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GHz SAW and FBAR devices manufactured using micromachining and nanoprocessing … · 2008-03-21 ·...

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GHz SAW and FBAR devices manufactured using micromachining and nanoprocessing of wide band gap semiconductors A.Müller*, D. Neculoiu*, A Dinescu*, C. Morosanu***, G. Konstantinidis**, D Vasilache*, M Dragoman* G. Sajin* *IMT-Bucharest, Romania, [email protected] ** FORTH IESL Heraklion, Crete, Greece;, *** National Institute of Material Physics (NIMP); Bucharest, Romania
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Page 1: GHz SAW and FBAR devices manufactured using micromachining and nanoprocessing … · 2008-03-21 · •The classical technologies for manufacturing SAW type resonators and filters

GHz SAW and FBAR devices manufactured using micromachining and

nanoprocessing of wide band gap semiconductors

A.Müller*, D. Neculoiu*, A Dinescu*, C. Morosanu***, G. Konstantinidis**, D Vasilache*, M Dragoman* G.

Sajin*

*IMT-Bucharest, Romania, [email protected]** FORTH IESL Heraklion, Crete, Greece;,

*** National Institute of Material Physics (NIMP); Bucharest, Romania

Page 2: GHz SAW and FBAR devices manufactured using micromachining and nanoprocessing … · 2008-03-21 · •The classical technologies for manufacturing SAW type resonators and filters

FBAR/SAW

d= membrane thickness

d= λ/2= vs/2fr (resonance)

fr= vs/2d

FBARs and SAWs resonate at their acoustic natural frequency (GHz range) not at their structural natural frequency (in the kHz range)

w=digit width= interdigit width 2w=λ/2=vs/2fr

fr=vs/4w;

vs~km/s; d~μm ; fr~GHz

Page 3: GHz SAW and FBAR devices manufactured using micromachining and nanoprocessing … · 2008-03-21 · •The classical technologies for manufacturing SAW type resonators and filters

Expected frequency responses for piezo and non-piezo materials

•All acoustic devices operate at resonance•Resonance occurs when the input impedance is at a minimum and anti-resonance occurs when it is at a maximum. The resonant frequency and the anti-resonant frequency are referred to as the series frequency and the parallel frequency respectively•A series resonant circuit allows a maximum current flow at resonant frequency, whereas a parallel resonant circuit allows a minimum

. At these frequencies the response is completely real and does not have an imaginary component.

Page 4: GHz SAW and FBAR devices manufactured using micromachining and nanoprocessing … · 2008-03-21 · •The classical technologies for manufacturing SAW type resonators and filters

•The classical technologies for manufacturing SAW type resonators and filters based on non-semiconductor materials like quartz, lithium niobate or lithium tantalate,are restricted to frequencies below 1 GHz

•Most FBAR structures reported in the last years were manufactured on ZnO a semiconductor incompatible with monolithic integration

AlN and GaN technology create the possibily of manufacturing of GHz frequencies operating acoustic devices monolithic integrable with other circuit elements

•In GHz SAW technology nanolithography for the IDT is necessary

•For FBAR structures it is necessary to develop very thin selfsustainable membranes

Page 5: GHz SAW and FBAR devices manufactured using micromachining and nanoprocessing … · 2008-03-21 · •The classical technologies for manufacturing SAW type resonators and filters

WHY TO INCREASE THE FREQUENCY?•The cellular phone system is evolving from a third generation (3G) system to a fourth generation (4G) system. The radio frequency of 4G systems is expected to be within the high-frequency range from 3 GHz to 6 GHz.

•Sensors based on SAW and FBAR structures have a sensitivity: S α f2

•WBG semiconductor (AlN, GaN) technology opened the possibility to use micromachining and nanoprocessing and to increase SAW and FBARoperating frequency

•AlN and GaN create the possibility to integrate monolithic the SAW and FBAR resonators with other circuit elements

Page 6: GHz SAW and FBAR devices manufactured using micromachining and nanoprocessing … · 2008-03-21 · •The classical technologies for manufacturing SAW type resonators and filters

SAW structures manufactured using nanolithographictechniques

The structures were manufactured on AlN thin films deposited by magnetron sputtering on high resistivity silicon

XRD diffraction pattern for a high oriented AlNfilm sputtered onto a <100> oriented Si substrate

Page 7: GHz SAW and FBAR devices manufactured using micromachining and nanoprocessing … · 2008-03-21 · •The classical technologies for manufacturing SAW type resonators and filters

First run

The idea of the experiment

Each IDT structure has 30 digits and 29 inter-digits. The digits and inter-digits have a length of 200μm, and an equal width of 200 nm for one type of test structures and 300nm for the other type.

Page 8: GHz SAW and FBAR devices manufactured using micromachining and nanoprocessing … · 2008-03-21 · •The classical technologies for manufacturing SAW type resonators and filters

The first step in the SAW structure manufacturing was the measurement pads patterning and deposition. Conventional photolithography, e-beam metalization (Ti/Au 20nm/200nm) and lift-off technique was used ( FORTH).

Due to the digits/interdigits dimensions, a direct writing process was used, for the IDT structure. The design transfer on the wafer was performed using a Scanning Electron Microscope (Vega from Tescan), equipped with an Electron Beam Lithography system (Elphy Plus from Raith) ( IMT).

Finally, Ti/Au (20/nm/200nm) is deposited by e beam and a lift-off process, is used to remove the unwanted metal (FORTH).

Page 9: GHz SAW and FBAR devices manufactured using micromachining and nanoprocessing … · 2008-03-21 · •The classical technologies for manufacturing SAW type resonators and filters

300nm lines in PMMA

A SAW structure with an IDT having metalic fingers and pitches of 300nm

Page 10: GHz SAW and FBAR devices manufactured using micromachining and nanoprocessing … · 2008-03-21 · •The classical technologies for manufacturing SAW type resonators and filters

Measurement results

Smith chart representation of the SAW resonator input

impedance (detail)

The resistance and the conductance of the SAW

resonator

Page 11: GHz SAW and FBAR devices manufactured using micromachining and nanoprocessing … · 2008-03-21 · •The classical technologies for manufacturing SAW type resonators and filters

fs = 2.7847 GHz and fp = 2.7879 GHz. The resulting acoustic velocity of the surface waves of 3.336 ms-1

is lower than the values reported in the literature [8] because of the wave interaction with rather thick metallic electrode.

The effective coupling coefficient is defined as:

From (2), the effective coupling coefficient, K2eff, has

a value of about 0.283 %. This value is closed to 0.25 % reported by other authors.

p

sp

p

seff f

ffffK

−=

4

22 π

Page 12: GHz SAW and FBAR devices manufactured using micromachining and nanoprocessing … · 2008-03-21 · •The classical technologies for manufacturing SAW type resonators and filters

Typical defects appeared in the 300 nm metallic lines of the IDT(a) disappearance of some lines and incomplete lift-off (b).

a b

Page 13: GHz SAW and FBAR devices manufactured using micromachining and nanoprocessing … · 2008-03-21 · •The classical technologies for manufacturing SAW type resonators and filters

The second run

Page 14: GHz SAW and FBAR devices manufactured using micromachining and nanoprocessing … · 2008-03-21 · •The classical technologies for manufacturing SAW type resonators and filters

SAW structure (W=300nm)

Page 15: GHz SAW and FBAR devices manufactured using micromachining and nanoprocessing … · 2008-03-21 · •The classical technologies for manufacturing SAW type resonators and filters

SAW structure (W=250nm)

Page 16: GHz SAW and FBAR devices manufactured using micromachining and nanoprocessing … · 2008-03-21 · •The classical technologies for manufacturing SAW type resonators and filters

SAW structure detail (w=150nm)

Page 17: GHz SAW and FBAR devices manufactured using micromachining and nanoprocessing … · 2008-03-21 · •The classical technologies for manufacturing SAW type resonators and filters

SAW - AlN 0.5 µm thick; 150 nm

2.6 2.9 3.1 3.4 3.6 3.9 4.1 4.2Frequency (GHz)

s21

-70

-65

-60

-55

-50

-45

-403.231 GHz-47.85 dB

DB(|S(2,1)|)8 a 150

DB(|S(2,1)|)8 c 150

2.6 2.9 3.1 3.4 3.6 3.9 4.1 4.2Frequency (GHz)

s11

-0.2

-0.15

-0.1

-0.05

0

DB(|S(1,1)|)8 a 150

DB(|S(1,1)|)8 c 150

Page 18: GHz SAW and FBAR devices manufactured using micromachining and nanoprocessing … · 2008-03-21 · •The classical technologies for manufacturing SAW type resonators and filters

Series connection of SAWs (detail) (w=300nm)

Page 19: GHz SAW and FBAR devices manufactured using micromachining and nanoprocessing … · 2008-03-21 · •The classical technologies for manufacturing SAW type resonators and filters

SAW - series connection (AlN 0.5 µm thick)

2.6 2.8 3 3.2 3.4 3.6 3.8 4 4.2Frequency (GHz)

SAW series connection

-1.6

-1.4

-1.2

-1

-0.8

-0.6

-11

-10

-9

-8

-7

-6

DB(|S(1,1)|) (L)serie 1 2

DB(|S(2,1)|) (R)serie 1 2

5.8 6 6.2 6.4 6.6 6.8 7 7.2 7.4Frequency (GHz)

SAW series connection

-3.6

-3.4

-3.2

-3

-2.8

-2.6

-2.4

-5

-4.75

-4.5

-4.25

-4

-3.75

-3.5DB(|S(1,1)|) (L)serie 1 4

DB(|S(2,1)|) (R)serie 1 4

6.487 GHzr 0.685516x -1.50271

0

-3.0

4.0

2.784 GHzr 0.881734x -3.63587

Page 20: GHz SAW and FBAR devices manufactured using micromachining and nanoprocessing … · 2008-03-21 · •The classical technologies for manufacturing SAW type resonators and filters

1.The GaN on silicon structure was grown by MOCVD

•The first AlN layer has a buffer function •The inter-layers (10 nm thick) are used in order to minimise the thermal stress and avoid the cracking of the GaN layers. •The Fe doping allows to compensate the native doping in GaN layers

GaN membrane layer ~ 2.2μm

FBAR structurswere fabricated on GaN and AlN

2. The AlN on silicon was deposited by magnetron sputtering The thickness was 2 µm and 0.357 µm

Page 21: GHz SAW and FBAR devices manufactured using micromachining and nanoprocessing … · 2008-03-21 · •The classical technologies for manufacturing SAW type resonators and filters

• Conventional contact lithography, e-gun Ti/Au (10nm/200nm) evaporation (top). • Lift-off techniques to define the FBAR structures on the top. • Backside lapping of the wafer to a thickness of about 150μm.• Al layer deposition (400nm) on the bottom (as mask during the RIE of silicon). • Backside patterning for the membrane formation.• Backside RIE of silicon down to the thin AlN layer using SF6 plasma. • Sputtering of 250 nm thin gold layer on the bottom of the wafer.

Cross section of the FBAR structure with the evaporated Ti/Au for the top metallization

and sputtered Au for the bottom contact. Sputtered Al is used as mask for the bulk-

micromachining of the membrane

Main technological flow steps

Page 22: GHz SAW and FBAR devices manufactured using micromachining and nanoprocessing … · 2008-03-21 · •The classical technologies for manufacturing SAW type resonators and filters

GaN membrane supported series connection of two FBAR structures (test structures)

Page 23: GHz SAW and FBAR devices manufactured using micromachining and nanoprocessing … · 2008-03-21 · •The classical technologies for manufacturing SAW type resonators and filters

GaN membrane FBAR W=2.2μm

Page 24: GHz SAW and FBAR devices manufactured using micromachining and nanoprocessing … · 2008-03-21 · •The classical technologies for manufacturing SAW type resonators and filters

0.5 1.5 2.5 3.5 4.5Frequency (GHz)

p

-16

-12

-8

-4

0

DB(|S(1,1)|)FBAR

DB(|S(2,1)|)FBAR

1 1.2 1.4 1.6 1.8 2

Frequency (GHz)

0

5

10

15

20

25

30

Res

ista

nce

[ohm

]

0

0.00833

0.0167

0.025

0.0333

0.0417

0.05

Con

duct

ance

[S]1.536 GHz

27.45 Ohm

1.5 GHz0.04131 S

Magnitude of the measures S parameters of the AlNbased FBAR 300 μm test

structure

AlN membrane FBAR

(w=2μm)

The resistance and the conductance of the two FBARsstructures connected in series

Page 25: GHz SAW and FBAR devices manufactured using micromachining and nanoprocessing … · 2008-03-21 · •The classical technologies for manufacturing SAW type resonators and filters

FBAR series connection (AlN membrane W= 0.357 µm)

6 7 8 9 10 11 12Frequency (GHz)

AlN FBAR 0.357 um

-25

-20

-15

-10

-5

0

-2.5

-2.1

-1.7

-1.3

-0.9

-0.5

DB(|S(1,1)|) (L)e0f

DB(|S(2,1)|) (R)e0f

DB(|S(1,1)|) (L)e6f

DB(|S(2,1)|) (R)e6f

Page 26: GHz SAW and FBAR devices manufactured using micromachining and nanoprocessing … · 2008-03-21 · •The classical technologies for manufacturing SAW type resonators and filters

Work in progress: •700nm thin membrane supported FBAR structure based on GaN micromachining

•50nm thin Mo metallization

Before membrane

manufacturingFinal structures

Page 27: GHz SAW and FBAR devices manufactured using micromachining and nanoprocessing … · 2008-03-21 · •The classical technologies for manufacturing SAW type resonators and filters

Best results obtained up to now

SAW device operating in the 5 GHz range, based on AlN/diamond, obtained with electronic lithography was reported [P. Kirsch et all. Appl Phys. Lett.88, 223504, 2006].

FBAR structure with operating frequency in the 5 GHz range, based on AlN, was reported [K-W Tay et al, Japanese J. of Appl. Phys. No. 3, 2004, p. 1122].

Page 28: GHz SAW and FBAR devices manufactured using micromachining and nanoprocessing … · 2008-03-21 · •The classical technologies for manufacturing SAW type resonators and filters

An emerging application of GaN FBARs - sensing of poison gases in harsh environmetal (1)

Sensitivity α f2

Page 29: GHz SAW and FBAR devices manufactured using micromachining and nanoprocessing … · 2008-03-21 · •The classical technologies for manufacturing SAW type resonators and filters

An emerging application of GaN FBARs - sensing of poison gases in harsh environmetal (2) the device

can be monolithic integrated with a HEMT on GaN

Page 30: GHz SAW and FBAR devices manufactured using micromachining and nanoprocessing … · 2008-03-21 · •The classical technologies for manufacturing SAW type resonators and filters

MSM GaN membrane structure for UV detection

Active area

(detail)

Contact pads

Membrane

Active area:20 fingers (10+10) 1µm wide;19 gaps (interdigits) 1µm wide;finger length 100 µm nontransparent metallization Ni/Au (20nm/100nm)

Page 31: GHz SAW and FBAR devices manufactured using micromachining and nanoprocessing … · 2008-03-21 · •The classical technologies for manufacturing SAW type resonators and filters

SEM photos of the 1 μm wide Ni/Au (20nm/100nm) lines The interdigit width was also about 1 μm

3200 3400 3600 3800 4000 4200

0.0

2.0x10-3

4.0x10-3

6.0x10-3

8.0x10-3

1.0x10-2

1.2x10-2

1.4x10-2

1.6x10-2

GaN substrate GaN Membrane

R(A

/W)

λ(A)

Page 32: GHz SAW and FBAR devices manufactured using micromachining and nanoprocessing … · 2008-03-21 · •The classical technologies for manufacturing SAW type resonators and filters

.

300 320 340 360 380 400

0.0

0.5

1.0

1.5

2.0

2.5

3.0

3.5

4.0

6V 10V 15V 20V

R(A

/W)

λ(nm)

membrane d3

-15 -10 -5 0 5 10 1510-13

10-12

10-11

1x10-10

1x10-9

1x10-8

1x10-7

d3C

urre

nt (A

)

Voltage (V)

first measurement second measurement third measuement fourth measurement

Page 33: GHz SAW and FBAR devices manufactured using micromachining and nanoprocessing … · 2008-03-21 · •The classical technologies for manufacturing SAW type resonators and filters

-16 -14 -12 -10 -8 -6 -4 -2 0 2 4 6 8 10 12 14 1610-13

10-12

10-11

1x10-10

1x10-9

sample2

first measurement second measurement third measuement

Cur

rent

(A)

Voltage (V)

0.45µm fingers and pitches GaN membrane MSM UV photodetector- work in progress

Page 34: GHz SAW and FBAR devices manufactured using micromachining and nanoprocessing … · 2008-03-21 · •The classical technologies for manufacturing SAW type resonators and filters

Conclusions

Micromachining and nanolithography can substantially improve:

- the frequency performances of acoustic devices on WBG semiconductors

-WBG SAW and FBAR based sensors performances

-performances of UV photodetectors

-


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