Frit Development for Sludge Batch 3/67531/metadc737483/m2/1/high_re… · CPC Chemical Process Cell...

Immobilization Technology Section WSRC-TR-2002-00491Savannah River Technology Center Rev. 0Westinghouse Savannah River Company

October 15, 2002

FRIT DEVELOPMENT FOR SLUDGE BATCH 3

D.K. PeelerT.B. Edwards

Westinghouse Savannah River CompanySavannah River Technology CenterAiken, South Carolina

Westinghouse Savannah River Company Savannah River Technology Center Aiken, SC 29808

PREPARED FOR THE U.S. DEPARTMENT OF ENERGY UNDER CONTRACT NO. DE-AC09-96SR18500

This document was prepared in conjunction with work accomplished under Contract No.DE-AC09-96SR18500 with the U. S. Department of Energy.

DISCLAIMER

This report was prepared as an account of work sponsored by an agency of the United StatesGovernment. Neither the United States Government nor any agency thereof, nor any of theiremployees, makes any warranty, express or implied, or assumes any legal liability or responsibilityfor the accuracy, completeness, or usefulness of any information, apparatus, product or processdisclosed, or represents that its use would not infringe privately owned rights. Reference herein toany specific commercial product, process or service by trade name, trademark, manufacturer, orotherwise does not necessarily constitute or imply its endorsement, recommendation, or favoring bythe United States Government or any agency thereof. The views and opinions of authors expressedherein do not necessarily state or reflect those of the United States Government or any agencythereof.

This report has been reproduced directly from the best available copy.

Available for sale to the public, in paper, from: U.S. Department of Commerce, National TechnicalInformation Service, 5285 Port Royal Road, Springfield, VA 22161,phone: (800) 553-6847,fax: (703) 605-6900email: [email protected] ordering: http://www.ntis.gov/help/index.asp

Available electronically at http://www.osti.gov/bridgeAvailable for a processing fee to U.S. Department of Energy and its contractors, in paper, from: U.S.Department of Energy, Office of Scientific and Technical Information, P.O. Box 62, Oak Ridge, TN37831-0062,phone: (865)576-8401,fax: (865)576-5728email: [email protected]

http://www.ntis.gov/help/index.asp

http://www.osti.gov/bridge

mailto:[email protected]

mailto:[email protected]


iii

FRIT DEVELOPMENT FOR SLUDGE BATCH 3

D.K. PeelerT.B. Edwards

Westinghouse Savannah River CompanySavannah River Technology CenterAiken, South Carolina

This report was prepared by Westinghouse Savannah River Company (WSRC) for the United StatesDepartment of Energy under Contract No. DE-AC09-96SR18500 and is an account of work performedunder that contract.


iv


v

Executive Summary

Several key criteria or aspects will provide the technical basis for selecting a frit for SB3. Theseinclude:

• Maximizing the projected Product Composition Control System (PCCS) operationalwindow size over the anticipated SB3 composition region

• Providing a frit that is robust or insensitive to anticipated sludge composition variation

• Improving or maintaining high waste loadings (WLs)

• Improving or maintaining high melt rates

• Providing a “frittable” additive or frit composition

Given the five key criteria can be competing, the basis for not only developing but ultimatelyselecting a frit for SB3 is complex. The selection process should not be made based on a singlecriterion but a collection of criteria that provide insight into the economics of processing SB3. Abalanced approach should be utilized in both the development and selection.

A unique, but technically sound methodology was developed and implemented for this study toguide frit development activities. The methodology utilized was a sequential, iterative processcapable of discerning the effects of frit composition on the projected PCCS operational windowsand robustness to sludge variation. Comparisons among the frits were conducted using objectivemetrics that were developed to aid in this decision making process.

The model-based assessments indicate that judicious selection of the frit can yield processableand durable products at attractive waste loadings for all washing scenarios. The results providesupport for the concept of developing specific frits for specific sludges to optimize PCCSoperational windows and waste throughput. Given this, an aggressive washing strategy may notbe required to assure processability or product quality as long as alternative frits are considered(assuming there are no other glass- or process-related restrictions such as anion solubility, H2

generation, redox control, or rheological control issues). Again, the assessments are based solelyon PCCS model predictions and do not include assessments of melt rate or frittability that are partof the integrated testing methodology. The integrated strategy should lower the risk ofintroducing a feed into DWPF that although on paper is very attractive (in terms of waste loading)results in a very difficult feed to process (in terms of melt rate). In fact, this strategy shouldprovide the basis for developing a decision matrix in which optimum waste throughput could betargeted.


vi

This page intentionally left blank.


vii

Acronyms

ASTM American Society for Testing and Materials

∆Gp preliminary glass dissolution estimator based on free energy of hydration

(in kcal/mol)

CPC Chemical Process Cell

DOE U.S. Department of Energy

DWPF Defense Waste Processing Facility

EV extreme vertice

HLW high-level waste

HLW PE High Level Waste Process Engineering

MAR Measurement Acceptability Region

MST monosodium titanate

NL[B] normalized boron release

PAR Property Acceptability Region

PCCS Product Composition Control System

PCT Product Consistency Test

PHA precipitate hydrolysis aqueous

REDOX reduction/oxidation

SB sludge batch

SME Slurry Mix Evaporator

SRS Savannah River Site

SRTC Savannah River Technology Center

TL liquidus temperature

THERMO Thermodynamic Hydration Energy Reaction Model

TTR technical task request


viii

η1150°C melt viscosity at 1150°C

WAPS Waste Acceptance Product Specifications

WL waste loading

WQR Waste Qualification Report

WSRC Westinghouse Savannah River Company


ix

Contents

Executive Summary .........................................................................................................................v

1.0 Introduction ...............................................................................................................................1

2.0 Objective ...................................................................................................................................5

3.0 The Strategy or Approach Supporting the Paper Study .............................................................7

5.0 Basis for SB3 Compositional Scenarios..................................................................................15

5.1 SB3 Compositions for Nominal Stage Assessments.........................................................15

5.2 Initial Projections of SB3 Composition as a Function of Washing...................................18

5.3 Accounting for Anticipated Sludge Variation...................................................................19

5.4 SB3 Composition as a Function of Decant .......................................................................22

6.0 Assessment of Linear Washing Scenarios (Phase 1): Nominal and Variation Stages ............25

6.1 Nominal Stage Assessment ...............................................................................................25

6.1.1 0% Washed Case..................................................................................................27

6.1.2 25% Washed Case................................................................................................30

6.1.3 50% Washed Case................................................................................................31

6.1.4 75% Washed Case................................................................................................32

6.1.5 100% Washed Case..............................................................................................32

6.2 Variation Stage Assessment (Phase 1): Linear Washing Scenarios..................................33

6.2.1 0% Washing Case ................................................................................................35

6.2.2 25% Washed Case................................................................................................36

6.2.3 50% Washed Case................................................................................................37

6.2.4 75% Washed Case................................................................................................37

6.2.5 100% Washed Case..............................................................................................38

7.0 Assessment of Decant Information (Phase 2): Nominal and Variation Stages ......................39

7.1 Nominal Stage Assessment: Decant Information (Phase 2)..............................................41

7.1.1 Decant #5 .............................................................................................................44

7.1.2 Decant #9 .............................................................................................................46

7.2 Variation Stage Assessment: Decant Information (Phase 2).............................................47

7.2.1 Decant #7 EV Assessment ...................................................................................52

7.2.2 Decant #12 EV Assessment .................................................................................54

7.2.3 Phase 2 Variation Stage: Decant #5 .....................................................................57

7.2.4 Phase 2 Variation Stage: Decant #9 .....................................................................59

8.0 MAR vs. PAR: Impact on Projected Waste Loading Intervals ...............................................61

9.0 Summary .................................................................................................................................65


x

10.0 Path Forward .........................................................................................................................69

10.1 Melt Rate...........................................................................................................................69

10.2 Frittability..........................................................................................................................72

11.0 References .............................................................................................................................73

Appendix A ....................................................................................................................................77

Appendix B ....................................................................................................................................81

Appendix C ....................................................................................................................................87

Appendix D ....................................................................................................................................89

Appendix E...................................................................................................................................161

Appendix F...................................................................................................................................173

Appendix G ..................................................................................................................................193

Appendix H ..................................................................................................................................213

Appendix I....................................................................................................................................233

Appendix J ...................................................................................................................................259


xi

List of Figures

Figure 3-1. Evaluation Strategy Utilized in the Nominal Stage Assessment of SB3 SludgeCompositions. ...........................................................................................................................7

Figure 3-2. Evaluation Strategy Utilized in the Variation Stage Assessment of SB3 SludgeCompositions. ...........................................................................................................................9


xii



xiii

List of Tables

Table 4-1. PAR Limits for Various Properties..............................................................................14

Table 5-1. Nominal SB3 Composition (in wt%, calcine oxide basis)...........................................17

Table 5-2. Estimated Na2C2O4 and Na2O Masses as a Function of Washing ...............................18

Table 5-3. Nominal Compositions of SB3 as a Function of Washing Scenario and Minimum andMaximum Values Assuming a ±10% Variation (mass fractions)...........................................21

Table 5-4. Projected SB3 Compositions as a Function of Decant (oxide basis, wt%)..................23

Table 6-1. Nominal Compositions of Candidate Frits (in wt% on an oxide basis).......................26

Table 6-2. Summary of Nominal Stage Assessments for Candidate SB3 Frits (waste loadingranges are in wt% on a calcined, oxide basis).........................................................................26

Table 6-3. Nominal Stage Assessment for the 0% Washed Nominal Sludge with Frit 202 over theWaste Loading Range of 25 – 60%. .......................................................................................28

Table 6-4. Summary of the Nominal and Variation Stage Assessments for Candidate SB3 Fritsand the Linear Washing Scenarios..........................................................................................34

Table 7-1. Summary of Frit Compositions (in wt% oxides) Used in the Nominal and VariationStages of the Decant (or Phase 2) Assessments......................................................................40

Table 7-2. Summary of Projected Operational Windows for the Phase 2 Nominal StageAssessment of the Decant Compositions................................................................................42

Table 7-3. Nominal Stage Assessment for Decant #5 and Frit 202 over the Waste Loading Rangeof 25 – 60%.............................................................................................................................43

Table 7-4. Minimum and Maximum Values for Decants #7 and #12 Used to Define EVs (wt%oxides).....................................................................................................................................48

Table 7-5. Variation Stage Results for Decant #7 with Frit 202...................................................50

Table 7-6. Summary of the Frit 202 Decant #7 Variation Stage Assessment ...............................51

Table 7-7. Summary of Frit Compositions (in wt% oxides) Used in the Phase 2 Nominal andVariation Stage Decant #7 Assessment. .................................................................................53

Table 7-8. Summary of Frit Compositions (in wt% oxides) Used in the Phase 2 Nominal andVariation Stage Decant #12 Assessment ................................................................................56

Table 7-9. Summary of Frit Compositions (in wt% oxides) Used in the Phase 2 Nominal andVariation Stage Decant #5 Assessment ..................................................................................58

Table 7-10. Summary of Frit Compositions (in wt% oxides) Used in the Phase 2 Nominal andVariation Stage Decant #9 Assessment ..................................................................................60

Table 8-1. Projected Waste Loading Ranges for Various Frit/Decant Combinations Using boththe PAR and MAR Acceptance Criteria .................................................................................62


xiv



1

1.0 Introduction

Approximately 130M L of sludge/supernate high-level radioactive waste (HLW) is currentlystored in underground carbon steel tanks at the Savannah River Site (SRS) in Aiken, SouthCarolina. The Defense Waste Processing Facility (DWPF) began immobilizing these wastes inborosilicate glass in 1996. Currently, the radioactive glass is being produced as a “sludge-only”composition by combining washed high-level sludge with glass frit and melting. The glass ispoured into stainless steel canisters that will eventually be disposed of in a permanent geologicalrepository.

Currently, DWPF is processing Sludge Batch 2 (SB2) and is planning to start processing SludgeBatch 3 (SB3) in the spring of 2004 (WSRC 2001).1 A sludge batch is defined as a single tank ofsludge slurry or a combination of sludge slurries from different tanks that has or will be qualifiedfor eventual transfer to DWPF. Sludge Batch 3 will be primarily Tank 7 sludge mixed with theheel of Sludge Batch1B (SB1B), contributions from Tanks 18 and 19, and an H-Canyon slurrycontaining precipitated Pu with Gd (Jilani 2002). The sludge from Tank 7 is expected to containseveral components that are considered atypical of DWPF sludge to date including higher levelsof noble metals than previously processed sludge batches (Peeler et al. 2002a). Other atypicalcomponents that may be present in this sludge batch include sand, coal, Am/Cm precipitate (Patel2002), sodium oxalate, and zeolite (Jantzen et al. 2002a). Based on the process history for Tank7, it is estimated that significant quantities of sand/coal (~7723 kg) and sodium oxalate (~300,000kg) have been added to this tank (Goslen 1984; Fowler 1980).

The quantities of sand, coal, and sodium oxalate may impact several processing parameters at theDWPF. High Level Waste Process Engineering (HLW PE) has issued a Task Technical Request(TTR) requesting the Savannah River Technology Center (SRTC) to address these processingimpacts (Rios-Armstrong 2002a). Fellinger (2002) provided a list of the various tasks that arecurrently being addressed prior to DWPF’s accepting SB3. Studies have been and are beingperformed by SRTC to assess the effects of sand, coal, sodium oxalate, the Pu/Gd stream, and thehigher levels of noble metals on various SB3 issues [Herman et al. (2002a); Peeler et al. (2002a),Bronikowski et al. (2002), Jantzen (2002b)].

One of the tasks identified by Fellinger (2002) involved an evaluation of potential frits for SB3.Rios-Armstrong (2002b) issued a more specific TTR to address the frit development activity aswell as a subsequent variability study. The focus of this report is solely on the frit developmentactivity, as the results of the variability study will be documented in a separate report.


• Maximizing the Product Composition Control System (PCCS) projected operationalwindow size over the anticipated SB3 composition region



1 Although the current HLW System Plan (WSRC 2001) projects the initiation of SB3 processing in the

spring of 2004, plans to expedite processing of SB3 are currently being assessed. If proven feasible,processing of SB3 could begin as soon as the spring/summer of 2003.


2


• Providing a “frittable” additive or frit composition2

The issues listed above will be used to guide the SB3 frit development task in an effort toimprove current DWPF baseline operations in terms of ease of processing, waste loading3 and/ormelt rate. The ability to maximize the size of the DWPF PCCS operational window providesflexibility in targeting waste loadings to meet processing goals. This is strictly an ease-of-processing goal targeted to provide as large of a compositional operating window and as muchflexibility as possible.

Another key criterion defining a viable frit for SB3 is the ability of the frit to be tolerant ofcompositional variation in the incoming waste stream. That is, providing a frit that is robust orinsensitive to relatively large variations in sludge composition (yields a relatively largeprocessing window when accounting for composition variation) is a major advantage. A “robust”frit will reduce uncertainties or questions associated with how the frit will respond to SB3 oncethe qualification sample is obtained and compared to what is being used as the nominal ortargeted composition in current testing. That is, a viable frit should not only be able to processthe nominal SB3 composition being used but should also be able to process (i.e., be robust to)realistic variations of that composition while still maintaining adequate processing and productcharacteristics. The degree of tolerance can be measured by the ability to produce acceptableglasses as one transitions from the nominal sludge case to compositions representing larger andlarger variation about the nominal.

Although the issue of waste loading is essentially built into the criterion of providing largeoperational windows, a short discussion of this important topic is still warranted. One method ofsupporting site and U.S. Department of Energy (DOE) goals of accelerated cleanup is to improvewaste loading. For DWPF, a new liquidus temperature (TL) model has been developed and ispending implementation. This model has been shown to yield higher waste loadings for projectedsludge batches (Brown et al. 2001). The waste loading projections provided by Brown et al.(2001) were based on Frit 165, Frit 200, and Frit 320. Frit 165 was developed to be a “generic”sludge-only frit (Soper et al. 1983), while Frit 200 was developed to be a “generic” coupledoperations (sludge-only plus high alkali from precipitate hydrolysis aqueous (PHA)) (Jantzen1988) frit. Frit 320 was developed specifically to improve melt rate for SB2 (Peeler et al. 2001a).Although these frits may be viable in terms of processing SB3, none were specifically developedfor this sludge batch and, hence, may not be “optimal” for the projected SB3 composition.Therefore, if the strategy is embraced of developing a frit for a specific sludge batch in an effortto improve waste loadings (and potentially melt rate), one may be able to take advantage of thespecific sludge components and adjust the frit composition accordingly in the manner that Frit200 was developed to accommodate PHA. This strategy may allow for the development of fritsthat provide not only a large PCCS processing window but simultaneously provide relatively highwaste loadings. Therefore, in the assessments that follow, not only is the size of the PCCSprojected processing window (the interval of viable waste loadings) provided for each frit ofinterest, but the ability of the frit to shift the PCCS operational window to higher waste loading isalso assessed. For example, two unique frits may both yield a 10% waste loading range with onefrit providing the acceptable window over a 31 – 40 % waste loading interval, while the otherallows processing over a 41- 50% waste loading interval. Depending upon other processing

2 The term of “frittable” refers to the ability to produce a prefabricated frit (glass) from the proposed glass additives.3 Waste loading (WL) in this report is simply calculated as the HLW oxide fraction of the final glass.


3

characteristics (e.g., melt rate), the higher waste loading interval may be more beneficial in termsof maximizing waste throughput and meeting the goals of accelerated clean-up.

As previously mentioned, although targeting higher waste loadings is a primary objective, otherprocessing constraints are also important. Another critical constraint being assessed in this task ismelt rate. Since DWPF is concerned with the amount of waste throughput to meet acceleratedmission plans, providing a frit that allows relatively high waste loadings but does not melt rapidlymay not be acceptable. On the other hand, selecting a frit that does not yield a comparativelyhigh waste loading but provides a higher melt rate may be beneficial in terms of wastethroughput. The balance between melt rate and waste loading must be carefully considered. Theconcept of this balance was recently evaluated in the assessment of the impact of higher wasteloading on melt rate for Frit 320 combined with SB2 (Lorier and McGrier 2002). However, thenotion that reduced melt rates at higher waste loading is unacceptable should be tempered with anevaluation of the total waste throughput. More specifically, during an assessment of the impactsof waste loading on melt rate, decisions on frit selection or targeted waste loading should not bemade solely on the relative melt rate. The decision needs to consider the total sludge throughputper unit time. Currently, no models exist that can be used a priori to gain insight into the meltrate of various systems. Therefore, this assessment will be made solely by using a testingmethodology that was shown to be effective for SB2 (Stone and Josephs 2001).

The last criterion listed above is the desire to have a “frittable” frit (i.e., the targeted fritcomposition will produce a glass that can be manufactured by a vendor) which stems from wasteacceptance issues. Use of a prefabricated frit instead of batch chemicals stems primarily fromwaste acceptance issues. Currently, DWPF uses a frit that is ultimately blended with the sludge.Samples of this blend are taken from the Slurry Mix Evaporator (SME), the compositionsdetermined, and properties are predicted from the measured composition to assure that they arewithin the processing window. Given the feed is acceptable in terms of various propertypredictions, the feed is transferred to the melter, converted to glass, and poured into canisters.This feed-forward process control strategy has been very effective in terms of assuringprocessability and product quality. Hence, frittability is an important criterion.

Given the five key criteria can be competing, the basis for not only developing but ultimatelyselecting a frit for SB3 is complex. The selection process should not be made based on a singlecriterion but on a collection of criteria that provide insight into the ease of processing SB3 whilestill making an acceptable glass. A balanced approach should be utilized in both the developmentand selection. Another factor that could play a significant role in the selection of a frit is theavailability of an existing frit versus any procurement and manufacturing costs for an alternativefrit given frit fabrication requires a significant lead time.

The focus of this report is on frit development activities conducted solely on the basis ofpredictions generated by DWPF’s PCCS glass property-composition models. More will be saidabout these models in the following sections, but for now it is enough to know that modelpredictions, and model predictions alone, were used to guide the development of the candidatefrits discussed below and to select, from these candidates, those frits that were judged worthy ofadditional consideration. This was a sequential, iterative process that may be summarized asfollows: candidate frits were identified for and compared across nominal sludge compositions(i.e., where each such composition is considered as a “best guess” view of SB3 sludge for apotential washing scenario). Two different sets of sludge compositions (an initial and a final)were used to represent potential nominal SB3 compositions. The initial set of compositions wasavailable early in the study and served as the basis for much of the preliminary development


4

efforts. The preliminary frits that were the most promising at this stage were carried over to astage of investigation that introduced variation around the nominal SB3 compositions. Thisapproach was used to provide an idea of the robustness or tolerance of a candidate frit toanticipated compositional variation (i.e., the ability of the frit to produce an acceptable productfor variations in the sludge based upon model predictions). Comparisons among the frits wereconducted using objective metrics, described below, that were developed to aid in this decisionmaking process. This two-staged (an assessment using only nominal compositions and then anassessment with variation introduced) approach was then conducted for the second (or final) setof SB3 compositions. The information resulting from these efforts will hopefully serve as part ofthe technical basis for the frit selection decision. Assessments of frittability and melt rate willcomplete this picture and these topics are to be covered in subsequent reports.

Objectives for this task are specified in Section 2.0. In Section 3.0, the strategy or approach fordeveloping and assessing new or existing frits is discussed. In Section 4.0, the propertyacceptance criteria are established that will be used to classify properties predicted from modelsas acceptable or unacceptable as projected operation windows are defined. Various SB3compositions (linear washing and decant composition projections) are summarized in Section 5.0from which assessments will be founded. Section 6.0 summarizes the Nominal and VariationStage assessments for the five linear washing scenarios. Section 7.0 provides a detaileddiscussion on the eleven decant compositions in terms of the Nominal and Variation Stageassessments. Section 8.0 provides insight into the use of various liquidus temperature acceptancecriteria and its impact on projected operational windows. Section 9.0 provides a summary ofthese assessments. Recommendations and a path forward are presented in Section 10.0.


5

2.0 Objective

The objective of this task is to provide DWPF with technical information from which a businessdecision can be made in terms of the frit selection for SB3. Several key criteria or aspects willprovide the basis for this decision:

• Maximize the PCCS projected operational window size over the anticipated SB3composition region

• Provide a frit that is robust or insensitive to anticipated sludge composition variation

• Improve or maintain high waste loadings

• Improve or maintain high melt rates

• Provide a “frittable” frit composition

The selection process should not be made based on a single criterion but rather on a collection ofcriteria that provide insight into both the economics and processability of SB3.

The focus of this report is solely on the frit development activities associated with maximizingthe projected PCCS operational windows and providing a frit that is robust to anticipated sludgevariation. Assessments of frittability and melt rate are to be covered in subsequent reports.

This work has been prepared to address technical issues discussed in Technical Task RequestHLW/DWPF/TTR-01-00027, Rev. 0 (Rios-Armstrong 2002b) and in accordance with the TaskTechnical and Quality Assurance Plan (Herman, Peeler, and Edwards 2002).


6



7

3.0 The Strategy or Approach Supporting the Paper Study

Two stages were used to assess various frit/sludge combinations: the Nominal Stage and theVariation Stage. The Nominal Stage utilized a nominal SB3 composition representing a potentialwashing scenario as outlined in Figure 3-1. In general, candidate frit compositions were assessedwith respect to their ability to provide a relatively large operational window based solely on aspecific nominal composition – no sludge variation was accounted for in this phase. Assessmentswere made using predictions from models currently implemented in DWPF over the wasteloading interval of interest (25 – 60 wt%). The property predictions assessed included those forliquidus temperature (TL), viscosity (η), durability (normalized boron release – NL[B]), andhomogeneity. Assessments were also conducted for the constraints associated with the sum ofalkali and/or Al2O3 concentrations (Edwards and Brown 1998; Peeler et al. 2000; Peeler et al.2001b; Peeler et al. 2002b; Herman et al. 2002b).4 The associated constraints for these propertieswere assessed at the Property Acceptability Region (PAR) limits (Brown and Postles 1996) –these limits are defined in the next section. Use of the PAR, instead of the more restrictiveMeasurement Acceptability Region (MAR) was thought to provide a consistent, easily computedmetric which could be used to compare, efficiently and effectively, the relatively large set ofcandidate frits. Although the PAR was used as the basis for the comparisons, an assessmentusing the MAR was performed on select frit/sludge combinations to assure that projectedoperational windows were not dramatically affected (see Section 8.0).

Figure 3-1. Evaluation Strategy Utilized in the Nominal Stage Assessment of SB3Sludge Compositions.

4 Given the projected high Na2O and Al2O3 concentrations in SB3, the potential of the projected glass compositions to

form nepheline was also assessed using a model provided by Li et al. (1997 and 1998). Although assessed, thepredictions did not limit the projected operational windows.

Select candidate

frit

Select a nominal

composition representing a washing option for

SB3

Evaluate over the sludge loading interval of 25 - 60 %

Determine the interval (if any) of sludge loading that yields acceptable glass for this

combination of frit and sludge


8

The use of a nominal SB3 composition is consistent with the approach used by Elder (2002) asinitial assessments were made using existing frits (320 and 202). It is recognized that theNominal Stage assessments do not account for anticipated compositional variation. Therefore, anincreased risk would result with respect to processability or product quality if a decision werebased solely on this assessment without accounting for compositional variation. For example,consider the case if the Tank 7-qualification sample did not “match” the nominal compositionanticipated for this tank. The obvious question would be: “For the frit selected, is there aprocessing window for this sludge?”. The intent or focus of the Variation Stage assessment wasto gain insight into the robustness of candidate frits with respect to compositional variation.

Figure 3-2 provides an overview of the Variation Stage assessment. Again, the major differencebetween the two stages is the fact that the Variation Stage builds into its assessment ananticipated variation of ±10% around the nominal composition.


9

Select candidate

frit

Generate the EVs (and centroid) of the sludge

region representing +/-10% of nominal for a washing option for SB3

Evaluate over the sludge loading interval of 25 - 60 %

Determine the interval (if any) of sludge loading that yields acceptable glass for all

EVs and centroid

Determine the percentage of the EVs and centroid that yield acceptable glass at any

sludge loading (within the interval of interest).

Determine the percentage of the EVs and centroid that yield acceptable glass over a

sludge loading interval of at least 5% (e.g., 36 to 40% sludge loading).

Compile the results of the evaluations for

comparisons among the frits and/or sludge washing scenarios

Figure 3-2. Evaluation Strategy Utilized in the Variation Stage Assessmentof SB3 Sludge Compositions.


10

The ±10% variation used to define a sludge compositional region was determined by grouping thecomponents of SB3 into two categories: major and minor oxides. The minors were consideredcollectively as an “Others” component of the sludge. For a selected, nominal SB3 composition(one representing a potential washing scenario), the concentration of each of the major oxideswas multiplied by 0.90 and 1.10 to determine an interval of possible values for its concentration.The concentrations of the minor components were summed, and this sum was multiplied by 0.90and 1.10 to determine an interval of possible values for “Others” with the relative proportions ofthe minors within the “Others” being determined by their nominal concentrations. (See Section5.0 for details.) A mixture of the major components and the “Others” (i.e., a composition wherethe sum of these concentrations adds to 1) with each component’s concentration being within itsinterval of possible values is a feasible composition of the sludge region providing thisrepresentation of SB3. Obviously, there are an infinite number of such feasible compositions insuch a sludge region.

Statistical mixture experimental design methods were used to obtain an initial and manageable setof such feasible compositions for each sludge region. These methods include algorithms that canbe used to determine the extreme vertices (the bounding compositions) of a sludge region, such asthat defined in the preceding paragraph. These algorithms are available in many statisticalsoftware packages. One such package in JMP Version 4.0.5 [SAS 2000] was used to generate theextreme vertices (EVs) for mixture regions of interest for this study.5 An additional composition,the centroid, was computed for each set of EVs generated during this study. The centroid of asludge region is determined by averaging all of the EVs for that sludge region and thiscomposition was included along with the EVs in the assessments described below.

Once the EVs were determined for the sludge region developed around each nominal SB3composition being considered, assessments were made using models currently implemented inDWPF over the waste loading interval of interest (25 – 60 wt%) – see Section 4.0 for a moredetailed discussion of the models and PAR limits. To obtain insight into the robustness ofcandidate frits to this sludge variation, three metrics were developed (as shown in Figure 3-2).These three metrics also provide a way to make meaningful comparisons among the candidatefrits for each sludge compositional region of interest. The first metric was simply the wasteloading interval over which all of the EVs and the centroid SB3 sludge compositions weredeemed acceptable based on the established acceptance criteria. The larger the projectedoperational window for this metric, the more robust the frit is to anticipated compositionalvariation. A 0% result for this metric indicates that there is no waste loading interval over whichall of the EVs and centroid are predicted to be processable.

The second metric defines the percentage of the EVs and centroid that yield an acceptable glass atsome waste loading of interest. That is, this metric provides the percentage of EVs and thecentroid that could be processed at some waste loading over the 25 – 60% interval. A highpercentage for this metric provides a fair and standard comparison between frits and is anindicator to the robustness or insensitivity of the frit to composition variations in sludge. Forexample, a 100% for this metric would indicate that all of the EVs generated (accounting for the±10% variation) and the centroid could be processable at some waste loading within the interval 5 The extreme vertices (EVs) for a particular sludge view are the "corner points" of the region determined

by applying the ± 10% variation about the nominal composition for that sludge view. Thecorresponding centroid for the sludge view is simply the arithmetic average of these EVs.


11

from 25 to 60%. A 50% result on this metric would indicate that only 50% of the EVs wouldyield acceptable glass at some waste loading between 25 – 60%.

The third metric builds upon the second and serves as a measure of the percentage of the EVs andcentroid that yield an acceptable glass over a minimum waste loading range of 5% within the 25 –60% window being evaluated. Again, the higher percentage calculated for this metric indicatesthat the specific frit composition is relatively robust to potential sludge composition variations.More specifically, a 100% for this metric would indicate that all of the EVs and centroid wouldbe processable over a (minimum) 5% waste loading interval. In the assessments that follow, ifthis metric yields an indicator of 100%, efforts will be made to identify the minimum wasteloading interval over which the EVs and centroid would be processable.

Additional metrics could be developed but the authors feel that the three being utilized provide anadequate indication of the projected operational windows and robustness of each candidate frit forthe waste streams of interest. These metrics should not be used as the sole basis for the fritselection process, but should be factored into the decision making process along with assessmentsof frittability and melt rate. The authors feel that the strategy being utilized for the developmentof the SB3 frit is not only technically defensible, but that it also provides a methodology thatcould be used for similar frit development activities in the future.

As previously mentioned, the assessments and comparisons documented here are based solely onmodel predictions; no experimental work was performed in support of these assessments. Theassessments are also a function of the underlying assumptions made with respect to the impacts ofsludge washing on the ultimate composition of SB3. It should also be noted that an additionalunderlying assumption is being made with respect to the projected operational windows by theuse of centroid and EV compositions. The assumption is that the property predictions for asludge region of interest are bounded by the predictions generated from the EVs and thatcompositions lying between the EVs (i.e., such as the centroid) would yield property predictionsthat are acceptable if those from the EVs were acceptable. This assumption is valid when theproperty behavior is expected to be linear over the compositional region of interest. Thisassumption adds minimum risk to the projected operational windows with the highest concernbeing predictions of TL from the highly non-linear TL model (Brown et al. 2001).


12



13

4.0 Property Acceptability Region (PAR) LimitsUsed for Assessments

The assessments discussed in this report are based solely on property predictions generated byglass-property models. Property measurements were not performed (experimentally) as part ofthis study. DWPF uses the PCCS to determine the acceptability of each batch of SME feedbefore processing in the melter. Acceptability is determined by the PCCS by imposing severalconstraints on the SME content composition. The PCCS constraints relate process or productproperties, which take into account modeling, analytic, and measurement uncertainties. Theuncertainties are accounted for in two steps. The first is the uncertainty due to the propertymodel, which when accounted for provides the Property Acceptability Region (PAR). Thesecond, and more restrictive, is the uncertainty due to sampling and analytical (grouped under theheading of measurement). This uncertainty is accounted for, when necessary, in addition to theproperty uncertainty, and the resulting region defines the Measurement Acceptability Region(MAR). The baseline document guiding the use of these models is “SME AcceptabilityDetermination for DWPF Process Control” by Brown and Postles (1996).

The property predictions assessed in this study included durability (Product Consistency Test[PCT] [ASTM 1998] response in terms of ∆GP), viscosity at 1150°C (η1150°C), TL (new model),homogeneity, and Al2O3 and alkali concentrations. Jantzen et al. (1995) and Brown et al. (2001)provide a more detailed discussion on the development of these models. To establish or projectoperational windows for sludge/frit scenarios of interest, the predicted properties must beassessed relative to established acceptance criteria. Acceptable predicted properties for thisassessment are based on satisfying their respective PAR limit values (see Table 4-1)—not themore restrictive MAR limits. Because the PAR limit for the new TL model is compositionallydependent (Brown et al. 2001), the PAR limit was conservatively set at 1010ºC to allow for aquick assessment. In fact, Brown et al. (2001) have demonstrated that the PAR limits for the newmodel will not be this restrictive (in terms of limiting the projected compositional operatingwindow) for various glass-forming systems. Therefore, in the assessment discussions that follow,if the new TL model limits the projected operational window, one must remember the use of thisconservatively set PAR limit. More specifically, failing this constraint (as currently defined) doesnot necessarily mean that it would be an unacceptable glass given the conservative 1010ºC PARlimit.

Predictions of homogeneity were calculated and the constraint was imposed in terms of limitingprojected operational windows. More specifically, a glass that failed the homogeneity constraintat the PAR but passed all other criteria was deemed unacceptable. This decision is based on thefact that the technical basis to replace the homogeneity constraint with the Al2O3 and sum ofalkali constraints is currently being developed. Although the results from previous studies(Edwards and Brown 1998; Peeler et al. 2000; Peeler et al. 2001b; Peeler et al. 2002b) indicatethat replacing the homogeneity constraint with the Al2O3 and sum of alkali constraints does notcompromise product quality and provides more flexibility for DWPF operations, Herman et al.(2002b) are performing the final task to address this issue. In that study, the technical basis forunconditional elimination or replacement of the homogeneity constraint via application of theAl2O3 and sum or alkali constraints is being assessed over a bounding compositional region.Given the results and/or conclusions were not available at the time this assessment was initiated,continued use of the homogeneity constraint to limit the projected operational window waswarranted.


14

Table 4-1. PAR Limits for Various PropertiesProperty PAR LimitTL (new) < 1010°C

∆GP (durability) > -12.7178 kcal/mol

η1150°C (melt viscosity) 21.5–105.4 Poise

Homogeneity > 210.92Al2O3 ≥ 3.0 wt% (in glass)6

Σalkali7 < 19.3 wt% (in glass)

6 The Al2O3 and ∑alkali limits were developed by Edwards and Brown (1998) to allow the homogeneity constraint to

be relaxed from the MAR to the PAR. An alternative criterion would be a minimum Al2O3 content of 4 wt% with noconstraint on the sum of alkali over the composition region evaluated.

7 Alkalis included in this sum are Na2O, Li2O, Cs2O, and K2O.


15

5.0 Basis for SB3 Compositional Scenarios

Two primary inputs are required to assess the projected operational windows, the waste loadingintervals, and the robustness: sludge or waste stream composition(s) and frit composition(s).Given the focus of this study is to develop frit compositions for SB3, defining the nominal SB3waste stream(s) and representing its (their) variation are required inputs. For a given wastestream composition, one can select candidate frit compositions, and ultimately assess or defineglass compositional regions or operating windows based on established acceptance criteria (seeSection 4.0).

Prior to receiving information from HLW PE with respect to the projected sludge compositions asa function of washing or decants, an initial phase (Phase 1) of frit assessments was made usingprojections of SB3 sludge compositions based on an assumed washing scenario. Existing ornewly-developed candidate frits were then assessed against these initial SB3 compositionsfollowing the strategy of Section 3.0 and the criteria of Section 4.0. Once the final (moredefinitive) washing or decant information for this study was received from HLW PE, a secondassessment (Phase 2) was made for the frits that appeared to be promising from the initialprojections given that differences did exist between the initial and final compositions. The resultsfrom these two phases of study are presented in Sections 6.0 and 7.0, respectively.

5.1 SB3 Compositions for Nominal Stage Assessments

Table 5-1 summarizes the nominal SB3 sludge composition (in oxide wt%) and masses (in kg) onan oxide basis as reported by Peeler et al. (2002a). This nominal SB3 composition includes theTank 51 heel, Tank 7 sludge (including sand and the Tank 18 and Tank 19 sludge transfers), andAm/Cm and Pu/Gd additions and is based on a weighted average of the individual sludge masseseither reported or calculated. The potential zeolite contribution from Tank 19 is not included. Itwas also assumed that the individual streams were evenly distributed or uniformly blended,resulting in a “constant” feed to the melter (once frit additions are made). More specifically, thenominal SB3 sludge compositions represented by Peeler et al. (2002a) assumed that none of theindividual waste streams or sludges comprising SB3 constituted a “spike” in the compositionduring processing of a limited portion of SB3. That is, each of the individual streams is assumedto be well blended into SB3. The nominal SB3 compositions (and thus the assessments basedupon them) do not account for any variation in the blending of the waste streams comprising SB3.

The nominal SB3 composition provided in Table 5-1 does not account for the sodium oxalate(Na2C2O4) that could be present in Tank 7 as reported by Goslen (1984) and Fowler (1980). Thetotal mass of sodium oxalate added to Tank 7 was estimated to be as high as 660,000 lbs (or299,640 kgs). Studies are being performed by SRTC to assess the effects of sodium oxalate ondifferent SB3 issues [Herman et al. (2002a); Bronikowski et al. (2002), Jantzen (2002b)]. One ofthe critical issues being addressed is the degree of washing that is required to meet specificoperational constraints (e.g., H2 generation and flammability), processing constraints (e.g., redoxcontrol), or product constraints (e.g., durability). Although not accounted for by Peeler et al(2002a), it is the intent of this assessment to address a series or suite of washing options thatultimately affect the amount of sodium transferred to the melter.

It also should be noted that the nominal composition does not account for the potentialintroduction of a monosodium titanate (MST) stream. Based on the HLW System Plan (WSRC2001) it is anticipated that a limited volume of MST will be blended into SB3. However, given


16

the current uncertainties of if, when, and/or how (e.g., blended over the entire SB3 campaign orspiked into a limited portion of the SB3 campaign) that stream would be blended with SB3; itscontribution was not accounted for in the initial assessment (Phase 1). Although not accountingfor this stream does add some technical risk to the projected operational windows in the initialassessment, its impact should be minimal. The latter statement being based on the fact that thevolume of MST is anticipated to be relatively low (~1200 kg/yr8; compared to the 366,886 kg ofSB3 without the contribution of sodium oxalate). In addition, risks should be minimal for mostof the cases considered in this report given the majority of the projected operational windows areeither durability or viscosity limited (given the relatively high sodium concentration in the finalglass). In these cases, and assuming the major impact of the MST (assumed to be primarily TiO2)would be to increase TL, the upper waste loading limits should not be impacted. It would only bein cases where the upper (or lower) waste loading interval is TL limited, that the introduction ofMST would be expected to cause changes to the projected operational windows. This latterstatement assumes the single-component solubility limit for TiO2 is not exceeded at the higherwaste loadings. The impact of TiO2 on glass properties is being assessed by Herman et al.(2002b), and the SB3 variability study will also assess this potential impact.

8 Based on personal communication with Mark Drumm (7/15/02), the current material balance information indicates

that the MST plant would send approximately 18,000 L of solution at 15 wt% MST to the DWPF each year.Assuming a 0.4 g/L solution and a full time operations, this would translate into approximately 2700 lbs of MST peryear coming into DWPF.


17

Table 5-1. Nominal SB3 Composition (in wt%, calcine oxide basis)(same as Case #4 as reported by Peeler et al. 2002a)

Oxide

SB3 baseline withPu/Gd and Am/Cm

Without Na2C2O4

Ag 6.85E-04Al2O3 18.102AmO2 4.28E-03BaO 0.25CaO 3.60CdO 1.18E-05Ce2O3 0.355Cm2O3 6.47E-04Cr2O3 0.374CuO 0.198Eu2O3 4.68E-05Fe2O3 40.270Gd2O3 0.051K2O 0.431La2O3 0.206Li2O 2.94E-03MgO 0.189MnO 7.177MoO3 2.17E-04Na2O 10.629Nd2O3 0.682NiO 1.611PbO 0.302Pd 0.037Pr2O3 0.186PuO2 0.052RuO2 0.278Rh 0.078SiO2 3.343Sm2O3 0.10ThO2 0.143TiO2 1.04E-04U3O8 10.188ZnO 0.411ZrO2 0.743Total 100.00Mass

(in kg)366886.24

Note: Anions/halides not reported.


18

5.2 Initial Projections of SB3 Composition as a Function of Washing

At the time this task was initiated, uncertainties associated with the actual quantity of Na2C2O4 inTank 7 and the fraction that would ultimately be transferred to SB3 given the various washingscenarios being considered were being addressed. From a glass formulation perspective andresulting properties, the unknown quantity of Na2O resulting from the Na2C2O4 will have a majorimpact on the overall sludge composition and ultimately the frit development efforts. That is, fritformulation efforts will have to account or compensate for the varying Na2O concentrations thatcould be present in the sludge and ultimately the glass as different washing schemes areconsidered. As one transitions from a 100% washed case to a 0% (or minimal) washed case, theassumption is that the amount of Na2O in sludge will increase. It has been further assumed in thePhase 1 assessment (due to the inaccessibility of sludge washing calculations) that washing onlyreduces the amount of Na2O contributed from the oxalate source which is soluble with no impacton other components associated with SB3 (as listed in Table 5-1). The result of this assumptionis essentially a dilution effect of the nominal SB3 composition with varying amounts of Na2O asthe different washing percentages are reviewed. For example, consider a 50% washed sludgecase. The 299,640 kg of Na2C2O4 would be reduced to ~149,820 kg (50% of the projected total)ultimately yielding an additional ~34,600 kg of Na2O which would be blended with the366,886.24 kg of nominal SB3. Given this assumption, the 100% washed case ultimately yieldsthe nominal SB3 composition provided by Peeler et al. (2002a) (referred to as Case #4 in thatreport). The 0% washed case should be bounding given that in this assessment, all of the sodiumoxalate would be transferred to the melter feed when in fact, a minimal amount of washing thatwill remove some Na2O and other soluble species is expected prior to transferring SB3 to DWPF.

Table 5-2 provides a summary of the Na2C2O4 and Na2O contributions (in kg) for the variouswashing schemes used in the Phase 1 assessment. It is recognized that the assumption thatwashing does not impact other components of the sludge may be partially unfounded; however,incorporating sludge variation (see Section 5.3) around the nominal sludge(s) to develop fritsshould bound this assumption.

Table 5-2. Estimated Na2C2O4 and Na2O Masses as a Function of Washing

Washing Na2C2O4 (kgs) Na2O (kgs)0% 299,640 138,584

25% 224,730 103,93850% 149,820 69,29275% 74,910 34,646100% 0 0

Given the uncertainties associated with the degree of washing that will be required to meetprocessing constraints (including solubility limits of anions), safety issues with respect tohydrogen generation, melter flammability, and product quality issues, several washing scenariosare being considered in the Phase 1 assessment. Note that the potential impacts of coal andoxalate on reduction/oxidation (REDOX) control is not being specifically addressed as part ofthis study – see Jantzen (2002b). Issues regarding anion solubility limits were also not addressedin this assessment. It is recognized that the concentration of sulfate, nitrate, and nitrite willincrease as one considers a less washed sludge, which may ultimately limit or dictate the degreeof washing targeted. Prior to finalizing or selecting a particular frit/sludge washing flowsheet, anevaluation of the anion solubility limits should be addressed. In the assessment of melt rate, one


19

must account for the nitrite and nitrate levels as these may have a significant impact on melt rate.However, the nitrite and nitrate levels will vary with the processing performed in the ChemicalProcess Cell (CPC) and the associated SB3 flowsheet. In any case, the flowsheet should result ina product that meets the nitrite destruction levels (i.e., all products should be less than 1000 mg/lnitrite), but will have different nitrate and formate concentrations depending on the processingstrategy selected.

Table 5-3 summarizes the nominal SB3 compositions for the washing scenarios (using theunderlying assumptions discussed above). Those oxides shown as bold are considered to bemajor components as the projected concentration of these oxides is thought to be > 0.5 wt% inglass over the waste loading range of interest (25 – 60 wt%). Those oxides not bolded wereclassified as minor (i.e., anticipated as not having a significant impact on predicted properties atthe concentrations expected in the glass). This is consistent with Plodinec et al. (1995) whoindicated that trace components (elements whose oxides are present in the glass at concentrationsless than 0.5 wt%) do not have a significant impact on glass durability. The “Others” component,shown in Table 5-3, is a total of all minor components in the sludge. For example, consider the0%, nominal washed case that indicates a 3.69 wt% “Others” group. This indicates that the minorcomponents account for 3.69 wt% of the sludge (calcined, oxide basis). The wt% shown by eachminor component represents the percentage of that component in “Others”. Therefore, thepercentage of each minor component in the sludge can be obtained simply by multiplying thepercentage of “Others” by the amount of “Others” in the sludge. Consider Cr2O3 and the 0%nominal washed case. The nominal SB3 sludge (0% washed) contains 3.69% of “Others” (minorcomponents) of which Cr2O3 is 7.37%. Therefore, the Cr2O3 content in the sludge would be0.272 wt%.

Based on the underlying assumptions previously discussed, the major impact of washing on theprojected nominal compositions is related strictly to Na2O concentrations. Concentrations ofNa2O in the nominal SB3 sludges range from 10.63 wt% to 35.13 wt% in the 100% washed case(no sodium oxalate transferred) to the 0% washed case (complete transfer of the sodium oxalate),respectively. The contribution of other alkali (Li2O, K2O, and Cs2O) to the various sludgeprojections is minimal with respect to Na2O (although their contributions will be considered).With respect to frit development activities, the wide range of Na2O will make it extremelydifficult (or impossible) to develop a single frit that is tolerant or insensitive to this largevariation. (It would be ideal to develop a single frit that would yield acceptable glasses for allwashing schemes over the waste loading interval of interest – assuming no adverse impacts ofother processing issues such as melt rate are encountered.) Given this large variation,adjustments in the alkali content of the frit are expected as the contribution of alkali from thewaste is accounted for. More specifically, as sludge washing is increased, the alkaliconcentration in sludge decreases, therefore, it is anticipated that the alkali content in the frit willincrease (perhaps making the targeted frit composition more “frittable” – a key criteria for fritselection as discussed in Section 1.0).

5.3 Accounting for Anticipated Sludge Variation

Minimum and maximum values for each of the major components and “Others” group are alsoshown in Table 5-3. These intervals are based on ±10% variation around the components in aneffort to capture potential sludge variation that may be observed during processing of SB3 andform the basis for the Variation Stage assessments. Although the official SB3 qualificationsample has not been obtained, historical differences between projections in WCSystems and


20

actual sample analysis have typically been within ±10% for the major oxides of interest. In someinstances, the analytical results of the qualification sample have indicated differences larger thanexpected when compared to WCSystems. However, it is felt that the use of the ±10% is onaverage a good approximation to the expected variation within a sludge batch. This does notindicate that any one of the nominal compositions will actually align itself (compositionally) withthe SB3 qualification sample.

As with the nominal sludge compositions, the most interesting issue associated with the additionof the ±10% variation is the resulting Na2O intervals. For the 0% washed case and a +10%variation, the Na2O concentration is approximately 38.65%. For the 100% washed case and a-10% variation (on the nominal), the Na2O concentration is approximately 9.57% (in sludge).Again, this large range in potential Na2O concentrations will obviously impact the fritdevelopment strategy as a balance between the alkali contribution from the sludge and frit ismaintained.

Stone and Josephs (2001) and Lambert et al. (2001) indicated that melt rate was directly related tototal alkali concentration (melt rate increased as total alkali increased) for the SB2-based glasses.Given this observation and the fact that the SB3 sludge could potentially provide a high % ofNa2O (considering an underwashed sludge), one option for the glass formulation strategy is totake advantage of the relatively high alkali concentration in the sludge to improve melt rate aswas done during the development of Frit 200 to accommodate the high alkali PHA stream(Jantzen 1988). In doing so, the approach must balance the desire to improve melt rate with therequirements to assure both processability (with respect to viscosity and liquidus temperature)and product performance (durability). To accomplish this, compositional adjustments to the fritwill be required. Focusing solely on the desire to enhance melt rate could result in the DWPFmaking a poor-quality product faster (ignoring the use of PCCS). It is expected however thatprojections of the operating window may become durability or viscosity (i.e., challenge the lowerlimit) limited as glass formulation efforts try to balance the desire to increase melt rate and/orwaste loading (both affecting waste throughput) with the desire to minimize the number ofwashes required. Developing a system which is durability limited (e.g., having predictions ofelemental releases that limit the upper waste loading range) would be appropriate. That couldindicate that enhanced melt rates may be realized without compromising product quality giventhe conservatism in the model predictions. Transferring from a liquidus temperature limitedsystem to a durability limited system may have advantages in terms of meeting the goals orobjectives of the accelerated clean-up mission.

Imm

obil

izat

ion

Tec

hnol

ogy

Sect

ion

W

SRC

-TR

-200

2-00

491

Sava

nnah

Riv

er T

echn

olog

y C

ente

r R

ev. 0

Wes

tingh

ouse

Sav

anna

h R

iver

Com

pany

21

Tab

le 5

-3.

Nom

inal

Com

posi

tion

s of

SB

3 as

a F

unct

ion

of W

ashi

ng S

cena

rio

and

Min

imum

and

Max

imum

Val

ues

Ass

umin

g a �1

0% V

aria

tion

(m

ass

frac

tion

s).

0% W

ashe

d25

% W

ashe

d50

% W

ashe

d75

% W

ashe

d10

0% W

ashe

dN

omin

alM

inM

axN

omin

alM

inM

axN

omin

alM

inM

axN

omin

alM

inM

axN

omin

alM

inM

axA

g 2O

0.00

01-

-0.

0001

--

0.00

01-

-0.

0001

--

0.00

01-

- A

l 2O

30.

1314

0.11

830.

1445

0.14

110.

1270

0.15

520.

1523

0.13

700.

1675

0.16

540.

1489

0.18

190.

1810

0.16

290.

1991

Am

O2

0.00

08-

-0.

0008

--

0.00

08-

-0.

0008

--

0.00

08-

- B

aO0.

0493

--

0.04

93-

-0.

0493

--

0.04

93-

-0.

0493

--

CaO

0.02

610.

0235

0.02

870.

0280

0.02

520.

0309

0.03

030.

0272

0.03

330.

0329

0.02

960.

0362

0.03

600.

0324

0.03

96C

e 2O

30.

0699

--

0.06

99-

-0.

0699

--

0.06

99-

-0.

0699

--

Cm

2O3

0.00

01-

-0.

0001

--

0.00

01-

-0.

0001

--

0.00

01-

-C

r 2O

30.

0737

--

0.07

37-

-0.

0737

--

0.07

37-

-0.

0737

--

CuO

0.03

90-

-0.

0390

--

0.03

90-

-0.

0390

--

0.03

90-

-E

u 2O

30.

0009

--

0.00

09-

-0.

0009

--

0.00

09-

-0.

0009

--

Fe 2

O3

0.29

230.

2631

0.32

150.

3138

0.28

240.

3452

0.33

870.

3049

0.37

260.

3680

0.33

120.

4048

0.40

270.

3624

0.44

30G

d 2O

30.

0100

--

0.01

00-

-0.

0100

--

0.01

00-

-0.

0100

--

K2O

0.08

48-

-0.

0848

--

0.08

48-

-0.

0848

--

0.08

48-

-L

a 2O

30.

0405

--

0.04

05-

-0.

0405

--

0.04

05-

-0.

0405

--

Li 2

O0.

0006

--

0.00

06-

-0.

0006

--

0.00

06-

-0.

0006

--

MgO

0.03

71-

-0.

0371

--

0.03

71-

-0.

0371

--

0.03

71-

-M

nO0.

0521

0.04

690.

0573

0.05

590.

0503

0.06

150.

0604

0.05

430.

0664

0.06

560.

0590

0.07

210.

0718

0.06

460.

0789

Na 2

O0.

3513

0.31

620.

3865

0.30

360.

2732

0.33

390.

2483

0.22

340.

2731

0.18

340.

1651

0.20

170.

1063

0.09

570.

1169

Nb 2

O3

0.00

00-

-0.

0000

--

0.00

00-

-0.

0000

--

0.00

00-

-N

d 2O

30.

1342

--

0.13

42-

-0.

1342

--

0.13

42-

-0.

1342

--

NiO

0.01

170.

0105

0.01

290.

0126

0.01

130.

0138

0.01

360.

0122

0.01

490.

0147

0.01

320.

0162

0.01

610.

0145

0.01

77P 2

O5

0.00

00-

-0.

0000

--

0.00

00-

-0.

0000

--

0.00

00-

-Pb

O0.

0595

--

0.05

95-

-0.

0595

--

0.05

95-

-0.

0595

--

PdO

0.00

72-

-0.

0072

--

0.00

72-

-0.

0072

--

0.00

72-

-Pr

2O3

0.03

67-

-0.

0367

--

0.03

67-

-0.

0367

--

0.03

67-

-Pu

O2

0.01

03-

-0.

0103

--

0.01

03-

-0.

0103

--

0.01

03-

-R

hO2

0.01

53-

-0.

0153

--

0.01

53-

-0.

0153

--

0.01

53-

-R

uO2

0.05

47-

-0.

0547

--

0.05

47-

-0.

0547

--

0.05

47-

-Si

O2

0.02

430.

0218

0.02

670.

0261

0.02

340.

0287

0.02

810.

0253

0.03

090.

0305

0.02

750.

0336

0.03

340.

0301

0.03

68Sm

2O3

0.01

97-

-0.

0197

--

0.01

97-

-0.

0197

--

0.01

97-

-T

hO2

0.02

82-

-0.

0282

--

0.02

82-

-0.

0282

--

0.02

82-

- T

iO2

0.00

00-

-0.

0000

--

0.00

00-

-0.

0000

--

0.00

00-

-U

3O8

0.07

390.

0666

0.08

130.

0794

0.07

150.

0873

0.08

570.

0771

0.09

430.

0931

0.08

380.

1024

0.10

190.

0917

0.11

21Z

nO0.

0809

--

0.08

09-

-0.

0809

--

0.08

09-

-0.

0809

--

ZrO

20.

1463

--

0.14

63-

-0.

1463

--

0.14

63-

-0.

1463

--

Oth

ers

0.03

690.

0332

0.04

060.

0396

0.03

560.

0435

0.04

270.

0385

0.04

700.

0464

0.04

180.

0511

0.05

080.

0457

0.05

59Su

m1.

0000

1.00

001.

0000

1.00

001.

0000


22

5.4 SB3 Composition as a Function of Decant

As previously stated, assessments were initially performed using the linear washing schemesprior to receiving projected sludge compositions as a function of washing (or decant) from HLWPE. Elder provided the compositional estimates of SB3 as a function of decant.9 The elementalconcentrations provided by Elder were converted to an oxide basis (by multiplying by theappropriate gravimetric factor) and these data are presented in Table 5-4. These nominalcompositions form the basis for the final phase assessments (Phase 2) as described in Section 7.0.

General observations of composition as a function of washing indicate that the Na2Oconcentrations decrease with increased washing (or decant). Initially, the Na2O concentrationdecreases relatively quickly with the differences becoming smaller as the decant numberincreases. All other components trend in the opposite direction – increased concentration as thedecant number increases. Although this trend was expected, the Na2O concentration for theminimum washed sludge (Decant #5) is lower than that associated with the nominal 0% washedcase (see Table 5-3), 31.205 versus 35.13 wt%, respectively. This difference is based on theassumptions made in the initial compositional projections given no washing models wereavailable at the time. Given this difference, frits developed for the 0% washed case may bealkali-deficient for the Decant #5 stream resulting in a smaller projected operational window orlower melt rate. This required alternative frits to be developed to compensate for the Na2Odifference.

It should also be noted that the compositional projections provided by Elder for the Phase 2assessment include significant quantities of TiO2 ranging from 2.154% to 2.627% in Decant #5 toDecant #15, respectively. TiO2 will be considered a major oxide when these sludges are evaluated– the impact of TiO2 will be accounted for in the various Phase 2 predictions. This is anotherdifference between the two assessments (Phase 1 vs. Phase 2) given the potential impact of theMST stream was not accounted for in the initial phase assessment.

To account for impact of sludge variation on projected operational windows, select frits wereevaluated in terms of their ability to process ±10% variation around each major oxide associatedwith two decants. This formed the Phase 2 Variation Stage of the paper study assessments. Morespecifically, ±10% variation around the Decant #7 was selected to assess the robustness of fritsdeveloped for the lower washed sludges. Frits developed for the higher washed sludges wereassessed against a ±10% variation around the Decant #12. This strategy was used given the±10% variation around Decant #7 captured the value of each major oxide associated with thenominal sludge compositions for Decant #5 through Decant #9.

9 Personal communication with H.H. Elder via email dated 7/30/02. Appendix A provides the data transmitted in the

personal communication (elemental wt%, calcine basis).

Imm

obil

izat

ion

Tec

hnol

ogy

Sect

ion

WSR

C-T

R-2

002-

0049

1Sa

vann

ah R

iver

Tec

hnol

ogy

Cen

ter

Rev

. 0W

estin

ghou

se S

avan

nah

Riv

er C

ompa

ny

23

Tab

le 5

-4.

Pro

ject

ed S

B3

Com

posi

tion

s as

a F

unct

ion

of D

ecan

t (ox

ide

basi

s, w

t%).

Oxi

deD

ecan

t #5

Dec

ant #

6D

ecan

t #7

Dec

ant #

8D

ecan

t #9

Dec

ant #

10D

ecan

t #11

Dec

ant #

12D

ecan

t #13

Dec

ant #

14D

ecan

t #15

Al 2

O3

13.8

4414

.348

14.7

7715

.139

15.4

6715

.743

16.0

0616

.253

16.4

5816

.669

16.8

86B

2O3

0.00

00.

000

0.00

00.

000

0.00

00.

000

0.00

00.

000

0.00

00.

000

0.00

0B

aO0.

192

0.19

80.

204

0.20

90.

214

0.21

80.

221

0.22

50.

228

0.23

10.

234

CaO

2.75

52.

855

2.94

03.

012

3.07

73.

132

3.18

53.

234

3.27

43.

316

3.36

0C

e 2O

30.

267

0.27

70.

285

0.29

20.

298

0.30

40.

309

0.31

30.

317

0.32

10.

326

Cr 2

O3

0.28

30.

293

0.30

20.

310

0.31

60.

322

0.32

70.

332

0.33

70.

341

0.34

5C

s 2O

0.00

00.

000

0.00

00.

000

0.00

00.

000

0.00

00.

000

0.00

00.

000

0.00

0C

uO0.

152

0.15

70.

162

0.16

60.

169

0.17

20.

175

0.17

80.

180

0.18

30.

185

Fe2O

330

.784

31.9

0532

.858

33.6

6434

.392

35.0

0735

.591

36.1

4136

.596

37.0

6537

.549

K2O

0.32

90.

341

0.35

20.

360

0.36

80.

375

0.38

10.

387

0.39

20.

397

0.40

2L

a 2O

30.

176

0.18

20.

187

0.19

20.

196

0.20

00.

203

0.20

60.

209

0.21

10.

214

Li 2

O0.

000

0.00

00.

000

0.00

00.

000

0.00

00.

000

0.00

00.

000

0.00

00.

000

MgO

0.14

40.

150

0.15

40.

158

0.16

10.

164

0.16

70.

169

0.17

20.

174

0.17

6M

nO5.

491

5.69

05.

860

6.00

46.

134

6.24

46.

348

6.44

66.

527

6.61

16.

697

MoO

30.

000

0.00

00.

000

0.00

00.

000

0.00

00.

000

0.00

00.

000

0.00

00.

000

Na 2

O31

.205

28.7

0126

.571

24.7

7023

.142

21.7

7020

.464

19.2

3518

.219

17.1

7016

.089

Nb 2

O3

0.00

00.

000

0.00

00.

000

0.00

00.

000

0.00

00.

000

0.00

00.

000

0.00

0N

iO1.

231

1.27

61.

314

1.34

61.

375

1.40

01.

423

1.44

51.

463

1.48

21.

501

PbO

0.23

00.

238

0.24

50.

251

0.25

70.

261

0.26

50.

270

0.27

30.

276

0.28

0Si

O2

1.60

31.

661

1.71

11.

753

1.79

11.

823

1.85

31.

882

1.90

61.

930

1.95

5T

hO2

0.11

00.

114

0.11

70.

120

0.12

20.

125

0.12

70.

129

0.13

00.

132

0.13

4T

iO2

2.15

42.

232

2.29

92.

356

2.40

72.

450

2.49

02.

529

2.56

12.

594

2.62

7U

3O8

7.79

28.

075

8.31

68.

520

8.70

58.

860

9.00

89.

147

9.26

29.

381

9.50

4Y

2O3

0.00

00.

000

0.00

00.

000

0.00

00.

000

0.00

00.

000

0.00

00.

000

0.00

0Z

nO0.

315

0.32

60.

336

0.34

40.

351

0.35

80.

364

0.36

90.

374

0.37

90.

384

ZrO

20.

568

0.58

90.

607

0.62

20.

635

0.64

60.

657

0.66

70.

676

0.68

40.

693

sum

99.6

2499

.610

99.5

9899

.588

99.5

7999

.572

99.5

6599

.558

99.5

5399

.547

99.5

41


24



25

6.0 Assessment of Linear Washing Scenarios (Phase 1):Nominal and Variation Stages

Using the available PCCS process/product models, various frits will be assessed as a function ofSB3 washing. Evaluating the predicted impacts and projected operating windows for candidatefrits will provide one of the primary criteria that should be used in the SB3 frit selection process.It is not the intent of this study to recommend a frit to DWPF for SB3—only to provide insightinto the selection process. In this section, Phase 1 assessments based on the nominal SB3 linearwashing scenarios are discussed using the strategy as defined for the Nominal Stage and for theVariation Stage.

6.1 Nominal Stage Assessment

Elder (2002) has performed calculations similar to those being utilized in the Nominal Stage ofthis study to determine that Frit 202 and Frit 320 are viable candidates for SB3 given a specificnumber of washes and decants.10 Frit 202 was developed by Jantzen et al. (1988) as a “generic”coupled operations frit – one that could be used for several combinations of sludge and sodiumrich PHA waste streams. Frit 320 was developed specifically for improving melt rate for SB2(Peeler et al. 2001a) – a sludge-only flowsheet. Although neither frit was developed specificallyfor SB3, the calculations performed by Elder (2002) indicate that Frit 202 and Frit 320 are viablecandidates for SB3 when considering different washing/decant options. This is consistent withthe assessments performed by Peeler et al. (2002a) for Frit 320 and SB3 (although sodium oxalatewas not accounted for). Given their viability and classification as “baseline” frits to this point,assessments using both frits will be made over all washing cases being considered.

Although the Nominal Stage analysis (based solely on nominal compositions) should provide acomparative or confirmatory analysis to the operational windows projected by Elder (2002),slight differences in the acceptance criteria, acceptable limits (PAR vs. MAR), and SB3compositions may yield slight differences. It is anticipated that the incorporation of the ±10%sludge variation in the Variation Stage will provide more insight into robustness and will boundElder’s calculations. Table 6-1 summarizes the current “baseline” and alternative candidate fritcompositions used in the initial phase assessments (refer to Table 5-3 for the sludgecompositions). The Nominal Stage assessment results are shown in Table 6-2.

10 Frit 202 is more refractory (less total alkali) and is therefore capable of handling a less washed sludge that would

contain more Na2O. The use of Frit 320 with an underwashed sludge has a higher potential to produce anunacceptable product (limited based on predictions of durability) given the high alkali content in the frit which wasthe basis for increasing melt rate for SB2.

Imm

obil

izat

ion

Tec

hnol

ogy

Sect

ion

WSR

C-T

R-2

002-

0049

1Sa

vann

ah R

iver

Tec

hnol

ogy

Cen

ter

Rev

. 0W

estin

ghou

se S

avan

nah

Riv

er C

ompa

ny

26

Tab

le 6

-1.

Nom

inal

Com

posi

tion

s of

Can

dida

te F

rits

(in

wt%

on

an o

xide

bas

is).

Fri

t20

2F

rit

320

Fri

t40

0F

rit

401

Fri

t40

2F

rit

403

Fri

t40

4F

rit

405

Fri

t40

6F

rit

407

Fri

t40

8F

rit

409

Fri

t41

0F

rit

411

Fri

t41

2F

rit

413

Fri

t41

4F

rit

415

Fri

t41

6F

rit

417

Fri

t41

8F

rit

419

Al 2

O3

--

--

--

--

--

--

-1

--

--

1-

--

B2O

38

820

3012

1512

2015

88

88

88

98

108

88

8L

i 2O

78

--

-3

35

5-

24

55

55

65

88

88

Na 2

O6

12-

--

--

--

66

65

1212

1514

1511

118

15S

iO2

7772

8070

8882

8575

8086

8482

8274

7571

7270

7273

7669

MgO

2-

--

--

--

--

--

--

--

--

--

--

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

100

Tab

le 6

-2.

Sum

mar

y of

Nom

inal

Sta

ge A

sses

smen

ts fo

r C

andi

date

SB

3 F

rits

(was

te lo

adin

g ra

nges

are

in w

t% o

n a

calc

ined

, oxi

de b

asis

).

Res

ults

Pre

sent

ed a

re f

rom

a W

aste

Loa

ding

Int

erva

l of

25%

to

60%

Fri

t20

2F

rit

320

Fri

t40

0F

rit

401

Fri

t40

2F

rit

403

Fri

t40

4F

rit

405

Fri

t40

6F

rit

407

Fri

t40

8F

rit

409

Fri

t41

0F

rit

411

Fri

t41

2F

rit

413

Fri

t41

4F

rit

415

Fri

t41

6F

rit

417

Fri

t41

8F

rit

419

0% w

ashe

dW

L (

nom

inal

)N

one

Non

e40

-53

32-4

646

-57

37-5

240

-53

32-4

432

-48

25%

was

hed

WL

(no

min

al)

31-4

0N

one

30-4

734

-51

45-5

540

-55

34-5

133

-51

50%

was

hed

WL

(no

min

al)

29-4

5N

one

26-4

528

-43

75%

was

hed

WL

(no

min

al)

29-3

526

-41

26-4

526

-45

26-4

325

-44

100%

was

hed

WL

(no

min

al)

Non

e25

-37

25-3

625

-36

25-3

425

-40


27

Projected operating windows (i.e., waste-loading ranges) for the five washing scenarios arepresented in Table 6-2 for each candidate frit composition over the waste loading interval ofinterest (25 – 60 wt%). In the following sections, various frit/sludge combinations are discussedin terms of the projected operational window and the property prediction limiting the lower andupper waste loadings. Initially, an in-depth discussion linking the details provided in Appendix Bto the summary table (Table 6-2) is provided to demonstrate how the summary table wasdeveloped. This discussion will provide insight into the comparison of the predicted properties tothe acceptance criteria and the influence they have on establishing or defining the projectedoperational windows. Given the understanding of how the summary table was developed andknowing the extensive number of combinations that result when coupling the candidate frits withthe different washing scenarios, detailed discussion of other frit/sludge systems will be brief andselect. Given the classification of Frit 202 and Frit 320 as “baseline” frits to this point, both willbe discussed to some degree for each washing scenario considered. Although a particular frit isnot specifically discussed in the text, one should not rule out its potential use. Again, thediscussions are intended to provide insight into how the summary table (Table 6-2) wasdeveloped and what information can be extracted and carried forward to the frit selection process.It must be recognized that the assessments and projected operational windows are based solely onmodel predictions – no experimental work was performed.

Detailed information regarding the predicted properties for the nominal compositions whencoupled with each candidate frit is provided in Appendix B (linear washing scenarios). Thecolumns identified as “Type” summarizes the specific sludge being evaluated with the secondcolumn (“Frit ID”) identifying the frit. The third column “Satisfies PAR” represents thecomparison of the predicted properties versus the PAR limits as shown in Table 4-1. The lasttwo columns specify the minimum and maximum WLs over which the specific sludge/fritcombination possess the characteristics described by the “Satisfies PAR” nomenclature.

6.1.1 0% Washed Case

For example, consider the 0% washed, SB3 nominal sludge case and Frit 202 (i.e., Table 6-3 is anexcerpt of this specific information from Appendix B). For Row #1 (which represents a wasteloading range between 25 – 28% – see last two columns), the “Satisfies PAR” nomenclatureindicates “Durable; Visc.; Not Homog; New TL; Al2O3; and Alkali.” This nomenclature indicatesthat the nominal sludge/Frit 202 combinations over the WL range of 25 – 28% satisfies the PARlimits (based on predictions using target compositions) for durability, viscosity, the new liquidustemperature model (New TL), the Al2O3 lower limit, and the sum of alkali upper limit (Alkali).However, this glass challenges the homogeneity constraint (as noted by “Not Homog”) at thePAR. That is, it fails to meet the homogeneity PAR acceptance value of 210.92 (as noted inTable 4-1) and thus is predicted to produce inhomogeneous glasses over this WL range. Basedon the acceptance criteria established in Section 4.0, this particular sludge/frit combination wouldbe restricted from DWPF processing based solely on the homogeneity constraint over the wasteloading range of 25 – 28%.

Imm

obil

izat

ion

Tec

hnol

ogy

Sect

ion

WSR

C-T

R-2

002-

0049

1Sa

vann

ah R

iver

Tec

hnol

ogy

Cen

ter

Rev

. 0W

estin

ghou

se S

avan

nah

Riv

er C

ompa

ny

28

Tab

le 6

-3.

Nom

inal

Sta

ge A

sses

smen

t for

the

0% W

ashe

d N

omin

al S

ludg

e w

ith

Fri

t 20

2 ov

er t

he W

aste

Loa

ding

Ran

ge o

f 25

– 6

0%.

Typ

eFr

it I

DSa

tisf

ies

PAR

Min

(Slu

dge

Loa

ding

(%

))M

ax(S

ludg

e L

oadi

ng (

%))

SB3

Nom

inal

for

Was

hing

@ 0

%20

2D

urab

le; V

isc;

Not

Hom

og; N

ew T

L; A

l2O

3; a

lkal

i25

28SB

3 N

omin

al f

or W

ashi

ng @

0%

202

Dur

able

; Vis

c; N

ot H

omog

; New

TL

; Al2

O3;

Not

alk

ali

2930

SB3

Nom

inal

for

Was

hing

@ 0

%20

2N

ot D

urab

le; V

isc;

Not

Hom

og; N

ew T

L; A

l2O

3; a

lkal

i31

33SB

3 N

omin

al f

or W

ashi

ng @

0%

202

Not

Dur

able

; Vis

c; H

omog

; New

TL

; Al2

O3;

alk

ali

3441

SB3

Nom

inal

for

Was

hing

@ 0

%20

2N

ot D

urab

le; N

ot L

Vis

c; H

omog

; New

TL

; Al2

O3;

alk

ali

4260


29

Continuing the discussion of the Frit 202, 0% washed SB3 combination, as waste loadings areincreased to 29 and 30%, not only is the homogeneity constraint failed (at the PAR) but the sumof alkali criterion is exceeded as well. It should be noted that in this case, the Al2O3

concentration is less than 4 wt% with the sum of alkali content exceeding 19.3%. If however, theAl2O3 concentration is ≥ 4.0 wt%, there is no sum of alkali limit (over the compositional rangetested), which is the case for waste loadings of 31% and higher for this system. Based on thepredicted property assessments, glasses in the 29 – 30% waste loading range are unacceptable andthus not processable. At WLs of 31% and higher, predictions of durability indicate unacceptableglasses may be produced even though the Al2O3 concentration is > 4.0% (otherwise the “NotAlkali” nomenclature would be shown). The low viscosity limit is exceeded (as indicated by the“Not L Visc”) at waste loadings between 42 – 60%.

Based on the assessment of the various property predictions, the SB3 nominal 0% washed sludgewhen coupled with Frit 202 does not yield an acceptable processing window. Table 6-2summarizes this assessment by the use of “none” indicating that there is not a projected operatingwindow for Frit 202/0% washed SB3 nominal sludge combinations over the 25 – 60 wt% WLrange based on the acceptance criteria established (see Table 4-1).

Using the information in Appendix B, a projected operational window for the Frit 320/0% SB3nominal sludge also does not exist. The primary criterion that eliminates this specific frit/sludgecombination is the prediction of durability. With the 0% washed sludge containingapproximately 35% Na2O and Frit 320 being a high alkali based frit (alkali added to improve meltrate for SB2 [Peeler et al. 2001a]), combining these two inputs over the waste loading range ofinterest would produce extremely high alkali based glasses – thus predictions of an unacceptabledurability or PCT response are expected.

Given the two “baseline” frits yield no processing window, alternative frits were developed forthe 0% washed nominal SB3 sludge. It should be noted that neither Frit 202 nor Frit 320 wasdeveloped for this specific waste stream so their application may not be warranted. Alternativefrits that were developed include: Frits 400, 401, 402, 403, 404, 405, and 406.11 As previouslymentioned, a detailed discussion on each of the systems is not warranted but the reader is referredto Appendix B for details of each system.

Based on the summary shown in Table 6-2, relatively large operational windows exist for all ofthe alternative frits when coupled with the nominal 0% washed SB3 composition. Frits 400, 401,and 402 are two component frits (with different SiO2/B2O3 ratios) which are depleted of alkaliand, thus, are compensating for the high alkali content of the 0% washed sludge. Projectedoperational windows for Frit 400, 401, and 402 are 40 – 53%, 32 – 46%, and 46 – 57% WL,respectively. Although relatively large operational windows exist for these three frits, otherfactors need to be considered in the frit selection process – melt rate and frittability. Based solelyon composition, the primary issue with these alkali-depleted frits will be the desire to have a“frittable” frit. If proven to be unfrittable, their use may be eliminated especially if an additivecomposition that is frittable yields a similar acceptable WL interval (assuming melt rates aresimilar).

11 During the frit development process, an alphanumeric nomenclature or system was used to identify specific frit

compositions. These alphanumeric identifiers have been converted to a numerical series (the 400 series). AppendixC provides the conversion chart.


30

To increase the likelihood of being able to produce a frit from additives, alkali additions to frits403, 404, 405, and 406 were made. Given the high concentration of Na2O in the sludge, Li2Owas used as the frit additive at relatively low concentrations. The low concentrations primarilybeing driven by issues associated with predictions of durability.

All of the alternative frits developed for the nominal 0% washed case appear to be primarycandidates. This latter statement being based solely on their respective, relatively large operatingwindows and the fact that the frits do contain alkali (Li2O) resulting in a higher potential to meetthe frittability constraint. The upper waste loadings projected for Frits 403, 404, 405, and 406 are52, 53, 44, and 48 wt%, respectively. Higher waste loadings are limited by predictions ofdurability and/or viscosity (challenging the low viscosity limit) which suggest that the frits beingdeveloped are taking advantage of the high alkali concentrations of the waste. More specifically,targeting higher waste loadings for the 0% washed nominal sludge yields glasses that are enrichedin alkali promoting the formation of a less durable glass and/or driving viscosities below theacceptable lower limit. Not only does this suggest that the frits are taking advantage of the highalkali in the sludge, but also that the property limiting upper waste loadings can be shifted frombeing a TL-limited system to a viscosity and/or durability limited system based on predictivemodels. It should be noted that for the alternative frits developed for the 0% washed case, allsystems are either durability or low viscosity limited on the upper waste loading side.

The extremely high upper waste loading limit (57%) predicted by Frit 402 is very attractive.However, as described in Section 6.2, its response to compositional variation is less than adequatewhich detracts from it being classified as a primary frit candidate.

Again, numerous comparisons could be discussed. The details from which the summary tablewas developed is presented in Appendix B so that the reader can assess or make specificcomparisons of interest.


As discussed in Section 5.0, as the degree of washing is increased, the Na2O concentration in thelinear washed sludge decreases. Therefore, frit development activities compensated by adjustingthe alkali concentration and type as well as their ratios in perspective frits. The Nominal Stagestrategy was used to assess the response of the projected operational window using modelpredictions to these compositional changes. Based on rudimentary glass science knowledge,enhancing the alkali concentration in the frit improves the likelihood of being able to manufacturea prefabricated frit from the proposed additives and potentially improves melt rate (based on theobservations by Stone et al. [2001] and Lambert et al. [2001]).

Given the classification as “baseline” frits, projected operational windows for Frit 202 and Frit320 will be discussed initially. In this section, general observations are made based on thedetailed information provided in Appendix B. The reader is referred to this appendix to obtainmore details or to make specific comparisons of interest.

As was the case for the 0% washed sludge, use of Frit 320 is prohibited with the 25% washednominal sludge over the entire WL range of interest due to durability predictions.12 The morerefractory (less alkali) Frit 202 does produce an operational window with the nominal 25% 12 Use of “prohibited” in this report refers to the inability to utilize a specific frit over the entire 25 – 60%

WL range of interest based solely on model predictions.


31

washed sludge from 31 – 40 wt%. Although the frit is more refractory, predictions of durabilitylimit access to waste loadings of 41% or greater.

Alternative frits developed for the 25% washed case include: 407, 408, 409, and 410. All of thesefrits yield relatively large operational windows based on model predictions with upper WL limitsin the low- to mid-50% range. Although developed for the 0% washed case, Frits 405 and 406provide operational windows for the 25% washed nominal sludge case. The ability of a single fritcomposition to provide operational windows for a range of sludge compositions is advantageousand demonstrates a degree of operational flexibility. It should be noted that the Nominal Stageassessment is based solely on nominal compositions with the Variation Stage specificallydesigned to provide insight into the robustness of each frit to possible compositional variation.


Continued washing of the sludge results in lower alkali concentrations that require compensationvia frit development or formulation activities in order to maintain a high degree of operationalflexibility. The 50% nominal washed sludge contains approximately 25% total alkali. Couplingthis nominal sludge with Frit 202 provides an operating window from 29 – 45 wt% with higherwaste loadings being limited by TL predictions – not durability or viscosity. Use of Frit 202 maybe advantageous not only from a WL perspective, but given the current availability of the frit,fabrication cost may be eliminated (assuming the quantity of frit existing would be sufficient toprocess SB3) or at least minimized (assuming a limited quantity would be required from avendor). The classification of Frit 202 as a primary candidate based solely on availabilityassumes all other factors (such as robustness, operational window size, and melt rate) are equal.If proven to meet or provide acceptable responses to the Variation Stage and melt rate, a costbenefit analysis should be performed (including adjustments for total waste throughput) to assessthe advantages and (potential) disadvantages of this frit.

Use of Frit 320 is still prohibited from a durability perspective with this nominal sludge –excessive alkali driving predictions of unacceptability. As the degree of washing increases, thealkali concentration in the sludge should decrease to a level in which Frit 320 could be utilized.

Based on the Frit 202 system being TL limited, compositional adjustments to drive the systemtoward being durability limited were attempted – primarily via increasing alkali concentration.The results were Frits 411 and 412. Appendix B confirms that the Frit 411 and Frit 412 basedglasses are either durability and/or low viscosity limited at the higher WLs. Based on modelpredictions, there is no advantage of either Frit 411 or 412 in terms of the maximum wasteloading that could be potentially achieved relative to Frit 202. In fact, use of Frit 412 reduces themaximum WL by 2%. However, the enhanced alkali concentrations may promote faster meltrates that could manifest into higher waste throughput. Lorier et al. (2002) demonstrated for aFrit 320 based system that optimum waste throughput was not achieved at the highest possiblewaste loading. Therefore, consideration of melt rate for these two frits (relative to Frit 202) iswarranted during the frit selection process. It should also be noted that the lower waste loadinglimits for Frit 411 and Frit 412 are extended due to less restrictive challenges to the homogeneityconstraint. This may provide more operational flexibility to DWPF although higher wasteloadings are desired or preferred, in general.


32


Given the overall reduction of alkali in the 75% washed sludge, Frit 320 provides its firstoperational window for this series of nominal sludge compositions. The WL range allowedextends from a low of 26% to a high of 41%. Waste loadings of 42% or greater, are limited bythe low viscosity criterion – not durability.

Coupling Frit 202 with the 75% washed nominal sludge composition also provides an operationalwindow (29 – 35%). Relative to the 25% and 50% washed cases with Frit 202, the windowbecame narrower or more restricted indicating that the use of Frit 202 may be more advantageousfor these lesser washed sludges. (Frit 202 provided no operational window for the 0% washedcase). High viscosity predictions limit access to WLs less than 29%; while predictions of TL

prohibit waste loadings greater than 35% for the 75% washed case.

Compositional adjustments to provide more operational flexibility to DWPF for this specificsludge are shown through Frits 413, 414, 415, and 416. All of these frits yield essentially thesame projected operational windows with respect to each other. Lower WLs are on the order of25 – 26%; with upper WLs ranging from 43 – 45%. When compared to Frit 320 and Frit 202, theupper WL limits achievable are higher with the alternative frit compositions developed by up to4% and 10%, respectively.

One interesting comparison is the operational windows provided by Frit 320 compared to thosefor Frit 416. Frit 416 is based on a very minor compositional change to Frit 320. Morespecifically, 1% of the Na2O was removed and added as Al2O3. This slight change providedaccess to both lower and higher WLs for this specific sludge. As previously discussed, the Frit320 based system failed the low viscosity limit at WLs of 42% and higher. The 1% Al2O3

increased the predicted viscosity in a manner to shift the upper WL limit from 41% to 44% priorto becoming both viscosity and TL limited at 45%. Implications of becoming TL limited at 45%are that additional shifts of Al2O3 for Na2O may not be effective in extending the upper WL limit– although other compositional adjustments are possible.


As previously mentioned, the 100% washed case represents a sludge composition with no Na2Ocontribution from sodium oxalate rendering this sludge to be relatively alkali deficient. Use ofFrit 202 is prohibited (over the WL range of interest) with the 100% washed nominal sludge casewith high viscosity and/or TL limiting both lower and upper WLs.

Coupling the 100% washed sludge with Frit 320 does provide an operational window (25 – 37%)with the system becoming TL limited at higher waste loadings. This is consistent with thefindings of Peeler et al. (2002a), which assessed the addition of Am/Cm and Pu/Gd on SB3(without sodium oxalate).

Alternative frits were developed (Frits 417, 418, and 419) to extend the upper waste loadinglevels and potentially improve melt rate by increasing the alkali content in the frit to compensatefor the low content of alkali in the sludge. This effort was semi-successful with respect to themodel-based projections of the operational window given that Frit 419 was the only alternativefrit to allow for higher waste loadings (based on use of the PAR criteria) when compared to theFrit 320 based system. The enhanced alkali concentration in Frit 419 may also promote highermelt rates that could manifest into higher waste throughput. Based on the observations by Stone


33

et al. (2001) and Lambert et al. (2001) the lower total alkali concentrations in Frits 417 and 418may yield slower melt rates than either Frit 320 or Frit 419. Coupling the projected slower meltrate with lower upper WLs provided a basis for not considering these two frits as primarycandidates.

6.2 Variation Stage Assessment (Phase 1): Linear Washing Scenarios

As mentioned in Section 6.1, the Nominal Stage assessments are based on nominal SB3compositions and do not account for anticipated compositional variation. Therefore, an increasedrisk would result with respect to processability or product quality if a decision were based solelyon this assessment without accounting for compositional variation. For example, consider thecase if the Tank 7 qualification sample did not “match” the nominal composition used (fromTable 5-3). The obvious question would be: “For the frit selected, is there a processing windowfor this sludge?” The intent or focus of this stage was to gain insight into the robustness ofcandidate frits with respect to compositional variation.

The Phase 1 Variation Stage was based primarily on EVs determined for each SB3 linear washingscenario accounting for a ±10% variation around the major oxide. Assessments were made usingmodels currently implemented in DWPF over the WL interval of interest (25 – 60 wt%). Table 6-4 summarizes the results of the Phase 1 Variation Stage assessment in terms of the three metrics(defined in Section 3.0) for each frit/sludge combination. Also shown in Table 6-4, are the resultsof the Phase 1 Nominal Stage assessment for completeness. It must be recognized that theassessments and projected operational windows are based solely on model predictions – noexperimental work was performed.

Detailed information regarding the predicted properties for the EV-based sludge compositions(for each washing scenario) when coupled with each candidate frit is provided in Appendix D.The column identified as “Sludge Loading (%)” summarizes the specific waste loading ofinterest. It should be noted that there are typically more than one row for each sludge loadinggiven the predicted properties for all EVs will vary dramatically. The second column inAppendix D (“Satisfies PAR”) represents the comparison of the predicted property versus thePAR limits as shown in Table 4-1. In this column, properties deemed unacceptable with respectto the PAR acceptance limits are preceded by “Not”. The last column (“# of EVs”) summarizesthe number of EVs whose common property predictions are classified by the “Satisfies PAR”column.

Again, numerous comparisons could be discussed. Detailed information is presented in AppendixD and summarized in Table 6-4 so specific comparisons of interest can be made. Highlightedbelow are some general comments regarding the Variation Stage assessments for both existingand alternative frits. The discussion primarily focuses on high level comparisons for a specificwashing scenario but when applicable comparisons may be made with respect to a frit’s ability totolerate multiple washing scenarios.

Imm

obil

izat

ion

Tec

hnol

ogy

Sect

ion

WSR

C-T

R-2

002-

0049

1Sa

vann

ah R

iver

Tec

hnol

ogy

Cen

ter

Rev

. 0W

estin

ghou

se S

avan

nah

Riv

er C

ompa

ny

34

Tab

le 6

-4.

Sum

mar

y of

the

Nom

inal

and

Var

iati

on S

tage

Ass

essm

ents

for

Can

dida

te S

B3

Fri

ts a

nd th

e L

inea

r W

ashi

ng S

cena

rios

.

Res

ults

Pre

sent

ed a

re f

rom

a W

aste

Loa

ding

Int

erva

l of

25%

to

60%

Fri

t20

2F

rit

320

Fri

t40

0F

rit

401

Fri

t40

2F

rit

403

Fri

t40

4F

rit

405

Fri

t40

6F

rit

407

Fri

t40

8F

rit

409

Fri

t41

0F

rit

411

Fri

t41

2F

rit

413

Fri

t41

4F

rit

415

Fri

t41

6F

rit

417

Fri

t41

8F

rit

419

WL

(no

min

al)

Non

eN

one

40-5

332

-46

46-5

737

-52

40-5

332

-44

32-4

8W

L a

ll E

Vs

(+/-

10%

)N

one

Non

eN

one

Non

e40

-45

43-4

637

-39

37-4

1%

EV

s at

Som

e W

L40

.089

.210

0.0

67.9

100.

010

0.0

100.

010

0.0

WL

of

5% o

r gr

eate

r33

.266

.810

0.0

61.8

100.

010

0.0

86.4

100.

00%

Min

imum

WL

Ran

ge-

-5

-9

7-

5

WL

(no

min

al)

31-4

0N

one

30-4

734

-51

45-5

540

-55

34-5

133

-51

WL

all

EV

s (+

/- 1

0%)

Non

e34

-37

37-3

834

-37

Non

e37

-42

36-4

2%

EV

s at

Som

e W

L80

.710

0.0

100.

010

0.0

43.0

100.

010

0.0

WL

of

5% o

r gr

eate

r59

.110

0.0

95.9

100.

038

.310

0.0

100.

025

%

Min

imum

WL

Ran

ge-

9-

9-

99

WL

(no

min

al)

29-4

5N

one

26-4

528

-43

WL

all

EV

s (+

/- 1

0%)

33-3

8N

one

Non

e%

EV

s at

Som

e W

L10

0.0

97.6

81.5

WL

of

5% o

r gr

eate

r10

0.0

86.2

66.4

50%

Min

imum

WL

Ran

ge12

--

WL

(no

min

al)

29-3

526

-41

26-4

526

-45

26-4

325

-44

WL

all

EV

s (+

/- 1

0%)

Non

eN

one

Non

eN

one

Non

e27

-39

%E

Vs

at S

ome

WL

100.

097

.289

.896

.082

.510

0.0

WL

of

5% o

r gr

eate

r79

.996

.086

.393

.680

.610

0.0

75%

Min

imum

WL

Ran

ge-

--

--

15

WL

(no

min

al)

Non

e25

-37

25-3

625

-36

25-3

425

-40

WL

all

EV

s (+

/- 1

0%)

26-3

525

-33

26-3

428

-31

28-3

6%

EV

s at

Som

e W

L10

0.0

100.

010

0.0

100.

010

0.0

WL

of

5% o

r gr

eate

r10

0.0

100.

010

0.0

100.

010

0.0

100%

Min

imum

WL

Ran

ge11

910

611


35

6.2.1 0% Washing Case

A detailed discussion for the Frit 202-based EVs is provided below to demonstrate how theinformation in Appendix D can be translated to provide insight into the robustness of each frit toanticipated sludge variation. More specifically, this detailed discussion will outline or guide thedefinition of the three metrics for the Frit 202 / sludge combination and translate how thesepromote or support the frit selection process. Again, Table 6-4 summarizes the information of allfrit / sludge combinations.

Consider the 0% washed EV-based sludges / Frit 202 information in Appendix D at the lowerwaste loading of interest – 25%. Four rows are shown at 25% WL with all four indicating thatthe glasses produced by this combination are predicted to be inhomogeneous (at the PAR) andthus would not be processable. A high percentage of the 455 EVs also fail either the Al2O3 and/orthe sum of alkali constraints. Therefore at 25% WL, there are no EV-based sludges that would beprocessable with Frit 202.

As waste loadings are increased, durability limitations as well as homogeneity, Al2O3 and sum ofalkali restrictions eliminate the potential to process at 26% WL. A review of each WL willindicate that there is no WL interval in which all EVs can be processed based on modelpredictions and the use of the PAR acceptance criteria. This is reflected in Table 6-4 by the“none” shown for the first metric. An effective method to identify potential WLs or WL rangesin which all 455 EVs can be processed is to scan the “# of EVs” column for 455 then evaluate the“Satisfies PAR” column to assure that all predicted properties are acceptable (“Not” should beabsent from that row). For example, consider WLs of 45% and higher (as shown in Appendix D).The “# of EVs” column contains 455 which indicates that all 455 EV-based glasses (with Frit202) fall into the same category. Unfortunately, a review of the “Satisfies PAR” indicates thatthese EV-based glasses are predicted to fail both the durability and viscosity PAR criteria. Thisagain results in the “none” entry for the first metric in Table 6-4 for this system indicating thatthere is no WL interval in which all EVs can be processed based on model predictions and the useof the PAR acceptance criteria.

Also provided in Appendix D is a summary table for each frit / sludge combination beingevaluated. The columns shown in this table are “WL Range”, “# of EVs and Centroid” and “% oftotal”. This summary table helps to define the second and third metrics for the Variation Stageassessments. The “WL Range” column indicates a waste loading interval (i.e., “0” indicates nointerval, “1” indicates a 1% WL interval, etc……) but does not specify the particular interval.The “# of EVs and Centroid” column indicates the number of EVs (out of the 455) that areprocessable within the corresponding WL interval. The third column provides the percentage ofthe 455 EVs. Consider the “WL Range” of “0” for the 0% washed, Frit 202 EV-based glasses.The summary indicates that 273 of the 455 EVs (or 60%) are not processable at any wasteloading over the WL range of 25 – 60 wt%. The converse of this is that approximately 40% ofthe EVs are processable at some waste loading – the second metric as shown in Table 6-4. Againthe second metric defines the percentage of the EVs and centroid that yield an acceptable glass atsome waste loading of interest. The higher the percentage the more robust the frit composition isto compositional variation of the sludge. For example, a 100% for this metric would indicate thatall of the EVs generated (accounting for the ±10% variation) and the centroid could beprocessable at some waste loading in the interval from 25 – 60%.

The third metric is also determined from the information provided in the summary tables shownin Appendix D for each system. This metric builds upon the second and serves a measure of the


36

percentage of the EVs and centroid that yield an acceptable glass over a minimum waste loadingrange of 5% within the 25 – 60% window being evaluated. For the Frit 202, 0% washed EV-based system, 304 of the 455 EVs (or ~66.8%) either have no operational windows or operationalwindows with a width of no more than 4% (perhaps not the same 4% across all the EVs).Conversely, 33.2% of the 455 EVs have operational windows greater than 4% – the secondmetric as shown in Table 6-4.

To summarize the Variation Stage assessment for the Frit 202, 0% washed sludge case, there isno WL interval in which all of the EVs could be processed, although 40% of the EVs could beprocessed at some WL. Only 33.2% of the EVs have operational windows of at least 5%. Thesemetrics, coupled with the fact that the Nominal Stage assessment based on the nominal waste 0%washed sludge did not possess an operational window, suggests that Frit 202 may not be aprimary candidate for this specific sludge envelope.

The same non-ideal results are shown for Frit 320, where the high alkali content of both thesludge and the frit produce durability limited systems. Therefore, if a 0% washed sludge isrealized (i.e., no or limited washing of the sludge), the use of Frit 202 or Frit 320 will beprohibited based on model predictions.

Alternative frits (Frit 400, 401, 402, 403, 404, 405, and 406) were developed during the NominalStage assessment and given model predictions are readily available, an assessment of theresponse to compositional variation was performed for each. Frits 400, 401, and 402 provideless than ideal results with respect to the three metrics. However, Frits 403, 404, 405, and 406indicate the ability to tolerate the projected compositional variation very well. That is, all 455EVs can be processed over some waste loading interval within the 25 – 60% range. As shown inTable 6-4, the 2nd and 3rd metrics for these four frit-based systems support the fact that these fritsare extremely robust to the projected compositional variation – 100% shown for all systems. Forexample, consider Frits 403 and 404 in which the projected operational windows over which allof the EVs could be processed are 40 – 45% and 43 – 46%, respectively. The minimum WLrange over which all of the EVs can be processed is 9% and 7%, respectively. The VariationStage assessment for these frits indicate an extremely high tolerance to this specific waste streamand the compositional envelope produced when considering the ±10% variation. These resultsmake Frit 403 and 404 strong candidates for consideration as the frit selection process continues –given a target sludge composition within the compositional range evaluated. Assessments of meltrate and frittability have not been taken into account in this latter statement.


Similar trends are observed with the Frit 202/25% washed sludge case as were observed with the0% washed sludge (see Table 6-4). Although the Nominal Stage assessment indicated a 31 –40% WL range over which glasses would be acceptable, accounting for compositional variationresults in a less than perfect system. To summarize the Variation Stage assessment for the Frit202, 25% washed sludge case, there is no WL interval in which all of the EVs could be processedalthough ~81% of the EVs could be processed at some WL. Only 59.1% of the EVs haveoperational windows of at least 5%. These metrics, coupled with the fact that the Nominal Stageassessment based on the nominal waste 25% washed sludge did not possess an operationalwindow, suggests that Frit 202 may not be a primary candidate for this specific waste stream orenvelope. Frit 320 continues to be durability limited, which restricts its use as a possiblecandidate for the 25% washed sludge.


37

The Variation Stage assessment also includes alternative frits (Frits 407, 408, 409, 410, 405, and406)13 developed during the Phase 1 assessment for the 25% nominal sludge. Frits 405, 407, 409and 410 show a high tolerance for compositional variation with relatively large processingwindows projected for all 465 EVs. Relatively high minimum WL ranges of 9% are projected foreach EV when coupled with each frit. Although the projected operational window for thenominal 25% sludge / Frit 408 system (Nominal Stage) was 40 – 55%, its response to the EVswas less attractive relative to other frits. Therefore, although the high waste loadings appearattractive, consideration of its ability to handle compositional variation should be factored into thefrit selection process.

Although not specifically developed for the 25% washed case, Frits 405 and 406 show flexibilityin being highly tolerant to the compositional variation associated with the 0% washed case butalso the 25% washed case as well. Projected WL ranges over which all 465 EVs could beprocessed are 34 – 37% and 37 – 38% for Frit 405 and 406, respectively. Assessment of the othermetrics suggest that Frit 405 is more tolerant with 100% of the EVs having a minimum WL rangeof 9%; whereas only 95.9% of the EVs have a minimum WL range of 5% for Frit 406.


When the 50% washed sludge is considered, the use of Frit 202 is very attractive. The NominalStage assessment provided an operational window of 29 – 45%. The Variation Stage assessmentindicates that all of the EVs can be processed over a WL range of 33 – 38% with 100% of theEVs having a minimum WL interval of 5%. In fact, the minimum WL interval for all of the EVsis 12% – a very positive statement about the potential use of Frit 202 within this compositionalenvelope. Frit 320 continues to provide no operational window due to predictions of durability orlow viscosity.

Given the positive assessments of Frit 202, only two alternative frits (Frit 411 and 412) weredeveloped during the Phase 1 Nominal Stage assessment – both rendering essentially the sameWL ranges based on the nominal sludge composition. The results of the Variation Stageassessment indicate that both frits are less tolerant to compositional variation relative to Frit 202.This latter statement is supported by the lack of a projected operational window over which allEVs could be processed. Based on an assessment of subsequent metrics, a more detailed analysissuggests that Frit 411 is slightly more robust to compositional variation than Frit 412.

It is known that Frit 202 is frittable, so unless Frit 202 has an adverse impact on melt rate or totalwaste throughput, the development of subsequent frits for this specific sludge should not bepursued. This is aided by the fact that Frit 202 is currently in stock at DWPF which mayeliminate (assuming the quantity of frit existing would be sufficient to process SB3) or at leastminimize (assuming a limited quantity would be required from a vendor) manufacturing costs.However, if Frit 411 shows a marked improvement in melt rate relative to Frit 202 (given thehigher total alkali content in the frit – see Table 6-1), further consideration should be made priorto eliminating it during the frit selection process.


As the Na2O concentration continues to decrease, a transition in candidate frits can be observed interms of the Phase 1 Variation Stage metrics. Although Frit 320 does not provide a WL range 13 Although Frits 405 and 406 were not specifically developed for the 25% washed case, given the positive Nominal

and Variation Stage assessments for the 0% washed case, they were included in this assessment.


38

over which all of the EVs can be processed, ~97% of the EVs could be processed at some WLand 96% of all the EVs have a minimum WL range of 5%. This transition was also observed inthe Nominal Stage assessment where the use of Frit 320 provided a 26 – 41% WL interval basedon the nominal 75% washed sludge composition. Although not ideal in its response to theapplied compositional variation, the depletion of alkali in the sludge makes Frit 320 a potentialcandidate for this compositional region.

Similar to the Frit 320 assessment, the Frit 202 Phase 1 Variation Stage assessment projects nowindow of opportunity over which all of the EVs could be processed. Although 100% of the 423EVs could be processed at some waste loading, only ~80% have a minimum WL range of 5%.Although less than perfect, these results should not eliminate Frit 202 as a possible candidate forthis particular waste stream or compositional envelope.

Of the four alternative frits (413, 414, 415, and 416) developed during the Nominal Stage, theresults of the Variation Stage assessments are somewhat negative for three (413, 414, and 415).The most interesting observation is the response of Frit 416 (a modified formulation of Frit 320 inwhich 1% of the Na2O was added as Al2O3). Although the compositional modification appears tobe negligible, its impact on predicted properties, which define the projected operational window,is rather high. As mentioned above, there was no WL or WL range over which all 423 EVs couldbe processed with Frit 320. The slight compositional modification of Frit 416 results in a 27 –39% WL range over which all of the EVs could be processed. This result indicates a hightolerance of Frit 416 to the applied compositional variation of ±10%. Evaluation of the thirdmetric provides additional insight into the robustness of Frit 416. A minimum WL range of 15%is predicted for each of the 423 EVs – a very strong statement in terms of flexibility.


The need for a less refractory frit becomes more evident in the Phase 1 Variation Stageassessment for this specific waste stream and compositional region. Based on model predictions,Frit 202 is not a candidate for the 100% washed nominal sludge; therefore, a Variation Stageassessment was not performed.

As discussed in the previous section (Nominal Stage assessment), coupling the 100% washednominal sludge with Frit 320 does provide an operational window (25 – 37%) with the systembecoming TL limited at higher waste loadings. This is consistent with the findings of Peeler et al.(2002a), which assessed the impact of the addition of Am/Cm and Pu/Gd on SB3. The results ofthe Variation Stage assessment indicate that Frit 320 is robust to compositional variation, as all365 EVs can be processed over a WL interval of 26 – 35%. Adding to this case, the resultsindicate that all 365 EVs have a minimum WL range of 11%.

The Variation Stage assessments of the alternative frits (416, 417, 418, and 419) indicate aresponse very similar to that of Frit 320. The WL ranges over which all 365 EVs can beprocessed are roughly the same for all four frits. Given Frit 320 has been “fritted” in support ofSB2 operations in DWPF, and assuming the alternative frits (416, 417, 418, and 419) can befritted, the frit selection process may be solely a function of melt rate. Although the availabilityof Frit 320 (assuming that not all is used during SB2 processing) may have some benefit in termsof a cost-benefit analysis.


39

7.0 Assessment of Decant Information (Phase 2):Nominal and Variation Stages

As previously stated, assessments were initially performed using the linear washing schemesprior to receiving projected sludge compositions as a function of washing (or decant) from HLWPE. Elder provided the compositional estimates of SB3 as a function of decant which formed thebasis for the Phase 2 assessments.14 The elemental concentrations provided by Elder wereconverted to an oxide basis (by multiplying by the appropriate gravimetric factor) and these datawere presented in Table 5-4.

Using the available PCCS process/product models, various frits will be assessed as a function ofSB3 washing. Given frits were developed and assessed for the linear washing scenarios, primarycandidates from that assessment will be assessed against the decant information. Compositionaladjustments will be made as necessary to account for the differences between the two sets ofsludge compositions. Table 7-1 provides a summary of the frit compositions used in the Phase 2Nominal and Variation Stage assessments for the decant information. As stated earlier, it is notthe intent of this study to recommend a frit to DWPF for SB3—only to provide insight into thefrit selection process.

In this section, assessments using the nominal SB3 decant information provided by Elder arediscussed using both the Nominal and Variation Stage strategies. The Nominal Stage assessmentwas performed on all 11 decant streams (Decant #5 – Decant #15). However, generation of 11sets of EVs and performing a full Variation Stage assessment of each frit for each EV set over aWL range of 25 – 60% would have been a time consuming and tedious process. A differentapproach was taken to define the EVs used in the Variation Stage assessment. Although analternative EV approach was taken, the Variation Stage strategy outlined in Section 3.0 did notchange.

14 Personal communication with H.H. Elder via email dated 7/30/02. Appendix A provides the data transmitted in the

personal communication (elemental wt%, calcine basis).

Imm

obil

izat

ion

Tec

hnol

ogy

Sect

ion

WSR

C-T

R-2

002-

0049

1Sa

vann

ah R

iver

Tec

hnol

ogy

Cen

ter

R

ev. 0

Wes

tingh

ouse

Sav

anna

h R

iver

Com

pany

40

Tab

le 7

-1.

Sum

mar

y of

Fri

t C

ompo

siti

ons

(in

wt%

oxi

des)

Use

d in

the

Nom

inal

and

Var

iati

on S

tage

sof

the

Dec

ant

(or

Pha

se 2

) A

sses

smen

ts

Oxi

deF

rit 4

06F

rit 4

05F

rit 4

09F

rit 4

10F

rit 4

20F

rit 4

21F

rit 4

22F

rit 4

23F

rit 2

02F

rit 4

11F

rit 4

12F

rit 4

16F

rit 3

20A

l 2O

3-

--

-1

1-

--

1-

1-

B2O

315

208

88

108

108

88

88

Li 2

O5

54

55

58

87

55

88

MgO

--

--

--

--

2-

--

-N

a 2O

--

65

77

33

612

1211

12S

iO2

8075

8282

7977

8179

7774

7572

72T

otal

100

100

100

100

100

100

100

100

100

100

100

100

100


41

7.1 Nominal Stage Assessment: Decant Information (Phase 2)

Projected operating windows (for the Nominal Stage assessment) for the fifteen decant scenariosare presented in Table 7-2 for each candidate frit composition over the waste loading range ofinterest (25 – 60 wt%). Initially, an in-depth discussion linking the details provided in AppendixE to the summary table (Table 7-2) is provided to demonstrate how the summary table wasdeveloped. This discussion will provide insight into the comparisons of the predicted propertiesto the acceptance criteria and the influence they have on establishing or defining the projectedoperational windows. Given the understanding of how the summary table was developed andknowing the extensive number of combinations that result when coupling the candidate frits withthe different decant scenarios, detailed discussions of other frit/sludge combinations will be brief,high level, and select. The primary focus will be on Decant #5 and Decant #9 given those havebeen established as focal points for both melt rate assessments and flow sheet developmentactivities by the SB3 technical team. Emphasis will be given to Frit 202 and Frit 320 given theirconsideration as “baseline” frits to this point. Alternative frits will be discussed to demonstratethe ability of frit development efforts to compensate for compositional changes based on thedegree of washing. Although a particular frit may not be specifically discussed in the followingsection, one should not rule out its potential use. Again, the discussions are intended to provideinsight into the how the summary table (Table 7-2) was developed and what information can beextracted and carried forward to the frit selection process. It must be recognized that theassessments and projected operational windows are based solely on model predictions – noexperimental work was performed.

Detailed information regarding the predicted properties for the nominal decant compositionswhen coupled with each candidate frit is provided in Appendix E. The column identified as“Type” summarizes the specific decant being evaluated with the second column (“Frit ID”)identifying the frit. The third column “Satisfies PAR” represents the comparison of the predictedproperties versus the PAR limits as shown in Table 4-1. The last two columns specify theminimum and maximum waste loadings over which the specific sludge/frit combinationpossesses the characteristics described by the “Satisfies PAR” nomenclature.

For example, consider Frit 202 coupled with the nominal Decant #5. Based on the informationpresented in Table 7-3 (information extracted from Appendix E), the WL interval over which thenominal Decant #5 composition could be processed is 33 – 39 wt%. Lower WLs (≤ 32 wt%) arerestricted by the homogeneity constraint (predictions indicate that this glass would beinhomogeneous – “Not Homog”). Durability predictions (“Not Durable”) prohibit WLs of 40%or higher.

Imm

obil

izat

ion

Tec

hnol

ogy

Sect

ion

W

SRC

-TR

-200

2-00

491

Sava

nnah

Riv

er T

echn

olog

y C

ente

r R

ev. 0

Wes

tingh

ouse

Sav

anna

h R

iver

Com

pany

42

Tab

le 7

-2.

Sum

mar

y of

Pro

ject

ed O

pera

tion

al W

indo

ws

for

the

Pha

se 2

Nom

inal

Sta

ge A

sses

smen

t of

the

Dec

ant

Com

posi

tion

s

Frit

406

Frit

405

Frit

409

Frit

410

Frit

420

Frit

421

Frit

422

Frit

423

Frit

202

Frit

411

Frit

412

Frit

416

Frit

320

Dec

ant #

5W

L (

nom

inal

)33

- 5

131

- 4

633

- 5

032

– 5

030

– 4

530

– 4

431

– 4

631

– 4

433

- 3

9no

neno

neno

neno

nelo

wer

lim

ithi

gh v

isc

Hom

oghi

vis

chi

vis

cH

omog

Hom

ogH

omog

Hom

ogho

mog

PCT

PCT

PCT

PCT

uppe

r lim

itlo

w v

isc

low

vis

cPC

TPC

T/lo

vis

cPC

TPC

TL

o vi

sclo

vis

cPC

TPC

TPC

TPC

TPC

T

Dec

ant #

6W

L (

nom

inal

)35

- 4

830

– 4

735

- 5

334

– 5

230

– 4

929

– 4

830

– 4

830

– 4

632

- 4

529

none

Non

eno

nelo

wer

lim

ithi

vis

cH

omog

hi v

isc

hi v

isc

Hi v

isc

Hom

ogH

omog

Hom

ogH

omog

Hom

ogH

omog

PCT

PCT

uppe

r lim

itT

LT

Llo

vis

clo

vis

cL

o vi

sclo

vis

clo

vis

clo

vis

clo

w v

isc

PCT

PCT

PCT

PCT

Dec

ant #

7W

L (

nom

inal

)36

- 4

230

– 4

137

- 5

235

– 5

231

- 5

128

– 4

929

– 5

029

– 4

831

– 4

728

- 3

829

- 3

5N

one

none

low

er li

mit

hi v

isc

hi v

isc

hi v

isc

hi v

isc

Hi v

isc

hi v

isc

Hom

ogH

omog

Hom

ogH

omog

Hom

og/P

CT

PCT

PCT

uppe

r lim

itT

LT

LT

LT

LL

o vi

sclo

vis

clo

vis

clo

vis

clo

w v

isc

PCT

PCT

PCT

PCT

Dec

ant #

8W

L (

nom

inal

)38

31 –

37

38 -

47

36 -

47

32 -

49

29 –

49

29 –

48

29 –

48

30 –

47

27 -

45

29 -

45

none

none

low

er li

mit

hi v

isc

hi v

isc

hi v

isc

hi v

isc

Hi v

isc

hi v

isc

hi v

isc

Hom

ogH

omog

Hom

ogH

omog

hom

ogPC

Tup

per

limit

TL

TL

TL

TL

TL

TL

TL

TL

TL

lo v

isc

Lo

visc

PCT

PCT

Dec

ant #

9W

L (

nom

inal

)no

ne32

– 3

439

- 4

438

- 4

433

- 4

630

– 4

530

– 4

528

– 4

529

– 4

426

- 4

628

- 4

626

- 3

8no

nelo

wer

lim

ithi

vis

chi

vis

chi

vis

chi

vis

cH

i vis

chi

vis

chi

vis

cH

omog

Hom

ogH

omog

Hom

ogho

mog

PCT

uppe

r lim

itT

LT

LT

LT

LT

LT

LT

LT

LT

Llo

vis

cL

o vi

sclo

vis

cPC

T

Dec

ant #

10W

L (

nom

inal

)no

neN

one

40 -

42

39 -

41

35 -

43

31 –

43

31 –

43

28 –

42

29 –

41

26 -

48

28 -

48

26 -

40

none

low

er li

mit

hi v

isc

hi v

isc

hi v

isc

hi v

isc

Hi v

isc

hi v

isc

hi v

isc

Hom

ogH

omog

Hom

ogH

omog

hom

ogPC

Tup

per

limit

TL

TL

TL

TL

TL

TL

TL

TL

TL

lo v

isc

Lo

visc

lo v

isc

lo v

isc

Dec

ant #

11W

L (

nom

inal

)no

neno

neno

neno

ne36

- 4

133

– 4

132

– 4

028

– 4

028

– 3

926

- 4

727

- 4

826

- 4

127

- 3

8lo

wer

lim

ithi

vis

chi

vis

chi

vis

chi

vis

chi

vis

chi

vis

chi

vis

chi

vis

cH

omog

Hom

ogH

omog

hom

ogH

omog

uppe

r lim

itT

LT

LT

LT

LT

LT

LT

LT

LT

LT

LT

Llo

vis

clo

vis

c

Dec

ant #

12W

L (

nom

inal

)no

neno

neno

neno

ne37

- 3

934

– 3

933

– 3

930

– 3

828

– 3

725

- 4

527

- 4

625

- 4

227

- 4

0lo

wer

lim

ithi

vis

chi

vis

chi

vis

chi

vis

chi

vis

chi

vis

chi

vis

chi

vis

chi

vis

c-

Hom

og-

Hom

ogup

per

limit

TL

TL

TL

TL

TL

TL

TL

TL

TL

TL

TL

lo v

isc

lo v

isc

Dec

ant #

13W

L (

nom

inal

)no

neno

neno

neno

ne38

35 –

38

34 –

37

30 –

37

28 –

36

25 -

43

26 -

44

25 -

43

26 -

41

low

er li

mit

hi v

isc

hi v

isc

hi v

isc

hi v

isc

Hi v

isc

hi v

isc

hi v

isc

hi v

isc

hi v

isc

Hom

og-

Hom

ogup

per

limit

TL

TL

TL

TL

TL

TL

TL

TL

TL

TL

TL

lo v

isc

lo v

isc

Dec

ant #

14W

L (

nom

inal

)no

neno

neno

neno

neN

one

3635

– 3

631

– 3

629

- 3

525

- 4

226

- 4

325

- 4

426

- 4

2lo

wer

lim

ithi

vis

chi

vis

chi

vis

chi

vis

cH

i vis

chi

vis

chi

vis

chi

vis

chi

vis

c-

Hom

og-

Hom

ogup

per

limit

TL

TL

TL

TL

TL

TL

TL

TL

TL

TL

TL

lo v

isc/

TL

lo v

isc

Dec

ant #

15W

L (

nom

inal

)no

neno

neno

neno

neN

one

Non

eN

one

33 –

34

30 -

33

25 -

41

26 -

41

25 -

42

26 -

43

low

er li

mit

hi v

isc

hi v

isc

hi v

isc

hi v

isc

Hi v

isc

hi v

isc

hi v

isc

hi v

isc

hi v

isc

-ho

mog

-ho

mog

uppe

r lim

itT

LT

LT

LT

LT

LT

LT

LT

LT

LT

LT

LT

Llo

vis

c

Imm

obil

izat

ion

Tec

hnol

ogy

Sect

ion

W

SRC

-TR

-200

2-00

491

Sava

nnah

Riv

er T

echn

olog

y C

ente

r R

ev. 0

Wes

tingh

ouse

Sav

anna

h R

iver

Com

pany

43

Tab

le 7

-3. N

omin

al S

tage

Ass

essm

ent f

or D

ecan

t #5

and

Fri

t 20

2ov

er th

e W

aste

Loa

ding

Ran

ge o

f 25

– 6

0%

Typ

eF

rit I

DS

atis

fies

PA

RM

in(S

ludg

e L

oadi

ng (

%))

Max

(Slu

dge

Loa

ding

(%

))D

ecan

t #5

202

Dur

able

; Vis

c; N

ot H

omog

; New

TL

; Al2

O3;

alk

ali

2532

Dec

ant #

520

2D

urab

le; V

isc;

Hom

og; N

ew T

L; A

l2O

3; a

lkal

i33

39D

ecan

t #5

202

Not

Dur

able

; Vis

c; H

omog

; New

TL

; Al2

O3;

alk

ali

4043

Dec

ant #

520

2N

ot D

urab

le; N

ot L

Vis

c; H

omog

; New

TL

; Al2

O3;

alk

ali

4460


44

Table 7-2 provides a summary of the acceptable operational windows for each decant/fritcombination based on model predictions. Three rows of information are supplied in Table 7-2.The first row is the WL interval over which both process and product performance criteria areacceptable. The second and third rows provide the criterion that restricts access to lower andupper waste loadings respectively. Those frit/decant combinations that provide an operationalwindow (albeit a single WL for select combinations) are shaded in gray. In general, theoperational windows of interest shift from left to right (in terms of candidate frit compositions) asone proceeds from Decant #5 to Decant #15 (or the degree of washing increases). As wasobserved with the linear washing assessments (see Section 6.1), this shift can be attributed to thevariable Na2O sludge concentration and the compensation taken in terms of frit developmentefforts. In general, as one proceeds from left to right in Table 7-2, the frits become less refractory(more alkali-rich) to account for the depletion of alkali in the more advanced washed sludges(higher decant numbers). For those frit/decant combinations in which model predictions do notproject an operational window, the limiting acceptance criteria are also provided for both theupper and lower WLs.

As previously stated, the primary focus will be on Decant #5 and Decant #9 given those havebeen established as focal points for both melt rate assessments and flow sheet developmentactivities by the SB3 technical team. Emphasis will also be given to Frit 202 and Frit 320 giventheir consideration as “baseline” frits to this point. Alternative frits will be discussed todemonstrate the ability of frit development efforts to compensate for compositional changesbased on the degree of washing. Although a particular frit may not be specifically discussed inthe following section, one should not rule out its potential use.

7.1.1 Decant #5

As shown in Table 7-2, projected operational windows exist for several frits. In general,predictions of either homogeneity or high viscosity define the lower WLs for each system. Theupper WL limits are defined by predictions of either low viscosity or durability. As with the lesswashed sludges in the linear washing assessments, challenges to durability and/or low viscosityprovide some indication that the frit development effort is taking advantage of the high alkalicontent of Decant #5. It should be noted that predictions of TL do not limit any of the Decant #5-based systems.

As previously discussed, an acceptable WL interval of 33 – 39% is projected for the Frit202/Decant #5 system with the lower and upper WLs being homogeneity and durability limited,respectively. Minor compositional adjustments to Frit 202 were made initially to provide insightinto the potential to improve the upper waste loading limit. Given the Frit 202 system wasdurability limited at WLs exceeding 39%, 1% of the total alkali content was removed andreplaced with Al2O3 to form Frit 420. Not only was the 1% alkali removed but also the ratio ofNa2O/Li2O was adjusted. This compositional adjustment resulted in a projected operationalwindow of 30 – 45% – not only improving the upper WL limit but the lower WL limit as wellproviding an overall larger window for processing. This larger operational window wouldprovide DWPF with more flexibility in terms of operational control. Although a largeroperational window exists for Frit 420, the system is still limited by predictions of homogeneityand PCT for the lower and upper WLs, respectively.

A second compositional adjustment was made to Frit 202 and/or Frit 420 to address a potentiallynon-technical issue. If a frit containing 8 wt% B2O3 (such as Frit 202, Frit 420, or Frit 320) isutilized, at WLs of ~38 wt%, the total B2O3 content in the glass approaches 5 wt%. If restricted


45

to borosilicate glass by the Waste Acceptance Product Specification (WAPS) (Plodinec et al.1995) and the current ASTM definition of a borosilicate glass is taken literally, WLs exceeding~38% would yield a glass composition containing less than 5% B2O3 (not accounting formeasurement uncertainties). This could potentially (and unnecessarily) restrict the acceptableWL range and limit DWPF operational flexibility. With the potential implication of restrictinghigher waste loadings, this becomes a more significant issue.

With Frit 202 and Frit 420 providing upper WLs of 39 and 45% respectively, application of the“borosilicate” definition may impose unnecessary limitations on the upper WL that could beachieved. Frit 421 was developed to address this potential issue. The B2O3 content in Frit 421 is10% which would require WL in excess of 50% to reduce the B2O3 content in glass to less than5% (ignoring measurement uncertainties). The results of the Phase 2 Nominal Stage assessmentwith Frit 421 and Decant #5 indicate that the increased B2O3 content (at the expense of SiO2) doeshave a slight negative impact on the upper WL limit (reduced from 45% with Frit 420 to 44%with Frit 421). However, at the upper WL of 44%, the B2O3 concentration in glass would be~5.6% meeting the ATSM definition (ignoring measurement uncertainties). These resultsindicate that slight modifications to Frit 202 can be made to improve the upper waste loadings(based on model predictions) and to address the definition of a “borosilicate” glass (if needed).Melt rate assessments may differentiate or play a significant role in the frit selection process ifone of these three frits is considered (assuming the modified compositions can be fritted).

Frits 422 and 423 were developed given the potential uncertainties or implications of having asystem being durability limited at the upper WL. Although the authors feel that having adurability limited system is of minimal concern given the conservatism built into the ∆GP

acceptance criteria, compositional adjustments to the frit can be made to shift the Decant #5-based system to be low viscosity limited (e.g., viscosity predictions at the upper WL exceed thelow viscosity limit as defined in Table 7-2). A minor reduction in the total alkali content (relativeto Frit 202) and a change in the alkali ratio were the primary bases for Frit 422. Frit 423 alsoaddressed the potential “borosilicate” issue given the upper WL with Frit 422 (with 8% B2O3)greatly exceed the ~38% level. As with the Frit 202 modifications, large operational windows areprojected for Frits 422 and 423 with upper WLs of 46 and 44%, respectively. Like theobservations in the Frit 202-based modifications, there appears to be a slight negative impact onthe upper WL limit as one increases the B2O3 concentration (at the expense of SiO2) in frit.

Results of the Phase 1 assessments with the linear washed nominal sludge compositions and EVs(see Section 6.0) indicated that Frits 405 and 406 were relatively robust to both the 0% and 25%washed cases. Given this high degree of flexibility for these frits and the fact that the Decant #5composition lies between these two washed sludges (for the major oxides), the large projectedoperational windows for Decant #5 are not surprising. Frit 405 and 406 yield upper WL limits of46 and 51% respectively. Given their high B2O3 concentrations, the non-technical issue ofproducing a borosilicate glass is not challenged with either frit over the acceptable WL range.Assessments of melt rate or frittability are needed to further evaluate their potential application toSB3 during the frit selection process.

Frits 409 and 410 were developed with the intent that Frit 202 may contain slightly too muchalkali for this particular decant. More specifically, given Frit 202 was developed as a “generic”coupled operations frit (with coupled operations providing a higher alkali content than the currentsludge-only flowsheet), frit development efforts were undertaken to investigate the potential toreduce the total alkali content of Frit 202 to enhance the upper waste loading limit whilemaintaining a frittable frit with high melt rates. Based on model predictions, Frits 409 and 410 do


46

improve the upper WL limit achievable (both indicating 50% WL) relative to Frit 202 (upper WLlimit of 39%). Upper WLs for Frit 409 and 410 are both 50% with each system being durabilitylimited at higher WLs. This indicates that the high alkali content of the sludge can becompensated for via frit development efforts to improve operational flexibility for DWPF. Theseresults give support for the concept of developing specific frits for specific sludges to optimizeoperational windows. However, imposition of the “borosilicate” definition, would have asignificant impact on the WL ranges of interest – eliminating WLs of 38% or greater fromconsideration.

It should be reiterated that although Frit 202 was developed for the “generic” coupled operationsflowsheet, model predictions (as summarized in Table 7-2) indicate that its use is feasible for thisspecific (and nominal) decant. The fact that larger operational windows can be developed bytargeting a specific waste stream should be expected. It should also be noted that the Phase 2Nominal Stage assessment indicates that Frit 202 provides an operational window for each decantsludge composition listed (one of four frits demonstrating this flexibility; the others being Frits421, 422, and 423). This observation demonstrates the robustness of these frits to handle a widerange of targeted decants recognizing that these are nominal compositions that do not account forcompositional variation. The Variation Stage assessment will provide further insight.

Frit 320 should also be mentioned given its classification as a “baseline” frit by Elder. ForDecant #5, model predictions do not provide an operational window for Frit 320. Predictions ofdurability limit all potential waste loadings of interest. Frits 411, 412, and 416 also fall into thiscategory for Decant #5 – durability limited based on model predictions. Given Frit 320 wasdeveloped to improve melt rate for SB2, its generic application to other sludge batches should bemade with caution. From the summary information presented in Table 7-2, Frit 320 onlybecomes a possible candidate once Decant #11 and more advanced washed sludges are obtained.

7.1.2 Decant #9

General observations for the Decant #9 Phase 2 Nominal Stage assessment indicate that the Na2Oconcentration in the nominal waste stream is being reduced to the point that a frit change may berequired. Although there are frits that can obviously tolerate the compositional range presentedby the two nominal streams of interest, alternative frits (Frits 411, 412, and 416 which are notfeasible with Decant #5) become possible candidates for this more washed sludge. All of theDecant #9/alternative frit (Frits 411, 412, and 416) combinations have projected operationalwindows with upper WLs ranging between 38 – 46%. It should also be noted that the glassformulation strategy of shifting the WL-limiting property to be non-TL based was successful forthese glasses. In all cases, the upper WL is limited by predictions of low viscosity reinforcing theconcept of the need for frit composition compensations as a function of washing. For the otherDecant #9 based systems, the upper WL is TL limited as a result of coupling the alkali-depletedsludge with an alkali-depleted frit.

The use of Frit 320 is still prohibited by predictions of durability. Select frits that werecandidates for Decant #5 are either prohibited (Frit 406) or provide extremely small operationalwindows (Frit 405 with a 32 – 34% WL interval) even for this nominal stream.

Use of Frit 202 provides a projected operational window of 29 – 44%. Although this WL intervalis very attractive it should be tempered with the potential issue of the borosilicate glass definition.That is, given only 8% B2O3 in the frit, WLs would be restricted to < 38% to produce a glass with


47

≥ 5% B2O3. Frit 421 (with 10% B2O3) not only addresses this issue but shifts the acceptable WLinterval to 30 – 45%.

In general, the typical WL interval projected for the Decant #9 nominal composition is ~30 –45% irrespective of frit compositions (a few exceptions exist). Therefore, the frit selectionprocess may hinge upon other key criteria such as melt rate and/or frittability. Availability (in thecase of Frit 202) may also play a role. However, prior to making a decision based solely on thePhase 2 Nominal Stage assessments, the response or tolerance to anticipated sludge variationshould be considered.

7.2 Variation Stage Assessment: Decant Information (Phase 2)

In the previous section, projected operational windows were developed for various fritcompositions based on the nominal decant information provided by Elder. Assessment of theprojected operational windows accounting for compositional variation will reduce the risk ofselecting a frit that will be intolerant of this anticipated change.

The Phase 1 Variation Stage assessment (see Section 6.2) for the linear washed sludges was basedprimarily on EVs determined for each nominal washing scenarios with a ±10% variation aroundeach major oxide. Assessments were made using the PCCS models currently implemented inDWPF over the WL interval of interest (25 – 60 wt%). Considering the large number of nominaldecants provided, generation of 11 sets of EVs, and performing a full assessment of each frit/EVset over a WL range of 25 – 60% would be a time consuming and tedious process. Therefore aslightly different approach was taken in terms of defining EVs for this assessment.

In the early stages of the SB3 integrated flowsheet development, no obvious technical issues wereidentified that could be used to eliminate a particular decant or range of decants.15 Therefore,glass formulation efforts were undertaken to maintain a bounding approach in an attempt toprovide as much information as possible for the frit selection process given the unknownsassociated with the targeted decant or washing strategy. To gain insight into the tolerance of eachfrit composition to potential sludge variation, two sets of EVs were generated. Upper and lowerbounds (using ±10% for each major oxide) were established for Decants #7 and Decant #12 (seeTable 7-4). These two decants were selected given the upper and lower ranges for each boundedtwo distinct (but overlapping) nominal decant ranges. The EVs associated with Decant #7 boundthe nominal Decant #5 and nominal Decant #11 compositions. The EVs associated with Decant#12 bound the nominal Decant #7 and Decant #15 compositions. Although Decant #5 or Decant#9 were not specifically evaluated , use of the respective set of overlapping EVs will provideinsight into the ability of each frit to handle compositional variation.16 It should be noted that theNa2O values between the two different sets of EVs do not overlap.

15 The decision to assess the EVs associated with Decants #7 and Decant #12 were made prior to the SB3 team

focusing the melt rate and flow sheet development efforts on Decant #5 and Decant #9. Given that, this report willfocus primarily on the Variation Stage assessment for Decant #7’s EVs.

16 In Sections 7.2.3 and 7.2.4, a Phase 2 Variation Stage assessment is performed focused solely on Decants #5 and #9,respectively.


48

Table 7-4. Minimum and Maximum Values for Decants #7 and #12 Used to Define EVs(wt% oxides).

Oxide Decant #7 Decant #12Min Nominal Max Min Nominal Max

Al2O3 13.299 14.777 16.255 14.628 16.253 17.879B2O3 0.000 0.000 0.000 0.000 0.000 0.000BaO 0.184 0.204 0.225 0.202 0.225 0.247CaO 2.646 2.940 3.234 2.910 3.234 3.557Ce2O3 0.256 0.285 0.313 0.282 0.313 0.345Cr2O3 0.272 0.302 0.332 0.299 0.332 0.366Cs2O 0.000 0.000 0.000 0.000 0.000 0.000CuO 0.146 0.162 0.178 0.160 0.178 0.196Fe2O3 29.572 32.858 36.144 32.527 36.141 39.755K2O 0.316 0.352 0.387 0.348 0.387 0.425La2O3 0.169 0.187 0.206 0.185 0.206 0.227Li2O 0.000 0.000 0.000 0.000 0.000 0.000MgO 0.139 0.154 0.169 0.152 0.169 0.186MnO 5.274 5.860 6.446 5.801 6.446 7.091MoO3 0.000 0.000 0.000 0.000 0.000 0.000Na2O 23.914 26.571 29.228 17.311 19.235 21.158Nb2O3 0.000 0.000 0.000 0.000 0.000 0.000NiO 1.183 1.314 1.445 1.301 1.445 1.590PbO 0.221 0.245 0.270 0.243 0.270 0.297SiO2 1.540 1.711 1.882 1.694 1.882 2.070ThO2 0.105 0.117 0.129 0.116 0.129 0.141TiO2 2.069 2.299 2.529 2.276 2.529 2.782U3O8 7.485 8.316 9.148 8.233 9.147 10.062Y2O3 0.000 0.000 0.000 0.000 0.000 0.000ZnO 0.302 0.336 0.369 0.332 0.369 0.406ZrO2 0.546 0.607 0.667 0.601 0.667 0.734

Although EVs were not considered for each specific decant, the Variation Stage strategy utilizedwas consistent with that defined in Section 3.0 and outlined in Figure 3-2. The three metricsdefined above were developed to gain insight into the robustness of candidate frits to sludgevariation.

Detailed information regarding the predicted properties for the Decant #7 EV-based sludgecompositions when coupled with select candidate frits is provided in Appendix F. The columnidentified as “Sludge Loading (%)” summarizes the specific waste loading of interest. It shouldbe noted that there are typically more than one row for each sludge loading given the predictedproperties for all EVs will vary dramatically. The second column in Appendix F (“SatisfiesPAR”) represents the comparison of the predicted properties versus the PAR limits as shown inTable 4-1. In this column, properties deemed unacceptable with respect to the PAR acceptancelimits are preceded by “Not”. For example, “Not Homog” indicates that glasses fail thehomogeneity PAR criteria. The last column (“# of EVs”) summarizes the number of EVs whosecommon property predictions are classified by the “Satisfies PAR” column.


49

A detailed discussion for the Frit 202-based EVs is provided below to demonstrate how theinformation in Appendix F can be translated to provide insight into the robustness of each frit toanticipated sludge variation. More specifically, this detailed discussion will outline the processused to define the three metrics and translate how these results impact the frit selection process.

Consider Table 7-5 (extracted from Appendix F) for the summary of the Variation Stageassessment for Frit 202 and the Decant #7 EVs. At WLs of 25 – 26%, all 915 EVs areunacceptable due to predictions of the resulting glasses being inhomogeneous. At 27% WL, 22of the 915 EVs are acceptable with the remaining 893 being classified as inhomogeneous.Predictions of homogeneity continue to restrict processing of select EVs through WLs of ≤ 34%.

Between 35 and 40% WL, all 915 EVs are acceptable and could be processed based on acomparison of the predicted properties and the PAR acceptance criteria established in Section 4.0.A review of each WL indicates that the projected operational window for this Frit 202-basedsystem is between 35 – 40%. At 41% WL, predictions of TL (“Not TL”) limit 4 of the 915 EVsfrom being processed. Durability predictions begin to restrict the acceptability of select glasses at43%. Predictions of low viscosity and TL become limiting factors at 44%.

An effective method to identify potential WLs or WL intervals in which all 915 EVs may beprocessed is to scan the “# of EVs” column for 915 then evaluate the “Satisfies PAR” column toassure that all predicted properties are acceptable (“Not” should be absent from that row).

Also provided below the detailed assessment in Appendix F is a summary table for each systembeing evaluated. This summary table has been extracted from the appendix for the Frit 200 basedsystem (see Table 7-6). The columns shown in this table are “WL Range”, “# of EVs andCentroid” and “% of total”. This summary table helps to define the second and third metrics forthe Variation Stage assessments. The “WL Range” columns indicates a waste loading range (i.e.,“0” indicates no interval, “1” indicates a 1% WL interval, etc…) but does not specify theparticular interval. The “# of EVs and Centroid” column indicates the number of EVs (out of the915) that are processable within the corresponding WL interval. The third column provides thepercentage of the 915 EVs. Consider the “WL Range” column for the Decant #7 EVs and Frit202. The initial value for “WL Range” is “8”. The fact that a “0” is not shown confirms the factthat all of the 915 EVs could be processed at some WL. In fact, each EV has a minimum wasteloading range of 8% within the 25 – 60% window being evaluated.

To summarize the Variation Stage assessment for the Frit 202, Decant #7 EVs, a WL range of 35– 40% is available over which all 915 EVs can be processed. All 915 of the EVs can beprocessed at some waste loading of interest with the minimum WL range being 8 wt%. Theseresults suggest that Frit 202 is extremely robust to the compositional variation presented by theEVs associated with Decant #7. Given that the minimums and maximums used to define the EVsencompass the nominal Decant #5 through the nominal Decant #12 compositions, Frit 202 is acandidate for this compositional envelope (based solely on the model assessments).


50

Table 7-5. Variation Stage Results for Decant #7 with Frit 202

Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 91526 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 91527 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 2227 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 89328 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 12428 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 79129 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 28229 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 63330 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 47030 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 44531 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 53131 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 38432 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 77732 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 13833 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 85733 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 5834 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 89734 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 1835 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91536 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91537 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91538 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91539 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91540 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91541 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91141 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 442 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 86442 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 5143 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 73943 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 13943 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 3744 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 744 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 56944 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 25044 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 8945 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 3545 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 39245 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 35045 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 8545 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 5346 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 3646 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 446 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 29246 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 39646 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 16046 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 2747 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 16547 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 4247 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 7147 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 38047 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 25748 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 12748 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 20048 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 2648 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 24248 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 32049 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 7649 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 287


51

Sludge Loading (%) Satisfies PAR # of EVs49 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 349 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 16949 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 38050 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 5450 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 42250 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 4250 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 39751 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 3951 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 47051 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 40652 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 2352 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 47552 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 41652 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 153 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 553 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 48253 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 42353 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 554 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 154 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 47554 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 40554 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 3455 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 46755 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 35455 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 9456 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 45856 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 30556 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 15257 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 44857 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 19957 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 26858 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 43958 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 13958 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 33759 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 43159 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 6559 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 41960 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 42260 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 3060 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 463

Table 7-6. Summary of the Frit 202 Decant #7 Variation Stage Assessment

WL Range # of EVs andCentroid

% of Total

8 12 1.319 24 2.62

10 16 1.7511 26 2.8412 39 4.2613 47 5.1414 163 17.8115 318 34.7516 178 19.4517 76 8.3118 16 1.75


52

7.2.1 Decant #7 EV Assessment

Table 7-7 summarizes the results of the Variation Stage assessment in terms of the three metricsfor the various decant EVs/frit combinations. Also shown in Table 7-7 are the results of thePhase 2 Nominal Stage assessment for completeness for the two decants being considered. Itmust be recognized that the assessments and projected operational windows are based solely onmodel predictions – no experimental work was performed.

In this section, some general observations are reported based on the summary informationpresented in Table 7-7. As discussed in detail above, Frit 202 should be considered a candidatefrit for the compositional region covered by the EVs representing Decant #7. All of the EVs canbe processed over a 35 – 40% WL range. All 915 of the EVs can be processed at some wasteloading of interest with the minimum WL range being 8%. These results suggest that Frit 202 isextremely robust to the compositional variation presented by the EVs associated with Decant #7.

The modifications made to Frit 202 (e.g., Frit 420 and Frit 421) also demonstrate a high degree offlexibility to process the Decant #7 EVs. Use of both Frit 420 and Frit 421 extended not only theupper WL range (relative to Frit 202) but the lower WL as well. Model predictions indicate thatFrit 421 has the largest window of the three with all of the EVs being processable over a WLrange of 32 – 42%. Although low WLs may not be of interest, having a larger operating windowmay prove advantageous. For Frit 420 and Frit 421, the minimum WL interval over which all ofthe EVs could be processed is 10 and 13%, respectively. Use of Frit 421 could address the non-technical issue of producing a borosilicate glass given its relatively high concentration of B2O3.

Frits 422 and 423 also demonstrate a high tolerance for the compositional envelope encompassedby the Decant #7 EVs. The projected WL interval for the Frit 422 system is 33 – 42%. The Frit423 based system yields a WL interval of 33 – 41% over which all of the EVs can be processed.The minimum WL interval for each EV for both systems is 14%.

Although Frits 409 and 410 provide operational windows for this set of EVs, the window sizesare less attractive. Frit 410 provides a WL interval of 38 – 41% over which all of the EVs couldbe processed while only a 40 – 41% window exists for the Frit 409-based EVs. Frit 410 mayprovide a slight advantage relative to Frit 409 given that 100% of the EVs have a minimum WLrange of 5%. The Frit 409-based assessment indicates that ~97% of the EVs have a minimumoperating window of 5%.

Although a WL range existed for Frits 405 and 406 when the nominal Decant #7 waste streamwas considered (see Table 7-2), when one accounts for the compositional variation, the metricsindicate that these frits are less attractive as compared to other frits. More specifically, the threemetrics provide an indication that use of either Frit 405 or Frit 406 would be less tolerant tocompositional variation relative to other frits. For both systems, there is no WL range over whichall of the EVs could be processed (as indicated by the “none” in Table 7-7). Approximately 58%of the EVs could be processed at some WL using Frit 406 while nearly all of the EVs (99.7%)could be processed at some WL with Frit 405. The percentage of EVs with a minimum WLrange of 5% is less than 70% for both frits. Based on these results, the use of Frits 405 or 406 forthis compositional region should be considered a low probability (all other factors being equalsuch as melt rate).

Imm

obil

izat

ion

Tec

hnol

ogy

Sect

ion

W

SRC

-TR

-200

2-00

491

Sava

nnah

Riv

er T

echn

olog

y C

ente

r R

ev. 0

Wes

tingh

ouse

Sav

anna

h R

iver

Com

pany

53

Tab

le 7

-7.

Sum

mar

y of

Fri

t C

ompo

siti

ons

(in

wt%

oxi

des)

Use

d in

the

Pha

se 2

Nom

inal

and

Var

iati

on S

tage

Dec

ant

#7 A

sses

smen

t.

Oxi

deF

rit 4

06F

rit 4

05F

rit 4

09F

rit 4

10F

rit 4

20F

rit 4

21F

rit 4

22F

rit 4

23F

rit 2

02A

l 2O

3-

--

-1

1-

--

B2O

315

208

88

108

108

Li 2

O5

54

55

58

87

MgO

--

--

--

--

2N

a 2O

--

65

77

33

6S

iO2

8075

8282

7977

8179

77T

otal

100

100

100

100

100

100

100

100

100

Dec

ant #

7Fr

it 4

06F

rit 4

05F

rit 4

09F

rit 4

10F

rit 4

20F

rit 4

21F

rit 4

22F

rit 4

23F

rit 2

02

Nom

inal

WL

(no

min

al)

36 –

42

30 –

41

37 –

52

35 –

52

31 –

51

28 –

49

29 –

50

29 –

48

31 –

47

Var

iatio

nW

L a

ll E

Vs

Non

eN

one

40 –

41

38 –

41

34 –

42

32 –

42

33 –

42

33 –

41

35 –

40

% E

Vs

at s

ome

WL

57.7

%99

.7%

100.

0%10

0.0%

100.

0%10

0.0%

100.

0%10

0.0%

100.

0%W

L o

f 5%

or

grea

ter

50.3

%67

.8%

96.8

%10

0.0%

100.

0%10

0.0%

100.

0%10

0.0%

100.

0%M

inim

um W

L r

ange

--

-5%

10%

13%

14%

14%

8%


54

7.2.2 Decant #12 EV Assessment

Table 7-8 summarizes the results of the Phase 2 Variation Stage assessment for the Decant #12EVs. Values for the three metrics are provided for each frit/sludge combination of interest. Alsoshown in Table 7-8 are the results of the Decant #12 Phase 2 Nominal Stage assessment forcompleteness. It must be recognized that the assessments and projected operational windows arebased solely on model predictions – no experimental work was performed.

Detailed information regarding the predicted properties for the Decant #12 EV-based sludgecompositions when coupled with each candidate frit is provided in Appendix G. The columnidentified as “Sludge Loading (%)” summarizes the specific waste loading of interest. It shouldbe noted that there are typically more than one row for each sludge loading given the predictedproperties for all 849 EVs will vary dramatically. The second column in Appendix G (“SatisfiesPAR”) represents the comparison of the predicted property versus the PAR limits as shown inTable 4-1. In this column, properties deemed unacceptable with respect to the PAR acceptancelimits are preceded by “Not”. The last column (“# of EVs”) summarizes the number of EVswhose common property predictions are classified by the “Satisfies PAR” column. An effectivemethod to identify potential WLs or WL intervals in which all 849 EVs can be processed is toscan the “# of EVs” column for 849 then evaluate the “Satisfies PAR” column to assure that allpredicted properties are acceptable (“Not” should be absent from that row).

The WL interval over which all 849 EVs can be processed with Frit 202 is relatively small (31 –32%). Metric #2 indicates that all of the EVs can be processed at some WL with 90.6% of theEVs having a minimum WL range of 5% (metric #3). The frits based on slight modifications toFrit 202 (Frit 420 and Frit 421) have very similar responses to the applied compositionalvariation. There is no WL or WL interval over which all the EVs could be processed. Theassessment indicates that 57.6% and 85.6% of the EVs could be processed at some WL with35.5% and 51.8% having a minimum 5% WL range for Frit 420 and Frit 421, respectively. Theless than perfect response of these three frits to the compositional variation indicates that thesemay not be primary candidates for this particular compositional envelope. The EVs defining thisregion include relatively low alkali concentrations which when coupled with more refractory fritstend to challenge the predicted TL and/or high viscosity acceptance criteria – see Appendix G.

Assessment of Frits 422 and 423 provide similar trends with the Frit 202-based systems (Frits202, 420, and 421). No WL or WL interval exists over which all 849 EVs can be processed withFrit 422. With Frit 423, although no interval is observed, all EVs could be processed at 33% WL– an extremely narrow operational window. Metrics #2 and #3 suggest that Frit 423 is slightlymore flexible given that 100.0% of the EVs are processable at some WL and 82.8% have aminimal WL range of 5%. This compares to the corresponding metric responses for Frit 422 of85.4% and 52.2%. With the only difference between the two frits being a 2% B2O3 for SiO2

adjustment, this suggests that the increased B2O3 concentration provides a slightly more flexiblesystem.

When the more alkali-rich frits (Frit 411, 412, and 416) are considered, the operational windowsbecome much more favorable and the overall robustness of the frits to compositional variationincreases. Consider Frits 411, 412, and 416 in which the WL intervals over which all 849 EVscould be processed are 28 – 39%, 30 – 40%, and 28 – 38%, respectively. The third metricsuggests that the minimum WL range for each EV is extremely high: 15%, 15%, and 12% forFrits 411, 412, and 416, respectively. The results of the Phase 2 Variation Stage assessment


55

indicate that if a higher washed sludge is targeted, Frit 411, 412, and 416 should be primarycandidates during the frit selection process (based solely on the paper study assessments).

An interesting comparison is the results of the Variation Stage assessment between Frit 320 andFrit 416. As discussed in an earlier section, Frit 416 was developed in response to theoverwhelmingly negative response of Frit 320 to the predicted durability for several of the linearwashing scenarios. The strategy for Frit 416 was to increase predicted durability by slightlylowering the total alkali content and adding Al2O3. Although a minor adjustment was made (1%reduction in Na2O content added as Al2O3) the impact on the projected operational windows wassignificant. For Frit 320 and Decant #12, there is no window over which all 849 EVs can beprocessed. A review of the information provided in Appendix G indicates that durabilitypredictions are the primary limitations over the 25 – 60% WL interval. Frit 416 provides a 28-38% WL interval over which all EVs could be processed with 100% of the EVs having aminimum WL range of 12%. This is a significant improvement in the ability of the frit to handlethe applied compositional variation with a minor change in frit composition.

Since the original decision was made to focus the Phase 2 Variation Stage assessment aroundDecants #5 and #12, the SB3 Technical team more recently decided to narrow the focus to spanthe range bounded by Decant #5 through Decant #9. The latter decision was made based on thelack of identifying any significant technical issues during the initial stages of the SB3 flowsheetdevelopment activities. Washing the sludge less does have advantages in terms of significanttime and labor savings in the pretreatment/retrieval operation. A reduced washing campaignshould also result in less water being sent to the evaporators. Conversely, targeting a morewashed sludge should reduce the total number of canisters produced by some incremental amountand may minimize components that have potentially negative impacts to either WL orprocessability (such as SO4). A cost-benefit analysis should be performed to fully understand theadvantages and disadvantages of selecting a targeted washing scenario. Even though the SB3team did not have access to a detailed cost-benefit analysis, they elected to narrow thedecant/washing focus to span a range covered by Decant #5 through Decant #9. Given thisdecision, the Variation Stage assessments for Decant #7 (Section 7.2.1) and the linear washingcases of 0%, 25% and perhaps 50% (see Section 6.2) are extremely valuable in terms ofidentifying potential frits to carry forward in the melt rate and frittability assessment leading intothe frit selection process. This latter statement does not suggest that the other assessments (boththe nominal and variation stages) are not valuable.

Given this decision and recognizing that the Variation Stage was not assessed for Decants #5 or#9 specifically, the frit development team decided to perform these assessments. Table 7-9summarizes the results of the Variation Stage assessment for the Decant #5 EVs. Table 7-10summarizes the results of the Variation Stage assessment for the Decant #9 EVs. Values for thethree metrics are provided for each frit/sludge combination of interest. Also shown in theirrespective tables are the results of the Phase 2 Nominal Stage assessments for completeness. Itmust be recognized that the assessments and projected operational windows are based solely onmodel predictions – no experimental work was performed.

Imm

obil

izat

ion

Tec

hnol

ogy

Sect

ion

W

SRC

-TR

-200

2-00

491

Sava

nnah

Riv

er T

echn

olog

y C

ente

r R

ev. 0

Wes

tingh

ouse

Sav

anna

h R

iver

Com

pany

56

Tab

le 7

-8. S

umm

ary

of F

rit

Com

posi

tion

s (i

n w

t% o

xide

s) U

sed

in th

e P

hase

2 N

omin

al a

nd V

aria

tion

Sta

ge D

ecan

t #1

2 A

sses

smen

t

Oxi

deF

rit 4

20F

rit 4

21F

rit 4

22F

rit 4

23F

rit 2

02F

rit 4

11F

rit 4

12F

rit 4

16F

rit 3

20A

l 2O

31

1-

--

1-

1-

B2O

38

108

108

88

88

Li 2

O5

58

87

55

88

MgO

--

--

2-

--

-N

a 2O

77

33

612

1211

12S

iO2

7977

8179

7774

7572

72T

otal

100

100

100

100

100

100

100

100

100

Dec

ant #

12Fr

it 4

20F

rit 4

21F

rit 4

22F

rit 4

23F

rit 2

02F

rit 4

11F

rit 4

12F

rit 4

16F

rit 3

20

Nom

inal

WL

(no

min

al)

37 –

39

34 –

39

33 –

39

30 –

38

28 –

37

25 –

45

27 –

46

25 –

42

27 –

40

Var

iatio

nW

L a

ll E

Vs

Non

eN

one

Non

e33

31 –

32

28 –

39

30 –

40

28 –

38

Non

e%

EV

s at

som

e W

L57

.6%

85.6

%85

.4%

100.

0%10

0.0%

100.

0%10

0.0%

100.

0%88

.1%

WL

of

5% o

r gr

eate

r35

.5%

51.8

%52

.2%

82.8

%90

.6%

100.

0%10

0.0%

100.

0%85

.5%

Min

imum

WL

ran

ge-

--

--

15%

15%

12%

-


57

7.2.3 Phase 2 Variation Stage: Decant #5

Detailed information regarding the predicted properties for the Decant #5 EV-based sludgecompositions when coupled with each candidate frit is provided in Appendix H. The columnidentified as “Sludge Loading (%)” summarizes the specific waste loading of interest. It shouldbe noted that there are typically more than one row for each sludge loading given the predictedproperties for all 927 EVs will vary dramatically. The second column in Appendix H (“SatisfiesPAR”) represents the comparison of the predicted property versus the PAR limits as shown inTable 4-1. In this column, properties deemed unacceptable with respect to the PAR acceptancelimits are preceded by “Not”. The last column (“# of EVs”) summarizes the number of EVswhose common property predictions are classified by the “Satisfies PAR” column. An effectivemethod to identify potential WLs or WL intervals in which all 927 EVs can be processed is toscan the “# of EVs” column for 927 then evaluate the “Satisfies PAR” column to assure that allpredicted properties are acceptable (“Not” should be absent from that row).

Given the high alkali concentration associated with the nominal Decant #5, when a ±10%variation is considered, it is anticipated that the extremely high alkali-based frits (such as Frit320, 416, 411, and 412) will not have projected operational windows over which all 927 EVs willbe processed. In fact, when the EVs associated with Decant #7 were assessed, these frits did notyield operational windows. Therefore, they were excluded from this assessment.

As the frit compositions become more refractory (moving from right to left in Table 7-9), thetolerance to the applied compositional variation should increase. In fact, a cursory review of theprojected windows associated with the Phase 2 Variation Stage for Decant #5 assessment supportthis latter statement.

No WL or WL interval exists over which all 927 EVs can be processed with Frit 202. A moredetailed review of the second and third metrics indicates that only 70% of the EVs can beprocessed at some WL with ~52% of those having a minimum 5% window. The results for Frits422, 423, 420, and 421 are somewhat more positive but still less than perfect (when compared toother frits in Table 7-9). The WL ranges over which all the EVs could be processed for these fritsis roughly a 2 – 4% window (all being in the mid-to-high 30’s). Subsequent metrics indicate aless than perfect response to the compositional variation applied.

The Phase 2 Variation Stage Decant #5 assessment for Frits 406, 405, 409, and 410 are verysimilar and provide feedback into the effect of the compensations required to handle the highconcentration and variation of alkali in the sludge. The 927 Decant #5 EVs could be processedby either of these frits over a relatively large WL interval. Waste loading intervals of 36 – 40%,36 – 39%, 36 – 41%, and 36 – 41%, respectively, are projected indicating a relatively high degreeof robustness for these frits. The second and third metrics are also very similar yielding 100%values which indicate that all 927 EVs could be processed at some WL with each having aminimum WL range of 5%. In fact, the minimum WL ranges are 6% or 9% depending upon thefrit.

Assessments of melt rate and/or frittability may play a significant role in determining the primaryfrit for Decant #5 and its resulting compositional envelope.

Imm

obil

izat

ion

Tec

hnol

ogy

Sect

ion

WSR

C-T

R-2

002-

0049

1Sa

vann

ah R

iver

Tec

hnol

ogy

Cen

ter

Rev

. 0W

estin

ghou

se S

avan

nah

Riv

er C

ompa

ny

58

Tab

le 7

-9. S

umm

ary

of F

rit

Com

posi

tion

s (i

n w

t% o

xide

s) U

sed

in th

e P

hase

2 N

omin

al a

nd V

aria

tion

Sta

ge D

ecan

t #5

Ass

essm

ent

Oxi

deF

rit 4

06F

rit 4

05F

rit 4

09F

rit 4

10F

rit 4

20F

rit 4

21F

rit 4

22F

rit 4

23F

rit 2

02A

l 2O

3-

--

-1

1-

--

B2O

315

208

88

108

108

Li 2

O5

54

55

58

87

MgO

--

--

--

--

2N

a 2O

--

65

77

33

6S

iO2

8075

8282

7977

8179

77T

otal

100

100

100

100

100

100

100

100

100

Dec

ant #

5Fr

it 4

06F

rit 4

05F

rit 4

09F

rit 4

10F

rit 4

20F

rit 4

21F

rit 4

22F

rit 4

23F

rit 2

02

Nom

inal

WL

(no

min

al)

33 –

51

31 –

46

33 –

50

32 –

50

30 –

45

30 –

44

31 –

46

31 –

44

33 –

39

Var

iatio

nW

L a

ll E

Vs

36 –

40

36 –

39

36 –

41

36 –

41

34 –

36

34 –

35

36 –

39

36 –

37

Non

e%

EV

s at

som

e W

L10

0.0%

100.

0%10

0.0%

100.

0%10

0.0%

100.

0%10

0.0%

100%

70.0

%W

L o

f 5%

or

grea

ter

100.

0%10

0.0%

100.

0%10

0.0%

92.1

%87

.8%

95.7

%90

.2%

51.6

%M

inim

um W

L r

ange

6%9%

6%6%

--

--

-


59

7.2.4 Phase 2 Variation Stage: Decant #9

Detailed information regarding the predicted properties for the Decant #9 EV-based sludgecompositions when coupled with each candidate frit is provided in Appendix I. The columnidentified as “Sludge Loading (%)” summarizes the specific waste loading of interest. It shouldbe noted that there are typically more than one row for each sludge loading given the predictedproperties for all 889 EVs will vary dramatically. The second column in Appendix I (“SatisfiesPAR”) represents the comparison of the predicted property versus the PAR limits as shown inTable 4-1. In this column, properties deemed unacceptable with respect to the PAR acceptancelimits are preceded by “Not”. The last column (“# of EVs”) summarizes the number of EVswhose common property predictions are classified by the “Satisfies PAR” column. An effectivemethod to identify potential WLs or WL intervals in which all 889 EVs can be processed is toscan the “# of EVs” column for 889 then evaluate the “Satisfies PAR” column to assure that allpredicted properties are acceptable (“Not” should be absent from that row). Table 7-10summarizes the Phase 2 Variation Stage assessments for Decant #9 (the Nominal Stageassessments are also shown for completeness).

Frit 202 should be considered a candidate frit for the compositional region covered by the Decant#9 EVs. All of the Decant #9 EVs can be processed over a WL range of 33 – 36% with theminimum WL range being 9% for each EV. These results suggest that Frit 202 is extremelyrobust to the compositional variation presented by the EVs associated with Decant #9.

The modifications made to Frit 202 (e.g., Frit 420 and Frit 421) also demonstrate flexibility toprocess the Decant #9 EVs with WL projections of 37 – 38% and 34 – 37%, respectively. Thesecond and third metrics indicate that Frit 421 may have a slight advantage over Frit 420.Although not as attractive as other frits, their use should be considered in further assessmentsinvolving melt rate and frittability.

The “higher” (Frits 412, 416, and 320) and “lower” (Frits 409 and 410) alkali containing frits areless attractive given their response to the Phase 2 Variation Stage assessments. Although theNominal Stage assessments indicate relatively large operating windows (exception of Frit 320 inwhich there was no window), only Frit 412 possesses a WL range over which all the EVs couldbe processed.

The assessment of Frits 422 and 423 (intermediate alkali containing frits) indicates both respondextremely well to the applied compositional variation. The projected WL ranges over which allthe EVs could be processed are 33 – 37% and 32 – 37%, respectively. With a minimum WLinterval of 6% and 10%, Frits 422 and 423 should be considered primary candidates within thiscompositional region. Assessments of melt rate and/or frittability may play a significant role forthis compositional region during the frit selection process.

Imm

obil

izat

ion

Tec

hnol

ogy

Sect

ion

WSR

C-T

R-2

002-

0049

1Sa

vann

ah R

iver

Tec

hnol

ogy

Cen

ter

Rev

. 0W

estin

ghou

se S

avan

nah

Riv

er C

ompa

ny

60

Tab

le 7

-10.

Sum

mar

y of

Fri

t C

ompo

siti

ons

(in

wt%

oxi

des)

Use

d in

the

Pha

se 2

Nom

inal

and

Var

iati

on S

tage

Dec

ant

#9 A

sses

smen

t

Oxi

deF

rit 4

09F

rit 4

10F

rit 4

20F

rit 4

21F

rit 4

22F

rit 4

23F

rit 2

02F

rit 4

12F

rit 4

16F

rit 3

20A

l 2O

3-

-1

1-

--

-1

-B

2O3

88

810

810

88

88

Li 2

O4

55

58

87

58

8M

gO-

--

--

-2

--

-N

a 2O

65

77

33

612

1112

SiO

282

8279

7781

7977

7572

72T

otal

100

100

100

100

100

100

100

100

100

100

Dec

ant #

9Fr

it 4

09F

rit 4

10F

rit 4

20F

rit 4

21F

rit 4

22F

rit 4

23F

rit 2

02F

rit 4

12F

rit 4

16F

rit 3

20

Nom

inal

WL

(no

min

al)

39 –

44

38 –

44

33 –

46

30 –

45

30 –

45

28 –

45

29 –

44

28 –

46

26 -

38

Non

eV

aria

tion

WL

all

EV

sN

one

Non

e37

– 3

834

– 3

733

– 3

732

– 3

733

– 3

632

– 3

5N

one

Non

e%

EV

s at

som

e W

L66

.1%

76.4

%10

0.0%

100.

0%10

0.0%

100.

0%10

0.0%

100.

0%58

.5%

31.1

%W

L o

f 5%

or

grea

ter

50.0

%53

.4%

94.4

%10

0.0%

100.

0%10

0.0%

100.

0%99

.9%

54.0

%28

.8%

Min

imum

WL

ran

ge-

--

6%6%

10%

9%-

--


61

8.0 MAR vs. PAR: Impact on ProjectedWaste Loading Intervals

Since the development of the new TL model (Brown et al. 2001), recent assessments (Peeler et al.2000; Peeler et al. 2001b; Peeler et al. 2002a) for DWPF have used the PAR criteria to assess theimpact of secondary waste streams or various frit compositions on select glass properties – notthe “more restrictive” MAR criteria. In these studies, use of the PAR criteria has allowed anefficient, “one-to-one” comparison in an effort to assess the impact of frit compositional changesor the addition of secondary waste streams on properties such as viscosity, homogeneity,durability, and liquidus temperature (which ultimately dictate projected operating windows). Asmentioned in Section 3.0, this same strategy was utilized in this report.

One may question the impact using this “conservative” TL limit has on the actual windows thatDWPF may anticipate (given the implementation of the product control system at the MAR).More specifically, “Is the use of the 1010°C truly conservative?” With respect to the SB3 fritdevelopment effort, the authors wanted to assure that the relatively large operational windowsprovided in the preceding sections are not reduced to an unmanageable level in terms ofminimizing DWPF flexibility to the point of inoperability.

Another potential issue resulting from the use of this conservative limit is the influence it mayhave on actual melter processing. More specifically, could the use of this conservative limit havea negative impact on subsequent assessments of processing glass within the melter (i.e., meltbehavior or melt rate)? This issue is addressed in detail in Section 10.0 (Path Forward).

In this section, the impacts of implementing or using this “conservative constraint” on theprojected operational windows are discussed in detail. Also discussed is the impact (or lackthereof) on this conservative constraint on the methodology being used not only for this specificassessment but future assessments that may be performed.

Appendix J provides an assessment of the projected operational windows for Decant #5 andDecant #9 using various frits based on the MAR criteria. The column identified as Frit/Decantindicates the specific frit/sludge combination being evaluated. The “% WL” column provides theWL. The next five columns labeled as “Durability”, “TL”, “Visc”, “Frit”, and Homog”,respectively, represent the MAR determination (in terms of pass or fail) for durability, liquidustemperature, viscosity, low/high frit, and homogeneity, respectively. A “blank” entry in aspecific cell under these columns indicates that the predicted property satisfies the MAR. For“durability”, “TL”, and “homog”, a “NO” in the respective cell indicates that the predictedproperty fails the MAR and that particular frit/sludge combination is not acceptable at that WL.For “visc” and “Frit”, if “high” or “low” are shown, this is an indication that the predictedproperty fails the MAR and on which side (high or low).

Table 8-1 provides a summary of the projected operational windows for various frit/decantcompositions expressed in terms of a waste loading range (based on a calcined oxide wt% basis)based on the use of both the PAR and MAR criteria. Also listed in the PAR column is theproperty that limits the particular frit/sludge combination from higher waste loadings.


62

Table 8-1. Projected Waste Loading Ranges for Various Frit/Decant CombinationsUsing both the PAR and MAR Acceptance Criteria

Decant #5 PAR MARFrit 202 33 – 39 (PCT) 33 – 37Frit 420 30 – 45 (PCT) 30 – 43Frit 421 30 – 41 (PCT/lo visc) 30 – 41Frit 409 33 – 50 (PCT) 34 – 48Frit 410 32 – 50 (PCT) 33 – 48Frit 422 31 – 46 (lo visc) 31 – 45Frit 423 31 – 44 (lo visc) 31 – 43

Decant #9Frit 202 29 – 44 (TL) 29 – 45Frit 420 33 – 46 (TL) 35 – 47Frit 421 30 – 45 (TL) 32 – 47Frit 411 26 – 45 (TL) 26 – 45Frit 422 30 – 45 (TL) 31 – 46Frit 423 28 – 45 (TL) 28 – 46

This table provides insight into the use of this “conservative” TL PAR limit on the actual windowsthat DWPF may anticipate (given the implementation of the product control system at the MAR).With respect to the SB3 frit development effort, the authors want to assure that operationalwindow for the recommended frit is not reduced to an unmanageable level in terms of minimizingDWPF flexibility to the point of inoperability once the MAR criteria are applied.

A review of the “upper waste loading limiting properties” indicates that predictions of durabilityand/or low viscosity limit access to higher waste loadings for the specific frit shown in Table 8-1when coupled with Decant #5. This is primarily a result of glass formulation efforts takingadvantage of the high Na2O content in this particular sludge (less washing) in an effort to increasewaste loadings as well as targeting enhanced melt rates given the historical knowledge thatincreased alkali concentrations improve melt rate.

A review of the Decant #9 based systems, indicates that all of these systems are TL limited interms of access to higher waste loadings. From previous DWPF process experience, TL has beenthe primary property that has limited access to higher waste loadings.

With respect to the impact of using the “less conservative” PAR criteria to assess projectedoperational windows, a review of projected waste loading range difference between the PAR andMAR is in order. Consider Decant #5 when coupled with Frit 202. Using the PAR criteria, theprojected waste loading interval is 33 – 39% with PCT (or predictions of durability) limitingaccess to higher waste loadings. When the MAR criteria are used, the WL interval is 33 – 37%;a 2% reduction in the upper WL limit achievable based on predictions of durability.

In general, use of the MAR criteria typically reduces the upper waste loading limit that can beobtained for the Decant #5 based systems. This is not surprising given the addition ofmeasurement uncertainty to the PAR predictions to the PCT and viscosity models leading to a


63

more conservative operating window. The use of the “conservative 1010°C PAR limit” does notcome into play for these systems.

For a direct assessment of the “conservative” 1010°C PAR criteria, one must evaluate TL limitedsystems (e.g., all of the Decant #9-based systems). In each of these systems, the upper wasteloading limit for the PAR is lower than that allowed by the MAR – indicating that the use of the1010°C TL PAR limit is conservative with respect to the upper waste loadings achievable. This isconsistent with that reported by Brown et al. (2001). More specifically, consider the Decant#9/Frit 202 system. Use of the PAR criteria established a projected waste loading interval of 29 –44%; while the projected waste loading interval using the MAR criteria is 29 – 45% (a 1%increase in the projected, achievable waste loading).

Based on the information reviewed since the development of the new TL model, the use of the1010°C PAR limit does appear to be “conservative” with respect to upper waste loadingprojections for systems that are TL limited. It appears that its use has not specificallymisrepresented (overestimated) potential waste loadings of interest (assuming TL limited systems)and has effectively supported a methodology to evaluate the impact of various frit or sludgecompositional changes on projected operational windows. It should be noted that waste loadingprojections are based on model predictions of viscosity, durability, homogeneity, and liquidustemperature as they compare to property acceptance criteria. The WL projections are notinfluenced by assessments of melt rate or cold cap behavior.


64



65

9.0 Summary

Current planning strategies project that DWPF should start processing SB3 in the spring of 2004(WSRC 2001). Sludge Batch 3 will be primarily Tank 7 sludge mixed with the heel of SludgeBatch 1B (SB1B), contributions from Tanks 18 and 19, and an H-Canyon slurry containingprecipitated Pu with Gd (Jilani 2002). The sludge from Tank 7 is expected to contain severalcomponents that are considered atypical of DWPF sludge to date including higher levels of noblemetals than previously processed sludge batches (Peeler et al. 2002a). Other atypical componentsthat may be present in this sludge batch include sand, coal, Am/Cm precipitate (Patel 2002),sodium oxalate, and zeolite (Jantzen et al. 2002a). Based on the process history for Tank 7, it isestimated that significant quantities of sand/coal (~7723 kg) and sodium oxalate (~300,000 kg)have been added to this tank (Goslen 1984; Fowler 1980).

A series of tasks have been identified and are currently being addressed prior to accepting SB3into DWPF (Fellinger 2002). One of the tasks identified involved an evaluation of potential fritsfor SB3, which is the sole focus of this report.


• Maximizing the PCCS projected operational window size over the anticipated SB3composition region





The issues listed above have been used to guide the SB3 frit development task in an effort toimprove current DWPF baseline operations in terms of ease of processing, waste loading, and/ormelt rate. The ability to maximize the size of the DWPF operational window provides flexibilityin targeting waste loadings to meet processing goals in support of the accelerated clean-upmission.

The focus of this report is on frit development activities conducted solely on the basis ofpredictions generated by DWPF’s glass property-composition models as they apply todetermining projected operational windows and assessing the robustness of a frit to compositionalvariation. Technical issues and results associated with melt rate and frittability are not discussedin this report but are critical inputs into the frit selection process. It is not the intent of this studyto recommend a frit to DWPF for SB3 – only to provide insight into the selection process.

A unique, but technically sound methodology was developed and implemented for this study toguide frit development activities. The methodology utilized was a sequential, iterative processthat may be summarized as follows: Candidate frits were identified for and compared acrossnominal sludge compositions (i.e., where each such composition is considered as a “best guess”view of SB3 sludge for a potential washing scenario). Two different sets of sludge compositions(an initial and a final) were used to represent potential nominal SB3 compositions. The initial set


66

of compositions was available early in the study and served as the basis for much of thepreliminary development efforts. The preliminary frits that were the most promising at this stagewere carried over to a stage of investigation that introduced variation around the nominal SB3compositions. This approach was used to provide an assessment of the robustness or tolerance ofa candidate frit to anticipated compositional variation (i.e., the ability of the frit to produce anacceptable product for variations in the sludge based upon model predictions). Comparisonsamong the frits were conducted using objective metrics, described below, that were developed toaid in this decision making process. This two-staged (an assessment using only nominalcompositions and then an assessment with variation introduced) approach was then conducted forthe second (or final) set of SB3 compositions. It should be noted that this portion of the overallfrit development strategy was based solely on model predictions.

At the time this task was initiated, uncertainties associated with the actual quantity of Na2C2O4 inTank 7 and the fraction that would ultimately be transferred to SB3 given the various washingscenarios being considered were being addressed. From a glass formulation perspective andresulting properties, the unknown quantity of Na2O resulting from the Na2C2O4 will have a majorimpact on the overall sludge composition and ultimately the frit development efforts. That is, fritformulation efforts will have to account for or compensate for the varying Na2O concentrationsthat could be present in the sludge and ultimately the glass as different washing schemes areconsidered. Concentrations of Na2O in the nominal SB3 sludges ranged from 10.63 wt% to 35.13wt%. With respect to frit development activities, the wide range of Na2O concentration made itextremely difficult to develop a single frit that is tolerant or insensitive to this large variation. (Itwould be ideal to develop a single frit that would yield acceptable glasses for all washingschemes over the waste loading interval of interest – assuming no adverse impacts of otherprocessing issues such as melt rate are encountered.) Therefore, frit development activitiescompensated by adjusting the alkali concentration and type as well as their ratios in perspectivefrits. More specifically, as sludge washing is increased, the alkali concentration in sludgedecreases, therefore, resulting in a shift to a higher alkali containing frit.

Based on model predictions, the Nominal and Variation Stage assessments of both existing andalternative (or newly developed) frits indicate that judicious selection of the frit can yieldprocessable and durable products at attractive waste loadings for all washing scenarios thatdemonstrate a high degree of tolerance for compositional variation. Given this, an aggressivewashing strategy may not be required to assure processability or product quality as long asalternative frits are considered (assuming there are not significant technical issues such as anionsolubility, H2 generation, redox control, or rheological control). Again, the assessments are basedsolely on model predictions and do not include assessments of melt rate or frittability.

Numerous comparisons could be made based on the information generated in this study. Generalobservations or results are bulletized below. It should be noted that the observations cited beloware based solely on the results of the paper study assessment and do not account for melt rate orfrittability. The reader is referred to the detail discussions within the main body of the report formore detailed assessments.

General observations from this study:

� Compositional frit adjustments can be made to compensate for various waste streamcompositions resulting from the washing strategy pursued. More specifically, frits can bedeveloped to provide relatively large operational windows with a high degree ofcompositional robustness over the entire compositional region evaluated.


67

� It would be ideal to develop a single frit that would yield acceptable glasses for all washingschemes (including compositional variation) over the waste loading interval of interest –assuming no adverse impacts of other processing issues such as melt rate are encountered.This would be an ideal situation from the perspective of balancing frit developmentrequirements with selecting a washing strategy to pursue. That is, minimal insight would berequired from the glass formulation team and the integrated flowsheet would be solely drivenby the washing strategy. Although conceptually enticing, this may result in a “non-optimized” system. The use of a single frit over such a large compositional region couldresult in a wide response in melt rate potentially leading to lower waste throughput forDWPF. This concept gives support for developing specific frits for specific sludges tooptimize operational windows and waste throughput (e.g., Frit 320 for SB2).

� The ability to compositionally compensate for the degree of washing via frit developmentefforts provides an incentive to further evaluate the potential to integrate a “low washedsludge” into the overall flowsheet. Washing the sludge less does have advantages in terms ofsignificant time, labor, and ultimately funding reductions in the pretreatment/retrievaloperation. A reduced washing campaign should also result in less water being sent to theevaporators. Assuming the source of alkali is not of concern, the enhanced alkaliconcentration in the under washed sludge could also improve melt rate (or at a minimummaintain melt rate relative to other sludge compositions). Conversely, targeting higherwashed sludge should reduce the total number of canisters produced by some incrementalamount and may minimize components that have potentially negative impacts to either WL orprocessability (such as SO4). A cost-benefit analysis should be performed to fully understandthe advantages and disadvantages of selecting a targeted washing scenario.

� Frit 202 is a viable frit candidate for specific washing scenarios. For the “mid-ranged”washing scenarios (e.g., 50% linear washing case, Decant #7, or Decant #9), Frit 202provides large operational windows and is extremely tolerant to compositional variation.This is consistent with Elder’s conclusions and his classification of Frit 202 as a “baseline”frit. However, use of Frit 202 with the extreme (in terms of washing strategy) sludgecompositions typically results in small (sometimes non-existent) projected operationalwindows. If a window does exist, the tolerance to compositional variation is low. Use of Frit202 may be advantageous not only from a WL perspective, but given the current availabilityof the frit, fabrication cost may be eliminated (assuming the quantity of frit existing would besufficient to process SB3) or at least minimized (assuming a limited quantity would berequired from a vendor). The classification of Frit 202 as a primary candidate based solely onavailability assumes all other factors (such as robustness, operational window size, and meltrate) are equal. If proven to meet or provide acceptable responses to the Variation Stage andmelt rate, a cost benefit analysis should be performed (including adjustments for total wastethroughput) to assess the advantages and (potential) disadvantages of this frit.

� Frit 320 is a viable frit for the more advanced washed sludges (e.g., 75% linear washing case,Decant #12 and above). The relatively high alkali concentrations in the frit are off-set by thelower Na2O concentration as the degree of washing increases resulting in operationalflexibility for DWPF. Combining Frit 320 with less washed sludges is typically prohibitedby predictions of durability (a direct result of the high alkali concentrations of both the sludgeand frit). Again, availability of Frit 320 (assuming it is not consumed during SB2 processing)may be advantageous from a cost-benefit analysis.

� To provide compositional operating regions for each washing scenario, alternative frits weredeveloped primarily based on alkali compensation with respect to the sludge. As with Frits202 and 320, the alternative frits are best suited over a limited compositional region. Thealternative frits do provide large operational windows and demonstrate a high degree ofrobustness to anticipated compositional variation.


68

� The concept of developing alternative frits for specific sludges (in an attempt to maximizethroughput and/or operational flexibility) was observed numerous times during theseassessments. One of the more interesting observations was the comparative responses of Frit320 and Frit 416 (a modified formulation of Frit 320 in which 1% of the Na2O was added asAl2O3) for the 75% washed sludge. Although the compositional modification appears to benegligible, its impact on predicted properties, which define the projected operational window,is rather high. No WL or WL range exists over which all 423 EVs could be processed withFrit 320. The slight compositional modification of Frit 416 results in a 27 – 39% WL rangeover which all of the EVs could be processed. This result indicates a high tolerance of Frit416 to the applied compositional variation of ±10%. Evaluation of the third metric providesadditional insight into the robustness of Frit 416. A minimum WL range of 15% is predictedfor each of the 423 EVs – a very strong statement in terms of flexibility. Assuming nosignificant changes in melt rate are observed, the slight compositional adjustment providesoperational flexibility to DWPF that is not available with existing frits.

� Historically, most of the previous sludge batches processed through DWPF have been TL

limited (in terms of the maximum waste loading achievable). An interesting outcome in thisassessment was the fact that frit development efforts could take advantage of the high alkalicontent of the sludge driving or forcing the low washed sludges to be durability limited. Thismay be beneficial from a waste loading and melt rate perspective.

� The use of the less conservative PAR criteria seems to be a viable and effective method toguide frit development activities. It appears that its use has not specifically misrepresented(overestimated) potential waste loadings of interest (assuming TL limited systems) and haseffectively supported a methodology to evaluate the impact of various frit or sludgecompositional changes on projected operational windows.

As previously mentioned, key criteria or aspects that will provide the technical basis for selectinga frit for SB3 include: (1) maximizing the projected operational window size (i.e., the wasteloading interval) over the anticipated SB3 composition region, (2) providing a frit that is robust orinsensitive to anticipated sludge composition variation, (3) improving or maintaining high wasteloadings (WLs), (4) improving or maintaining high melt rates, and (5) providing a “frittable”additive or frit composition. Given the five key criteria can be competing, the basis for not onlydeveloping but ultimately selecting a frit for SB3 is complex. The selection process should not bemade based on a single criterion but a collection of criteria that provide insight into theeconomics of processing SB3. A balanced approach should be utilized in both the developmentand selection. The selection may be solely a business decision assuming no technicalshowstoppers are identified. Another factor that could play a significant role in the selection of afrit is the availability of an existing frit versus any procurement and manufacturing costs for analternative frit. The bottom line is that all the available information should be used to perform acost / benefit analysis that could serve as input to the frit selection process.

An integrated methodology has been developed and is being utilized (and is in place for SB3) todevelop frits for specific sludge batches. The methodology should include assessments of (a)projected operational windows using current model predictions, (b) melt rate, and (c) frittability.This integrated strategy would lower the risk of introducing a feed into DWPF that although onpaper is very attractive (in terms of waste loading) results in a very difficult feed to process (interms of melt rate). In fact, this strategy should provide the basis for developing a decisionmatrix in which optimum waste throughput could be targeted.


69

10.0 Path Forward

As previously mentioned, five key criteria or aspects will provide the technical basis for selectinga frit for SB3. These include:

• Maximizing the projected operational window size (i.e., the waste loading interval) over theanticipated SB3 composition region





The current report addresses the first three items from a prediction standpoint – no experimentalassessments were made to confirm predictions. The overall strategy has not discounted theimportance of the remaining two criteria: melt rate and frittability. Parallel activities (outlined inHerman, Peeler and Edwards 2002) are on-going to assess these criteria which will form asignificant portion of the frit selection process. These two criteria are discussed below.

10.1 Melt Rate

One method of supporting site and U.S. DOE goals of accelerated cleanup is to improve wasteloading. For DWPF, a new TL model has been developed and implemented which has proven toyield higher waste loadings for projected sludge batches (Brown et al. 2001). As previouslymentioned, although targeting higher waste loadings is a primary objective, other processingconstraints are also important. In the assessments discussed in this report, waste loadingprojections were not influenced by assessments of melt rate or cold cap behavior given there iscurrently no model to perform such an evaluation that is sensitive enough to discern between theglass compositions of interest (much less a 1% change in waste loading). That is, the projectedoperational windows are defined independent of melt rate projections from a model perspective.As discussed in Section 1.0, a major objective of the SB3 glass formulation team was to provideoperational flexibility to DWPF via large operational windows while maintaining both high WLand an acceptable melt rate. Therefore, although no models were available to assess melt rate asa function of frit composition, compositional adjustments were based on the general trendsobserved during the development of Frit 320 for SB2 (Peeler et al. 2001a). More specifically, thealkali concentration in the frit was directly related to melt rate.

The balance between melt rate and waste loading should be carefully considered. Although everyeffort was made to indirectly develop frit compositions in terms of melt rate, the concern is thattargeting the maximum WL allowed by model predictions may not necessarily lead to optimummelt rate or waste throughput. In fact, Lorier and McGrier (2002), have shown that for the Frit320 based system, increased waste loading can have a negative impact on melt rate above somecritical value. The concept that reduced melt rates at higher waste loading is unacceptable shouldbe tempered with an evaluation of the total waste throughput. More specifically, during anassessment of the impacts of waste loading on melt rate, decisions on frit selection or targetedwaste loading should not be made solely on the relative melt rate. The decision should considerthe total sludge throughput per unit time. Note that currently there are no models that can be useda priori to gain insight into the melt rate of various systems. This assessment will be made solely


70

by using a testing methodology that has been shown to be effective for SB2 (Stone and Josephs2001).

Therefore, as frit development efforts proceed for SB3 (or for future sludge batches), anassessment of melt rate must be included in the development of the integrated flowsheet toaccount for this disconnect. Assessments not only associated with projected operational windows(currently based on model predictions) but the impact on melt rate or melt behavior must beaddressed (experimentally). In support of the accelerated clean up mission, the primary focusshould be on determining the parameters that define optimal waste throughput (or work off)which may be a compromise between waste loading and melt rate.

Integration of melt rate assessments for select frit/sludge combinations is part of the SB3flowsheet development program. The assessment of melt rate will be one of three major criteriaused in the frit selection process – the other two being operational flexibility and frittability. Theresults of the melt rate and frittability assessments are not covered in this report. However, thestrategy being used in the melt rate assessment to address the potential impact of the“conservative 1010°C” PAR constraint for TL with respect to melt rate or melt behavior in DWPFis briefly discussed below.

The model-based assessments provide valuable information with respect to how the projectedoperational windows respond to compositional variation around a nominal sludge composition forvarious frits. This information will form one of the three key inputs to the frit selection process.The final decision of selecting a frit will not be based solely on the projected operational sizes orrobustness of a frit – melt rate or cold cap behavior being critical as well. One question thatshould be asked and addressed is: “Does it really matter that model predictions allow extremelyhigh waste loadings if the DWPF melter processing is hindered or inefficient due to an erraticcold cap behavior or extremely slow melt rate?” To address this issue, the SB3 frit developmentteam has integrated an assessment of melt rate for candidate frit compositions into its program inan effort to provide not only relatively high WLs but to maximize waste throughput via a balancebetween melt rate and WL. An ideal scenario would be that maximum waste throughput isattained at the maximum waste loading.

As discussed in Sections 6.0 – 7.0, both existing and newly developed frits were assessed in termsof their projected operational windows for various washing scenarios. The results provide insightinto the compositional adjustments needed to compensate for the various levels or degrees ofwashing. The Variation Stage assessments provide valuable insight into the robustness orflexibility of each frit to handle compositional sludge variation. The Nominal and VariationStage assessments allowed candidate frit compositions to be screened with respect to theirpotential application to SB3. For example, a frit that did not provide an operational window (fora specific sludge composition or compositional region) should not be carried forward in furtherassessments (melt rate and/or frittability) given the models would ultimately not allow DWPF toprocess.

Given the decision of the SB3 team to focus primarily on the compositional region bounded byDecants #5 and #9, plans for melt rate assessments have been developed based on these twonominal waste streams. An initial frit down selection occurred based on model assessments (i.e.,those frits that indicated relatively large processing windows and had a positive response on theability to handle compositional variation as a function of various washing scenarios). The resultsof both Nominal and Variation Stage assessments associated with Decants #5, #7, and #9 willplay an integral role in this down selection process.


71

To directly compare the effect of frit composition on melt rate, the task team identified the needto maintain a constant acid addition strategy (at least within a particular washing scenario) as wellas to select “common” waste loadings for each frit/sludge system. The constant acid additionstrategy is intended to eliminate (or at least minimize) any overwhelming impacts of the acidaddition strategy on melt rate so a relative measure of the effect of frit composition on melt ratecan be obtained. More specifically, given the focus of this effort is on differentiating the effect offrit composition on melt rate, the team did not want the acid addition strategy (which is currentlyunder development for SB3) to suppress this assessment.

The use of “constant waste loadings” should provide a sound technical basis for two assessments.The first being a direct comparison of melt rate between frit-based systems at a constant wasteloading. The second major assessment will be the impact of waste loading changes on melt ratewithin a specific system. The latter providing insight into the total waste throughput curve for aparticular frit/sludge system. Based on the MAR information provided in Section 8.1, the SB3melt rate team elected to use WLs of 30, 35, and 40% in the initial melt rate assessments. It isrecognized that electing to use a “common” waste loading range provides some disadvantagesand adds some risk. One disadvantage is the fact that the WL intervals for the various frit/sludgesystems are not consistent so use of a common waste loading interval forces one to select non-bounding (below and above) the lower and upper WL limits as defined by model predictions.This could lead to an assessment of melt rate in a compositional region that would not be allowedin DWPF based on model predictions or not provide full coverage at the upper WLs limits ofinterest. For example, consider the two Frit 202 based systems. When coupled with Decant #5,the projected operational window based on MAR predictions is 33 – 37%. Both the 30% and40% WL melt rate tests may be questionable given they lead to unacceptable products based onsome criteria. However, the WL interval to be used bounds the anticipated processing regionfrom which the effect of WL on melt rate can be viewed. The use of 30% and 40% for the Frit202/Decant #9 melt rate tests are non-bounding tests (MAR predictions allow for a 29 – 45%window). Although not bounding, assessment of melt rate can be made over a majority of theWL interval to provide insight into the total waste throughput curve. Given the use of constantWLs, comparisons of melt rate can be made between the two sludge cases providing input intothe targeted washing strategy.

Although potentially not bounding or unacceptable, the melt rate information obtained can beused as a guide to understand the impacts of WL on melt rate and should provide the template forthis relationship from which melt rate interpolations could be made (albeit with some risk).

It should also be noted that the initial set of screening tests will be based on the dry fed melt ratefurnace which also induces some risks, although minimal, based on recent data linking the dry fedsystem to slurry fed melters. This initial screening based on dry fed testing will be factored intothe frit selection process from which a minimum number of primary frit candidates would bedefined. Upon identification of the primary frit candidates, more detailed melt rate testing shouldbe performed which could include dry feed tests at intermediate WLs to fill out the melt rateversus waste loading curve, slurry feed melt rate tests as a function of WL, and/or mini-meltertests.


72

10.2 Frittability

The last criteria to discuss is the desire to have a “frittable” frit (i.e., the targeted frit compositionwill produce a glass that can be manufactured by a vendor) which stems from waste acceptanceissues. Currently, DWPF uses a frit that is ultimately blended with the sludge. Samples of thisblend are taken from the Slurry Mix Evaporator (SME), the compositions determined, andproperties are predicted from the measured composition which are verified to be within theprocessing window. Given the feed is acceptable in terms of various property predictions, thefeed is transferred to the melter, converted to glass, and poured into canisters. This feed-forwardprocess control strategy has been very effective in terms of assuring processability and productquality. The use of a prefabricated frit has alleviated or minimized issues associated with mixing,sampling, and homogenizing the contents of the SME, which serves as the basis for the processcontrol strategy. It is therefore desirable to provide a “frittable” frit for DWPF. Althoughdesirable, this criterion was not used as a strict constraint during the frit selection process in ordernot to limit the alternative processing situations/cases submitted for DWPF review.

In order to assess this criterion, two approaches have been taken. The first approach was toassume an upper frit melt temperature of 1450°C and experimentally determine if the targetedcompositions could be melted at this temperature. This assessment is being performed on thelaboratory scale and is an on-going task at the time this report was written. It was recognized thatthis approach had risks associated which included: (1) laboratory scale tests being solely used as ameasure of a vendor’s ability to implement or produce tonnage quantities and (2) not only is therea need to define an upper temperature limit but also an associated viscosity-temperaturerelationship. The former is being addressed by a request (albeit informal) for a vendor to reviewa list of primary frit candidate compositions to determine the potential for the vendor to utilize anexisting melter technology to cost effectively produce the frits. The second issue is beingaddressed within SRTC as the viscosity versus temperature relationships for select candidate fritcompositions is being formally measured. Again, this information alone will not be used to makethe final frit selection but will form a valuable portion to be used during the frit selection process.


73

11.0 References

ASTM 1998. Standard Test Methods for Determining Chemical Durability of NuclearWaste Glasses: The Product Consistency Test (PCT), ASTM C-1285-98, 1998.

Bronikowski, MG, MC Thompson, FR Graham, TL Fellinger, WR Wilmarth, and DT Hobbs,2002. Technical Task and Quality Assurance Plan for Assessing Downstream Effects ofPlutonium/Gadolinium in Sludge Washing and SRAT, WSRC-RP-2002-00178 WestinghouseSavannah River Company.

Brown, KG, and RL Postles. 1996. SME Acceptability Determination for DWPF Process Control,WSRC-TR-95-0364, Revision 3, Westinghouse Savannah River Company, Aiken, SouthCarolina, 1996.

Brown KG, CM Jantzen, and G Ritzhaupt. 2001. Relating Liquidus Temperature to Compositionfor Defense Waste Processing Facility (DWPF) Process Control, WSRC-TR-2001-00520,Westinghouse Savannah River Company, Aiken, South Carolina.

Edwards TB, and KG Brown. 1998. Evaluating the Glasses Batched for the Tank 42 VariabilityStudy (U), SRT-SCS-98-017, Revision 0, Westinghouse Savannah River Company, Aiken, SouthCarolina.

Elder, HH. 2002. Impact of Processing Americium and Curium in ESP, DWPF, and Saltstone,Savannah River Site, High Level Waste Process Engineering Position Paper, HLW-SDT-2001-00244, Rev. 1.

Fellinger, TL. 2002. Sludge Batch 3 – Overall Program View (U), WSRC-RP-2002-00353,Westinghouse Savannah River Company, Aiken, South Carolina.

Fowler, JR. 1980. “Estimate of Maximum Amount of Reducing Agents and Sand in the SRPWaste for DWPF TDS”, Don’t Say It Write Memo, September 9, 1980.

Goslen, AQ. 1984. “Estimated Sodium Oxalate in the Tank Farm”, March 22, 1984.

Herman, CC, TL Fellinger, NE Bibler, and DC Koopman. 2002a. Scoping SRAT Runs withSimulated Sludge Batch 3, SRT-GPD-2002-00044, Westinghouse Savannah River Company,Aiken, South Carolina.

Herman, CC, KG Brown, DK Peeler, and TB Edwards. 2002b. Selecting Glass Compositions forPhase 2 of the Reduction of Constraints Study, WSRC-RP-2002-00236, Revision 0,Westinghouse Savannah River Company, Aiken, South Carolina.

Herman, CC, DK Peeler, and TB Edwards. 2002. Task Technical and QA Plan: Sludge Batch 3Variability Studies with Simulants, WSRC-RP-2002-00386, Westinghouse Savannah RiverCompany, Aiken, South Carolina.

Jantzen, CM. 1988. Glass Composition and Frit Formulation Developed for DWPF, DPST-88-952, E.I. du Pont de Nemours and Company, Savannah River Laboratory, Aiken, South Carolina.


74

Jantzen, CM, JB Pickett, KG Brown, TB Edwards, and DC Beam. 1995. Process/ProductModels for the Defense Waste Processing Facility (DWPF): Part I. Predicting Glass Durabilityfrom Composition Using a Thermodynamic Hydration Energy Reaction Model (THERMO) (U),WSRC-TR-93-672, Rev. 1, Volume 1, Westinghouse Savannah River Company, Aiken, SouthCarolina.

Jantzen, CM, RF Swingle, and FG Smith. 2002a. Impact of Tank 19F Zeolite Mound on DWPFVitrification of Sludge Batch 3, WSRC-TR-2002-00288, Rev. 0, Westinghouse Savannah RiverCompany, Aiken, South Carolina.

Jantzen, CM. 2002b. REDOX Studies and Modeling for DWPF Sludge Batch 3, WSRC-RP-2002-00341, Westinghouse Savannah River Company, Aiken, South Carolina.

Jilani, I. 2002. Evaluation of Impact of HLW of Using Gadolinium as a Neutron Poison forPlutonium, Technical Task Request, NMMD-HTS-2002-010, Westinghouse Savannah RiverCompany, Aiken, South Carolina.

Lambert, DP, TH Lorier, DK Peeler, and ME Stone. 2001. Melt Rate Improvement for DWPFMB3: Summary and Recommendations, WSRC-TR-2001-00148, Westinghouse Savannah RiverCompany, Aiken, South Carolina.

Li, H, JD Vienna, PR Hrma, DE Smith, and MJ Schweiger. 1997. “Nepheline Precipitation inHigh-Level Waste Glasses: Compositional Effects and Impact on the Waste FormAcceptability.” In Scientific Basis for Nuclear Waste Management XX, Vol. 465, pp. 261-268.Materials Research Society, Pittsburgh, Pennsylvania.

Li, H, B Jones, P Hrma, and JD Vienna. 1998. “Compositional Effects on Liquidus Temperatureof Hanford Simulated High-Level Waste Glasses Precipitating Nepheline (NaAlSiO4),” Ceram.Trans. 87, pp 279-288, American Ceramic Society, Westerville, Ohio.

Lorier, TH and PL McGrier. 2002. Melt Rate Improvement for the DWPF: Higher WasteLoading Testing, WSRC-TR-2002-00344, Westinghouse Savannah River Company, Aiken,South Carolina.

Patel, PM. 2002. Evaluation of Impacts of Sludge Containing “Americium/Curium” on H2

Generation and Glass Quality, Technical Assistance Request, HLW/DWPF-TAR-02-0007,Westinghouse Savannah River Company, Aiken, South Carolina.

Peeler DK, TB Edwards, KG Brown, RJ Workman, and IA Reamer. 2000. Reduction ofConstraints: Applicability of the Homogeneity Constraint for Macrobatch 3 (U), WSRC-TR-2000-00358, Revision 0, Westinghouse Savannah River Company, Aiken, South Carolina.

Peeler, DK, TH Lorier, DF Bickford, DC Witt, TB Edwards, KG Brown, IA Reamer, RJWorkman, JD Vienna. 2001a. Melt Rate Improvement for DWPF MB3: Frit Development andModel Assessment, WSRC-TR-2001-00131, Revision 0, Westinghouse Savannah RiverCompany, Aiken, South Carolina.

Peeler DK, KG Brown, and TB Edwards. 2001b. Reduction of Constraints: Technical Statusreport on the Applicability of the Homogeneity Constraint for Sludge-Only Processing, WSRC-TR-2001-00538, Revision 0, Westinghouse Savannah River Company, Aiken, South Carolina.


75

Peeler, DK, NE, Bibler, and TB Edwards. 2002a. An Assessment of the Impacts of AddingAm/Cm and Pu/Gd Waste Streams to Sludge Batch 3 (SB3) on DWPF H2 Generation Rates andGlass Properties, WSRC-TR-2002-00145, Westinghouse Savannah River Company, Aiken,South Carolina.

Peeler DK, KG Brown, TB Edwards, DR Best, RJ Workman, and IA Reamer. 2002b. Reductionof Constraints: Phase 1 Experimental Assessment of Centroid-Based Sludge-Only Glasses,WSRC-TR-2002-00120, Revision 0, Westinghouse Savannah River Company, Aiken, SouthCarolina.

Plodinec MJ, KG Brown, SL Marra, CM Jantzen, and TB Edwards. 1995. “Technical Bases forthe DWPF Glass Product Control Program”, In: Waste Qualification Report (WQR), WSRC-IM-91-116-5, Revision 1, Volume 5, Aiken, South Carolina.

Rios-Armstrong, MA. 2002a. Technical Task Request, Sludge Batch 3 Carbon Content Analysis,TTR-HLW/DWPF/TTR-02-0017, 4/25/2002.

Rios-Armstrong, MA., 2002b. Sludge Batch 3 Variability Studies with Simulants,HLW/DWPF/TTR-02-0027.

SAS Institute, Inc., JMP® Statistics and Graphics Guide: JMP Version 4, SAS Institute, Inc,Cary, North Carolina, 2000.

Soper, PD, DD Walker, MJ Plodinec, GJ Roberts and LF Lightner. 1983. “Optimization ofGlass Composition for the Vitrification of Nuclear Waste at the Savannah River Plant,” Ceram.Bull. Volume 62, No. 9, pp. 1013–1018.

Stone, ME and JE Josephs. 2001. Melt Rate Improvements for DWPF MB3: Melt Rate FurnaceTesting, WSRC-TR-2001-00146, Rev. 0, Westinghouse Savannah River Company, Aiken, SouthCarolina.

Westinghouse Savannah River Company (WSRC). 2001. Savannah River Site High Level WasteSystem Plan (HLW), HLW-2001-00040, Revision 13, Aiken, South Carolina.


76



77

Appendix A

Nominal Decant Compositions(Personal Communication with H.H. Elder)

Imm

obil

izat

ion

Tec

hnol

ogy

Sect

ion

W

SRC

-TR

-200

2-00

491

Sava

nnah

Riv

er T

echn

olog

y C

ente

r R

ev. 0

Wes

tingh

ouse

Sav

anna

h R

iver

Com

pany

79

Ele

men

tal

wt.

%D

ecan

t #5

Dec

ant #

6D

ecan

t #7

Dec

ant #

8D

ecan

t #9

Dec

ant #

10D

ecan

t #11

Dec

ant #

12D

ecan

t #13

Dec

ant #

14D

ecan

t #15

Al

7.33

7.59

7.82

8.01

8.18

8.33

8.47

8.60

8.71

8.82

8.93

B0.

000.

000.

000.

000.

000.

000.

000.

000.

000.

000.

00B

a0.

170.

180.

180.

190.

190.

190.

200.

200.

200.

210.

21

Ca

1.97

2.04

2.10

2.15

2.20

2.24

2.28

2.31

2.34

2.37

2.40

Ce

0.23

0.24

0.24

0.25

0.25

0.26

0.26

0.27

0.27

0.27

0.28

Cr

0.19

0.20

0.21

0.21

0.22

0.22

0.22

0.23

0.23

0.23

0.24

Cs

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

Cu

0.12

0.13

0.13

0.13

0.14

0.14

0.14

0.14

0.14

0.15

0.15

Fe21

.53

22.3

122

.98

23.5

424

.05

24.4

824

.89

25.2

725

.59

25.9

226

.26

K0.

270.

280.

290.

300.

310.

310.

320.

320.

330.

330.

33

La

0.15

0.16

0.16

0.16

0.17

0.17

0.17

0.18

0.18

0.18

0.18

Li

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

Mg

0.09

0.09

0.09

0.10

0.10

0.10

0.10

0.10

0.10

0.10

0.11

Mn

4.25

4.41

4.54

4.65

4.75

4.84

4.92

4.99

5.06

5.12

5.19

Mo

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

Na

23.1

521

.29

19.7

118

.38

17.1

716

.15

15.1

814

.27

13.5

212

.74

11.9

4N

b0.

000.

000.

000.

000.

000.

000.

000.

000.

000.

000.

00

Ni

0.97

1.00

1.03

1.06

1.08

1.10

1.12

1.14

1.15

1.16

1.18

Pb

0.21

0.22

0.23

0.23

0.24

0.24

0.25

0.25

0.25

0.26

0.26

Si0.

750.

780.

800.

820.

840.

850.

870.

880.

890.

900.

91T

h0.

100.

100.

100.

110.

110.

110.

110.

110.

110.

120.

12T

i1.

291.

341.

381.

411.

441.

471.

491.

521.

541.

551.

58

U6.

616.

857.

057.

237.

387.

517.

647.

767.

867.

968.

06Y

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

Zn

0.25

0.26

0.27

0.28

0.28

0.29

0.29

0.30

0.30

0.30

0.31

Zr

0.44

0.45

0.46

0.48

0.49

0.49

0.50

0.51

0.52

0.52

0.53


80



81

Appendix B

Summary of the Projected Operational Windows for the Nominal Washing Cases

Imm

obil

izat

ion

Tec

hnol

ogy

Sect

ion

W

SRC

-TR

-200

2-00

491

Sava

nnah

Riv

er T

echn

olog

y C

ente

r R

ev. 0

Wes

tingh

ouse

Sav

anna

h R

iver

Com

pany

82

SB3

Nom

inal

Was

hing

Com

posi

tion

s w

ith

Sele

cted

Fri

ts

Typ

eFr

it I

DSa

tisf

ies

PAR

Min

(Slu

dge

Loa

ding

(%

))M

ax(S

ludg

e L

oadi

ng (

%))

SB3

Nom

inal

for

Was

hing

@ 0

%20

2D

urab

le; V

isc;

; N

ot H

omog

; New

TL

; A

l2O

3 ; a

lkal

i25

28SB

3 N

omin

al f

or W

ashi

ng @

0%

202

Dur

able

; Vis

c; ;

Not

Hom

og; N

ew T

L ;

Al2

O3

; Not

alk

ali

2930

SB3

Nom

inal

for

Was

hing

@ 0

%20

2N

ot D

urab

le; V

isc;

; N

ot H

omog

; New

TL

; A

l2O

3 ; a

lkal

i31

33SB

3 N

omin

al f

or W

ashi

ng @

0%

202

Not

Dur

able

; Vis

c; ;

Hom

og; N

ew T

L ;

Al2

O3

; alk

ali

3441

SB3

Nom

inal

for

Was

hing

@ 0

%20

2N

ot D

urab

le; N

ot L

Vis

c; ;

Hom

og; N

ew T

L ;

Al2

O3

; alk

ali

4260

SB3

Nom

inal

for

Was

hing

@ 0

%32

0N

ot D

urab

le; V

isc;

; N

ot H

omog

; New

TL

; A

l2O

3 ; N

ot a

lkal

i25

28SB

3 N

omin

al f

or W

ashi

ng @

0%

320

Not

Dur

able

; Not

L V

isc;

; N

ot H

omog

; New

TL

; A

l2O

3 ; N

ot a

lkal

i29

30SB

3 N

omin

al f

or W

ashi

ng @

0%

320

Not

Dur

able

; Not

L V

isc;

; N

ot H

omog

; New

TL

; A

l2O

3 ; a

lkal

i31

31SB

3 N

omin

al f

or W

ashi

ng @

0%

320

Not

Dur

able

; Not

L V

isc;

; H

omog

; New

TL

; A

l2O

3 ; a

lkal

i32

60SB

3 N

omin

al f

or W

ashi

ng @

0%

AD

urab

le; N

ot H

Vis

c; ;

Not

Hom

og; N

ew T

L ;

Al2

O3

; alk

ali

2531

SB3

Nom

inal

for

Was

hing

@ 0

%A

Dur

able

; Not

H V

isc;

; H

omog

; New

TL

; A

l2O

3 ; a

lkal

i32

39SB

3 N

omin

al f

or W

ashi

ng @

0%

AD

urab

le; V

isc;

; H

omog

; New

TL

; A

l2O

3 ; a

lkal

i40

53SB

3 N

omin

al f

or W

ashi

ng @

0%

AD

urab

le; N

ot L

Vis

c; ;

Hom

og; N

ew T

L ;

Al2

O3

; alk

ali

5454

SB3

Nom

inal

for

Was

hing

@ 0

%A

Not

Dur

able

; Not

L V

isc;

; H

omog

; New

TL

; A

l2O

3 ; a

lkal

i55

60SB

3 N

omin

al f

or W

ashi

ng @

0%

BD

urab

le; N

ot H

Vis

c; ;

Not

Hom

og; N

ew T

L ;

Al2

O3

; alk

ali

2530

SB3

Nom

inal

for

Was

hing

@ 0

%B

Dur

able

; Vis

c; ;

Not

Hom

og; N

ew T

L ;

Al2

O3

; alk

ali

3131

SB3

Nom

inal

for

Was

hing

@ 0

%B

Dur

able

; Vis

c; ;

Hom

og; N

ew T

L ;

Al2

O3

; alk

ali

3246

SB3

Nom

inal

for

Was

hing

@ 0

%B

Dur

able

; Not

L V

isc;

; H

omog

; New

TL

; A

l2O

3 ; a

lkal

i47

50SB

3 N

omin

al f

or W

ashi

ng @

0%

BN

ot D

urab

le; N

ot L

Vis

c; ;

Hom

og; N

ew T

L ;

Al2

O3

; alk

ali

5160

SB3

Nom

inal

for

Was

hing

@ 0

%C

Dur

able

; Not

H V

isc;

; N

ot H

omog

; New

TL

; A

l2O

3 ; a

lkal

i25

31SB

3 N

omin

al f

or W

ashi

ng @

0%

CD

urab

le; N

ot H

Vis

c; ;

Hom

og; N

ew T

L ;

Al2

O3

; alk

ali

3236

SB3

Nom

inal

for

Was

hing

@ 0

%C

Dur

able

; Vis

c; ;

Hom

og; N

ew T

L ;

Al2

O3

; alk

ali

3752

SB3

Nom

inal

for

Was

hing

@ 0

%C

Not

Dur

able

; Not

L V

isc;

; H

omog

; New

TL

; A

l2O

3 ; a

lkal

i53

60SB

3 N

omin

al f

or W

ashi

ng @

0%

DD

urab

le; N

ot H

Vis

c; ;

Not

Hom

og; N

ew T

L ;

Al2

O3

; alk

ali

2531

SB3

Nom

inal

for

Was

hing

@ 0

%D

Dur

able

; Not

H V

isc;

; H

omog

; New

TL

; A

l2O

3 ; a

lkal

i32

39SB

3 N

omin

al f

or W

ashi

ng @

0%

DD

urab

le; V

isc;

; H

omog

; New

TL

; A

l2O

3 ; a

lkal

i40

53SB

3 N

omin

al f

or W

ashi

ng @

0%

DN

ot D

urab

le; V

isc;

; H

omog

; New

TL

; A

l2O

3 ; a

lkal

i54

54SB

3 N

omin

al f

or W

ashi

ng @

0%

DN

ot D

urab

le; N

ot L

Vis

c; ;

Hom

og; N

ew T

L ;

Al2

O3

; alk

ali

5560

SB3

Nom

inal

for

Was

hing

@ 0

%E

Dur

able

; Not

H V

isc;

; N

ot H

omog

; New

TL

; A

l2O

3 ; a

lkal

i25

31SB

3 N

omin

al f

or W

ashi

ng @

0%

ED

urab

le; N

ot H

Vis

c; ;

Hom

og; N

ew T

L ;

Al2

O3

; alk

ali

3245

SB3

Nom

inal

for

Was

hing

@ 0

%E

Dur

able

; Vis

c; ;

Hom

og; N

ew T

L ;

Al2

O3

; alk

ali

4657

SB3

Nom

inal

for

Was

hing

@ 0

%E

Not

Dur

able

; Vis

c; ;

Hom

og; N

ew T

L ;

Al2

O3

; alk

ali

5858

SB3

Nom

inal

for

Was

hing

@ 0

%E

Not

Dur

able

; Not

L V

isc;

; H

omog

; New

TL

; A

l2O

3 ; a

lkal

i59

60SB

3 N

omin

al f

or W

ashi

ng @

0%

OD

urab

le; V

isc;

; N

ot H

omog

; New

TL

; A

l2O

3 ; a

lkal

i25

31SB

3 N

omin

al f

or W

ashi

ng @

0%

OD

urab

le; V

isc;

; H

omog

; New

TL

; A

l2O

3 ; a

lkal

i32

44SB

3 N

omin

al f

or W

ashi

ng @

0%

OD

urab

le; N

ot L

Vis

c; ;

Hom

og; N

ew T

L ;

Al2

O3

; alk

ali

4546

Imm

obil

izat

ion

Tec

hnol

ogy

Sect

ion

W

SRC

-TR

-200

2-00

491

Sava

nnah

Riv

er T

echn

olog

y C

ente

r R

ev. 0

Wes

tingh

ouse

Sav

anna

h R

iver

Com

pany

83

Typ

eFr

it I

DSa

tisf

ies

PAR

Min

(Slu

dge

Loa

ding

(%

))M

ax(S

ludg

e L

oadi

ng (

%))

SB3

Nom

inal

for

Was

hing

@ 0

%O

Not

Dur

able

; Not

L V

isc;

; H

omog

; New

TL

; A

l2O

3 ; a

lkal

i47

60SB

3 N

omin

al f

or W

ashi

ng @

0%

PD

urab

le; N

ot H

Vis

c; ;

Not

Hom

og; N

ew T

L ;

Al2

O3

; alk

ali

2530

SB3

Nom

inal

for

Was

hing

@ 0

%P

Dur

able

; Vis

c; ;

Not

Hom

og; N

ew T

L ;

Al2

O3

; alk

ali

3131

SB3

Nom

inal

for

Was

hing

@ 0

%P

Dur

able

; Vis

c; ;

Hom

og; N

ew T

L ;

Al2

O3

; alk

ali

3248

SB3

Nom

inal

for

Was

hing

@ 0

%P

Not

Dur

able

; Not

L V

isc;

; H

omog

; New

TL

; A

l2O

3 ; a

lkal

i49

60SB

3 N

omin

al f

or W

ashi

ng @

25%

202

Dur

able

; Vis

c; ;

Not

Hom

og; N

ew T

L ;

Al2

O3

; alk

ali

2530

SB3

Nom

inal

for

Was

hing

@ 2

5%20

2D

urab

le; V

isc;

; H

omog

; New

TL

; A

l2O

3 ; a

lkal

i31

40SB

3 N

omin

al f

or W

ashi

ng @

25%

202

Not

Dur

able

; Vis

c; ;

Hom

og; N

ew T

L ;

Al2

O3

; alk

ali

4144

SB3

Nom

inal

for

Was

hing

@ 2

5%20

2N

ot D

urab

le; N

ot L

Vis

c; ;

Hom

og; N

ew T

L ;

Al2

O3

; alk

ali

4560

SB3

Nom

inal

for

Was

hing

@ 2

5%32

0N

ot D

urab

le; V

isc;

; N

ot H

omog

; New

TL

; A

l2O

3 ; N

ot a

lkal

i25

28SB

3 N

omin

al f

or W

ashi

ng @

25%

320

Not

Dur

able

; Vis

c; ;

Not

Hom

og; N

ew T

L ;

Al2

O3

; alk

ali

2929

SB3

Nom

inal

for

Was

hing

@ 2

5%32

0N

ot D

urab

le; V

isc;

; H

omog

; New

TL

; A

l2O

3 ; a

lkal

i30

31SB

3 N

omin

al f

or W

ashi

ng @

25%

320

Not

Dur

able

; Not

L V

isc;

; H

omog

; New

TL

; A

l2O

3 ; a

lkal

i32

60SB

3 N

omin

al f

or W

ashi

ng @

25%

FD

urab

le; N

ot H

Vis

c; ;

Not

Hom

og; N

ew T

L ;

Al2

O3

; alk

ali

2529

SB3

Nom

inal

for

Was

hing

@ 2

5%F

Dur

able

; Not

H V

isc;

; H

omog

; New

TL

; A

l2O

3 ; a

lkal

i30

39SB

3 N

omin

al f

or W

ashi

ng @

25%

FD

urab

le; V

isc;

; H

omog

; New

TL

; A

l2O

3 ; a

lkal

i40

55SB

3 N

omin

al f

or W

ashi

ng @

25%

FD

urab

le; N

ot L

Vis

c; ;

Hom

og; N

ew T

L ;

Al2

O3

; alk

ali

5656

SB3

Nom

inal

for

Was

hing

@ 2

5%F

Not

Dur

able

; Not

L V

isc;

; H

omog

; New

TL

; A

l2O

3 ; a

lkal

i57

58SB

3 N

omin

al f

or W

ashi

ng @

25%

FN

ot D

urab

le; N

ot L

Vis

c; ;

Hom

og; N

ot N

ew T

L; A

l2O

3 ; a

lkal

i59

60SB

3 N

omin

al f

or W

ashi

ng @

25%

OD

urab

le; N

ot H

Vis

c; ;

Not

Hom

og; N

ew T

L ;

Al2

O3

; alk

ali

2527

SB3

Nom

inal

for

Was

hing

@ 2

5%O

Dur

able

; Vis

c; ;

Not

Hom

og; N

ew T

L ;

Al2

O3

; alk

ali

2829

SB3

Nom

inal

for

Was

hing

@ 2

5%O

Dur

able

; Vis

c; ;

Hom

og; N

ew T

L ;

Al2

O3

; alk

ali

3047

SB3

Nom

inal

for

Was

hing

@ 2

5%O

Dur

able

; Not

L V

isc;

; H

omog

; New

TL

; A

l2O

3 ; a

lkal

i48

50SB

3 N

omin

al f

or W

ashi

ng @

25%

OD

urab

le; N

ot L

Vis

c; ;

Hom

og; N

ot N

ew T

L; A

l2O

3 ; a

lkal

i51

57SB

3 N

omin

al f

or W

ashi

ng @

25%

ON

ot D

urab

le; N

ot L

Vis

c; ;

Hom

og; N

ot N

ew T

L; A

l2O

3 ; a

lkal

i58

60SB

3 N

omin

al f

or W

ashi

ng @

25%

PD

urab

le; N

ot H

Vis

c; ;

Not

Hom

og; N

ew T

L ;

Al2

O3

; alk

ali

2529

SB3

Nom

inal

for

Was

hing

@ 2

5%P

Dur

able

; Not

H V

isc;

; H

omog

; New

TL

; A

l2O

3 ; a

lkal

i30

33SB

3 N

omin

al f

or W

ashi

ng @

25%

PD

urab

le; V

isc;

; H

omog

; New

TL

; A

l2O

3 ; a

lkal

i34

51SB

3 N

omin

al f

or W

ashi

ng @

25%

PD

urab

le; V

isc;

; H

omog

; Not

New

TL

; Al2

O3

; alk

ali

5252

SB3

Nom

inal

for

Was

hing

@ 2

5%P

Dur

able

; Not

L V

isc;

; H

omog

; Not

New

TL

; Al2

O3

; alk

ali

5359

SB3

Nom

inal

for

Was

hing

@ 2

5%P

Not

Dur

able

; Not

L V

isc;

; H

omog

; Not

New

TL

; Al2

O3

; alk

ali

6060

SB3

Nom

inal

for

Was

hing

@ 2

5%Q

Dur

able

; Not

H V

isc;

; N

ot H

omog

; New

TL

; A

l2O

3 ; a

lkal

i25

29SB

3 N

omin

al f

or W

ashi

ng @

25%

QD

urab

le; N

ot H

Vis

c; ;

Hom

og; N

ew T

L ;

Al2

O3

; alk

ali

3044

SB3

Nom

inal

for

Was

hing

@ 2

5%Q

Dur

able

; Vis

c; ;

Hom

og; N

ew T

L ;

Al2

O3

; alk

ali

4555

SB3

Nom

inal

for

Was

hing

@ 2

5%Q

Dur

able

; Vis

c; ;

Hom

og; N

ot N

ew T

L; A

l2O

3 ; a

lkal

i56

58SB

3 N

omin

al f

or W

ashi

ng @

25%

QD

urab

le; N

ot L

Vis

c; ;

Hom

og; N

ot N

ew T

L; A

l2O

3 ; a

lkal

i59

60SB

3 N

omin

al f

or W

ashi

ng @

25%

SD

urab

le; N

ot H

Vis

c; ;

Not

Hom

og; N

ew T

L ;

Al2

O3

; alk

ali

2529

SB3

Nom

inal

for

Was

hing

@ 2

5%S

Dur

able

; Not

H V

isc;

; H

omog

; New

TL

; A

l2O

3 ; a

lkal

i30

33SB

3 N

omin

al f

or W

ashi

ng @

25%

SD

urab

le; V

isc;

; H

omog

; New

TL

; A

l2O

3 ; a

lkal

i34

51SB

3 N

omin

al f

or W

ashi

ng @

25%

SN

ot D

urab

le; V

isc;

; H

omog

; New

TL

; A

l2O

3 ; a

lkal

i52

52SB

3 N

omin

al f

or W

ashi

ng @

25%

SN

ot D

urab

le; N

ot L

Vis

c; ;

Hom

og; N

ew T

L ;

Al2

O3

; alk

ali

5360

SB3

Nom

inal

for

Was

hing

@ 2

5%T

Dur

able

; Not

H V

isc;

; N

ot H

omog

; New

TL

; A

l2O

3 ; a

lkal

i25

29

Imm

obil

izat

ion

Tec

hnol

ogy

Sect

ion

W

SRC

-TR

-200

2-00

491

Sava

nnah

Riv

er T

echn

olog

y C

ente

r R

ev. 0

Wes

tingh

ouse

Sav

anna

h R

iver

Com

pany

84

Typ

eFr

it I

DSa

tisf

ies

PAR

Min

(Slu

dge

Loa

ding

(%

))M

ax(S

ludg

e L

oadi

ng (

%))

SB3

Nom

inal

for

Was

hing

@ 2

5%T

Dur

able

; Not

H V

isc;

; H

omog

; New

TL

; A

l2O

3 ; a

lkal

i30

32SB

3 N

omin

al f

or W

ashi

ng @

25%

TD

urab

le; V

isc;

; H

omog

; New

TL

; A

l2O

3 ; a

lkal

i33

51SB

3 N

omin

al f

or W

ashi

ng @

25%

TN

ot D

urab

le; N

ot L

Vis

c; ;

Hom

og; N

ew T

L ;

Al2

O3

; alk

ali

5260

SB3

Nom

inal

for

Was

hing

@ 5

0%20

2D

urab

le; V

isc;

; N

ot H

omog

; New

TL

; A

l2O

3 ; a

lkal

i25

28SB

3 N

omin

al f

or W

ashi

ng @

50%

202

Dur

able

; Vis

c; ;

Hom

og; N

ew T

L ;

Al2

O3

; alk

ali

2945

SB3

Nom

inal

for

Was

hing

@ 5

0%20

2D

urab

le; V

isc;

; H

omog

; Not

New

TL

; Al2

O3

; alk

ali

4649

SB3

Nom

inal

for

Was

hing

@ 5

0%20

2D

urab

le; N

ot L

Vis

c; ;

Hom

og; N

ot N

ew T

L; A

l2O

3 ; a

lkal

i50

60SB

3 N

omin

al f

or W

ashi

ng @

50%

320

Not

Dur

able

; Vis

c; ;

Not

Hom

og; N

ew T

L ;

Al2

O3

; Not

alk

ali

2526

SB3

Nom

inal

for

Was

hing

@ 5

0%32

0N

ot D

urab

le; V

isc;

; N

ot H

omog

; New

TL

; A

l2O

3 ; a

lkal

i27

27SB

3 N

omin

al f

or W

ashi

ng @

50%

320

Not

Dur

able

; Vis

c; ;

Hom

og; N

ew T

L ;

Al2

O3

; alk

ali

2835

SB3

Nom

inal

for

Was

hing

@ 5

0%32

0N

ot D

urab

le; N

ot L

Vis

c; ;

Hom

og; N

ew T

L ;

Al2

O3

; alk

ali

3656

SB3

Nom

inal

for

Was

hing

@ 5

0%32

0N

ot D

urab

le; N

ot L

Vis

c; ;

Hom

og; N

ot N

ew T

L; A

l2O

3 ; a

lkal

i57

60SB

3 N

omin

al f

or W

ashi

ng @

50%

GD

urab

le; V

isc;

; N

ot H

omog

; New

TL

; A

l2O

3 ; a

lkal

i25

25SB

3 N

omin

al f

or W

ashi

ng @

50%

GD

urab

le; V

isc;

; H

omog

; New

TL

; A

l2O

3 ; a

lkal

i26

45SB

3 N

omin

al f

or W

ashi

ng @

50%

GD

urab

le; N

ot L

Vis

c; ;

Hom

og; N

ew T

L ;

Al2

O3

; alk

ali

4646

SB3

Nom

inal

for

Was

hing

@ 5

0%G

Not

Dur

able

; Not

L V

isc;

; H

omog

; New

TL

; A

l2O

3 ; a

lkal

i47

53SB

3 N

omin

al f

or W

ashi

ng @

50%

GN

ot D

urab

le; N

ot L

Vis

c; ;

Hom

og; N

ot N

ew T

L; A

l2O

3 ; a

lkal

i54

60SB

3 N

omin

al f

or W

ashi

ng @

50%

ID

urab

le; V

isc;

; N

ot H

omog

; New

TL

; A

l2O

3 ; a

lkal

i25

27SB

3 N

omin

al f

or W

ashi

ng @

50%

ID

urab

le; V

isc;

; H

omog

; New

TL

; A

l2O

3 ; a

lkal

i28

43SB

3 N

omin

al f

or W

ashi

ng @

50%

IN

ot D

urab

le; V

isc;

; H

omog

; New

TL

; A

l2O

3 ; a

lkal

i44

46SB

3 N

omin

al f

or W

ashi

ng @

50%

IN

ot D

urab

le; N

ot L

Vis

c; ;

Hom

og; N

ew T

L ;

Al2

O3

; alk

ali

4754

SB3

Nom

inal

for

Was

hing

@ 5

0%I

Not

Dur

able

; Not

L V

isc;

; H

omog

; Not

New

TL

; Al2

O3

; alk

ali

5560

SB3

Nom

inal

for

Was

hing

@ 7

5%N

ot D

urab

le; N

ot H

Vis

c; ;

Not

Hom

og; N

ot N

ew T

L; N

ot A

l2O

3; a

lkal

i26

26SB

3 N

omin

al f

or W

ashi

ng @

75%

202

Dur

able

; Not

H V

isc;

; N

ot H

omog

; New

TL

; A

l2O

3 ; a

lkal

i25

25SB

3 N

omin

al f

or W

ashi

ng @

75%

202

Dur

able

; Not

H V

isc;

; H

omog

; New

TL

; A

l2O

3 ; a

lkal

i27

28SB

3 N

omin

al f

or W

ashi

ng @

75%

202

Dur

able

; Vis

c; ;

Hom

og; N

ew T

L ;

Al2

O3

; alk

ali

2935

SB3

Nom

inal

for

Was

hing

@ 7

5%20

2D

urab

le; V

isc;

; H

omog

; Not

New

TL

; Al2

O3

; alk

ali

3655

SB3

Nom

inal

for

Was

hing

@ 7

5%20

2D

urab

le; N

ot L

Vis

c; ;

Hom

og; N

ot N

ew T

L; A

l2O

3 ; a

lkal

i56

60SB

3 N

omin

al f

or W

ashi

ng @

75%

320

Dur

able

; Vis

c; ;

Not

Hom

og; N

ew T

L ;

Al2

O3

; alk

ali

2525

SB3

Nom

inal

for

Was

hing

@ 7

5%32

0D

urab

le; V

isc;

; H

omog

; New

TL

; A

l2O

3 ; a

lkal

i26

41SB

3 N

omin

al f

or W

ashi

ng @

75%

320

Dur

able

; Not

L V

isc;

; H

omog

; New

TL

; A

l2O

3 ; a

lkal

i42

46SB

3 N

omin

al f

or W

ashi

ng @

75%

320

Dur

able

; Not

L V

isc;

; H

omog

; Not

New

TL

; Al2

O3

; alk

ali

4760

SB3

Nom

inal

for

Was

hing

@ 7

5%32

0-M

Dur

able

; Vis

c; ;

Hom

og; N

ew T

L ;

Al2

O3

; alk

ali

2544

SB3

Nom

inal

for

Was

hing

@ 7

5%32

0-M

Dur

able

; Not

L V

isc;

; H

omog

; Not

New

TL

; Al2

O3

; alk

ali

4560

SB3

Nom

inal

for

Was

hing

@ 7

5%H

Dur

able

; Vis

c; ;

Not

Hom

og; N

ew T

L ;

Al2

O3

; alk

ali

2525

SB3

Nom

inal

for

Was

hing

@ 7

5%H

Dur

able

; Vis

c; ;

Hom

og; N

ew T

L ;

Al2

O3

; alk

ali

2645

SB3

Nom

inal

for

Was

hing

@ 7

5%H

Dur

able

; Not

L V

isc;

; H

omog

; New

TL

; A

l2O

3 ; a

lkal

i46

46SB

3 N

omin

al f

or W

ashi

ng @

75%

HD

urab

le; N

ot L

Vis

c; ;

Hom

og; N

ot N

ew T

L; A

l2O

3 ; a

lkal

i47

60SB

3 N

omin

al f

or W

ashi

ng @

75%

KD

urab

le; V

isc;

; N

ot H

omog

; New

TL

; A

l2O

3 ; a

lkal

i25

25SB

3 N

omin

al f

or W

ashi

ng @

75%

KD

urab

le; V

isc;

; H

omog

; New

TL

; A

l2O

3 ; a

lkal

i26

45SB

3 N

omin

al f

or W

ashi

ng @

75%

KD

urab

le; N

ot L

Vis

c; ;

Hom

og; N

ew T

L ;

Al2

O3

; alk

ali

4646

SB3

Nom

inal

for

Was

hing

@ 7

5%K

Dur

able

; Not

L V

isc;

; H

omog

; Not

New

TL

; Al2

O3

; alk

ali

4760

Imm

obil

izat

ion

Tec

hnol

ogy

Sect

ion

W

SRC

-TR

-200

2-00

491

Sava

nnah

Riv

er T

echn

olog

y C

ente

r R

ev. 0

Wes

tingh

ouse

Sav

anna

h R

iver

Com

pany

85

Typ

eFr

it I

DSa

tisf

ies

PAR

Min

(Slu

dge

Loa

ding

(%

))M

ax(S

ludg

e L

oadi

ng (

%))

SB3

Nom

inal

for

Was

hing

@ 7

5%L

Dur

able

; Vis

c; ;

Not

Hom

og; N

ew T

L ;

Al2

O3

; alk

ali

2525

SB3

Nom

inal

for

Was

hing

@ 7

5%L

Dur

able

; Vis

c; ;

Hom

og; N

ew T

L ;

Al2

O3

; alk

ali

2643

SB3

Nom

inal

for

Was

hing

@ 7

5%L

Dur

able

; Not

L V

isc;

; H

omog

; New

TL

; A

l2O

3 ; a

lkal

i44

46SB

3 N

omin

al f

or W

ashi

ng @

75%

LD

urab

le; N

ot L

Vis

c; ;

Hom

og; N

ot N

ew T

L; A

l2O

3 ; a

lkal

i47

60SB

3 N

omin

al f

or W

ashi

ng @

100

%20

2D

urab

le; N

ot H

Vis

c; ;

Hom

og; N

ew T

L ;

Al2

O3

; alk

ali

2527

SB3

Nom

inal

for

Was

hing

@ 1

00%

202

Dur

able

; Not

H V

isc;

; H

omog

; Not

New

TL

; Al2

O3

; alk

ali

2837

SB3

Nom

inal

for

Was

hing

@ 1

00%

202

Dur

able

; Vis

c; ;

Hom

og; N

ot N

ew T

L; A

l2O

3 ; a

lkal

i38

60SB

3 N

omin

al f

or W

ashi

ng @

100

%32

0D

urab

le; V

isc;

; H

omog

; New

TL

; A

l2O

3 ; a

lkal

i25

37SB

3 N

omin

al f

or W

ashi

ng @

100

%32

0D

urab

le; V

isc;

; H

omog

; Not

New

TL

; Al2

O3

; alk

ali

3852

SB3

Nom

inal

for

Was

hing

@ 1

00%

320

Dur

able

; Not

L V

isc;

; H

omog

; Not

New

TL

; Al2

O3

; alk

ali

5360

SB3

Nom

inal

for

Was

hing

@ 1

00%

MD

urab

le; V

isc;

; H

omog

; New

TL

; A

l2O

3 ; a

lkal

i25

36SB

3 N

omin

al f

or W

ashi

ng @

100

%M

Dur

able

; Vis

c; ;

Hom

og; N

ot N

ew T

L; A

l2O

3 ; a

lkal

i37

55SB

3 N

omin

al f

or W

ashi

ng @

100

%M

Dur

able

; Not

L V

isc;

; H

omog

; Not

New

TL

; Al2

O3

; alk

ali

5660

SB3

Nom

inal

for

Was

hing

@ 1

00%

ND

urab

le; V

isc;

; H

omog

; New

TL

; A

l2O

3 ; a

lkal

i25

34SB

3 N

omin

al f

or W

ashi

ng @

100

%N

Dur

able

; Vis

c; ;

Hom

og; N

ot N

ew T

L; A

l2O

3 ; a

lkal

i35

60SB

3 N

omin

al f

or W

ashi

ng @

100

%R

Dur

able

; Vis

c; ;

Hom

og; N

ew T

L ;

Al2

O3

; alk

ali

2540

SB3

Nom

inal

for

Was

hing

@ 1

00%

RD

urab

le; V

isc;

; H

omog

; Not

New

TL

; Al2

O3

; alk

ali

4142

SB3

Nom

inal

for

Was

hing

@ 1

00%

RD

urab

le; N

ot L

Vis

c; ;

Hom

og; N

ot N

ew T

L; A

l2O

3 ; a

lkal

i43

60SB

3 N

omin

al f

or W

ashi

ng @

100

%32

0-M

Dur

able

; Vis

c; ;

Hom

og; N

ew T

L ;

Al2

O3

; alk

ali

2536

SB3

Nom

inal

for

Was

hing

@ 1

00%

320-

MD

urab

le; V

isc;

; H

omog

; Not

New

TL

; Al2

O3

; alk

ali

3755

SB3

Nom

inal

for

Was

hing

@ 1

00%

320-

MD

urab

le; N

ot L

Vis

c; ;

Hom

og; N

ot N

ew T

L; A

l2O

3 ; a

lkal

i56

60


86



87

Appendix C

Conversion Table of Frits Nomenclatures


88

Numeric Alphanumeric400 A401 B402 E403 C404 D405 O406 P407 Q408 F409 S410 T411 G412 I413 H414 K415 L416 320-M417 M418 N419 R420 202-M421 202-M2422 U423 U2


89

Appendix D

Phase 1 Assessment of Linear Washing Scenarios


90

Paper Study Results for 0% Washing with Frit 202(# of EVs = 455)

Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Visc; Not Homog; New TL ; Al2O3 ; Not alkali 6325 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 20725 Durable; Visc; Not Homog; New TL ; Not Al2O3; Not alkali 10425 Durable; Visc; Not Homog; New TL ; Not Al2O3; alkali 8126 Durable; Visc; Not Homog; New TL ; Al2O3 ; Not alkali 8826 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 26426 Not Durable; Visc; Not Homog; New TL ; Al2O3 ; Not alkali 10327 Durable; Visc; Not Homog; New TL ; Al2O3 ; Not alkali 5827 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 24527 Not Durable; Visc; Not Homog; New TL ; Al2O3 ; Not alkali 15228 Durable; Visc; Not Homog; New TL ; Al2O3 ; Not alkali 428 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 27528 Not Durable; Visc; Not Homog; New TL ; Al2O3 ; Not alkali 15228 Not Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 2429 Durable; Visc; Not Homog; New TL ; Al2O3 ; Not alkali 1529 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 24629 Not Durable; Visc; Not Homog; New TL ; Al2O3 ; Not alkali 14729 Not Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 4730 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 6130 Durable; Visc; Not Homog; New TL ; Al2O3 ; Not alkali 3030 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 15430 Not Durable; Visc; Not Homog; New TL ; Al2O3 ; Not alkali 14030 Not Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 7031 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 11931 Durable; Visc; Not Homog; New TL ; Al2O3 ; Not alkali 3831 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 6831 Not Durable; Visc; Not Homog; New TL ; Al2O3 ; Not alkali 13731 Not Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 9332 Durable; Visc; Homog; New TL ; Al2O3 ; Not alkali 2332 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 15832 Durable; Visc; Not Homog; New TL ; Al2O3 ; Not alkali 1332 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 1532 Not Durable; Visc; Homog; New TL ; Al2O3 ; Not alkali 1832 Not Durable; Visc; Not Homog; New TL ; Al2O3 ; Not alkali 12132 Not Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 10733 Durable; Visc; Homog; New TL ; Al2O3 ; Not alkali 3133 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 16533 Not Durable; Visc; Homog; New TL ; Al2O3 ; Not alkali 3133 Not Durable; Visc; Not Homog; New TL ; Al2O3 ; Not alkali 11533 Not Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 11334 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 18234 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 5934 Not Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 21435 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 17135 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 14935 Not Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 13536 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 15436 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 20236 Not Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 9937 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 14037 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 27237 Not Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 4338 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 11238 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 34339 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 5239 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 839 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 395


91

Sludge Loading (%) Satisfies PAR # of EVs40 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 13540 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 32041 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 19841 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 25742 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 26042 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 19543 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 31743 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 13844 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 43344 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 2245 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 45546 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 45547 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 45548 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 45549 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 45550 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 45551 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 45552 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 45553 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 45554 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 45555 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 45556 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 45557 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 45558 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 45559 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 45560 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 455

WL Range # of EVs and Centroid % of Total0 273 601 10 2.19780222 4 0.879120883 7 1.538461544 10 2.19780225 10 2.19780226 14 3.076923087 18 3.956043968 37 8.131868139 41 9.01098901

10 31 6.81318681


92


Sludge Loading (%) Satisfies PAR # of EVs25 Not Durable; Visc; Not Homo; New TL ; Al2O3 ; Not alkali 27025 Not Durable; Visc; Not Homo; New TL ; Not Al2O3; Not alkali 18526 Not Durable; Visc; Not Homo; New TL ; Al2O3 ; Not alkali 45527 Not Durable; Not L Visc; Not Homo; New TL ; Al2O3 ; Not alkali 5827 Not Durable; Visc; Not Homo; New TL ; Al2O3 ; Not alkali 39728 Not Durable; Not L Visc; Not Homo; New TL ; Al2O3 ; Not alkali 16428 Not Durable; Not L Visc; Not Homo; New TL ; Al2O3 ; alkali 1628 Not Durable; Visc; Not Homo; New TL ; Al2O3 ; Not alkali 10628 Not Durable; Visc; Not Homo; New TL ; Al2O3 ; alkali 16929 Not Durable; Not L Visc; Not Homo; New TL ; Al2O3 ; Not alkali 19729 Not Durable; Not L Visc; Not Homo; New TL ; Al2O3 ; alkali 5329 Not Durable; Visc; Homo; New TL ; Al2O3 ; Not alkali 229 Not Durable; Visc; Homo; New TL ; Al2O3 ; alkali 8129 Not Durable; Visc; Not Homo; New TL ; Al2O3 ; Not alkali 5629 Not Durable; Visc; Not Homo; New TL ; Al2O3 ; alkali 6630 Not Durable; Not L Visc; Homo; New TL ; Al2O3 ; Not alkali 1130 Not Durable; Not L Visc; Homo; New TL ; Al2O3 ; alkali 430 Not Durable; Not L Visc; Not Homo; New TL ; Al2O3 ; Not alkali 21630 Not Durable; Not L Visc; Not Homo; New TL ; Al2O3 ; alkali 8530 Not Durable; Visc; Homo; New TL ; Al2O3 ; Not alkali 730 Not Durable; Visc; Homo; New TL ; Al2O3 ; alkali 11330 Not Durable; Visc; Not Homo; New TL ; Al2O3 ; Not alkali 330 Not Durable; Visc; Not Homo; New TL ; Al2O3 ; alkali 1631 Not Durable; Not L Visc; Homo; New TL ; Al2O3 ; Not alkali 8031 Not Durable; Not L Visc; Homo; New TL ; Al2O3 ; alkali 12731 Not Durable; Not L Visc; Not Homo; New TL ; Al2O3 ; Not alkali 13731 Not Durable; Not L Visc; Not Homo; New TL ; Al2O3 ; alkali 9731 Not Durable; Visc; Homo; New TL ; Al2O3 ; alkali 1432 Not Durable; Not L Visc; Homo; New TL ; Al2O3 ; Not alkali 8132 Not Durable; Not L Visc; Homo; New TL ; Al2O3 ; alkali 14732 Not Durable; Not L Visc; Not Homo; New TL ; Al2O3 ; Not alkali 12132 Not Durable; Not L Visc; Not Homo; New TL ; Al2O3 ; alkali 10633 Not Durable; Not L Visc; Homo; New TL ; Al2O3 ; Not alkali 8233 Not Durable; Not L Visc; Homo; New TL ; Al2O3 ; alkali 19833 Not Durable; Not L Visc; Not Homo; New TL ; Al2O3 ; Not alkali 10933 Not Durable; Not L Visc; Not Homo; New TL ; Al2O3 ; alkali 6634 Not Durable; Not L Visc; Homo; New TL ; Al2O3 ; alkali 33634 Not Durable; Not L Visc; Not Homo; New TL ; Al2O3 ; alkali 11935 Not Durable; Not L Visc; Homo; New TL ; Al2O3 ; alkali 37235 Not Durable; Not L Visc; Not Homo; New TL ; Al2O3 ; alkali 8336 Not Durable; Not L Visc; Homo; New TL ; Al2O3 ; alkali 43436 Not Durable; Not L Visc; Not Homo; New TL ; Al2O3 ; alkali 2137 Not Durable; Not L Visc; Homo; New TL ; Al2O3 ; alkali 45538 Not Durable; Not L Visc; Homo; New TL ; Al2O3 ; alkali 45539 Not Durable; Not L Visc; Homo; New TL ; Al2O3 ; alkali 45540 Not Durable; Not L Visc; Homo; New TL ; Al2O3 ; alkali 45541 Not Durable; Not L Visc; Homo; New TL ; Al2O3 ; alkali 45542 Not Durable; Not L Visc; Homo; New TL ; Al2O3 ; alkali 45543 Not Durable; Not L Visc; Homo; New TL ; Al2O3 ; alkali 45544 Not Durable; Not L Visc; Homo; New TL ; Al2O3 ; alkali 45545 Not Durable; Not L Visc; Homo; New TL ; Al2O3 ; alkali 45546 Not Durable; Not L Visc; Homo; New TL ; Al2O3 ; alkali 45547 Not Durable; Not L Visc; Homo; New TL ; Al2O3 ; alkali 45548 Not Durable; Not L Visc; Homo; New TL ; Al2O3 ; alkali 45549 Not Durable; Not L Visc; Homo; New TL ; Al2O3 ; alkali 455


93

Sludge Loading (%) Satisfies PAR # of EVs50 Not Durable; Not L Visc; Homo; New TL ; Al2O3 ; alkali 45551 Not Durable; Not L Visc; Homo; New TL ; Al2O3 ; alkali 45552 Not Durable; Not L Visc; Homo; New TL ; Al2O3 ; alkali 45553 Not Durable; Not L Visc; Homo; New TL ; Al2O3 ; alkali 45554 Not Durable; Not L Visc; Homo; New TL ; Al2O3 ; alkali 45555 Not Durable; Not L Visc; Homo; New TL ; Al2O3 ; alkali 45556 Not Durable; Not L Visc; Homo; New TL ; Al2O3 ; alkali 45557 Not Durable; Not L Visc; Homo; New TL ; Al2O3 ; alkali 45558 Not Durable; Not L Visc; Homo; New TL ; Al2O3 ; alkali 45559 Not Durable; Not L Visc; Homo; New TL ; Al2O3 ; alkali 45560 Not Durable; Not L Visc; Homo; New TL ; Al2O3 ; alkali 455


94

Paper Study Results for 0% Washing with Frit A (400)(# of EVs = 455)

Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 27025 Durable; Not H Visc; ; Not Homog; New TL ; Not Al2O3; alkali 18526 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 45527 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 45528 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 45529 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 8329 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 37230 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 13530 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 32031 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 22131 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 23432 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 22832 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 22733 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 28033 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 17534 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 33634 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 11935 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 37235 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 8336 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 43436 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 2137 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 45538 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 35038 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 10539 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 27339 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 18240 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 21040 Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 340 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 24241 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 13541 Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 1841 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 30242 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 3342 Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 642 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 37942 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 3743 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 38343 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 7244 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 34944 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 10645 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 31945 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 13646 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 30046 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 15547 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 28847 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 16748 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 24048 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 17448 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 4149 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 14549 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 17849 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 13250 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 11950 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 18250 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 15451 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 9751 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 18451 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 174


95

Sludge Loading (%) Satisfies PAR # of EVs52 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 7752 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 19052 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 10252 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 8653 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 1153 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 5053 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 19253 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 16653 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 3654 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 2854 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 1454 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 1154 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 18554 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 19154 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 2655 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 1955 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 3855 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 355 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 16255 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 22755 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 656 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 756 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 9956 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 10256 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 24356 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 457 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 157 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 19357 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 257 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 24657 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 1358 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 18458 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 24758 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 2459 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 17359 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 24359 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 3960 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 16660 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 24060 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 49

WL Range # of EVs and Centroid % of Total0 49 10.76923081 28 6.153846152 30 6.593406593 33 7.252747254 11 2.417582425 13 2.857142866 7 1.538461547 2 0.439560448 3 0.659340669 5 1.0989011

10 69 15.164835211 94 20.659340712 41 9.0109890113 28 6.1538461514 40 8.7912087915 2 0.43956044


96

Paper Study Results for 0% Washing with Frit B (401)(# of EVs = 455)

Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 27025 Durable; Not H Visc; ; Not Homog; New TL ; Not Al2O3; alkali 18526 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 45527 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 45528 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 44728 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 829 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 8329 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 22429 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 14830 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 12730 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 10530 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 830 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 21531 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 16131 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 831 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 6031 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 22632 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 6032 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 16832 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 22733 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 28033 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 17534 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 33634 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 11935 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 37235 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 8336 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 43436 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 2137 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 45237 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 338 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 43638 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 1939 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 40639 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 4940 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 37640 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 7941 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 34341 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 11242 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 31642 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 13943 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 29543 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 16044 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 544 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 26144 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 16944 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 2045 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 745 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 15145 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 17445 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 11745 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 646 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 4146 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 8346 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 18046 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 15147 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 7247 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 647 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 29


97

Sludge Loading (%) Satisfies PAR # of EVs47 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 17647 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 17248 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 7748 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 4248 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 448 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 14548 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 18749 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 6449 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 14249 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 4849 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 20150 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 4450 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 19550 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 21651 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 2351 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 20051 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 23252 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 952 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 20152 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 24553 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 253 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 19553 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 24753 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 1154 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 18654 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 24754 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 2255 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 17555 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 24755 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 3356 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 16756 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 24156 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 4757 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 14857 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 24057 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 6758 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 13458 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 24058 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 8159 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 8559 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 23659 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 13460 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 2560 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 23460 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 196

WL Range # of EVs and Centroid % of Total5 9 1.978021986 17 3.736263747 36 7.912087918 63 13.84615389 78 17.1428571

10 60 13.186813211 35 7.6923076912 19 4.1758241813 40 8.7912087914 34 7.4725274715 32 7.0329670316 28 6.1538461517 4 0.87912088


98

Paper Study Results for 0% Washing with Frit E (402)(# of EVs = 455)

Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 27025 Durable; Not H Visc; ; Not Homog; New TL ; Not Al2O3; alkali 18526 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 45527 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 45528 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 45529 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 8329 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 37230 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 13530 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 32031 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 22131 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 23432 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 22832 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 22733 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 28033 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 17534 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 33634 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 11935 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 37235 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 8336 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 43436 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 2137 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 45538 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 45539 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 45540 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 45541 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 45542 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 45442 Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 143 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 44043 Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 1544 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 31544 Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 3044 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 11045 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 20945 Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 6245 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 18446 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 11346 Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 10046 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 24247 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 4147 Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 11347 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 29147 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 1048 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 648 Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 5548 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 29948 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 9549 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 29549 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 16050 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 28450 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 17151 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 20951 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 17551 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 7152 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 13452 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 181


99

Sludge Loading (%) Satisfies PAR # of EVs52 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 14053 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 10653 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 18353 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 16654 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 8954 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 18854 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 17855 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 7255 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 19055 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 19356 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 5156 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 19756 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 1156 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 19657 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 3357 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 20057 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 13757 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 8558 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 858 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 558 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 758 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 19758 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 18658 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 5259 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 359 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 2759 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 17359 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 22359 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 759 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 2260 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 5860 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 13360 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 24560 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 1760 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 2


10 26 5.7142857111 6 1.3186813212 11 2.4175824213 17 3.73626374


100

Paper Study Results for 0% Washing with Frit C (403)(# of EVs = 455)

Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 27025 Durable; Not H Visc; ; Not Homog; New TL ; Not Al2O3; alkali 18526 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 45527 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 45528 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 45529 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 8329 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 37230 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 13530 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 32031 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 22131 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 23432 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 22832 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 22733 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 28033 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 17534 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 33634 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 11935 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 32835 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 1035 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 4435 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 7336 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 26436 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 17036 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 2137 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 19837 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 25738 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 13938 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 31639 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 2039 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 43540 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 45541 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 45542 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 45543 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 45544 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 45545 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 45546 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 34646 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 10947 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 30747 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 14848 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 28048 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 548 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 17049 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 25849 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 1449 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 18350 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 22850 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 2950 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 2450 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 17451 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 351 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 17851 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 6251 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 14351 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 6952 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 2352 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 12652 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 79


101

Sludge Loading (%) Satisfies PAR # of EVs52 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 18452 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 4353 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 4053 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 5453 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 11953 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 22553 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 1754 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 4854 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 2354 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 1354 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 11654 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 25354 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 255 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 3355 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 13955 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 355 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 1355 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 26756 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 1056 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 16656 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 27957 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 157 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 16757 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 28157 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 658 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 15158 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 28058 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 2459 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 13759 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 27459 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 4460 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 9860 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 27360 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 84

WL Range # of EVs and Centroid % of Total9 24 5.27472527

10 69 15.164835211 74 16.263736312 77 16.923076913 44 9.6703296714 54 11.868131915 35 7.6923076916 78 17.1428571


102

Paper Study Results for 0% Washing with Frit D (404)(# of EVs = 455)

Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 27025 Durable; Not H Visc; ; Not Homog; New TL ; Not Al2O3; alkali 18526 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 45527 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 45528 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 45529 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 8329 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 37230 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 13530 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 32031 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 22131 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 23432 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 22832 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 22733 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 28033 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 17534 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 33634 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 11935 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 37235 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 8336 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 43436 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 2137 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 43737 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 1838 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 30838 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 14739 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 24239 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 21340 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 18440 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 27141 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 11541 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 34042 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 542 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 45043 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 45544 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 45545 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 45546 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 45547 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36147 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 9448 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 31148 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 14449 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 27649 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 1049 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 16950 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 25750 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 1750 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 18151 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 21551 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 4451 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 19652 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 17452 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 7152 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 2852 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 18253 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 253 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 13253 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 9753 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 150


103

Sludge Loading (%) Satisfies PAR # of EVs53 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 7454 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 1854 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 7254 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 12554 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 19354 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 4755 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 3255 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 2655 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 14455 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 23655 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 1756 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 3356 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 3356 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 456 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 12056 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 26456 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 157 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 1157 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 15557 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 157 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 1157 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 27758 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 158 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 16858 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 28058 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 659 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 15159 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 28059 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 2460 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 13860 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 27360 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 44

WL Range # of EVs and Centroid % of Total7 10 2.19780228 5 1.09890119 115 25.2747253

10 93 20.439560411 62 13.626373612 48 10.549450513 30 6.5934065914 18 3.9560439615 71 15.604395616 3 0.65934066


104

Paper Study Results for 0% Washing with Frit O (405)(# of EVs = 455)

Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali; No Neph 17925 Durable; Not H Visc; ; Not Homog; New TL ; Not Al2O3; alkali; No Neph 2725 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali; No Neph 9125 Durable; Visc; ; Not Homog; New TL ; Not Al2O3; alkali; No Neph 15826 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali; No Neph 13026 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali; No Neph 32527 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali; No Neph 327 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali; No Neph 45228 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali; No Neph 45529 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali; No Neph 8329 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali; No Neph 37230 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali; No Neph 13530 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali; No Neph 32031 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali; No Neph 22131 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali; No Neph 23432 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali; No Neph 22832 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali; No Neph 22733 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali; No Neph 28033 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali; No Neph 17534 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali; No Neph 33634 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali; No Neph 11935 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali; No Neph 37235 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali; No Neph 8336 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali; No Neph 43436 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali; No Neph 2137 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali; No Neph 45538 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali; No Neph 45539 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali; No Neph 45540 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali; No Neph 37540 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali; No Neph 8041 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali; No Neph 31241 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali; No Neph 14342 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali; No Neph 28842 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali; No Neph 842 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali; No Neph 15943 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali; No Neph 243 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali; No Neph 27343 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali; No Neph 13143 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali; No Neph 4944 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali; No Neph 2244 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali; No Neph 23844 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali; No Neph 17344 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali; No Neph 2245 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali; No Neph 5345 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali; No Neph 19245 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali; No Neph 20345 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali; No Neph 746 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali; No Neph 9046 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali; No Neph 14146 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali; No Neph 22447 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali; No Neph 18647 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali; No Neph 2947 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali; No Neph 24048 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali; No Neph 20248 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali; Neph Likely 7048 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali; No Neph 183


105

Sludge Loading (%) Satisfies PAR # of EVs49 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali; No Neph 19049 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali; Neph Likely 22149 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali; No Neph 4450 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali; Neph Likely 250 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali; No Neph 17650 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali; Neph Likely 23050 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali; No Neph 4751 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali; Neph Likely 11251 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali; No Neph 5351 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali; Neph Likely 551 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali; Neph Likely 25451 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali; No Neph 3152 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali; Neph Likely 13552 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali; No Neph 452 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali; Neph Likely 1452 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali; Neph Likely 28652 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali; No Neph 1653 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali; Neph Likely 11553 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali; Neph Likely 2553 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali; Neph Likely 31554 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali; Neph Likely 5554 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali; Neph Likely 5854 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali; Neph Likely 33854 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali; Neph Likely 455 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali; Neph Likely 1655 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali; Neph Likely 3755 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali; Neph Likely 36055 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali; Neph Likely 4256 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali; Neph Likely 34256 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali; Neph Likely 11357 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali; Neph Likely 31857 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali; Neph Likely 13758 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali; Neph Likely 30858 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali; Neph Likely 14759 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali; Neph Likely 29559 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali; Neph Likely 16060 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali; Neph Likely 28960 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali; Neph Likely 166

WL Range # of EVs and Centroid % of Total3 18 3.956043964 44 9.670329675 38 8.351648356 21 4.615384627 18 3.956043968 10 2.19780229 21 4.61538462

10 16 3.5164835211 18 3.9560439612 19 4.1758241813 23 5.0549450514 36 7.9120879115 29 6.3736263716 7 1.5384615417 43 9.4505494518 92 20.219780219 2 0.43956044


106

Paper Study Results for 0% Washing with Frit P (406)(# of EVs = 455)

Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 27025 Durable; Not H Visc; ; Not Homog; New TL ; Not Al2O3; alkali 18526 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 45527 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 45528 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 45529 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 8329 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 31829 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 5430 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 13130 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 14630 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 430 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 17431 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 17431 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 3431 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 4731 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 20032 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 14032 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 232 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 8832 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 22533 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 1933 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 26133 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 17534 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 33634 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 11935 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 37235 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 8336 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 43436 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 2137 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 45538 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 45539 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 45540 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 45541 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 45542 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 41242 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 4343 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 32143 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 13444 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 29644 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 15945 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 28045 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 17546 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 26546 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 246 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 18847 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 147 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 25047 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 11647 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 8848 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 1548 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 22148 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 17248 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 4749 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 3949 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 18249 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 20549 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 2950 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 59


107

Sludge Loading (%) Satisfies PAR # of EVs50 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 14850 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 24250 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 651 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 13451 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 6151 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 26052 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 17452 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 952 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 27253 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 15953 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 1453 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 28254 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 13854 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 2854 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 28955 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 8455 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 6255 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 30956 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 5456 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 7456 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 32256 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 557 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 657 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 7257 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 33457 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 4358 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 1658 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 31758 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 12259 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 30559 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 15060 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 29160 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 164


10 15 3.296703311 12 2.6373626412 20 4.395604413 16 3.5164835214 16 3.5164835215 10 2.197802216 5 1.098901117 14 3.0769230818 162 35.604395619 51 11.2087912


108


Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 46526 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 46527 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 46528 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 4728 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 41829 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 9529 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 37030 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 19430 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 27131 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 23331 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; Not alkali 9031 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 14232 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 30032 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 16533 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36833 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 3833 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 633 Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 5334 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 35134 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 5934 Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 5535 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 32735 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 12535 Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 1336 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 28036 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 18537 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 27037 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 19538 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 26038 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 20539 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 25239 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 21340 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 24340 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 22241 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 23241 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 23342 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 22242 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 942 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 23443 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 21543 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 9643 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 15444 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 144 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 20644 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 18144 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 7745 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 1445 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 18645 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 23345 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 3246 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 7646 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 11746 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 26346 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 947 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 12947 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 5847 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 27747 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 1


109

Sludge Loading (%) Satisfies PAR # of EVs48 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 16948 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 348 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 548 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 28849 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 12149 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 2149 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 32350 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 7950 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 5050 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 33550 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 151 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 3851 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 8451 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 33351 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 1052 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 652 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 9752 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 32652 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 3653 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 7953 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 29453 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 9254 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 5854 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 27754 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 13055 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 3755 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 26455 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 16456 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 656 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 25656 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 20357 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 25057 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 21558 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 24458 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 22159 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 23959 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 22660 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 23660 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 229


10 3 0.6451612911 3 0.6451612912 7 1.5053763413 6 1.2903225814 11 2.365591415 44 9.4623655916 36 7.7419354817 14 3.0107526918 44 9.4623655919 54 11.6129032


110



111


Sludge Loading (%) Satisfies PAR # of EVs25 Not Durable; Visc; ; Not Homo; New TL ; Al2O3 ; Not alkali 46526 Not Durable; Visc; ; Not Homo; New TL ; Al2O3 ; Not alkali 28026 Not Durable; Visc; ; Not Homo; New TL ; Al2O3 ; alkali 18527 Not Durable; Visc; ; Homo; New TL ; Al2O3 ; Not alkali 327 Not Durable; Visc; ; Homo; New TL ; Al2O3 ; alkali 5227 Not Durable; Visc; ; Not Homo; New TL ; Al2O3 ; Not alkali 25827 Not Durable; Visc; ; Not Homo; New TL ; Al2O3 ; alkali 15228 Not Durable; Visc; ; Homo; New TL ; Al2O3 ; Not alkali 2628 Not Durable; Visc; ; Homo; New TL ; Al2O3 ; alkali 8928 Not Durable; Visc; ; Not Homo; New TL ; Al2O3 ; Not alkali 21628 Not Durable; Visc; ; Not Homo; New TL ; Al2O3 ; alkali 13429 Not Durable; Not L Visc; ; Not Homo; New TL ; Al2O3 ; Not alkali 329 Not Durable; Visc; ; Homo; New TL ; Al2O3 ; Not alkali 11029 Not Durable; Visc; ; Homo; New TL ; Al2O3 ; alkali 11429 Not Durable; Visc; ; Not Homo; New TL ; Al2O3 ; Not alkali 10829 Not Durable; Visc; ; Not Homo; New TL ; Al2O3 ; alkali 13030 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; Not alkali 630 Not Durable; Not L Visc; ; Not Homo; New TL ; Al2O3 ; Not alkali 8730 Not Durable; Not L Visc; ; Not Homo; New TL ; Al2O3 ; alkali 230 Not Durable; Visc; ; Homo; New TL ; Al2O3 ; Not alkali 10230 Not Durable; Visc; ; Homo; New TL ; Al2O3 ; alkali 13330 Not Durable; Visc; ; Not Homo; New TL ; Al2O3 ; Not alkali 630 Not Durable; Visc; ; Not Homo; New TL ; Al2O3 ; alkali 12931 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; Not alkali 4131 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 4331 Not Durable; Not L Visc; ; Not Homo; New TL ; Al2O3 ; Not alkali 7431 Not Durable; Not L Visc; ; Not Homo; New TL ; Al2O3 ; alkali 3731 Not Durable; Visc; ; Homo; New TL ; Al2O3 ; Not alkali 7331 Not Durable; Visc; ; Homo; New TL ; Al2O3 ; alkali 17731 Not Durable; Visc; ; Not Homo; New TL ; Al2O3 ; alkali 2032 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 18532 Not Durable; Not L Visc; ; Not Homo; New TL ; Al2O3 ; alkali 7532 Not Durable; Visc; ; Homo; New TL ; Al2O3 ; alkali 20533 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 31933 Not Durable; Not L Visc; ; Not Homo; New TL ; Al2O3 ; alkali 4333 Not Durable; Visc; ; Homo; New TL ; Al2O3 ; alkali 10334 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 44334 Not Durable; Visc; ; Homo; New TL ; Al2O3 ; alkali 2235 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 46536 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 46537 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 46538 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 46539 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 46540 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 46541 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 46542 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 46543 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 46544 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 46545 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 46546 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 46547 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 46548 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 46549 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 46550 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 46551 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 46552 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 46553 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 465


112

Sludge Loading (%) Satisfies PAR # of EVs54 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 46555 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 46556 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 46557 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 46558 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 46559 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 46560 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 45760 Not Durable; Not L Visc; ; Homo; Not New TL; Al2O3 ; alkali 8


113

Paper Study Results for 25% Washing with Frit F (408)(# of EVs = 465)

Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 46526 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 46527 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 5527 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 41028 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 11528 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 35029 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 22429 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 24130 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 24130 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 22431 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 33331 Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 131 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 13132 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 36332 Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 2732 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 7533 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 32833 Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 9433 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 4334 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 30734 Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 15835 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 27035 Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 19536 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 25736 Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 20837 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 25037 Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 21538 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 24338 Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 22239 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 23839 Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 22740 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 23640 Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 22941 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 23341 Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 23242 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 22942 Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 23643 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 22843 Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 23744 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 22744 Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 23845 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 22245 Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 24346 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 21646 Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 24846 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 147 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 15347 Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 25047 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 6147 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 148 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 8048 Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 24348 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 13048 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 1249 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 1249 Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 22249 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 19249 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 39


114

Sludge Loading (%) Satisfies PAR # of EVs50 Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 14850 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 19750 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 12051 Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 8851 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 19151 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 18652 Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 1152 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 18052 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 27453 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 17053 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 29554 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 15054 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 31555 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 12955 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 33656 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 10956 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 35657 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 9557 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 37058 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 7258 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 39359 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 1059 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 3659 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 40159 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 1559 Not Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 360 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 260 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 2760 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 660 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 35460 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 3460 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 3460 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 260 Not Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 6


10 28 6.0215053811 21 4.5161290312 34 7.3118279613 14 3.01075269


115

Paper Study Results for 25% Washing with Frit O (405)(# of EVs = 465)

Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 46325 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 226 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 36226 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 10327 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 5527 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 19227 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 21828 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 10628 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 4528 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 928 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 30529 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 5829 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 529 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 16629 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 23630 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 230 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 23930 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 22431 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 33431 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 13132 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 39032 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 7533 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 42233 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 4334 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 46535 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 46536 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 46537 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 46538 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 46238 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 339 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 44839 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 1740 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 41140 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 5441 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36041 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 10542 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 31142 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 15443 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 28643 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 17944 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 26944 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 19645 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 645 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 25345 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 20646 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 9046 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 16246 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 21347 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 16847 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 647 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 7747 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 21448 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 17848 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 3648 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 3448 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 19048 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 2749 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 143


116

Sludge Loading (%) Satisfies PAR # of EVs49 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 10549 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 1249 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 12449 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 8150 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 11250 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 16550 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 150 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 6550 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 12251 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 8851 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 22651 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 751 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 14452 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 4452 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 23652 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 18553 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 3153 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 23953 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 19554 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 2054 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 24054 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 20555 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 855 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 24455 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 21255 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 156 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 156 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 24256 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 21356 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 957 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 23357 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 21357 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 1958 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 22458 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 20558 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 3659 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 21559 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 20159 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 4960 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 20760 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 19460 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 64


10 22 4.731182811 43 9.2473118312 88 18.924731213 63 13.548387114 55 11.82795715 44 9.4623655916 41 8.817204317 59 12.68817218 31 6.6666666719 12 2.58064516


117

Paper Study Results for 25% Washing with Frit P (406)(# of EVs = 465)

Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 46526 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 46527 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 5527 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 41028 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 11528 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 35029 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 22429 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 24130 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 24130 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 22431 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 33231 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 13131 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 232 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 35232 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 2132 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 3832 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 5433 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 27733 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 14533 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 4334 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 20734 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 25835 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 10935 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 35636 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 2736 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 43837 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 46538 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 46539 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 46239 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 340 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 44540 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 2041 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 40941 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 5642 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 35242 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 11343 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 30643 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 15944 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 28244 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 18345 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 26645 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 19946 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 25746 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 20847 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 25147 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 21448 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 24548 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 22049 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 249 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 23749 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 22650 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 6050 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 17650 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 22951 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 7051 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 1051 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 10451 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 220


118

Sludge Loading (%) Satisfies PAR # of EVs51 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 6152 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 8152 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 3752 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 4052 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 19652 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 11153 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 8153 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 9553 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 1453 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 14153 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 13454 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 4754 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 14854 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 9154 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 17955 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 3255 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 22555 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 1655 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 19256 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 1956 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 24556 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 20157 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 757 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 24857 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 20757 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 358 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 158 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 24458 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 21058 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 1059 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 23759 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 20559 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 2360 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 22660 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 20060 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 39


10 11 2.365591411 5 1.0752688212 9 1.9354838713 5 1.0752688214 6 1.2903225815 3 0.6451612916 17 3.6559139817 50 10.752688218 115 24.731182819 63 13.5483871


119

Paper Study Results for 25% Washing with Frit Q (407)(# of EVs = 465)

Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 46325 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 226 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 36226 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 10327 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 5527 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 19227 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 21828 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 10628 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 4528 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 928 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 30529 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 5829 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 529 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 16629 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 23630 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 230 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 23930 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 22431 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 33431 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 13132 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 39032 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 7533 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 42233 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 4334 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 46535 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 46536 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 46537 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 46538 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 46238 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 339 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 44839 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 1740 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 41140 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 5441 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36041 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 10542 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 31142 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 15443 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 28643 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 17944 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 26944 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 19645 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 645 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 25345 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 20646 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 9046 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 16246 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 21347 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 16847 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 647 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 7747 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 21448 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 17848 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 3648 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 3448 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 19048 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 2749 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 143


120

Sludge Loading (%) Satisfies PAR # of EVs49 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 10549 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 1249 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 12449 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 8150 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 11250 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 16550 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 150 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 6550 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 12251 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 8851 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 22651 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 751 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 14452 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 4452 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 23652 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 18553 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 3153 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 23953 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 19554 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 2054 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 24054 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 20555 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 855 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 24455 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 21255 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 156 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 156 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 24256 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 21356 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 957 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 23357 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 21357 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 1958 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 22458 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 20558 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 3659 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 21559 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 20159 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 4960 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 20760 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 19460 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 64


10 22 4.731182811 43 9.2473118312 88 18.924731213 63 13.548387114 55 11.82795715 44 9.4623655916 41 8.817204317 59 12.68817218 31 6.6666666719 12 2.58064516


121

Paper Study Results for 25% Washing with Frit S (409)(# of EVs = 465)

Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 46526 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 46527 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 5527 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 41028 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 11528 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 35029 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 22429 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 24130 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 24130 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 22431 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 33331 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 13131 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 132 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 35232 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 2532 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 3832 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 5033 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 27933 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 14333 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 4334 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 21034 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 25535 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 11235 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 35336 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 3036 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 43537 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 46538 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 46539 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 46540 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 46541 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 46542 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 46543 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 41543 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 5044 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36844 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 9745 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 33745 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 12846 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 29646 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 16947 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 27647 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 18948 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 26648 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 19949 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 25049 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 849 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 20750 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 20850 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 4250 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 3150 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 18451 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 551 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 15651 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 7951 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 11251 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 11352 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 2152 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 83


122

Sludge Loading (%) Satisfies PAR # of EVs52 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 12552 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 18952 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 4753 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 3353 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 753 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 1953 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 16253 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 22153 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 2354 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 2554 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 8354 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 154 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 10454 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 24654 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 655 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 1055 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 16355 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 3455 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 25555 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 356 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 256 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 19756 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 25556 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 1157 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 19357 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 25157 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 2158 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 18758 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 24558 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 3359 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 17559 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 23959 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 5160 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 13960 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 23660 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 90


10 13 2.7956989211 32 6.8817204312 46 9.8924731213 63 13.548387114 53 11.397849515 51 10.967741916 41 8.817204317 38 8.1720430118 44 9.4623655919 48 10.3225806


123

Paper Study Results for 25% Washing with Frit T (410)(# of EVs = 465)

Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 46526 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 46527 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 5527 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 41028 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 11528 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 35029 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 22429 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 24130 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 23730 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 20830 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 430 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 1631 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 30831 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 3631 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 2631 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 9532 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 24132 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 14932 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 7533 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 15033 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 27233 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 4334 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 6834 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 39735 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 535 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 46036 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 46537 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 46538 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 46539 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 46540 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 46541 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 46542 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 46543 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 42843 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 3744 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 37444 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 9145 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 33945 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 12646 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 30846 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 15747 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 27847 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 18748 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 26948 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 19649 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 25149 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 849 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 1549 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 19150 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 350 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 20450 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 4350 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 9750 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 11851 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 2051 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 13151 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 9051 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 169


124

Sludge Loading (%) Satisfies PAR # of EVs51 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 5552 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 4152 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 152 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 6452 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 12552 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 20752 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 2753 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 4553 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 6053 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 653 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 11153 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 23553 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 854 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 2554 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 14254 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 154 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 4754 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 25055 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 955 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 19555 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 355 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 25555 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 356 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 356 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 19856 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 25256 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 1257 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 19357 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 25057 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 2258 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 18758 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 24458 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 3459 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 17759 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 23959 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 4960 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 14060 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 23660 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 89


10 16 3.4408602211 24 5.1612903212 23 4.9462365613 22 4.731182814 41 8.817204315 59 12.68817216 57 12.258064517 45 9.6774193518 41 8.817204319 54 11.612903220 53 11.3978495


125


Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 5625 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 39926 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 526 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 1726 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 43327 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 6527 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 39028 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 19528 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 26029 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 24829 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 20730 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 35130 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 10431 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 41431 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 4132 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 44232 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 1333 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 45534 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 45535 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 45536 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 45537 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 45538 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 45539 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 44739 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 840 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 41340 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 4241 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 34241 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 11342 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 27842 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 17743 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 24743 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 20844 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 23544 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 22045 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 23145 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 22446 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 746 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 21946 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 22947 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 5347 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 347 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 16847 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 23148 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 6348 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 1548 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 13648 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 22548 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 1649 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 11749 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 3649 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 5049 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 21349 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 3950 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 11850 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 16150 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 350 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 118


126

Sludge Loading (%) Satisfies PAR # of EVs50 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 5551 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 8251 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 21651 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 8151 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 6551 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 1152 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 3052 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 29052 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 4152 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 5852 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 3653 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 653 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 33153 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 653 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 4153 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 7154 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 31754 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 1754 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 12155 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 29355 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 655 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 15656 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 26756 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 18857 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 25957 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 19658 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 25558 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 20059 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 25259 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 20360 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 24860 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 207



127


Sludge Loading (%) Satisfies PAR N Rows25 Not Durable; Visc; ; Homo; New TL ; Al2O3 ; Not alkali 325 Not Durable; Visc; ; Homo; New TL ; Al2O3 ; alkali 2225 Not Durable; Visc; ; Not Homo; New TL ; Al2O3 ; Not alkali 24725 Not Durable; Visc; ; Not Homo; New TL ; Al2O3 ; alkali 18326 Not Durable; Visc; ; Homo; New TL ; Al2O3 ; Not alkali 2826 Not Durable; Visc; ; Homo; New TL ; Al2O3 ; alkali 5326 Not Durable; Visc; ; Not Homo; New TL ; Al2O3 ; Not alkali 20526 Not Durable; Visc; ; Not Homo; New TL ; Al2O3 ; alkali 16927 Not Durable; Visc; ; Homo; New TL ; Al2O3 ; Not alkali 12427 Not Durable; Visc; ; Homo; New TL ; Al2O3 ; alkali 8327 Not Durable; Visc; ; Not Homo; New TL ; Al2O3 ; Not alkali 8927 Not Durable; Visc; ; Not Homo; New TL ; Al2O3 ; alkali 15928 Not Durable; Visc; ; Homo; New TL ; Al2O3 ; Not alkali 13928 Not Durable; Visc; ; Homo; New TL ; Al2O3 ; alkali 12428 Not Durable; Visc; ; Not Homo; New TL ; Al2O3 ; Not alkali 5928 Not Durable; Visc; ; Not Homo; New TL ; Al2O3 ; alkali 13329 Not Durable; Visc; ; Homo; New TL ; Al2O3 ; Not alkali 15129 Not Durable; Visc; ; Homo; New TL ; Al2O3 ; alkali 23129 Not Durable; Visc; ; Not Homo; New TL ; Al2O3 ; Not alkali 3629 Not Durable; Visc; ; Not Homo; New TL ; Al2O3 ; alkali 3730 Not Durable; Visc; ; Homo; New TL ; Al2O3 ; alkali 42630 Not Durable; Visc; ; Not Homo; New TL ; Al2O3 ; alkali 2931 Not Durable; Visc; ; Homo; New TL ; Al2O3 ; alkali 45231 Not Durable; Visc; ; Not Homo; New TL ; Al2O3 ; alkali 332 Not Durable; Visc; ; Homo; New TL ; Al2O3 ; alkali 45533 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 2533 Not Durable; Visc; ; Homo; New TL ; Al2O3 ; alkali 43034 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 8134 Not Durable; Visc; ; Homo; New TL ; Al2O3 ; alkali 37435 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 13535 Not Durable; Visc; ; Homo; New TL ; Al2O3 ; alkali 32036 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 31536 Not Durable; Visc; ; Homo; New TL ; Al2O3 ; alkali 14037 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 37137 Not Durable; Visc; ; Homo; New TL ; Al2O3 ; alkali 8438 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 40938 Not Durable; Visc; ; Homo; New TL ; Al2O3 ; alkali 4639 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 44939 Not Durable; Visc; ; Homo; New TL ; Al2O3 ; alkali 640 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 45541 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 45542 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 45543 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 45544 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 45545 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 45546 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 45547 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 45548 Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 148 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 45449 Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 549 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 45050 Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 750 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 44650 Not Durable; Not L Visc; ; Homo; Not New TL; Al2O3 ; alkali 251 Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 351 Durable; Not L Visc; ; Homo; Not New TL; Al2O3 ; alkali 551 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 425


128

Sludge Loading (%) Satisfies PAR N Rows51 Not Durable; Not L Visc; ; Homo; Not New TL; Al2O3 ; alkali 2252 Durable; Not L Visc; ; Homo; Not New TL; Al2O3 ; alkali 952 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 36452 Not Durable; Not L Visc; ; Homo; Not New TL; Al2O3 ; alkali 8253 Durable; Not L Visc; ; Homo; Not New TL; Al2O3 ; alkali 1053 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 29453 Not Durable; Not L Visc; ; Homo; Not New TL; Al2O3 ; alkali 15154 Durable; Not L Visc; ; Homo; Not New TL; Al2O3 ; alkali 1054 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 25154 Not Durable; Not L Visc; ; Homo; Not New TL; Al2O3 ; alkali 19455 Durable; Not L Visc; ; Homo; Not New TL; Al2O3 ; alkali 1055 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 24055 Not Durable; Not L Visc; ; Homo; Not New TL; Al2O3 ; alkali 20556 Durable; Not L Visc; ; Homo; Not New TL; Al2O3 ; alkali 1056 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 23256 Not Durable; Not L Visc; ; Homo; Not New TL; Al2O3 ; alkali 21357 Durable; Not L Visc; ; Homo; Not New TL; Al2O3 ; alkali 1157 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 22757 Not Durable; Not L Visc; ; Homo; Not New TL; Al2O3 ; alkali 21758 Durable; Not L Visc; ; Homo; Not New TL; Al2O3 ; alkali 1258 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 22358 Not Durable; Not L Visc; ; Homo; Not New TL; Al2O3 ; alkali 22059 Durable; Not L Visc; ; Homo; Not New TL; Al2O3 ; alkali 1359 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 21659 Not Durable; Not L Visc; ; Homo; Not New TL; Al2O3 ; alkali 22660 Durable; Not L Visc; ; Homo; Not New TL; Al2O3 ; alkali 1460 Not Durable; Not L Visc; ; Homo; New TL ; Al2O3 ; alkali 20660 Not Durable; Not L Visc; ; Homo; Not New TL; Al2O3 ; alkali 235


129

Paper Study Results for 50% Washing with Frit G (411)(# of EVs = 455)

Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 18025 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 27526 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 24026 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 21527 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 34227 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 11328 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 41828 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 3729 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 44229 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 1330 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 43030 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 2531 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 41031 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 4532 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 38632 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 6933 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36533 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 9034 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 34734 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 10835 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 31735 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 13836 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 29136 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 16437 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 26537 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 19038 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 25938 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 19639 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 25439 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 20140 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 25040 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 20541 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 24741 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 20842 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 24342 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 21243 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 23943 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 1443 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 20244 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 344 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 23344 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 6144 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 15845 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 1745 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 21645 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 9145 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 13146 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 3746 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 19446 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 19246 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 3247 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 13147 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 347 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 8347 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 947 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 21347 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 1648 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 109


130

Sludge Loading (%) Satisfies PAR # of EVs48 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 5048 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 4148 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 2348 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 22948 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 349 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 5749 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 13349 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 1649 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 1549 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 23450 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 2250 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 19350 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 150 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 150 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 23750 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 151 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 351 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 21351 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 23751 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 252 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 152 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 21252 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 23352 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 953 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 21053 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 23053 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 1554 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 20854 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 22454 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 2355 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 20755 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 22155 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 2756 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 20556 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 21556 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 3557 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 20257 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 20157 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 5258 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 20158 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 16658 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 8859 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 20059 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 11759 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 13860 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 19860 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 7060 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 187


10 17 3.73626374


131

WL Range # of EVs and Centroid % of Total11 10 2.197802212 6 1.3186813213 2 0.4395604414 6 1.3186813215 3 0.6593406616 2 0.4395604417 2 0.4395604418 3 0.6593406619 6 1.3186813220 20 4.395604421 48 10.549450522 84 18.461538523 44 9.6703296724 26 5.7142857125 6 1.31868132


132

Paper Study Results for 50% Washing with Frit I (412)(# of EVs = 455)

Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 2525 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; Not alkali 9825 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 33226 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 8126 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; Not alkali 8926 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 28527 Durable; Visc; ; Homog; New TL ; Al2O3 ; Not alkali 227 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 20527 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; Not alkali 6827 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 16927 Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; Not alkali 1128 Durable; Visc; ; Homog; New TL ; Al2O3 ; Not alkali 1828 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 24528 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; Not alkali 2428 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 12928 Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; Not alkali 3528 Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 429 Durable; Visc; ; Homog; New TL ; Al2O3 ; Not alkali 2629 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 34129 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; Not alkali 529 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 2429 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; Not alkali 1529 Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; Not alkali 3129 Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 1330 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36930 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 5730 Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 2931 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 35131 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 10131 Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 332 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 32132 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 13433 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 29333 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 16234 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 26734 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 18835 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 25935 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 19636 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 25536 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 20037 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 25037 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 20538 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 24738 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 20839 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 24339 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 21240 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 23940 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 21641 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 23641 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 21942 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 23342 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 22243 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 23143 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 1243 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 21244 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 144 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 22444 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 61


133

Sludge Loading (%) Satisfies PAR # of EVs44 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 16945 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 1145 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 21245 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 9345 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 13946 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 2946 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 19146 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 19746 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 3847 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 12747 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 8947 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 147 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 21847 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 2048 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 14148 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 1148 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 5548 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 848 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 23548 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 549 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 11049 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 7149 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 2749 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 549 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 24250 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 5750 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 15150 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 250 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 24551 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 1651 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 19251 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 24451 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 352 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 20652 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 24052 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 953 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 20553 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 23453 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 1654 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 20254 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 22954 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 2455 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 20155 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 22455 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 3056 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 20056 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 22156 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 3457 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 19857 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 21157 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 4658 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 19658 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 19458 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 6559 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 19459 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 15759 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 10460 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 19060 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 10060 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 165


134


10 6 1.3186813211 2 0.4395604412 3 0.6593406613 1 0.2197802214 4 0.8791208815 2 0.4395604416 4 0.8791208817 3 0.6593406618 7 1.5384615419 30 6.5934065920 80 17.582417621 18 3.9560439622 28 6.1538461523 49 10.769230824 9 1.97802198


135


Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 5225 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 36925 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 226 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 17626 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 19726 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 1126 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 3927 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 21227 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 12927 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 4027 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 4228 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 21328 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 1228 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 17028 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 2829 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 8729 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 32829 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 830 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 6930 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 35431 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 3331 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 39032 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 432 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 40732 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 1233 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 31833 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 10534 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 23534 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 18835 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 21335 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 21036 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 20636 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 21737 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 17737 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 24638 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 10438 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 31939 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 3039 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 39340 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 240 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 42141 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 42342 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 42343 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 42344 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 42345 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 42346 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 42347 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 42348 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 42349 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 42350 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 42351 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 42352 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 852 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 41553 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 4753 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 37654 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 7654 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 347


136

Sludge Loading (%) Satisfies PAR # of EVs55 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 12655 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 29756 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 22956 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 19457 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 33757 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 8658 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 35158 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 7259 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 38059 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 4360 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 41060 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 13

WL Range # of EVs and Centroid % of Total1 9 2.127659572 38 8.983451543 23 5.437352254 15 3.546099295 65 15.36643036 52 12.29314427 12 2.836879438 21 4.964539019 57 13.4751773

10 80 18.912529611 43 10.165484612 8 1.89125296


137


SLUDGE LOADING (%) SATISFIES PAR # OF EVS25 Durable; Visc; ; Homog; New TL ; Al2O3 ; Not alkali 3225 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 16725 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; Not alkali 1825 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 16025 Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; Not alkali 4025 Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 626 Durable; Visc; ; Homog; New TL ; Al2O3 ; Not alkali 4026 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 22526 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; Not alkali 1026 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 10626 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; Not alkali 1026 Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; Not alkali 2626 Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 627 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 37327 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 827 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 2227 Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 2028 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 38928 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 128 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 3028 Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 329 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 39129 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 3230 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 39130 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 3231 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 39431 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 2932 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 39632 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 2733 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 39833 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 2534 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 40334 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 2035 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 40535 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 1836 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 40536 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 1837 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 40637 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 1738 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 638 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 40238 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 1539 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 4439 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36839 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 139 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 1040 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 6940 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 34540 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 740 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 241 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 11741 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 29741 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 942 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 22542 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 142 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 18942 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 142 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 7


138

SLUDGE LOADING (%) SATISFIES PAR # OF EVS43 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 30543 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 2643 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 7243 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 1443 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 644 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 25544 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 9444 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 3444 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 3644 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 445 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 21745 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 16045 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 745 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 3545 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 446 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 20846 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 19846 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 146 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 1246 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 447 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 20147 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 21747 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 147 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 448 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 17648 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 24348 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 449 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 10349 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 31649 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 450 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 3550 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 38450 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 350 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 151 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 251 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 41851 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 352 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 42252 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 153 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 42253 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 154 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 42355 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 42356 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 42357 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 42358 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 42359 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 42360 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 423


10 1 0.2364066211 13 3.0732860512 23 5.4373522513 14 3.30969267


139

WL Range # of EVs and Centroid % of Total14 17 4.0189125315 10 2.3640661916 124 29.314420817 105 24.82269518 33 7.8014184419 37 8.7470449220 14 3.3096926721 1 0.23640662


140

Paper Study Results for 75% Washing with Frit 320-M (416)(# of EVs = 423)

Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 37125 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 5226 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 41126 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 1227 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 42328 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 42329 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 42330 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 42331 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 42332 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 42333 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 42334 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 42335 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 42336 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 42337 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 42338 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 42339 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 42340 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 140 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 42241 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 2641 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 37841 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 1942 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 6542 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 142 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 25242 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 10543 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 7443 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 1143 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 16343 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 17544 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 8344 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 10644 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 13244 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 10245 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 15145 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 14245 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 5745 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 7346 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 18146 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 16146 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 1046 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 7147 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 12747 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 23547 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 147 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 6048 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 4548 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 35048 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 2849 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 849 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 40949 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 650 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 42351 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 42352 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 42353 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 42354 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 42355 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 423


141

Sludge Loading (%) Satisfies PAR # of EVs56 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 42357 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 42358 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 42359 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 42360 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 423



142

Paper Study Results for 75% Washing with Frit H (413)(# of EVs = 423)

Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Visc; ; Homog; New TL ; Al2O3 ; Not alkali 2425 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 16625 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 6025 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; Not alkali 825 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 125 Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; Not alkali 5825 Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 10626 Durable; Visc; ; Homog; New TL ; Al2O3 ; Not alkali 2226 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 20526 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 3626 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; Not alkali 2826 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 2026 Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; Not alkali 3626 Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 7627 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 28127 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 11427 Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 2828 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 29028 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 12928 Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 429 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 29929 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 12430 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 31230 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 11131 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 32431 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 9932 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 33232 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 9133 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 34533 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 7834 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 34834 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 7535 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 35235 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 7136 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 35436 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 6937 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36337 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 6038 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36538 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 5839 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36939 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 5440 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 37440 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 4941 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 441 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 37341 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 4642 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 2442 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 35742 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 1242 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 3043 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 3943 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 30843 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 3443 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 3343 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 944 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 4744 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 7


143

Sludge Loading (%) Satisfies PAR # of EVs44 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 21144 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 11844 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 3444 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 645 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 6545 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 11145 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 12945 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 8545 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 3346 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 14546 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 14346 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 3746 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 6646 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 3247 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 16647 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 15047 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 947 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 6647 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 3248 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 15248 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 18748 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 5448 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 2948 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 149 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 8849 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 28649 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 2249 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 2449 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 350 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 2450 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 36950 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 350 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 1350 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 1451 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 151 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 39751 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 151 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 2452 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 40552 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 1853 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 40553 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 1854 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 40554 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 1855 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 40655 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 1756 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 40856 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 1557 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 41057 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 1358 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 41458 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 959 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 41459 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 960 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 41660 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 7


144


10 1 0.2364066211 2 0.4728132412 2 0.4728132413 9 2.1276595714 6 1.4184397215 17 4.0189125316 20 4.7281323917 21 4.9645390118 46 10.874704519 131 30.969267120 80 18.912529621 11 2.60047281


145

Paper Study Results for 75% Washing with Frit K (414)(# of EVs = 423)

Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Visc; ; Homog; New TL ; Al2O3 ; Not alkali 2825 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 16725 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; Not alkali 225 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 15325 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; Not alkali 425 Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; Not alkali 5625 Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 1326 Durable; Visc; ; Homog; New TL ; Al2O3 ; Not alkali 3026 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 22526 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 9926 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; Not alkali 2026 Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; Not alkali 3626 Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 1327 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36027 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 327 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 3527 Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 2528 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36528 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 5428 Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 429 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 37329 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 5030 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 37630 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 4731 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 38031 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 4332 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 38132 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 4233 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 38433 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 3934 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 39134 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 3235 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 39135 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 3236 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 39136 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 3237 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 39437 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 2938 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 39638 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 2739 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 39839 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 2540 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 40340 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 2041 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 341 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 40241 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 1842 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 3242 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 37342 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 242 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 1643 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 5843 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 31443 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 3443 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 1243 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 544 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 6544 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 6


146

Sludge Loading (%) Satisfies PAR # of EVs44 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 21744 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 11844 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 1644 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 145 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 8345 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 11045 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 13245 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 8545 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 1346 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 15346 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 14346 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 5146 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 6646 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 1047 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 18847 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 15047 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 1047 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 6647 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 948 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 17448 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 18648 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 5548 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 849 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 10549 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 28849 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 2349 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 750 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 3450 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 38150 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 350 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 450 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 151 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 251 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 41751 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 452 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 41952 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 453 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 41953 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 454 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 41954 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 455 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 41955 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 456 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 41956 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 457 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 42057 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 358 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 42158 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 259 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 42259 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 160 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 423



147


10 1 0.2364066211 3 0.7092198612 3 0.7092198613 5 1.182033114 8 1.8912529615 15 3.5460992916 10 2.3640661917 14 3.3096926718 41 9.6926713919 158 37.352245920 108 25.531914921 18 4.25531915


148

Paper Study Results for 75% Washing with Frit L (415)(# of EVs = 423)

Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Visc; ; Homog; New TL ; Al2O3 ; Not alkali 2225 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 15925 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 3825 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; Not alkali 1025 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 825 Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; Not alkali 5825 Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 12826 Durable; Visc; ; Homog; New TL ; Al2O3 ; Not alkali 2126 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 19026 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 1126 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; Not alkali 2926 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 3526 Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; Not alkali 3626 Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 10127 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 22427 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 17127 Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 2828 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 23028 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 18928 Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 429 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 23529 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 18830 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 24530 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 17831 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 25531 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 16832 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 27032 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 15333 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 28633 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 13734 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 29434 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 12935 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 30035 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 12336 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 31336 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 11037 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 32437 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 9938 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 33238 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 9139 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 34439 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 7940 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 640 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 34140 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 1440 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 6241 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 1341 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 33741 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 4841 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 2542 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 2842 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 32442 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 142 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 5642 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 1443 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 10543 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 1643 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 216


149

Sludge Loading (%) Satisfies PAR # of EVs43 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 2343 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 5643 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 744 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 13744 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 8944 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 9344 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 4444 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 6045 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 14745 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 13745 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 2145 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 6045 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 5846 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 15446 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 15446 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 846 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 5746 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 5047 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 15547 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 18847 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 147 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 3147 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 4848 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 13648 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 23648 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 648 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 4448 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 149 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 7549 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 30649 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 3249 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 1050 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 2250 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 35950 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 1350 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 2951 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 151 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 38551 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 151 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 3652 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 39152 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 3253 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 39153 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 3254 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 39154 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 3255 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 39455 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 2956 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 39656 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 2757 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 39657 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 2758 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 40158 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 2259 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 40559 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 1860 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 40560 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 18


150


10 10 2.3640661911 7 1.6548463412 20 4.7281323913 13 3.0732860514 17 4.0189125315 17 4.0189125316 6 1.4184397217 6 1.4184397218 114 26.950354619 65 15.366430320 20 4.7281323921 2 0.47281324


151


Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36125 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 426 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36527 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36528 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36529 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36530 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36531 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36532 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36533 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36534 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36535 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36536 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 34036 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 2537 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 23637 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 12938 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 16938 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 19639 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 8939 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 27640 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 1640 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 34941 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 36542 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 36543 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 36544 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 36545 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 36546 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 36547 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 547 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 36048 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 2248 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 34349 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 5049 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 31550 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 10350 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 26251 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 15251 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 21352 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 17452 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 19153 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 18553 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 18054 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 19954 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 16655 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 22155 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 14456 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 26556 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 10057 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 31157 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 5458 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 33058 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 3559 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 34859 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 1760 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 35860 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 7


152

WL Range # of EVs and Centroid % of Total11 25 6.8493150712 104 28.493150713 67 18.356164414 84 23.013698615 69 18.904109616 16 4.38356164


153

Paper Study Results for 100% Washing with Frit M (417)(# of EVs = 365)

Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36125 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 426 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36527 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36528 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36529 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36530 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36531 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36532 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36533 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36534 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36535 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 34835 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 1736 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 24736 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 11837 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 17537 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 19038 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 10038 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 26539 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 1839 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 34740 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 36541 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 36542 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 36543 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 36544 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 36545 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 36546 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 36547 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 36548 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 36549 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 36550 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 950 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 35651 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 3451 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 33152 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 6052 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 30553 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 12253 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 24354 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 16054 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 20555 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 17855 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 18756 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 19056 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 17557 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 20857 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 15758 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 23458 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 13159 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 29159 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 7460 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 31860 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 47


154



155

Paper Study Results for 100% Washing with Frit 320-M (416)(# of EVs = 365)

Sludge Loading (%) Satisfies PAR N Rows25 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36526 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36527 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36528 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36529 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36530 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36531 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36532 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36533 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36534 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36034 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 535 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 28135 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 8436 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 19436 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 17137 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 13037 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 23538 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 3938 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 32639 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 36540 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 36541 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 36542 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 36543 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 36544 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 36545 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 36546 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 36547 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 36548 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 36549 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 36550 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 1050 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 35551 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 3551 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 33052 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 6152 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 30453 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 13253 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 23354 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 16254 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 20355 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 17855 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 18756 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 19056 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 17557 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 20957 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 15658 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 24558 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 12059 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 30159 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 6460 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 32260 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 43


156


10 79 21.643835611 87 23.835616412 64 17.534246613 91 24.931506814 39 10.6849315


157

Paper Study Results for 100% Washing with Frit N (418)(# of EVs = 365)

Sludge Loading (%) Satisfies PAR N Rows25 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 4425 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 31725 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 426 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 1526 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 35027 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 327 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36228 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36529 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36530 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36531 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36532 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36332 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 233 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 27833 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 8734 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 19234 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 17335 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 12235 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 24336 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 2836 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 33737 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 36538 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 36539 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 36540 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 36541 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 36542 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 36543 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 36544 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 36545 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 36546 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 36547 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 36548 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 36549 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 36550 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 36551 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 36552 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 36553 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 36554 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 36555 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 36556 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 356 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 36257 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 1957 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 34658 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 4858 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 31759 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 10059 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 26560 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 15160 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 214


158

WL Range # of EVs and Centroid % of Total6 1 0.27397267 16 4.383561648 100 27.39726039 68 18.630137

10 65 17.808219211 88 24.10958912 27 7.39726027


159

Paper Study Results for 100% Washing with Frit R (419)(# of EVs = 365)

Sludge Loading (%) Satisfies PAR N Rows25 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 28625 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 7525 Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 426 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 32626 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 3927 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 34927 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 1628 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36529 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36530 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36531 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36532 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36533 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36534 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36535 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36536 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36537 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 337 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36238 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 1938 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 34438 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 239 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 4739 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 139 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 23639 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 8140 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 5940 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 4240 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 14040 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 12441 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 4141 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 11141 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 9241 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 12142 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 1342 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 16142 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 3042 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 16143 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 18643 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 143 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 17844 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 20044 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 16545 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 22245 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 14346 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 26646 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 9947 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 31247 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 5348 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 33048 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 3549 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 34849 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 1750 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 35750 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 851 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 36451 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 152 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 36553 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 365


160

Sludge Loading (%) Satisfies PAR N Rows54 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 36555 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 36556 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 36557 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 36558 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 36559 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 36560 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 365



161

Appendix E

Nominal Stage Assessment for Various Decants


162

Type Frit ID Satisfies PAR Min(Sludge Loading (%)) Max(Sludge Loading (%))Decant #5 202 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 32Decant #5 202 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 33 39Decant #5 202 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 40 43Decant #5 202 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 44 60Decant #5 202-M Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 27Decant #5 202-M Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 28 29Decant #5 202-M Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 30 45Decant #5 202-M Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 46 48Decant #5 202-M Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 49 60Decant #5 202-M2 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 29Decant #5 202-M2 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 30 44Decant #5 202-M2 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 45 46Decant #5 202-M2 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 47 60Decant #5 320 Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; Not alkali 25 28Decant #5 320 Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 29 30Decant #5 320 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 31 60Decant #5 320-M Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 29Decant #5 320-M Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 30 32Decant #5 320-M Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 33 60Decant #5 G Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 29Decant #5 G Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 30 40Decant #5 G Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 41 60Decant #5 I Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; Not alkali 25 28Decant #5 I Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 29 30Decant #5 I Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 31 40Decant #5 I Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 41 60Decant #5 O Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 26Decant #5 O Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 27 30Decant #5 O Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 31 46Decant #5 O Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 47 55Decant #5 O Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 56 58Decant #5 O Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 59 60Decant #5 P Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 30Decant #5 P Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 31 32Decant #5 P Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 33 51Decant #5 P Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 52 58Decant #5 P Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 59 59Decant #5 P Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 60 60Decant #5 S Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 30Decant #5 S Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 31 32Decant #5 S Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 33 50Decant #5 S Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 51 51Decant #5 S Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 52 60Decant #5 T Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 30Decant #5 T Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 31 31Decant #5 T Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 32 50Decant #5 T Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 51 60Decant #5 U Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 30Decant #5 U Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 31 46Decant #5 U Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 47 48Decant #5 U Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 49 60Decant #5 U2 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 30Decant #5 U2 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 31 44Decant #5 U2 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 45 47Decant #5 U2 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 48 60Decant #6 202 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 31Decant #6 202 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 32 45Decant #6 202 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 46 47Decant #6 202 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 48 58Decant #6 202 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 59 60


163

Type Frit ID Satisfies PAR Min(Sludge Loading (%)) Max(Sludge Loading (%))Decant #6 202-M Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 28Decant #6 202-M Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 29 29Decant #6 202-M Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 30 49Decant #6 202-M Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 50 53Decant #6 202-M Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 54 60Decant #6 202-M2 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 26Decant #6 202-M2 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 27 28Decant #6 202-M2 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 29 48Decant #6 202-M2 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 49 52Decant #6 202-M2 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 53 59Decant #6 202-M2 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 60 60Decant #6 320 Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; Not alkali 25 27Decant #6 320 Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 28 29Decant #6 320 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 30 32Decant #6 320 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 33 60Decant #6 320-M Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 28Decant #6 320-M Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 29 34Decant #6 320-M Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 35 60Decant #6 G Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 28Decant #6 G Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 29 29Decant #6 G Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 30 42Decant #6 G Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 43 60Decant #6 I Durable; Visc; ; Not Homog; New TL ; Al2O3 ; Not alkali 25 27Decant #6 I Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 28 29Decant #6 I Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 30 42Decant #6 I Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 43 60Decant #6 O Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 28Decant #6 O Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 29 29Decant #6 O Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 30 47Decant #6 O Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 48 48Decant #6 O Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 49 60Decant #6 P Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 29Decant #6 P Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 30 34Decant #6 P Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 35 48Decant #6 P Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 49 52Decant #6 P Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 53 60Decant #6 S Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 29Decant #6 S Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 30 34Decant #6 S Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 35 53Decant #6 S Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 54 58Decant #6 S Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 59 60Decant #6 T Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 29Decant #6 T Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 30 33Decant #6 T Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 34 52Decant #6 T Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 53 58Decant #6 T Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 59 60Decant #6 U Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 25Decant #6 U Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 26 29Decant #6 U Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 30 48Decant #6 U Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 49 56Decant #6 U Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 57 59Decant #6 U Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 60 60Decant #6 U2 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 29Decant #6 U2 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 30 46Decant #6 U2 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 47 55Decant #6 U2 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 56 59Decant #6 U2 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 60 60Decant #7 202 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 30Decant #7 202 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 31 47Decant #7 202 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 48 51Decant #7 202 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 52 57Decant #7 202 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 58 60


164

Type Frit ID Satisfies PAR Min(Sludge Loading (%)) Max(Sludge Loading (%))Decant #7 202-M Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 27Decant #7 202-M Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 28 30Decant #7 202-M Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 31 51Decant #7 202-M Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 52 53Decant #7 202-M Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 54 60Decant #7 202-M2 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 27Decant #7 202-M2 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 28 49Decant #7 202-M2 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 50 53Decant #7 202-M2 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 54 60Decant #7 320 Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; Not alkali 25 27Decant #7 320 Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 28 28Decant #7 320 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 29 33Decant #7 320 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 34 60Decant #7 320-M Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 27Decant #7 320-M Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 28 36Decant #7 320-M Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 37 60Decant #7 G Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 27Decant #7 G Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 28 38Decant #7 G Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 39 43Decant #7 G Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 44 59Decant #7 G Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 60 60Decant #7 I Durable; Visc; ; Not Homog; New TL ; Al2O3 ; Not alkali 25 27Decant #7 I Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 28 28Decant #7 I Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 29 35Decant #7 I Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36 44Decant #7 I Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 45 60Decant #7 O Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 28Decant #7 O Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 29 29Decant #7 O Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 30 41Decant #7 O Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 42 50Decant #7 O Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 51 60Decant #7 P Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 28Decant #7 P Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 29 35Decant #7 P Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36 42Decant #7 P Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 43 54Decant #7 P Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 55 60Decant #7 S Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 28Decant #7 S Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 29 36Decant #7 S Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 37 52Decant #7 S Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 53 54Decant #7 S Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 55 60Decant #7 T Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 28Decant #7 T Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 29 34Decant #7 T Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 35 52Decant #7 T Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 53 54Decant #7 T Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 55 60Decant #7 U Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 27Decant #7 U Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 28 28Decant #7 U Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 29 50Decant #7 U Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 51 53Decant #7 U Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 54 60Decant #7 U2 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 28Decant #7 U2 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 29 48Decant #7 U2 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 49 52Decant #7 U2 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 53 60Decant #8 202 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 29Decant #8 202 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 30 47Decant #8 202 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 48 48Decant #8 202 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 49 60Decant #8 202-M Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 26Decant #8 202-M Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 27 31Decant #8 202-M Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 32 49


165

Type Frit ID Satisfies PAR Min(Sludge Loading (%)) Max(Sludge Loading (%))Decant #8 202-M Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 50 53Decant #8 202-M Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 54 60Decant #8 202-M2 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 26Decant #8 202-M2 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 27 28Decant #8 202-M2 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 29 49Decant #8 202-M2 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 50 51Decant #8 202-M2 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 52 60Decant #8 320 Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; Not alkali 25 26Decant #8 320 Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 27 28Decant #8 320 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 29 35Decant #8 320 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 36 58Decant #8 320 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 59 60Decant #8 320-M Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 26Decant #8 320-M Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 27 37Decant #8 320-M Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 38 57Decant #8 320-M Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 58 60Decant #8 G Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 26Decant #8 G Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 27 45Decant #8 G Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 46 51Decant #8 G Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 52 55Decant #8 G Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 56 60Decant #8 I Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 28Decant #8 I Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 29 45Decant #8 I Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 46 48Decant #8 I Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 49 56Decant #8 I Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 57 60Decant #8 O Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 28Decant #8 O Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 29 30Decant #8 O Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 31 37Decant #8 O Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 38 51Decant #8 O Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 52 60Decant #8 P Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 28Decant #8 P Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 29 37Decant #8 P Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 38 38Decant #8 P Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 39 56Decant #8 P Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 57 60Decant #8 S Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 28Decant #8 S Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 29 37Decant #8 S Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 38 47Decant #8 S Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 48 56Decant #8 S Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 57 60Decant #8 T Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 28Decant #8 T Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 29 35Decant #8 T Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36 47Decant #8 T Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 48 55Decant #8 T Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 56 60Decant #8 U Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 28Decant #8 U Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 29 48Decant #8 U Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 49 51Decant #8 U Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 52 60Decant #8 U2 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 28Decant #8 U2 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 29 48Decant #8 U2 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 49 49Decant #8 U2 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 50 60Decant #9 202 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 28Decant #9 202 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 29 44Decant #9 202 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 45 50Decant #9 202 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 51 60Decant #9 202-M Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 25Decant #9 202-M Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 26 32Decant #9 202-M Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 33 46Decant #9 202-M Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 47 54


166

Type Frit ID Satisfies PAR Min(Sludge Loading (%)) Max(Sludge Loading (%))Decant #9 202-M Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 55 60Decant #9 202-M2 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 25Decant #9 202-M2 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 26 29Decant #9 202-M2 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 30 45Decant #9 202-M2 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 46 52Decant #9 202-M2 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 53 60Decant #9 320 Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; Not alkali 25 25Decant #9 320 Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 26 27Decant #9 320 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 28 36Decant #9 320 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 37 55Decant #9 320 Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 56 60Decant #9 320-M Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 25Decant #9 320-M Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 26 38Decant #9 320-M Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 39 48Decant #9 320-M Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 49 53Decant #9 320-M Not Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 54 60Decant #9 G Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 25Decant #9 G Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 26 46Decant #9 G Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 47 51Decant #9 G Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 52 60Decant #9 I Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 27Decant #9 I Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 28 46Decant #9 I Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 47 52Decant #9 I Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 53 60Decant #9 O Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 27Decant #9 O Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 28 31Decant #9 O Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 32 34Decant #9 O Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 35 53Decant #9 O Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 54 60Decant #9 P Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 27Decant #9 P Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 28 35Decant #9 P Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 36 38Decant #9 P Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 39 57Decant #9 P Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 58 60Decant #9 S Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 27Decant #9 S Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 28 38Decant #9 S Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 39 44Decant #9 S Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 45 57Decant #9 S Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 58 60Decant #9 T Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 27Decant #9 T Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 28 37Decant #9 T Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 38 44Decant #9 T Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 45 57Decant #9 T Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 58 60Decant #9 U Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 27Decant #9 U Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 28 29Decant #9 U Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 30 45Decant #9 U Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 46 53Decant #9 U Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 54 60Decant #9 U2 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 25Decant #9 U2 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 26 27Decant #9 U2 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 28 45Decant #9 U2 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 46 51Decant #9 U2 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 52 60

Decant #10 202 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 25Decant #10 202 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 26 28Decant #10 202 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 29 41Decant #10 202 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 42 51Decant #10 202 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 52 60Decant #10 202-M Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 25Decant #10 202-M Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 26 34Decant #10 202-M Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 35 43


167

Type Frit ID Satisfies PAR Min(Sludge Loading (%)) Max(Sludge Loading (%))Decant #10 202-M Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 44 55Decant #10 202-M Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 56 60Decant #10 202-M2 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 25Decant #10 202-M2 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 26 30Decant #10 202-M2 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 31 43Decant #10 202-M2 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 44 54Decant #10 202-M2 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 55 60Decant #10 320 Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; Not alkali 25 25Decant #10 320 Not Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 26 27Decant #10 320 Not Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 28 37Decant #10 320 Not Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 38 48Decant #10 320 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 49 53Decant #10 320 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 54 60Decant #10 320-M Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 25Decant #10 320-M Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 26 40Decant #10 320-M Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 41 51Decant #10 320-M Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 52 60Decant #10 G Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 25Decant #10 G Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 26 48Decant #10 G Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 49 49Decant #10 G Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 50 60Decant #10 I Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 27Decant #10 I Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 28 48Decant #10 I Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 49 50Decant #10 I Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 51 60Decant #10 O Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 27Decant #10 O Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 28 32Decant #10 O Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 33 54Decant #10 O Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 55 60Decant #10 P Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 27Decant #10 P Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 28 33Decant #10 P Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 34 39Decant #10 P Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 40 58Decant #10 P Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 59 60Decant #10 S Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 27Decant #10 S Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 28 39Decant #10 S Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 40 42Decant #10 S Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 43 59Decant #10 S Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 60 60Decant #10 T Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 27Decant #10 T Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 28 38Decant #10 T Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 39 41Decant #10 T Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 42 58Decant #10 T Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 59 60Decant #10 U Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 27Decant #10 U Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 28 30Decant #10 U Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 31 43Decant #10 U Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 44 54Decant #10 U Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 55 60Decant #10 U2 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 26Decant #10 U2 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 27 27Decant #10 U2 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 28 42Decant #10 U2 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 43 52Decant #10 U2 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 53 60Decant #11 202 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 26Decant #11 202 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 27 27Decant #11 202 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 28 39Decant #11 202 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 40 52Decant #11 202 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 53 60Decant #11 202-M Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 25Decant #11 202-M Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 26 35Decant #11 202-M Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36 41


168

Type Frit ID Satisfies PAR Min(Sludge Loading (%)) Max(Sludge Loading (%))Decant #11 202-M Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 42 57Decant #11 202-M Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 58 60Decant #11 202-M2 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 25Decant #11 202-M2 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 26 32Decant #11 202-M2 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 33 41Decant #11 202-M2 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 42 55Decant #11 202-M2 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 56 60Decant #11 320 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 26Decant #11 320 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 27 38Decant #11 320 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 39 50Decant #11 320 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 51 60Decant #11 320-M Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 25Decant #11 320-M Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 26 41Decant #11 320-M Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 42 49Decant #11 320-M Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 50 60Decant #11 G Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 25Decant #11 G Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 26 47Decant #11 G Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 48 49Decant #11 G Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 50 60Decant #11 I Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 26Decant #11 I Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 27 48Decant #11 I Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 49 49Decant #11 I Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 50 60Decant #11 O Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 26Decant #11 O Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 27 30Decant #11 O Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 31 34Decant #11 O Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 35 55Decant #11 O Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 56 60Decant #11 P Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 26Decant #11 P Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 27 31Decant #11 P Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 32 41Decant #11 P Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 42 60Decant #11 S Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 26Decant #11 S Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 27 39Decant #11 S Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 40 41Decant #11 S Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 42 60Decant #11 T Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 26Decant #11 T Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 27 39Decant #11 T Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 40 59Decant #11 T Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 60 60Decant #11 U Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 26Decant #11 U Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 27 31Decant #11 U Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 32 40Decant #11 U Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 41 55Decant #11 U Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 56 60Decant #11 U2 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 26Decant #11 U2 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 27 27Decant #11 U2 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 28 40Decant #11 U2 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 41 54Decant #11 U2 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 55 60Decant #12 202 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 27Decant #12 202 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 28 37Decant #12 202 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 38 54Decant #12 202 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 55 60Decant #12 202-M Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 25 36Decant #12 202-M Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 37 39Decant #12 202-M Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 40 58Decant #12 202-M Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 59 60Decant #12 202-M2 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 25 33Decant #12 202-M2 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 34 39Decant #12 202-M2 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 40 56Decant #12 202-M2 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 57 60


169

Type Frit ID Satisfies PAR Min(Sludge Loading (%)) Max(Sludge Loading (%))Decant #12 320 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 26Decant #12 320 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 27 40Decant #12 320 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 41 48Decant #12 320 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 49 60Decant #12 320-M Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 25 42Decant #12 320-M Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 43 47Decant #12 320-M Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 48 60Decant #12 G Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 25 45Decant #12 G Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 46 50Decant #12 G Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 51 60Decant #12 I Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 26Decant #12 I Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 27 46Decant #12 I Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 47 50Decant #12 I Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 51 60Decant #12 O Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 26Decant #12 O Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 27 28Decant #12 O Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 29 35Decant #12 O Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 36 57Decant #12 O Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 58 60Decant #12 P Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 26Decant #12 P Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 27 29Decant #12 P Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 30 42Decant #12 P Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 43 60Decant #12 S Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 26Decant #12 S Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 27 38Decant #12 S Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 39 42Decant #12 S Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 43 60Decant #12 T Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 26Decant #12 T Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 27 38Decant #12 T Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 39 40Decant #12 T Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 41 60Decant #12 U Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 26Decant #12 U Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 27 32Decant #12 U Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 33 39Decant #12 U Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 40 57Decant #12 U Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 58 60Decant #12 U2 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 26Decant #12 U2 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 27 29Decant #12 U2 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 30 38Decant #12 U2 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 39 55Decant #12 U2 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 56 60Decant #13 202 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 27Decant #13 202 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 28 36Decant #13 202 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 37 55Decant #13 202 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 56 60Decant #13 202-M Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 25 37Decant #13 202-M Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 38 38Decant #13 202-M Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 39 59Decant #13 202-M Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 60 60Decant #13 202-M2 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 25 34Decant #13 202-M2 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 35 38Decant #13 202-M2 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 39 57Decant #13 202-M2 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 58 60Decant #13 320 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 25Decant #13 320 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 26 41Decant #13 320 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 42 47Decant #13 320 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 48 60Decant #13 320-M Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 25 43Decant #13 320-M Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 44 45Decant #13 320-M Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 46 60Decant #13 G Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 25 43Decant #13 G Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 44 51


170

Type Frit ID Satisfies PAR Min(Sludge Loading (%)) Max(Sludge Loading (%))Decant #13 G Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 52 60Decant #13 I Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 25Decant #13 I Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 26 44Decant #13 I Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 45 51Decant #13 I Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 52 60Decant #13 O Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 25Decant #13 O Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 26 27Decant #13 O Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 28 36Decant #13 O Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 37 58Decant #13 O Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 59 60Decant #13 P Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 25Decant #13 P Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 26 28Decant #13 P Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 29 43Decant #13 P Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 44 60Decant #13 S Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 25Decant #13 S Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 26 36Decant #13 S Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 37 43Decant #13 S Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 44 60Decant #13 T Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 25Decant #13 T Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 26 36Decant #13 T Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 37 41Decant #13 T Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 42 60Decant #13 U Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 25Decant #13 U Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 26 33Decant #13 U Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 34 37Decant #13 U Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 38 58Decant #13 U Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 59 60Decant #13 U2 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 25Decant #13 U2 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 26 29Decant #13 U2 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 30 37Decant #13 U2 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 38 56Decant #13 U2 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 57 60Decant #14 202 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 26Decant #14 202 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 27 28Decant #14 202 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 29 35Decant #14 202 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 36 56Decant #14 202 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 57 60Decant #14 202-M Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 25 36Decant #14 202-M Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 37 38Decant #14 202-M Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 39 60Decant #14 202-M2 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 25 35Decant #14 202-M2 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 36 36Decant #14 202-M2 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 37 58Decant #14 202-M2 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 59 60Decant #14 320 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 25Decant #14 320 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 26 42Decant #14 320 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 43 46Decant #14 320 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 47 60Decant #14 320-M Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 25 44Decant #14 320-M Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 45 60Decant #14 G Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 25 42Decant #14 G Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 43 53Decant #14 G Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 54 60Decant #14 I Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 25Decant #14 I Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 26 43Decant #14 I Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 44 53Decant #14 I Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 54 60Decant #14 O Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 25Decant #14 O Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 26 26Decant #14 O Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 27 37Decant #14 O Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 38 59Decant #14 O Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 60 60


171

Type Frit ID Satisfies PAR Min(Sludge Loading (%)) Max(Sludge Loading (%))Decant #14 P Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 25Decant #14 P Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 26 27Decant #14 P Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 28 44Decant #14 P Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 45 60Decant #14 S Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 25Decant #14 S Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 26 35Decant #14 S Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 36 44Decant #14 S Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 45 60Decant #14 T Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 25Decant #14 T Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 26 35Decant #14 T Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 36 42Decant #14 T Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 43 60Decant #14 U Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 25Decant #14 U Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 26 34Decant #14 U Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 35 36Decant #14 U Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 37 59Decant #14 U Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 60 60Decant #14 U2 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 25Decant #14 U2 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 26 30Decant #14 U2 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 31 36Decant #14 U2 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 37 57Decant #14 U2 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 58 60Decant #15 202 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 26Decant #15 202 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 27 29Decant #15 202 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 30 33Decant #15 202 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 34 57Decant #15 202 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 58 60Decant #15 202-M Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 25 35Decant #15 202-M Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 36 39Decant #15 202-M Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 40 60Decant #15 202-M2 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 25 35Decant #15 202-M2 Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 36 36Decant #15 202-M2 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 37 60Decant #15 320 Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 25Decant #15 320 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 26 43Decant #15 320 Durable; Not L Visc; ; Homog; New TL ; Al2O3 ; alkali 44 44Decant #15 320 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 45 60Decant #15 320-M Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 25 42Decant #15 320-M Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 43 46Decant #15 320-M Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 47 60Decant #15 G Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 25 41Decant #15 G Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 42 54Decant #15 G Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 55 60Decant #15 I Durable; Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 25Decant #15 I Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 26 41Decant #15 I Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 42 54Decant #15 I Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 55 60Decant #15 O Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 25Decant #15 O Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 26 38Decant #15 O Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 39 60Decant #15 P Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 25Decant #15 P Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 26 26Decant #15 P Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 27 45Decant #15 P Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 46 60Decant #15 S Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 25Decant #15 S Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 26 34Decant #15 S Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 35 45Decant #15 S Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 46 60Decant #15 T Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 25Decant #15 T Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 26 34Decant #15 T Durable; Not H Visc; ; Homog; Not New TL; Al2O3 ; alkali 35 44Decant #15 T Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 45 60


172

Type Frit ID Satisfies PAR Min(Sludge Loading (%)) Max(Sludge Loading (%))Decant #15 U Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 25Decant #15 U Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 26 35Decant #15 U Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 36 60Decant #15 U2 Durable; Not H Visc; ; Not Homog; New TL ; Al2O3 ; alkali 25 25Decant #15 U2 Durable; Not H Visc; ; Homog; New TL ; Al2O3 ; alkali 26 32Decant #15 U2 Durable; Visc; ; Homog; New TL ; Al2O3 ; alkali 33 34Decant #15 U2 Durable; Visc; ; Homog; Not New TL; Al2O3 ; alkali 35 58Decant #15 U2 Durable; Not L Visc; ; Homog; Not New TL; Al2O3 ; alkali 59 60


173

Appendix F

Phase 2 Variation Stage Assessment for Decant #7


174

Paper Study Results for 7 Decants with Frit 202(# of EVs = 915)

Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 91526 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 91527 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 2227 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 89328 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 12428 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 79129 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 28229 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 63330 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 47030 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 44531 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 53131 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 38432 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 77732 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 13833 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 85733 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 5834 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 89734 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 1835 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91536 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91537 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91538 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91539 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91540 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91541 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91141 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 442 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 86442 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 5143 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 73943 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 13943 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 3744 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 744 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 56944 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 25044 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 8945 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 3545 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 39245 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 35045 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 8545 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 5346 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 3646 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 446 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 29246 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 39646 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 16046 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 2747 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 16547 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 4247 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 7147 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 38047 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 25748 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 12748 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 20048 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 2648 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 24248 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 32049 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 7649 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 287


175

Sludge Loading (%) Satisfies PAR # of EVs49 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 349 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 16949 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 38050 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 5450 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 42250 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 4250 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 39751 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 3951 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 47051 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 40652 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 2352 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 47552 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 41652 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 153 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 553 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 48253 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 42353 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 554 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 154 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 47554 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 40554 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 3455 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 46755 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 35455 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 9456 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 45856 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 30556 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 15257 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 44857 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 19957 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 26858 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 43958 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 13958 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 33759 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 43159 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 6559 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 41960 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 42260 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 3060 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 463

WL Range # of EVs and Centroid % of Total8 12 1.311475419 24 2.62295082

10 16 1.7486338811 26 2.8415300512 39 4.2622950813 47 5.1366120214 163 17.814207715 318 34.754098416 178 19.453551917 76 8.3060109318 16 1.74863388


176

Paper Study Results for 7 Decants with Frit 202M (420)(# of EVs = 915)

Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 10825 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 80726 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 25026 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 66527 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 45827 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 45728 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 50628 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 38128 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 2528 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 329 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 68629 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 7129 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 9129 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 6730 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 56230 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 29530 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 5831 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 28231 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 62331 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 1032 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 16832 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 74733 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 2333 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 89234 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91535 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91536 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91537 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91538 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91539 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91540 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91541 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91542 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91543 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91143 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 444 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 86644 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 4945 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 76245 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 15346 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 63346 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 28247 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 55047 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 36548 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 50548 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 41049 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 7249 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 38449 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 43149 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 2850 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 8550 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 1150 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 30550 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 43750 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 6850 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 951 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 11751 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 5951 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 214


177

Sludge Loading (%) Satisfies PAR # of EVs51 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 39951 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 12652 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 23452 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 14252 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 4152 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 32352 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 17553 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 19953 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 27253 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 653 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 20053 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 23854 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 13754 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 39654 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 8154 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 30155 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 5255 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 48555 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 455 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 37456 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 2256 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 49856 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 38156 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 1457 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 657 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 50457 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 34457 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 6158 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 49958 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 28658 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 13059 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 48859 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 18459 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 24360 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 47860 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 12160 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 316

WL Range # of EVs and Centroid % of Total10 4 0.4371584711 32 3.4972677612 65 7.1038251413 88 9.6174863414 80 8.743169415 54 5.9016393416 43 4.6994535517 36 3.9344262318 37 4.0437158519 46 5.027322420 91 9.9453551921 279 30.491803322 60 6.55737705


178

Paper Study Results for 7 Decants with Frit 202-M2 (421)(# of EVs = 915)

Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 10825 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 80225 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 526 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 24126 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 53326 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 926 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 13227 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 38727 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 22827 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 7127 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 22928 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 25628 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 3228 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 27528 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 35229 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 15929 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 61829 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 13830 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 1730 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 84030 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 5831 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 90531 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 1032 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91533 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91534 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91535 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91536 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91537 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91538 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91539 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91540 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91541 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91542 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91543 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 90643 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 944 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 84644 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 6945 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 72745 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 18846 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 59746 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 31847 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 4747 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 48447 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 37347 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 1148 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 10348 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 148 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 33848 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 41648 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 5048 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 749 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 13049 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 2849 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 24649 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 40649 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 10550 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 255


179

Sludge Loading (%) Satisfies PAR # of EVs50 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 8850 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 5150 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 36250 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 15951 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 23351 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 25151 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 1551 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 20951 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 20752 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 17152 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 36552 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 10252 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 27753 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 9153 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 46153 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 1253 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 35154 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 4754 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 47954 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 38955 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 2455 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 49155 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 39655 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 456 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 856 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 49656 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 38956 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 2257 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 157 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 49257 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 33657 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 8658 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 48358 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 27658 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 15659 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 47359 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 16559 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 27760 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 46260 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 11360 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 340

WL Range # of EVs and Centroid % of Total13 2 0.2185792314 43 4.6994535515 93 10.163934416 82 8.9617486317 100 10.928961718 133 14.535519119 98 10.710382520 47 5.1366120221 221 24.153005522 87 9.5081967223 9 0.98360656


180

Paper Study Results for 7 Decants with Frit O (405)(# of EVs = 915)

Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 91526 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 6126 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 85427 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 14827 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 73827 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 2928 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 33528 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 42028 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 2228 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 13829 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 39129 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 13729 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 10029 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 28730 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 24530 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 2730 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 35130 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 29231 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 13731 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 67831 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 10032 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 1332 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 84632 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 1032 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 4633 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 82933 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 8634 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 68534 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 23035 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 56235 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 35336 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 50836 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 40737 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 48437 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 43138 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 46738 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 44839 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 45639 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 45940 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 44940 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 46641 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 44341 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 47242 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 43842 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 47743 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 42543 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 49044 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 40044 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 51545 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 34245 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 57346 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 28346 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 63247 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 447 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 17547 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 73648 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 2248 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 89


181

Sludge Loading (%) Satisfies PAR # of EVs48 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 9548 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 70949 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 3149 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 15549 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 1349 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 71650 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 1850 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 43850 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 45951 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 651 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 62251 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 28752 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 152 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 73252 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 18253 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 86153 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 5454 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 91555 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 91556 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 91557 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 91558 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 91559 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 88559 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 3060 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 83160 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 84


10 17 1.857923511 9 0.9836065612 17 1.857923513 16 1.7486338814 46 5.027322415 74 8.0874316916 136 14.86338817 88 9.6174863418 46 5.027322419 22 2.40437158


182

Paper Study Results for 7 Decants with Frit P (406)(# of EVs = 915)

Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 91526 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 6126 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 85427 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 14827 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 76728 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 35728 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 55829 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 49129 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 42430 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 59630 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 31931 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 81531 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 10032 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 86932 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 4633 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 89733 Durable; Not H Visc; Homog; Not New TL; Al2O3 ; alkali 1433 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 434 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 68934 Durable; Not H Visc; Homog; Not New TL; Al2O3 ; alkali 10234 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 12435 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 45735 Durable; Not H Visc; Homog; Not New TL; Al2O3 ; alkali 24335 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 21536 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 8336 Durable; Not H Visc; Homog; Not New TL; Al2O3 ; alkali 34336 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 47136 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 1837 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 1837 Durable; Not H Visc; Homog; Not New TL; Al2O3 ; alkali 21437 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 48637 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 19738 Durable; Not H Visc; Homog; Not New TL; Al2O3 ; alkali 9938 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 48238 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 33439 Durable; Not H Visc; Homog; Not New TL; Al2O3 ; alkali 739 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 46539 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 44340 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 45540 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 46041 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 44941 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 46642 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 44342 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 47243 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 43843 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 47744 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 42444 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 49145 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 39845 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 51746 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 33946 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 57647 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 27847 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 63748 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 16948 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 74649 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 11649 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 799


183

Sludge Loading (%) Satisfies PAR # of EVs50 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 4250 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 87351 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 1851 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 89752 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 7952 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 652 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 83053 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 16653 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 74954 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 33854 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 57755 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 58055 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 33556 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 71556 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 20057 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 84157 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 7458 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 91358 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 259 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 91560 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 915


10 45 4.9180327911 37 4.0437158512 93 10.163934413 54 5.9016393414 71 7.7595628415 44 4.8087431716 28 3.0601092917 14 1.5300546418 8 0.8743169419 2 0.21857923


184

Paper Study Results for 7 Decants with Frit S (409)(# of EVs = 915)

Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 91526 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 6126 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 85427 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 14827 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 76728 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 35728 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 55829 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 49129 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 42430 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 59630 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 31931 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 81531 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 10032 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 86932 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 4633 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 91333 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 234 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 79734 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 11835 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 70635 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 20936 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 43336 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 48237 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 23737 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 67838 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 10538 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 81039 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 939 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 90640 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91541 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91542 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 90342 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 1243 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 82743 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 8844 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 69944 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 21645 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 57845 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 33746 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 52246 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 39347 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 49547 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 42048 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 47848 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 43749 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 46149 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 45450 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 45450 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 46151 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 44651 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 46952 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 3452 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 40652 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 47553 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 12753 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 1453 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 30453 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 470


185

Sludge Loading (%) Satisfies PAR # of EVs54 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 14354 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 5554 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 22854 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 44454 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 4555 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 27755 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 12355 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 1455 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 40755 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 9456 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 19256 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 34556 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 23456 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 13256 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 1257 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 10757 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 51157 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 10757 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 13657 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 5458 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 2958 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 60558 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 1558 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 12558 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 14159 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 759 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 56859 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 8959 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 25160 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 52960 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 3160 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 355


10 18 1.9672131111 19 2.0765027312 13 1.4207650313 18 1.9672131114 17 1.857923515 11 1.2021857916 11 1.2021857917 13 1.4207650318 88 9.6174863419 330 36.0655738


186

Paper Study Results for 7 Decants with Frit T (410)(# of EVs = 915)

Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 91526 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 6126 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 85427 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 14827 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 76728 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 35728 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 55829 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 49129 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 42430 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 59630 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 31931 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 81531 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 10032 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 82832 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 4632 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 4133 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 75533 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 16034 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 59634 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 31935 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 30035 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 61536 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 18236 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 73337 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 4437 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 87138 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91539 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91540 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91541 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91542 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 89642 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 1943 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 81643 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 9944 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 68344 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 23245 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 57145 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 34446 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 51846 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 39747 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 49347 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 42248 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 47548 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 44049 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 45949 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 45650 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 45350 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 46251 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 1251 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 43351 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 47052 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 11852 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 852 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 32152 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 46853 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 16553 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 4253 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 265


187

Sludge Loading (%) Satisfies PAR # of EVs53 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 44354 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 34154 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 9354 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 3554 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 40954 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 3755 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 29255 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 27355 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 355 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 25955 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 8856 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 18956 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 43356 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 15756 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 12556 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 1157 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 9657 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 60157 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 3357 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 13057 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 5558 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 2958 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 63258 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 11858 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 13659 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 559 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 58759 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 6959 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 25460 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 53460 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 2960 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 352


10 65 7.1038251411 35 3.8251366112 11 1.2021857913 16 1.7486338814 20 2.1857923515 14 1.5300546416 14 1.5300546417 12 1.3114754118 11 1.2021857919 264 28.85245920 160 17.4863388


188

Paper Study Results for 7 Decants with Frit U (422)(# of EVs = 915)

Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 85125 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 6426 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 6126 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 66926 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 18527 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 14827 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 28827 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 47928 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 18228 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 4128 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 17528 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 51729 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 7729 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 41429 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 42430 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 59630 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 31931 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 81531 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 10032 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 86932 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 4633 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91534 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91535 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91536 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91537 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91538 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91539 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91540 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91541 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91542 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91543 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 89643 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 1944 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 81744 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 9845 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 69145 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 22446 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 58246 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 33347 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 247 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 52047 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 39348 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 10448 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 39148 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 42049 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 17349 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 1049 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 30449 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 42850 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 35550 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 6750 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 10650 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 38751 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 41751 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 20451 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 3351 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 25851 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 3


189

Sludge Loading (%) Satisfies PAR # of EVs52 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 39252 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 28652 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 352 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 18352 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 5153 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 33953 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 41653 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 5953 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 10154 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 27754 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 48454 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 15455 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 21055 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 50055 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 20455 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 156 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 12156 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 52156 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 26456 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 957 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 2857 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 53857 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 29257 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 5758 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 358 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 52458 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 24058 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 14859 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 51559 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 15559 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 24560 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 50460 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 8660 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 325



190

Paper Study Results for 7 Decants with Frit U2 (423)(# of EVs = 915)

Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 18625 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 72926 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 2426 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 6126 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 83027 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 14827 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 76728 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 35728 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 55829 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 49129 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 42430 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 59630 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 31931 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 81531 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 10032 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 86932 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 4633 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91534 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91535 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91536 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91537 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91538 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91539 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91540 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91541 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91542 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91142 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 443 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 87043 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 4544 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 78344 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 13245 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 145 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 66945 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 24546 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 9346 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 47546 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 34747 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 17647 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 34047 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 39948 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 35248 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 3248 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 14048 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 39149 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 43749 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 17549 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 3649 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 26750 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 43050 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 26950 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 750 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 18750 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 2251 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 38051 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 39651 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 6851 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 71


191

Sludge Loading (%) Satisfies PAR # of EVs52 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 32952 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 46952 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 152 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 11653 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 26853 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 47653 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 17154 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 19954 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 48554 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 23155 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 12055 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 50355 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 28955 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 356 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 3156 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 51456 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 33456 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 3657 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 657 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 51657 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 29957 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 9458 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 51158 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 20358 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 20159 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 50059 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 14259 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 27360 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 49060 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 6460 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 361



192



193

Appendix G



194


Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 1625 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 70925 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 12426 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 9226 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 57626 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 1026 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 17127 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 14227 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 25027 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 26227 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 19528 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 12928 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 2628 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 40028 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 29429 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 10129 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 229 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 61129 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 13530 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 2030 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 80530 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 2431 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 84932 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 84933 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 80433 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 4534 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 59234 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 25735 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 45035 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 39936 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 41436 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 43537 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 40137 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 44838 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 36138 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 48839 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 23839 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 61140 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 8840 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 76141 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 1141 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 83842 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 84943 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 84944 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 84945 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 84946 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 84947 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 84948 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 84949 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 84950 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 550 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 84451 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 8251 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 76752 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 15752 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 69253 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 19253 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 657


195

Sludge Loading (%) Satisfies PAR # of EVs54 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 44754 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 40255 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 67855 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 17156 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 71756 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 13257 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 77957 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 7058 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 83958 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 1059 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 84960 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 849


10 146 17.19670211 154 18.13898712 64 7.5382803313 6 0.70671378


196

Paper Study Results for 12 Decants with Frit 202-M (420)(# of EVs = 849)

Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 50925 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 34026 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 69426 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 15527 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 82527 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 2428 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 84929 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 84930 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 84931 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 84932 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 84933 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 83433 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 1534 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 72634 Durable; Not H Visc; Homog; Not New TL; Al2O3 ; alkali 134 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 12235 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 58935 Durable; Not H Visc; Homog; Not New TL; Al2O3 ; alkali 8735 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 17336 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 32236 Durable; Not H Visc; Homog; Not New TL; Al2O3 ; alkali 16236 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 23736 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 12837 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 4537 Durable; Not H Visc; Homog; Not New TL; Al2O3 ; alkali 14037 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 39137 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 27338 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 1538 Durable; Not H Visc; Homog; Not New TL; Al2O3 ; alkali 12738 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 39738 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 31039 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 139 Durable; Not H Visc; Homog; Not New TL; Al2O3 ; alkali 8039 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 39939 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 36940 Durable; Not H Visc; Homog; Not New TL; Al2O3 ; alkali 1340 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 36040 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 47641 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 22641 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 62342 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 7642 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 77343 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 543 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 84444 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 84945 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 84946 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 84947 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 84948 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 84949 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 84950 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 84951 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 84952 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 84953 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 84954 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 84955 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 4255 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 80756 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 138


197

Sludge Loading (%) Satisfies PAR # of EVs56 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 71157 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 17857 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 67158 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 37258 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 47759 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 66059 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 18960 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 70560 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 144



198


Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 50925 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 34026 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 69426 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 15527 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 82527 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 2428 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 84929 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 84930 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 82830 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 2131 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 71531 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 13432 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 66832 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 18133 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 42533 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 42434 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 16734 Durable; Not H Visc; Homog; Not New TL; Al2O3 ; alkali 134 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 67734 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 435 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 10035 Durable; Not H Visc; Homog; Not New TL; Al2O3 ; alkali 2835 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 62835 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 9336 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 2636 Durable; Not H Visc; Homog; Not New TL; Al2O3 ; alkali 2436 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 49836 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 30137 Durable; Not H Visc; Homog; Not New TL; Al2O3 ; alkali 237 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 42637 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 42138 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 40938 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 44039 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 39539 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 45440 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 33640 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 51341 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 20041 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 64942 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 5842 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 79143 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 443 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 84544 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 84945 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 84946 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 84947 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 84948 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 84949 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 84950 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 84951 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 84952 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 84953 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 2653 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 82354 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 12554 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 72455 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 17055 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 679


199

Sludge Loading (%) Satisfies PAR # of EVs56 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 28056 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 56957 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 57757 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 27258 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 69758 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 15259 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 74059 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 10960 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 81560 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 34


10 62 7.3027090711 42 4.9469964712 8 0.94228504


200


Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Visc; Homog; New TL ; Al2O3 ; Not alkali 4725 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 8725 Durable; Visc; Not Homog; New TL ; Al2O3 ; Not alkali 24025 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 28025 Not Durable; Visc; Not Homog; New TL ; Al2O3 ; Not alkali 13125 Not Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 6426 Durable; Visc; Homog; New TL ; Al2O3 ; Not alkali 24426 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 17026 Durable; Visc; Not Homog; New TL ; Al2O3 ; Not alkali 2626 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 23526 Not Durable; Visc; Homog; New TL ; Al2O3 ; Not alkali 1826 Not Durable; Visc; Not Homog; New TL ; Al2O3 ; Not alkali 10826 Not Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 4827 Durable; Visc; Homog; New TL ; Al2O3 ; Not alkali 25027 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 25427 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 18227 Not Durable; Visc; Homog; New TL ; Al2O3 ; Not alkali 5127 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 227 Not Durable; Visc; Not Homog; New TL ; Al2O3 ; Not alkali 7227 Not Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 3828 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 67928 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 2228 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 9228 Not Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 5629 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 70629 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 13129 Not Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 1230 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 71230 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 13731 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 71631 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 13332 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 72232 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 12733 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 72933 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 12034 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 73434 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 11535 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 73835 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 11136 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 74436 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 10537 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 4137 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 70937 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 2437 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 7538 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 7238 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 68238 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 8038 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 1539 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 11139 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 64739 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 7839 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 1340 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 35340 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 40840 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 8841 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 59241 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 171


201

Sludge Loading (%) Satisfies PAR # of EVs41 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 8642 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 63542 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 13142 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 8343 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 69443 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 843 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 6643 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 8144 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 67344 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 8544 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 1044 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 8145 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 49345 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 27845 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 7846 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 37446 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 40146 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 7447 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 34547 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 43347 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 7148 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 33448 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 44548 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 7049 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 30849 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 47449 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 6750 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 20450 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 57950 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 5750 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 951 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 7351 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 71351 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 3951 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 2452 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 852 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 77952 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 1252 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 5053 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 78853 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 153 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 6054 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 79154 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 5855 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 79255 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 5756 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 79356 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 5657 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 79357 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 5658 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 79458 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 5559 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 79559 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 5460 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 79560 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 54

WL Range # of EVs and Centroid % of Total0 101 11.89634861 1 0.117785632 6 0.70671378


202


10 20 2.355712611 39 4.5936395812 183 21.554770313 210 24.734982314 58 6.8315665515 24 2.8268551216 20 2.355712617 42 4.9469964718 92 10.83627819 4 0.47114252


203


Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 50925 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 34026 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 69426 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 15527 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 82527 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 2428 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 84929 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 84930 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 84931 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 84932 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 84933 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 84934 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 84935 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 84936 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 84937 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 84938 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 84939 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 2339 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 82640 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 12540 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 72441 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 17041 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 67841 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 142 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 28742 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 51842 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 4443 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 45943 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 13043 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 16043 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 10044 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 43244 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 26744 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 3244 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 11845 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 41245 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 33045 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 645 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 10146 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 40646 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 40946 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 3447 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 38547 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 46347 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 148 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 30748 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 54249 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 17449 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 67550 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 5250 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 79751 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 251 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 84752 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 84953 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 84954 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 84955 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 84956 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 849


204

Sludge Loading (%) Satisfies PAR # of EVs57 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 84958 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 84959 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 84960 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 849



205

Paper Study Results for 12 Decants with Frit G (411)(# of EVs = 849)

Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 50925 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 34026 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 69426 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 15527 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 82527 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 2428 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 84929 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 84930 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 84931 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 84932 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 84933 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 84934 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 84935 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 84936 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 84937 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 84938 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 84939 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 84940 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 82940 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 2041 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 68841 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 16142 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 48842 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 36143 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 42443 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 42544 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 40944 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 44045 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 39245 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 45746 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 33246 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 51747 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 1647 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 20047 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 63348 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 448 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 10448 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 5648 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 68549 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 149 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 16449 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 349 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 68150 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 20450 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 64551 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 49251 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 35752 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 69252 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 15753 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 72453 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 12554 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 79554 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 5455 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 84455 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 556 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 84957 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 84958 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 849


206

Sludge Loading (%) Satisfies PAR # of EVs59 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 84960 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 849



207

Paper Study Results for 12 Decants with Frit I (412)(# of EVs = 849)

Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 13425 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 71526 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 43226 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 41727 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 55727 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 29228 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 77128 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 7829 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 83729 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 1230 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 84931 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 84932 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 84933 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 84934 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 84935 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 84936 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 84937 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 84938 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 84939 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 84940 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 84941 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 81341 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 3642 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 66142 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 18843 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 46843 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 38144 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 42144 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 42845 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 40745 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 44246 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 38846 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 46147 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 447 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 947 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 30547 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 53148 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 1948 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 8348 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 15348 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 59449 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 1349 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 15149 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 3549 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 65050 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 150 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 19850 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 150 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 64951 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 48651 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 36352 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 68952 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 16053 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 72353 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 12654 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 79154 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 5855 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 842


208

Sludge Loading (%) Satisfies PAR # of EVs55 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 756 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 84957 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 84958 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 84959 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 84960 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 849



209


Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 13425 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 71526 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 43226 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 41727 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 55727 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 29228 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 77128 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 7829 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 83729 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 1230 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 77530 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 7431 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 68731 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 16232 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 63832 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 21133 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 26633 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 58334 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 13634 Durable; Not H Visc; Homog; Not New TL; Al2O3 ; alkali 1134 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 68734 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 1535 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 6435 Durable; Not H Visc; Homog; Not New TL; Al2O3 ; alkali 2835 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 60035 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 15736 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 936 Durable; Not H Visc; Homog; Not New TL; Al2O3 ; alkali 836 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 46136 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 37137 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 41737 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 43238 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 40638 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 44339 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 38239 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 46740 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 28640 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 56341 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 13741 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 71242 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 4242 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 80743 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 143 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 84844 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 84945 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 84946 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 84947 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 84948 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 84949 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 84950 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 84951 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 84952 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 84953 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 153 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 84854 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 6654 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 78355 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 149


210

Sludge Loading (%) Satisfies PAR # of EVs55 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 70056 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 18456 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 66557 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 42057 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 42958 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 67358 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 17659 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 71259 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 13760 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 77460 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 75


10 67 7.8916372211 50 5.8892815112 15 1.76678445


211


Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 13425 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 71526 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 41926 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 41626 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 1326 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 127 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 48327 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 23327 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 7427 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 5928 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 62128 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 4628 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 15028 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 3229 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 39229 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 44529 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 1230 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 15730 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 69231 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 11131 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 73832 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 2532 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 82433 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 84934 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 80734 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 4235 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 59435 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 25536 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 45236 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 39737 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 41437 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 43538 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 40338 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 44639 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 36839 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 48140 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 25040 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 59941 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 9641 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 75342 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 1442 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 83543 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 84944 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 84945 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 84946 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 84947 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 84948 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 84949 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 84950 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 84951 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 151 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 84852 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 5752 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 79253 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 14653 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 70354 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 18154 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 668


212

Sludge Loading (%) Satisfies PAR # of EVs55 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 39555 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 45456 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 66756 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 18257 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 70757 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 14258 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 76458 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 8559 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 83059 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 1960 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 849


10 70 8.2449941111 124 14.605418112 99 11.660777413 74 8.7161366314 31 3.6513545315 4 0.47114252


213

Appendix H



214


Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 92726 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 92727 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 92728 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 92729 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 7229 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 85530 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 21630 Durable; Visc; Not Homog; New TL ; Al2O3 ; Not alkali 18530 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 52631 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 33431 Durable; Visc; Not Homog; New TL ; Al2O3 ; Not alkali 17331 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 42032 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 46432 Durable; Visc; Not Homog; New TL ; Al2O3 ; Not alkali 7132 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 28232 Not Durable; Visc; Not Homog; New TL ; Al2O3 ; Not alkali 9332 Not Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 1733 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 50933 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 19633 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 1833 Not Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 20434 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 60634 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 2434 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 9734 Not Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 20035 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 54535 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 26235 Not Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 12036 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 52236 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 33336 Not Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 7237 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 50137 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 41937 Not Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 738 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 47938 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 44839 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 45839 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 46940 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 43840 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 48941 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 41941 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 2041 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 48842 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 40442 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 18542 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 33843 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 38943 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 41743 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 12144 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 1644 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 35744 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 51244 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 4245 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 9045 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 26845 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 56345 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 646 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 275


215

Sludge Loading (%) Satisfies PAR # of EVs46 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 7346 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 57947 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 30947 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 61848 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 28648 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 64149 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 27349 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 65450 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 22750 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 1450 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 68651 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 15251 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 3351 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 73951 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 352 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 4652 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 7552 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 76852 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 3853 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 553 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 4653 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 72853 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 14854 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 254 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 66254 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 26355 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 61755 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 31056 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 57856 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 34957 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 56057 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 36758 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 54658 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 38159 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 52959 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 39860 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 51460 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 413


10 19 2.0496224411 16 1.7259978412 25 2.6968716313 82 8.8457389414 16 1.7259978415 33 3.5598705516 144 15.533980617 96 10.3559871


216


Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 92726 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 5326 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 74226 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 13227 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 20427 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 30727 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 41628 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 27228 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 10728 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 6628 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 48229 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 21329 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 129 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 25229 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 46130 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 530 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 53830 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 38431 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 71931 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 20832 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 82332 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 10433 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 85933 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 6834 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 92735 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 92736 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 92737 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 89737 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 3038 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 78038 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 14739 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 69339 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 23440 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 59540 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 33241 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 54041 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 38742 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 52042 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 40743 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 50043 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 42744 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 47944 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 44845 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 45945 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 145 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 46746 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 43846 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 11546 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 37447 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 147 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 41947 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 27747 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 23048 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 3248 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 37348 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 45748 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 6549 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 94


217

Sludge Loading (%) Satisfies PAR # of EVs49 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 29749 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 51949 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 1750 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 17850 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 19850 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 55151 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 35251 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 1051 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 56552 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 33552 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 1452 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 57853 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 28153 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 4053 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 60654 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 16754 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 12254 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 63855 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 8355 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 19355 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 64555 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 656 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 2556 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 22556 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 62056 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 5757 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 157 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 19457 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 59257 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 14058 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 12958 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 56758 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 23159 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 6659 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 55259 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 30960 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 360 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 53960 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 385


10 81 8.7378640811 39 4.2071197412 21 2.2653721713 17 1.8338727114 8 0.8629989215 4 0.4314994616 4 0.4314994617 13 1.4023732518 18 1.9417475719 35 3.7756202820 107 11.542610621 284 30.636461722 5 0.53937433


218


Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 40225 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 52526 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 4926 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 19026 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 426 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 68427 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 1127 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 20427 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 71228 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 33828 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 58929 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 46529 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 46230 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 54330 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 38431 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 71931 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 20832 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 82332 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 10433 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 85933 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 6834 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 92735 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 92736 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 82936 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 9837 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 73137 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 19638 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 66038 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 26739 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 55039 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 37740 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 53040 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 39741 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 51041 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 41742 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 48942 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 43843 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 46743 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 46044 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 44744 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 8944 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 39145 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 42945 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 24445 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 25446 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 3046 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 38146 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 44046 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 7647 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 6447 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 33347 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 50647 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 2448 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 16348 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 22048 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 54348 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 149 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 346


219

Sludge Loading (%) Satisfies PAR # of EVs49 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 2249 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 55950 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 35550 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 57251 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 34551 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 58252 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 27952 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 1752 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 63153 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 23553 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 4753 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 64554 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 13554 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 13154 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 65654 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 555 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 3855 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 18555 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 66855 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 3656 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 356 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 15956 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 63356 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 13257 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 9957 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 58657 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 24258 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 2358 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 56358 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 34159 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 54959 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 37860 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 53460 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 393


10 26 2.8047464911 19 2.0496224412 13 1.4023732513 5 0.5393743314 3 0.323624615 8 0.8629989216 15 1.6181229817 36 3.8834951518 60 6.4724919119 55 5.9331175820 37 3.9913700121 74 7.9827400222 179 19.3096009


220


Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 81025 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 11726 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 51426 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 41327 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 37827 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 54928 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 11028 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 10128 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 1828 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 69829 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 229 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 23229 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 69330 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 42530 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 50231 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 46931 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 45832 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 57032 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 35733 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 75333 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 17434 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 82334 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 10435 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 88435 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 4336 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 92737 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 92738 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 92739 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 92740 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91240 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 1541 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 88641 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 4142 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 79542 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 13243 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 69643 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 23144 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 1544 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 62144 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 29145 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 17745 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 40645 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 34446 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 37346 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 18846 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 36647 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 42847 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 2247 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 5247 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 35747 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 6848 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 35448 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 11948 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 948 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 27648 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 16949 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 27749 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 322


221

Sludge Loading (%) Satisfies PAR # of EVs49 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 8849 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 24050 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 16050 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 42350 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 150 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 34351 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 10551 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 43451 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 38852 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 7452 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 44652 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 40753 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 4853 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 45253 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 42754 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 2354 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 45654 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 44754 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 155 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 655 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 45355 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 46055 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 856 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 43856 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 46156 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 2857 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 42057 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 45857 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 4958 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 40558 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 45358 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 6959 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 39059 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 45059 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 8760 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 37460 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 44460 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 109


10 47 5.0701186611 68 7.3354908312 112 12.081984913 182 19.633225514 202 21.790722815 146 15.749730316 88 9.4929881317 41 4.4228694718 3 0.3236246


222

Paper Study Results for 5 Decants with Frit P (406)(# of EVs = 927)

Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 92726 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 92727 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 92728 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 12828 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 79929 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 23229 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 69530 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 42530 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 50231 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 46631 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 35231 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 331 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 10632 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 49032 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 13332 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 8032 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 22433 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 40333 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 633 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 35033 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 16834 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 27234 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 55134 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 10435 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 5535 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 82935 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 4336 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 92737 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 92738 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 92739 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 92740 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 92741 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 91141 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 1642 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 88342 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 4443 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 79143 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 13644 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 69144 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 23645 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 63345 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 29446 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 58346 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 34447 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 55947 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 36848 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 248 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 54448 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 38149 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 12349 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 39549 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 39649 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 649 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 750 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 15650 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 450 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 22950 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 409


223

Sludge Loading (%) Satisfies PAR # of EVs50 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 12951 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 21651 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 5551 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 6351 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 37051 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 22352 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 18852 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 14152 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 1652 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 29352 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 28953 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 10153 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 25753 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 18953 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 38054 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 7454 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 44754 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 754 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 39955 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 5055 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 45855 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 41956 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 2556 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 46256 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 44057 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 657 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 46157 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 45557 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 558 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 158 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 44558 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 45658 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 2559 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 42759 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 45359 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 4760 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 41060 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 44960 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 68


10 59 6.3646170411 29 3.1283710912 27 2.9126213613 32 3.4519956914 67 7.2276159715 78 8.4142394816 74 7.9827400217 60 6.4724919118 242 26.105717419 31 3.34412082


224


Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 92726 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 92727 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 92728 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 12828 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 79929 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 23229 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 69530 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 42530 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 50231 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 46631 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 35631 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 331 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 10232 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 49532 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 13732 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 7532 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 22033 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 40833 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 633 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 34533 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 16834 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 27734 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 54634 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 10435 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 6335 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 82135 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 4336 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 92737 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 92738 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 92739 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 92740 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 92741 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 92742 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 82642 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 10143 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 73143 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 19644 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 66544 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 26245 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 55545 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 37246 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 53446 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 39347 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 51347 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 41448 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 49348 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 43449 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 47249 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 7549 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 38050 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 750 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 44650 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 22550 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 24951 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 4351 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 36451 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 2651 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 410


225

Sludge Loading (%) Satisfies PAR # of EVs51 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 8452 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 7052 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 26652 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 8052 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 48352 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 2853 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 14953 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 1853 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 10253 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 13253 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 52453 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 254 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 11754 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 23354 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 2254 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 1454 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 54155 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 6955 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 30255 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 55656 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 1556 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 34356 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 56656 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 357 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 157 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 34657 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 56057 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 2058 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 30758 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 54758 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 7359 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 28459 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 53159 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 11260 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 26760 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 51460 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 146


10 42 4.5307443411 51 5.5016181212 110 11.866235213 35 3.7756202814 33 3.5598705515 21 2.2653721716 39 4.2071197417 66 7.119741118 176 18.985976319 194 20.9277238


226


Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 92726 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 92727 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 92728 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 12828 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 79929 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 23229 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 68729 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 830 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 41530 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 32230 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 1030 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 18031 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 39831 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 8831 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 7131 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 37032 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 34532 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 2632 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 22532 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 33133 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 20933 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 54433 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 17434 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 834 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 81534 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 10435 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 88435 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 4336 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 92737 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 92738 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 92739 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 92740 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 92741 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 92742 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 84542 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 8243 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 74543 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 18244 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 67344 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 25445 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 56745 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 36046 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 53646 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 39147 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 51647 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 41148 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 49648 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 3748 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 39449 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 849 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 46849 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 19149 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 26050 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 4850 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 40850 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 38050 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 9151 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 82


227

Sludge Loading (%) Satisfies PAR # of EVs51 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 32851 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 2651 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 45251 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 3952 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 15652 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 352 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 16452 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 9652 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 50252 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 653 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 20053 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 14053 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 4353 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 2153 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 52354 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 13254 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 25754 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 53855 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 6755 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 30655 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 55456 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 1456 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 34656 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 56456 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 357 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 157 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 34757 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 55857 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 2158 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 31058 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 54658 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 7159 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 28459 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 52959 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 11460 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 27260 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 51360 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 142


10 48 5.1779935311 43 4.638619212 63 6.796116513 69 7.443365714 34 3.6677454215 26 2.8047464916 18 1.9417475717 34 3.6677454218 67 7.2276159719 286 30.852211420 90 9.70873786


228


Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 33125 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 59626 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 9426 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 83327 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 92728 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 12828 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 79929 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 23229 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 69530 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 42530 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 50231 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 46931 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 45832 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 57032 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 35733 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 75333 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 17434 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 82334 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 10435 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 88435 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 4336 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 92737 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 92738 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 92739 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 92740 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 82340 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 10441 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 71941 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 20842 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 65842 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 26943 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 55043 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 37744 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 53044 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 1244 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 38545 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 645 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 50545 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 16845 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 24846 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 4646 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 44546 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 31846 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 11847 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 9847 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 37247 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 41747 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 4048 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 16948 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 28248 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 46948 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 749 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 31949 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 11349 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 49550 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 41450 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 150 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 512


229

Sludge Loading (%) Satisfies PAR # of EVs51 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 39951 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 52852 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 35752 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 2752 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 54353 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 26953 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 9953 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 55954 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 19854 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 15854 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 57155 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 10255 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 24355 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 58256 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 2456 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 28156 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 60156 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 2157 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 457 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 28057 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 57957 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 6458 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 26658 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 56258 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 9959 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 22759 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 54759 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 15360 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 16260 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 53260 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 233


10 59 6.3646170411 72 7.7669902912 29 3.1283710913 22 2.3732470314 17 1.8338727115 11 1.1866235216 57 6.1488673117 65 7.0118662418 59 6.3646170419 16 1.7259978420 93 10.032362521 143 15.426105722 29 3.12837109


230


Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 92726 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 92727 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 92728 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 12828 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 79929 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 23229 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 69530 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 42530 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 50231 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 46931 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 45832 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 57032 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 35733 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 75333 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 17434 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 82334 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 10435 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 88435 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 4336 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 92737 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 92738 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 90938 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 1839 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 79239 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 13540 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 69540 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 23241 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 61841 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 30942 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 54442 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 442 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 37943 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 343 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 52143 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 13543 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 26844 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 4244 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 46044 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 26444 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 16145 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 9745 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 38545 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 40845 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 3746 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 17046 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 29346 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 46046 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 447 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 30247 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 13947 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 48648 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 41948 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 448 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 50449 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 40849 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 51950 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 39350 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 534


231

Sludge Loading (%) Satisfies PAR # of EVs51 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 37051 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 951 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 54852 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 33152 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 3352 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 56353 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 24153 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 11153 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 57554 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 14854 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 18254 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 59755 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 4655 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 24555 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 61755 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 1956 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 1356 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 26756 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 60556 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 4257 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 157 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 25457 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 57757 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 9558 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 20258 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 55958 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 16659 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 14259 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 54559 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 24060 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 7260 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 52860 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 327


10 49 5.2858683911 31 3.3441208212 22 2.3732470313 12 1.2944983814 55 5.9331175815 71 7.6591154316 55 5.9331175817 21 2.2653721718 88 9.4929881319 126 13.59223320 52 5.60949299


232



233

Appendix I



234


Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 18525 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 70426 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 8426 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 3026 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 77527 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 127 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 10627 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 78228 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 33628 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 55329 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 49129 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 39830 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 63630 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 25331 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 82531 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 6432 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 87732 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 1233 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 88934 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 88935 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 88936 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 88937 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 85937 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 3038 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 74038 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 14939 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 58639 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 30340 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 49140 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 39841 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 46141 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 42842 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 44442 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 44543 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 43543 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 45444 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 42644 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 46345 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 40345 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 48646 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 32346 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 56647 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 447 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 2847 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 22647 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 63148 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 3148 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 10748 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 7348 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 67849 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 1849 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 16649 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 1049 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 69550 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 650 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 37550 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 508


235

Sludge Loading (%) Satisfies PAR # of EVs51 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 67551 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 21452 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 75052 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 13953 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 83053 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 5954 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 88754 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 255 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 88956 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 88957 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 88958 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 87958 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 1059 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 85359 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 3660 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 83060 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 59


10 120 13.498312711 171 19.235095612 101 11.361079913 28 3.149606314 29 3.2620922415 58 6.5241844816 108 12.148481417 141 15.860517418 91 10.236220519 26 2.92463442


236


Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 29525 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 59426 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 48326 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 40627 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 60727 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 28228 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 82528 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 6429 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 87729 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 1230 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 87930 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 1031 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 75831 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 13132 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 69732 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 19233 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 33333 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 55634 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 18634 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 70335 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 10235 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 78736 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 1336 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 87637 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 88938 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 88939 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 86139 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 2840 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 72140 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 16841 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 56441 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 32542 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 48142 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 40843 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 45443 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 43544 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 44244 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 44745 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 43345 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 45646 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 42646 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 46347 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 40247 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 48748 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 31648 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 57349 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 22649 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 66350 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 9050 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 79951 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 551 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 1951 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 86552 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 10152 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 252 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 78653 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 16153 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 728


237

Sludge Loading (%) Satisfies PAR # of EVs54 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 25754 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 63255 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 63155 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 25856 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 71956 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 17057 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 79757 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 9258 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 87758 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 1259 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 88960 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 889


10 17 1.9122609711 23 2.587176612 15 1.6872890913 17 1.9122609714 23 2.587176615 59 6.6366704216 50 5.6242969617 118 13.273340818 93 10.461192419 48 5.3993250820 18 2.0247469121 7 0.78740157


238


Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 29525 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 59426 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 48326 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 40627 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 60227 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 28227 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 528 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 71728 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 4328 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 10828 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 2129 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 69429 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 129 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 18329 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 1130 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 29930 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 59031 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 17631 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 71332 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 8532 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 80433 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 433 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 88534 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 88935 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 88936 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 88937 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 88938 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 88838 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 139 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 84139 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 4840 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 69340 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 19641 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 54341 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 34642 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 47342 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 41643 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 45143 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 43844 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 43944 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 45045 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 43245 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 45746 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 42446 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 46547 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 38947 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 50048 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 29548 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 59449 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 149 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 16949 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 71950 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 350 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 7650 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 7550 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 73551 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 651 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 149


239

Sludge Loading (%) Satisfies PAR # of EVs51 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 851 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 72652 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 252 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 22552 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 66253 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 60253 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 28754 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 70554 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 18455 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 78155 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 10856 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 86756 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 2257 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 88958 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 88959 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 88960 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 889


10 74 8.3239595111 83 9.3363329612 34 3.8245219313 20 2.2497187914 24 2.6996625415 15 1.6872890916 15 1.6872890917 25 2.8121484818 64 7.1991001119 94 10.573678320 90 10.123734521 88 9.8987626522 48 5.3993250823 4 0.44994376


240


Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 3825 Durable; Visc; Not Homog; New TL ; Al2O3 ; Not alkali 3825 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 12625 Not Durable; Visc; Not Homog; New TL ; Al2O3 ; Not alkali 40925 Not Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 27826 Durable; Visc; Homog; New TL ; Al2O3 ; Not alkali 926 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 11226 Durable; Visc; Not Homog; New TL ; Al2O3 ; Not alkali 1926 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 7026 Not Durable; Visc; Homog; New TL ; Al2O3 ; Not alkali 1126 Not Durable; Visc; Not Homog; New TL ; Al2O3 ; Not alkali 37426 Not Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 29427 Durable; Visc; Homog; New TL ; Al2O3 ; Not alkali 1727 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 17027 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 2627 Not Durable; Visc; Homog; New TL ; Al2O3 ; Not alkali 18127 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 1027 Not Durable; Visc; Not Homog; New TL ; Al2O3 ; Not alkali 18327 Not Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 30228 Durable; Visc; Homog; New TL ; Al2O3 ; Not alkali 928 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 21428 Not Durable; Visc; Homog; New TL ; Al2O3 ; Not alkali 25028 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 4228 Not Durable; Visc; Not Homog; New TL ; Al2O3 ; Not alkali 9828 Not Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 27629 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 22929 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 45129 Not Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 20930 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 24030 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 59730 Not Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 5231 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 25031 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 63531 Not Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 432 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 25632 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 63333 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 26433 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 133 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 62434 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 26734 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 9734 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 52535 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 26835 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 16435 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 45736 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 136 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 27636 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 27836 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 33437 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 9137 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 19637 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 56337 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 3938 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 14838 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 14538 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 58638 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 1039 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 236


241

Sludge Loading (%) Satisfies PAR # of EVs39 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 6439 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 58940 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 30440 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 240 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 58341 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 31141 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 57842 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 31842 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 57143 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 32943 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 56044 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 33844 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 55145 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 34145 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 54846 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 34446 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 54547 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 34747 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 54248 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 32548 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 2548 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 53949 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 25049 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 10449 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 53550 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 12550 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 23450 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 52450 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 651 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 3251 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 32951 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 49751 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 3152 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 36252 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 47052 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 5753 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 36453 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 45153 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 7454 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 36754 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 43854 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 8455 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 36855 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 43055 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 9156 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 37056 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 41156 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 10857 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 37157 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 36657 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 15258 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 37458 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 26658 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 24959 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 37559 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 12459 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 39060 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 37560 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 3760 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 477


242


10 7 0.7874015711 10 1.1248593912 61 6.8616422913 89 10.011248614 32 3.59955006


243


Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 29525 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 29925 Not Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 29526 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 46026 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 9526 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 2326 Not Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 31127 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 47027 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 4827 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 13727 Not Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 23428 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 50528 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 32028 Not Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 6429 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 49229 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 38529 Not Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 1230 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 48730 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 40231 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 48331 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 40632 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 47932 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 41033 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 47433 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 41534 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 47134 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 41835 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 46735 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 42236 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 46436 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 5336 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 37237 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 1837 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 44237 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 13337 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 29638 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 5738 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 40038 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 16238 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 27039 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 20639 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 24839 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 39039 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 4540 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 28140 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 16940 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 42540 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 1441 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 34541 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 10341 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 44142 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 42642 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 2042 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 44343 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 44443 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 44544 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 44144 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 448


244

Sludge Loading (%) Satisfies PAR # of EVs45 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 43945 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 45046 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 42746 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 1046 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 45247 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 35747 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 7747 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 45548 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 21348 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 22048 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 45649 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 7649 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 35449 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 45950 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 1650 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 41250 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 45750 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 451 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 351 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 42451 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 44951 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 1352 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 152 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 42452 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 43852 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 2653 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 42353 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 43153 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 3554 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 42254 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 42154 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 4655 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 42255 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 38355 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 8456 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 41956 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 29056 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 18057 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 41857 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 14757 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 32458 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 41758 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 7758 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 39559 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 41659 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 1459 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 45960 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 41460 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 260 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 473



245


10 4 0.4499437611 2 0.2249718812 41 4.6119235113 112 12.598425214 84 9.448818915 59 6.6366704216 84 9.448818917 78 8.77390326


246

Paper Study Results for 9 Decants with Frit I (412)(# of EVs = 889)

Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 3825 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 85126 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 13226 Durable; Visc; Not Homog; New TL ; Al2O3 ; Not alkali 7426 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 68327 Durable; Visc; Homog; New TL ; Al2O3 ; Not alkali 227 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 37627 Durable; Visc; Not Homog; New TL ; Al2O3 ; Not alkali 12927 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 38228 Durable; Visc; Homog; New TL ; Al2O3 ; Not alkali 3028 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 48528 Durable; Visc; Not Homog; New TL ; Al2O3 ; Not alkali 9828 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 27629 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 68029 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 20930 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 83730 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 5231 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 88531 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 432 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 88933 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 88934 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 88935 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 88936 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 87736 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 1237 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 85137 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 3838 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 82638 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 6339 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 80239 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 8740 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 77840 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 11141 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 75441 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 13542 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 73142 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 15843 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 69943 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 19044 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 244 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 65944 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 5044 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 17845 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 2145 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 60345 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 845 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 12645 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 13146 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 5846 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 47446 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 6946 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 14346 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 14547 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 17547 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 2347 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 18347 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 18847 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 291


247

Sludge Loading (%) Satisfies PAR # of EVs47 Not Durable; Visc; Homog; New TL ; Al2O3 ; alkali 2948 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 16248 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 18348 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 3448 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 16448 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 34649 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 9749 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 29549 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 649 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 11849 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 37350 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 6950 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 39450 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 4250 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 38451 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 4451 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 44951 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 39652 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 3052 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 45852 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 40153 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 2253 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 46453 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 40053 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 354 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 654 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 47554 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 38154 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 2755 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 255 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 47655 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 29355 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 11856 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 47456 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 15156 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 26457 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 47157 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 7757 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 34158 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 46758 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 1558 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 40759 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 46459 Not Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 259 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 42360 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 46160 Not Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 428


10 21 2.3622047211 20 2.2497187912 20 2.2497187913 18 2.0247469114 41 4.6119235115 42 4.72440945


248



249


Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 3825 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 85126 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 13226 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 75727 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 37827 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 51128 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 50328 Durable; Not H Visc; Homog; Not New TL; Al2O3 ; alkali 1228 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 37429 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 51529 Durable; Not H Visc; Homog; Not New TL; Al2O3 ; alkali 15229 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 20929 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 1330 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 39130 Durable; Not H Visc; Homog; Not New TL; Al2O3 ; alkali 32930 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 3230 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 11730 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 2031 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 29431 Durable; Not H Visc; Homog; Not New TL; Al2O3 ; alkali 39531 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 17431 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 2231 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 432 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 5332 Durable; Not H Visc; Homog; Not New TL; Al2O3 ; alkali 24532 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 39432 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 19733 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 1733 Durable; Not H Visc; Homog; Not New TL; Al2O3 ; alkali 15933 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 42133 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 29234 Durable; Not H Visc; Homog; Not New TL; Al2O3 ; alkali 9134 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 43034 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 36835 Durable; Not H Visc; Homog; Not New TL; Al2O3 ; alkali 835 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 41535 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 46636 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 35736 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 53237 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 24137 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 64838 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 9538 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 79439 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 2039 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 86940 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 240 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 88741 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 88942 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 88943 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 88944 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 88945 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 88946 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 88947 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 88948 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 88949 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 88950 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 2250 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 867


250

Sludge Loading (%) Satisfies PAR # of EVs51 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 12951 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 76052 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 17452 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 71553 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 31053 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 57954 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 66354 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 22655 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 73455 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 15556 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 82156 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 6857 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 88557 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 458 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 88959 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 88960 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 889


10 5 0.5624297


251


Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 3825 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 85126 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 13226 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 75727 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 37827 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 51128 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 51528 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 37429 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 68029 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 20930 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 83730 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 5231 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 88531 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 432 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 88933 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 88934 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 88935 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 88936 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 83236 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 5737 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 73337 Durable; Not H Visc; Homog; Not New TL; Al2O3 ; alkali 437 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 15238 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 59838 Durable; Not H Visc; Homog; Not New TL; Al2O3 ; alkali 6538 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 22639 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 11439 Durable; Not H Visc; Homog; Not New TL; Al2O3 ; alkali 16539 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 53639 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 7440 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 2740 Durable; Not H Visc; Homog; Not New TL; Al2O3 ; alkali 14940 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 48240 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 23141 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 141 Durable; Not H Visc; Homog; Not New TL; Al2O3 ; alkali 9541 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 46741 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 32642 Durable; Not H Visc; Homog; Not New TL; Al2O3 ; alkali 1342 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 44642 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 43043 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 43743 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 45244 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 42944 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 46045 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 41745 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 47246 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 37246 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 51747 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 27147 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 61848 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 12348 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 76649 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 6049 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 82950 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 850 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 88151 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 889


252

Sludge Loading (%) Satisfies PAR # of EVs52 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 88953 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 88954 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 88955 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 6655 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 82356 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 15256 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 73757 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 22057 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 66958 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 59158 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 29859 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 70559 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 18460 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 78160 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 108


10 62 6.9741282311 87 9.7862767212 40 4.4994375713 19 2.1372328514 4 0.44994376


253


Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 3825 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 85126 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 13226 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 75727 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 37827 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 51128 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 51528 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 37429 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 68029 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 20930 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 83730 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 5231 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 88531 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 432 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 88933 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 88934 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 88134 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 835 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 76835 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 12136 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 71336 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 17637 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 52737 Durable; Not H Visc; Homog; Not New TL; Al2O3 ; alkali 837 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 35438 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 14338 Durable; Not H Visc; Homog; Not New TL; Al2O3 ; alkali 6438 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 65138 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 3139 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 4739 Durable; Not H Visc; Homog; Not New TL; Al2O3 ; alkali 7939 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 56639 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 19740 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 640 Durable; Not H Visc; Homog; Not New TL; Al2O3 ; alkali 3540 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 49340 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 35541 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 46541 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 42442 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 44542 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 44443 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 43643 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 45344 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 42844 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 46145 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 41245 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 47746 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 36346 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 52647 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 25747 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 63248 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 11648 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 77349 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 3949 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 85050 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 650 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 88351 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 889


254

Sludge Loading (%) Satisfies PAR # of EVs52 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 88953 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 88954 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 3854 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 85155 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 14055 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 74956 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 19356 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 69657 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 44157 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 44858 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 68658 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 20359 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 75859 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 13160 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 84760 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 42


10 116 13.04836911 81 9.1113610812 62 6.9741282313 56 6.299212614 30 3.3745781815 8 0.8998875116 1 0.11248594


255


Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 3825 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 85126 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 13226 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 75727 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 37527 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 46427 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 327 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 4728 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 45728 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 27628 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 5828 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 9829 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 50629 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 11329 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 17429 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 9630 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 22430 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 61330 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 5231 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 13331 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 75231 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 432 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 3332 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 85633 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 88934 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 88935 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 88936 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 88937 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 88938 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 87738 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 1239 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 79139 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 9840 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 63440 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 25541 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 51441 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 37542 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 46642 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 42343 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 44643 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 44344 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 43844 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 45145 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 43045 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 45946 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 41446 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 47547 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 36847 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 52148 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 26748 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 62249 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 12549 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 76450 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 1950 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 5750 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 81351 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 251 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 122


256

Sludge Loading (%) Satisfies PAR # of EVs51 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 851 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 75752 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 17452 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 71553 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 30453 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 58554 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 66054 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 22955 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 73355 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 15656 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 82056 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 6957 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 88457 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 558 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 88959 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 88960 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 889


10 89 10.011248611 73 8.2114735712 33 3.71203613 23 2.587176614 17 1.9122609715 21 2.3622047216 17 1.9122609717 24 2.6996625418 94 10.573678319 151 16.985376820 93 10.461192421 46 5.1743532122 5 0.5624297


257


Sludge Loading (%) Satisfies PAR # of EVs25 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 3825 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 67725 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 17426 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 13026 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 21426 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 226 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 54327 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 13327 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 4327 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 24527 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 46828 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 7928 Durable; Not H Visc; Not Homog; New TL ; Al2O3 ; alkali 128 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 43628 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 37329 Durable; Not H Visc; Homog; New TL ; Al2O3 ; alkali 129 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 67929 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 20930 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 83730 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 5231 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 88531 Durable; Visc; Not Homog; New TL ; Al2O3 ; alkali 432 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 88933 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 88934 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 88935 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 88936 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 88937 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 88938 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 86438 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 2539 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 74639 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 14340 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 58840 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 30141 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 49241 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 39742 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 46142 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 42843 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 44443 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 44544 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 43544 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 45445 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 42845 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 46146 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 40646 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 48347 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 33647 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 55348 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 1248 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 24648 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 63149 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 2249 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 9649 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 8749 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 68450 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 1650 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 15450 Durable; Visc; Homog; New TL ; Al2O3 ; alkali 16


258

Sludge Loading (%) Satisfies PAR # of EVs50 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 70351 Durable; Not L Visc; Homog; New TL ; Al2O3 ; alkali 751 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 27651 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 60652 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 64952 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 24053 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 72853 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 16154 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 80754 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 8255 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 88155 Durable; Visc; Homog; Not New TL; Al2O3 ; alkali 856 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 88957 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 88958 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 88959 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 88960 Durable; Not L Visc; Homog; Not New TL; Al2O3 ; alkali 889

WL Range # of EVs and Centroid % of Total10 34 3.8245219311 92 10.348706412 116 13.04836913 111 12.485939314 52 5.8492688415 29 3.2620922416 26 2.9246344217 39 4.3869516318 81 9.1113610819 143 16.085489320 123 13.835770521 43 4.83689539


259

Appendix J

MAR Calculations for Various Frit/Decant Combinations

Imm

obil

izat

ion

Tec

hnol

ogy

Sect

ion

WSR

C-T

R-2

002-

0049

1Sa

vann

ah R

iver

Tec

hnol

ogy

Cen

ter

Rev

. 0W

estin

ghou

se S

avan

nah

Riv

er C

ompa

ny

260

Frit/

Dec

ant

% W

LD

urab

ility

TL

Vis

cFr

itH

omog

Al 2

O3

alka

liT

LV

isc

∆GP

Hom

og20

2-D

ecan

t #5

25H

igh

NO

3.46

17.6

175

0.1

81.0

2-1

0.64

619

8.96

202-

Dec

ant #

526

NO

3.60

17.7

976

0.4

76.7

4-1

0.78

820

0.63

202-

Dec

ant #

527

NO

3.74

17.9

877

0.1

72.5

8-1

0.92

920

2.31

202-

Dec

ant #

528

NO

3.88

18.1

677

9.6

68.5

3-1

1.07

120

3.98

202-

Dec

ant #

529

NO

4.01

18.3

578

8.9

64.6

2-1

1.21

220

5.65

202-

Dec

ant #

530

NO

4.15

18.5

379

7.8

60.8

2-1

1.35

420

7.33

202-

Dec

ant #

531

NO

4.29

18.7

280

6.5

57.1

5-1

1.49

620

9.00

202-

Dec

ant #

532

NO

4.43

18.9

081

4.9

53.6

1-1

1.63

721

0.67

202-

Dec

ant #

533

4.57

19.0

982

3.0

50.2

0-1

1.77

921

2.34

202-

Dec

ant #

534

4.71

19.2

783

0.9

46.9

1-1

1.92

121

4.02

202-

Dec

ant #

535

4.85

19.4

583

8.6

43.7

5-1

2.06

221

5.69

202-

Dec

ant #

536

4.98

19.6

484

6.1

40.7

1-1

2.20

421

7.36

202-

Dec

ant #

537

5.12

19.8

285

3.4

37.8

0-1

2.34

521

9.03

202-

Dec

ant #

538

NO

5.26

20.0

186

0.5

35.0

2-1

2.48

722

0.71

202-

Dec

ant #

539

NO

5.40

20.1

986

7.3

32.3

7-1

2.62

922

2.38

202-

Dec

ant #

540

NO

5.54

20.3

887

4.1

29.8

4-1

2.77

022

4.05

202-

Dec

ant #

541

NO

5.68

20.5

688

0.6

27.4

3-1

2.91

222

5.73

202-

Dec

ant #

542

NO

5.81

20.7

588

6.9

25.1

5-1

3.05

322

7.40

202-

Dec

ant #

543

NO

Low

5.95

20.9

389

3.1

22.9

9-1

3.19

522

9.07

202-

Dec

ant #

544

NO

Low

6.09

21.1

189

9.2

20.9

6-1

3.33

623

0.74

202-

Dec

ant #

545

NO

Low

6.23

21.3

090

5.1

19.0

4-1

3.47

823

2.42

202-

Dec

ant #

546

NO

Low

6.37

21.4

891

0.8

17.2

3-1

3.62

023

4.09

202-

Dec

ant #

547

NO

Low

6.51

21.6

791

6.5

15.5

4-1

3.76

123

5.76

202-

Dec

ant #

548

NO

Low

6.65

21.8

592

1.9

13.9

7-1

3.90

323

7.44

202-

Dec

ant #

549

NO

Low

6.78

22.0

492

7.3

12.5

0-1

4.04

523

9.11

202-

Dec

ant #

550

NO

Low

6.92

22.2

293

2.5

11.1

4-1

4.18

624

0.78

202-

Dec

ant #

551

NO

Low

7.06

22.4

193

7.6

9.88

-14.

328

242.

4520

2-D

ecan

t #5

52N

OL

ow7.

2022

.59

942.

68.

73-1

4.46

924

4.13

202-

Dec

ant #

553

NO

Low

7.34

22.7

794

7.5

7.67

-14.

611

245.

8020

2-D

ecan

t #5

54N

OL

ow7.

4822

.96

952.

36.

70-1

4.75

324

7.47

202-

Dec

ant #

555

NO

Low

7.61

23.1

495

6.9

5.82

-14.

894

249.

14

Imm

obil

izat

ion

Tec

hnol

ogy

Sect

ion

WSR

C-T

R-2

002-

0049

1Sa

vann

ah R

iver

Tec

hnol

ogy

Cen

ter

Rev

. 0W

estin

ghou

se S

avan

nah

Riv

er C

ompa

ny

261

202-

Dec

ant #

556

NO

Low

7.75

23.3

396

1.5

5.02

-15.

036

250.

8220

2-D

ecan

t #5

57N

OL

ow7.

8923

.51

965.

94.

31-1

5.17

725

2.49

202-

Dec

ant #

558

NO

Low

8.03

23.7

097

0.3

3.67

-15.

319

254.

1620

2-D

ecan

t #5

59N

OL

ow8.

1723

.88

974.

63.

11-1

5.46

125

5.83

202-

Dec

ant #

560

NO

Low

8.31

24.0

697

8.8

2.60

-15.

602

257.

5120

2-M

-Dec

ant #

525

Hig

hH

igh

NO

4.21

16.8

673

1.6

121.

22-9

.459

204.

4020

2-M

-Dec

ant #

526

Hig

hH

igh

NO

4.34

17.0

574

2.3

114.

94-9

.616

206.

0020

2-M

-Dec

ant #

527

Hig

hN

O4.

4717

.25

752.

610

8.85

-9.7

7420

7.60

202-

M-D

ecan

t #5

28H

igh

NO

4.60

17.4

476

2.6

102.

92-9

.931

209.

2020

2-M

-Dec

ant #

529

NO

4.72

17.6

477

2.3

97.1

6-1

0.08

921

0.80

202-

M-D

ecan

t #5

304.

8517

.83

781.

691

.58

-10.

246

212.

4020

2-M

-Dec

ant #

531

4.98

18.0

379

0.7

86.1

8-1

0.40

321

4.00

202-

M-D

ecan

t #5

325.

1118

.22

799.

580

.95

-10.

561

215.

6020

2-M

-Dec

ant #

533

5.24

18.4

280

8.1

75.9

1-1

0.71

821

7.20

202-

M-D

ecan

t #5

345.

3718

.61

816.

471

.04

-10.

876

218.

8020

2-M

-Dec

ant #

535

5.50

18.8

082

4.5

66.3

5-1

1.03

322

0.40

202-

M-D

ecan

t #5

365.

6219

.00

832.

361

.85

-11.

191

222.

0020

2-M

-Dec

ant #

537

5.75

19.1

984

0.0

57.5

3-1

1.34

822

3.60

202-

M-D

ecan

t #5

385.

8819

.39

847.

453

.39

-11.

505

225.

2020

2-M

-Dec

ant #

539

6.01

19.5

885

4.6

49.4

3-1

1.66

322

6.80

202-

M-D

ecan

t #5

406.

1419

.78

861.

745

.65

-11.

820

228.

4020

2-M

-Dec

ant #

541

6.27

19.9

786

8.5

42.0

5-1

1.97

823

0.00

202-

M-D

ecan

t #5

426.

3920

.17

875.

138

.63

-12.

135

231.

6020

2-M

-Dec

ant #

543

6.52

20.3

688

1.7

35.3

8-1

2.29

323

3.20

202-

M-D

ecan

t #5

44N

O6.

6520

.55

888.

032

.31

-12.

450

234.

8020

2-M

-Dec

ant #

545

NO

6.78

20.7

589

4.2

29.4

1-1

2.60

823

6.41

202-

M-D

ecan

t #5

46N

O6.

9120

.94

900.

226

.68

-12.

765

238.

0020

2-M

-Dec

ant #

547

NO

Low

7.04

21.1

490

6.1

24.1

2-1

2.92

223

9.61

202-

M-D

ecan

t #5

48N

OL

ow7.

1721

.33

911.

921

.73

-13.

080

241.

2120

2-M

-Dec

ant #

549

NO

Low

7.29

21.5

391

7.5

19.4

9-1

3.23

724

2.80

202-

M-D

ecan

t #5

50N

OL

ow7.

4221

.72

923.

017

.41

-13.

395

244.

4120

2-M

-Dec

ant #

551

NO

Low

7.55

21.9

292

8.4

15.4

9-1

3.55

224

6.01

202-

M-D

ecan

t #5

52N

OL

ow7.

6822

.11

933.

613

.71

-13.

709

247.

6120

2-M

-Dec

ant #

553

NO

Low

7.81

22.3

093

8.7

12.0

8-1

3.86

724

9.21

Imm

obil

izat

ion

Tec

hnol

ogy

Sect

ion

WSR

C-T

R-2

002-

0049

1Sa

vann

ah R

iver

Tec

hnol

ogy

Cen

ter

Rev

. 0W

estin

ghou

se S

avan

nah

Riv

er C

ompa

ny

262

202-

M-D

ecan

t #5

54N

OL

ow7.

9422

.50

943.

810

.59

-14.

024

250.

8120

2-M

-Dec

ant #

555

NO

Low

8.06

22.6

994

8.7

9.22

-14.

182

252.

4120

2-M

-Dec

ant #

556

NO

Low

8.19

22.8

995

3.5

7.99

-14.

339

254.

0120

2-M

-Dec

ant #

557

NO

Low

8.32

23.0

895

8.2

6.88

-14.

497

255.

6120

2-M

-Dec

ant #

558

NO

Low

8.45

23.2

896

2.8

5.88

-14.

654

257.

2120

2-M

-Dec

ant #

559

NO

Low

8.58

23.4

796

7.3

4.99

-14.

811

258.

8120

2-M

-Dec

ant #

560

NO

Low

8.71

23.6

697

1.7

4.20

-14.

969

260.

4120

2-M

2-D

ecan

t #5

25H

igh

Hig

hN

O4.

2116

.86

733.

410

4.37

-9.7

8520

4.40

202-

M2-

Dec

ant #

526

Hig

hN

O4.

3417

.05

744.

298

.84

-9.9

3820

6.00

202-

M2-

Dec

ant #

527

NO

4.47

17.2

575

4.4

93.4

7-1

0.09

120

7.60

202-

M2-

Dec

ant #

528

NO

4.60

17.4

476

4.4

88.2

6-1

0.24

420

9.20

202-

M2-

Dec

ant #

529

NO

4.72

17.6

477

4.0

83.2

0-1

0.39

721

0.80

202-

M2-

Dec

ant #

530

4.85

17.8

378

3.4

78.3

1-1

0.55

021

2.40

202-

M2-

Dec

ant #

531

4.98

18.0

379

2.5

73.5

8-1

0.70

321

4.00

202-

M2-

Dec

ant #

532

5.11

18.2

280

1.3

69.0

1-1

0.85

621

5.60

202-

M2-

Dec

ant #

533

5.24

18.4

280

9.8

64.6

1-1

1.00

921

7.20

202-

M2-

Dec

ant #

534

5.37

18.6

181

8.0

60.3

7-1

1.16

221

8.80

202-

M2-

Dec

ant #

535

5.50

18.8

082

6.1

56.2

9-1

1.31

622

0.40

202-

M2-

Dec

ant #

536

5.62

19.0

083

4.0

52.3

8-1

1.46

922

2.00

202-

M2-

Dec

ant #

537

5.75

19.1

984

1.6

48.6

4-1

1.62

222

3.60

202-

M2-

Dec

ant #

538

5.88

19.3

984

8.9

45.0

5-1

1.77

522

5.20

202-

M2-

Dec

ant #

539

6.01

19.5

885

6.1

41.6

3-1

1.92

822

6.80

202-

M2-

Dec

ant #

540

6.14

19.7

886

3.2

38.3

7-1

2.08

122

8.40

202-

M2-

Dec

ant #

541

6.27

19.9

786

9.9

35.2

7-1

2.23

423

0.00

202-

M2-

Dec

ant #

542

NO

6.39

20.1

787

6.6

32.3

4-1

2.38

723

1.60

202-

M2-

Dec

ant #

543

NO

6.52

20.3

688

3.1

29.5

6-1

2.54

023

3.20

202-

M2-

Dec

ant #

544

NO

6.65

20.5

588

9.4

26.9

3-1

2.69

323

4.80

202-

M2-

Dec

ant #

545

NO

6.78

20.7

589

5.6

24.4

6-1

2.84

623

6.41

202-

M2-

Dec

ant #

546

NO

Low

6.91

20.9

490

1.6

22.1

4-1

2.99

923

8.00

202-

M2-

Dec

ant #

547

NO

Low

7.04

21.1

490

7.4

19.9

6-1

3.15

323

9.61

202-

M2-

Dec

ant #

548

NO

Low

7.17

21.3

391

3.2

17.9

4-1

3.30

624

1.21

202-

M2-

Dec

ant #

549

NO

Low

7.29

21.5

391

8.8

16.0

5-1

3.45

924

2.80

202-

M2-

Dec

ant #

550

NO

Low

7.42

21.7

292

4.2

14.3

0-1

3.61

224

4.41

202-

M2-

Dec

ant #

551

NO

Low

7.55

21.9

292

9.6

12.6

8-1

3.76

524

6.01

Imm

obil

izat

ion

Tec

hnol

ogy

Sect

ion

WSR

C-T

R-2

002-

0049

1Sa

vann

ah R

iver

Tec

hnol

ogy

Cen

ter

Rev

. 0W

estin

ghou

se S

avan

nah

Riv

er C

ompa

ny

263

202-

M2-

Dec

ant #

552

NO

Low

7.68

22.1

193

4.8

11.2

0-1

3.91

824

7.61

202-

M2-

Dec

ant #

553

NO

Low

7.81

22.3

093

9.9

9.83

-14.

071

249.

2120

2-M

2-D

ecan

t #5

54N

OL

ow7.

9422

.50

944.

98.

59-1

4.22

425

0.80

202-

M2-

Dec

ant #

555

NO

Low

8.06

22.6

994

9.7

7.46

-14.

377

252.

4120

2-M

2-D

ecan

t #5

56N

OL

ow8.

1922

.89

954.

66.

44-1

4.53

025

4.01

202-

M2-

Dec

ant #

557

NO

Low

8.32

23.0

895

9.2

5.52

-14.

683

255.

6120

2-M

2-D

ecan

t #5

58N

OL

ow8.

4523

.28

963.

84.

70-1

4.83

625

7.21

202-

M2-

Dec

ant #

559

NO

Low

8.58

23.4

796

8.3

3.98

-14.

990

258.

8120

2-M

2-D

ecan

t #5

60N

OL

ow8.

7123

.66

972.

73.

34-1

5.14

326

0.41

S-D

ecan

t #5

25H

igh

Hig

hN

O3.

4615

.36

735.

316

4.40

-8.3

3820

1.37

S-D

ecan

t #5

26H

igh

Hig

hN

O3.

6015

.57

746.

515

6.18

-8.5

1120

3.01

S-D

ecan

t #5

27H

igh

Hig

hN

O3.

7415

.79

757.

214

8.17

-8.6

8320

4.65

S-D

ecan

t #5

28H

igh

NO

3.88

16.0

076

7.6

140.

37-8

.856

206.

29S-

Dec

ant #

529

Hig

hN

O4.

0116

.22

777.

613

2.78

-9.0

2820

7.93

S-D

ecan

t #5

30H

igh

NO

4.15

16.4

378

7.3

125.

41-9

.200

209.

57S-

Dec

ant #

531

Hig

h4.

2916

.65

796.

611

8.25

-9.3

7321

1.21

S-D

ecan

t #5

32H

igh

4.43

16.8

680

5.7

111.

32-9

.545

212.

85S-

Dec

ant #

533

Hig

h4.

5717

.08

814.

410

4.61

-9.7

1721

4.49

S-D

ecan

t #5

344.

7117

.29

822.

898

.13

-9.8

9021

6.13

S-D

ecan

t #5

354.

8517

.50

831.

191

.87

-10.

062

217.

77S-

Dec

ant #

536

4.98

17.7

283

9.1

85.8

4-1

0.23

521

9.41

S-D

ecan

t #5

375.

1217

.93

846.

880

.04

-10.

407

221.

05S-

Dec

ant #

538

5.26

18.1

585

4.3

74.4

6-1

0.57

922

2.69

S-D

ecan

t #5

395.

4018

.36

861.

569

.12

-10.

752

224.

34S-

Dec

ant #

540

5.54

18.5

886

8.7

64.0

1-1

0.92

422

5.98

S-D

ecan

t #5

415.

6818

.79

875.

559

.12

-11.

096

227.

62S-

Dec

ant #

542

5.81

19.0

188

2.2

54.4

7-1

1.26

922

9.26

S-D

ecan

t #5

435.

9519

.22

888.

750

.04

-11.

441

230.

90S-

Dec

ant #

544

6.09

19.4

389

5.0

45.8

3-1

1.61

423

2.54

S-D

ecan

t #5

456.

2319

.65

901.

241

.86

-11.

786

234.

18S-

Dec

ant #

546

6.37

19.8

690

7.2

38.1

0-1

1.95

823

5.82

S-D

ecan

t #5

476.

5120

.08

913.

134

.56

-12.

131

237.

46S-

Dec

ant #

548

6.65

20.2

991

8.8

31.2

4-1

2.30

323

9.10

S-D

ecan

t #5

49N

O6.

7820

.51

924.

328

.13

-12.

475

240.

74

Imm

obil

izat

ion

Tec

hnol

ogy

Sect

ion

WSR

C-T

R-2

002-

0049

1Sa

vann

ah R

iver

Tec

hnol

ogy

Cen

ter

Rev

. 0W

estin

ghou

se S

avan

nah

Riv

er C

ompa

ny

264

S-D

ecan

t #5

50N

O6.

9220

.72

929.

725

.22

-12.

648

242.

38S-

Dec

ant #

551

NO

Low

7.06

20.9

493

5.0

22.5

2-1

2.82

024

4.03

S-D

ecan

t #5

52N

OL

ow7.

2021

.15

940.

220

.02

-12.

992

245.

67S-

Dec

ant #

553

NO

Low

7.34

21.3

694

5.2

17.7

1-1

3.16

524

7.31

S-D

ecan

t #5

54N

OL

ow7.

4821

.58

950.

215

.59

-13.

337

248.

94S-

Dec

ant #

555

NO

Low

7.61

21.7

995

4.9

13.6

5-1

3.51

025

0.59

S-D

ecan

t #5

56N

OL

ow7.

7522

.01

959.

711

.88

-13.

682

252.

23S-

Dec

ant #

557

NO

Low

7.89

22.2

296

4.2

10.2

7-1

3.85

425

3.87

S-D

ecan

t #5

58N

OL

ow8.

0322

.44

968.

78.

83-1

4.02

725

5.51

S-D

ecan

t #5

59N

OL

ow8.

1722

.65

973.

17.

53-1

4.19

925

7.15

S-D

ecan

t #5

60N

OL

ow8.

3122

.86

977.

46.

38-1

4.37

125

8.79

T-D

ecan

t #5

25H

igh

Hig

hN

O3.

4615

.36

735.

715

0.39

-8.2

9920

1.37

T-D

ecan

t #5

26H

igh

Hig

hN

O3.

6015

.57

747.

014

2.86

-8.4

7220

3.01

T-D

ecan

t #5

27H

igh

Hig

hN

O3.

7415

.79

757.

713

5.54

-8.6

4520

4.65

T-D

ecan

t #5

28H

igh

NO

3.88

16.0

076

8.1

128.

41-8

.818

206.

29T

-Dec

ant #

529

Hig

hN

O4.

0116

.22

778.

112

1.47

-8.9

9120

7.93

T-D

ecan

t #5

30H

igh

NO

4.15

16.4

378

7.8

114.

73-9

.164

209.

57T

-Dec

ant #

531

Hig

h4.

2916

.65

797.

110

8.19

-9.3

3721

1.21

T-D

ecan

t #5

32H

igh

4.43

16.8

680

6.2

101.

85-9

.510

212.

85T

-Dec

ant #

533

4.57

17.0

881

4.9

95.7

2-9

.683

214.

49T

-Dec

ant #

534

4.71

17.2

982

3.4

89.7

9-9

.855

216.

13T

-Dec

ant #

535

4.85

17.5

083

1.7

84.0

6-1

0.02

821

7.77

T-D

ecan

t #5

364.

9817

.72

839.

678

.55

-10.

201

219.

41T

-Dec

ant #

537

5.12

17.9

384

7.4

73.2

4-1

0.37

422

1.05

T-D

ecan

t #5

385.

2618

.15

854.

968

.15

-10.

547

222.

69T

-Dec

ant #

539

5.40

18.3

686

2.1

63.2

6-1

0.72

022

4.34

T-D

ecan

t #5

405.

5418

.58

869.

258

.58

-10.

893

225.

98T

-Dec

ant #

541

5.68

18.7

987

6.0

54.1

1-1

1.06

622

7.62

T-D

ecan

t #5

425.

8119

.01

882.

749

.85

-11.

238

229.

26T

-Dec

ant #

543

5.95

19.2

288

9.2

45.8

0-1

1.41

223

0.90

T-D

ecan

t #5

446.

0919

.43

895.

641

.96

-11.

584

232.

54T

-Dec

ant #

545

6.23

19.6

590

1.7

38.3

2-1

1.75

723

4.18

T-D

ecan

t #5

466.

3719

.86

907.

734

.88

-11.

930

235.

82T

-Dec

ant #

547

6.51

20.0

891

3.6

31.6

4-1

2.10

323

7.46

Imm

obil

izat

ion

Tec

hnol

ogy

Sect

ion

WSR

C-T

R-2

002-

0049

1Sa

vann

ah R

iver

Tec

hnol

ogy

Cen

ter

Rev

. 0W

estin

ghou

se S

avan

nah

Riv

er C

ompa

ny

265

T-D

ecan

t #5

486.

6520

.29

919.

328

.60

-12.

276

239.

10T

-Dec

ant #

549

NO

6.78

20.5

192

4.8

25.7

5-1

2.44

924

0.74

T-D

ecan

t #5

50N

OL

ow6.

9220

.72

930.

223

.10

-12.

622

242.

38T

-Dec

ant #

551

NO

Low

7.06

20.9

493

5.5

20.6

3-1

2.79

524

4.03

T-D

ecan

t #5

52N

OL

ow7.

2021

.15

940.

718

.34

-12.

967

245.

67T

-Dec

ant #

553

NO

Low

7.34

21.3

694

5.7

16.2

2-1

3.14

024

7.31

T-D

ecan

t #5

54N

OL

ow7.

4821

.58

950.

714

.28

-13.

313

248.

94T

-Dec

ant #

555

NO

Low

7.61

21.7

995

5.4

12.5

0-1

3.48

625

0.59

T-D

ecan

t #5

56N

OL

ow7.

7522

.01

960.

210

.88

-13.

659

252.

23T

-Dec

ant #

557

NO

Low

7.89

22.2

296

4.7

9.41

-13.

832

253.

87T

-Dec

ant #

558

NO

Low

8.03

22.4

496

9.2

8.09

-14.

005

255.

51T

-Dec

ant #

559

NO

Low

8.17

22.6

597

3.6

6.90

-14.

178

257.

15T

-Dec

ant #

560

NO

Low

8.31

22.8

697

7.9

5.85

-14.

351

258.

79U

-Dec

ant #

525

Hig

hH

igh

NO

3.46

16.1

172

3.3

102.

24-8

.876

201.

37U

-Dec

ant #

526

Hig

hN

O3.

6016

.31

734.

897

.07

-9.0

4120

3.01

U-D

ecan

t #5

27H

igh

NO

3.74

16.5

274

5.7

92.0

6-9

.206

204.

65U

-Dec

ant #

528

NO

3.88

16.7

275

6.4

87.1

7-9

.371

206.

29U

-Dec

ant #

529

NO

4.01

16.9

376

6.6

82.4

1-9

.536

207.

93U

-Dec

ant #

530

NO

4.15

17.1

377

6.5

77.7

9-9

.702

209.

57U

-Dec

ant #

531

4.29

17.3

478

6.1

73.3

2-9

.867

211.

21U

-Dec

ant #

532

4.43

17.5

479

5.4

68.9

8-1

0.03

221

2.85

U-D

ecan

t #5

334.

5717

.75

804.

464

.79

-10.

197

214.

49U

-Dec

ant #

534

4.71

17.9

581

3.1

60.7

4-1

0.36

221

6.13

U-D

ecan

t #5

354.

8518

.15

821.

656

.83

-10.

528

217.

77U

-Dec

ant #

536

4.98

18.3

682

9.8

53.0

7-1

0.69

321

9.42

U-D

ecan

t #5

375.

1218

.56

837.

849

.45

-10.

858

221.

05U

-Dec

ant #

538

5.26

18.7

784

5.5

45.9

8-1

1.02

322

2.69

U-D

ecan

t #5

395.

4018

.97

853.

042

.65

-11.

189

224.

34U

-Dec

ant #

540

5.54

19.1

886

0.4

39.4

7-1

1.35

422

5.98

U-D

ecan

t #5

415.

6819

.38

867.

436

.43

-11.

519

227.

62U

-Dec

ant #

542

5.81

19.5

987

4.3

33.5

4-1

1.68

422

9.26

U-D

ecan

t #5

435.

9519

.79

881.

030

.79

-11.

849

230.

90U

-Dec

ant #

544

6.09

19.9

988

7.6

28.1

8-1

2.01

423

2.54

U-D

ecan

t #5

456.

2320

.20

894.

025

.71

-12.

180

234.

18

Imm

obil

izat

ion

Tec

hnol

ogy

Sect

ion

WSR

C-T

R-2

002-

0049

1Sa

vann

ah R

iver

Tec

hnol

ogy

Cen

ter

Rev

. 0W

estin

ghou

se S

avan

nah

Riv

er C

ompa

ny

266

U-D

ecan

t #5

46L

ow6.

3720

.40

900.

223

.39

-12.

345

235.

82U

-Dec

ant #

547

NO

Low

6.51

20.6

190

6.2

21.2

0-1

2.51

023

7.46

U-D

ecan

t #5

48N

OL

ow6.

6520

.81

912.

219

.14

-12.

675

239.

10U

-Dec

ant #

549

NO

Low

6.78

21.0

291

7.9

17.2

2-1

2.84

124

0.74

U-D

ecan

t #5

50N

OL

ow6.

9221

.22

923.

515

.43

-13.

006

242.

38U

-Dec

ant #

551

NO

Low

7.06

21.4

392

9.0

13.7

6-1

3.17

124

4.03

U-D

ecan

t #5

52N

OL

ow7.

2021

.63

934.

412

.22

-13.

336

245.

67U

-Dec

ant #

553

NO

Low

7.34

21.8

393

9.5

10.8

0-1

3.50

124

7.31

U-D

ecan

t #5

54N

OL

ow7.

4822

.04

944.

79.

50-1

3.66

624

8.94

U-D

ecan

t #5

55N

OL

ow7.

6122

.24

949.

68.

30-1

3.83

225

0.59

U-D

ecan

t #5

56N

OL

ow7.

7522

.45

954.

67.

22-1

3.99

725

2.23

U-D

ecan

t #5

57N

OL

ow7.

8922

.65

959.

36.

23-1

4.16

225

3.87

U-D

ecan

t #5

58N

OL

ow8.

0322

.86

963.

95.

35-1

4.32

725

5.51

U-D

ecan

t #5

59N

OL

ow8.

1723

.06

968.

54.

56-1

4.49

325

7.15

U-D

ecan

t #5

60N

OL

ow8.

3123

.26

973.

03.

86-1

4.65

825

8.79

U2-

Dec

ant #

525

Hig

hN

O3.

4616

.11

725.

187

.98

-9.2

0120

1.37

U2-

Dec

ant #

526

Hig

hN

O3.

6016

.31

736.

583

.44

-9.3

6220

3.01

U2-

Dec

ant #

527

Hig

hN

O3.

7416

.52

747.

579

.02

-9.5

2320

4.65

U2-

Dec

ant #

528

NO

3.88

16.7

275

8.1

74.7

3-9

.684

206.

29U

2-D

ecan

t #5

29N

O4.

0116

.93

768.

370

.56

-9.8

4520

7.93

U2-

Dec

ant #

530

NO

4.15

17.1

377

8.2

66.5

1-1

0.00

620

9.57

U2-

Dec

ant #

531

4.29

17.3

478

7.8

62.5

9-1

0.16

721

1.21

U2-

Dec

ant #

532

4.43

17.5

479

7.1

58.8

1-1

0.32

721

2.85

U2-

Dec

ant #

533

4.57

17.7

580

6.0

55.1

5-1

0.48

821

4.49

U2-

Dec

ant #

534

4.71

17.9

581

4.7

51.6

2-1

0.64

921

6.13

U2-

Dec

ant #

535

4.85

18.1

582

3.2

48.2

3-1

0.81

021

7.77

U2-

Dec

ant #

536

4.98

18.3

683

1.4

44.9

6-1

0.97

121

9.42

U2-

Dec

ant #

537

5.12

18.5

683

9.3

41.8

2-1

1.13

222

1.05

U2-

Dec

ant #

538

5.26

18.7

784

7.0

38.8

2-1

1.29

322

2.69

U2-

Dec

ant #

539

5.40

18.9

785

4.5

35.9

5-1

1.45

422

4.34

U2-

Dec

ant #

540

5.54

19.1

886

1.8

33.2

0-1

1.61

422

5.98

U2-

Dec

ant #

541

5.68

19.3

886

8.8

30.5

9-1

1.77

522

7.62

U2-

Dec

ant #

542

5.81

19.5

987

5.7

28.1

0-1

1.93

622

9.26

U2-

Dec

ant #

543

5.95

19.7

988

2.4

25.7

5-1

2.09

723

0.90

Imm

obil

izat

ion

Tec

hnol

ogy

Sect

ion

WSR

C-T

R-2

002-

0049

1Sa

vann

ah R

iver

Tec

hnol

ogy

Cen

ter

Rev

. 0W

estin

ghou

se S

avan

nah

Riv

er C

ompa

ny

267

U2-

Dec

ant #

544

Low

6.09

19.9

988

9.0

23.5

2-1

2.25

823

2.54

U2-

Dec

ant #

545

NO

Low

6.23

20.2

089

5.3

21.4

1-1

2.41

923

4.18

U2-

Dec

ant #

546

NO

Low

6.37

20.4

090

1.5

19.4

3-1

2.57

923

5.82

U2-

Dec

ant #

547

NO

Low

6.51

20.6

190

7.5

17.5

7-1

2.74

023

7.46

U2-

Dec

ant #

548

NO

Low

6.65

20.8

191

3.4

15.8

3-1

2.90

123

9.10

U2-

Dec

ant #

549

NO

Low

6.78

21.0

291

9.1

14.2

0-1

3.06

224

0.74

U2-

Dec

ant #

550

NO

Low

6.92

21.2

292

4.7

12.6

9-1

3.22

324

2.38

U2-

Dec

ant #

551

NO

Low

7.06

21.4

393

0.2

11.2

9-1

3.38

424

4.03

U2-

Dec

ant #

552

NO

Low

7.20

21.6

393

5.5

10.0

0-1

3.54

524

5.67

U2-

Dec

ant #

553

NO

Low

7.34

21.8

394

0.7

8.81

-13.

706

247.

31U

2-D

ecan

t #5

54N

OL

ow7.

4822

.04

945.

87.

72-1

3.86

624

8.94

U2-

Dec

ant #

555

NO

Low

7.61

22.2

495

0.7

6.73

-14.

027

250.

59U

2-D

ecan

t #5

56N

OL

ow7.

7522

.45

955.

65.

83-1

4.18

825

2.23

U2-

Dec

ant #

557

NO

Low

7.89

22.6

596

0.3

5.02

-14.

349

253.

87U

2-D

ecan

t #5

58N

OL

ow8.

0322

.86

964.

94.

30-1

4.51

025

5.51

U2-

Dec

ant #

559

NO

Low

8.17

23.0

696

9.5

3.65

-14.

671

257.

15U

2-D

ecan

t #5

60N

OL

ow8.

3123

.26

973.

93.

07-1

4.83

225

8.79

202-

Dec

ant #

925

Hig

hN

O3.

8715

.60

827.

010

1.68

-8.7

5920

3.77

202-

Dec

ant #

926

NO

4.02

15.7

183

9.3

97.4

8-8

.826

205.

6320

2-D

ecan

t #9

27N

O4.

1815

.81

851.

193

.36

-8.8

9220

7.50

202-

Dec

ant #

928

NO

4.33

15.9

186

2.6

89.3

0-8

.958

209.

3620

2-D

ecan

t #9

294.

4916

.02

873.

885

.32

-9.0

2421

1.23

202-

Dec

ant #

930

4.64

16.1

288

4.6

81.4

1-9

.090

213.

0920

2-D

ecan

t #9

314.

7916

.23

895.

177

.58

-9.1

5621

4.96

202-

Dec

ant #

932

4.95

16.3

390

5.3

73.8

3-9

.222

216.

8220

2-D

ecan

t #9

335.

1016

.43

915.

370

.16

-9.2

8821

8.69

202-

Dec

ant #

934

5.26

16.5

492

5.0

66.5

7-9

.355

220.

5520

2-D

ecan

t #9

355.

4116

.64

934.

463

.07

-9.4

2122

2.42

202-

Dec

ant #

936

5.57

16.7

594

3.5

59.6

6-9

.487

224.

2820

2-D

ecan

t #9

375.

7216

.85

952.

456

.33

-9.5

5322

6.15

202-

Dec

ant #

938

5.88

16.9

596

1.1

53.1

0-9

.619

228.

0220

2-D

ecan

t #9

396.

0317

.06

969.

549

.95

-9.6

8522

9.88

202-

Dec

ant #

940

6.19

17.1

697

7.8

46.9

0-9

.751

231.

7420

2-D

ecan

t #9

416.

3417

.27

985.

843

.95

-9.8

1823

3.61

Imm

obil

izat

ion

Tec

hnol

ogy

Sect

ion

WSR

C-T

R-2

002-

0049

1Sa

vann

ah R

iver

Tec

hnol

ogy

Cen

ter

Rev

. 0W

estin

ghou

se S

avan

nah

Riv

er C

ompa

ny

268

202-

Dec

ant #

942

6.50

17.3

799

3.7

41.0

9-9

.884

235.

4720

2-D

ecan

t #9

436.

6517

.47

1001

.338

.34

-9.9

5023

7.34

202-

Dec

ant #

944

6.81

17.5

810

08.7

35.6

8-1

0.01

623

9.20

202-

Dec

ant #

945

6.96

17.6

810

16.1

33.1

2-1

0.08

224

1.07

202-

Dec

ant #

946

NO

7.11

17.7

910

23.1

30.6

7-1

0.14

824

2.93

202-

Dec

ant #

947

NO

7.27

17.8

910

30.1

28.3

2-1

0.21

424

4.80

202-

Dec

ant #

948

NO

7.42

18.0

010

36.9

26.0

7-1

0.28

124

6.67

202-

Dec

ant #

949

NO

Low

7.58

18.1

010

43.5

23.9

3-1

0.34

624

8.53

202-

Dec

ant #

950

NO

Low

7.73

18.2

010

50.0

21.8

9-1

0.41

325

0.39

202-

Dec

ant #

951

NO

Low

7.89

18.3

110

56.3

19.9

6-1

0.47

925

2.26

202-

Dec

ant #

952

NO

Low

8.04

18.4

110

62.5

18.1

3-1

0.54

525

4.13

202-

Dec

ant #

953

NO

Low

8.20

18.5

210

68.6

16.4

0-1

0.61

125

5.99

202-

Dec

ant #

954

NO

Low

8.35

18.6

210

74.5

14.7

8-1

0.67

725

7.86

202-

Dec

ant #

955

NO

Low

8.51

18.7

210

80.3

13.2

6-1

0.74

325

9.72

202-

Dec

ant #

956

NO

Low

8.66

18.8

310

86.0

11.8

4-1

0.81

026

1.58

202-

Dec

ant #

957

NO

Low

8.82

18.9

310

91.5

10.5

2-1

0.87

626

3.45

202-

Dec

ant #

958

NO

Low

8.97

19.0

410

97.0

9.29

-10.

942

265.

3220

2-D

ecan

t #9

59N

OL

ow9.

1319

.14

1102

.48.

17-1

1.00

826

7.18

202-

Dec

ant #

960

NO

Low

9.28

19.2

411

07.6

7.13

-11.

074

269.

0420

2-M

-Dec

ant #

925

Hig

hN

O4.

6214

.85

805.

715

1.21

-7.5

7220

9.21

202-

M-D

ecan

t #9

26H

igh

4.76

14.9

781

8.4

145.

10-7

.654

211.

0020

2-M

-Dec

ant #

927

Hig

h4.

9115

.08

830.

713

9.08

-7.7

3621

2.79

202-

M-D

ecan

t #9

28H

igh

5.05

15.1

984

2.6

133.

17-7

.818

214.

5820

2-M

-Dec

ant #

929

Hig

h5.

2015

.31

854.

212

7.35

-7.9

0021

6.38

202-

M-D

ecan

t #9

30H

igh

5.34

15.4

286

5.4

121.

65-7

.982

218.

1720

2-M

-Dec

ant #

931

Hig

h5.

4815

.54

876.

311

6.03

-8.0

6421

9.96

202-

M-D

ecan

t #9

32H

igh

5.63

15.6

588

6.9

110.

54-8

.146

221.

7520

2-M

-Dec

ant #

933

Hig

h5.

7715

.76

897.

210

5.16

-8.2

2822

3.55

202-

M-D

ecan

t #9

34H

igh

5.92

15.8

890

7.3

99.8

9-8

.310

225.

3420

2-M

-Dec

ant #

935

6.06

15.9

991

7.0

94.7

4-8

.392

227.

1320

2-M

-Dec

ant #

936

6.21

16.1

192

6.5

89.7

3-8

.474

228.

9320

2-M

-Dec

ant #

937

6.35

16.2

293

5.8

84.8

2-8

.556

230.

7220

2-M

-Dec

ant #

938

6.50

16.3

394

4.8

80.0

5-8

.638

232.

5120

2-M

-Dec

ant #

939

6.64

16.4

595

3.6

75.4

1-8

.720

234.

30

Imm

obil

izat

ion

Tec

hnol

ogy

Sect

ion

WSR

C-T

R-2

002-

0049

1Sa

vann

ah R

iver

Tec

hnol

ogy

Cen

ter

Rev

. 0W

estin

ghou

se S

avan

nah

Riv

er C

ompa

ny

269

202-

M-D

ecan

t #9

406.

7916

.56

962.

270

.90

-8.8

0123

6.09

202-

M-D

ecan

t #9

416.

9316

.68

970.

566

.52

-8.8

8423

7.89

202-

M-D

ecan

t #9

427.

0816

.79

978.

762

.29

-8.9

6623

9.68

202-

M-D

ecan

t #9

437.

2216

.90

986.

658

.19

-9.0

4824

1.47

202-

M-D

ecan

t #9

447.

3717

.02

994.

454

.25

-9.1

2924

3.26

202-

M-D

ecan

t #9

457.

5117

.13

1002

.050

.44

-9.2

1124

5.06

202-

M-D

ecan

t #9

467.

6517

.25

1009

.446

.77

-9.2

9324

6.85

202-

M-D

ecan

t #9

477.

8017

.36

1016

.643

.26

-9.3

7524

8.64

202-

M-D

ecan

t #9

48N

O7.

9417

.47

1023

.739

.89

-9.4

5725

0.44

202-

M-D

ecan

t #9

49N

O8.

0917

.59

1030

.736

.68

-9.5

3925

2.23

202-

M-D

ecan

t #9

50N

O8.

2317

.70

1037

.533

.62

-9.6

2125

4.02

202-

M-D

ecan

t #9

51N

O8.

3817

.82

1044

.130

.71

-9.7

0325

5.81

202-

M-D

ecan

t #9

52N

O8.

5217

.93

1050

.627

.94

-9.7

8525

7.61

202-

M-D

ecan

t #9

53N

O8.

6718

.05

1056

.925

.34

-9.8

6725

9.40

202-

M-D

ecan

t #9

54N

OL

ow8.

8118

.16

1063

.222

.88

-9.9

4926

1.19

202-

M-D

ecan

t #9

55N

OL

ow8.

9618

.27

1069

.320

.57

-10.

031

262.

9820

2-M

-Dec

ant #

956

NO

Low

9.10

18.3

910

75.2

18.4

1-1

0.11

326

4.78

202-

M-D

ecan

t #9

57N

OL

ow9.

2518

.50

1081

.116

.39

-10.

195

266.

5720

2-M

-Dec

ant #

958

NO

Low

9.39

18.6

210

86.8

14.5

2-1

0.27

726

8.36

202-

M-D

ecan

t #9

59N

OL

ow9.

5418

.73

1092

.412

.79

-10.

359

270.

1520

2-M

-Dec

ant #

960

NO

Low

9.68

18.8

410

97.9

11.2

0-1

0.44

127

1.95

202-

M2-

Dec

ant #

925

Hig

hN

O4.

6214

.85

808.

013

0.95

-7.8

9820

9.21

202-

M2-

Dec

ant #

926

Hig

h4.

7614

.97

820.

712

5.54

-7.9

7621

1.00

202-

M2-

Dec

ant #

927

Hig

h4.

9115

.08

832.

912

0.21

-8.0

5321

2.79

202-

M2-

Dec

ant #

928

Hig

h5.

0515

.19

844.

911

4.97

-8.1

3121

4.58

202-

M2-

Dec

ant #

929

Hig

h5.

2015

.31

856.

410

9.84

-8.2

0921

6.38

202-

M2-

Dec

ant #

930

Hig

h5.

3415

.42

867.

610

4.80

-8.2

8621

8.17

202-

M2-

Dec

ant #

931

Hig

h5.

4815

.54

878.

599

.85

-8.3

6421

9.96

202-

M2-

Dec

ant #

932

5.63

15.6

588

9.1

95.0

1-8

.441

221.

7620

2-M

2-D

ecan

t #9

335.

7715

.76

899.

490

.28

-8.5

1922

3.55

202-

M2-

Dec

ant #

934

5.92

15.8

890

9.4

85.6

5-8

.597

225.

3420

2-M

2-D

ecan

t #9

356.

0615

.99

919.

181

.13

-8.6

7422

7.13

202-

M2-

Dec

ant #

936

6.21

16.1

192

8.5

76.7

3-8

.752

228.

9320

2-M

2-D

ecan

t #9

376.

3516

.22

937.

872

.44

-8.8

2923

0.72

Imm

obil

izat

ion

Tec

hnol

ogy

Sect

ion

WSR

C-T

R-2

002-

0049

1Sa

vann

ah R

iver

Tec

hnol

ogy

Cen

ter

Rev

. 0W

estin

ghou

se S

avan

nah

Riv

er C

ompa

ny

270

202-

M2-

Dec

ant #

938

6.50

16.3

394

6.8

68.2

7-8

.907

232.

5120

2-M

2-D

ecan

t #9

396.

6416

.45

955.

564

.22

-8.9

8523

4.30

202-

M2-

Dec

ant #

940

6.79

16.5

696

4.1

60.2

9-9

.062

236.

0920

2-M

2-D

ecan

t #9

416.

9316

.68

972.

456

.48

-9.1

4023

7.89

202-

M2-

Dec

ant #

942

7.08

16.7

998

0.5

52.8

1-9

.218

239.

6820

2-M

2-D

ecan

t #9

437.

2216

.90

988.

449

.25

-9.2

9524

1.47

202-

M2-

Dec

ant #

944

7.37

17.0

299

6.2

45.8

3-9

.373

243.

2620

2-M

2-D

ecan

t #9

457.

5117

.13

1003

.842

.54

-9.4

5024

5.06

202-

M2-

Dec

ant #

946

7.65

17.2

510

11.1

39.3

8-9

.528

246.

8520

2-M

2-D

ecan

t #9

477.

8017

.36

1018

.336

.36

-9.6

0624

8.64

202-

M2-

Dec

ant #

948

NO

7.94

17.4

710

25.4

33.4

6-9

.683

250.

4420

2-M

2-D

ecan

t #9

49N

O8.

0917

.59

1032

.330

.71

-9.7

6125

2.23

202-

M2-

Dec

ant #

950

NO

8.23

17.7

010

39.1

28.0

9-9

.838

254.

0220

2-M

2-D

ecan

t #9

51N

O8.

3817

.82

1045

.725

.60

-9.9

1625

5.81

202-

M2-

Dec

ant #

952

NO

Low

8.52

17.9

310

52.1

23.2

4-9

.994

257.

6120

2-M

2-D

ecan

t #9

53N

OL

ow8.

6718

.05

1058

.421

.03

-10.

071

259.

4020

2-M

2-D

ecan

t #9

54N

OL

ow8.

8118

.16

1064

.618

.94

-10.

149

261.

1920

2-M

2-D

ecan

t #9

55N

OL

ow8.

9618

.27

1070

.716

.99

-10.

227

262.

9820

2-M

2-D

ecan

t #9

56N

OL

ow9.

1018

.39

1076

.615

.16

-10.

304

264.

7820

2-M

2-D

ecan

t #9

57N

OL

ow9.

2518

.50

1082

.413

.47

-10.

382

266.

5720

2-M

2-D

ecan

t #9

58N

OL

ow9.

3918

.62

1088

.111

.90

-10.

459

268.

3620

2-M

2-D

ecan

t #9

59N

OL

ow9.

5418

.73

1093

.710

.45

-10.

537

270.

1520

2-M

2-D

ecan

t #9

60N

OL

ow9.

6818

.84

1099

.29.

12-1

0.61

527

1.95

G-D

ecan

t #9

25N

O4.

6218

.60

745.

280

.63

-11.

037

209.

21G

-Dec

ant #

926

4.76

18.6

775

8.3

77.1

8-1

1.07

321

1.00

G-D

ecan

t #9

274.

9118

.73

771.

073

.80

-11.

109

212.

79G

-Dec

ant #

928

5.05

18.7

978

3.4

70.4

7-1

1.14

421

4.58

G-D

ecan

t #9

295.

2018

.86

795.

567

.21

-11.

180

216.

38G

-Dec

ant #

930

5.34

18.9

280

7.3

64.0

3-1

1.21

621

8.17

G-D

ecan

t #9

315.

4818

.99

818.

860

.90

-11.

252

219.

96G

-Dec

ant #

932

5.63

19.0

583

0.1

57.8

5-1

1.28

722

1.75

G-D

ecan

t #9

335.

7719

.11

841.

154

.87

-11.

323

223.

55G

-Dec

ant #

934

5.92

19.1

885

1.8

51.9

6-1

1.35

922

5.34

G-D

ecan

t #9

356.

0619

.24

862.

349

.12

-11.

395

227.

13

Imm

obil

izat

ion

Tec

hnol

ogy

Sect

ion

WSR

C-T

R-2

002-

0049

1Sa

vann

ah R

iver

Tec

hnol

ogy

Cen

ter

Rev

. 0W

estin

ghou

se S

avan

nah

Riv

er C

ompa

ny

271

G-D

ecan

t #9

366.

2119

.31

872.

546

.37

-11.

430

228.

93G

-Dec

ant #

937

6.35

19.3

788

2.6

43.6

9-1

1.46

623

0.72

G-D

ecan

t #9

386.

5019

.43

892.

441

.09

-11.

502

232.

51G

-Dec

ant #

939

6.64

19.5

090

2.0

38.5

7-1

1.53

823

4.30

G-D

ecan

t #9

406.

7919

.56

911.

436

.13

-11.

574

236.

09G

-Dec

ant #

941

6.93

19.6

392

0.5

33.7

7-1

1.60

923

7.89

G-D

ecan

t #9

427.

0819

.69

929.

531

.50

-11.

645

239.

68G

-Dec

ant #

943

7.22

19.7

593

8.3

29.3

1-1

1.68

124

1.47

G-D

ecan

t #9

447.

3719

.82

947.

027

.21

-11.

717

243.

26G

-Dec

ant #

945

7.51

19.8

895

5.5

25.1

9-1

1.75

224

5.06

G-D

ecan

t #9

46L

ow7.

6519

.95

963.

823

.26

-11.

788

246.

85G

-Dec

ant #

947

Low

7.80

20.0

197

1.9

21.4

1-1

1.82

424

8.64

G-D

ecan

t #9

48L

ow7.

9420

.07

979.

919

.65

-11.

860

250.

44G

-Dec

ant #

949

Low

8.09

20.1

498

7.7

17.9

8-1

1.89

525

2.23

G-D

ecan

t #9

50L

ow8.

2320

.20

995.

416

.40

-11.

931

254.

02G

-Dec

ant #

951

Low

8.38

20.2

710

02.9

14.9

0-1

1.96

725

5.81

G-D

ecan

t #9

52L

ow8.

5220

.33

1010

.313

.48

-12.

003

257.

61G

-Dec

ant #

953

Low

8.67

20.4

010

17.6

12.1

6-1

2.03

825

9.40

G-D

ecan

t #9

54N

OL

ow8.

8120

.46

1024

.710

.91

-12.

074

261.

19G

-Dec

ant #

955

NO

Low

8.96

20.5

210

31.7

9.75

-12.

110

262.

98G

-Dec

ant #

956

NO

Low

9.10

20.5

910

38.6

8.67

-12.

146

264.

78G

-Dec

ant #

957

NO

Low

9.25

20.6

510

45.3

7.67

-12.

181

266.

57G

-Dec

ant #

958

NO

Low

9.39

20.7

210

52.0

6.75

-12.

217

268.

36G

-Dec

ant #

959

NO

Low

9.54

20.7

810

58.5

5.90

-12.

253

270.

15G

-Dec

ant #

960

NO

Low

9.68

20.8

410

64.9

5.13

-12.

289

271.

95U

-Dec

ant #

925

Hig

hN

O3.

8714

.10

801.

912

6.86

-6.9

8920

6.17

U-D

ecan

t #9

26H

igh

NO

4.02

14.2

381

5.4

121.

86-7

.079

208.

01U

-Dec

ant #

927

Hig

hN

O4.

1814

.35

828.

411

6.94

-7.1

6820

9.84

U-D

ecan

t #9

28H

igh

4.33

14.4

784

1.0

112.

09-7

.258

211.

67U

-Dec

ant #

929

Hig

h4.

4914

.60

853.

210

7.33

-7.3

4821

3.51

U-D

ecan

t #9

30H

igh

4.64

14.7

286

5.0

102.

63-7

.438

215.

34U

-Dec

ant #

931

4.79

14.8

587

6.4

98.0

2-7

.528

217.

17U

-Dec

ant #

932

4.95

14.9

788

7.5

93.5

0-7

.617

219.

00U

-Dec

ant #

933

5.10

15.0

989

8.3

89.0

7-7

.707

220.

84

Imm

obil

izat

ion

Tec

hnol

ogy

Sect

ion

WSR

C-T

R-2

002-

0049

1Sa

vann

ah R

iver

Tec

hnol

ogy

Cen

ter

Rev

. 0W

estin

ghou

se S

avan

nah

Riv

er C

ompa

ny

272

U-D

ecan

t #9

345.

2615

.22

908.

784

.72

-7.7

9722

2.67

U-D

ecan

t #9

355.

4115

.34

918.

880

.46

-7.8

8622

4.50

U-D

ecan

t #9

365.

5715

.47

928.

776

.30

-7.9

7622

6.34

U-D

ecan

t #9

375.

7215

.59

938.

372

.24

-8.0

6622

8.17

U-D

ecan

t #9

385.

8815

.71

947.

668

.28

-8.1

5523

0.00

U-D

ecan

t #9

396.

0315

.84

956.

664

.42

-8.2

4523

1.83

U-D

ecan

t #9

406.

1915

.96

965.

560

.66

-8.3

3523

3.67

U-D

ecan

t #9

416.

3416

.09

974.

057

.02

-8.4

2523

5.50

U-D

ecan

t #9

426.

5016

.21

982.

453

.48

-8.5

1423

7.33

U-D

ecan

t #9

436.

6516

.33

990.

550

.05

-8.6

0423

9.17

U-D

ecan

t #9

446.

8116

.46

998.

546

.73

-8.6

9424

1.00

U-D

ecan

t #9

456.

9616

.58

1006

.243

.54

-8.7

8424

2.83

U-D

ecan

t #9

467.

1116

.71

1013

.740

.45

-8.8

7324

4.67

U-D

ecan

t #9

47N

O7.

2716

.83

1021

.137

.49

-8.9

6324

6.50

U-D

ecan

t #9

48N

O7.

4216

.95

1028

.334

.64

-9.0

5324

8.33

U-D

ecan

t #9

49N

O7.

5817

.08

1035

.331

.92

-9.1

4325

0.17

U-D

ecan

t #9

50N

O7.

7317

.20

1042

.229

.32

-9.2

3225

2.00

U-D

ecan

t #9

51N

O7.

8917

.33

1048

.826

.84

-9.3

2225

3.83

U-D

ecan

t #9

52N

OL

ow8.

0417

.45

1055

.324

.49

-9.4

1225

5.67

U-D

ecan

t #9

53N

OL

ow8.

2017

.58

1061

.822

.26

-9.5

0225

7.50

U-D

ecan

t #9

54N

OL

ow8.

3517

.70

1068

.020

.15

-9.5

9125

9.33

U-D

ecan

t #9

55N

OL

ow8.

5117

.82

1074

.118

.16

-9.6

8126

1.16

U-D

ecan

t #9

56N

OL

ow8.

6617

.95

1080

.116

.30

-9.7

7126

3.00

U-D

ecan

t #9

57N

OL

ow8.

8218

.07

1085

.914

.56

-9.8

6026

4.83

U-D

ecan

t #9

58N

OL

ow8.

9718

.20

1091

.612

.94

-9.9

5026

6.66

U-D

ecan

t #9

59N

OL

ow9.

1318

.32

1097

.211

.43

-10.

040

268.

49U

-Dec

ant #

960

NO

Low

9.28

18.4

411

02.7

10.0

5-1

0.13

027

0.33

U2-

Dec

ant #

925

Hig

hN

O3.

8714

.10

804.

110

9.77

-7.3

1520

6.17

U2-

Dec

ant #

926

Hig

hN

O4.

0214

.23

817.

610

5.35

-7.4

0020

8.01

U2-

Dec

ant #

927

Hig

hN

O4.

1814

.35

830.

610

1.00

-7.4

8620

9.84

U2-

Dec

ant #

928

4.33

14.4

784

3.2

96.7

2-7

.571

211.

67U

2-D

ecan

t #9

294.

4914

.60

855.

492

.51

-7.6

5621

3.51

U2-

Dec

ant #

930

4.64

14.7

286

7.1

88.3

7-7

.742

215.

34U

2-D

ecan

t #9

314.

7914

.85

878.

584

.31

-7.8

2721

7.17

Imm

obil

izat

ion

Tec

hnol

ogy

Sect

ion

WSR

C-T

R-2

002-

0049

1Sa

vann

ah R

iver

Tec

hnol

ogy

Cen

ter

Rev

. 0W

estin

ghou

se S

avan

nah

Riv

er C

ompa

ny

273

U2-

Dec

ant #

932

4.95

14.9

788

9.6

80.3

3-7

.912

219.

00U

2-D

ecan

t #9

335.

1015

.09

900.

376

.43

-7.9

9822

0.84

U2-

Dec

ant #

934

5.26

15.2

291

0.8

72.6

2-8

.083

222.

67U

2-D

ecan

t #9

355.

4115

.34

920.

968

.89

-8.1

6922

4.50

U2-

Dec

ant #

936

5.57

15.4

793

0.7

65.2

4-8

.254

226.

34U

2-D

ecan

t #9

375.

7215

.59

940.

261

.69

-8.3

4022

8.17

U2-

Dec

ant #

938

5.88

15.7

194

9.5

58.2

3-8

.425

230.

00U

2-D

ecan

t #9

396.

0315

.84

958.

554

.87

-8.5

1023

1.84

U2-

Dec

ant #

940

6.19

15.9

696

7.4

51.5

9-8

.596

233.

67U

2-D

ecan

t #9

416.

3416

.09

975.

948

.42

-8.6

8123

5.50

U2-

Dec

ant #

942

6.50

16.2

198

4.2

45.3

5-8

.766

237.

33U

2-D

ecan

t #9

436.

6516

.33

992.

342

.38

-8.8

5223

9.17

U2-

Dec

ant #

944

6.81

16.4

610

00.2

39.5

1-8

.937

241.

00U

2-D

ecan

t #9

456.

9616

.58

1008

.036

.74

-9.0

2224

2.83

U2-

Dec

ant #

946

7.11

16.7

110

15.4

34.0

8-9

.108

244.

67U

2-D

ecan

t #9

47N

O7.

2716

.83

1022

.831

.53

-9.1

9324

6.50

U2-

Dec

ant #

948

NO

7.42

16.9

510

29.9

29.0

8-9

.279

248.

33U

2-D

ecan

t #9

49N

O7.

5817

.08

1036

.926

.75

-9.3

6425

0.17

U2-

Dec

ant #

950

NO

Low

7.73

17.2

010

43.8

24.5

2-9

.450

252.

00U

2-D

ecan

t #9

51N

OL

ow7.

8917

.33

1050

.422

.40

-9.5

3525

3.83

U2-

Dec

ant #

952

NO

Low

8.04

17.4

510

56.9

20.4

0-9

.620

255.

67U

2-D

ecan

t #9

53N

OL

ow8.

2017

.58

1063

.218

.50

-9.7

0625

7.50

U2-

Dec

ant #

954

NO

Low

8.35

17.7

010

69.5

16.7

1-9

.791

259.

33U

2-D

ecan

t #9

55N

OL

ow8.

5117

.82

1075

.515

.03

-9.8

7726

1.16

U2-

Dec

ant #

956

NO

Low

8.66

17.9

510

81.4

13.4

5-9

.962

263.

00U

2-D

ecan

t #9

57N

OL

ow8.

8218

.07

1087

.211

.98

-10.

047

264.

83U

2-D

ecan

t #9

58N

OL

ow8.

9718

.20

1092

.910

.62

-10.

133

266.

66U

2-D

ecan

t #9

59N

OL

ow9.

1318

.32

1098

.59.

36-1

0.21

826

8.49

U2-

Dec

ant #

960

NO

Low

9.28

18.4

411

03.9

8.20

-10.

304

270.

33

Date post:	28-Sep-2020
Category:	Documents
Upload:	others
View:	0 times
Download:	0 times

Frit Development for Sludge Batch 3/67531/metadc737483/m2/1/high_re… · CPC Chemical Process Cell...

Documents