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chain-of-custody by assigning a metaTRACE Control Number to each sample which identifies it through all further handling. The sample is recorded in the Master Log under this number, and the Control Number is written on the sample container* An internal chain-of-custody record (see SOPs) is initiated for each sample and each handling of the sample is documented on this record. . , -, ^>,-'~ T }("- , " - • ' '; " ' metaTRACE maintains large, locked, refrigerated and nonrefrigerated storage areas with provisions for hazardous material storage. After necessary preservation of the sample, the'Sample Custodian stores each sample in the appropriate area, filed under the metaTRACE control Number. Records are maintained,of sample transfer within the laboratory- Samples which vill not be analyzed by metaTRACE are handled in essentially the same way, with the metaTRACE Project Manager responsible for notifying the sample Custodian of receipt of samples. Samples transferred to another laboratory are accompanied by the custody record.
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Page 1: for each sample and each handling of the sample is … ICAP/AA Laboratory for the analysis of metals o Tech Laboratory containing automated instrumentation, for example, Technicon

chain-of-custody by assigning a metaTRACE Control Number toeach sample which identifies it through all further handling.The sample is recorded in the Master Log under this number,and the Control Number is written on the sample container*An internal chain-of-custody record (see SOPs) is initiatedfor each sample and each handling of the sample is documentedon this record.

. , -, ^>,-'~ T }("- , " - • ' '; " 'metaTRACE maintains large, locked, refrigerated andnonrefrigerated storage areas with provisions for hazardousmaterial storage. After necessary preservation of thesample, the'Sample Custodian stores each sample in theappropriate area, filed under the metaTRACE control Number.Records are maintained,of sample transfer within thelaboratory- Samples which vill not be analyzed by metaTRACEare handled in essentially the same way, with the metaTRACEProject Manager responsible for notifying the sampleCustodian of receipt of samples. Samples transferred toanother laboratory are accompanied by the custody record.

Page 2: for each sample and each handling of the sample is … ICAP/AA Laboratory for the analysis of metals o Tech Laboratory containing automated instrumentation, for example, Technicon

Section 4. PROCUREMENT QUALITY CONTROL

In general, procurements fall into two classes - materialsand services.

Materials

When applicable. Purchase Requisitions include qualityrequirements and these requirements are incorporated in thePurchase Order. Appropriate materials ara subjected toacceptance tests or incoming inspection and records of thesetests are maintained.

The requisitioning laboratory (GC,GC/MS, etc) is responsiblefor evaluating the quality of purchased materials andnotifying the Operations Manager of any deficiency. TheOperations Manager initiates Vendor Corrective Action Ifnecessary.

Limited shelf life materials such as chemicals are identifiedand the expiration date noted on individual* containers.Documentation of QC approved lots of reagents, QC checkresults, dates of receipt and expiration dates are maintainedby the QA Manager.

Services

In addition to the control over procured materials, arigorous•program of procured services control is maintained.Any subcontractors employed by metaTRACE, Inc. are requiredto conform to metaTRACE's quality program. For example, if aservice laboratory performs some analytical work undercontract to metaTRACE, that laboratory must describe its QCprocedures and subait documentation of the QC work performed.In addition, netaTRACE routinely incorporates QC samples(blanks, duplicates or samples whose true values are know tonetaTRACE) in the sample load so that they are unrecognizableto the subcontractor. The results on these samples providean independent measure of the quality of the subcontractor'swork.

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Section S. FACILITIES AND EQUIPMENT'

metaTRACE facilities and instrumentation represent the state-of-the-art for commercial analytical laboratories. We havetaken advantage of our start-up and purchased the mostsophisticated instrumentation available for the productionand management of high quality analytical data. The foundersof metaTRACE also used their decades of laboratory managementexperience to direct the design of our new facility. So -literally from the ground up, the netaTRACE laboratory isuniquely equipped to handle the requirements of today's mostcomplex and demanding environmental programs.

Facilities

The design of our new 27,000 square foot facility optimizesthe flow of samples, information and staff. The samplereceiving area's 3,000 square feet includes four truck bays,a secured solvent and waste storage area, and two walk-incoolers: one for medium to high hazard samples and the otherfor conventional samples. From the receiving area, samplesgo directly into either the Preparation Laboratory or theRegulated Access Area (RAA). The 2,000 square footPreparation Laboratory is designed for the efficientpreparation of large numbers of low to medium hazard samplesfor instrumental analysis. The RAA, for high hazard samplepreparation, has negative pressure air flow to preventcontamination' from entering other areas of the laboratory.Employees enter the RAA through airlocks complete with changeand shower facilities. Extracts proceed from the RAA througha pass-through to instrument laboratories. The RAA alsoprovides the ability to prepare highly toxic or radioactivesamples by remote robotic manipulation.

From the sample Preparation Laboratories, samples flow intoone of several netaTRACE instrument laboratories:

o ICAP/AA Laboratory for the analysis of metals

o Tech Laboratory containing automated instrumentation,for example, Technicon Autoanalyzers

o Chromatography Laboratory (GC, 1C, HPLC) equipped withpositive air pressure to isolate the lab from the samplepreparation areas

o GC/MS Laboratory where 0 GC/MS systems operate; lab hasa totally independent air handling system with charcoaland HEPA filters and positive air pressure• «

o Radiochemistry Laboratory with instrumentation designedfor various low level radiological analyses

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IIli

Computer terminals are located in the laboratories and y Joffices of metaTRACE Program Managers to allow easy access to ^*^our computerized Laboratory Information Management System(LIMS) which tracks samples through every stage of handling,from receipt through disposal, and captures analyticalresults, thereby facilitating reporting.

Equipment

A current list of major equipment at metaTRACE is included asTable 1.

ii

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TABLE 1 METATRACE MAJOR INSTRUMENTATION

1 Instrument Quantity Mantif acturar hade! Purchase1 . ""'"" iSflifi

• Gcia Chromatograph/ 3 . . v Hewlett Packard 5968A - 1986/(Mass Spectrometer ,,^ 1988 :'RTB Data System andLibrary (Wiley/NBS) ,_\r , f

"19- track magnetic tape - flAutosampler

1-aas Chromatograph/ 3 Hewlett Packard 5995 1986/ :Mass Spectrometer 1986Spllt/splitlessInjection; Capillary

I Splitter for odorI characterizationAutosaropler - * • ; •

JGas Chromatograph/ 4 Hewlett Packard 5970 1986Mass Spectrometer/

• " ' RTE Data System ... ^ ,„, ,,•.„,.„.-Mbrary (Wiley/

'9-track magnetic tape . , . ;-, «,.(,, ;,,;.

(Purge and Trap 3 r,Telgnar • • L5C2 1986AI.S/Heated Purge

(Gas Chromatograph ' 4 Hewlett Packard 5690 1986Ci. pi llary /Packed.Column(Autoinjector'Autosampler * , .; , ,„FI/EC/NP Detectors - - ' . ° ^ . . .JPJD/Hall Detectors - > -.

Gas Chromatograph 2 Hewlett Packard 5680 : 1966lAutoinjector ' .**•-••« , , ., • • :| Ant os amplerTl/EC/NP Detectors . ,_ -Q ,,>ffV- ,

;. , - ^ -.. •;i:.;; -'l— •"—— • . Lj ,,v .. - -,,; f] Inductively-Coupled i Thermo Jarrell Ash 1100 ••;•:. ' 1986'Argon Plasma Vacuum"Spectrometer

i , .. ,-.. : ," * - •" ' . . • • • • ' " .

A1 -mic Absorption 1 Thermo Jarrell Ash 12E ' 1086••rometer ; • • " . • " : . " " " " ' ' • : • - • • : -

Atomic Absorption 2 Perkin Elmer 30308 1987Spectrometer

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••Jf\ TABLE 1 HETATRACK MAJOR INSTRUMENTATIONI (continued)

.Instrument Quantity Manufacturer nocifti Purchase

Total Organic Carbon 2 Dohrmann-Xertex DC160 1986jijAnalyzer

Total Organic Halogen 1 Dohrmann-Xertex DX20A 1966jBAnalyser(4Ion Chronatograph 1 Dionex ' 40201 1986. *H t*LC Modu A eH1 'Autoanalyzer 1 Technicon TRAC800 1986

ItjHigh-Pressure Liquid 1 Perkin Elmer 410 1986! BChromatographAutosampler . .

Spectrophotometer 1 Milton Roy 601 1986

1 Spectrophotometer 2 Perkin Elmer 1420 Ratio 1987Recording

I fCoal Analyzer 1 Fisher Scientific 490 1987

I* "1 /rurbidimeter 1 HF Scientific DRT100B 1966

/ Single Detector 1 Tennelec LB5100 1967j (Automated Low Back- Series 3ground Gas ProportionalCounter

> Mult i-Detector (8) 1 Tennelec LB4000-8 1987Low Background Gas

fijProportional Counterii)Alpha Scintillation 4 Random SC-5 1987

, Counter for Radon Cellsn '1 'Alpha Spectroscopy 1 EG&G Ortec multi- 1987Counting System with 8 component

I Detectors. Electronics systemIpnd Computer

Gamma Spectrometry 2 Princeton miUtfi 0387 :;• ''ounting System with Gamma Tech componentatrinsic Germanium system ss^uctector. Electronics* T

j bomputer, Shielding

i|

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TABLE 1 METATRACE MAJOR INSTRUMENTATION: (continued)

Network available software: . - . . . >i -r '•_ .^f ,"/;.,..I rBase 5000 ;

dBase III Plusr Lotus 1.2,3[ Crosstalk XVI

WordstarWordPerfect

! IBM Assistant Series' pfs: First Choice

FormtoolI Reflection VII

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Section 6. EQUIPMENT MAINTENANCE

metaTRACE follows an orderly program of positive actions toprevent the failure of equipment or instruments during use.This preventive maintenance and careful calibration helpsto assure accurate measurements from instrumentation.Routine maintenance procedures are followed for allinstruments, glassware, deionlzed water, reagents andanalytical balances. These procedures are outlined in themetaTRACE SOP No. G030, included as Appendix D.

II ;,,?.- .;•:.!:•- flRl»OOU67

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Section 7. ANALYTICAL PROCEDURES

f . ,-."'' • • • ! ; ' ; , ' " • - ' • • - . . . ' •metaTRACE offers full-service capabilities for organic, :Inorganic and radiochemistry analyses of air, groundwater,surface water, wastewater, potable water, soil, hazardouswastes and biological camples. Routine services offered bymetaTRACE include: •/,.;;; , r.-o complete analytical services for organics/inorganics

o analysis of toxics, including dioxins-and furans

o analysis of mixed waste or co-contaminated wastes

o radiochemistry analyses : •"

o quick turnaround for remedial programs '

o TCLP analyses

o Appendix VIII and IX analyses . .

o hazardous waste analyses

o explosives analysis (military compounds).1 ,' ' ' " , '"/!''..' ••.,.- y" -rr, . • • - " . ' - ' • ' " -. V_/ o EPA priority pollutant, RCRA, SARA analyses

t o industrial hygiene sample analysis) o 'air quality analyses, Including odor characterization

. o methods development/validation studies . -

Special Capabilities and Services '• 'I ' " . J » | T ™ - „ 1 - •-,- I...•;. : • • . . , . , , , . - - - ' -.

Rad iochem tea 1 Analyses

I n e t a T R A C E offers a full range of radioanalytical servicesemploying new, state-of-the-art, fully computerized radiationdetection instrumentation* Our counting equipment reflectsthe variety and number required to process a . large sampleflow with maximum efficiency. Multi-detector and automatedsystems are routinely used to measure total uranium, radium-228, and other alpha, beta and gamma emitting radionuclides,

Ias well as for screening potentially contaminated samples.Specific alpha scintillation detectors are employed tomeasure both radium -2 2 6 and' radon-222* Isotopic thorium,

i uranium and transuranic analyses are performed usingI . computerized, multi-detector alpha spectrometric system.

metaTRACE has analyzed assorted 'media for gross screening andisotopic parameters, as well as standard chemical analyses onco-contaminated or high hazard camples.

.:.;;>"., <:<<-<>. flRif 001*68

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Explosives Analysis

metaTRACE has extensive expertise and experience, bothcorporate and individual, in the analysis of explosives andother military compounds in environmental samples. Theprimary analytical method for explosives analysis employsUS Army Toxic and Hazardous Materials Agency (USATHAMA)methodology. This method, originally developed for the Armyby metaTRACE principals, utilizes High Performance LiquidChromatography and is able to determine, in a singleanalysis, the following explosives, byproducts anddegradation products: 2,4,6-TNT; 2,4-DNT; 2,6-DNT; Tetryl;RDX; HMX; NB; 1,3-DNB; 1,3,5-TNB; and four anino/nitrodegradation products of TUT and DNT. metaTRACE has employedthis methodology for the analysis of hundreds of samples fora remedial action project in the midwest. In addition,metaTRACE principals have prior experience in the analysis ofthousands of environmental samples for explosives and othermilitary compounds from military facilities.

Specific Analytical Procedures

Analytical procedures and methodology generally followestablished EPA protocol. Table 2 is a list of the methods <. ,used for particular analytes or fractions. Implementation of V—'these methods is facilitated by the metaTRACE SOPs. The onlyvariance from EPA established methods allowed is for clients,e.g. USATHAMA', whose QA/QC requirements are more stringentthan those of the EPA, or where EPA methods do not exist forthe requested analytes. Separata SOPs for this type of work -have been prepared and are used as required. Included inAppendix E are the Tables of Contents from the General (G),General Methodology (GM), and Contract Laboratory Program(CLP) SOPs, • some of which have been included in total inother appendices.

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Table 2. metaTRACE Analytical Methoodology

Parameter Water Method ^ Soil/Sediment Method

Priority PollutantsBNAs EPA 625 RCRA 82706Volatiles EPA 624 EPA 8$40Metals EPA 200 series EPA 7000 seriesPest/PCBs EPA 608 , EPA 8080Cyanide EPA 335.2 * EPA 9010Phenols EPA 42Q.PU, RCRA 9065' ' ' :" : ' "., "tir- "*;/'.--" « • :>.•:',:• - .

HSL Compounds EPA IFB protocol EPA IFB protocol

TNT, 2-4 and2-6 DNT, nitro-benzene and . :trinitrobenzene USATHAMA 8G USATHAMA 811

, . . , - - ;Total OrganicCarbon EPA 415.1 RCRA 9060

1 ''. Tot-al Organic- •^-^ . Halide EPA 450.1 RCRA 9020

EP Toxicity * '(metals only) EPA 1310 RCRA 1310

Total metals EPA 200 series RCRA 7000 series(CLP listing) ,ICP metalsFurnace metals ,

BOD (5 day) EPA 405.1 -, EPA 405.1 i;

Acidity EPA 350.1{ ,, n EPA 350.1

Alkalinity , EPA 310.1 EPA 310.1 ; -•"',"'./.. • "'•', r • - -• • :•!• • . ' , - . • . ' • ; • "

Carbonate/ : Standard StandardBicarbonate ' Methods 203 , Methods 203,

'• • - ' • ' • • • , / ' " , . " . . . " , . - • . • ( . - - , •Sulfate : f ' tPA 375.2 ' EPA 375.2

Chloride .EPA 325.1 , RCRA 9250/9251/9252

Hardness , -EPA 130.2 • EPA 130.2i t " - , - * , - , • • • • ; - - , . - - , . . ^ ~VX Lithium ! Standard rf Standard

Methods 317 , Methods 317

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Table 2. metaTRACE Analytical Methodology(continued)

Parameter Water Kethod Soil/Sediment Method

Asbestos EPA methodology EPA methodology

Nitrate EPA* 352.1 RCRA 9200

Nitrate +Nitrite EPA 353.2 EPA 353.2

Nitrite EA 354.1 EPA 354.1

Nitrogen series' along with chloride, fluoride and sulfate maybe analyzed utilizing the ion Chromatograph method-EPA 300.0

Nitroaromatics EPA 609 EPA 609

PolynuclearAromatics EPA 610 EPA 8090.

Haloethers EPA 611 EPA 611

ChlorinatedHydrocarbons EPA 612 EPA 612

PurgeableHalocarbons EPA 601 RCRA 8010/8015

PurgeableAromatics EPA 602 RCRA 802O

Phenols EPA 604 RCRA 8040

Ignitability EPA 1020 EPA 1020

Corrosivity EPA 111O * EPA 1110

Reactivity EPA 9010/9030 EPA 9010/9030

Bacteria, Standard Standardfecal strep Methods 910 Methods 910

Bacteria, Standard Standardfecal coliform Methods 908 Methods 908

Bacteria, Standardtotal colifora Methods 909 RCRA 9132

Chlorine, .total residual EPA 330.1 EPA 330.1

Color ' EPA 110.2 EPA 110.2

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I Table 2. metaTRACE Analytical Methodology^ "(continued)i\ J Parameter Water Method Soil/Sediment Method

Conductance, ' „ , ; - Jspecific EPA 120.1 f>: RCRA 9050

Fluoride - •'"(electrode) EPA 340.2 ,, EPA 340.2 -I

, 1(distillation) EPA 340.1 ' EPA 340.1

I1 Fluoride

\ Nitrogen,ammonia EPA 350.1 EPA 350.1

fl\ . i. • -v Nitrogen,

Kjeldahl EPA 351.2 EPA 351.2

1 Nitrogen,organic .. EPA 351.1 EPA 351.1

1 Oil (TCTFE) EPA 413.1 RCRA 9070

BOD (20 day) EPA 507 . EPA 507

I ; COD EPA 410.1/ EPA 410.1/"Vr^ 410.2 ' 410.2

j Total Petroleum EPA 418.1 RCRA 3550/1 Hydrocarbons EPA 418.1

a Dissolvedj Oxygen EPA 360.1 EPA 360.1

\3A

pH EPA 150.1 RCRA 9045/9041• £Ortho Phosphorus EPA 365.1 !l. . . EPA 365.1

I Total Phosphorus EPA 365.4. EPA 365.4I '. yr,^ . --... .! 'f,: : -

Dissolved Solids EPA 160.2 EPA 160.2, ... • -. . • i;>- ,-: -•- - •• 'Settleable Solids EPA 160.3 EPA 160.3

• - ' f1" """ s : • •

« Suspended Solids EPA 160.1 EPA 160.1

I Total Solids EPA 160.3 **rr EPA 160.3

1 Volatile Solids EPA 160.4 EPA 160.4 ;

Sulfide • EPA 376.1 RCRA 9030

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Table 2. metaTRACB Analytical Methodology(continued)

I Parameter . HatfiE MfitllCd Soil/Sediment Method

Distilled Sulfide EPA 376.1 EPA 376.1! .

Sulfite EPA 377.1 EPA 377.1

, Surfactants EPA 425.1 EPA 425.1

Turbidity EPA 180.1 EPA 180.1

1 Viscosity ASTM ASTM

, Moisture Content EPA 160.3 EPA 160.31j BTU Value ASTM ASTM

j Ash Content ASTM ASTM

Sulphur Content ASTM ASTM

• 2,3,7,8-TCDD EPA 613 N/A

. 2,3,7,8-TCDD EPA CLP EPA CLP'2,3,7,8-TCDD Region VII Region VII \ — **

Rapid Prep Rapid Prep

1 Total Tetrathrough Octa

i dibenzodloxins/ RCRA 8280 RCRA 8280I furans (ASME) (ASME)

Radiological Parameters t> iGross Alpha EPA 900. OO1 RCRA 9310

) Gross Alpha,1 Coprecipitation EERF 00-022 EERF 00-02

, Gross Radium Alpha EPA 903.0 RCRA 9315* ., •

Gross Beta EPA 900.00 RCRA 9310

:«, Radium-226,Radon Emanation - EPA 903.1 EPA 903.1

Radium-226,* Proportional

Counting SM 70S3 • SM 705

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1

Table 2. metaTRACE "Analytical Methodology(continued)

„ - - -Parameter Water Method Soil/Sediment Method

: Radium-228, ' i'] Proportional -:-•",.- ^ ^" s "••y counting EPA 904.0 : RCRA 9320• Total Uranium, ^- !j. Radiochemical EPA 908.0 EPA 908.0

I Total Uranium,] ICAP EPA 200.74 EPA 200.7t. Isotopic Uranium EERF 00.07 EERF 00.07

j Isotopic Thorium EERF 00.07 EERF 00.07

I. Isotopic Plutonium EERF 00.07 EERF 00.07

I Americiuro-241 EERF AM.01 EERF AM.01

Lead-210 HASL Pb.Ol45 HASL Pb.Ol

Strontium-89 SM 704 SM 704

_j Strontium-90 HASL Sr-05 HASL Sr-05

Iodine-131 -radlochemical SM 710B -———————

Iodine-131, direct1 counting EPA 901.1 EPA 901.1

Gamma EmittingRadionuclide EPA 901.1 EPA 901.1

1. Prescribed Procedures for Measurement of Radioactivity inDrinking Hater, EPA 600/4-BO-032, 1982.

2 Eastern Environmental Radiation Facility, Radiochemistry1 Procedures Manual, EPA 520/5-84-006, 1984. •

3 Standard Methods for the Examination of Hater and, Wastewater, 16th Ed., 1985*

' 4 Methods for the Chemical Analyses of Water and Wastes, EPA€00/4-79-020.

5 EML Procedures Manual, HASL-300, 25th Ed., 1982.

6 SW-846, 3rd Edition, September 1986.

,;.,;••.' ,-' flRl»OOI»7lf

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Section 8. CALIBRATION PROCEDURES AND FREQUENCY

The metaTRACE Quality Control Program includes strictadherence to routine calibration procedures. Detailedprocedures and instrumentation to be utilized depend onspecific projects; plans for calibration are developed forthese specific projects. General calibration procedures andfrequencies are outlined in metaTRACE SOP Numbers G026 andG030, included as Appendix F and Appendix D, respectively.

i

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section «. LIMITS OF DETECTIONLimits of detection are determined as outlined in SOP G034,included as Appendix G. The MDL'c obtained by this procedureare used to judge the significance of a single measurementand is designed for a broad variety of physical and chemicalmethods. Values generally used for EPA target compounds arethose required by the most recent CLP contract, also includedin Appendix G. , *r vt y

- - . ^ ' "••'".' • -, -:*3 •:•• " ' ' ' . - ' " • rSection 10. ANALYSIS OF QUALITY CONTROL SAMPLES

AND DOCUMENTATION

netaTRACE makes use of intralaboratory testing to achieve thebest possible performance within its own laboratories and 'interlaboratory testing to compare that performance with -other laboratories* „<-_, r \f ;

Intralaboratory testing is performed to demonstrate that theanalytical system is in control, to identify any sources oferror within the measurement method, and to. establish theprecision and accuracy of the method. '

metaTRACE uses a laboratory blank prepared according to thespecific method and matrix requirements. Method blanks arerun with every analysis batchi they aid in demonstrating goodcontrol, or in investigating problems. Some of the potentialsources of error*.are the operator or analyst, equipment,calibration, or the operating conditions.

• = * . . • • ' ' . - ' 'metaTRACE uses Laboratory Control Standards (LCS), and/orspiked blank whose true values are known to the analyst toestablish that the analytical procedure is in control, Alaboratory control standard Is a blank into which a knownamount of the analyte(s) of interest is(are) epiked. Samplesmust be tied to the LCS by means of a date or batchidentifier. Recorded data generated by'the analysis of the •LCS"will be used to construct a Control chart (see-Attachment2) and control limits will be established. After analysis ofeach batch of samples, the analyst must check the appropriatecontrol chart to ensure that the analysis value for the LCSfalls within the control limits for that method. If the LCSexceeds the control limits, corrective action is taken; nofurther samples are analyzed until analysis of an LCS showsthe methodology is in control* . •A surrogate standard,.is a mixture of compounds spiked intoall camples unless a specif ic exception is made in thefl«teftKbditself. . The surrogate standard has applications to organicanalytes determined by GC £ GC/MS procedures and may be usedto determine recoveries and therefore matrix interferences.

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A matrix spike is an environmental sample spiked with thecompounds of interest or a representative cocktail of these •compounds. The matrix spike is used to determine the effectof the matrix on recovery, rather than as a control sample.

I . The matrix spike has applications to inorganic and organici analyses and may be used to determine chemical recoveries\ from the environmental matrix.

Precision is determined on replicate samples; if theses replicate samples are standard reference materials, accuracy

can be determined at the same time. Acceptance limits areestablished using tha range between the duplicates. During

j analysis, if the range of a set of duplicates falls beyond| the control limit, tha data will be regarded as unreliable.t Immediate corrective action will be taken and the analyses, repeated. Matrix spika and matrix spike duplicate samples^ per CLP protocol will be used to satisfy the duplicate| criteria for GC and GC/MS analyses.

I Quality Control criteria for GC and GC/MS analyses, when noti CLP protocol, will be determined by windows established from1 such analyses performed using the type of quality control

i frequencies listed below. • *

j HES FREQUENCY! CONTROLORGANIC ANALYSES

Blank 1 Surrogate Compounds

LCS and/or 1 % Recovery, analytesSpiked Blank of interest

Duplicate . 1 R P D* " '-Y~ VL- . \J1 Matrix Spike 1 % Recovery of target

/ analyte(s)

• Matrix Spike Dup. (2) . 1 RPD and * Recoveryi • - - ' 'INORGANIC ANALYSES,

I - .. - - ' ^ - . • . - _- : -

Blank. > 1- .- ' No contamination

i LCS and/or . 1 % Recovery, analytes: Spiked Blank of interest

, Quplicate 1 RPD

Matrix Spike*2) 1 ' • • • " , ' ; /% Recovery of targetv analyte(s)1 Frequency is based a batch of 20 samples or less of f

similar matrix or whenever samples are extracted,whichever is more frequent.

2 MS/MSD analyses will be performed per client request.

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|I

I Blind QC samples are periodically inserted into a sequence ofsamples by the QA Manager." Blind QC samples are prepared

'-" designee independently from the laboratory operations staff\ ; and serve as an independent check on the analyst's' ~ performance. Blind QC samples may be obtained from reference

materials purchased from the EPA, NBS, ERA or any othercertified quality control source. Blind QC samples can alsobe prepared from sample splits or previously analyzed samplesof known concentrations under the guidance and control of theQA Manager. They are initiated into metaTRACE's chain-ofcustody routine as a normal sample and handled as such untilanalysis and reporting of results is complete. Results ofperformance on QC samples is compiled and documented by theQA Manager.

' Interlaboratory tests are designed to compare the performanceof several laboratories. . Usually, identical sample sets aresubmitted to a relatively large number of laboratories. A.coordinating lab receives all the results and summarizes thedata so that any participating laboratory can evaluate andimprove its own performance. netaTRACE laboratoriesparticipate regularly in Water Supply Performance'Evaluations; Water Pollution Performance surveys; AsbestosBulk Sample Analysis QA Program; and specialized auditprograms such as that for Level 1 Environmental Assessmentanalyses. Both internal staff members and the QA Managerevaluate the results; if any results are not within thecontrol limits established by the coordinating laboratory,

C J corrective action is initiated at metaTRACE.V——— «" , • . . • -• f : • • 1> . ' , . . . . - - , -. •

'••: :-" v;:: "i <;.•'.'''.• ;l "*

. .»->.'J ?. ' t t

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Section 11. CORRECTIVE ACTION

' • ' • " " • " : . . ' 'Perhaps the single most important part of any qualityassurance program is a well-defined, effective policy forcorrecting quality problems. metaTRACE maintains a closed-loop corrective action system under the direction of the QAManager with full management support. While the entire QAProgram operates to prevent problems, it also serves toidentify and correct those that may exist. Usually theseproblems require either immediate corrective action or long-tern corrective action. •

Immediate corrective Action

Specific QC procedures and checklists are designed to helpanalysts detect the need for corrective action. Instrumentor equipment malfunctions and associated repairs are mostamenable to immediate corrective action by the analyst,before erroneous data is generated. metaTRACE*s QCprocedures incorporate method or equipment specific operatingranges or instrument tuning and/or calibration proceduresdesigned to define instrument performance. Analysts areresponsible for ensuring that each piece of equipment orinstrument meets method or manufacturer criteria prior tosample analysis. Corrective action night include , jrecalibration of instruments, reanalysis of known QC samples, -and, if necessary, of actual field samples* The action mayalso include-disassembly and cleaning or replacement ofequipment/instrument parts. metaTRACE maintains servicecontracts on all major instrumentation as a precautionagainst instrument downtime. All instrument repairs arerecorded in individual laboratory maintenance notebooks.

Longterm Corrective Action•Any quality control problen identified by standard QCprocedures, control charts, performance or system auditswhich cannot be resolved by immediate corrective action fallsinto the long-tern category. metaTRACE uses established QCparameters, to identify out-of-control situations, andidentifies procedures to ensure that out-of-controlsituations are reported to appropriate personnel responsiblefor ensuring that the problem is corrected as part of aclosed-loop action. The essential steps in the metaTRACElong-term corrective action systen are:

o ' Identify the out-of-control situation. This is bestaccomplished through the daily review of established QCcharts which define acceptable method performance.

o Assign responsibility for investigating the problem.

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\

o Investigate the cause of the out-of-control situation andidentify affected data,: jn

o Determine a corrective action plan to eliminate'theproblem. Action plans may require changes in, or thedevelopment of additional SOPs, additional training forpersonnel, or maintenance/repair of equipment/instruments. .

o Assign responsibility and implement the corrective'actionplan. . . . . . - . . - - • • • - -----"—""""" ^ . , , . - . - - •

o Monitor and evaluate data to establish the effectivenessof the corrective action ""

o Verify that the chosen corrective action has eliminatedthe out-of-control problem. Reanalyze affected samples andreport data. - - — -

Documentation of the problem ie important to the system. ACorrective Action Request ie initiated by the QA Managerimmediately after a situation is indentified. This report,included as Figure 3, identifies the problem, possible causesand the person responsible for action on-the problem. Theresponsible person may be anyone within the metaTRACEorganization. If no person is easily identified asresponsible for action, the QA Manager investigates thesituation and determines who is responsible.

The corrective Action Report-includes a description of thecorrective action planned and the date it was initiated, andspace for follow-up actions. The QA Manager checks to besure that the initial action is appropriate and has been ~implemented and, at appropriate later d&tes, rechecks to seethat the problem has been fully solved. The report aids theQA Manager in follow-up and-makes any quality problems ~ -visible to management; it may also prove valuable in solvingfuture similar problems. ——-

: (;. 7- ,t-r-Mf!-- •*

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Figure 3. metaTRACE Corrective Action FormCorrective Action Request Form No.

OriginatorPerson Responsiblefor Replying

Description of problem

DataContractInvolved

•and when identified:

;

State cause of problem f if known or suspected :_.. ,_,_•

Sequence of Corrective Action: (If no responsible person isidentified, notify QC Coordinator immediately. Submit all CAforms to QC Coordinator for'initial approval of CA.) *

State Date, Person, and Action Planned:

CA Initially Approved By:_________________• Date.

Follow-up Dates___________________ ____________

Final CA" Approved By:________________________ Date.

Information copies to:

Responsible Person/Department QC x^XCoordinator:__________________________________________

QC Manager:.

Department Manager:____;______• fl R k 0 0 k 81

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Section 12. HOW3ING TIKES AND PRESERVATION- •' t r-:-:.'K}$

The following table presents the normal preservation methods and holdingtimes followed by netaTRACE. Some agencies and clients require differentholding times. Differences are addressed on an individual basis in thelaboratory portion of the Project QA Plan* - •-- -------

Table 2. Containers, Preservation, Storage, and Holding Times* -\ - _ ^ 4 i • "". r

Container f : V; Preservative °-*£ Jfax. HoldingParameter Water Soil Rater Soil • Time all

INORGANIC TESTS

G Cool,4°C Cool,4°C 14 days

G /Cool,4°C Cool,4°C 14 days

G C90l,4°C Cool,4°C 28daysH2S04 to pH<2

Asbestos P G . ,cCoolf4oC Cool,4oC 48 hours

Bicarbonate P G !V Hone None Analyzerequired required Immediately

Biochemical- faxygen Demand ,., rr.% :Carbonaceous (BOD) . ; , t I

P G ; Cool,4oC Cool,4oC 48 hours

Bromide P G r T;Jilohe None V. :required required 28 days

Carbonate P G nc|fone None Analyzerequired required Immediately

Chemical Oxygen ^f^ r,,Demand (COD) P G , Cool,4°c Cool,4°C 28 days

H2S04 to pH<2

Chloride P G r> ftohe Nonerequired required 28 days

Chlorine, TotalResidual - P N/A / tJHone t N/A Analyze

- required Immediately

Color P N/A Cool,4°C N/A 46 hours

"vanide. Total P !- G CoolV4°C Cool,4°C 14NaOH to pH>120.6g Ascorbic

.( A Amenable to NaOH to pH>12V i

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Table 2. Containers, Preservation, Storage, and Holding Timesa(COKD'T)

Container PreservativejS d Max. HoldingParameter Hater Soil Water Soil Time all

j ._________________ ' ' ' ' ' __________ Matrices0-

Dissolved Oxygen

Probe G N/A None N/A AnalyzeBottle required Immediately

] and TopI - . . - - " " " ' '

Winkler G N/A Fix on Site N/A 8 hours-| Bottle Store in dark| and Top

Flouride P G None None . 28 days1 required required

Hardness P N/A HNO3 or H2SO4 N/A 6 monthsj to pH<2

Iodide P G Cool,4°C Cool,4°C 24 hours

; Iodine P G None None Analyzerequired required Immediately

Kjeldahl & OrganicNitrogen P G Cool,4°C Cool,4°C 28 days

H2SO4 to pH<2

| Metals1Chromium VI P G Cool,4°C Cool,4°c 24 hoursMercury P G HNO3 to pH<2 Cool,4°C 28 daysOthers P G HNO3 to pH<2 Cool,4°C 6 months

Nitrate P G Cool,4°C Cool,4°C 48 hours

Nitrate plusNitrite P G Cool,4°C Cool,4°C 28 days

H2S04 to pH<2

Nitrite P G *Coolf4 c Cool,4°C 48 hoursOil £ Grease G G Cool,4°C Cool,4°C 28 days

H2SO4 to pH<2

Orthophosphate P G Filter onsite Cool,4°C 48 hoursCool,4°C

pH P G None None Analyzerequired required Immediately-

flRl*OOt»83

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Table 2. containers, Preservation, storage, and Holding Times"

Phenols — *» : .• VU(,

to pH<2Phosphorous,Elemental G G Cool,4°C Cool,4°C 48 hoursPhosphorous^ "V^r.rO* Total P,G G ^ Cool,4°C Cool,4°C 28 days

H2S04 to pH<2 .,-Silica, Dissolved ' • • • ! "' +'*I-^' •or Total p G cobi,4°C Cool.4°C 28 daysResidue

Filterable p K/A • fcool 4<>r M/» ^ -.Settleable P N/A .- ' cool 2<>c N/A L*?SNonfilterable ! iff1 c ^A 48 hoursTotal(TSS> « »^ Cool,4°C N/A -

Specificconductance P G G.,f Cyol.4«c Cool,4«>c 28 days

Sulfate P G Cool,4°C Cool,4«C 28 days

Sulfide P G cool,4«C Coolf4«C 7 days. Add'Zinc Acetate

plus NaOH to pll>9Sulfite P G „ None Analyze

••:•><•'t'ffi*. ed required: Inaediatelysurfactants P , c . 'cooi.. cbol,4°c 48 hoursTeBperature P 6 H None Analyre

required required Imnediately

TUrbldity . _P.'.-•'•• ••VA. 'tafa; .. VA • ; 48 hoursORGANIC TESTsl : : V"^^ a'-. v

Acrolein £Acrylonitrile s s BCoolf4°C Cool,4°c 14 days*

Ila2S2039 °aySpll to 4-5k

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Table 2. Containers, Preservation, storage, and Holding Times*(COND'T)

Container^ Preservative ^ Max. HoldingParameter Water Soil Vater Soil Time all -_ ___________________________ • ________ Matrices0

Chlorinated G G Cool,4°C Cool,4°C 7 days until/Hydrocarbons1 40 days after

extraction

Haloethers1 G G Cool,4°C Cool,4°C 7 days until/0.008% Na2S2O39 store in 40 days afterStore in dark dark extraction

Nitroaromatics &Zsophorone1 G G Cool,4°C Cool,4°C 7 days until/

0.008% Na9S2O39 store in 40 days afterStore in dark dark extraction

Nitrosamines1'0 G G Cool,4°C Cool,4°C 7 days until/0.008% Na2S2O3& Store in 40 days afterStore in dark dark extraction

PCBs G G Cool,4°C Cool,4°C 7 days until/40 days afterextraction

Pesticides1 G G Cool,4°C Cool,4°C 7 days until/pH 5-9? 40 days after

extraction

Phenols1 G G Cool,4°C Cool,4°C 7 days until/O.O08% Na2S2O39 40 days after

extraction

Ph thai ateEsters1 G G Cool,4°C Cool,4°C 7 days until/

40 days after• "• .. . ' extraction

PolynuclearAromatic !Hydrocarbons1 G G Cool,4°C Cool,4°C 7 days until

0.008% Na,S2O3? Store in 40 days afterStore in dark dark extraction

Purgeable .AromaticHydrocarbons S "" S Cool,4°C Cool,4°C 14

0.008% Na2SHC1 to pH<2

Purgeable .Halocarbons S S . Cool,4°C Cool,4°C 14 days

0.003%

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Table 2. Containers, Preservation, storage, and Holding Times*(COND'T)

G « A«oS°i'4!C a Oool °C 7 days until/°'°°?% "a2s2°3g 40 days after1 ' " J extraction

Total OrganicCarbon G G Cool,4°C Cool,4°C 28 days

HCl or H2so4to"i>H<2

Total Organic ;Halogen G G h Cool,4°C Cool,4°c 7 days

|( HN03 to pH<2 yVolatile Organic ' • • • " * ; -

| Compounds G G Cool C Cool,40c 14 daysTetrachloroethylene ; m ?,,.••: :

ITrichloroethylene ^ , - -i; Hr . . '1,1,1-trichloroethane V ;; "

. 1,1-dichloroethylene r>1- >trans-l,2-dichloro- ^ :ethylene G G , Cool,4<>C Cool,4°C .10 days

Total Petroleum • 'Hydrocarbons p rP ,Cool,4«C Cobl,4°C 10 days

., *Y tfVJPh ; A_ — . _ _ • • - ' . . . ™

H2sr4

NOTES Analytes not listed should "be preserved at 4°C and held noti ...xonger than.7 days. ~ "1 - . . ; - ' . . - : ; . - -.*.-.::

/ . . ., ri .....;..:':,jr.fsriH." !••

flRltOOI*86

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Table 2 - References/Definitions

a •' " ' •'- - ' 'a Preservatives and holding times are from Federal RegisterVol. 49, No. 209, Friday, October 26, 1984, Page 432607and Characterization of Hazardous Waste Sites: £ MethodsManual—-Volume II. Sampling Methods. Second Edition.EPA-600/4-84-076. „ Container requirements are consistentwith these references.

b P - PolyethyleneG » Amber Glass with Teflon-lined capS - Glass Vial with Teflon-lined septum cap •

c Sample preservation should be performed immediately uponsample collection. For composite samples, each aliquotshould be preserved at time of collection. When use ofan automatic sampler makes it impossible to preserve eachaliquot, samples may by preserved by maintaining at 4°Cuntil compositing and sample splitting is completed.

d .When any sample is to be shipped by common carrier orsent through the U.S. Hall, it must comply with Dept. ofTransportation Hazardous Materials Regulations (49 CFRPart 172). The person offering such material for trans-portation is responsible for ensuring such compliance.For the preservation requirements in this table, theOffice of Hazardous Materials, Materials TransportationBureau, Dept. of Transportation, has determined thatthe Hazardous Materials Regulations do not apply to thefollowing materials! Hydrochloric Acid (HCl) in watersolutions at concentrations of 0.04% by weight or less(pH about 1.96 or greater); Nitric Acid (UNO*) in watersolutions at concentrations of 0.15% by weight or less•(pH about 1.62 or greater); Sulfuric Acid (H2SO4) inwater solutions at concentrations of 0.35% by weight orless (pK about 1.15 or greater); and Sodium Hydroxide(NaOH) in water solutions at concentrations of 0.080% byweight or less (pH about 12*3 or less).

e Samples should be analyzed as soon as possible aftercollection. The times listed are the maximum times thatsamples may be held before analysis and still beconsidered valid. Some samples may not be stable for themaximum time period given in the table. A laboratory isobligated to hold the sample for a shorter time if know-ledge exists to show this is necessary for sampleintegrity.

* If samples cannot be filtered within 48 hours, add 1 mlof a .2.71% solution of mercuric chloride to inhibftbacterial growth. .

9 Should only be used in the presence of residual chlorine.

JIRI»OOI»87

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l

Table 2 - References/Definitions(continued)

n Maximum holding time is 24 hours when sulfide is present.Optionally, all samples may be tested with lead acetatepaper before pH adjustment in order to determine ifsulfide is present. If eulfide is present, it can beremoved by addition of cadmium nitrate powder until anegative spot test ie obtained. This sample is filteredand then NaOH is added to pH 12.

* . - v.- • -: - •>, i* t. .. " -' - ' " ' '1 For dissolved metals, filter immediately on-site before

adding preservatives. f;ct ' , *

J Guidance applies to samples to be analyzed by GC, LC or,GC/HS for specific compounds.

* The pH adjustment is not required if acrolein will notbe measured. Samples for acrolein receiving no pHadjustment must be analyzed within 3 days of sampling.

" ' '' ' ' . , , ' - . • • • -t-* ;-i ) ".' '••'-. ' ' • :• . '• - ' -1 When the extractable analytes of concern fall within a

single chemical category, the specified. preservativeand maximum holding times must be observed for optimumsafeguard integrity. When the analytes of concern fallwithin two or more chemical categories, the sample may bepreserved by cooling to 4°C, reducing residual chlorinewith 0.008% sodium thiosulfatc, storing in the dark, andadjusting pH to 6-9; samples preserved in this manner maybe held for 7 days before extraction and 40 days afterextraction. Exceptions to this optimal preservation andholding time procedure are noted in footnotes 9, * and n.. . \ ' 4 , -•

* If 1,2-diphenlyhydrazine*is likely to be present, adjustthe pH of the sample to 4.0 ± 0.2 to prevent rearrange-ment to benzidine. . <::-.;•:. ': ' '- 4 "" - "

„ • ' " ''v'Vtd'r-,- • ":n Extracts nay be stored up to 7 days before analysis -if

storage is conducted under an inert (oxidant free)* atmosphere. V< - >-f^\ •••••.r . '.-.••..". i"! « - . - - •0 For the analysis of diphenylnitrosamine, add 0.008%

Na2S2O3 and adjust the pH to 7-10 with NaOH within 24hours of campling. r-

The pH adjustment may be performed upon receipt at thelaboratory and may be omitted if the samples are extractedwithin 72 hours of collection. For the analysis ofaldrin, add 0.008% Na2S2O3.

Sample-receiving no pH adjustment must be analyzed wifchin7 days of sampling.

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Section 13. APPROVALS FROM OTHER AGENCIES

Federal

o metaTRACE is participating in the USEPA's ContractLaboratory Program (CLP) for organics analysis and rapidturnaround dioxin analyses(Contact: Angelo Carasea 202/382-7906)

o metaTRACE has been licensed by the US Nuclear RegulatoryCommission to perform analyses on co-contaminated wastes(both chemical and radiological)

o metaTRACE is certified by the US Army Toxic fi HazardousMaterials Agency (USATHAMA) for a wide range of parametersunder the CLASS contract(Contact: Douglas Stevenson 301/671-3348)

o metaTRACE has been certified by the US Navy Energy andEnvironmental Support Activity (NEESA) to perform analyticalprograms at Naval installations. This certification alsoapplies to US Air Force programs.(Contact: Mitzi S. Miller 615/576-2361)

o metaTRACE has been certified by the US Army Corps ofEngineers Missouri River Division.(Contact: Ann B. Strong 601/634-3600)

• States

o State of New Jersey (Contact: Andrew Fishman609/292-3950)

o State of New York (Contact: Matthew Caruso518/474-8519

o State of California (Contacts Fred Seto415/540-3003)

o State of Missouri (Contact: Jerry Lane 314/751-6400)

o State of Florida (Contact: Howard Rarick 904/359-6449)

o State of South Carolina (Contact: R. Wayne Davis- - 9803/737-7025)

o State of Wisconsin (Contact: Ron Arneson 608/237H7133L)

o State of Tennessee (Contact: Charles Mickle 615/262-6354)

ARttOO<*89

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1

1

11II

Section. 14. DOCUMENT CONTROL

The varied activities of toetaTRACE require many forms ofdocument control to provide completeness and traceability,clear sample identification and chain-of custody information,confidentiality, current 'technical and QC proceduredescriptions, and retrieval of information. Documentsgenerated include computer programs, lab data sheets,,technical drawings, official project memos and reports. TheStandard Operating Procedures address document controlprocedures appropriate to each technical work area; generalinformation is provided in this section.

Measures to Ensure Completeness and Traceability

Notebooks and standardized data forms are used, and logs ofgathered data and its sources are maintained to ensurecompleteness and traceability. Bound and paginated notebooksare used for laboratory analysis. The notebooks are page-numbered in single-or double- page versions; the pagenumbering ensures that data is not removed or added.Completed pages are dated and witnessed. ' The double-pagebooks are used with carbon paper to provide a copy of thedata* The Laboratory Standard Operating Procedures containdetailed sections on laboratory notebook use.

Standardized data forms are designed to gather the completeset of data needed for a particular technical activity.Telephone Conversation Reports, and Instrument CalibrationSheets are examples of the many types of data sheets used bymetaTRACE's staff members. The standardized forms alsoensure the comparability of data gathered by different peopleworking on the same task.

Document control of data gathered from various sources ismaintained by keeping a record or log of all the data. Thelog includes the title and/or description of each item, itssource and/or author and the date it was received. It isuseful to number each data item and provide a keywork orother very brief summary of the contents.

Project Document Inventory

Some projects require the compilation of a document inventorycontaining all project documents. EPA's National EnforcementInvestigations Center (NEIC) has outlined requirements forthis type of document control in two publications: "NEICPolicies and Procedures Manual* and "EnforcementConsideration for Evaluation of Uncontrolled Hazardous WasteDisposal Sites by Contractors.*

flRlt.OOI»90

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metaTRACE follows the rigorous NEIC requirements whenappropriate. They include the designation of a Document

J( Control Coordinator and the identification of accountabledocuments. Preserialized sample identification tags andchain-of-custody records are used and a unique project code

i is used for all project documents.

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1t Section 15. QUALITY ASSURANCE REPORTS TO MANAGEMENT

'\— ; Internal Reports

The QA Manager prepares written quarterly reports on QC .* activities for the Laboratory Technical Director and otherI laboratory managers. .These reports detail the results of QA

procedures, problems encountered, and any corrective actionwhich may have been required. All Corrective Action Formsare submitted to the QA Manager for initial approval of, theplanned corrective action, and a copy is provided to theTechnical Director. All system audit reports are provided tothe Technical Director. ' •

Reports to Client

Each data transmittal will-contain a summary of QA/QCactivities; this summary will include:

o estimates of precision,7 accuracy and completeness of data

o reports of performance and system audits

o quality problems found "

o corrective actions taken

The final report of data will include a summary of QA/QCactivities during the project. The QA Manager is responsiblefor the preparation this report.

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I - leUTRACE Precision. Ac cur icy anri Coopleteness Objectives

Parameter Method Matrix Precision Accuracy Coepleteness(RPD) (1) (Z)

Antioony 200.7 Hater (20 BO-110 90200.7 Soil (23 75-113 90

Arsenic 206.2 Hater <20 60-130 90206.2 Soil <23 55-135 90

brim 200.7 Hater (20 65-113 90200.7 Soil <25 BO-120 90

Berylliui 200.7 Hater <20 85-110 90200.7 Soil <25 BO-113 90

Catlflioo 200.7 Hater <20 B5-110 90213.2 Soil <25 75-125 ; 90

Chroftiuo 200.7 Hater (20 BO-110 90200.7 Soil <25 75-115 90

Cobalt 200.7 Hater <23 60-110 90200.7 Soil <30 73-113 90

Copper 200.7 Hater <20 BO-110 90200.7 Soil (23 73-115 90

'Iron " 200.7 Hater <20 BO-115 90200.7 Soil <25 75-120 90

Lead 200.7 Hater (20 60-110 90239.2 Soil <23 70-123 90

Rercary 245.1 Hater <20 75*120 90243.1 Soil (23 70-123 90

.Hickel. . . • - . - . . . .200.7 - • -Hater . ... -<23 ' .-9IMIO - -90" • ' 200.7 Soil * . (30 83-113 90

Selenittft ' 270.2 Hater <20 60-130 90270.2 Soil <23 53-133 90

Silver . MO. 7 Hater (20 70-115 90200.7 Soil <25 65-120 90

#

ThalliDi 279.2 Hater <20 70-123 90279.2 Soil ' (25 65-130 _ . 90

Tia 282.2 Hater . NO Not Available Hot AvailableH2.2 Soil HD

200.7 Hater <20 65-110 90240.7 Soil (25 * BO-US 90

1 t

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- MtiTRACE Precision, Accuracy and Completeness Objectives

Paraneter Dethotf Nilrlr|^v Precision- Accaracy tapletentsiIRPDI U) (I)...

' linc »0.' fatir<? (20 90-115 90200.7 Soil u> (25 85-120 W

•! Cllciui NO.? '"*tir;;; " (20 65-120 90200.7 Soil - (25 80-125 90

Ma9°esi« 200.7 Hater & <20 85-110 90"' . 200.7 Soil — <25 80-115 90

. Manjanese 200.7 later — (20 , 60-105 904 200.7 Soil K< (25 75-110 90

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' - oelaTRACE Precision, Accuracy antf Coapleteness Objectives

Parameter tletbotf Natrii , Precision Accuracy Completeness(RPD) ID II)

Acidity 350.1 Hater <20 60-120 90350.1 Soil (30 75-125 90

Alkalinity 310.1 Hater (20 80-120 90} 310.1 Soil (30 75-123 90I

Antoni a 420.0 Hater (20 90-110 90-, 120.0 Soil (30 60*120 90

BTU ASM DBOB Hater <20 80-120 90ASM OB09 Soil (30 75-123 90

I Broslde 300.0 Hater (20 60-120 90i 300.0 Soil (30 75-125 90ii Chloride 300.0 Hater (20 75-110 90

300*0 Soil (30 70-113 90

I COD 410.4 Hater (20 BO-110 90410.4 Soil (30 70-120 90

Fluoride 300.0 Hater (20 75-110 90300.1 Soil (30 70-113 90

i Fluoride ' 340.2 Hater KB HD NO340.2 Soil HD KD HD

T Flashpoint 1010 Hater <20 80-120 901010 Soil (30 73-123 90i

Oil ane* Grease • 413.1 Hater (20 70-120 901 413.1 Soil (30 60-130 90I '

(titrate 300.6 Hater (20- • . 70-120 90i 300.0. Soil (30 60-130 90

pH 150.1 Hater (20 1U 90150.1 Soil (30 HA 90

lion-Filterable Residue 160.2 Hater (20 BO-110 90160.2 Soil (30 70-120 90

aFilterable Dissolved Solids 160.1 Hater <20 BO-120 90

160.1 Soil (30 70-130 90

Sulfatf ~ 300.6 Hater (20 65-110 90300.0 Soil (30 75-113 90

* Total Cyanide 335.2 Hater (20 • 60-110 903J5.2 «-" * 70-120 90

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1 - netaTRACE Precision, Accuracy and Completeness Objectives

Paraneter ^ Method Matrix :i*v1 Precision Accuracy CoapletenessK -^ IRPDI m m

Total Phenols 420.1 Hater (20 60-120 90; 420.1 Soil '•> (30 50-130 90

* -

L Sulfide 376.1 Hater:;! NO NO KDt 376.1 Soil ND ND ND

j TOC 415.2 Hater::,- (20 60-110 90n 415.2 Soil (30 70-120 90j • . -:• • fl'-> - - ' .'.:"••

TQI 450.0 Hater ' (20 70-120 90• 450.0 Soil (30 60-125 90I r. ' , ^ • '• -' Phosphorous 365.4 Hater (20 80-120 90| 365.4 Soil . (30 70-130 90

\ Specific Brivity 213E Hater (20 60-120 90i 213E Soil ^ ; (30 70-130 90

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\ - oeta TRACE Precision, Accuracy and Coapleteness Objectives

.,

Parameter Method Matrii Precision Accuracy Coapleteness(RPD) II) (I)

1,3-Dinitrobenzeiie USAT»AKA Hater (30 20-70 85US07

USATHAHA Soil (40 55-120 85IHM ;

1,3,5-Trinitrobenzene USATHAflA Hater (30 ' 10-55 85UW7

USATHAHA Soil (« 40-110 85LK07

2,4-Dinitrotoluene USATKAHA Hater (30 55-125 83UH07 >

USATHAttA Soil (40 75-123 65LH07

2,6-Dlaitrotoluene USATHARA Hater (30 60-120 65IW07

USATHAHA Soil (40 70-113 83LH07

Nitrobenzene U5ATHAW Hater (30 20-60 85 \JUK07 ^

USATHAHA Soil (40 35-125 85"U07

2,4,4-Triaitrotolitene USATKAKA Hater (30 50-110 851W07

USATHAHA Soil (40 70-120 83LH07

''sticides:4,4-DDT 608 Hater * (30 70-110 83

6080 Soil (50 33-120 83t

AldrU 608 Hater (20 75-110 836080 Soil (30 ' 65-120 63

^ Bieldrii - 608 Hater (20 70-110 ' 858080 Soil (30 65-120 83

* Endrin ' 608 Hater (20 75-110 838080 Soil (30 60-120 63

, Heptacblor 606 Hater (20 73-100 856080 Soil . (30 63-110 JB5

Lindane 608 Hater (20 70-110 851 8030 Soil (30 60-120 . 83

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3 * netaTRACE Precision, Accuracy and Completeness Objectives

Parameter ..... ,~,. Method Natrh " Precision Accuracy Completeness^ HV IRPD) III U)

0s (as Aroclors) 608 Hater ' <20 65-125 8080BO Soil (30 60-125 60

£>' .DO/PCOf 8280 later - ' (40 40-120 65

8260 Soil (40 40-120 . 65

ARIfOOit98

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- netaTRACE Precision, Accuracy and Conpletenesi Objectives

Paraaeter Method ftatrli Precision Accuracy Completeness(RPD) U) 111

' laliles:Toluene d8 624 , Hater (15 80-130 90

6240 Soil (25 HD 90i

Bronofluorobenzene 624 Hater (IS 80-130 90' . 8240 Soil (25 NO 90

'> l,2-Dicbloroethane-d4 624 Hater (15 80-120 90! 8240 Soil (25 ND 90

I ai Volatiles:I Wlrobeniene-dS 625 Hater (30 20-100 85

8270 Soil (50 40-90 85L: 2-Fiuorobiphenyl 625 Hater (30 30-120 85

8270 Soil (50 40-80 85

* Terphenyl-dl4 625 Hater (30 50-140 65I * 8270 Soil (50 BO-150 65

1 Pfaenol-dS 623 . Hater (40 20-100 858270 Soil (60 10-50 85

i2-FJuoropbenol • 623 Hater (40 20-120 65

' 8270 Soil (60 10-60 85i

2,4.6-TriirosophMol 623 Hater (40 80-120 65*t 8270 Soil (60 40-110 85

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netaTRACE Precision, Accuracy and Coapleteness Objectives

Faraoeter Method Matrii Precision Accuracy Cospleteness' .'<. !'<-••.*' IRPDI m .m*' -litlies:

1,1-dicbloroetbene CLPi „ Hater') (14 61-145 85ttPi Soil-> (22 59-172 85

»' ••Trichloreethene CLPi Hater "•> (14 71-120 85

CLP» ; Soil i--- (24 62-137 65

1 Chlorobenzene CLP* Nater^ (13 , 75-130 85 •CLP« Soil ^ > (21 il 60-133 85

i Toluene CLP* ' HaUr^;> (13 76-125 85OPt Soil S"-> <2| 59-139 65

f Benzene CLP* Hater **> (II 76-127 65OP* Soil £•:• (21 M-142 85

e-«-Volatiles: i ,> • •1,2,4-trichlorobenieoe CLPt Hater1 (28 39-98 85

Soil (23 SB-107 85

later (31 46-118 85CLP> Soil (19 31-137 85

2,4-dioitrotolvene . CLPi Hater <3B 24-96 65CLP« Soil (47 28-6? . 85

PyrtaB on »**- <31 26-127 65(36 35-142 85

«e 41-116 15CLPi Soil (38 41-126 15

1,4-diChlorobenzene <nar. «„„ n !«,-«»„;

CLf* ""r «0 9-103 K<« 17-109 B5

<« 12-87 85<35 26-90 85

\ 2-chleropnenol " ' ' apt"tf 25-102 85

<« 23-97 B3' <55 ' 26-ID3 85

<30 10-80 85foil <50 IHH ,3

flfil* 00500

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- aetaTRACE Precision, Accuracy and Coopleteness Objectives

Paraneter Method Hatrii Precision Accuracy Completeness(RPD) U) (Z)

r tes: ' . .S ;Ufcriation obtained fron USEfA Contract Laboratory Progran

L, Dilative Percent Difference

)=Hol Determined

v=Hol Available

"1 precision and accuracy objectives are based UOM historical laboratory results.

•! sticidesiLiodane CLPi . Hater (15 56-123 65

CLPi * Soil (SO 46-127 85

I Heptacfalor CLP* Hater (20 40-131 65CLP* Soil. (31 35-130 - 85

i Aldrin CLP* Hater (22 40-120 85CLPi , Soil (43 34-132 65

,1 DieldrU CLPi Hater (IB 52-126 65| CLP* Soil (36 31-134 85

I Endrin CLP* Hater (21 56-121 63* CLPi Soil (45 42-139 83

4,4'-DBT CLPi Hater (27 38-127 BSt aPi Soil (SO 23-134 85

ARU0050I

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SECTION 4.0 EQUIPMENT CAPABILITIES' - ' * '

FIELD SAMPLING AND ANALYSIS EQUIPMENT

Alliance maintains an extensive inventory of air, water, soil and waste field samplingand analysis equipment and has ready access to instruments owned by other TKCcompanies. All equipment is stored in o central location and is maintained andcalibrated on a regular schedule in order to ensure reliable data and prevent costlydelays. Before equipment is sent out on, an assignment, it is calibrated according tothe manufacturer's recommendations end worn or broken parts are replaced. .Equipment in the field is tracked as to the assignment for which it is being usedand the date it is expected to be returned. This ensures that equipment is availablewhen needed. In the field, equipment is re-calibrated before each use to make surethat any loss of accuracy due to transport has been corrected and to take intoaccount temperature and humidity changes. When equipment is returned, it islogged in, checked for damage, cleaned and repaired as necessary and relumed toequipment inventory, ready for use again. Table 4.1 presents an itemized list ofavailable equipment.

The equipment and facilities described in Table 4.1 are available for all projects usneeded. If required, additional support equipment, including carpentry and machinetools, is also provided. Alliance can design and construct specialized apparatus formonitoring, sample collection, and chemical characterization ot virtually tiny *iic.

MOBILE LABORATORIES

Alliance maintains two mobile laboratories for use in projects requiring onsileanalysis. Each can be set up for waste, water, soil and sediment analyses. Inaddition, Alliance's Environmental Monitoring Trailer is available for long-termmonitoring assignments. Alliance's Mobile Lab can be used for onsite analyticalactivities conducted for the duration of any long-term project. This 47.S ft x 7.5trailer was custom designed and equipped to specifically handle onsite analyticalrequirements. The laboratory con be equipped with organic and/or inorganicinstrumentation, as required, and was designed with adequate bench, top andcounter space to allow for such possibilities. A second, small laboratory

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custom-built for Alliance by Design Space International. The 16 x 8 ft trailer wasdesigned so that instrumentation equipment can be easily placed into an existingrack mount. Numerous configurations cnn be assembled along with data acquisitionsystems and strip chart recorders.

HEALTH AND SAFETY EQUIPMENT

Alliance has considerable experience In preparing hazardous waste site health andsafety plans, and can provide qualified, experienced personnel to serve as onsitehealth and safety coordinators. Alliance also maintains an adequate inventory ofhealth and safety equipment for outfitting crews and monitoring potential exposuresto hazardous and toxic materials (Table 4.2). This inventory is centrally maintainedand is automatically reordered as stocks are depleted, which enables Alliance crewsto quickly respond to concurrent site assessments without delays due to a lack ofproper health and safety equipment.

flRl+00503

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TABLE 4.1 FIELD SAMPLING AND ANALYSIS EQUIPMENT

Item , Manufacturer Quantity

v, -

Wastewater Sampler, automaticsequential/composite I SCO Model 2100 • • . •-. , **

Recording Flowmeter • I SCO Model 1870 .. 2

Sampling Pumps Cole-Farmer 6

Kemmerer Water Sampler VlldCo 2

Water Sewage Sampler VUR Scientific 2

Portable Field Laboratory Hach DR/EL 2 ,2

Dissolved Oxygen Meter Yellow Springs Instrument Co. 2

Conductivity Test Meter Hach Chemical Co. r ; 2

pH/nV Meters Orion Research Model 701A ; 3

Ultrasonic Flowmeter Dynansontci ; 1

Wastewater Sampler, automatic Quality Control Equipment Co.,/, ... - .Model CVE-76 c tv , 2• * • • "

Water Sampler >,, .«-3,, ,,'poran v . 2 :•

Ground Water

Submersible Pumps ' ' ' IEA " 1

Peristaltic Pumps ISCO 5„.,. ,.,,.n rs., j.,;/.: r ' v v"- , : ' -= r -s-

Teflon Sample Lines Assorted Assorted

Bailers, Teflon/Staonless Steel T1HCO 15

Water Level Indicators Johnson UOP 2

(Continued)

AftltOOSOti

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TABLE 4.1 (Continued)

Item Manufacturer Quantity

Sediments

Petit Ponar Dredge VildCo -. 1

Peterson Dredge VildCo 1

Sediment Corer • VildCo 1

Soil/Solids

Stainless Steel Soil Auger 2

Split Spoon Sampler . 1t *

Hazardous Material! ' ..:

Apparatus for CompatibilityTeating-pH, Redox, flammabllity,water reactivity, cyanide, sulfur 2

Collwasa, Teflon and GlassSludge Samplers 6

HP 5840A (ECD, FID) Hewlett-Packard 1

PE 3920B (ECD. FID) Perkln-Elmer 1

HP 5890 (ECD, FID) Hewlett-Packard 1

AID Model 511 GC Analytical Inst. Co. 1

Carls 9704 GC Carle 1

Orion 701A pH/mV Meter Orion Company 1

Non-dispersive 1R (CO) Bendlx 2

Non-dispersive IR (CO) Monitor Labs 2

(Continued)

flRlfOOSOS

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TABLE :4.1 (Continued)

Item ' ::-*^--*i Manufacturer Quantity

NO/NO, Chemiluminescent Gases Monitor Labs * 5

Flame lonlzatlon (Hydrocarbon) Bendlx 2

Oa Chemiluminescent Gases Monitor Labs 4

Gas/dilution Calibrator ^ Monitor Labs 1

Fluorescent S0a Monitor Labs 8

Flarne-lonlration OVA ):Foxboro 2

Photo*lonlratlon Detector ' HNU Corp. f 3

Photo-lonlzatlon .. ' Photovac 1

Vacuum Hl-Vol General Metals 10

Recording Respirable Dust Monitor 'HIE Model RDM-301 1

Respirable Dust Monitor ^ r ; «IE Model RDM-101 11 • ... ' ,.,! V'i- "I'''

Particle Mass Monitor HIE Model RDM-201 - . 1

Ambient Particulate Mass Monitor HIE Model AFM . 2

Fibrous Aerosol Monitor j ^^MIE FAM 2

Real-Time Aerosol Monitor MIE RAM 2

Direct Weather Measure 2

Thermistor Weather Measure • 2

Direct Climatronlcs 2

Sulfur Dioxide Monitor Monitor Labs Model 8850 2

Sulfur Dioxide Monitor Thermo Electron Model 43 3

(Continued)

A V-G .'1-' '

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TABLE 4.1 (Continued)

Item Manufacturer Quantity

NO/NO. Monitor • Monitor Labs Model 8840 2

NO/NO. Analyzer Thermo Electron Model 14 DE 2

Carbon Monoxide Monitor Ho rib a Instruments 1

Carbon Monoxide Monitor Ecolyzer . 5

Dynanlc Calibrator •-- 1

Hydrocarbon Analyzer Bendlx 2

Dlchotonoua Sampler Sierra Instrument* 2

Recorders Soltec 3

Permeation Tube Water Bath --- 1

Instrument Shelters EKTO I

Hi-Volume Air Samplers General Metal Works ModelCMWL-200 20

Portable Calibration System Monitor Labs Inc. Model 8500 2

Wind Speed and Direction Sensorswith Expanded Recorder' Cllmatronics 1

W00507

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TABLE 4.2 FIELD SAMPLING AND ANALYSIS EQUIPMENT

Item ;- Manufacturer . Quantity

personnel Safety *• :^; :

Personal Monitoring Pump ' HSA Monltalre, Model S 6. . i • ': ! ''-I'-' <i'*''1

Personal Monitoring Pump .DuPont F-125 1C

Personal Monitoring Pump . DuPont P-4000 10

Stain Detector Tube Kit Bendix Model 8014K 2

Stain Detector Tube Kit . f Drager Model 31 2

Combustible Gas/0s Analyzer ''Energetics Science Model 60*400 2

Portable Organic Vapor Analyzer . Century Model OVA"-108 2

Fhotolonlzatlon Analyzer HNU Model PI-101 4

Respirator Fit Test Stations GCA . 2

—•/ Tyvek Protective Clothing Helco Assorted

Chemical Resistant Coveralls Helco 12

Full-Face Respirator, Ultra-Twin ^ HSA 12

Comfo II, Half-Face Respirator ' ' USA- ' . _,., 20

Self-Contained Breathing Apparatus MSA Model 401 6

Cascade Breathing Air Systems , . ^ ' 2

Respirator Cartridges :l- ;'? ^ ' -KSA ; , , -Assorted

First Aid Kits' : ^ Helco „ - .. • . Assorted

ARlfOOSOS

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COMPUTER CAPABILITIES

The Alliance team routinely uses computer programming and data processing insupport of contract work across a wide range of technical areas. Microcomputers,minicomputers, and mainframes are all employed as necessary for a spectrum ofapplications including data base management, modeling, graphics, accounting,project management/ data entry, and technical publications. All Alliance teamcomputer systems can readily communicate with outside microcomputers,minicomputers, and mainframes to exchange information using communicationhardware and software systems available in-house.

The extensive computer resources of the Alliance team are supplemented by thebroad experience of our computer applications staff, which includes computerprogrammers, systems analysts, environmental scientists, engineers, and projectmanagers. This diverse team of professionals offers a wide range of approaches todata processing and management, including a thorough evaluation ofmicro/mini/mainframe alternatives and existing software versus tailored softwaredevelopment.

Computer Hardware ond Graphics

Alliance has access to the TRC Companies PRIME 2655 computer and theNational Computer Center (NCC) IBM 3090 and VAX cluster, bibliographicdatabases such as DIALOG, NJH/EPA Chemical Information System, TOXLINC,and various other service bureau systems. Alliance has Installed a high-speedtelecommunications link to the NCC which allows output from completed jol* ID beprinted locally rather than off-site. A Dataproducts LB-615 600-line-pcr-minuteband printer is connected to a dedicated high-speed data line through a Racal-Milgo9600 baud modem. Alliance completed a major upgrade in its data communicationssystem involving the installation of high speed communication links, including nHarris 1600 Series remote job entry (RJE) station, a Harris 9300 communicationscontroller with a 118 megabyte hard drive, a tape backup system and a local arennetwork, and a 600 line-per-minute line printer running RJE/SNA protocol. IBMPC/XT microcomputers are connected to the network to facilitate filflfihloaltfhdownloading from host systems. Other communication links include Digital DEC-

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writers and CRTs operating at 2400 baud, IBM PC/XTs equipped with 2400 baudHayes Smartmodems, and portable IBM and IBM-compatible microcomputers with2400 baud modems. .s jr

In general, the Prime or NCC IBM is used for the analysis of very large data basesusing SAS (Statistical Analysis System), FORTRAN, COBOL, PL/1, and otherscientific and database software packages. For less resource-intensive activities,Alliance uses microcomputers. These machines are widely used for bothindependent applications and applications involving communication with mainframe,mini- and microcomputers. The majority of technical computing is done onAlliance's more than 60 PC-XTi and PC-ATs, many of which are equipped withmath coprocessors, graphics boards,-and 1 MB RAM. • This makes them ideallysuited for a wide range of data analysis, modeling, data base management, andsoftware development applications. /; y

Hardcopy draft output is provided by Epson and Epson-compatible dot matrixprinters. When necessary, higher quality printouts are obtained using a host of iii-house letter-quality printers including IBM Quietwriters, NEC Spinwriters, and aXerox 4045 laser printer. Alliance olsp has three Hewlett-Packard LaserJet laserprinters tied into its networks and one Hewlett-Packard LaserJet Series II as itstand-alone device.

Alliance has developed & state-of-the-art graphics system to support its statisticaland modeling efforts, facilitating rapid data manipulation, evaluation of modelresults, and presentation of final figures, and providing high-quality graphic outputat minimal expense. For most graphics applications, Alliance uses a Tektronix 4112graphics workstation, a 16-bit CP/M-86 CPU with more than 400K RAM, a 10-megabyte hard disk and an 8" floppy drive; this workstation operates in bothgraphics and text modes. For other graphics applications; Alliance has access to 2other Tektronix terminals, PC ATs with VGA monitors, 2 Hewlett Packard 7550A8-pen plotter, and a Hewlett Packard LaserJet Series II laser printer. The HP 8-pen plotttcrs feature 0.001 inch resolution, automatic paper feed, variable penspeeds up to 80 cm/sec, and their own graphics language, and can produce highquality plots on 8.5 x 11 inch or 11 x 17 inch paper or transparencies. Highresolution plots can also be produced at the National Computer Center on EPA'sCALCOMP plotter. The graphics system also includes a digitizing tablet and aTektronix 4612 hardcopy unit, which produces black and white copies fiiifficieiff fan

flfttOOSIO

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most draft reports and many final figures. Alliance also uses a COMPAQ 386-16with 2 MB RAM, a 40 megabyte hard drive, an EGA monitor, and an 80387-16math coprocessor for graphics applications.

Software

Alliance programmers have access to, and familiarity with, virtually all majorprogramming languages and software packages for organization, maintenance, andmanipulation of data, FORTRAN 77, PASCAL and BASIC are are among thelanguages supported on TRCCs Prime. Users of the NCC IBM and VAX haveaccess to a wealth of programming languages, software packages, and utilityprograms. SAS and SAS/GRAPH, FORTRAN, PL/I, and COBOL are among themost routinely used languages; BASIC, EASYTRIEVE, and NATURAL alsoemployed.

*Microcomputers at Alliance utilize widely available software such as LOTUS 1-2-3,dBASB HI PLUS, Autocad, Venture Publisher, STATPRO, and a host of additionalpackages for data base management, graphics, accounting, project management, dataentry, and word processing.

Technical Publications

Alliance maintains separate and complete Technical Publications Departments forrapid and efficient turnaround of all technical reports and other projects in theChapel Hill and Bedford offices. In Alliance's Chapel Hill office, the TechnicalPublications Department has 3 IBM-compatible microcomputers for wordprocessing,also using WordPerfect 5.0. These wordprocessing stations also have VenturaPublisher, Lotus, and dBASE III capabilities. A XEROX 4045 laser printer is usedfor document quality printing. Alliance's Chapel Hill office has two PitneyBowes D750 high volume copiers which have a monthly volume of 60,000 copieseach. This equipment provides for rapid and efficient turnaround on the reportsand documents which Alliance delivers to its clients.

The Bedford Technical Publications Department is equipped withsix IBM-compatible microcomputers using WordPerfect 5.0, the cotyoratewstanuartl

v*

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for word processing. The Document Production section has a Sun 386i workstationwhich acts as a network flip server for a Macintosh desktop publishing system andIBM-compatible microcomputers. The Sun 3861 has both MS-DOS and Unixoperating systems. The workstation runs Frame Maker to create final documents byelectronically merging text and graphics, and outputs hard copy to a laser printer.The main graphics program for drawings, charts, 35mm slides, overheadtransparencies and graphs is MacDraw II. In addition, the Alliance Bedford officehas a Kodak Ektaprint 300 high volume duplicator and complete binding facilities.The Kodak duplicator has a 500,000 copy per month capacity.

TRC FACILITIES AND EQUIPMENT

TRC has consolidated support facilities at its East Hartford, Connecticut corporateheadquarters and adjacent environmental laboratories. These facilities include:

• Computer Laboratory/Polo Reduction Facility_ _ _ . . . . - ; - • • , jVfiT':TRC maintains several in-housc computer systems, external communications links,and software for data handling find analysis.

PRIME 2655 Computer • This system includes 8 megabytes of memory, 315 and496 megabyte disc drives, a streamer tape system, a high speed printer, a matrixprinter/plotter, and 12 FT/200 terminals, including graphics capabilities.FORTRAN 77, PASCAL, and BASIC languages are supported. This computerhas Remote Job Entry (RJE) and is linked by a dedicated line to U.S.Government computer facilities (National Computer Center) in Research TrianglePark, North Carolina. The RJE fa clso capable of being switched for high-speedcommunication with most other computer cites required for any project.

Microcomputers * TRC has a complement of microcomputers and intelligentterminals as part of its in-house 'facilities. These include IBM and IBM-compatible XT and AT PCs. To enhance the output of the PCs, TRC has alaser printer and plotters that can plot up to a size D. The microcomputers arecapable of establishing communication links with other micro-, mini-, andmainframe computers at speeds up to 9600 baud. Microcomputer softwareroutinely used at TRC Companies can be found in Table 4.3.

Afi<(005l2

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TABLE 4.3. SAMPLE OF MICROCOMPUTER SOFTWARE ROUTINELYUSED AT TRQ COMPANIES

OPERATING SYSTEMS; DOS (VERSION 3.3)DOS (VERSION 3.0)CP/M-86

PROGRAMMING LANGUAGES/COMPILERS: MICROSOFT FORTRANMS BASICMICROSOFT C

. . PASCAL

COMMUNICATIONS SOFTWARE: SMARTCOM IIPROGRAMMITE CROSSTALK XVI

DATA BASE MANAGEMENT SOFTWARE: DBASE IIDBASE III PLUSDBASE IVRBASECLIPPERDATA BASE MANAGER IIPFS FILEREFLEX

SPREADSHEETS: LOTUS 1-2-3SUPERCALC

GRAPHICS/STATISTICAL SOFTWARE: LOTUS 1-2-3STATPROSURFERSYSTATRATS ,SASAUTOCADEASYFLOWHARVARD

1 , PACEMAKERPC-PAINT .

> ; £U , -.--* '

A D !• n n r- . *

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TABLE 4.3. SAMPLE OF MICROCOMPUTER SOFTWARE ROUTINELYUSED AT TEC COMPANIES

WORD PROCESSORS/EDITORS: , . -; 1? r;..''.= .,.. ,,.,; , MULTIMATE

,1 WORDSTARWORD PERFECT

7 PFS WRITEEPSILON

' . •. .. ; . ; ut I RE2 "- ' " "• ; 'MISCELLANEOUS: NORTON UTILITIES ;

'(DATA RECOVERY/DISK MANAGEMENT)tNTRYPOXNT . , . . - - *i(DATA ENTRY)

ARliOOSU

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Cooperative Agreements * Our in-house facilities are augmented by cooperativeagreements with NTIS (National Computer Center), Combustion Engineering, , jInc., United Technologies Research Center, and United Computing Systems, Inc.These agreements provide TRC with access to IBM, CDC, CRAY, and UNIVAChigh-speed mainframe computing systems.

Data Handling - Data reduction facilities include in-house standardized datareduction computer programs developed to facilitate data processing. Tlteprograms allow for the capability to retrieve data from remote data loggers viadial up telephone lines connected to microcomputers and intelligent terminals.The system also allows for interactive verification, validation, and editing of thedata collected and processed using TRC computer and data reduction equipment.Data reduction equipment is used to convert aerometrlc strip chart data intohourly averages which, in turn, are processed by data reduction software.

Plotting - In addition to the tabular output produced by air dispersion models,selected models ore designed to produce concentration isoplclh plots, and plottingroutines can be applied to the output of most other models to display the modelresults on a site-specific map. The map digitizing capability combined with theplotting capability of TRCs computers significantly enhance the value ofdispersion model output when either topographic or demographic features are ofconcern.

AR1*005I5

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Computer Aided Design (CAD) System - This state-of-the-art computer drafting^ and publishing system includes four microcomputers and associated software. The

basic unit is an ACER 1100 with 4 megabyte random access memory (RAM), 65V—/ megabytes of fixed drive space, a standard 360 kilobyte floppy disk drive, a high

density 1.25 megabyte floppy disk drive and a NEC multisync!) 13" color monitor.A Cal-Comp 1023 D-Size plotter is used for drawings up to 24" x 36" in papersize. Also used are a Hewlett-Packard 7475A plotter and a Toshiba Page Laser12 for drawings up-to 11" x 17' in size.. Software used includes Auto Cad Release10, Microsoft Windows, Page Maker Release 3 and PC Paint.

• Models and Software Library

Software support on the TRC computers is extensive. The most recent versionsof all 31 atmospheric dispersion models in EPA's UNAMAP series ore available.In addition, the RTDM, LAPPES (complex terrain), CALINE3, GMLINE, IMM(mobile), Shell SPILLS (toxic release), CRSTER/OCS, OCD, ASLI (oir-seu-landinteraction), SAI (reactive plume); EPA PLUVUE (visibUity), CDMDEP,DIFKIN, and Ex Ex models are supported. Software development andcompilation can be performed using FORTRAN 77, PASCAL,and BASIC.

; Various microcomputer software packages provide several data base management,i j operating system, file editor, word processing, spreadsheet, statistical, plotting, and

language compilation alternatives.

Some of the available models are listed below.

PRIME Computer Models; v :> -: - -' ^ ..-..._,. 91*, tl * . •- - • = • ' • " . ' .'

SPECTRA TRC wind trajectory model ^ .SPILLS Toxic release source and dispersion modelRTDM Single source complex terrain model

'LAPPES Complex terrain modelCALINE3 Line source dispersion model , . .

'"' GMLINE Une source dispersion model,!• : .,.* -i --.! .j (. B. .. ..-.Hi I- , r • - .

•'•""•• ASU/LAMAir, tea, land interaction model for wind simulation in coastalS ' ' ' ' ' r "'- ' ? I i ' '- |H !f ., .1 1 , -" ^ it* "I"' -' "I ' • 'areas •

• FLARE Model used to simulate plume rise from flare stacks2-D Wind 2-Dimensbnarwind flow model for horizontal winds in complex

'-' terrain y ' " : " / ' JL:;;": ' ' * . " .^ J DEGADIS Dense gas dispersion model

moos 16

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PC Models; t• .,... ; . . "',:- .Hie/Springer Chemical evaporation model -

. USAF/Kahler Chemical evaporation modelArmy/CIewell Chemical evaporation modelOntario ' " " ' ' " . : -- • . . .» • ' " •Ministry Toxic release source and dispersion model of EnvironmentNYSDEC Model Volatile emissions from soilsTRC Odor Model describing near-field dispersion of odorous emissions

EPA Models «n PRIME or PCs

RAM Multiple point and area source, short-term dispersionmodel . - : — , ' .

RAMMET Meteorological preprocessor program •CRSTER Single source location, short- and, long-term dispersion

modelCDM Multiple point and area source, long-term dispersion modelCDMQC CDM modified for additional output , vAPRAC3 Urban scale carbon monoxide dispersion modelHIWAY2 Line source dispersion modelVALLEY Multiple point and area source, short- or long-term,

complex terrain dispersion modelTEM8 Short term episodic dispersion modelTCM2 Long-term cllmatological dispersion modelPAL Point, area, and line source dispersion modelMPTER Multiple point source dispersion model with terrain

adjustments ... ,COMPLEXI Multiple point source complex terrain dispersion model

with sector averaging in the horizontalCOMPLEXII Multiple point source complex terrain dispersion model

with normal distribution in both the horizontal and verticalBLP Line and point source dispersion model designed to-handle

-industrial sources where plume rise and downwash effectsfrom stationary line sources are important

ISCST Short-term dispersion model able to assess Jfliftifatntffdeposition and settling, downwash, area, volume, point, and

• • line sources

ARI»005I7

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ISCLT Long-term version of ISC using meteorological frequencydistributions

MPTDS ; Modified Version of MPTER which handles gravitational: . • settling and depositionSHORTZ Short-terni, complex terrain dispersion model able to

handle multiple point, area, and volume sourcesLONGZ Long-term version of SHORTZ using meteorological

frequency distributionsCOMPLEX/PFM Modified version of the COMPLEX models

accounting for potential flowMESOPAC Meteorological preprocessor program for regional modelsMESOPUFF Variable trajectory regional model for determining multiple

point source impacts at long distancesMESOPLUME MESOSCALE flume segment model for SO, and SO,

applications over long distances ' 'MESOFILE Postprocessor for MESOPLUME and MESOPUFFROADWAY Finite difference line source modelROADCHEM Modified ROADWAY models handling chemical reactionsPTMAX Single point source maximum short-term screening modelPTDIS Single point source short-term screening modelPTMTP Multiple point source short-term screening modelCHAVG Postprocessor for computing running averages for hourly

. - : ' , r, concentrations;,;, .UTMCON Program to convert latitude and longitude to UTM

coordinates and vice versaEPAPUF EPA integrated puff dispersion modelINPUFF EPA instantaneous release modelSRI Puff Time dependent puff model and wind field model

Publications Department

TRCs Publications Department is committed to high professional standards. Atechnical editor cooperates with the Graphics Section, Word Processing Centerand Copy Center in the efficient review end production of tectfipjcfal Rerip,reports and proposals. The manager of the department is respohsible'for 'thecoordination of jobs -arid assures quality and efficiency.

AR(t005!8

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Word Processing .Center'

TRCf Word Processing Center, staffed by professional word processingoperators, is equipped with a state-of-the-art, automated office Informationsystem (Wang VS 225) with a laser printer to ensure the rapid and efficientproduction of reports. This system permits quick and easy access toInformation and Includes the ability to sort lists. In addition, each operatoris familiar with corporate style requirements.

Crannies .

The Graphics Section, staffed by experienced graphics personnel, is backedby the latest equipment for the preparation and production of technicaldrawings, maps, diagrams, flow charts and graphs. This department alsohandles the design, layout and camera-ready artwork required forpresentation materials, displays, brochures and slides.

Cumr Facilities

Copying at TRC Is done on a high-speed copying system with additionalcapabilities of automatic, collating and sorting, photoredticlion, production oftransparencies for special presentations, back-to-back copying and processingcomputer printout sheets. Hie center also maintains the highest qualitybinding systems and a telecopier.

moosis

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SECTION 5.0 IIEAL'IH & SAFE1Y PROGRAM' *

ARU00520

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SECTION 5.0 HEALTH & SAFE1T PROGRAM

All Alliance field personnel are 'trained in accordance with the OSHA requirementsof 29 CFR 1910. Prior to the conduct of any field activities, each employee hascompleted a 40-hour Hazardous Waste training course. Staff members complete an8-hour refresher training course on an annual basis. Project managers also receive8 hours of supervisory training. This training enables the employee to evaluate (hepotential dangers and/or contaminants associated with a particular field investigation,and to determine the appropriate sampling gear, monitoring devices, and personalprotective equipment, based on these characteristics. Copies of trainingcertifications are available upon request.

A Health & Safety Plan is prepared prior to the initiation of any field activities.This plan details the known and suspected hazards present at the site, all samplingand decontamination methods, personal protective equipment to be used bysampling personnel, any monitoring devices which will be used, and locations andtelephone numbers of nearby emergency services. All sampling personnel arefamiliar with the specifics of the Health & Safety Plan prior to the conduct of fieldactivities.

Alliance has instituted a medical monitoring program for sampling personnel. Thisconsists of a detailed, baseline medical exam conducted prior to the employeeconducting any fieldwork for Alliance, as well as annual medical exams targetedtoward contaminants which may have been present at field sites visited during theprevious year.

flRI*00524

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• ULtiC^rfl Uvs W~IL.../ BI iK .1 rr/it. n.,(,. T. ,ii u_.j*. . — .. ,.. ..,.litMl North • Earth Cily. MO

Introducing.,...

metaTRACE, )nc;r .

more than just a laboratory.' - -"-r "V i*»il

1 -— t -(" " hi '

.' .T'F "-

AR<i00522

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SUMMARY OF CAPABILITIES

GENERAL BACKGROUND INFORMATION

metaTRACE, Inc. is an analytical laboratory established in1968 in St. Louis, Missouri. A wholly-owned subsidiary 'ofTRC Companies, Inc. of E. Hartford* Connecticut, metaTRACEwas founded to support and facilitate the environmental andradiological monitoring, measurement and reportingrequirements of consultants, industry and government byproviding routine and custom analytical chemistry services.

metaTRACE was founded by professionals with over 50 years ofcombined experience in environmental consulting andlaboratory management. Dr. David C. Kennedy, President andChief Executive Officer, formerly served as Vice Presidentand Manager, Environmental Division, for a major, nationalconsulting firm with extensive laboratory capabilities. Dr.Carol H. Byington, metaTRACE Executive Vice President andTechnical Director* formerly served as Assistant VicePresident and Laboratory Director for a major, environmentaland analytical consulting firm.

GENERAL CAPABILITIES

metaTRACE offers full-service capabilities for organic,inorganic and radiochemistry analyses of air, groundwater,surface water, Wastewater, potable water, soil, hazardouswastes and biological samples. Routine services offered bymetaTRACE include:

o complete analytical services for organics/inorganics

o analysis of toxics, including dioxins and furans

o analysis of nixed waste or co-contaminated wastes

o radiochemistry analyses

o quick turnaround for remedial programs

o TCLP analyses

o Appendix VIII and IX analyses

o hazardous waste analyses

o explosives analysis (military compounds)

o EPA priority pollutant, RCRA, SARA analyses

o industrial hygiene sample r

yfc' .-.is fir ARU00523

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' . , - .

o air quality analyses, including odor characterization

o methods development/validation studies

SPECIAL CAPABILITIES AND SERVICES

metaTRACE offers a full range of radioanalytical servicesemploying new, state-of-the-art, fully computerized radiationdetection equipment/instrumentation. Our counting equipmentreflects the variety and-number required to process a largesample flow with maximum efficiency. MuIti-detector andautomated systems are routinely used to measure totaluranium,; radium-226, and other alpha, beta and gamma emittingradionuclides, as well as for screening potentiallycontaminated samples. Specific alpha scintillation detectorsare employed to measure both radium-226 and radon-222.Isotopic thorium, uranium and transuranic analyses areperformed using a fully-computerized, multi-detector alphaspeetrometric system. metaTRACE has analyzed assorted mediafor cross screening and ieotopic parameters, as well asstandard chemical analyses on co-contaminated or high hazardcamples.' . * . . • • • • ' " h-tir x. >•':"".'- -, '' " .'.',

Explosives AnalvgJB ., - r* , >- • . , .. , • ,'•- - ;•- , >,'|'>-.-'""'

metaTRACE has extensive expertise and experience, bothcorporate and individual, in the analysis of explosives andother military compounds in environmental samples. Theprimary analytical method for explosives analysis employsUS Army Toxic and Hazardous,Materials Agency (USATHAMA)methodology. This method; originally developed for the Armyby metaTRACE principals* utlliees High Performance LiquidChromatography and is able to determine, in a singleanalysis, the followingjexplosives, byproducts anddegradation products: 2,4»6«TNT; 2,4-DHT; 2,6-DNT; Tetryl;RDX; HMX; NB; 1,3-DNB; 1,3,5-THB; and four amino/nitrodegradation products of THT and DNT. .metaTRACE has employedthis methodology for the analysis of hundreds of samples fora remedial action project J.n the_ midwest. In addition,metaTRACE principals have prior experience in the analysis ofthousands of environmental samples for explosives and othermilitary compounds from military facilities.

Value-Added Service ... * c' i -r •' -.' - •'. •'

To be competitive in today's analytical services market.metaTRACE provides clients vith what we call a **v*ftt\ej-a,qpejaservice. This service, provided by our project managementstaff aided by our computerized Laboratory InformationManagement System (LIMS), translates into better service toour clients. When you become a metaTRACE client, you will be

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assigned a Project Manager who will be your principal pointof contact in the organization. The metaTRACE ProjectManager has no other .responsibilities within the laboratoryexcept to-assure that his/her clients' analytical needs aremet. metaTRACE Project Managers are not salesmen but ' 'professional environmental chemists with a businessbackground. Their charter is to provide data of the highestquality, on tha date it was promised, along with ensuringthat all contractual obligations are met.

Laboratory Information Management System ' .

To aid our Project Managers, metaTRACE utilizes a state-of-the-art, computerized Laboratory Information ManagementSystem (LIMS). Known as LAB WORKS, this system is designed tomanage the flow of samples through the laboratory. LAB WORKSprovides managersr analysts and technicians instant access toall the information they need regarding samples in thelaboratory, enabling them to perform their duties in the mostefficient manner possible.

Some of the key features of LAB WORKS are summarized below:

o LAB WORKS is a network system of personal computers toallow maximum flexibility and potential for expansion.Only recently has networking technology advanced to thepoint where sufficient core is available to efficientlyhandle a LIMS system. metaTRACE took advantage of ourstartup to gain the most advanced technology on themarket. . • * '

o When samples.are received and logged in, they receivea metaTRACE number and corresponding bar code whichvirtually eliminates misldentification of samples dueto key punch or transcription errors.

o Samples are tracked. according to holding times withbacklog reports supplied to section managers on adaily basis. .This eliminates "missed" holding timesdue to overlooked samples.

o A feature that may be of particular interest to manyis the ability to allow clients direct access to theirvalidated data. In addition, the client can query thesystem for sample status on their program.

We feel that the metaTRACE project management system, aidedby the most advanced information management system available,enables us to provide client support beyond any of eturcompetitors. We urge you to visit our facility, m«evourstaff, and see for yourself what metaTRACE has to offer.

The newly acquired QA Formaster software includes a link-up with the GC/MS systems used for BNA and VOA analyses,

.;•:-.•: , , flR*»00525

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allowing electronic data transfer of files after thoroughreview by laboratory section managers and validation bythe Quality Assurance1Manager. This system will bedirectly linked to the Kelson Chromatography System,in thevery near future to include pesticide/PCB analyses in theautomated .data transfer.system.

'•„ " f~ i -'f S- .'"' 1 ^ •-The Ward Scientific software package has recently boonacquired to automate inorganic data transfer ..from ICAPanalyses. Similar to the organic data software, onlyvalidated data is approved for automated file transfer.

FACILITIES .V/'.l r'Y^L*Y'--I-' ."• ' * • " ' ' ' . " . . ' -'"" : ' ' . . . I ' . ; - " ? ? " "£* if b V.- - " -" - ' . - i '.

metaTRACE facilities and instrumentation represent the state-of-the-art for commercial.-analytical laboratories. We tookadvantage of our start-up and purchased the mostsophisticated instrumentation available for the productionand management of high quality analytical data. The foundersof metaTRACE also used their decades of laboratory managementexperience to direct the design of our new facility. So -literally from the ground up, the metaTRACE laboratory Isuniquely equipped to handle the requirements of today's mostcomplex and demanding environmental programs.

*

The design of our 30,000 square foot facility optimizes theflow of samples, Information and staff. The sample receivingarea's 3,000 square feet includes four truck bays, a securedsolvent and waste storage area, and two walk-in coolers: onefor medium to high hazard samples and the other forconventional samples. From the receiving area, samples godirectly into either the Preparation Laboratory or theRegulated Access Area (RAA). The 2,000 square footPreparation Laboratory is designed for the efficientpreparation of large numbers of low to medium hazard samplesfor instrumental analysis. The RAA, for high hazard samplepreparation, has negative pressure air flow to preventcontamination from entering other areas of the laboratory.Employees enter the RAA through airlocks complete with changeand shower facilities. Extracts proceed from the RAA througha pass-through to instrument laboratories.' The RAA alsoprovides the ability to prepare highly toxic or radioactivesamples by remote robotic manipulation.

From the sample Preparation Laboratories, samples flow intoone of several metaTRACE instrument laboratories:

o ICAP/AA Laboratory for the analysis of metals

o Tech Laboratory containing automated instrumentation,for example, Technicon Autoanalyzers

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"^ • o Chromatography Laboratory (GC, 1C, HPLC) equipped withpositive air pressure to isolate the lab from the samplepreparation areas

o GC/MS Laboratory where 10 GC/MS systems operate; lab hasa totally independent air handling system with charcoaland HEPA filters and positive air pressure

o Radiochemistry Laboratory with instrumentation designedfor various low level radiological analyses

Computer terminals are located In the laboratories andoffices of metaTRACE Program Managers to allow easy access toour computerized Laboratory Information Management System(LIMS) which tracks.samples through every stage of handling,from receipt through disposal, and captures analyticalresults, thereby facilitating reporting.

INSTRUMENTATION-„ . * * *

Table 1 provides a listing of analytical equipment andinstrumentation owned by metaTRACE, Inc.

flRl*00527• " „* , 'S •'' i-, *.. r . > , tr* i t *r. 3 ~> - ~

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I ; NBS)-

"TABLE 1 METATRACE MAJOR INSTRUMENTATION' Ci .-:S.. ;: •»:;,

Instrument * j Quantity Manufacturer Model pure' Date

Gas Chromatograph/ . 3^r-tc Hewlett Packard 5988A : 1986Mass Spectrometer ' 198tR T E Data System a n d . . .Library (Wiley/HBS) -, G b9-track magnetic tapeAutosaropler .

- . - = , ; - i d ' ' . ' . . ' ' - - -Gas Chromatograph/ 3 Hewlett Packard 5995 ' 19B6Mass Spectrometer • 1988Split/cplitless ,h: T ^ 'Injection; Capillary F :Splitter for odor , v - 1; ' •• /characterization - 'Aut os ampler ' ' -

Gas Chromatograph/ 4 ivi Hewlett Packard 5970* 19B6Mass Spectrometer/MSD; RTE Data System - ,, , - i^and Library (Wiley/

9-track magnetic .tape ; Ki It

Purge and Trap ^ .3. |i- Tekmar LSC2 1986ALS/Heated Purge

• - - ••.-.;•••" k-r;i/? . " . " , ' ' -Gas Chromatograph 4 Hewlett Packard 5890 198GCapillary /PackedColumn . - . - - . .Autoin JectorAutosampler . •• -7 sFI /EC/HP DetectorsPID/Hall Detectors . <

Gas Chromatograph 2 . Hewlett Packard 5680 1986Autoin Jector -Autosampler •FI/EC/MP Detectors , , n ef T - :

3. , * - - ' . ' ' - S.r FJ--- *l'r-i'li _ L .- _ - -

Inductively-Coupled 1 Thermo Jarrell Ash 1100 1906Argon Plasma VacuumSpectrometer

Atomic Absorption f ' 'J -' J4 Thermo Jarrell Ash ,t2Ef - ermo arre s ,t2E . 19BGSpectrometer • . /

Atomic Absorption 2 Perkin Elmer 3030B 1987Spectrometer •

eS:^Us-MA ARU00528

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'TABLE 1 METATRACE MAJOR INSTRUMENTATION(continued)

Instrument ; Quantity Manufacturer Model Purcl

Total Organic Carbon 2 Dohrmann-Xertex DC 180 1988Analyzer

Total Organic Halogen 1 Dohrmann-Xertex DX20A 1988Analyzer

Ion Chromatograph 1 Dionex . 40201 1986HPLC Module

Autoanalyzer 1 Technicon TRAC800 1986

High-Pressure Liquid 2 Perkin Elmer 410 1986/Chromatograph 1988Autosampler

UV Spectrophotometer 1 Milton Roy 601 1986

IR Spectrophotometer 2 Perkin Elmer 1420 Ratio 19»?Recording i

Coal Analyzer 1 Fisher Scientific 490 1987

Turbidimeter 1 HF Scientific DRT100B 1986

Single Detector 1 Tenneleo LB5100 1987Automated Low Back- Series 3ground Gas ProportionalCounter

Multi-Detector (8) 1 Tennelec LB4000-8 1987Low Background GasProportional Counter

Alpha Scintillation 4 Random SC-5 . 1987Counter for Radon Cells .

Alpha Spectroscopy 1 EG&G Ortec multi- 1987Counting System with 8 ' componentDetectors, Electronics systemand Computer

Gamma Spectroroetry 2 Princeton multi- 1987Counting System with' • Gamma Tech componentIntrinsic Germanium syatsmDetector, Electronics.Computer* Shielding

flR«*00529

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' TABLE 1 METATRACE MAJOR INSTRUMENTATION: (continued)

tInstrument Quantity Manufacturer Model pure

Date

Gamma Spectrometry 4 Tennelec/ multi- 1987Counting System with ^ -.,•;.. Nucleus componentNal (Tl) Detector, «, : ; systemElectronics, Computer * .Shielding v; '5JLiquid Scintillation 1 . P a c k a r d 2200CA 1987Counter ,^_ , ;.,", ^'1 :".,, •

Assorted Survey ' 5 Ludlum assorted 1987Meters with Alpha, ; ? n <ViiiBeta and Gamma "Probes

pH Meters, probes 10 Orion ** 701A 1986

Balances 9 Fisher XA, XT 1986Mettler AE160

PE160

Extractors . ;Soxhlet 12 Fisher assorted 1986Liquid-Liquid 24 Herschberg/Wolf R3753-100 1986

Reliance

Distillation EquipmentCyanide 15 Reliance Glass R3166-100 19B6Phenol 11 Fisher Scientific assorted 1966Oil/Grease 10 Fisher Scientific assorted 1986

Laboratory Information 1Management SystemModified LABWORKS soft-ware on microcomputernetwork:

1 IBM - AT2 . IBM PC conv.16 IBM XT equiv.1 Hayes Modem

1200 baud _

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TABLE 1 METATRACE MAJOR INSTRUMENTATION(continued)

Network available software:

rBase 6000dBase III PlusLotus 1.2,3Crosstalk XVIWordstarWordPerfectIBM Assistant Seriespf s*: First ChoiceFormtoolReflection VII

AR«»0053I

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JJ

TABLE 2 METATRACE ANALYTICAL METHODOLOGY

Parameter Water Method Soil/Sediment. Method

Priority Pollutants :BNAs EPA 625 RCRA 82706Volatiles EPA 624 EPA 8240Metals EPA 200 series EPA 7000 seriesPest/PCBs ' EPA 608 EPA 8080 .,Cyanide , . EPA 335,2 EPA 9010Phenols ' - EPA 420.1 RCRA

i j Total Organic

HSL Compounds EPA IFB protocol EPA IFB protocol

TNT, 2-4 and2-6 DNT, nitro- ;benzene andtrinitrobenzene USATHAMA 6G USATHAMA 8H

Total OrganicCarbon r EPA 415.1 RCRA 9060 *

Halide EPA 450.1 RCRA 9020 --

EP Toxiclty(metals only) EPA 1310 RCRA 1310

Total metals EPA 200 series RCRA 7000 series(CLP listing)ICP metalsFurnace metals , . . - . . ;

EPA 405.1 EPA 405.1

EPA 350.1 EPA 350.1 :. , , - ' .<Tf.': * / • ' • ' -

EPA 310.1 EPA 310.1

Carbonate/ \ Standard :" - StandardBicarbonate Methods 203 .Methods 203 •

Sulfate EPA 375.2 EPA 375.2

Chloride EPA 325.1 f RCRA 9250/9251/9252I

Hardness EPA 130.2 EPA 130.2

i^ Lithium Standard StandardI Methods 317 Methods 317

flRi»00532

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TABLE 2 METATRACK ANALYTICAL METHODOLOGY(continued)

Parameter *' Water Mftthod Soil/Sediment Method

Asbestos EPA methodology EPA methodology

Nitrate EPA 352.1 RCRA 9200

Nitrate +Nitrite EPA. 353.2 EPA 353.2

Nitrite EPA 354.1 EPA.354.1

Nitrogen series along with chloride, fluoride and sulfate maybe analyzed utilising the ion Chromatograph method-EPA 300.0

Nitroaromatics EPA 609 EPA 609

PolynuclearAromatics EPA 610 EPA'8090

Haloethers EPA 611 EPA 611

Chlorinated -Hydrocarbons EPA 612 EPA 612

PurgeableHalocarbons EPA 601 RCRA 8010/8015

PurgeableAromatics EPA 602 RCRA 8020

Phenols EPA 604 RCRA 8040

Ignitabillty EPA 1020 EPA 1020

Corrosivity EPA 1110 EPA 1110

Reactivity EPA 9010/9030 EPA 9010/9030

Bacteria, Standard Standardfecal strep Methods 910 Methods 910

Bacteria, Standard Standardfecal collform Methods 908 Methods 908

Bacteria, . Standardtotal coll form Methods 909 RCRA 9132

Chlorine.total residual EPA 330.1 EPA 330.1

Color EPA 110.2 :AR(t005-33

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TABLE 2 METATRACE ANALYTICAL METHODOLOGY(continued)

Parameter Hater HcLthad Soii/sedim^n^Distilled Sulfide EPA 376.1 EPA 376.1

Sulflte EPA 377.1 EPA 377.1

Surfactants EPA 425.1 EPA 425.1

Turbidity EPA 180,1 EPA 180.1Viscosity ASTM * ' ' ' ASTM

Moisture Content EPA 160.3 EPA 160.3

BTU Value ASTM ASTM

Aah Content ASTM ASTM .•

Sulphur Content ASTM ASTM

2,3,7,8-TCDD - EPA 613 N/A

2,3,7,8 -TCDD EPA CLP EPA CLP

2,3,7,8-TCDD .Region VII Region VIIRapid Prep Rapid Prep

Total Tetrathrough Octa * . -dlbensodioxlns/ RCRA 8280 RCRA 8280furans (ASME) ' (ASME)

Radiological Parameters: . .

Gross Alpha EPA 800.001 RCRA 9310 ;Gross Alpha, '""• * . ?.•">£! .,££•'' ••'"•"••'-- •Coprecipltation EERF 00-02* EERF 00-02Gross Radium Alpha EPA 803.0 1 ,fDO-; RCRA 8315

Gross Beta , UFA 800>00 Uct:; RCRA 8310

Radium-226,Radon Emanation EPA 803; It a s-r'd EPA 803.1

Radium-226, 'Proportional - rfi ; * ^ . ! • ' ' "Counting SM 705* SM 705

' ,~^£,t -t;-••• ' -f- -

ct\.t*"-.-••;.'•;.".

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TABLE 2 METATRACE ANALYTICAL METHODOLOGY(continued)

, Parameter ; .MatfiT Method Soil/Sediment Method!

Radium-228,i Proportional1 Counting EPA 904.0 RCRA 9320

i Total Uranium,| Radiochemical EPA 908.0 EPA 908.0

Total Uranium.I ICAP EPA 200. 7« EPA 200.7i

Isotopic Uranium EERF 00.07 EERF 00.07

j Isotopic Thorium EERF 00.07 EERF 00.07

. Isotopic Plutonium EERF 00.07 EERF 00.07

' Americium-241 EERF AM. 01 EERF AM. 01

Lead-210 HASL Pb.Ol** HASL Pb.Ol ,

Strontium-89 SM 704 SM 704

I Strontium-90 HASL Sr-05 HASL Sr-05

Iodine-131| radiochemical SM 710B ———————

Iodine-131, direct .I counting EPA 901 . 1 EPA 901 . 1

Gamma EmittingRadionuolide EPA 901.1 EPA 901.1

* Prescribed Procedures for Measurement of Radioactivity inDrinking Water, EPA 600/4-80-032, 19B2.

a Eastern Environmental Radiation Facility, RadiochemistryProcedures Manual,, EPA 520/5-84-006, 1984.

* Standard Methods for the Examination of Water andWastewater, 16th Ed., 1985.

* Methods for the Chemical Analyses of Water and Waste*.. .EPA600/4-79-020.

* EML Procedures Manual, HASL 300, 25th Ed., 1982.

* • SW-B46. 3rd Edition, September 1986.

,..,.,. flRl*00535

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TABLfc 2 METATRACE; ANALYTICAL METHODOLOGY* ' (continued )

Parameter : Hater Method Soil /SedimentConductance, ,specific EPA 120.1 T, RCRA 8050

Fluoride .. r , .... . - - - , - , . . . - •(electrode) EPA 340.2 ' EPA 340.2

f "''''-• \' ' - h .;'Fluoride ;(distillation) EPA 340.1 EPA 340.1

Sir ,- -, f — - ' T - • ''Nitrogen, . '-- • •• , ~_ /'""'ammonia EPA 350.1 EPA 350.1Nitrogen,KJeldahl EPA. 951. 2 .: / EPA 351.2Nitrogen, ' sorganic / PA 351-1 EPA 351.1Oil (TCTFE) EPA 413-1 o RCRA 9070

T i .

I , BOD (20 day) EPA 507 EPA 507

COD EPA 410, I/ EPA 410*1/410vje ( 410.2

Total Petroleum EPA 418. 1 , > RCRA 3550/Hydrocarbons ;: /r EPA 416.1

• - * -i ' '' -- L" - ...

DissolvedOxygen EPA 360.1 r EPA 360.1

PH EPA IBO.,1, ,,: RCRA 8045/8041Ortho Phosphorus EPA 365.1 EPA 365.1

Total Phosphorus EPA 365.4 EPA 365.4

Dissolved Solids EPA 160,2 EPA 160.2

Settleable Solids EPA 160,3 EPA 160.3

Suspended Solids EPA 160 .[J EPA 160.1' ^ .' '[ •''-•• * 'Total Solids EPA 160.3 #5 EPA 160.3 f

Volatile Solids EPA 160.4 EPA 160.4- ^ " - .- •' -

Sulfide EPA 376,1 RCRA 9030

/IRtfQ0536

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TABLE 3 SAMPLE CONTAINER, PREPARATIONAND PRESERVATIVE REQUIREMENTS

Water Sample Preparation PreservativeContainer TVPOi

f Volatile Organic 2-40 ml VOA vials Water-no prep ColdCompounds Soi1-soap/water,

i D.I. rinse,I oven dry

. Base/Neutral and 1 gal amber glass Soap/water, D.I. ColdAcid Extractable rinse, acetone

1 Organic Compounds rinse, methyleneand Pest/PCBs chloride rinse

! Pioxin 1 gal amber glass Soap/water, D.I. 'Cold(2,3,7,8-TCDD) ' rinse, acetone

. rinse,, methylenej chloride rinse

yanide 1 qt plastio . D.I. rinse SodiumHydroxide/Cold

• Phenols, Total 1 amber glass D.I. .rinse Sulfuricj (250 or 500 ml) oven dry Acid/Cold

Metals Analysis 2-1 qt plastic 1:1 HNOj rinse, Nitric Acid/! when CLP metals D.I. rinse Cold1 required

j Sulfate 1 qt plastio D.I. rinse Cold

Ilexavalent 250 ml plastic 1:1 UNO* rinse. Cold• Chromium D.I. rinse

Oil and grease 2-1 qt glass Freon rinse SulfuricAcid/Cold

i . - . - * "• Total Organic 1 qt plastio D.I. rinse, ColdCarbon oven dry .

| nitrate 1 qt plastic-may D.I. rinse, SulfuricTOC sample oven dry Acid/Cold

Tetrachloroethylene 2-40 ml VOA vials Water-no prep C61~dI'richloroethylene Soil-soap/water',,1,1-trichloroethane D.I. rinse,,1-dichloroethylene oven dry

Urans-1,2-dichloro-tithylene

: •':'.- flRl»00537

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tABLE 3 SAMPLE CONTAINER, PREPARATIONAND PRESERVATIVE REQUIREMENTS

Analvte Water Sample ,'* , Preparation PreservativeContainer

Benzene 2-40 ml vialc Water-no prep Cold ''Ethylbenzene ' Soil-soap/water,Toluene ' . . . . , - > ^; l "D-I- rinse,

' -" I - ' - - ' . •- •• ^ ^ ;;;;ii|.. . oven dry / ' " , ":-" ' ' ' * f , • • i '• - ' 'Nitroaromatlcs: 1 gal amber class Cold

2,4,6-TNT , . „„„.,.„ > . - ; • - , • " ' • " - • ^2.6-DNT : -'• ' - "-L "i-.Cli*/ 1;1..-, • • ••'••- - .-.- ! - '• " ::2,4-DNT -.-:- - , ' "• ; ' - & """1,3,5-TNB . ,,,„ v .1,3-DNB; NB; : -,^liDX; HNX; Tetryl . v,t 1.,- r •.."•-Asbestos ^ 1 qt plastic '^ . No preparation Cold

Total Petroleum 1 qt plastic Freon rinse • Sulfuricrocarbons , - Acid/Cold

D.I.=deionized water , ,«^ * • ,For sampling soil, 2-250 ml wide-mouth amber glass Jars per site aresufficient for above parameter list/cold preservative.

For sampling soil/sediment with high"water content, 2-1 qt wide-mouthamber class Jars per site are required/cold preservative.Many of the above tests can be taken from the same containers wheneverpreservative/volume requirements remain the same.

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CERTIFICATIONS/APPROVALS

Federal

o metaTRACE is participating in the USEPA's ContractLaboratory Program (CLP) for organics analysis and rapidturnaround dloxin analyses(Contact: Angelo Carasea 202/382-7906)

o metaTRACE has been licensed by the US Nuclear RegulatoryCommission to perform analyses on co-contaminated wastes(both chemical and radiological)

o metaTRACE is certified by the US Army Toxic & HazardousMaterials Agency (USATHAMA) for a wide range of parametersunder the CLASS contract(Contact: Douglas Stevenson 301/671-3348)

o metaTRACE has been certified by the US Navy Energy andEnvironmental Support Activity (NEESA) to perform analyticalprograms at Naval installations. This certification alsoapplies to US Air Force programs. .(Contact: Mitzi S. Miller 615/576-2361)

o metaTRACE has been certified by the US Army Corps ofEngineers Missouri River Division.(Contact: Ann B. Strong 601/634-3600)

o US Department of Agriculture certification for importingsoil samples.

States

o State of New York (Contact: Matthew Caruso518/474-8519

o State of California (Contact: Fred Seto415/540-3003)

o State of Missouri (Contact: Jerry Lane 314/751-6400)

o State of Florida (Contact: Howard Rarick 904/359-6449)

o State of South Carolina (Contact: R. Wayne Davis803/737-7025)

o State of Wisconsin (Contact: Ron Arneson 608/267-7633)

o State of Tennessee (Contact: Charles Mickle 615 26'2-tf3B4)

o State of Kansas (pending)

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metaTRACE ORGANIZATION AND PERSONNEL

metaTRACE ORGANIZATION

The overall organization of metaTRACE is shown in Figure 1.metaTRACE designed this management organization and itsmanagement systems based on the many years of experience ofthe principals.in the commercial laboratory business. Webelieve it is the best system for efficiently managing theanalysis of large volumes of samples while, at the same time,maintaining high quality and responsiveness to thespecialized needs of individual clients. The elements of theoverall metaTRACE management structure are described below.

" ]1. Principal Responsible Corporate Official' ;Dr. David C. Kennedy, as President and CEO of metaTRACE,provides top corporate oversight on technical and financialperformance and supports the Technical Director in securingthe necessary resources for successful project performance.

2. Technical Director 5 • r " *Dr. Carol H, Byington serves aa Technical Director. She hascomplete responsibility and accountability for achieving allproject requirements -technical, schedule, and financial.Dr. Byington, as Executive Vice President of metaTRACE, hasdirect control of all technical resources to accomplishproject objectives. .

o Document Control/Sample Control Manager 'Ms. Barbara B. Gillam serves as{Document Production andControl Manager. She manages the timeliness and quality ofall project deliverables..

o Information Management Systems Manager ' 'Mr. John A. Hayden is the manager of the Information SystemsDepartment.. . He is responsible }for the administrative'controland operations related to computerised data processing forboth Internal company use and output to customers. He isalso responsible for assessing current and future metaTRACEneeds involving computers, robotics, automation/and relatedsoftware. ••' ' ,,...j i . -• - •—-' •- - •- "3. Project Administration J,,,J. ; <-. i -^ :Mr. Kenneth Baughman, Assistant Vice President, is' "'responsible for all program management activities. Throughhis Program Managers and their {Project Managers* the specificrequirements of individual projects and clients are .. ~.:-translated into results and deliverebles. Under the - ,metaTRACE matrix management system, Mr. Baughman and hismanagement staff represent the client and advocate hisinterests in executing the projects through the Laboratory :Operations organization. The Quality Assurance Manager andthree Program Managers are under Mr. Bauehman's control.

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L .-1 metaTRACE Organization

i

D.C. Kennedy, Ph.D.President

K.T. ArinlcControl 1 er

7 C.H. Byington, PtV.D.Executive Vice President

Technical Director

B.B. GillamManager f Document

Control/Sample Control

J. HaydenInfo. Management Systems

\ R.K. RobesonVice President

Operations Management

K.J. BaughmanVice President

Project Administration

Organic AnalysesH.. Borg

Inorganic Analyses-, P« Hamburg ; - ~

Sample PreparationJ. CollIns

Radiological PreparationR. Patterson

QA/QCC. Scarpallina

Environmental ProgramsR. Mannz

Radiological ProgramsP. Kelly

DOD Program!M. MartiM

Radiological AnalysesE. Holland

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o Quality Assurance Manager ;Mr. Christopher D. Scarpellino serves as the QualityAssurance Manager. A rigorous QA/QC program has beenimplemented at metaTRACE. Mr. Scarpellino manages and .'monitors this program, directs the production of Laboratoryand Project QA Plans, and administers the various Federal andState laboratory certification programs.

o Environmental Programs.'Mr. Richard H. Mannz is theEnvironmental Program Manager and is responsible for managingenvironmental projects for which chemical analyticalrequirements predominate.

,' k..... | n". ' ' i-o Radiological Programs. Mr. Patrick Kelly is the

Radiological Program Manager and is responsible for managingprojects that have a large radiological analyticalrequirement. , , :

L . • - -

o DOD Programs. Ma. Marie ah M. Martin serves as theDepartment of Defense Program Manager and is responsible formanaging military projects and programs, including the U.S.Army Toxic and Hazardous Materials Agency (USATHAMA) ContractLaboratory Analytical Support Services (CLASS) Program.4. Laboratory Operations Management ". •Mr. Ross K. Robeson, Vice President, is the LaboratoryOperations Manager. All laboratory production functions areunder his direct control and supervision. He is responsiblefor the timely production of quality analytical results. ;There are five key laboratory operational functions under hismanagement control, each managed by an experienced technicalsupervisor.. These are: ":',':'.''.*'.#" \ . ';- • ' - ; ' , ..'', '' ''•

• ' . •' ', ? " '-., IS.;-T-- -- . . ' " • ' ' ' ' " " , , . , . • ' 'o Organic Analysis. Mr Harry M. Borg is the supervisor ofthe Organic Analysis Department/ He is responsible for .scheduling and reviewing all analyses performed by GasChromatography-(GC), GC/Mass Spectrometry, High-PerformanceLiquid Chromatography (HPLC), and Ion Chromatography (1C).- . - , • • • „ " " " H I - - ' " • • ' * * ~ . • . • , " 'o Inorganic Analysis. Mr. Paul B. Humburg is the "

supervisor of the Inorganic Analysis Department'. He isresponsible for scheduling and reviewing all AtomicAbsorption (AA) and Emission Bpectroscopy and InductivelyCoupled Argon Plasma (ICAP) Atomic.Emission Spectrometry andmiscellaneous inorganic methods/ h . 'o Sample Preparation. Mr. John E. Colllns is the

supervisor of the Sample Preparation Department, He itsresponsible for both Inorganic and organic sample preparationfor low, medium and high-hazard camples, excludingradiological preparations. ' f

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o Radiological Preparation. Ms. Roxanne Patterson is thesupervisor of the Radiological Preparation Department. SheIs responsible for'scheduling and reviewing the analyticalresults from all radiological sample preparation.

o Radiological Analysis. Ms. Elalne M. Holland is thesupervisor of the Radiological Analysis Department. She isresponsible for scheduling and reviewing the results ofalpha, beta and gamma counting and spectrometry.

PERSONNEL ;

Resumes of key staff members are included in the followingpages.

QUALITY ASSURANCE RESPONSIBILITIES

Procedures for recording and reviewing data at several levelsare employed to minimize human and automated data handlingerrors.

Laboratory Analyst . ,Data review and validation begins with the analyst performingthe analysis. The analyst is responsible for:

1. Utilizing methodology without unauthorizedmodifications.

2. Meeting required QC criteria for any specified tuningand/or calibration requirements (go/no-go criteria).

3. Performing all sample analyses including methods blanks,check standards, replicates and spikes as specified bythe method or project QA Plan.

4. Verification and acceptable performance of samplespecific QC requirements (i.e., surrogate spikerecovery)* ;

5. Recording data in laboratory notebooks, data sheets, andsummary sheets (per Standard Operating Procedure NG012).

6. A minimum of 10% of manual calculations should beindependently recalculated as an initial review.

7. Computer generated calculations should be reviewedInitially and spot checked to verify softwareperformance.

Laboratory Supervisor.. - - - / ' . - •The laboratory supervisor is responsible for the review and

validation of data generated by his/her laboratory componentsof the data include:

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1. Verification of operational parameters such as GCconditions, etc. as required by the specific methodemployed.

2. Review of tuning and/or calibration data to verifymethod specific acceptance criteria.

3. Review of method specific QC data such as surrogatespike recoveries, duplicate precision, spike recoveries,and QC control limits.

4. Review of method specific identification criteriasuch as mass spectra or retention times.

5. Hand calculations of manual and computer generatedcalculations.

Data Review/Validation Group

The data review/validation group is independent of theoperations portion of the laboratory and is responsible for:

1. Screening all data to ensure that the appropriate QCprocedures and criteria were used.

2. Review of method specific identification criteriasuch as mass spectra or retention times.

3. Hand calculations of manual and computer generatedcalculations.

4. Providing summary Information to the QA Manager toobtain approval for the Information Systems group tobegin automated generation of the requisite reportforms.

5. Review of the final data package to ensure Its accuracyand completeness prior to delivery to projectadministration and the client.

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RESUMES OF KEY PERSONNEL

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RESUME: DAVID KENNEDY, Ph.D.PRESIDENT/CHIEF EXECUTIVE OFFICER

MPLOYMENT

• 1966 to date: President and Chief Executive Officer,. > , metaTRACE ; Inc.

• 1980 to 1986: Vice President and St. Louis OfficeManager* "Envirodyne Engineers, Inc.

• 1974 to 19801 Senior Associate, Envirodyne Engineers,Inc.

* 1969 to 1974: Project Scientist/Group Leader, Rohm and, . .... : . ' -Haas *(5d.;;tnX \ _ ... •-...-•

* 1967. to 1969: 'Research Assistant, Ames Laboratory, U.S.. Atomic Energy Commission . -.

SUMMARY OF EXPERIENCE ;:^>^ / / .

Dr. Kennedy is President and Chief Executive Officer ofmetaTRACE, a highly sophisticated analytical laboratoryrecently established in St. Louis, Missouri. Dr. Kennedybrings 20 years of analytical chemistry and corporatemanagement experience to metaTRACE, Before foundingmetaTRACE with Dr; Carol Byington,' he served as VicePresident and St. Louis Office Manager for EnvirodyneEngineers. Under his tenure at Envirodyne, their laboratoryexperienced tremendous growth and expansion. He now presidesover one of the finest laboratories in the nation, equippedwith state-of-the-art instrumentation and capable of alltypes of analyses. As President and CEO, he is responsiblefor all metaTRACE technical, financial and contractualmatters. Highlights of Dr. Kennedy's career include thefollowing: t • • ' . . . .

* Responsible Corporate Officer f or USEPA ContractLaboratory Program Contracts for the analyses of theAnalysis of Organ! cs in Multimedia Samples. Analysisof 2,3,7,8-TCDD and analysis of PCDD's and PCDF's underSpecial Analytical Services., Also served as ProjectPrincipal for Sampling and Analysis Technical ServicesContract (SATS), USEPA," Research Triangle Park, N.C.

• Project Principal for thirteen contamination surveys, performed for the U.S. tfl Army, Toxic and Hazardous

Materials Agency, Aberdeen Proving GrouncL J1D, -defined the. extent and potential for migrtfetlion 'ofchemical contamination at Army Installationsnationwide.

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DAVID C. KENNEDY, PH.D. (continued)

• Project Manager for U.S. Army contract to surveyand recommend alternative for the disposal of the

j Weldon Spring Chemical Plant, a contaminated uraniumfeed materials plant in St. Charles, Missouri.

• Project Principal for the development andimplementation of a closure pigment plan inSt. Louis, Missouri; this project involved the

I neutralization of 130,000 tons of undigested titaniumj ore.

• Program Director for USEPA contracts to developeffluent guidelines and standards of performance

' for the synthetic rubber, organic chemicals,plastics and synthetics, plastics fabrication,

| timber products, petroleum refining, and sealantsI and adhesives industries.

* • Developed zero discharge wastewater treatmentI system and analytical monitoring plan for federal1 research facility using carcinogenic chemicals.

• Managed Industrial research and developmentprojects for the development of air and waterpollution control products and processes based

\ on polymeric adsorbent, ion exchange and liquidI extraction technology; developed process technology

for hydrometallurglcal extraction of metals from ores.

I EDUCATION _

I Ph.D., Analytical Chemistry, Iowa State University, 1969..1 B.S., Chemistry, Iowa State University, 1965.

i PROFESSIONAL DATAI - - . . . , " • . _ - , < . : • . • , •

• Dr. Kennedy is a nationally-recognized authority inthe fields of ion exchange and polymeric adsorption

j technology.

• Recipient of three John C. Vaaler awards forl significant developments in chemical processing.

• Author of over 30 publications and Invited leot«rer. in the fields of * environmental chemistry and cnetfiiealI technology.

• Program Chairman, Chromatography Symposium, 171st i

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DAVID C. KENNEDY, PH.D. (continued)* >: „ f.i i ,,'•'-

- • , . - . . ; . r ;i,rrv , •- •• Program Chairman, Chromatography Symposium, 171st

American Men of Science. ,!

• Member-American Association for the Advancement ofScience, American Chemical Society, St. Louis

• Community College Curriculum Advisory Committee,'University of Missouri,* St. Louis IndustrialAdvisory Board .

A R If 00,5 It 7

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RESUME: CAROL H. BYINGTON, Ph.D.EXECUTIVE VICE PRESIDENT/TECHNICAL DIRECTOR

EMPLOYMENT HISTORY

• 1986 tp date:. Executive Vice President and TechnicalDirector, metaTRACE, Inc.

• 1984 to 1986: Assistant Vice President, EnvirodyneEngineers, Inc.

» 1973 to 1984: Associate, Analytical Chemist,Envirodyne Engineers, Inc.

• 1971 to 1973: Teaching Assistant, University ofTennessee

» 1967 to 1970: Laboratory Assistant, Black HillsState College

SUMMARY Q EXPERIENCE

r

Dr. Byington is Co-Founder, Executive Vice' President andTechnical Director of metaTRACE, a sophisticated analyticallaboratory established in 1986 for the analysis ofenvironmental and radiological samples. She is responsiblefor all technical, project management and analytical qualityassurance functions of metaTRACE. Dr. Byington has 15 yearsof experience in analytical chemistry, laboratory management,and analytical project management. Before founding metaTRACEwith Dr. David Kennedy, she served as Assistant VicePresident and Manager, Analytical Services for EnvirodyneEngineers, Inc. Under her management, Envirodyne' slaboratory more than doubled in physical size and volume ofanalyses and became a leader in the analysis of hazardouswaste. Dr. Byington'.s experience includes the following:• Managed all technical analyses (organic and inorganic)

for laboratory with sales of $2 million per year;responsible for obtaining laboratory certifications fromUSEPA, U.S. Navy, U.S. Army Toxic and HazardousMaterials Agency, and states of Missouri, Illinois andSouth Carolina.

• Project Manager for all analytical tasks for environ-mental contamination surveys at twelve U.S. Armyinstallations nationwide for the U.S. Army Toxicand Hazardous Materials Agency in Aberdeen ProvingGround, Maryland.

• Project Principal for laboratory analyses for tguoundwater monitoring programs and basin characterization , jstudies at the U.S. Department of Energy's Savannah ^~^River Plant in Aiken, South Carolina.

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CAROL H. BYINGTON (continued)

Analytical Manager for USEPA effluent guidelinesdevelopment studies for synthetic rubber, organicchemicals, plastics fabrication and sealants/adhesives industrial categories. .

Project Principal for ell analytical contracts underUSEPA Contact Laboratory Program for the analysis ofsamples from Superfund hazardous waste sites nation-wide.

• Project Principal for Illinois Environmental ProtectionAgency Contract Laboratory Program for the analysis ofsamples from state and federal Superfund sites.

• Project .Scientist for development of continuousmonitoring program to detect trace quantities of - . .

• carcinogens in effluents of a federal toxicologicalresearch facility. ^ " ; ^

• Project Principal for"analyses associated with con-firmation studies performed at four Naval facilitiesfor the U.S. Naval Facilities Engineering Command-Atlantic Division as part of the Naval Control ofInstallation Pollutant Program.

EDUCATION - J ^ i » '

Ph.D., Analytical Chemistry*"University of Tennessee, 1977.B.S., Chemistry, Black Hills State College, ,1970.

PROFESSIONAL DATA -: • / "^ ^ \ • * - ' . " "

• Extensive background in organic and inorganic sampleanalysis Including gas'Chromatography, gas .Chromatography/mass spectrometry, atomic absorptionspectroscopy, liquid Chromatography, etc. .. \ .

; • -. " ' ' '" ',''•''£ *.'*.* '.' ' • ' . ' , . . - • - • ' ' '*" '

• Experienced in development,and implementation oflaboratory quality assurance programs. .

! , .. . -. • • • •"» • IP "« J \f " ' ' ' . i ... » . -

' ' . . . . ' .. i .- ^-. w * i »{>•' . ••' - . f . - . , . .

• ;Member-American'Chemical Society,'Phi Kappa Phi..AirPollution Control Association. . . ,

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RESUME: PATRICK KELLYPROGRAM MANAGER .- RADIOLOGICAL PROGRAMS

EMPLOYMENT HISTORY .

• . 1987 to date: Program Manager, Radiological Programs,metaTRACE, Inc.

• 1983 to 1986: Supervisor, Radiological Services, NUSCorporation

• 1980 to 1982: Laboratory Assistant, BiochemistryLaboratory, University of Pittsburgh

SOMMARY Q£ EXPERIENCE ^ -

Mr. Kelly is responsible for the management of all metaTRACEprojects requiring radiological analyses. He has extensiveexperience in this area, having supervised the radiochemistrylaboratory for NUS Corporation in Pittsburgh .for three years.He was responsible for all work involving radioactivematerial and provided radiochemical and Health Physicsconsultation to industrial and governmental clients, focusingon co-contaminated material. His responsibilities includedreview and validation of all radiochemical data, calibrationsof radiation detection equipment, radiochemical methoddevelopment and training, and development of NUS's QualityAssurance Program for radionuclides.

• Radiation Safety Officer for Laboratory ServicesDivision of NUS; authored amendment to Type B Broad •Scope License with US Nuclear Regulatory Commission,including extensive Radiation Protection Program.Responsibilities included maintenance , of laboratorylicense with NRC, supervision of all health physicsrelated functions, and training for all divisionpersonnel in Radiation Protection and Health Physics.

• Project Manager for work with co-contaminated material.Developed Health and Safety Protocol for standardchemical analyses on medium-level radioactive samples;clients' included US Department of Energy contractors,and nuclear utilities throughout the United States;projects involved organic, inorganic and radiochemicalparameters. Also managed project for local utilityfor bioassay analyses on plant workers.

• Developed and executed procedures for all types afradiochemical analyses (10 CFR 61* environmental,.and transuranic samples); operation and calibrationof radiation detection equipment (gas proportional,liquid scintillation, alpha-gamma and beta-gamma

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PATRICK T. KELLY (continued)

Mt'i': v ' . ; ' . ' . :coincidence counting systems, alpha and gamma spectro-. meters).

EDUCATION • . - :,'?; ;V C "A fi 1 !'" :

D.S., Chemistry/Environmental Biology, University ofPittsburgh. 1982. •t3tiw"••;'•- • •

M.S., Health Physics, University of Pittsburgh, 1967. •

PROFESSIONAL DATA ( ; ,«?H ,y* ;.\.;.... v^- ; ',:.>C *f* i; • . . .. .. .- ;

. h, • - • ** Member, American Association for the Advancement ofScience, American Nuclear Society, Health Physics 'Society "*« *'[-:

; • :* f« £ if: ""I

' fi.-jo I'ji

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RESUME: MARLEAH M. MARTINPROJECT MANAGER

EMPLOYMENT HISTORY

o 1987 to date: Environmental ProjectManager, metaTRACE, Inc.

o 1979 to 1987: Assistant Chemist, Peabody Coal CompanySUMMARY fig EXPERIENCE

As Environmental Project Manager, Ms. Martin is responsiblefor the day-to-day management of projects in theenvironmental area. She reports to the metaTRACEEnvironmental Program Manager and represents her clients'•interests at metaTRACE. Ms. Martin brings extensiveexperience in environmental chemistry to her position atmetaTRACE. She formerly worked as a chemist for Peabody CoalCompany and is familiar with procedures, methods andinstrumentation for the analysis of environmental samples.Her 7 years of experience and expertise includes thefollowing:

o Experienced in handling laboratory instrumentation forion, metal, mercury, sulfur, and other analyticaldeterminations for coal, water, soil and trace samples.Responsible for interacting between sections of thePeabody. Coal Company laboratory to optimize instru-mentation usage, scheduling, and workloads.

o Coordinated acid rain analysis project for PeabodyCoal Company in conjunction with Bituminous CoalResearch and the National Coal Association.Responsible for analysis of rain samples, compil-ation of data, development of correlations andother statistical data from monitoring stations.

o Participated in various biological sampling andidentification•projects.

o Participated in national air pollution study in St.Louis for Harvard University (through Southern IllinoisUniversity-Edwardsville); responsibilities includedmonitoring air. quality, sampling and analysis on SOx andNOx pollutants. .

EDUCATION

M.S., Environmental Science, Southern Illinois University ^—4at Edwardsville, 1985.B.A., Biology (minor: Chemistry), Southern IllinoisUniversity at Edwardsville, 1976.

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RESUME: LAURY R. TAAKEENVIRONMENTAL PROJECT MANAGER

EMPLOYMENT ."IISTORY :J :!"

* 1987 to date: v "Environmental Project Manager, imetaTRACE, Inc.

• 1981 to 1987: Environmental Scientist, Peabody CoalCompany,; "Illinois Division

* 1978 to 1981: Area 'Water Quality Coordinator, Peabody. -• ' 'Coal'Company* Illinois Division

NUMMARY C£ EXPERIENCE

Mr. Taake brings nine years of technical and laboratoryexperience to his position of Environmental Project Managerat metaTRACE. He is responsible for Initiating andimplementing government and industrial contracts foranalytical services. He manages projects to assure that allcontractual, quality control, scheduling and cost objectivesare met. He prepares final reports for clients andcoordinates his projects with the laboratory manager, sectionmanagers and Project Managers to assure that both client andinhouse goals are achieved. His experience includes thefollowing:

• As as Environmental Scientist for Peabody Coal Company,collected, analyzed and interpreted water quality datain accordance with applicable state and federal regula-tions. Included sampling, monitoring and reporting ofbaseline groundwater and stream monitoring systems.Processed data -into report form and made available toregulatory authorities. Accompanied regulatoryauthorities on inspections and submitted follow upreports to management.

* Entered, retrieved, analyzed and graphically presentedmonitoring data through Water Quality Data Base System.

* Coordinated Peabody Coal, Illinois Division, RCRAhazardous waste, waste oil and PCB compliance programs.Included identifying and Inventorying all chemicals ateach mine site, completing hazardous waste manifests,and inventorying and testing electrical transformers.

• Coordinated and developed wildlife programs feu; P ajbodyCoal. Illinois .Division.

• Project Supervisor, production well/pipeline project.Duties included coordinating contractors' site visits.

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LARRY R. TAAKE (continued) V J•*+- • >* ^i

overseeing acquisition and timely arrival of materials.supervising installation of production well and

, associated pipelines, and ensuring project completionwithin contract limits.

; • As Area Water Quality Coordinator for Peabody Coal,l Illinois Division, responsibilities included field

sampling, monitoring and reporting/coordinating ofI permitted and other mine related water discharge systems; for southern Illinois and western Kentucky mining

operations. Performed laboratory analyses foracidity/alkalinity, pH and total suspended solids.

EDUCATIONt - ' " ' : ~ . .

| B.S., Zoology/Wildlife Management, Southern IllinoisUniversity - Carbondale, IL, 1978. . .

I Post-graduate, Business Administration, John A. LoganCollege, Carterville, IL, 1981-82.

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RESUME: PAUL B. IIUMBUKGPRINCIPAL CHEMIST

EMPLOYMENT HISTORY - • - . < - : f

* 1986 to date: Principal Chemist, metaTRACE, Inc.

• 1984 to 1986: Inorganic Laboratory Manager,Envirodyne Engineers, Inc.

• 1977 to 1984: Environmental Chemist and SafetyManager,-Envirodyne Engineers, Inc.

• 1975 to 1976: Teaching Assistant, University ofr Missourl-Et. Louis

SUMMARY OF EXPERIENCE r -J "v

Mr. Humburg is an experienced chemist who brings nine yearsof laboratory management and analytical spectroscopyexperience to'his position with metaTRACE, a new, ' .sophisticated laboratory founded in 1986 in St. Louis,Missouri. Prior to Joining metaTRACE, Mr. Humburg wasassociated with Envirodyne Engineers as Inorganic LaboratorySection Manager, supervising wet chemistry and instrumentalanalyses including spectroscopy (atomic absorption, ICP,etc.) His experience includes the following:, \:.-1 . - .. . '• - " • !-;•-'.-^ r>; :.- - - • - - •• Safety Manager for field and laboratory tasks associated

with contamination surveys performed for the U.S. Armyat Detroit Arsenal, St. Louis Area Support Center andthe Riverbank, CornhusKer, and Louisiana Army ammunitionplants.

* Served as Internal Safety Manager and Chairman, SafetyCommittee at Envirodyne; responsible for establishingand implementing safety program for high-hazardlaboratory and instructing laboratory personnel insafety requirements for the handling, storage anddisposal of hazardous wastes.

* Inorganic Analysis Manager for contamination surveysof twelve government installations for U.S. ArmyToxic and Hazardous Materials Agency (USATHAMA).

• Extensive experience performing metals analysis onsoils, sediments and water; conducted trace metalanalyses associated with NPDES permit programs(thallium, silver, arsenic, selenium, antimony).Verification of discharge pollutants includedanalysis of turn-around deadlines.

• Project Chemist (metals analyses uses) for USEPAproject for the development of effluent guidelines

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PAUL B. HUMBURG (continued)

and standards of performance for various industrialcategories.

• Accredited by State of Missouri for metals analysesin drinking water samples. .

• Manager, Inorganic Analyses for hazardous wastemonitoring programs at U.S. Department of Energy'sSavannah River Plant in Aiken, South Carolina.

* Manager, Inorganic Analyses for U.S. GeologicalSurvey project to analyze samples from AberdeenProving Ground, MD; analysis of samples from theGreat Lakes region; and water quality testingprograms conducted by the U.S. Army Corps ofEngineers (St. Louis).

• Assisted with internal tracing procedures usingdyes and a Perkin-Elmer 100 x-ray unit while •- 'stationed at the 21st General Hospital,.-Ft. LeonardWood, Missouri.

EDUCATION

B.S., Chemistry, University of Missouri-St. Louis, 1977.

PROFESSIONAL DATA

• Member-American Chemical Society, Society forApplied Spectroscopy

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RESUME: . EUGENE M. WATSONi j CHEMIST

, EMPLOYMENT HISTORY i - .1" ... - -.:/J Jif •; . •• -- - •' ' - " " : - -"'

* 1986 to date: Chemist, metaTRACE, Inc.

' • 1985 to 1986: GC Chemist, Gulf Coast Laboratories

, • 1982 to 1984: Laboratory Assistant, Blackburn College'i

SUMMARY EXPERIENCE

Mr. Watson is an experienced chemist in the areas of gasChromatography, gas Chromatography /mass spectrometry, andgeneral wet chemistry. Specific examples of his proficiency

! are listed below. *• Performed extraction, analysis and documentation of

I volatile organic acids, base neutrals/ac'ids,1 polychlorinated biphenyls, hydrocarbons and other

organic compounds in matrices that included water,waste, soils, and foods.

-i j • Performed dioxin analyses by GC/MS for metaTRACE• . -— USEPA contract for rapid response dioxin analyses;I project required 16 hour turnaround of results.

• Performed gas Chromatography analyses for Weldon Springj Sites Remedial Action Project.

• Experienced in performing analyses within guidelines ofj a strict quality assurance/quality control program that/ meets or exceeds USEPA Contract Laboratory Program

requirements.

i * Methodologies utilized include USEPA Methods 601, 602,' 604, 624, and 625.

1 • Designed and implemented scheduling process for organicI Chromatography division.

. * Conducted field sampling; collaborated on analyticalI ' research projects.

. • Experienced in operation/maintenance of Hewlett-Packard 5890 and 5880 GC; Perkin Elmer 410 HPLC;

1 Hewlett-Packard 5.890 and 5995 GC/MS; Perkin ElmerSigma 3B and 6410 GC; Tracor 565 GC; Varian 3700

i GC; Tekmar LSC-2 and LSC-3 concentrators.

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EUGENE M. WAT50N (continued)

* Experienced in analysis of environmental samplesusing Alpha/Beta Proportional Counter.

EDUCATION

B.A., Biology (minor Chemistry), Blackburn College, 1984

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' _ RESUME: ELAINE M. HOLLAND,, RADIOCHEM1ST; RADIATION SAFETY OFFICER ,

lX*- EMPLOYMENT HISTORY

• 1986 to date: Radiochemist, metaTRACE, Inc.

.• 1980 to 1985: Chemist, Goodyear-Atomic Corporation,Piketon, OH

• 1978 to 1979: Teacher, Waverly City Schools, OH

• PUMMARY £E EXPERIENCE ^ , ,

Ms. Holland is an experienced Chemist formerly with thei Goodyear Atomic Corporation in Piketon, Ohio, where she wasj responsible for performing routine chemical analyses and

methods research and development. She trained personnel inproper analytical techniques and safe handling practices of

I radioactive and hazardous materials. Aside from her1 radiological chemistry duties at metaTRACE, she serves as the

company's Radiation Safety Officer. Some of herI accomplishments are as follows: • •'

• Skilled in a. wide range of analytical methods with oversix years of experience in analytical techniques andinstrumentation. *

• • Experienced in training personnel in accepted laboratoryj and radiological practices.•

• Consolidated, edited and revised analytical procedures.' used in Chemical Analysis Department at Goodyear Atomicj Corporation.

* .Constructed, installed and operated state-of-the-artI gamma spectrometer.i

* Installed, calibrated and operated state-of-the-artinductively-coupled plasma spectrometer. •

e Six years experience analyzing fissionable materials forspecific isotopes and total activity; included an equalbalance between general wet chemistry methodology, andinstrumentation (gamma spectrometry, alpha spectroscopy.counting techniques, liquid scintillation analysis),

• Performed radio-pharmaceutical analyses; experienced inhandling curie levels of radioisotopes.

• Extensive experience in low-level alpha, beta and gammaradionucllde detection in environmental samples^

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L

ELAINE M. HOLLAND (continued)

EDUCATION • .

B.S., Education (Science), Ohio State University, Cum Laude,1978

PROFESSIONAL DATA/PUBLICATIONS

* Member, American Chemical Society

* Publication: "Comparison of Several AnalyticalTechniques for the Determination of Technetium in theEluants of. Commercially Available 99HO/99TC RadionuclideGenerators", with M.E. Holland, W. R. Heineman and E.Deutsch, Ini*. Jour. Applletj Had, and Isotopes. Vol. 37,No. 2, pp. 165-171, 1986.

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RESUME: . ALLEN M. FIELDENVIRONMENTAL PROJECT MANAGER

EMPLOYMENT HISTORY

* 1987 to date: Environmental Project Manager, .metaTRACE, Inc.

• 1985 to 1986: Equipment Evaluator/Master EquipmentList Leadman, Illinois Power Company

* ' 1980 to 1983: Director Environmental/Right of WayDepartments, Soyland Power Cooperative

gUMMARY QE EXPERIENCE

Mr. Field brings 5 years of technical experience tometaTRACE, Inc. He serves as Environmental Project Manager,acting as liaison between the laboratory and metaTRACEclients. Significant achievements in his career include thefollowing:• Project Manager for environmental analysis projects for

industrial/governmental clients involving both Inorganicand organic analyses; assures that all clientrequirements are followed and is responsible for thereporting of all results, QC procedures, etc.

• Obtained construction and operation permits for powerplant and tranismission facilities; conducted publicand interagency information meetings to gain acceptanceof'corporate projects.

• Provided liaison to federal, state and local regulatoryagencies and coordination with architect/engineer firmsto incorporate pollution control requirements.

* Selected power plant sites; performed appraisal servicesfor property values; negotiated real estate acquisitionsand managed corporate real estate holdings.'

• Compiled and classified mechanical and electricalcomponents and instrumentation utilizing designdrawings, equipment lists» vendor manuals, plantmodifications, purchasing and receiving records,and various nuclear codes and standards.

• Performed auditing and field verification of computerrecords and walking down plant systems to ensure thatinstalled equipment complied with data base records,design standards and safety requirements.

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ALLEN M. FIELD (continued) ,

Education

M.S., Zoology, Eastern Illinois University, 1982.B.S., Environmental Biology, Eastern Illinois University,

1974.

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RESUME: RICHARD H. MANHZMANAGER, ENVIRONMENTAL PROGRAMS

EMPLOYMENT HISTORY —• - • • : ••>•.'• f r • • ; "' ". • ' ' •. .•t ' • - - • _

• 1986 to date: Manager ifef Environmental Programs,metaTRACE, Inc. .

• 1985 to 1986: Program Manager, Envirodyne Engineers

• 1980 to 1985: Corporate.Biologist, Peabody Coal Co.

• 1978 to 1980: Assistant Chemist,-Peabody Coal Co.,; Central Laboratory

• 1978: Pharmacy technician, Barnes Hospital,St. Louis, MO

SUMMARY OF EXPERIENCE - ': ) '""" ••**• •"•«•"••••"«• _ .V^»? t '..!'• .' ' -

Mr. Mannz brings eight years of technical and laboratoryexperience to metaTRACE, Inc., a newly formed analyticallaboratory in St. Louis,. Missouri. As Manager ofEnvironmental Programs, he is responsible for implementationand fulfillment of analytical contracts from government andprivate industry sources; direct projects to ensure thattechnical goals, quality assurance requirements, internal andexternal scheduling, and costs are coordinated tosuccessfully complete a project. He also arrangespreparation of final reports and invoices for servicescompleted; coordinates with the laboratory manager, sectionmanagers and client project managers to meet both client andin-house goals. He most recently served as a Project Managerfor Envirodyne Engineers.- His experience includes thefollowing:

* Project Manager for the Illinois EnvironmentalProtection Agency Contract Laboratory Program for-theanalysis of samples from state and federal Superfundsites.

* Managed and coordinated all phases necessary in theDuPont Project SRP Groundwater Monitoring Program, anetwork of 180 wells sampled quarterly for groundwatermonitoring programs.

• Project Manager for the laboratory analyses for a U.S.Navy program involving the characterization of threefuel station sites.

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RICHARD II. MANNZ (continued)

• Corporate Biologist duties at Peabody Coal Companyincluded producing environmental documents for variousregulatory requirements; water chemistry monitoring andInterpretation; aquatic and terrestrial taxonmicidentification, interpretation and technical writeup;participated In planning, organizing and budgetingdepartmental activities.

* Mr. Mannz performed general inorganic laboratoryanalyses including atomic absorption, electrode,analyses, gravimetric procedures and other environmentalanalytical procedures as an Assistant Chemist with thePeabody Coal Company, Central Laboratory in Freeburg,Illinois.

• - Mr. Mannz has presented and published several scientificpapers and a book on various environmental topics.

EDUCATION

M.S., Environmental Science, Southern Illinois University atEdwardsville, 1984.

•B.S., Majors in Environmental Biology and Zoology /ChemistryMinor, Eastern Illinois University, 1977.

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RESUME: CHRISTOPHER D. SCARPELMNOQUALITY ASSURANCE MANAGER

MPLOYMENT

o 1986 to date: .Quality Assurance Manager, metaTRACE

o 1982 to 1968: Senior Scientist, EG&G Idaho, Inc.

o 1978 to 1982: Research Assistant, Univ. of Iowa \pCJMHARY QE EXPERIENCE ', . . -

- -., " ,-.-.' -- t ,¥,;•• V. (•-''"•: "-"' ' - ' " • " ' •Mr. Scarpellino has 10 years of experience in environmentalchemistry and engineering. His wide range of experienceincludes project management, quality assurance/qualitycontrol and research. Highlights of his career include thefollowing: . '

o Served as Quality Assurance Of ficer for the EG&G INELHazardous Waste Site Evaluation Program, associated withConsent Order /Compliance Agreement between DOE-ID and EPARegion X; assisted in the development of computer-based datamanagement system for chemical analytical data validation,verification and evaluation to satisfy requirements of EPAContract Laboratory Program; reviewed analytical results,assisted in sampling and analysis plan development; providedoversight of field QA efforts.

o Task Manager of independent laboratory verificationprogram for DOD demonstration project to evaluate electricaltransformer PCB ret refill technologies designed to achievereclassification of transformers to non-PCD status.

o Program Coordinator for EG&G SARA Title III ComplianceProgram to ensure compliance with Federal, state and localright-to-know regulations, including worker training and MSDStracking systems, and hazardous materials inventory system.

o Program Manager for DOD Hazardous Waste Analysis PlanUpdate including detailed hazardous waste sampling andanalysis plan development to meet EPA and State of Californiaregulations; provided contractual guidance and subcontractingservices for laboratory analyses, and modifications ofhazardous waste inventory and worker right-to-knowdocumentation systems.

o Provided technical review and evaluation of chemicalsampling and analyses for DOD industrial waste collectionsystem evaluation and DOD dioxin incineration programcluding full-scale EPA trial burn, and delisting of

residual material.

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^ CHRISTOPHER b! SCARPELLINO(continued)

o Member, initial task force to determine RCRA compliancestatus of EG&G/INEL facilities.

EDUCATION

M.S., Civil and Environmental Engineering, University ofIowa, 1982.

B.S., Fisheries and Wildlife Biology, Iowa State University,1977.

PROFESSIONAL DATA

Member, American Chemical Society (since 1978) ,. AmericanSociety for Testing and Materials (since 1983) /

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RESUME: KENNETH J. BAUGHMANASSISTANT VICE PRESIDENT

* . MANAGER, PROJECT ADMINISTRATIONEMPLOYMENT HISTORY *^;

• " ' " .- " ' ' . . -

9 1987 to date: Assistant Vice President and Manager/. Project Administration, metaTRACE, Inc.

• ' ' • ; , • ' ' ' ' » "r* ^ J ' • t " ^ .: . .* 1985 to 1987: Supervisor, Organic Analysis Group,

Western Research Institute "

• 1983 to 1985: Senior Scientist, Lockheed Engineeringand Management Services Company

• 1980 to 1983: Scientist/Organic Analysis Coordinator,Radian Corporation

f - - - 1 v

• 1979 to 1980: Laboratory Manager, Enviro-MedLaboratories, Inc. , .

• * 1975 to 1979? Forensic Chemist, Louisiana State PoliceCrime Laboratory * .

UMMARY EXPERIENCE

I j Mr. Baughman is an Assistant Vice President of metaTRACE, ."-" Inc. , a new and highly sophisticated analytical laboratory in

St. Louis, Missouri. He also holds the position of Managerof Project Administration With supervisory responsibilitiesfor all metaTRACE Program/Project Managers. . ^ -He brings to metaTRACE 12 years of experience in GC, GC/MSand HRMS analytical procedures and methodology, high hazardanalyses and laboratory quality; assurance. His experienceincludes the following: «.%-"* -'' '

• Drafted and implemented USEPA' s high concentrationorganic protocol and managed one of only three CLPlaboratories to provide rthic service to EPA. .

Designed and developed a part-per-trillion dioxin/furan methodology and capability for GC/HRMS.

Rewrote the USEPA Contract Laboratory Protocol forlow/medium organics analysis.Served as technical expert during USEPA pre-award andpost-award on-slte laboratory evaluations.

Served as USEPA (EMSL-LV) technical reprdsenxajcoiv atnumerous national EPA caucuses and conferences onanalytical methods, protocol revision and data review

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KENNETH J. BAUGHMAN (continued)

• Implemented and managed EPA CLP contract whichincluded numerous Special Analytical Services (SAS)projects for specialized analyses.

h

• Performed complex chemical analyses utilizing bothFinnlgan and Hewlett-Packard GC/MS systems. Experiencedin mass spectral interpretation, data review, qualitycontrol, data validation and reporting.

EDUCATION

B.S. Biology, University of New Mexico, 1974Advanced Courses in Chemistry, University of Virginia, 1978.Advanced Courses in Chemistry, University of Texas, 1980.Numerous short courses, 1975-1984.

PUBLICATIONS

R.L. Spragglns, R.G. Oldham, K.J. Baughman and C.L. Frescott,"Organic Analysis Using High-Temperature Purge and TrapTechniques,** Advances in tha Identification and Analysis ofOrganic Pollutants in Water. Lawrence H. Keith ed. , p. 747.

R.D. Cox, K.J. Baughroan and R.D. Earp, "A GeneralizedScreening and Analysis Procedure for Organic Emissions fromHazardous Waste Disposal Sites,** Management g£ UncontrolledHazardous Waste Sites. 1982, Third National Conference.

**A Comprehensive Scheme for Auditing Contract LaboratoryData-Military 105 D,M K.J. Baughman, J.C. Fan, J.W. Fowler,F.C. Garner, K.S. Kuraar and M.T. Homsher, LockheedEngineering and Management Co., J.M. Moore and J.G. Pear son,US Environmental Protection Agency-Environmental MonitoringSystems Laboratory, Las Vegas, NV. Presented at AmericanSociety of Quality Control, Raleigh, NC, September 12, 1984.

L.P. Jackson. W.E. Blanton, S.L. Chong and K.J. Baughman,"Characterization of Solid Wastes from Conventional CoalCombustion Processes,** 1986, US Dept. of Energy, MorgantownEnergy Technology Center, Report of Investigations, ContractNumber DE-AC21-84LC11059.

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RESUME: . T. WILL SOLOMONASSISTANT VICE PRESIDENT

EMPLOYMENT HISTORY MrU:: ' ;

• 1986 to date: Assistant,Vice President, metaTRACE, Inc.

• 1964 to 1986: Manager of Laboratory Operations,Envirodyne Engineers, Inc.

•i * • ! ; * ' ' '• . . . ( , . , ' , . . • - "

• 1979 to 1984: Manager. Pesticide/Contaminant andVitamin, "Drug.and Nutrient Laboratory;Hazardous Waste Manager; R&D Safety '.Manager; Radiation Safety Officer,Ralston Purina Company

• 1973 to 1979: Group.Leader/Analytical Chemist, RalstonPurina Company

SUMMARY OF EXPERIENCE

Mr. Solomon brings 12 years of technical and laboratorymanagement experience to metaTRACE, a state-of-the-artanalytical laboratory in St. Louie, Missouri. He has , ... ,extensive knowledge of organic and inorganic Instrumentalanalyses, quality assurance protocols and laboratory safety.Most recently, he served as Operations Manager of theEnvirodyne Engineers laboratories.: His experience includesthe following:

* Project Manager for metaTRACE USEPA contract if or the "rapid response analysis of dipxin; contract involvesanalysis of up to 100 samples per day by GC/MS withanalyses completed within 16 hours of sample receipt.,

• Manager, Organic Analyses for basin characterizationstudies and groundwater monitoring program at theU.S. Department of Energy's Savannah River Plant inAiken, South Carolina.

• Coordinated laboratory analyses of samples collectedat hazardous waste sites nationwide under USEPAContract Laboratory Program.

• Organic Analysis Manager for samples collectedduring environmental contamination surveys at U.S.Army installations nationwide for the U.S. ArmyToxic and Hazardous Materials Agency.• i

* Project Manager for dioxin analysis of samples - - - - -collected at various Missouri sites for USEPARegion VII.

a r* i i '* * i* I H :i w L- '- f.' / i r-

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T. WILL SOLOMQN (continued) . j

• Manager of Ralston Purina pesticide/contaminantlaboratory which included pesticide residues, PCBs,PBBs, Aflatoxln,-priority pollutants, environmentalresidues and other miscellaneous fat soluble analyses.

• Developed and managed hazardous waste managementprogram including the ordering, storage, distributionhandling and disposal of hazardous materials; hasworking knowledge of local, state and federalregulations, including Department of Transportationrequirements. •

• Developed and implemented laboratory safety program(including medical surveillance) and emergencyprocedures.

EDUCATION

M.A., Business Administration, Webster University, 1980.B.S., Chemistry, University of Missouri, 1971.PROFESSIONAL DATA/PUBLICATIONS

• - ' •• • Member, Association of Official Analytical Chemists

(Quality Assurance and Safety Committees), AmericanChemical Society.

• Past Member, Executive Committee* National SafetyCouncil R&D Section; Advisory Board, National SafetyCouncil, St. Louis Section.

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RESUME: . ROXANNE PATTERSONRADIOLOGICAL SAMPLE PREPARATION

EMPLOYMENT HISTORY

• 1988 to date: Radiological Sample PreparationSupervisor, metaTRACE, Inc.

• 1985 to 1988: Supervisory Analyst, Radiochemistry, •University of Iowa Hygienic Laboratory

* 1983 to 1985: Technician, Environmental Microbiology,University of Iowa Hygienic Laboratory

• 1979 to 1983: Technician, Department of Pathology,University of Iowa Hospitals/Clinics

SUMMARY EXPERIENCE

Ms. Fatterson is an experienced radiochemistry' supervisoryanalyst formerly associated with the University of IowaHygienic Laboratory in Iowa City, Iowa. Her experienceincludes the following:* Conducted gamma spectroscopy analyses of samples under

Nuclear Regulatory Commission contract.

* Performed radiochemical analyses of environmentalsamples for NRC, Iowa State Department of NaturalResources and private sector clients.

• Compiled radiochemical data; formulated reports ofdata to clients.

* Conducted nitrate analyses of drinking water samplesusing Technicon Autoanalyzer II.

• Performed microbiological, chemical and microscopicanalyses of water and milk samples.

• Prepared specimens for hematology and chemical analysis.

EDUCATION

Iowa Methodist School of Nursing, Des Moines, IA, 1967-66.University of Iowa, Iowa City, IA, 1982.

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SUMMARY OF PROJECT EXPERIENCE

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SUMMARY OF PROJECT EXPERIENCE.:::':! f - "• ' . ..' '

Procurement Activity/Contract ing Officer , '..,-.-MK-Ferguson Company - ' • 'ri -(for US Department of Energy) ,Weldon Spring, MO *Subcontract Administrator: Kon Lee (314)441-6080

Contract No./Type3569-1002-1978/Unit Pricing-Hot to Exceed

Award Cost/Final Coat1) FY 87: $950,000/$420,0002) FY 68: $1,226,000 not to exceed3) FY 89: $700,000 not to exceed ;

: '. , '.. ... .. ., •- •• , ,: ;fw::./ " " ' ^ • / ~ ;//'Period of Performance t c; . *'1) FY 87: 3/87-11/87 ^r2) FY 68: 12/67-9/8B ;3) FY 89: 9/68-9/89 ? ,1 •

. : • , . . '• -. - ?.'7 l " ' ' • • : " ' f /"The MK-Ferguson Company is the Project Management Contractorfor the US Department of Energy for the Weldon Spring SitesRemedial Action Project (WSSRAP): An extensivei ten-year,;$397 million remediation program to decontaminate the sitewas begun in 1986. The Weldon Spring Site incorporates amothballed uranium feed materials production plant, a nearbyquarry and adjacent properties and environs. Actions will bedirected toward remediating coils, eediments, waters andstructures contaminated primarily by low levels of naturaluranium and thorium, TNT,;and asbestos. ''

metaTRACE was selected to analyze environmental samples fromthe site for chemicals, explosives and radiological . .contaminants so that MK-Ferguson can plan, monitor andcertify cleanup actions. Large numbers of environmentalsamples have been analyzed for such parameters as natural -uranium, isotopic thorium, radium 226 and 226, prioritypollutants, TNT, DNT* and asbestos. metaTRACE has developedand maintains a rigorous quality assurance/quality controlprogram for this project which is closely monitored by MK-Ferguson. _ -; . - - - .•?•.; 'to :^le'<U :' " ••/- -*'";• ;|"-' i_'-'- •/-,-.. -

I * "" — • ' " ' '* '' \ I , !* im- 1 V'- >P * * •"'•" L " - »

A unique aspect of this project has been massive datamanagement requirements, metaTRACE developed and implementeda remote data transfer system to expedite the flow of data tothe client and insure data quality. All quality assuV^d,analytical data in our Laboratory Information Management';" : ~System (LIMS) computer is transmitted daily to the client'scomputer system via a modem. Thus, on a daily basis, theclient has direct access to the moct recent validatedanalytical results and is able to make rapid assessments ofongoing work and initiate field changes, if nen»«-—-, duringthe course of on-site activities.

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Procurement Activity /Contract ing OfficerE.I. duPont de Nemours & Co., Inc.Savannah River Plant, SCContracting Officer: M.B. Spletzer (803)725-2433

Contract No . /TypeAX-843925/Indefinite Quantity

Award Cost/Finalnot to exceed $3,557,000/ work in progress

Period of Performance ,5/88-5/91

metaTRACE was selected to provide sampling and analyticalsupport to a series of different projects at the DOE'sSavannah River Plant. The scope of- work ranges from a.background soil study to the analysis of samples from areascontaminated with constituents of both chemical andradiological origin. The analyses performed include thecomplete range of radiochemical parameters from fissionproducts via gamma spectroscopy to the naturally occurringUranium chain nuclides using alpha spectrometry; ICP and AAmetals;, physical characteristics; and Appendix VIIIcompounds. All analyses involve electronic transfer of dataTha specific parts of this project are detailed below.

Release Qrdfir. Mo^ JL ~ it Background Soils Study whichinvolves the inorganic and radiochemical characterization ofvarious sites and development of appropriate Inorganicsampling protocol for metals analyses.

RaJgasQ CrdiC H°- 8 • Analysis of soils samples from theSeparation F Area A-Llne for volatile organ ics, metals andradiochemical, parameters. ,

. .

Release Ordar No. jii Analysis of soil cores from the 716-AMotor Shop Seepage Basin and the D-Area Oil Basin fororganlo, inorganic and radiochemical* parameters, Including EPToxicity Extraction and analyses. . '

Raleaaa Order No.' 10: Analysis of soils from the BurningRubble Pits for organic and inorganic analyses. Allparameters required Contract Laboratory Program (CLP)Protocol for data generation ands reporting.

' " , ' • . -, • •* ' ' • . . - • *" " •'"•.""'Release Order No. 11: ; Analysis of archived soil n amnJ.ea_ fromthe L-Area Oil and Chemical Basin for a full settafradiochemical parameters. • .

" '

Release Order flo. 12; Analysis of radioactively ;contaminated water samples from the F and H Area Seepage. t - " •• ' - • • , - • ( • . . .

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Basins for physical, inorganic and radiochemical parameters.Gamma spectrometry data were required two weeks from samplereceipt. ' . . - . . - , - o n*fc<' t - . • , - . * - ' , . . _ . . ., . • r , ' • . • - • • . - - , . . - . - • , • - ' • - . ; ' , ' - - .

, ... - j-* i- •*• ?v-i«« T*r- • '•' - .' ' . , , '. ' . . . , . , . - < . - - , - r^-itjXi*.**"-" • " ' * ; ' ; " ' , • " ' . :

Procurement Activitv/Contrltetlng OfficerLaw Environmental, Inc. not = >Kennesaw, -GA . - j -.= . - ; .r , • ' ' ".' ,Project Manager: D. Collier Jackson (404)421-3400 .

Contract No. /Type e-:: tf" :r f87063/Unit Pricing v - s'rJ: : ' . . ; . '

Award Price/Final Cost$65,000/$65,000

Period of Performance -8/87-2/88

- - ^ - - - : • T * " , * *Law Environmental, Inc., under contract to the US Army Corpsof Engineers, performed a remedial investigation to establishthe extent of surface contamination at the Weldon SpringTraining Area, Weldon Spring, Missouri. metaTRACE performedall chemical analyses on coil, sediment and surface watersamples required for this investigation. Soil/sedimentsamples were analyzed for volatile organics, semi-volatileorganics, nltroaromatics, sulfur, dioxin (2,3,7,8-TCDDisomer), DDT and RCRA metals. Surface water samples wereanalyzed for volatile organice, semi-volatile organics,nitroaromatics, nitrate, fiulfate and RCRA metals. '. . ,, -

Procurement Activity /Contracting OfficerOS Army Toxic and Hazardous Materials AgencyAberdeen Proving Ground. f4fl) *r- >Contracting Officers Rep. * Hary Ann Ryan

671-3348' :

Contract No. /Type vir -r - ^Contract No. DAAA15-87-D-0014/Indefinite Quantity

Cost/F nal Cost$10 , 000 , 000/ongoing

Period flf. Performance,6/87-6/92 -•t.)\-i;-i»v{tcr) rf«6fr:.-.: -- • :-• '•

The US Army Toxic and Hazardous Materials Agency (t&AtttAMA~)has an ongoing requirement to Identify and quantify productsand byproducts which may be found on or near militaryinstallations as a result of past or ongoing manufacturing,demilitarization, testing, storage or disposal operations.The extent of specific contamination ' * * ' * "^cationof potential sources is important if • pi, nnc 7 complement

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or improve comprehensive cleanup programs. In addition,USATHAMA monitors the progress at installations whereremedial Investigations have been completed. metaTRACE- isproviding analytical laboratory services in support andimplementation of various Installation restoration programs.Under this contract, metaTRACE is analyzing soil, surfacewater, groundwater, sediment, and air samples to define theareas and level of contamination. The analytical dataprovided by metaTRACE is being used to determine the extentof contamination at installations, determine possible sourcesof contamination, and determine the potential forcontamination migration. All data produced is of a qualitywhich may be used in litigation.

Procurement Activity /Contracting OfficerDSEPAWashington, DCContracting Officer: Angelo Carasea (202)382-3115

Contract No . /Ty pa " ' • . ;Contract No. 68-01-7441/Indefinite QuantityAward Cost/Final Cost , ' . '$7 , 800 f 000/ongoing

Period of Performance7/87-7/92

metaTRACE was awarded the rapid response dioxin analysiscontract for the USEPA. metaTRACE is analyzing environmentalsamples by HRGC/LRMS for the presence of dioxin to supportUSEPA Region VII remedial action programs. This contractcalls for analyses to be completed within 16 hours of samplereceipt and transmitted electronically to the USEPA RegionVII Kansas City office.. metaTRACE has analyzed soil samplesat the rate of 100 per day with samples being received by2:00pra with results transmitted electronically to the clientby 6: 00am the following morning.

Procurement Activity /Contracting OfficerDames & Moore* Inc.(for US Navy)Bethesda, MDProject Manager: Dr. Steve Lemont (301)652-2215

Contract N o . /Typ« . . .Not Applicable/Unit Pricing

Award Price/Final Cost$120,000/$120,000

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Period of Performance3/87-11/88

Dames & Moore, under contract to Martin Marietta for the USNavy, is performing site contamination surveys at Naval andAir Force installations. Phase I Involved a survey of theGreat Lakes Naval Training Center near Chicago, IL. "metaTRACE performed all chemical analyses required for thissurvey. The survey focused on six areas of concern at the,training center and involved the analysis of groundwater .samples from 52 monitoring wells for TDS, TOG, volatileorganics (method 624), chloride, zinc, iron, lead, mercury,oil and grease, PCBs, chromium and tetraethyl lead. Inaddition, metaTRACE analyzed 86 soil samples for lead, zinc,chromium and volatile organics (method 624). This projectrequired that metaTRACE receive laboratory certification fromthe Naval Energy and Environmental Support Activity (NEESA)in Port Hueneme, CA. . .: t (

Procurement Activity/Contracting OfficerUSEPA Contract Laboratory ProgramWashington , DCProject Officer: Angelo Carasea (202)382-3115

Contract No . /TypeContract No. 68-01 -7417/Indefinite Quantity •

Cost/Final Cost$869 , 000/ongoing

Period of Performance • .7/87-7/90

metaTRACE is * participant in the USEPA Contract LaboratoryProgram, performing GC/MS analysis of organics in multimediasamples. This three year contract involves the analysis oforganics (priority pollutants, HSLs, pesticides/herbicides)in solid and liquid matrices using GC/MS and :GC procedures.

Procurement Activity /Contract! tic Officer \ -)*.--Law Environmental, Inc. _ " *>^r- -•.--.. f- ' ;(for OS Army Corps of Engineers) if . * . - - • •Kennesaw, GAi '• "-*': • •-"T"'j ^ */•*-*•• • - - ta_ ^ . . _ _ . . ..-_ . , : -.Project Manager: Louis Karably (404)421-3400

Contract No. /Type (; "., ,, **, - - - - - -1-87063/Unit Pricing ^ -Award Price/Final Costnot .to exceed $30,260/S30,280

flRI*00577

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J

Award Price/Final Price$27,000/$27,000

Period of Performapce5/88-8/88

CBC Environmental Services was under contract to perform aninvestigation of potential groundwater contamination at ahazardous waste landfill in Wisconsin. metaTRACE performedAppendix IX organic analyses on a monthly basis for thisinvestigation. Groundwater monitoring samples were analyzedfor volatile organics, semivolatile organics, pesticides/PCBsand chlorinated herbicides.

Procu reman t Activity/Contracting OfficerEngineering-ScienceAtlanta, GAProject Manager: Jimmy Duncnn/Robert Thoera (404)325-0770

Contract No .Not Applicable/Unit Pricing

Award Price/Final Price1) Michigan ANG: $50,000/$50,0002) Chanute AFB : .$100,000/$100,000

Period of Performance1) Michigan ANG: 9/87-9/882) Chanute AFB: 12/87-6/88

Engineering-Science was under contract to the US Air Forceand the Michigan Air .National Guard to perform contaminationinvestigations at two facilities. Martin MariettaCorporation provided quality assurance oversight for bothsites: Chanute AFB (IL) and the Michigan Air National GuardBase. metaTRACE was under contract to Engineering-Science toperform all analytical aspects of the investigations.Analyses performed on water and soil samples 'includeconventional priority pollutant analyses (volatiles, semi-volatiles, and metals. metaTRACE was successful in obtaininglaboratory certification from Martin Marietta prior toperforming these analyses.

Procurement Activity/Contracting Of f iearViar & CompanyAlexandria, VAProject Administrator: Tony Nesky (703)557-2490

Confrraqt No . /Typa3791F/Unit Pricing AR^00578

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Period o^ Performance8/87-6/88} • L "

Law Environmental, Inc. conducted a site assessment of theFire Fighting Area/Drum Storage Area, Fort Bliss, TX. Thisinvestigation was performed,for the US Army Corps ofEngineers. metaTRACE performed all chemical analyses on soilsamples collected from these areas; Soil samples wereanalyzed for purgeable aromatic hydrocarbons, purgeable 'halocarbons, barium, cadmium, chromium, lead, silver,arsenic, mercury and selenium.

. - . . • • : • i - • . ' - , '- ^ i.-: • - ' . ' ' . . . - . . >

Procurement Activity/Contracting OfficerEG&G Idaho, Inc.Idaho Falls, IDProject Officer: Larry Croft (617)924-9061 ,

Contract No. /Type •• 'C67-131450/Fixed Price ™

Award Price/Final Price$192,865/$192,865

Period of Performance3/88-11/88

EG&G Idaho, under contract to the US Department of Energy, isresponsible for the operation and management of the DOE*sIdaho National Engineering Laboratory (INEL) in southeasternIdaho. Under subcontract to EG&.G, metaTRACE was responsiblefor the collection end analysis of environmental samples fromthe Army Materials Technology Laboratory (AMTL) in Watertown,MA. Samples included surface soils, subsurface soils,sludges, water, composite dust samples and partlculate airsamples. metaTRACE analyzed additional samples collected ..from sediments, 'cores and water resulting from monitoringwells and geophysical surveycoreholes. All sampling andanalysis activities followed procedures established by the US

{ Army Toxic and Hazardous Materials Agency (USATHAMA). lUSATHAMA certification was required prior to performing anyanalyses under this subcontract.r Besides chemicalparameters, metaTRACE analyzed fiaroples for radiologicalparameters (gamma spectrum, gross -alpha and pure betaemitters, and transuranics).

Procurement Activity/Contracting OfficerCBC Environmental Services . . .Oak Creek, WIProject Manager: Sue Lipo (414)764-7005

Contract No./Type .B, n n _ _ _NA/Unit pricing.. HnHUOD/9

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Award Price/Final Cost$33,300/$33,300

Period o_£ Parformanea , ,. • •5/87 - 6/87

Vlar is the Sample Management Office for the EPA ContractLaboratory Program (CLP). Through the Special AnalyticalServices (SAS) Program, metaTRACE analyzed soil, sludge andwater samples, including many difficult matrices. Allsamples were analyzed for the full spectrum of organic andinorganic compounds, plus complete radiochemical analyses fornatural series Uranium-Thorium nuclides and fission products.All work required CLP Data Package deliverables.

Procurement Activity/Contracting Officer *KRT Inc.Concord, MA • • / 'Project Administrator: William Doerr (617)369-8910

Contract No./Typa88015/Unit Pricing

Award Price/Final Cost$29,000/$33,850

Period oj£ Performanea -9/87 - 5/88

) . i • ' • ' ; - . i •ERT contracted roetaTRACS to provide full analytical supportfor the initial investigation of a contaminated ore producingsite in Ohio. This was an extensive project, involving

j direct monitoring of radiation levels on site, surveys, airmonitoring and the direction of all sample collectionactivities. Sample matrices included water* soil, air

I filters and solid ore, analyzed for'Isotopic Uranium,J Thorium, Radium, Lead and Polonium 210, with many samples

analyzed on a rush basis. metaTRACE also participated, in ai Joint study with the U.S. Nuclear Regulatory .Commission (NRC)j through Oak Ridga Associated Universities (ORAU). The

purpose of tha study was to validate metaTRACE* s data byanalyzing blind samples prepared by ORAU, and verify theresults.for NRC's approval.

t Procuremant Activity/Contracting QffleerI Confidential Client

._ Contract No. /TypaI NA/Unit Pricing

Award Price/Final Cost '

flR!»OOS80

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Period pf.Performance . : f %f » ' . "2/88 - 3/fes , •,.;,:y,Y" •Two major beverage manufacturers contracted metaTRACE toprovide analytical support in response to potentialcontamination of consumer products. The suspectedcontaminant was Polonium 210, which is used in'staticeliminator guns for cleaning the cans prior to filling themwith product. This project'required developing:methodologiesappropriate to unusual matrices. All work was performed onan emergency basis, with results available in less than -twenty four hours in many cases. Through metaTRACE'sefforts, the manufacturers Were able to certify theirproducts free from radiological contamination and continueproduction.

Procurement Activity/Contracting pffleer . /Confidential Client

\ .. • ~ ' ~ - ,*'. •Contract No./Type ^NA/Unit Pricing

Award Price/Final Cost$8000/$8400

Period of Performance10/87 - 11/87

'%•'- "„.*• - " • " 1 $t.:-. W !'•";" . ' - . . • • - _ • _ .. • • ; "TThrough an independent consultant, metaTRACE was contractedto provide analytical support on a site investigation for amajor pharmaceutical manufacturer. Prior to beginning newconstruction, our client had to demonstrate to the NuclearRegulatory-Commission's satisfaction that previous work had'not contaminated an adjacent area. A complete radiochemical :soil investigation was performed, including isotopic analysesof. the Uranium and.Thorium series radionuclides.

Procurement Activity/Contracting pfficer ,E.I. duPont de Nemours & Co., Inc.Savannah River Plant, SCContracting Officer: H.B. Spletzer (803)725-2433

Contract No./TypeAX-798814/Indefinite Quantity

Award Cost/Final' Costnot to exceed $125,000/$5,000

Period p_f, Performance9/87-2/88 rt. - J '

"-fcftis.it *- ' • :•' " " )»

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metaTRACE was selected as the analytical subcontractor toduPont at. the DOE's Savannah River Plant for the DOE (HQ)Environmental Survey project. As part of this survey,metaTRACE analyzed water; soil-sediment; sludge; waste;vegetation; crustaceans; deer bone, flesh and thyroidtissues; and raccoon bone, flesh, and thyroid tissues forvarious constituents. Parameters/methods included drinkingwater metals; TCLP metals; ICP metals; gross alpha, beta;gamma spectroscopy; tritium; 129-1; 99-Tc; 90-Sr, U(T); 14-C;HTO; SO4; N0> ; Fl; Cl; CN; corrosivity; volatile organics;semi -volatile organics; TCLP extractable organics;pesticides; PCBs; etc. •

Procurement Activity /Contracting OfficerDonahue, Rajkowski, Hansmeler(for confidential client)St. Cloud. MNProject Manager: Mr. Paul Rajkowski (612) 251-1055

Contract No . /TypeNot Applicable/Unit Pricing

Award Price/Final Priea$25,000/525,000

Period of Performance4/87-4/87

Under extremely fast-turnaround requirements, metaTRACEsampled and analyzed1 18 groundwater and soil samples forvarious pesticides and herbicides for a pilot scalemonitoring program to assess non-point groundwatercontamination by agrichemicals* Three methods were utilizedfor these analyses: GC/MS, EPA 608 (f luorisil) , and aninternally developed method for chloramban analysis. Allanalyses were completed within 2 weeks. .

Procurement Aotivltv/Contraeting OfficerConfidential ClientSt. Louis, MO

Contract N o . /Type - • " ' " ' " " - .Not Applicable/Unit Pricing

Award Price/Final Prlca .$21,000/$21,000

Period of Performance3/87-3/87

A major St. Louis industrial concert .nrnaroundanalysis of 32 soil samples to asset flRlinQ582 .amlnation

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at a wood preserving facility. metaTRACE completed the .analyses for pentachlorophenol in 72 hours. All analyseswere conducted by GC/MS (EPA Method 8250) and Included allinternal quality control.•"*" *••**':'

Procurement Activity/Contracting OfficerTRC Environmental Consultants, Inc. .(for Hamilton Standard Co.) •" . :E, Hartford, CTProject Manager: Eileen P!Amico (201)269- 8631

Contract No./TypeNot applicable/Unit Pricing ,

Award Cost/Final Cosfr - ! 1$16,000/$16,000 . " !

Period of Performance \ .1/87-3/87

r i 'TRC Environmental Consultants conducted treatability studies[and pilot plant investigations for the Hamilton StandardCompany to evaluate the efficiency of a persulfate oxidationprocess for destroying organic compounds. Hamilton Standardis developing a waste treatment system for use in NASA'sspace station. metaTRACE analyzed standards prior toinjection into the system 'and analyzed the final effluent forvolatiles and semi-volatiles (by GC/MS). In addition,metaTRACE performed various GC analyses for alcohols, amines,'phenols and phthalates; TOG; and other parameters by ionChromatography. • -• - •• • • ' •r- ' ' •• ' : "; '"• •;'..'.:

Procurement Activity/Contracting OfficerViar and Company, Inc./USEPA . . ;Alexandria, VA . .'•-?<£&"•':!:* •'': : -.'."- • - ' • " ' •' " ".,--•" ;: '• - '.- ,Project Manager: Emile Boulos (202)382-7942 ;" ', ,

( . • I - , .. i •. • - J.-: '•* ' * • - " /Contract No./Type -. . ' , ; - : . -SAS-2914HQ/Unit Pricing €^ M£)

Award Cost/Final Cost -$23,100/$23,100 : , V :

Period of Performance ' ' !5/87-9/87

metaTRACE participated in the EPA-sponsored method vaird tlcn-study of draft method 680, "Identific»**- -ement ofPesticides and PCBs by Gas Chromatogr . ometry.**metaTRACE was one of seven labbratoritapproximately 15 water and -eoll sampl — -.rom theseanalyses will be used to calculate and establish

'

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interlaboratory precision and accuracy statements for themethod. The contract also required the utilization of EPAsupplied Format B electronic data transfer software, tosubmit GC/MS data.

Procurement Activity/Contracting OfficerAlliance Technologies CorporationBedford, MAProject Manager: Douglas Roeck (617)275-9000

Contract No./Tvpa19037/Unit Pricing

Award Cost/Final Cost .$29,528/$29,528

Par104 of Performance10/87-4/88

Alliance Technologies conducted a sampling and analysis..program for the City of Fall River, MA municipal refuseincinerator in response to an Order by the Massachusetts >Department of Environmental Quality Engineering (DEQE). The x^xprogram called for sampling and analysis of flue gasemissions, residual ash,, scrubber ash and spent scrubberwater. metaTRACE analyzed samples for specific groups andisomers of polychlorinated dibenzodloxlns/dibenzofurans(PCDD/PCDF). Data from these analyses were used to determinesource compliance with DEQE*s ambient guidelines fordioxin/furans and to evaluate whether special handling *-procedures were required for the ash and water discharged bythe incinerator.

Procurement Activity/Project ManagerLafser & Schreiber, Ino. .(for Continental Cement, Ino.)St. Louis, HOProject Manager: Fred Lafser (314)534-2268 -

Contract No./TypeNot Applicable/Unit Pricing

Award Cost/Final'Cost •$20tOOO/$20,000

Period of Performance3/87-7/87

Lafser & Schreiber was the consultant of record for theContinental Cement Company, who was - 't for awaste solvent supplement fuel procet Ibal, MOfacility. metaTRACE, under agreemet , . - - ,

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Schreiber, conducted performance testing of organic blendsand emissions to establish criteria for the destruction andremoval efficiencies (DRE) of the system. • This project-Involved the analysis of HCl, particulates, lead, mercury,beryllium and Principal Organic Hazardous Constituents :.(POHCs) of the process emissions.

Procurement Activity/Contracting OfficerConfidential Client

Contract No./TypeUnit Pricing/Indefinite Quantity

Award Cost/Final Cost ^ - l- ; " ;'.„",. ;Not to exceed $30,000/$25,000"-; T

--'•-,-• . ;. r"; ... . v l"± 0'-:•- •" '- - - •'--. - - . , •: . * i, . " ' ; " *Period of Performance

7/87-6/88 : :

metaTRACE was under contract to supply field sampling andanalytical services in support of the client's routinequarterly RCRA groundwater monitoring and .special hazardouswaste remediation projects." The analyses included routineorganic and Inorganic chemical parameters as well as totaldibenzodioxin and dibenzofuran analysis by GC/MS.

Procurement Activity/Contracting OfficerConfidential ClientSt. Louis, MO ..

Contract Ho./TypeNA/Unit Pricing , __:

_- .• • •' - l , , - £ . : : ^ -'"-•."'.

Award 'Price/Final'Price$114,000/$114,000 -..'•'•'-' tPeriod of Performance -9/87-12/87 - ~?'r:\Ye-ic Tc::-.- -"-. '- .. 'metaTRACE was retained by this industrial client to perform apesticide analysis/soil persistence.study. The clientdesired to determine the persistence in soil of a new, secrettest product. metaTRACE analyzed 600 soil camples by GC induplicate for this test product and supplied the client withboth hard copy to meet *FDA registration requirementispand fdatein computerized format (tape). All analyses were performed -under GLP (Good Laboratory Practice) guidelines. Results ofthis study are being used by the client to obtain FDAregistration for their new product. . • .

. ''• i ' '• - •

ft H:?.....,-..-!,--.: ARl*00585

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Procurement Activity/Contracting Of f lear.Confidential Client .St. Louis; MO •

Contract No . /TypaPO B000080/Fixed Price

Award Cost/Final Cost$3,000/$3,000

Period of Performance3/87-6/87

metaTRACE participated in an inter laboratory methodvalidation study conducted by this industrial client. Thisstudy involved analyses performed on common agriculturalherbicides by GC/MS. The duration of the study wasapproximately three months. . -

*

Procurement Activity/Contractlng Officer ,McDonnell Douglas Aircraft CorporationSt. Louis, MOProject Manager: Mr. Robert Kaatman (314)895-5235

Contract No. /Type715024/Onit Pricing; Indefinite Quantity

Award Price/Final Price v$150,000/$150,000

Pario'd Qf Performance4/87-2/88

McDonnell Douglas Aircraft Corporation issued an analyticalcontract to metaTRACE to perform all laboratory analyses forwater/was tewater, deposit samples, known and unknownhazardous and non-hazardous wastes, oil, coal,microbiological and/or radionuclides. In addition, metaTRACEperformed monthly NPDES sampling of McDonnell Douglasoutfalls (composite and 'grab samples).

Procurement Activity /Contracting OfficerB.C. Jordan CompanyPortland, ME •Project Manager: Dr. Bruca Wallin (207)775-5401

Contract fto . /Type , 'None/Unit Pricing

Award Cost/Final Cost$25,000/325,000

i s ARd00586

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Period of Performance4/87-6/87 . f ^ :

E.G. Jordan Company was retained to conduct a groundwater1monitoring program at a landfill in the Eastern UnitedStates. This landfill is known to be the cause ofgroundwater contamination in the area, and -the operators areunder a court order to provide analytical data pertaining togroundwater contaminants. metaTRACE was under contract toE.C. Jordan to analyze groundwater samples for volatileorganics, semi-volatile organics, PCBs, 2,3,7,8-TCDD,priority pollutant metals, and other inorganic and organiccompounds. The court mandated that strict USEPA methodologyand quality control be followed during this quick turnaroundproject. _ '...., ,, •, , • - ' ' [ " " •"•'•• '-"'-:, , i- <, •>- - •- ,f

Procurement Activity /Contracting Officer ' , :Enviresponse/Alliance Technologies CorporationBedford, MAProject Manager: Geoff Ring (201)906-6821 -.Contract No . /Type • > IUnit Pricing/Indefinite Quantity 'Award Cost/Final Cost$350,000/$350,000 '--.'Period of Performance7/87-1/88 - :r

Enviresponse/Alliance Technologies Corporation issued an ' -''analytical services contract to metaTRACE to perform a !variety of chemical analyses in support of the Office ofToxic Substances (OTS) evaluation of the US EnvironmentalProtection Agency's mobile incinerator system located at theDenny Farms Dioxin Site in McDowell, Missouri, Chemicalanalyses Included metals, volatile organics, semi-volatileorganics and total dibentodioxln/dibenzofurans. metaTRACEprovided 24 hour turnaround of analytical data for severalcritical samples during the test burn.

Procurement ctiylty /Contract ing OfficerConfidential Client . ••'

Contract No . /Type •• • , -NA/Time and Materials .

Award Cost/Final Cost , . , , . • . ;$69,000/$69,000 V ' ' ' " ^ '

Period af Performancevav-9/87

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metaTRACE was under contract to a number of PrincipalResponsible Parties (PRP) to provide a quality control reviewand validation of both organic and inorganic data generated .as part of the US Environmental Protection Agency's ContractLaboratory Program (CLP) from a superfund hazardous wastesite located in the western United States. The data may beused during litigation, and expert witness testimony may beprovided by one or more of the metaTRACE staff.

Procurement Activity /Contracting OfficerTRC Environmental 'Consultants, Ino.Denver, COProject Officer: Stephen Bundy (303)792-5555

Contract No . /TypaNot applicable/Unit Pricing

Cost/Final Cost$7200/$7200

Pariod of Performance2/87-3/87

TRC performed a preliminary hazardous waste siteinvestigation for the Arizona Public Service power plant inFour Corners, New Mexico, suspected of being contaminatedwith chlorinated organic solvents. Shallow soil cores weretaken on an extensive grid network. metaTRACE analyzed alarge number of soil core sections for seven specificchlorinated compounds -using GC/MS purge and trap techniques.

Procurement, Activity/Contracting Off iearAlliance Technologies Corporation(for New York Dept. of Environmental Conservation)Love Canal, NY - . ' . .Project Manager: Mr. Ed Paduto (617) 275-5444

* . •

Contract No . /Typa .Not Applicable/Unit Pricing

Award Price/Final Price$110,000/$110,000-

Period of Performance3/87-5/87

Alliance Technologies Corporation issued an analyticalcontract to metaTRACE to perform total tetra through octadibenzodioxln/dlbenzofuran analyses ** «•«»»*%••*. «* the Jointtechnology and evaluation of a roobil olyslsunit (incinerator) and its associate . the Love

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Canal Leachate Treatment Facility In Niagara Falls, New York.Four sets.of modified Method 5 Sampling Train camples andnumber of'waste feed samples were analyzed to calculate-anddetermine the dloxin/furan destruction efficiencies (DRE) forthe mobile unit. The entire project was under the directionof the New York State Department of EnvironmentalConservation (NYSDEC), the Hazardous Waste EngineeringResearch Laboratory (HWERL), the Office of Research andDevelopment (ORD), and the US Environmental Protection Agency(USEPA). metaTRACE successfully underwent the NYSDECcertification process to participate In this program.

flRt*00589

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AVTKI FIBERS FRONT ROYAL INC,AVTEX FIBERS SITE

APPENDIX APERSONNEL RESUMES

ADMINISTRATIVE ORDERDocket No. III-90-01-DC

Prepared for U.S. Environmental Protection AgencyHazardous Waste Management Division

Region III

Noveaber 7, 1989

AVTEX FIBERS FRONT ROYAL INC.Cendrick LaneP.O. Box 1169

Front Royal, Virginia 22630

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, APPENDIX A

PERSONNEL RESUMES

This appendix contains resumes of personnel assigned to this project fromthe following companies!

Avtex Fibers Front Royal, Inc.Alliance Technologies Corporation (Resumes included in Statement ofQualifications

S.D* Myers, Inc.ConcoChemical Waste Management, Inc.

AR<f0059l

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AYTCX FIBERS FRONT ROYAL INC.AYTEX FIBERS SITE

AVTEX FIB EESraONT ROYAL INC.. - : - , ilO"'. :'' ' '

PERSONNEL AND QUALIFICATIONSBECTlONIi

ORDER

Hma)«rl989

AVTZX HBOEfl raOlTT EOTALIKC,KoMekltMP.O. Box WM

12530jfionanuH1 : '

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C. KENNETH WAGNER11 Portsmouth Road

Front Royal, VA 22630Home phone (703) 636-2109

Office phone (703) 635-2141, Ext. 110

OBJECTIVE Management responsibility 1n a position where my skills willbe utl11zed; where commltment to my employer 1s requlred;and where there Is an opportunity to make a meaningfulcontribution to the success of the operation.

SUMMARY; I am an experienced professional with a solid record ofpromotion In the management of a large multi-product syntheticfibers producing corporation. Have training 1n maintenancemanagement, project management* budget management, and a provenrecord of an, ability to work well with people, supervisors tpeers, and subordinates.

EXPERIENCE; All experience has been with American Viscose Corporationand Its successors, FMC Corporation and Avtex Fibers Inc.except for a two-year tour of duty 1n the U. S. A1r Force.

AVTEX FIBERS FRONT ROYAL INC., Front Royal, VA1/87 - Present Vice President - Engineering

Bottom line responsibility for all design, funding, procurementand cost control of capital projects and all maintenancefunctions In the Plant. Member of the Corporate operatingcommittee. Extensive experience 1n negotiation with stateand federal agencies, contractor firms, vendors and suppliers,and union negotiations both corporate and local. Coordinatepurchase of capital and repair material with purchasing staffsto control cash flow and at the same time meet projectdeadlInes. Develop and coordlnate priority systems forallocation of personnel and equipment to maintain and operatethe plant facilities within funds available. Develop andInitiate cost reduction projects to provide additional capitalto upgrade plant facilities. Responsible for directingactivities of approximately 35 salary and 300 hourly employeesand an annual budget of approximately $20,000,000.

8/79 - 1/87 Assistant Plant Manager - EngineeringBasically the same job description and functions as describedabove. Job title changed with reorganization of overallcorporate structure making the Front Royal plant a separatecorporation. During the past 6 years as either V.P. ofEngineering or Assistant Plant Manager - engineering budgetswere met to within * 0.1X annually.

12/77 - 8/79 Maintenance ManagerReported to Assistant Plant Manager - Engineering. Responsiblefor all maintenance functions within the Front Royal plant.Assisted in developing a meaningful work order system forthe plant so as to determine priority, scope r*& .warfc—costestimating, plant and corporate approvals, and brerr-over&evi«gmaterial procurement and directing the Implementation of thescope of work. Develop and administer a planning and schedulingfunction with the Engineering Department to coordinate theassignment of personne* *A """"* «f*^<«ntly execute the scopeof work with minimum 1< ssary expense. Direct

, „ . . , - : responsibility for ap.^. ^-^ ilary and 300 hourlyARttQ0593

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continued)

9/75 - 12/77 Chief Plant Engineerthisassignmentwas at our Radford, Virginia plant. Itentailed establishing an engineering department 1n a relativelynew plant. Planned and Implemented preventative maintenanceprogram, developed and Implemented a job training programfor hourly craftsmen,, prepared and administered budgets andbudget control..systems. Developed and Implemented training

r programs for foremen sand supervisors to enhance their ability-• " to lead and motivate personnel. During the period I served

at the Radfprd V#l«nt» the maintenance costs were reducedby 50X and the machine running efficiency was Increased by'about 75*. It j*ast; during this period that FMC sold theirfibers operations to Avtex Fibers Inc.

8/72 - 9/75 Project Managerthisassignment, was at our FMC Fibers Division, CentralEngineering 'group ;ln 1 Media, PA. Responsibilities coveredall aspects of,.. Project management from, conception tofulfillment. Develop engineering scopes from manufacturingscopes, supervise all phases of the project design. Select

'» equipment vendors arid contractors, prepare bid requests, analyzebid returns and select successful vendors and prepare purchaserequisitions. Develop critical path charts and develop projectbudgets. Develop: follow-up procedures to Insure projectcompletion on schedule and within budget limitations. Projectbudgets ranged from 160,000 to $10,000,000 and up to 15 projectswere being supervised simultaneously at several of our plants.All projects supervised were completed on schedule and withinbudget limits. , ,_., t r :•:'"•!"- . „ • • . . . . . j f i • ' • » • " ; • "

• - • . I-, -,, t . • • -2/63- 8/72 "- Plant Engineer "*

This position was at our Lewistown, PA plant. Duties were'much the same as the Assistant Plant; Manager - Engineeringat the Front Royal plant as described above. Totalresponsibility for approximately 40 salary and 550 hourlypersonnel Including approximately 6 graduate engineers. Duringthis period* FMC Corporation purchased air physical assetsof The American Viscose Corporation. - " «r H

1/62 - 2/63 Maintenance Engineer / >This position was at the Lewistown, PA plant. Duties Included

; direct supervision of 2 Maintenance .Supervisors, 1 Utility.; Supervisor, 5 office personnel .and Indirect supervision of

;: ;approximately 700 ^hourly personnel1 r and 25 foremen., ' Responsibilities included the manning distribution for all1 maintenance functions of the operating and service departments

and all capital projects assigned by the Plant Engineer toplant forces. Acted as llason between plant personnel andcontractor supervision on all capital projects assigned forcontractor completion. / ; - ; ,

8/56 - 1/62 Staff EngineerThis position was at our Lewistown, PA plant. Dutres intrutfetJscoping and estimating both capital and maintenance workrequests. Coordinate originations with plant staff membersand/or department heads. Design with drafting departmentpersonnel. Select «•"»/•»..* •»* -~oed1te materials requiredand coordinate witJ glneer to Insure efficient

. .execution of the , mng ndivldual projects varied- *'-, from budgets of fln^OOQli °°- UP to '°° projects

onooino

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EXPERIENCE(Continued)

8/54 - 8/56 United States Air ForceAircraft Maintenance OfficerResponsible for total maintenance of seventeen B-47 aircraftand supervision of staff of approximately 74 non-commissionedofficers and airmen. Attained the rank of 1st Lieutenant.This was one of three squadrons in the wing and I was successfulIn attaining the highest percentages of successful missionsboth routine and max efforts on unscheduled alerts of thethree squadrons.

6/53 - 8/54 Junior EngineerThis position was at our Lewistown, PA plant, This was entrylevel from college and my primary assignment was that ofpipefitter foreman. Responsible for the day to day supervisionof approximately 50 hourly personnel. This position gaveme the opportunity to develop my managerial skills and myability to work with other, people successfully.

EDUCATION; Massachusetts Institute of TechnologyBS - Mechanical Engineering - 1953

- U. S. Air Force Maintenance Officer SchoolChanute AFB, Rantoul, IL - 1955

REFERENCES; David A. Tousignant, President Eldon E. CampbellAvtex Fibers Front Royal Inc. Plant Manager (Retired)P. 0. Box 1874 1005 Horseshoe DriveMiddleburg, VA 22117 Front Royal, VA 22630

: (703) 687-5359 (703) 735-8176

John N. Gregg ' ' Charles M. Huber, MDPresident S CEO 315 West 10th StreetAvtex Fibers Inc. , Front Royal, VA 22630221. South Aberdeen Avenue (703) 736*6131St. David's, PA 19087(215) 687-2348 Ralph S. Markee

Executive Vice PresidentJohn 6. Knight Avtex Fibers Front Royal IncVice President (Retired) Route 1, Box 3483Avtex Fibers Front Royal Inc. Front Royal, VA 22630501 Ross Avenue (703) 635-5714

. Front Royal, VA 22630(703) 636-2702

C. Ray EnicksPlant Manager (Retired)139 Gloucester RoadFront Royal, VA 22630(703) 635-7310

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'

Pout J. MoiinaJr.

BSME 1974. New Jersey Institute of Technology (NCE»Society or Professional Advancement. Brunswick. NJ.Pnuematic Conveying of Bulk Solids, Polymer ExtrusionHercules Inc., Management School

5/89- Avtex Fibers Front Royal, fee. l fPresent Utilities Engineer: f

Duties include all facets of Powerhouse Dept. Head forSteam Generation & Turbine operation, Proj. Mgr. EPAregulatory compliance on Underground Storage Tanks andPCB detection and clean-up. (Supervise S Sal. & 39 HrJy ).

2/89- CalJaghan ConsuUanls,"lftc.n" rPresent Owner: .

Consulting Engineering worJ: for Jocal and national Industry.Continuing growth.

9/88- Murray Machinery, Inc.2/89 Plant Manager:

Duties included total Plant management of 9.5 million dollarsactive fabrication work (pulp & paper machinery, chip millequipment) Accountable for 40 wage-roll/saiary personnelPosition consolidated and eliminated due to CorporateTake-over. tvivx^r1'-*;-' . !* ?' •-"• "" "•'

9/84- Hi-Une Machine. Inc.7/88 Plant Engineer: r r

Accountable for all phases of manufacture (fabrication &machine shops). Design. Building modifications, Governmentestimating/contract bidding/contract administration (familiarwith QAR, FAR, & MIL standards) Personnel relations (hiring,terminations/policy). Operate nw^dnfM nnrnnrate Safety,OSHA enforcement, R&D. Ace °n flnd fl R 0 0 5 9 6salary peribnhei.

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Company closure.

7/74- Hercules Inc.8/84 Multi-Plant supervising Project Engineer: $40.000/yr.

Accountable for capital expenditures for 3 plants ($6.5 million)Supervised 1 1 Engineers/3 Draftsmen

(1/82-8/84)

Plant Engineer:Accountable for Engineering and Maintenance for anAmmonium Nitrate and Nitric Acid Plant. ($1.5 millionmaintenance/$3.0 million capital) Accountable for 1 5 wage-roll/salary personnel.J 1/80- 1/82 Promoted

Project Engineer/Senior Design Engineer:Project work $Jk- 38.5 Million for polypropolene Fiber/FilmPlant (Field engineer on construction of $38.5 million FilmPlant, Equipment setting/start-up/troubie shoot, piping.H VAC. Structural installation. 2.5 yr. project) •7/74-1 1/80 Promoted.

74-75 Jackson River Vocatonal CenterNight School Automotive Instructor

85-86 Apprentice Blue Print Reading Instructor

Married, seven childrenPurchasing home

15 Years Automotive MechanicsCustom Paintwork (conventional-electro static)Welding (MIG/Stick, FLuicore. Sub-arc)NDT (dye-penetant, mag-particle. X-ray)Machine operation (MiiisXaihes.Punch pressesjrake press)Drafting & DesignWoodworking/cabinet makingGovernment DOD ContractingAffiliated with ASMB&NSPB .EPA, PCB. and RCRA Project Management

REFERENCES UPON REQUEST

^ : ARU00597

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AVTEX FIBERS FRONT ROYAL INC.AVTEX FIBERS SITE

ALLIANCETechnologies Corporation

Contractor qualifications and personnel rcauncsfor ALLIANCE Technologies Corporation tie indodcdinAPPENDDCFofthisWORXPLAN. . .

AEMMSTRATTVE CRtER

Prepared fcr

V. S. Ibvlnaaaiui fatoctioa Agency

Region ffi

AVIECnBERSFRCKTROYALINC.netl69W* 22630

AR<f00598

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AVTEX FIBERS FRONTROYALIMC.AYTEX FIBERS SITE

5. D.MYERS / TRANSFORMER CONSULTANTS

PERSONNEL AND QUALIFICATIONS

SECTttHS.2

ADMMSTBAI1VE 0£D£B

Pnjvtt for

U. I. ExriraiaoUl FrotKdoi Apiqr

Honm>*r 1989

AVIEZnBCSS FROHT fiOYAL SIC.XtiMeklttlF.O.BoiliM

FmM Boji TJrjiila 22630

ARU00599

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7

RESUME OF

MHW A. FRITZ

Mr. Fries has twelve year* of diversified experience in handling. 'labeling and transportation of hazardous materials for S.D. Hyers, Ine.He ia authorized by the etate of Karyland to conduct Controlled KazerdoueSubstance Drivers Training Programs.VOiUC EXPERIENCE• • W MHBMMMHIH n MB « _

S.D. Kycrs» Inc.180 South Ave.Tallaadge, OB 44278 £

HELD SERVICE MANAGER (7/B7 - Present)

Hespqnsibiliticat. . , • - t -.. f • -Interactions and negotiations filth federal* state and local regulatory agencies.Regulatory compliance vlth DOT and TSCA.Development and implementation of hazardous vaste handling and driverstraining programs. .".%? ^ ;Inspections of outside carriers for compliance to regulations.Semi-annual updating sessions vith all drivers snd crev to keep all practicesin line vith lav changes*

FIELD SERVICE PRODUCTION SUPERVISOR (1/86 - 7/87)

Responsibilities *Directing the movement of all hazardous vaste material by the Field ServiceDivision throughout tha United States* .Monitor driver and Jobsite personnel for compliance to all regulations.Insure that all vehicles are maintained According to federal and atate standards.FIELD SERVICE CHEW LEADER (1/80 - 1/86) .

Responsibilities f* '

Direction of all onsite activities prior to and during the handling ofhazardous vaste* 'Inspection of finished loads for proper .labcling» leading and manifesting.

. **.

ARU00600.- 4

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TRANSFORMERCONSULTANTS

DAVID F. BICHSEL

AUGUST 8, 1982

ExperienceSix years experience in fluid handling and PCB removal. David has supervisedall types of PCB cleanup work in more than seven eteces. His reaponsibilltltsInclude labelingymanifeeting, packaging, supervising of crevs( and evaluatingneeds of the cuetomer for compliance. He Is also certified by the etete ofMaryland to haul hazardous waste.

HARK ROBERTS

JULY 28, 1986*

ExperienceMark has completed all of the S, D, Myers safety and environmental training.He has supervised crevs on jobs in Texas, Tennessee, New Jersey, Ohio* andMichigan. His responsibilities include all aspects of compliance as wellas development of grid samples to determine the extent of customer contamination.

flR!*0060l

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AVTEX FIBERS FRONTROYAL INC.AVTEXFBERSSITE

STEAMKATHAfMiTof VA

PERSONNEL AND QUALIFICATIONS

f r *

l i ^ ADMOnSTSATZVE ORDER

0. 8,

P.O. Box 116922630

ARi*00602

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Corporate Summary:

STEAM KAT HAZ MAT OF VIRGINIA

Steam Kat Haz Mat of Virginia Is one of three operational divisionsof Clean America/ Inc/ of Baltimone,* MD. As such it Is has onlyone year existance but key personnel and total coporate historyinclude five years environmental compliance contracting work. Thecorporate predecessor organization to Steam Kat Haz Mat completedprojects in five states. These projects Included compliance workunder the Clean Water Act, Resource Conservation and Recovery Act,Toxic Substances Control Act/ Comprehensive Environmental Response/Compensation and Liability Act and Superfund Amendment andReauthorlzatlon Act. Field crews of up to twelve men have workedon a 24-hour basis under all types of weather and terrainconditions. Crews have operated as far away from the corporateoffice in Richmond/ VA/ as Philadelphia and San Francisco.Compliance/ recovery and clean up work has typically involvedcoordinating strategies and tactics with the client/ various stateand federal regulatory agencies and disposal facilities. Technicalabilities Include preparing a dellsting petition under the ResouceConservation and Recovery Act and drafting an environmentalassessment under the California Department of Healthpolychlorinated blphenyl clean up standards.

ARi*00603

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. W. BRYANT BARNES

EDUCATION: ' 'J.R. Tucker High School.-1969 :

EXPERIENCES ' " • .-'.'a ?ru-- ' '." ' ' " ..- • • .act;!1 . . - . . . • - • -Eight years experience in all aspects of corporate

environmental compliance from sales to project management topersonal supervision of up to 40-man work crews involved in allaspects of compliance with Clean Water Act/ Resource Conservationand Recovery Act/ Toxic Substances Control Act and ComprehensiveEnvironmental Response/ Compensation and Liability Act. Projectsand response actions include emergency response to oil spills/pipeline ruptures/ train derailments/ truck accidents/ In-planthazardous materials and wastei spills; underground recovery andremediation and dellsting of RCRA-regulated wastes. Over one dozenpolychlorlnated biphenyl (PCB) decontamination projects fromVirginia and Maryland to California. . - .

ARt(0060lf

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GEORGE C. WALTON

EDUCATION:Penn State University. MS - Biology. 1974U S Army Explosive Ordnance Disposal School. 1976U S Environmental Protection Agency Response Manager

Operations Course. 1985.CERTIFICATIONS!

Certified Hazardous Materials Manager (Master Level)Certified Safety ExecutiveFellow/ American Institute of Chemists

EXPERIENCE: ! . - ' • " ' •

Fourteen years experience in all phases of emergency responseand environmental compliance from recovery of military andcommercial explosives to commercial hazardous materials and wastes.Served as part of an EPA Regional Response Team and worked onsixteen Superfund sites and over three hundred emergency responseand hazardous waste disposal projects in 26 states. Conductedhazardous waste operation and emergency response (HazWOPER)training programs as well as compliance programs for the VirginiaEmergency Management Association and the Virginia EnvironmentalHealth Association.

W

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- DOWNIE B. BARNES

I I EDUCATION?^ Randolph Henry. 1985 IK

OSHA HazWOPER Training (40 CFR 1910.120). 1988

EXPERIENCE!. : . . ., -. i -. cnl^Cflt- - - • •Five years operational experience in oil and hazardous waste

clean up and.disposal. One years experience as office manager offull service environmental response company. Specific dutiesIncluded hands-on recovery'b£ oil/ hazardous chemical materials and

; polychlorlnated blphenyle '(PCBs). In addition/ supervision ofsmall field crews involved in all types of environmental operationsunder a wide variety of Conditions and circumstances to includeadverse access and weather.

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JACKIE MC ALLISTER

EDUCATION!Prince Edward Academy. 1960OSHA HazWOPER Training (40 CFR 1910.120). 1988.

EXPERIENCE!

Five years experience managing field crews involved Inhazardous waste and emergency response operations. Specificprojects included recovery/ Identification/ transportation anddisposal of hazardous waste in accordance with ResourceConservation and Recovery Act (RCRA; 40 CFR 260-267). In addition/supervised crew decontaminating polychlorinated blphenyl's (PCBs)form a transformer facility in accordance with the Toxic SubstanceControl Act (TSCA; 40 CFR 760) and California health standards.

ARlf00607

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ERIC M. BANE

EDUCATION: ':' .K ":-.Flshburne Military School/ Waynesboro, VA. 1982Ferrum College, Perturn, VA. 1987. BS - Environmental ScienceOSHA HazWOPBR Training (40 CFR 1910.120). 1968Chlorine Safety Seminar. 1988

LICENSE!Commonwealth of Virginia Class III Water/Wastewater Treatment

Plant Operator. -

EXPERIENCE!

Two and one-half years experience in environmental compliance.Experience Includes operation of a 7 MGD (million gallons per day)wastewater treatment plant and independent operation of a 2 MGDdrinking water filtration plant serving approximately 20,000residents. Additional experience includes Resource Conservationand Recovery Act (RCRA) recovery/ identification/ transportationand disposal of hazardous waste and emergency response. Fieldduties included monitoring and sampling of air and water/ preparinghazardous waste for transportation and supervision of small workcrews. Supervision includes dally management of remediation crewdecontaminating polychlorinated biphenyl's (PCBs) from anoperational factory in accordance with federal (TSCA; 40 CFR 760)and California standards

ARlt00608

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AYTOC FIBERS FRONTROYAL INC.AVTEX FIBERS SITE

ROB INSON PIPE CLEANING COMPANY

PERSONNEL AND QUALIFICATIONS

ncnoirej

ADMHBIRAIJVI ORDER

V. 8. EiYiromtiul Protictioa A uqr

ScgioilD

AVTEX HBEEfl PSOHT fiOTAL QIC.KalriekUMP.O. Box 11(9

AR1«00609

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ROBINSON PIPE CLEANING CO.

HAZARDOUS VASTE CLEANING

Robin*on Pipe Cleaning Company h&i cleaned approximately 60.000*of 6" - 72" atom and eanltavy *ewere, removing Dioxin and otherhazardous chemicals. This project covered the Love Canal areaof Niagara Palit, New York, and took approximately four nonthito complete. All of our equipment bad to be decontaminated ---before returning to ovr boat.-.**••*Robineon Pipe Cleaning Company ie one of the nost experiencedenvironmental contractor! in the nation.

mt")6"'

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OCT IB '89 12142 ROBINSON PIPE CLCanlNC CO. 84 PA P. iROBINSON PIPE CLEANING CO.

Pcat-lt"1 brand fax transmntal memo 7671r

RESUME .OFROBERT J. MCMILLEN

Started with Robinson Pipe Cleaning Company as a laborer in 1972 andworked his way up to Assistant Superintendent for all of our variousservices, specializing In cloeed-olrcuit television Inspection.•Bob McMlllen spent several months supervising and working vith theNew York State Department of Environmental Conservation in.thecleaning of scorn and sanitary aevars in the Love Canal area ofNiagara Falls, Kev York*

RESUME OFWILLIAM A. BURCHELL

Started vith Robinson Pipe Cleaning Company In 1986* • 12 years priorexperience la Coke Plant, Byproduct Steel Making Facilities* CheracialPlants and Pover Stations at different levels of management - Foreman,Superintendent* Manager and Vice-President.

RESUME OPMICHAEL J, LOHC

Started with Robinson Pipe Cleaning Company In 1976. Hie capacityvith Robinson Pipe Cleaning Company is supervisory at this time,promoted to general manager in January, 1979. Mr. Long Is our safetyco-ordinator; Is Involved In our sales and bid responsibilities.

RESUME OF .EVELYN H* FUMCA

Started vith Robinson Pipe Cleaning Company as. a secretary in 1958,Mrs. Punka is now Secretory-Treasurer of the Corporation. She alsohandles the duties of Controller and Office Manager.'

RESUME OPCLARENCE JOKES

Has 13 years of experience In the field of storm and sanitary sever ,..cleaning as a working foreman. Re also has years of experience in theroddlng of conduit and placing of fiber optic cable for thetelephone companies.

AR<t006il

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AVTEX FIBERS FROHT ROYAL INC.AYTEX FIBERS SITE

ODNCO

JffiCXXWU

A0MMBTRAT1VE ORDER

Pn}mi for

V. 8. EaviroiAtatil FiPtietloa A aey

AVTEX FIBERS ROKT ftOYAl IHC,KnfricfclueP.O. Box 1169

22530

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CONGO CORP.LAWNSIDE.NJ.

Prime contractor employed to install hydraulic cement in sumpinverts throughout the sever system. See detailed sketch. This firm isemployed on the plant site for many typical construction projects in theconcrete, insulation, and masonary areas.

The work plan consists of thirty (30) manholes locations fromA-44 thru outfall 003. Two 12 hour shifts will be utilized until the scope ofwork is completed. Air monitoring and proper entry safety precautions willbe utilized at all times. Pnuematic membranes will be used to plug flowinto and out of the sumps until the concrete installation is complete.

Personnel and Qualifications

£. Fletcher - Superintendent22 yrs. military service . .20 yrs. construction, brick mason, concrete finisher, coating?

specialist, foreman, and superintendent.

E. Noffsinger - Brick masonIS yrs. concrete finisher and foreman

J. Lutek - Brick masonS yrs concrete finisher and foreman

flRt+00613

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i i

AVTOC FIBERS FRONTROYAL INC,AVTEX FIBERS SITE

CH EVflCA L WASTE MANAGEMENT INC

PERSONNEL AND QUALIFICATIONS

OKDE8

Fnpnl for

0. 8. EatinuataulFrouctioi Aptqr

•I v-%•> ..-••-. li'

, J ,. I • • . i • ' rO C , . . '• LI ... I

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Chemical WasteManagement

TECHNICAL SERVICES JOB POSITION TRAINING BEQlTOEMENrS LIST v j.

Position Titlei Field Analvst/Pro-iect Leader

Prepared Byt JOHN BAKER___________(Nama/Tltle/Signature)

Approvals;

1. General Manager:______________________(Name/Signature/Date)

2. Technical ServicesOperations Manager:

(Name/Signacure/Date)

A. GENERAL TRAINING

1.000 New Employee Orientation (mandatory for all new employees)1.10 Introduction1.20 Welcome to the Company1.30 OM's Environmental Policy1.40 * Regulation Compliance1.50 CERCLA Overview

2.000 Basic Safety TValning(l)2.10 Environmental and Chemical Hazard Recognition2.20 Hazardous Wasta Characteristics and Basic Control Methods2.21 Chemical Properties of Hazardous Materials2.22 Basic Toxicology2.23 ILVs and FEts2.24 Hazard Comunication Standards and Information Sources (2) (3)2.25 Medical Surveillance Overview(2)2.26 Employee and Environmental Monitoring2.30 Personnel Protective Equipment(3)2.31 Fundamentals of PPE<3)2.32 Fundamentals of Respiratory ProtectionO)2.33 Air Purifying Respirators(3)2.34 Basic Protective Equipment (Level C) Inspection, Donning and

Ranoval(3)2.35 Supplied Air Respirators(3)2.36 Advanced Protective Equipment (Level B)(3)2.40 Heat Stress and Dermatitis2.50 Hearing 'Conservation Orientation2.60 Generic Site Safety Plan Review2.70 Site Control and Decontamination2.80 Site Evaluation and Preparar*— ««•«»*«

i 3 . » ,-^-n ARU006I5

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Technical Services Job PositionTraining Requirements ListPage 2

2.90 Site Security2.100 Cconunication Systems2.110 General Safe Work Practices

3.000 Basic Emergehcy'Responfie and Preparednesso'iS Contingency Plan Review and Incident Reporting(3)3.20 Fire/Explosion fteventlon and Protection -3.21 _ Flre Extinguisher Practiced)3.30 First Aid(4) ; v;3.40 CPR(3) V3.50 _ Emergency Medical Procedures

_3?60.. .iasic Spill Response(1) Mandatory for employees ttoo vlll work at project sites full orpart-time. - ..- - -• - -;:r;-r < -•-(2) Hatbe conpleted by office'eDployees.(3) Annual refresher training is required.(4) Refresher training is required: every 3 years.

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iecnnical Services Job PositionTraining Requirements ListPage 3

B. JOB-SPECIFIC TRAINING

Record in the space provided the course descriptions from the MasterList that are required for job position duties (attach additional pageslisting these courses if necessary) .

1.0001.201.301.401.50

Waste Analysis PlanAnalysis RequirementsSample Collection ProceduresSample Analysis MethodsContainer Marking

2.0002.102.202.30

Materials HandlingLifting Techniaues • .Drum Handling SafetvDrum Sampling. Classification. Staging and/orTransport

2.402.702.802.902.1002.1102.1402.1502.1602.170V2.200

Liouids Pumping and BulkingLab-Pack Preparation and ShipmentExplosives HandlingRadioactive Materials Identification and ContainmentCompressed Gas Cylinder HandlingLockout (1) vGrounding and Bonding (2) x-Con fined Space Entrv (3)Operation of Hand and Power ToolsAir Compressor Care. Use and LimitationsOn-Site Storaae

3.000

3.20.3. 50

Ecruipment/Vehicle Inspection. Operation of Forklifts.Over-the-Road Vehicles fForklifts. Trucks. Fume Hood)On— Site Storage Area (ForkliftsJOff-Site Transport Vehicles f Trucks)

4.000

4.204.40

6.0006.20

Eouipment/Vehicle Corrective Maintenance IncludingInspection of (Forklifts, Trucks. Fume Hood)On-Site Storage (Forklifts. Trucks. Fume Hood)Off-Site Transport Vehicles (Trucks)

Phase I Reoulatorv Compliance Procedure Training (1)On-Site Storaae•PAP•Vehicle/Container Inspection RCRA•TSDF Waste Acceptance Standards•Lab-Pack Manual•EPA Standards

moosi?. 'i,

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Technical Services Job PositionTraining Requirements ListPage 3

B. JOB-SPECIFIC TRAININg - (CONTINUED) ^." (*'*

Record in the space provided the course descriptions from the MasterList that are required for Job position duties (attach additional pageslisting these courses if necessary). .:6.40 Off -Site Transport

•DOT Hazardous Materials Shipment•PAP•Vehicle/Container Inspection RCRA•TSDF Waste Acceptance Standards•Lab-Pack Manual

6.50 Laboratorv•PAP • .•Lab-Pack Manual

e.ooo8.15

Project Manaflement ProceduresPersonnel Travel Arrangements

fi.16 Prolect-Specifie Continoencv Plan DeveioDment8.178.208.258.30

Operations Plan ReviewMobilizationSite PreparationPro-feet Activation and Comoletion Accord! no toPlans and Contracts

8.408.47

DemobilizationSite Shutdown

10.00010.10

10.20

Hazard Ass*»sKTn(»nt (4)Explosimeter Capabilities. faHhratlnn. USA.Limitations, Routine MaintenanceToxic Gas Testing Instruments Capabilities.Ca1ibration. Use Limitations. Routine Maintenance

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Technical Services Job PositionTraining Requirements ListPage 4

(1) Ccoplete before working under reduced supervision.(2) Corplete before transferring flanraable liquids under reduced

supervision.(3) Complete before entering a confined space.

Complete before using test equipment under reduced supervision ofqualified employee.

ARJ*006I9

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Technical Services Job PositionTraining Requirements List~ 5

C. SPECIAL SKILLS TRAINING ! t i

(Reserved for listing unique skills training based upon employee'sassignment to special .v duties such as contingency plan emergencycoordinator). \1.OOP Contingency Plan Team Member Training4.0005.000

Defensive Driving*Fingerprint Testing

.*. i T.* ... . .„ -, t --- m \ * " . > • . - ' • . -

*Within one year of

MANAGEMENT TRAINING

hirer,•'>. .., . »» •

(Reserved for Technical'-Services management down to the first*linesupervisor to teach them personnel management and hazardous vastemanagement skills).

1.000Phase II Regulatory Compliance Training4 . 000 Effective Supervision Program, if applicable.

>

r ~ . . * -A 'f * * :-' ; • • - ' - • • .

- • -- • • . ...; "', :-i $*• " J ,.• :.. • "• ' • • ' ' ' '' ' • • . - . ' • ; '

E.. PRDJECT-SPECinC TRAININC? * |i? " !?

1.0002.0003.000 :6.0006.000

• ' ' * ' " ^ ""''" " " ^ _•-•-•_' ;Operating Plan and Site Layout ReviewProject-Specific Hazard CcoxnunicationProject-Specificltegulatory ReviewContingency Plan Review ;: Project-Specific On-tiie-Job Training ;

HOT LEAVE BLANKS. PUT N/A IF NOT APPLICABLE.

AR<(00620

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waste Management, inc. .POSITION DESCRIPTION

POSITION TITLE Prolect Leader/ Field Analyst_________

PIWISIQM/LOCATION Technical Services- HCPQHTSTQ Operations Manager

INCUMBENT——Various Field Analysts____ APPROVAL_Ififfnawff •! immMim Cve**)**'!

0»tt

1) Basle Function (Briefly summarize the overall function andobjective of the position omitting specific duties.)

Responsible for running jobs, supervising field technicians andanalysts and contact with customers on a regular basis. Performsthe manual and technical tasks necessary to safely handle hazard-ous waste through all phases of labpacking., sampling, andremoval of waste material from each project site.

2) Specific Duties and_Responsibilities (List each significantduty and responsibility, attach additional sheet if necessary.)1. Classifies, segregates and packages hazardous wastes.2. Performs analytical testing on unknown chemicals.3.. Maintains accurate, legible records.4. Prepares labpacks and non-labpack drums for shipment.

Preparation includes packaging, labeling, marking, andplacarding according to DOT. Preparation also includesloading, blocking and bracing containers in vehicle.

5* Completes manifests for shipment.• 6. Collects representative samples according to the Waste

Analysis Plan. Delivers samples to Technical Ma«*t»r-7. Overpacks non-labpack containers in poor condition- sov *niey

can be shipped.8. Has working knowledge of safety equipment and requirements

I -) for use of equipment.9. Drives trucks and forklifts.10. Responsible for performinn um-v *•« -—* -ontract specifications

^ ;<:;; ftRiiOOesf

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<* **J

-2-

11. Supervision of field analysts and technicians.12. Responsible for enforcing safety policies. >,13. Responsible for remaining in compliance with PAP and

Regulatory Agencies.

3) Skills, Education and Qualifications Required (Indicate the•Kills, education, experience and qualifications required forthis position.) >;.. • j1. Educations B.S, in one of the sciences.2. Experiences College chemistry background. 'Minimum one years

experience as a field analyst. F3. The following skills are preferred}

r . -i f | * J '; 1

a. Good verbal and written skills.. rb. Ability to supervise other workers.c., Valid drivers license. L . ,

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Page 166: for each sample and each handling of the sample is … ICAP/AA Laboratory for the analysis of metals o Tech Laboratory containing automated instrumentation, for example, Technicon

KMT5.ICAL fcXAMINATION OF DRIVERSNom«: __,

2_»,.:*' ~ •• —- - ^-Moight g ft. ——^2—— In. Wotghl ° ^^—— fci. D N.w Cortificaiion

HEALTH HISTORYWA« *• .. - ' _. •/ • .«TO$ wo ' n ., .' f Yf iD «f Mood or iplnot lnjwrit». "' Q o£ Norvovi Homoen,O V Soilurti, fin, convuliioni, or foinflng. D JkC thtumotit ftvtr.O IT iKtomlvo confintmonl by Wnoit or ln|vfy. ,•' J5', 'i;D 'P- Aithmo. i " 'O J& Cardiovatcwlor diitait. . Q & Ridoty dii»io. -'O f- Twbtrcvfotii. ~ O f£ MvKulor diiooit. , . .O i : SypMii....... ' - '• , ; D & Sufftring from any otntr ditcoM.O ;1 Oonorrhoo. - -. - ; "-"" Q f£ Ptrmontnl dtftet from «n»n. dhto» or injury.O £• OtobtHl, - •' ' .,.,.„, Q gT Ptjrthiotric ditordtr.O r OoftrointtitinaTvlctr. Q p< Any other norvowi ditordcr.

If ant wor lo any of Mio obovo 1* yoi. Oiploln; -^__- -._._ L f_" '.._*_ " ' • — • U^ __ __ __ __ _ _

PHYSICAL EXAMINA TIONGENERAL APPEARANCE AND DEVEIOPMVISION: Par dhtonco: Vght »/ &f) * Uft »/ 30* ' O WHhoul corrodlM lonioi NzTWith torroeti«t lonici if worn- . — - "^«. flk _ L_ x. a —«d n

Rvidoneo of dhooto of tafwry: Kght;.

AUDIOMETRIC TCST (com loto only If avdiomtior b mod fa frit booring) dnibol loti of 900 HIat 1.000 Hi ______

If organic di**oit b OfOWnl. It fulty cornpontaltd?Wooo acoiivro* vjwolic

^————*

Accommodotton RightKnoo Joriu: Rieht: Normol

Uft: " Normolf

lowor..—————f . .. .H f"———— SpinoURORATORY AND OTHER PEC1AL ftNOINGS: IMno: V" **• / JLT7 - _______ -*IK I U/jf Sugar

Oihor laboratory dote (torology. ok) _- .__-._- ' _-i___'.._Radiological data -• - —-.—.-— _---.r-:-n_-n...--...- |I«tirocordiogroph

6CNCIJAMES E. BELLAMY. 0.0.

(Ooto of OKOfitinotion) (Addrou of oiomfnlAg doctor;D CHECK HERE If NOT QUALIFIED . . . . . . .

NOT1: Thhfocfion to b« complotod only whon vtoval lost k condwettd by • IconTE: TMucction to fe

(Ooto of abomination) • (Addrotiaf oiamlnof) (No»t of o-omintr) (Print)

(kgnaivrtoT'S CERTIFICATE

Safety »('i Mmo) (Print)

(49CPR9°MI*99l.49)«fld«rHKIinowlodgf of Mi dv*ioi. I find Mm f uattfiod WB " **•'•fit'SJiffiU C Roltarnv/ OrDr^J QiWHtiOv only vwon woarlng corroctivo lontoi. \ '.,.'" .; < • • «« ' « * 1*1. ^^ &~^oouatifiod«nv«ii#n»oaring«iiooriiig«id. EnviroCare Health sefvrcer

^ A complotod OMminoHon form for (Mi ponon b on ffl* hi *y Wfwo «t

ARi*0062lt ROOK NO. >•

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, ?; WASlt WLNAGEMENT INCORPORATED" 'iPHYSICAL EXAMINATION AUTHORIZATION AND REPORT

John Baker l«s-M-9«?i_____ rigid Analv«»Name SS Number " Job Title ,

Date and Time of Appointment March 21. 1989 11*00 A.M.(Date) (Time)

Examination Type (circle one) ABC Cu) EMgnit ^—^ ^DhrfsRKJson for Examination: __ Pre-placement \/ln ServiceAvenue _ Return to Duty _ Termination Treatment

Attached In Medical Provider Guide Hot RequiredJob Description: ____________ or 4 _________ or _____Exposure Data: _________ or ' •: • • or _____PPE Required: _______________ °* "* or -

Previous Medical Data Location! Note; Do not eat or drink tvalvafm hoursto 8che£vl«d phy«ic«l, *•fr\ t

ES* f MSite Designate Jpf ~. Mte

FROM: Dr. JAMES E. BELLAMY. P.O.(Examinins Physician)

I have personally examined J_6~JL*+, /3jJ-jLJA~* and have informedthis person of the examination results and any conditions requiringfurther examinations and treatment in writing.

In addition, 1 have personally evaluated tht described job duties,required personal protective equipment (including a respirator), theresults of the required ancillary studies and 1 have determined thatthis person: . . . - - -n - - - - . •;-- • • , . :

la medically qualified for tht job described and can wear arespirator and personal protectivt equipment.

_ Is HOT medically qualified for tht job described.__ la medically qualified for tht job described vith tht following

limitations t __ - • • •_______" ___

limitations effective until:

PHYSICIAMADDRESSt FnvlroCaro Hoolth Cenrtm

VM-HR03 """ em!cal Waste Mgml5/g7 . .Technical Services Division

41-65 Doremus Avenue

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\

ARI»00626

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CHEMICAL WASTE MANAGEMENTEASTERN REGION

TECHNICAL SERVICES DIVISIONRESPIRATOR PIT TEST RECORD

Date of Teat:Name of Employee: __

Location of Fit Test: A.4&t£s*t A/J.

Respirator Selection

1 2

Manufacturer ASfl ! _

Pace Piece (half or full l

Size /Vftfitf/n

Cartridge Used

Positive/Negative Pressure .

Isoaayl Acetate

Irritant Smoke -

Other (Explain)

EMPLOYEE ACKNOWLEDGE AND DOCUMENTATION:; .. ..

1) I have been informed about the nature of cgspiratory hazardsand the reasons for using the respirator. pS. Yes ( ) No

2) I have been instructed in the proper use, limitations,inspection and maintenance of the respirator. / i Yes [ 1 No

Person Tested: jff ____* Slgnatuft/Title

s*Pit Test Performed By:

Signature/title

COMMENTS:

TEST EXERCISES:Breath normally, breath deeply. Move head in all directions(side to sidet up and down) inhaling when-full range of motion isachieved. Talking. Jogging in place. .

AR(*00627

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i J *«r th« underaigntd, hav« attended an informal training ••••ion addressing

and discussing the following topicat Customer Relations, Vehicle Inspection Kftporta,

Trip Keports, W«»tt Profiles, Special rfaste Profiles, «nd Profile Kec«rtific«tions.

Session conducted at the C*i office ioetted at the Aberdeen Proving Ground, Friday

hovember 11, 1988*

-ft- ^

~-jC-

«RI>00628

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flft«*00629

Page 172: for each sample and each handling of the sample is … ICAP/AA Laboratory for the analysis of metals o Tech Laboratory containing automated instrumentation, for example, Technicon

INSTRUCTOR!

ATTENDANCE RPrnon

LOCATION:

»

;tv<ri<:;

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ORIENTATION

31 tfffl LOCATICW/nHB jL*Jt /# iDATB:^_______...... _ „ _,,„.„„, . « „ _ _ « _ ^

The following employees were given an orientation of Cheoical Kast* Management.The people were shown general Chemical Waste Management policies as relatedto'their job. They were alao shown how to properly don and remove Level CProtection.

Ttie employees understand their responsibilities in regard to conpany policies*as outlined in the seminar, and will pcactive these on .the job.

PRINT YOUR NAME SIGNATURE

TRAINER'S SIGNATURE Mm #TA A R k 0 0 6 3 I

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HAZARD COHMUKICATION STANDARDSAND

INFORMATION SOURCES

PATE.

The following eaploycts successfullr eoapleted this course. The course coveredaaployaee llght-to-Knov as per OSHA Haxard Conmunieation Standard* infonationOD labels, KSDS's (Katcrial Safety Data Sheets), route* of entry and types ofexposure. A three (3) volume set of binders which contain information on allState Right-to-Know lavs, reference guides and Information and special reportspertaining to the tame. A Right-to-Knov booklet was given to each personattending toe course.

PRINT YOUR HAKE SICHATORE

TRAINER'S v ^ Mm U fl/ AR^00632

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RESPIRATORY HOTECTION

M9?

Itie following people were trained on both Level B and Level C BreathingProtection (Filtered Air and Supplied Air). All the following peoplewill wear appropriate breathing protection on the job site that is.required and will maintain* sanitize and store their respiratory equip-'went properly as defined by CWM Safety Policies as instructed. .. , ,

PRINT KXJR MAMP

TOAINER'S SIGNATURE

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SPILL RESPONSE/FIRE FIGHTING

PATE. J&. IW LOCATION/TPCx Mf/tirl* A/JJ J **Qfl

The following errploye*s have been instructed on the basis of spill responseand fire fighting. The course gave the employees a basic knowledge of whatto do in a spill or fire situation. Qrployees were told that in a spill orfire situation if initial response, by them/ cannot control the situation/ theyshould call appropriate help.

The employees understand the basic types of spill response and fire fighting thatthey are required to perform on their job. . •

PRINT TOUR NAME SIGNATURE

1*AINER!$ glCNATORE jffm.ffh»/jff* A R fc 0 0 6 3 •*

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*"•"""•'""" *:' '-V >''*

•mix f .J. ttcnmWtlt &rf/>

ruiett ^ ' ' ~

SSOOTS

«Nt$l

ATTINPttS

UIMt. NAKI

y jcVg -__-_, — ^ - - ....J. ^ vl/*T

• v

gICNAT0RC<<) *

ARd00635

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STATE AKD LOCALREGULATORY. AWARENESS

DATE: trf, LOCATION

The following people were made aware of stste and local lavs (andregulations which control hazardous waste managexeent and the protectionof people and tha environment.

TRAINER'S SIGNATDXX

ARU00636

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IXnODOCTXOIt TO RZOTLAnOK AIOREXm

«A«l y^ L/ • lOCAnOK/TP-tt

The following people tuccessfolly completed this Coapliaaee Awarenesscourse* This course gave an overview of key federal environmental lawstuch as the Clean Vster Act* ICRA and TSCA. Eo >leye«t learned thepurpose and ft me tore of each l*v; the difference between wles sadpermits i and the responsibility of each person, as veil as thecorporation to comply with federal, state and local lews and regulations '(as vail as VMZ/CWK policies) related to hazardous vsate management andthe protection of people and tha environment.

PRINT TOPR KAHE SICTATPRE

77

TRAINER'S SIGNATURE J_____________________-7T-0—————1^———————|^. P •————————————

• *

ARU00637

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RCRA OVERVIEW AND FACILITY COMPLIANCE ACTIONS

DATE: Mrt/tJ tfM LOCATION/TIME:

The following people successfully completed this RCRA orientation.This orientation included: RCRA Interim Status standards for a TSDF;the status of our Part B application; overview of the site's layout andwaste handling processes; a review of our internal watte managementcontrol system, PAP B-900 and our Waste Analysis Plan; site securitymeasures; the site inspection system; alarm systems and emergencyequipment; our contingency plan and evacuation routes; the purpose ofhazardous waste manifests; and the responsibilities of employees inhelping to comply with the RCRA standards. •

PRINT YOUR NAME SIGNATURE

- r. t

TRAINER'S SIGNATURE

«R!t00638

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rUNDAMBHAL CHMSTOY

*

The following employees were given a seminar in fundamental chemistrydealing with properties and hazard of different classes of chemicals.'Each employee understands their responsibility to use their knowledgeof chemical properties and hazards when working with chemicals on ,their job. ^

PRINT YOUR NAME SIGNATURE

TRAINER'S SIGNATURE „ .

, ,,,, -CK ARU00639_.;»juU^/u; .. ,. , .: ,,>-„--.:,.,„... v^ • • •

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HAZARDOUS WASTE CHARACTERISTICSAND

BASIC CONTROL METHODS

DATI: rt .o LOCATION/TIME ;

The following people successfully completed this Hazardous WasteCharacteristics and Basic Control Methods course. The course gave theemployees an awareness of the hazardous properties of wastes such asflamoability, explosivity, corrosivity, and oxidation. Employees werealso made aware of two conanon hazard warning labeling systems: theNational Fire Protection Association (NFPA) and the Department ofTransportation (DOT) systems. Finally, employees learned thedose/response concept concerning exposure to potentially harmfulsubstances, the routes of exposure, the difference between acute andchronic effects, basic personal hygiene methods and bow to researchinformation on USDS' s and our own Waste Profile sbeets.

PRINT YOUR NAME .SIGNATURE

TRAINER'S SIGNATURE

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TECHNICAL SERVICES JOB POSITION TRAINING REQUIREMENTS LIST

Position Title: Field Analvst/Proiect Leader

Prepared Byi PHTLLIP LAWHON(Nane/Title/Slgnature)

Approvals?* _ , . , - " ' '

1. General Manager i(NanE/Signa cure/Pate)

2. Technical ServicesOperations Manager:

r .y* <Na__e/Signacure/Date)r .*,-,_- i . '. - -

A. GENERAL GAINING

1.000 New Eoployee Orientation (mandatory for all new employees)1*10 Introduction1.20 Welcome to the Coopany1.30 CtWs Environmental Policy'1.40 * Regulation Carpi-Lance1.50 C__RC1A Overview2.000 Basic Safety Training(1)2.10 Environmental and Chonical Hazard Recognition2.20 Hazardous Waste Characteristics and Basic Control Methods2.21 Chemical Proerties of Hazardous Materials2.22 Basic Toxlco]2.23 TLVs end PI2.24 Hazard Cooziu-lcaclon Standards and Information,Sources (2) (3)2.25 Medical Surveillance Overview(2)2.26 Enployee and Environmental Monitoring2.30 Personnel Protective Equipment(3)2.31 Fundament-ale of PFE(3)2.32 Rmdamentals of Respiratory Protection(3)2.33 Air Purifying Respirators(3)2.34 Basic Protective Equipcoenc (Level C) Inspection, Donning and

Removal(3)2.35 Supplied Air Respirators(3)2.36 Advanced Protective Equipment (Level B)(3)2.40 Heat Stress and Dermatitis >2.50 Hearing Conservation Orientation2.60 Generic Site Safety Plan Review2.70 Site Control and Deccnta-til-nation2.80 Site Evaluation and Preparation Overview

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Technical Services Job PositionTraining Requirements List

2

2.90 Site Security2.100 Cconnnicatlon Systems2.110 General Safe (fork Practices3.000 Basic Emergency Response and Preparedness3.10 Contingency Plan Review and Incident Reporting(3)3.20 Fire/Explosion Prevention and Protection3.21 Fire Extinguisher Practice(3)3.30 First Aid<4)3.40 CPR(3)3.50 Emergency Medical Procedures3.60 Basic Spill Response

(1) Mandatory for employees who will work at project sites .full orpart-tine.

(2) Must be corpleted by office employees.(3) Annual refresher training is required.(4) Refresher training is required every 3 years.

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tfc.Technical Services Job PositionTraining Requirements List

je 3

B. JOB-SPECIFIC TRAINING *r:..'?>i;:. .

Record in the space provided the course descriptions from the MasterList that are required for job position duties -(attach additional pages

, listing these courses if necessary).

1.000i.io1.301.40J.50

_2.000_ J.io2.202.30

2.402.702.802.902.1002.1102.1X02.1502.1602.170'2.2pO

3.000

. 3.203.50

4.000

4.204.40

6.0006.20

Waste Analysis PlanAnalysis RequirementsSample Collection Procedures *Sample Analysis MethodsContainer Marking -

--.-....-••- - ' • j - . . , - --Materials Handling-Liftlna Techniaues .Drum Hardliner SafetvDrum Samplina, Classification. Staaino and/orTransoortLlouids Pumpina and Bulkino •Lab-Pack Preparation and Shipmentexplosives HandlinoRadioactive Materials Identification and ContainmentCompressed Gas Cvllnder HandlinoLockout rnGround Ina and Bondina 121Confined Space Entrv 13}Operation of Hand and Power ToolsAir Compressor Care. Use and Limitations 'On-Site :storaae--.. ----... . . . . . . • -Eauicment/Vehlcle Inspection, Operation of PorkliftarOver-the-Road Vehicles tForkllfts. Trucks. Pume Hood)On-Site Storaoe Area (PorkllftslOff-Site Transport Vehicles fTrucksl ^.„ . .... . ... -,-- ~—~" ----- "-- •• , ,., -- - .-Eouioment/Vehicle Corrective Maintenance Ip^tudipaInspection of fForklifts. Trucks. Fume Hoc* )On-Slte -Storaoe fForklifts. Trucks. Fume tfood)Off-Slte- ransriort Vehicles ITrueks)

Phase I Reau^atorv Compliance Procedure Trai,pino <1)On-Site -Storaoe *"*• B &D ,.... - .i __ . o-.""——**--"*™* i™""""11 '• "

•Vehicle/container Inspection RCRA*TSDF Waste Acceptance Standards•Lab-Pack Manual -~-n r•EPA Standards ™

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Technical Services Job PositionTraining Requirements ListPage 3

B. JOB-SPECIFIC mDfl-NG - (CONTINUED)

Record in the space provided the course descriptions from the MasterList that are required for job position duties (attach additional pageslisting these courses if necessary) .

6.40 Off-Site Transport•DOT Hazardous Materials Shipment•PAP•Vehicle/Container Inspection RCRA•TSDP Waste Acceptance Standard*•Lab-Pack Manual

6.50 Laboratorv•PAP ' .•Lab-Pack Manual

.8.0008.158.168.178.208.258.30

Project Management ProceduresPersonnel Travel ArranaementsProject-Specific Contlnoency Plan DevelopmentOperations Plan ReviewMobilizationSite PreparationProject Activation and Completion According toPlans and Contracts

8.40 Demobilization8.47 Site Shutdown

JO. 000JO-10

10.20

Hazard Assessment 14)Eyplosimef (»r Capflh \ i t< e* . O»1 fhrat 4 nn r fl o .Limitations* Routine MaintenanceToxic Gas Testino Instruments Capabilities.

.^—

Calibration* Use Limitations. Routine Maintenance

ARi*006(tit

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Technical Services Job PositionTraining Requirements ListPage 4

(1) Complete before working under reduced supervision.(2) Ccoplete before transferring flarm-able liquids under .reducedsupervision. ^--.^ ^ ;(3) Complete before entering a confined space.(4) Complete before using test equipment under reduced supervision ofqualified employee. : yr rf -- •

ARitOOGdS

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Technical Services Job PositionTraining Requirements List

£.

C. SPECIAL SKILLS TRAINING

(Reserved for listing unique skills training based upon employee'sassignment to special duties such as contingency plan emergencycoordinator).1.000 Contingency Plan Team Member Training4.0005.000

Defensive Driving*Fingerprint Testing

*

'Within one year of hire.MANAGEMENT TRAIN-TO . .

(Reserved for Technical Services management down to the first-linesupervisor to teach them personnel management and hazardous vastemanagement skills).

1.000__Phase II Regulatory Compliance Training4.000 Effective Supervision Program, if applicable.

,

PROJECT-SPECIFIC TRAINING

1.0002.0003.0006.0008.000

Operating Plan and Site Layout ReviewProject-Specific Hazard CconunicatlohProject-Specific Regulatory ReviewContingency Plan ReviewProject-Specific On-the-Job Training

DO NOT LEAVE BLANKS. PUT N/A IF NOT APPLICABLE.

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i jwaste Management, inc.

POSITION DESCRIPTION

POSITION TITLE " Project Leader/ Field Analyat ___

DIVISION/LOCATION Technical Services* REPORTSTO Operations Managerirtiiwi

mr.Mu.ncMT Various Field Analysts____ APPROVAL_________'._______

0*t*

1) Basic Function (Briefly summarize the overall function andobjective of the position omitting specific duties.)

Responsible for running jobs, supervising field technicians andanalysts and contact with customers on a regular basis. Performsthe manual and technical tasks necessary to safely handle hazard-ous waste through all phases of labpacking, sampling, andremoval of waste material from each project site.

2) Specific DutlcB and Responsibilities (List each significantduty and responsibility* attach additional sheet if necessary.)1. Classifies, segregates and packages hazardous wastes.2. Performs analytical testing on unknown chemicals.3. Maintains accurate, legible records. :4. Prepares labpacks and non-labpack drums for shipment.

Preparation includes packaging, labeling, marking, andplacarding according to DOT. Preparation also includesloading, blocking and bracing containers in vehicle.

5. Completes manifests for shipment.• 6. Collects representative camples according to the Waste

Analysis Plan. Delivers samples to Technical Manager.7* Overpacks non-labpack containers in poor condition", ea, they

can be shipped.8. Has working knowledge of safety equipment and requirements

for use of equipment.9. Drives trucks and forklifts.10. Responsible for performing work to meet contract specifications

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-2-

)11. Supervision of field analysts and technicians.12. Responsible for enforcing safety policies.13. Responsible for remaining in compliance with PAP and

Regulatory Agencies.

3) Skills, Education and Qualifications Required (Indicate theskills, education, axperienca and qualifications required forthis position.)1. Education: B.S. in one of the sciences.2. Experience! College chemistry background. Minimum one years

experience as a field analyst.3. The following skills are preferred:

, - '' * -.. t ~ • ~ 'a. Good verbal and written skills..b. Ability to supervise other workers.c. Valid drivers license.

RRU006U8

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F MARYLAND, CHS VEHICLE OPETOB'S CERTIFICATE

ffluiwd toDrivtr UcanteCertified ByExpiration Date

I tt A

V^

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Philip Lawhon - Chemical Wastit Mannoprnpn*'^ Tnr.

HAS SUCCESSFULLY COMPLETED AHAZARDOUS WASTE (CHS) TRANSPORTERSTRAINING PROGRAM ADMINISTERED BYBOGERT CONSULTING SERVICES AND

APPROVED BY THE MARYLAND DEPARTMENTOF THE ENVIRONMENT.

CHARUSRBOOCRT

March 26, 1988

;>,- :• *-.'• ?i V: •"

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w*y • •$Cr*S»&l &

MATERIALS, HAtaXXES. .-HIKS;

ATTENDANCE RECORD

NAME (PRINT PLEASE) ' JCfe TITLE ~"" SICWHIRE

V

He /J^

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Chemical Waste Management, Inc.Technical Services DivisionRO.Box96Sealston. Virginia 22547 v J703/775-9000 ^

PROTECTIVE BREATHING EQUIPMENT FIT TEST RECORD

DATE s i JA/M. ,J M 0*?______ LOCATION s fS)PQ l_^0rgf• . * _—~v l . _

NAMSt t^hillQ Lfl .On DEPART.! f&IU

BREATHING APPARATUS!

BRAND flOSA MODEL _ _ _ __ _SI2EHALF FACE "tT_______ FULL FACB

TEST METHOD l

POSITIVE/NEGATIVE PRESSURE TEST VISOMAYL ACETATESMOKB

Bas this person been instructed on the proper user limitations,and care of this unit? YES v/ NO.

Was written instructions for th£4 unit provided?YES \/_ NO

V,/PERSON TESTED s

TURN IN UNITt

REASON(Explain)

SAFETY OFFICER! u i (L • (r&ttffTLSignature

•NOTEs This record, will be filed by the Safety Officer.

AR(f00652

Page 195: for each sample and each handling of the sample is … ICAP/AA Laboratory for the analysis of metals o Tech Laboratory containing automated instrumentation, for example, Technicon

Thh ttrlifajH txptrtt J /Mr* from j<tt tit J It rt*t»*llt 9*fythrough wollmtm in _W nmpltiio* *f **otbtr M*(iimt4i*

Fint Aid Count,

American Red Cross: This ccrtiEes that

PBIUiIP A. LAWHON •; y'has completed theMULTIMEDIA STANDARD FIRST AID.course of instruction

•t CHEMICAL WASTE MANAGEMENTCHESAPEAKE, 1

OCT. IB. 1988

flRU00653

Page 196: for each sample and each handling of the sample is … ICAP/AA Laboratory for the analysis of metals o Tech Laboratory containing automated instrumentation, for example, Technicon

si

Page 197: for each sample and each handling of the sample is … ICAP/AA Laboratory for the analysis of metals o Tech Laboratory containing automated instrumentation, for example, Technicon

REFRESHER TRAINING

The following have attcoded the SEAT STRESS & PREVENTION• . • refresher training .class Cor OP HIN. (length-of

tine) on MAT 26. 1989 .

SICNATORK

ID

is)

21)

13) r ~ TK.' KJUM

INSTRUCTORS)

19)r * •/

' V

20) ^

Page 198: for each sample and each handling of the sample is … ICAP/AA Laboratory for the analysis of metals o Tech Laboratory containing automated instrumentation, for example, Technicon

American Red CrOSS COURSE RECORD: FIRST AID /c

JompltM antf pmvw rt«ords promptly. CartHkatn ara tnuad to Inttructon only upon rtealptof • oomplttfd count racer*Conuet tfw toe* Rad Croii ehaptar for Information cortcamlnfl aupplln, KlKiry rtcordlnt.caniflata*. and Imignta.If teachlnf Hi a tocttion that li not tarvkad by a chaptar. contact tna ipproprlatt dlvtitonrt«*dqu«rttn off km.

NUMBER COURSE NAME

NAUC Or tMSTRUCTOH ItMV Plrit. MMtftol TlklPKONI NUMliR

Ahlhr .NO

STRIC* AOORCS* ' CITr. STATS ./ ZIP COOt

IKS Rfitrfl JSL M /t?. Mrti ff&fiiMAU. 076(0NAMtoVir^RUCTOR'S (tHAPTtR'OP AUTHORliATIOH '

NAUC OP CO/IKSTRUCTOR (tan. P«i MlddtiC ^tlCIPHONI NUMBtRt,n

•TftCtT AOOMC33 CITY, «T ATI ZIP COO I

NAMK OP CO* INSTRUCTOR'S CHAPTER Of AUTHORIZATION CITY. IT AT I

NAUI QP CHAFTIH WHIfll COURSE WAS CONDUCTED CITY. IT ATI

COURSC

Balks Pint AMStandard Flnt Aid andFtnonat SafatyMultimedia Stand**P lm AidAdvanced Flat Aid andErntrpancy CmCFfl ILaetun MtihodlCPR (Modular Syitam)CPU: Ran for Lift(UdurtMathodlCPU: Rnt for Ufa(Uodultr Syittm)

NO

m

6A

COURSE

Baile Pint Aid R«vtewSt*xt-r_1 Fim AM antPanonal Saftty Ravlt*MuHknadia St.ndar*Full Aid Raviaw

CfR (Uctura Method)rWVWMfCPR (Modular SyttamRaviaw

NAU* AMD AO.DM5* OP OROANI2ATION WHIR! COURSIJ»A» CO A DUCT I

10/ft/tt 7.SSEND CERTIFICATE* TO » Q OBOArtlZATlQN JDDHCM^ Q IHSTMUCTORt ADOMU QlN»TRUCTOR WILL CALC PQR

ASSISTING INSTRUCTOR! OR AIDES CHAPTER OF AUTHORIZATION TVTB OF INSTBUCrtJR RATWQ TYFE OF AIDE

**« tfi ti counthMtth« Amwkan R«d Crow.

NOTC. II • cv-trwwcior It ItowA tb» M-lnttructotSlCfNAfURB'DP tN*f«UCTO« ItOMATOB* OP CO-INSTRUCTOR

THIS SFACI FOR DIVISION USE

NOTE, LIST NAMES. ADDRESS. AND GRADES OF ALL PARTICIPANTS. LISTING IS OPTIONAL FOR BASIC FIRST AID COURSES TAUGHT INSCHOOLS. UNDER "GRADE." MARK "P" FOR PASSING, "f FOR PAIL I NO. AND "INC" FOR INCOMPLETE.

ADDRESS (Numbtr. Strati. Oty. St*ta, Zip CodtlPARTICIPANT'S NAME ILan Nama Flrttl

Page 199: for each sample and each handling of the sample is … ICAP/AA Laboratory for the analysis of metals o Tech Laboratory containing automated instrumentation, for example, Technicon

' •••"'"' 1 " f

CrOSS I COURSE RECORD: FIRST AID fc

, and proeta rtcordi promptly. Cartif teatn art teiuad to Innirvcton only upon ractipf{ raeomptrttdoouritrtcord. : tV >oni«ci tf* toot Rad Creu ehaptar for Information coneamlng mppIlM, KtMty rtcordlng.>— Brtlfk»ta ar>d tmignla. . ; « i „.,,...1 ;,* N Machir* hi a location *at H not atrvieatf by a ehaptar. connet tfw aftHopr latt tfMilon

naadgiHrwg oftfca. ; ET

NUMBER COURSE NAME

NAMI OP INSTRUCTOR ILMt *lr«t MltftfltJ v > TILIPHONt NUMftf R NO

j/>/>////NAME Of IMSTMWCTOR-S OHAPTIRP AUTHORIZArtON

STREET AOOffCSS . ••• ••• - - CITY. STATE ZIP COOI

NAUC OP CO-INSTRUCTOR-* CHAPTIM OP AUTHORIZATION CITY. ftTATI

Of CMAFTIR WHERE COURSE WAS CONDUCTED CITY, »TAT<

COURSE

•aakFlmAUStandard FM AM andFvnonalSafary

Pint AWAoVane«d Pint Aid andCnwgancyCariCPRlLjcturr Method)Crfl {Modular Syittm)CTA:ftaoif«rLifa(LaeturtM«tn«d1CFft:RacaforUfa(UoduUrtynaml

MO

man

4fl

COURSE

St-ndardFlmAJdantFwaonaf Sartty Ravlc*MurHmadla StandwdFlnt Aid RtvlawA-fvw>eed Flm Aid•nd tmarpency Cam

CPR (Lacturt Mtthodl

CPR (Modular Svsttmlfltvinv

NAUC AND AOOR&ftS OP ORGANIZATION WHERE COURSE WASCONtfUCTf ONAMg AND AOOR&U OP ORGANIZATIONeft*?*/ MsfT/ftMji/nt/fSiS'M Gr* i *!>*;£ Girth*. Kf. 7.S_ _S£NO CERTIFICATES TO » Q OROANfZATION A6ORtO Q INSTRUCTOR'S AOORf«3 /Q INSTRUCTdR WILL CALL FOR

NAMES OF ASSISTING INSTRUCTORS OR AIDES CHAPTER OF AUTHORIZATION TYPE OF JCTRUCfflfl TYPE OF AIDE RATING

tfwrt «hb oeun* MB MM MnducwtfIn

. II a •e-h-rtnicior la itatMi. aM«o-ln«tnjctof .... ___, __ .__ ,__ . _ __ _ _ _ _ _ _ __ _ __ ... . .mutt ab* tlgn •« town* rawrd. ^ SldhXrOftV&P INSTRUCTOR •lONATUffC OP CO-INSTRUCTOR

THIS STACC FOR DIVISION USE

NOTE, UST NAMES. ADDRESS. AND GRADES OF ALL PARTICIPANTS. LISTING IS OPTIONAL FOR BASIC FIRST AID COURSES TAUGHT INSCHOOLS. UNDER '•GRADE.'* MARK T* FOR PASSING. "F" FOR FAILING. AND "INC" FOR INCOMPLETE.PARTICIPANT'S NAME Ran Namt Flnt) ADDRESS (Numbtr, Stnm. CHy. <tm. tip Codtl GRADE

' / " iwtfi/ifa BeAtn. Hi.biutPA*i. Va. Ji'

Men/tut rtL'f.f»f<h*'.M. HIM•L fftiJM . PJ>;/,'6 . JULIOI

J7SX £ ffttAh.Wtre fjyi. KvpA/rf RutlfrOf

Page 200: for each sample and each handling of the sample is … ICAP/AA Laboratory for the analysis of metals o Tech Laboratory containing automated instrumentation, for example, Technicon

fed

Thtt cenifta tha certifies ihaCharles M. Bias -. .

ADULT CPI

ite Mgmt .+ has com•wcourse or ins

Chata-wi. Amerinn Kttf Cnm

fUdCroai

This ctrtifla thaAlfred P. Histr

ADUII CPBh»oomicount of ins«Chemi<j ftftSkte HcnntChesaOct.

Due

Anwrfc**lUdCroai

This cmifla tfiaDADULT CPX

couneofiruwutjc vt MUByw-MM _w

^ Chenifca feyte Mgat

Oct. II. 199Date

ChatrmM. Amn-nn fed

Cm*

crmfia thaPhilip A* LawhoneomiSjhe ADULT CP*

«te uSBltChesapeake* Va.

Oefi- 17. 1988Date couAt oMnp(ete4

O&vl-VM.ChUrmM. AmefteM Rrd Cmm I

• - V)ft Rl* 00 658

Page 201: for each sample and each handling of the sample is … ICAP/AA Laboratory for the analysis of metals o Tech Laboratory containing automated instrumentation, for example, Technicon

. f*OTf! Ihrtntn* in Cirdlopulmonirr Heswwtoihm fcnti

N«n,-fcb»B_. 3 wmi,viRcmM! ' ***'—"""""——"""—*"Chapter MepmentatnrInsinicior

Holder'i l-siutm^——————— " a— ~ l •

Holder'i

Chapter RrpreKnuilve _ /.

Cen

NOTEi IWnfnf In Cirrflopulmbnary RefuKlai.on (CPRtto nlld for one fnr from the mine completion due

NOTE: Trtining hi Cardiopulmonirr Resufcfuiion (CPR)to «JW for one year ftom the coune

Name «f Chtpter

Oupw RcpraencnK*ftmrvcior

Holder) Slfnnure

Page 202: for each sample and each handling of the sample is … ICAP/AA Laboratory for the analysis of metals o Tech Laboratory containing automated instrumentation, for example, Technicon

REFRESHER TRAXHXHG

Tha following hav* attended the •UK/a' *xa£r«shas training claaa for I hy. 3fi rvim. (length of

tine) on _F/k 2.

PRIOT HAKB • SICHATPRB

S. Soil2)

61

7)

9)

10)

131.

14).

15).

16)

19).

20).

21)

IHSTROCTOR(S)t

&&-*k

Page 203: for each sample and each handling of the sample is … ICAP/AA Laboratory for the analysis of metals o Tech Laboratory containing automated instrumentation, for example, Technicon

3) .I *

10).

11).

12).

13)

15

18 )

20).

21).

TRA1HIHG"N

f RIOT HAKR————— - . SICHATtM

-Z M1,/ / V. .?/ -t ,9)___ • ....,__.. .,, ,. ...,.._ ... '• '

lirSTOOCTOR(S)| -n ^

AR4006.6I

Page 204: for each sample and each handling of the sample is … ICAP/AA Laboratory for the analysis of metals o Tech Laboratory containing automated instrumentation, for example, Technicon

&XRK8BE1 TR&XIXB8

Tha following hav« attended than ol^tSpirV 1

refresher training class for 8 hAxv^ (length of____ _tiaa) on JtM. .g

PRIKT HAKK SICHATPRB

_J JU£

6)

7)

8)

9)

10)

11)

12)

13)

14)

13)

16)

17)

18)

19)

/ /iiu

^ n >*. .20) •

«% • *

IN3TROCTOR(S)l

s: "ScM.it ; 7

Page 205: for each sample and each handling of the sample is … ICAP/AA Laboratory for the analysis of metals o Tech Laboratory containing automated instrumentation, for example, Technicon

Chemical Waste Management, Inc.Technical Services DivisionPO. Box 96Sealston. Virginia 22547703/775-9000

PROCEDURES FOR SENDING SAMPLESTO DISPOSAL FACILITIES

i ., j-.. ."*DATE! //-A>- €*1_____• LOCATION: ________________

Training on the proper procedures for sending samples to dis-posal facilities. Training included packing of samples forshipment, proper labeling of the packages, and the proper ship-ping company to use. !

ATTENDED BYi

Printed Name Signature

TRAINER - S SIGNATURE 1

ARl(00663

Page 206: for each sample and each handling of the sample is … ICAP/AA Laboratory for the analysis of metals o Tech Laboratory containing automated instrumentation, for example, Technicon

Chemical Waste Management, Inc.Technical Services DivisionPQ 8ox96Seateton, Virginia 22547703/775-9000

SITE SAFETY RULES

DATE: //-.LX-6 ' LOCATIONST

ATTENDED BY:» *

Printed Name

r Vu^D L At*s\AAs\i [ /^^

• ~ - -

».

— . - --••' - •" ". .._..-. . - -

* ....— •- - -ji "

..... . .... • - ----- - • -•. .,.. ... ... .,— • -•- - - - '

• - — - -•- -

Signature

ffi&j _ JU,/ ' . C-"

-.

--- •/* - "'".'V'/-— ••• \^& : & oTRAINER'S SIGNATURE « iVWWL* « r* • < +*fif*)fUJL-Ofih f/Kt>DESCRIPTION OF TRAINING l ' 0

^ T* ^

flRl»0066i»

Page 207: for each sample and each handling of the sample is … ICAP/AA Laboratory for the analysis of metals o Tech Laboratory containing automated instrumentation, for example, Technicon

Chemical Waste Management, Inc.Technical Services DivisionPO.Box96

U S e a l s l o n . Virginia 22547 . ;703/775-9000

BASIC PERSONAL PROTECTIVE EQUIPMENT

DATE! -/A. 3?-/1) . LOCATION:

Training includes donning and removal of basic personal pro-tective equipment. \, -

^ f L, J . J MB.!. •«•

ATTENDED BY:

Printed Name Signature

TRAINER'S SIGNATURESy '

S>^^A?ittOrV

ARi*006653C " "

Page 208: for each sample and each handling of the sample is … ICAP/AA Laboratory for the analysis of metals o Tech Laboratory containing automated instrumentation, for example, Technicon

TECHNICAL SERVICES DIVISIONSAFETY MEETING/7RAININB

DATEiINSXRUCIORi " __J fl flK ^ A * ^ ™ ^ **™h* ^ ^ ^ * ^ .I" V*ftSUBJECT: fcraL ViLAd fe7HOURSt / —^

8.

9.

10.11.

12.

13.

lA.

16.

17.

18.

19.

20.

21.

i. £L2. w" • __

3« />\flf s <fr4.5.

..,-•,:.•••.•,-.- flR«. 00666CC-C -Jl^-i.--

Page 209: for each sample and each handling of the sample is … ICAP/AA Laboratory for the analysis of metals o Tech Laboratory containing automated instrumentation, for example, Technicon

PRESENT* 1.

2.

3.

4.

5.6.7.8.

9.

11.12.

_,. 13.

17.

18.,

20.

TECHNICAL SERVICES DIVISIONSAFETY MEETING/TOAINING

DATE:INSTRUCTOR: ~ __________SUBJECT: "p U.: rn,>9. k' HtvHTZTHOURS: . V<*.*i}fl .!s

•"'*-"• '"

Page 210: for each sample and each handling of the sample is … ICAP/AA Laboratory for the analysis of metals o Tech Laboratory containing automated instrumentation, for example, Technicon

Chemical Waste Management, Inc.Technical Services DivisionPO. Box 96Sealston. Virginia 22547703/775-9000

HEALTH ft ENVIRONMENTAL AWARENESS

DATE: /^-*^Q ' LOCATION:

ATTENDED BY:

Printed Name

^k 7/*/7 / -,J^^ r «-—

Signature

/£$ 4 (;,V Wvvf^^ ' ^^ J ' ^^

._..... . --

. ;

.. . - --•• ••-

- -

TRAINER'S SIGNATURE t L /LS . • y >7.u " - •*•

DESCRIPTION OF TRAINING:

wv

Page 211: for each sample and each handling of the sample is … ICAP/AA Laboratory for the analysis of metals o Tech Laboratory containing automated instrumentation, for example, Technicon

Chemical Waste Management, Inc.Technical Services DivisionPO. Box 96Sealslon. Virginia 22547703/775*9000

SAFETY RULES

DATE. /M-7. gC ) LOCAT10Hj

ATTENDED BY:

Printed Name Signature

TRAINER'S SIGNATURElvO»-DESCRIPTION OF TRAINING!

Page 212: for each sample and each handling of the sample is … ICAP/AA Laboratory for the analysis of metals o Tech Laboratory containing automated instrumentation, for example, Technicon

Chemical Waste Management, Inc.Technical Services DivisionPC Box 96Seatelon. Virginia 22547 v J703/775-9000 -

FIRE EXTINGUISHER & LEVELS OF RESPIRATOR PROTECTIONAND EMERGENCY SPILL RESPONSE

DATE: /X."/~0 '_____ LOCATION:

ATTENDED BY:

Printed Name

u******

Signature

TRAINER'S SIGNATURE: , -A jE... yi-afl ^ f .rt

ARl.00670

Page 213: for each sample and each handling of the sample is … ICAP/AA Laboratory for the analysis of metals o Tech Laboratory containing automated instrumentation, for example, Technicon

Chemical Waste Management,' Inc.Technical Services DivisionPO.Box96Sealston. Virginia 22547

i j 703/775-9000

.BASIC PERSONAL PROTECTIVE EQUIPMENT

DATE: /A-A n 7- T .LOCATION:

Training includes donning and removal of basic personal pro-tective equipment# -,_ %—-r-^ -" ' . . . ' , • - - -. •-'- " '

ATTENDED BY;

Printed Name Signature

TRAINER'S SIGNATURE:

Page 214: for each sample and each handling of the sample is … ICAP/AA Laboratory for the analysis of metals o Tech Laboratory containing automated instrumentation, for example, Technicon

Chemical Waste Management, Inc.Technical Services DivisionPO.Box96Sealston. Virginia 22547 v J703/775-9000 -

HAZARDOUS HASTE CLASSIFICATION

DATE: .-- LOCATION:

Training and discussion of hazardous waste classification.Subjects include DOT hazard classes and proper shipping names ,EPA waste classifications (F,K,U, and P lists), proper ship-ping names for PCB materials (state "B" codes), and the useof reference materials including the applicable parts of 40and 49 CFR and the Condensed Chemical Dictionary. The rele-vance of the EPA and DOT regulations to labpacking and mani-festing is also included*

ATTENDED BY:

Printed Namo Signature

TRAINER'S SIGNATURE t

Page 215: for each sample and each handling of the sample is … ICAP/AA Laboratory for the analysis of metals o Tech Laboratory containing automated instrumentation, for example, Technicon

Chemical Waste Management Inc.Technical Services Division

2254703/775-9000

PROCEDURES FOR SENDING SAMPLESTO DISPOSAL FACILITIES

DATE: /3.- /"W f^tv: LOCATION:

Training on the proper procedures for sending samples to dis-posal facilities* Training included packing of samples forshipment, proper labeling of the packages, and the proper shiping company to use. ?f . i

• * - ••• F r"" "''!.'"'• ' •' — "• - ' . . - i • • "! '- : " ',_-' """ ~"!K t '•'"• "' ' "' ' - ' " ' " . ' '

ATTENDED BY: ,

_ • ' . . ? . . . f 'Printed Name

Ok -1 S\ I L - •-— -•••——— •F — ' > f «* fc—»'<C« C *X >) '' * ' I1

. ' ' ' . ' - • f- '•• 1.,

„„,_„,} ,,„*

. -, -w'- • ,

" .. ...-.J,-• " ' " " " • _ J.

,_,_,-.»i~.V«i'"

"""" - ... •._-, J.. -.. .j - u.rl!!-

,. ... — ••- Ij

_,- — — "'

- ^ JU ~l ••

Signature.

&IL&L0 C5-Cl.u,l/ , . , . *

" - " " " "„ ..- ... - - - - - - -"

_ . .„ .... ..--» - - -

.r . ' - ' -

..... • - - . . - • - - - •

,, „— - . • -- " - ' • ' • - "

Jt ..,.. . - - • - • • - - '• •-„+,..«.««•- ' •» -- - • • • " - • '

••'• •---"• . - - - •.,„„*. -- •• - -

„.,„.„ . . ,. .— - •-- - •

.,„"..,- - - - -* - • • " " " '

„.,*=,-—• • ' " " " . '

TRAINER'S SIGNATURE: ii'/L/-/U 1 **>&X)JiLy d*j*\ r'oll " ' ' -

,-;: ARl. 00673

Page 216: for each sample and each handling of the sample is … ICAP/AA Laboratory for the analysis of metals o Tech Laboratory containing automated instrumentation, for example, Technicon

Chemical Waste Management, Inc.Technical Services DivisionPO. Box 96Sealston. Virginia 22547 V J703/775-9000

DATE: 12 ~/~

LABPACX GUIDELINES

LOCATION:

Training and discussion to provide a brief overview of themethods and regulations which apply to labpacking. Subjectsinclude Model City and Email* landfill packing requirements,TWI incineration packing requirements, marking and labelingof containers, and handling of reactives. Some specific con-siderations for discussion include picric acid, short-chainedethers and other potentially explosive compounds, aerosols,and gas cylinders, biologicals, radioactives , and dioxin con-taining compounds. •

ATTENDED BY:

Printed Name Signature/\ /

TRAINER'S SIGNATURE«

flRl*0067l*


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