.0 0.0 0.0 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 0.0 0.0 0.0 0.0 6 0.0 0.0 0.0 0.0 7 0.0 0.0 0.0 0.0 8 0.0 0.0 0.0 0.0 LOGVP1 1 1 MISSING MISSING MISSING MISSING 2 0.0 0.0 0.0 0.0 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 0.0 0.0 0.0 0.0 6 0.0 0.0 0.0 0.0 7 0.0 0.0 0.0 0.0 8 0.0 0.0 0.0 0.0 LNPR1 1 1 MISSING MISSING MISSING MISSING 2 0.0 0.0 0.0 0.0 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 0.0 0.0 0.0 0.0 6 0.0 0.0 0.0 0.0 7 0.0 0.0 0.0 0.0 8 0.0 0.0 0.0 0.0

58

ASPEN PLUS PLAT: WINDOWS VER: 28.0 09/01/2013 PAGE 14 EXPT 380 - TRIAL 1A (++) PHYSICAL PROPERTIES SECTION PARAMETER VALUES (CONTINUED) LOGPR1 1 1 MISSING MISSING MISSING MISSING 2 0.0 0.0 0.0 0.0 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 0.0 0.0 0.0 0.0 6 0.0 0.0 0.0 0.0 7 0.0 0.0 0.0 0.0 8 0.0 0.0 0.0 0.0 LNPR2 1 1 MISSING MISSING MISSING MISSING 2 0.0 0.0 0.0 0.0 LOGPR2 1 1 MISSING MISSING MISSING MISSING 2 0.0 0.0 0.0 0.0 PLTDEPOL 1 1 MISSING MISSING MISSING MISSING 2 0.0 0.0 0.0 0.0 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 0.0 0.0 0.0 0.0 6 0.0 0.0 0.0 0.0 7 0.0 0.0 0.0 0.0 8 0.0 0.0 0.0 0.0 9 0.0 0.0 0.0 0.0 10 1.00000+03 1.00000+03 1.00000+03 1.00000+03 WAGNER25 1 1 MISSING MISSING MISSING MISSING 2 0.0 0.0 0.0 0.0 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 0.0 0.0 0.0 0.0 6 MISSING MISSING MISSING MISSING 7 0.0 0.0 0.0 0.0 8 1.00000+03 1.00000+03 1.00000+03 1.00000+03 CPIGHY 1 1 MISSING MISSING MISSING MISSING 2 0.0 0.0 0.0 0.0 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 0.0 0.0 0.0 0.0 6 0.0 0.0 0.0 0.0 7 1.00000+03 1.00000+03 1.00000+03 1.00000+03 8 MISSING MISSING MISSING MISSING DNLDIP 1 1 2.76800 00 3.20910 00 3.91430 00 1.78630+01 2 2.62120-01 2.86100-01 2.87720-01 5.86060+01 3 3.04210+02 1.26200+02 1.54580+02 -9.53960+01 4 2.90800-01 2.96600-01 2.92400-01 2.13890+02 5 0.0 0.0 0.0 -1.41260+02 6 2.16580+02 6.31500+01 5.43500+01 2.73160+02 7 3.04210+02 1.26200+02 1.54580+02 6.47100+02 DNLPDS 1 1 MISSING MISSING MISSING MISSING 2 0.0 0.0 0.0 0.0 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 0.0 0.0 0.0 0.0 6 1.00000+03 1.00000+03 1.00000+03 1.00000+03 RHOM 1 0.0 0.0 0.0 0.0 VLPO 1 1 MISSING MISSING MISSING MISSING 2 0.0 0.0 0.0 0.0 3 0.0 0.0 0.0 0.0

59

ASPEN PLUS PLAT: WINDOWS VER: 28.0 09/01/2013 PAGE 15 EXPT 380 - TRIAL 1A (++) PHYSICAL PROPERTIES SECTION PARAMETER VALUES (CONTINUED) 4 0.0 0.0 0.0 0.0 5 0.0 0.0 0.0 0.0 6 0.0 0.0 0.0 0.0 7 0.0 0.0 0.0 0.0 8 0.0 0.0 0.0 0.0 9 0.0 0.0 0.0 0.0 10 0.0 0.0 0.0 0.0 11 0.0 0.0 0.0 0.0 12 1.00000+03 1.00000+03 1.00000+03 1.00000+03 DNLCOSTD 1 1 MISSING MISSING MISSING MISSING 2 0.0 0.0 0.0 0.0 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 1.00000+03 1.00000+03 1.00000+03 1.00000+03 DNLEXSAT 1 1 MISSING MISSING MISSING MISSING 2 MISSING MISSING MISSING MISSING 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 0.0 0.0 0.0 0.0 6 0.0 0.0 0.0 0.0 7 0.0 0.0 0.0 0.0 8 MISSING MISSING MISSING MISSING 9 6.00000 00 6.00000 00 6.00000 00 6.00000 00 10 0.0 0.0 0.0 0.0 11 1.00000+03 1.00000+03 1.00000+03 1.00000+03 DNLTMLPO 1 1 MISSING MISSING MISSING MISSING 2 0.0 0.0 0.0 0.0 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 4.00000 00 4.00000 00 4.00000 00 4.00000 00 6 0.0 0.0 0.0 0.0 7 1.00000+03 1.00000+03 1.00000+03 1.00000+03 DNLRACK 1 1 MISSING MISSING MISSING MISSING 2 0.0 0.0 0.0 0.0 3 MISSING MISSING MISSING MISSING 4 0.0 0.0 0.0 0.0 5 0.0 0.0 0.0 0.0 6 1.00000+03 1.00000+03 1.00000+03 1.00000+03 PSANT 1 1 MISSING MISSING MISSING MISSING 2 MISSING MISSING MISSING MISSING 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 1.00000+03 1.00000+03 1.00000+03 1.00000+03 PSTDEPOL 1 1 MISSING MISSING MISSING MISSING 2 0.0 0.0 0.0 0.0 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 0.0 0.0 0.0 0.0 6 0.0 0.0 0.0 0.0 7 0.0 0.0 0.0 0.0 8 0.0 0.0 0.0 0.0 9 0.0 0.0 0.0 0.0 10 1.00000+03 1.00000+03 1.00000+03 1.00000+03 PSTMLPOL 1 1 MISSING MISSING MISSING MISSING 2 0.0 0.0 0.0 0.0

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ASPEN PLUS PLAT: WINDOWS VER: 28.0 09/01/2013 PAGE 16 EXPT 380 - TRIAL 1A (++) PHYSICAL PROPERTIES SECTION PARAMETER VALUES (CONTINUED) 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 0.0 0.0 0.0 0.0 6 0.0 0.0 0.0 0.0 7 0.0 0.0 0.0 0.0 8 0.0 0.0 0.0 0.0 9 8.00000 00 8.00000 00 8.00000 00 8.00000 00 10 0.0 0.0 0.0 0.0 11 1.00000+03 1.00000+03 1.00000+03 1.00000+03 CPSPO1 1 1 MISSING MISSING MISSING 3.81518+03 2 0.0 0.0 0.0 1.25816+02 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 -8.65820+04 5 0.0 0.0 0.0 0.0 6 0.0 0.0 0.0 0.0 7 0.0 0.0 0.0 5.00000+01 8 1.00000+03 1.00000+03 1.00000+03 3.00000+02 DHSFRM 1 0.0 0.0 0.0 -2.92920+08 CPSDIP 1 1 -1.82820+04 2.74200+04 -1.38000+04 -2.62490+02 2 1.36030+03 1.70100+02 1.37900+03 1.40520+02 3 -1.21520+01 2.21250 00 0.0 0.0 4 5.15800-02 0.0 0.0 0.0 5 -7.69900-05 0.0 0.0 0.0 6 2.50000+01 3.70000+01 1.34600+01 3.15000 00 7 2.16580+02 6.30000+01 4.37800+01 2.73150+02 CPSXP1 1 1 MISSING MISSING MISSING MISSING 2 MISSING MISSING MISSING MISSING 3 MISSING MISSING MISSING MISSING 4 0.0 0.0 0.0 0.0 5 0.0 0.0 0.0 0.0 6 0.0 0.0 0.0 0.0 7 0.0 0.0 0.0 0.0 8 0.0 0.0 0.0 0.0 9 0.0 0.0 0.0 0.0 10 0.0 0.0 0.0 0.0 CPSXP2 1 1 MISSING MISSING MISSING MISSING 2 MISSING MISSING MISSING MISSING 3 MISSING MISSING MISSING MISSING 4 0.0 0.0 0.0 0.0 5 0.0 0.0 0.0 0.0 6 0.0 0.0 0.0 0.0 7 0.0 0.0 0.0 0.0 8 0.0 0.0 0.0 0.0 9 0.0 0.0 0.0 0.0 10 0.0 0.0 0.0 0.0 CPSXP3 1 1 MISSING MISSING MISSING MISSING 2 MISSING MISSING MISSING MISSING 3 MISSING MISSING MISSING MISSING 4 0.0 0.0 0.0 0.0 5 0.0 0.0 0.0 0.0 6 0.0 0.0 0.0 0.0 7 0.0 0.0 0.0 0.0 8 0.0 0.0 0.0 0.0 9 0.0 0.0 0.0 0.0 10 0.0 0.0 0.0 0.0

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ASPEN PLUS PLAT: WINDOWS VER: 28.0 09/01/2013 PAGE 17 EXPT 380 - TRIAL 1A (++) PHYSICAL PROPERTIES SECTION PARAMETER VALUES (CONTINUED) CPSXP4 1 1 MISSING MISSING MISSING MISSING 2 MISSING MISSING MISSING MISSING 3 MISSING MISSING MISSING MISSING 4 0.0 0.0 0.0 0.0 5 0.0 0.0 0.0 0.0 6 0.0 0.0 0.0 0.0 7 0.0 0.0 0.0 0.0 8 0.0 0.0 0.0 0.0 9 0.0 0.0 0.0 0.0 10 0.0 0.0 0.0 0.0 CPSXP5 1 1 MISSING MISSING MISSING MISSING 2 MISSING MISSING MISSING MISSING 3 MISSING MISSING MISSING MISSING 4 0.0 0.0 0.0 0.0 5 0.0 0.0 0.0 0.0 6 0.0 0.0 0.0 0.0 7 0.0 0.0 0.0 0.0 8 0.0 0.0 0.0 0.0 9 0.0 0.0 0.0 0.0 10 0.0 0.0 0.0 0.0 CPSXP6 1 1 MISSING MISSING MISSING MISSING 2 MISSING MISSING MISSING MISSING 3 MISSING MISSING MISSING MISSING 4 0.0 0.0 0.0 0.0 5 0.0 0.0 0.0 0.0 6 0.0 0.0 0.0 0.0 7 0.0 0.0 0.0 0.0 8 0.0 0.0 0.0 0.0 9 0.0 0.0 0.0 0.0 10 0.0 0.0 0.0 0.0 CPSXP7 1 1 MISSING MISSING MISSING MISSING 2 MISSING MISSING MISSING MISSING 3 MISSING MISSING MISSING MISSING 4 0.0 0.0 0.0 0.0 5 0.0 0.0 0.0 0.0 6 0.0 0.0 0.0 0.0 7 0.0 0.0 0.0 0.0 8 0.0 0.0 0.0 0.0 9 0.0 0.0 0.0 0.0 10 0.0 0.0 0.0 0.0 TREFHS 1 2.98150+02 2.98150+02 2.98150+02 2.98150+02 CPSPO 1 1 MISSING MISSING MISSING MISSING 2 0.0 0.0 0.0 0.0 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 0.0 0.0 0.0 0.0 6 0.0 0.0 0.0 0.0 7 0.0 0.0 0.0 0.0 8 0.0 0.0 0.0 0.0 9 0.0 0.0 0.0 0.0 10 0.0 0.0 0.0 0.0 11 0.0 0.0 0.0 0.0 12 1.00000+03 1.00000+03 1.00000+03 1.00000+03 CPSTMLPO 1 1 MISSING MISSING MISSING MISSING 2 0.0 0.0 0.0 0.0

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ASPEN PLUS PLAT: WINDOWS VER: 28.0 09/01/2013 PAGE 18 EXPT 380 - TRIAL 1A (++) PHYSICAL PROPERTIES SECTION PARAMETER VALUES (CONTINUED) 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 0.0 0.0 0.0 0.0 6 5.00000 00 5.00000 00 5.00000 00 5.00000 00 7 0.0 0.0 0.0 0.0 8 1.00000+03 1.00000+03 1.00000+03 1.00000+03 DGSFRM 1 0.0 0.0 0.0 -2.36760+08 VSPOLY 1 1 MISSING MISSING MISSING 1.96500-02 2 0.0 0.0 0.0 0.0 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 0.0 0.0 0.0 0.0 6 0.0 0.0 0.0 0.0 7 1.00000+03 1.00000+03 1.00000+03 1.00000+03 DNSDIP 1 1 3.29390+01 3.78700+01 4.45520+01 5.30300+01 2 6.84200-02 -6.02720-02 0.0 -7.84090-03 3 -2.84700-04 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 0.0 0.0 0.0 0.0 6 1.43100+02 2.06500+01 2.06500+01 2.33150+02 7 2.16580+02 6.31500+01 2.06500+01 2.73150+02 VSPO 1 1 MISSING MISSING MISSING MISSING 2 0.0 0.0 0.0 0.0 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 0.0 0.0 0.0 0.0 6 0.0 0.0 0.0 0.0 7 0.0 0.0 0.0 0.0 8 0.0 0.0 0.0 0.0 9 0.0 0.0 0.0 0.0 10 0.0 0.0 0.0 0.0 11 0.0 0.0 0.0 0.0 12 1.00000+03 1.00000+03 1.00000+03 1.00000+03 DNSTMLPO 1 1 MISSING MISSING MISSING MISSING 2 0.0 0.0 0.0 0.0 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 0.0 0.0 0.0 0.0 6 0.0 0.0 0.0 0.0 7 0.0 0.0 0.0 0.0 8 0.0 0.0 0.0 0.0 9 8.00000 00 8.00000 00 8.00000 00 8.00000 00 10 0.0 0.0 0.0 0.0 11 1.00000+03 1.00000+03 1.00000+03 1.00000+03 KSPOLY 1 1 MISSING MISSING MISSING MISSING 2 0.0 0.0 0.0 0.0 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 0.0 0.0 0.0 0.0 6 0.0 0.0 0.0 0.0 7 1.00000+03 1.00000+03 1.00000+03 1.00000+03 UFGRPD 1 1 3.85000+03 3.82000+03 3.83000+03 1.30000+03 2 1.00000 00 1.00000 00 1.00000 00 1.00000 00 3 MISSING MISSING MISSING MISSING 4 MISSING MISSING MISSING MISSING

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ASPEN PLUS PLAT: WINDOWS VER: 28.0 09/01/2013 PAGE 19 EXPT 380 - TRIAL 1A (++) PHYSICAL PROPERTIES SECTION PARAMETER VALUES (CONTINUED) 5 MISSING MISSING MISSING MISSING 6 MISSING MISSING MISSING MISSING 7 MISSING MISSING MISSING MISSING 8 MISSING MISSING MISSING MISSING 9 MISSING MISSING MISSING MISSING 10 MISSING MISSING MISSING MISSING 11 MISSING MISSING MISSING MISSING 12 MISSING MISSING MISSING MISSING 13 MISSING MISSING MISSING MISSING 14 MISSING MISSING MISSING MISSING 15 MISSING MISSING MISSING MISSING 16 MISSING MISSING MISSING MISSING 17 MISSING MISSING MISSING MISSING 18 MISSING MISSING MISSING MISSING 19 MISSING MISSING MISSING MISSING 20 MISSING MISSING MISSING MISSING 21 MISSING MISSING MISSING MISSING 22 MISSING MISSING MISSING MISSING 23 MISSING MISSING MISSING MISSING 24 MISSING MISSING MISSING MISSING UFGRPL 1 1 3.85000+03 3.82000+03 3.83000+03 1.30000+03 2 1.00000 00 1.00000 00 1.00000 00 1.00000 00 3 MISSING MISSING MISSING MISSING 4 MISSING MISSING MISSING MISSING 5 MISSING MISSING MISSING MISSING 6 MISSING MISSING MISSING MISSING 7 MISSING MISSING MISSING MISSING 8 MISSING MISSING MISSING MISSING 9 MISSING MISSING MISSING MISSING 10 MISSING MISSING MISSING MISSING 11 MISSING MISSING MISSING MISSING 12 MISSING MISSING MISSING MISSING 13 MISSING MISSING MISSING MISSING 14 MISSING MISSING MISSING MISSING 15 MISSING MISSING MISSING MISSING 16 MISSING MISSING MISSING MISSING 17 MISSING MISSING MISSING MISSING 18 MISSING MISSING MISSING MISSING 19 MISSING MISSING MISSING MISSING 20 MISSING MISSING MISSING MISSING 21 MISSING MISSING MISSING MISSING 22 MISSING MISSING MISSING MISSING 23 MISSING MISSING MISSING MISSING 24 MISSING MISSING MISSING MISSING UFGRP 1 1 3.85000+03 3.82000+03 3.83000+03 1.30000+03 2 1.00000 00 1.00000 00 1.00000 00 1.00000 00 3 MISSING MISSING MISSING MISSING 4 MISSING MISSING MISSING MISSING 5 MISSING MISSING MISSING MISSING 6 MISSING MISSING MISSING MISSING 7 MISSING MISSING MISSING MISSING 8 MISSING MISSING MISSING MISSING 9 MISSING MISSING MISSING MISSING 10 MISSING MISSING MISSING MISSING 11 MISSING MISSING MISSING MISSING

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ASPEN PLUS PLAT: WINDOWS VER: 28.0 09/01/2013 PAGE 20 EXPT 380 - TRIAL 1A (++) PHYSICAL PROPERTIES SECTION PARAMETER VALUES (CONTINUED) 12 MISSING MISSING MISSING MISSING 13 MISSING MISSING MISSING MISSING 14 MISSING MISSING MISSING MISSING 15 MISSING MISSING MISSING MISSING 16 MISSING MISSING MISSING MISSING 17 MISSING MISSING MISSING MISSING 18 MISSING MISSING MISSING MISSING 19 MISSING MISSING MISSING MISSING 20 MISSING MISSING MISSING MISSING 21 MISSING MISSING MISSING MISSING 22 MISSING MISSING MISSING MISSING 23 MISSING MISSING MISSING MISSING 24 MISSING MISSING MISSING MISSING DHVLDP 1 1 2.17300+07 7.49050+06 9.00800+06 5.66000+07 2 3.82000-01 4.04060-01 4.54200-01 6.12040-01 3 -4.33900-01 -3.17000-01 -4.09600-01 -6.25700-01 4 4.22130-01 2.73430-01 3.18300-01 3.98800-01 5 0.0 0.0 0.0 0.0 6 2.16580+02 6.31500+01 5.43600+01 2.73160+02 7 3.04210+02 1.26200+02 1.54580+02 6.47100+02 DHVLB 1 1.63703+07 5.56831+06 6.78526+06 4.06937+07 DHVLPO 1 1 MISSING MISSING MISSING MISSING 2 0.0 0.0 0.0 0.0 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 0.0 0.0 0.0 0.0 6 0.0 0.0 0.0 0.0 7 0.0 0.0 0.0 0.0 8 0.0 0.0 0.0 0.0 9 0.0 0.0 0.0 0.0 10 0.0 0.0 0.0 0.0 11 0.0 0.0 0.0 0.0 12 1.00000+03 1.00000+03 1.00000+03 1.00000+03 DHVLTDEW 1 1 MISSING MISSING MISSING MISSING 2 0.0 0.0 0.0 0.0 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 MISSING MISSING MISSING MISSING 6 4.00000 00 4.00000 00 4.00000 00 4.00000 00 7 0.0 0.0 0.0 0.0 8 1.00000+03 1.00000+03 1.00000+03 1.00000+03 MUVDIP 1 1 2.14800-06 6.55920-07 1.10100-06 1.70960-08 2 4.60000-01 6.08100-01 5.63400-01 1.11460 00 3 2.90000+02 5.47140+01 9.63000+01 0.0 4 0.0 0.0 0.0 0.0 5 0.0 0.0 0.0 0.0 6 1.94670+02 6.31500+01 5.43500+01 2.73160+02 7 1.50000+03 1.97000+03 1.50000+03 1.07315+03 MUVPDS 1 1 MISSING MISSING MISSING MISSING 2 0.0 0.0 0.0 0.0 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 1.00000+03 1.00000+03 1.00000+03 1.00000+03 MUVCEB 1 1 MISSING MISSING MISSING MISSING 2 MISSING MISSING MISSING MISSING

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ASPEN PLUS PLAT: WINDOWS VER: 28.0 09/01/2013 PAGE 21 EXPT 380 - TRIAL 1A (++) PHYSICAL PROPERTIES SECTION PARAMETER VALUES (CONTINUED) 3 0.0 0.0 0.0 0.0 4 0.0 0.0 0.0 0.0 5 1.00000+03 1.00000+03 1.00000+03 1.00000+03 MUVSUT 1 1 MISSING MISSING MISSING MISSING 2 0.0 0.0 0.0 0.0 3 0.0 0.0 0.0

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