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Hazardous... · Client Sample ID: PCB-101 Lab Sample ID: 720-78005-2 PCB-1248 RL 700 ug/Kg Analyte...

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ANALYTICAL REPORTTestAmerica Laboratories, Inc.TestAmerica Pleasanton1220 Quarry LanePleasanton, CA 94566Tel: (925)484-1919

TestAmerica Job ID: 720-78005-1Client Project/Site: EVC/ROBLE

For:Ninyo & Moore1956 Webster StreetSuite 400Oakland, California 94612

Attn: Bill Larkin

Authorized for release by:3/10/2017 11:19:54 AMDimple Sharma, Senior Project [email protected]

Designee for

Paloma Duong, Project Manager I(925)[email protected]

This report has been electronically signed and authorized by the signatory. Electronic signature isintended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

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Table of Contents

Client: Ninyo & MooreProject/Site: EVC/ROBLE

TestAmerica Job ID: 720-78005-1

Page 2 of 19TestAmerica Pleasanton

3/10/2017

Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1

Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2

Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3

Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4

Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5

Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6

Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11

QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12

QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13

Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14

Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15

Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16

Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17

Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 18

Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19

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Definitions/GlossaryTestAmerica Job ID: 720-78005-1Client: Ninyo & Moore

Project/Site: EVC/ROBLE

Qualifiers

GC Semi VOA

Qualifier Description

D Surrogate or matrix spike recoveries were not obtained because the extract was diluted for analysis; also compounds analyzed at a

dilution may be flagged with a D.

Qualifier

X Surrogate is outside control limits

F1 MS and/or MSD Recovery is outside acceptance limits.

Glossary

These commonly used abbreviations may or may not be present in this report.

¤ Listed under the "D" column to designate that the result is reported on a dry weight basis

Abbreviation

%R Percent Recovery

CFL Contains Free Liquid

CNF Contains no Free Liquid

DER Duplicate error ratio (normalized absolute difference)

Dil Fac Dilution Factor

DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample

DLC Decision level concentration

MDA Minimum detectable activity

EDL Estimated Detection Limit

MDC Minimum detectable concentration

MDL Method Detection Limit

ML Minimum Level (Dioxin)

NC Not Calculated

ND Not detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit

QC Quality Control

RER Relative error ratio

RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points

TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)

TestAmerica Pleasanton

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Case NarrativeClient: Ninyo & Moore TestAmerica Job ID: 720-78005-1Project/Site: EVC/ROBLE

Job ID: 720-78005-1

Laboratory: TestAmerica Pleasanton

Narrative

Job Narrative720-78005-1

Comments

No additional comments.

Receipt

The samples were received on 3/2/2017 3:30 PM; the samples arrived in good condition, properly preserved and, where required, on ice.

The temperature of the cooler at receipt was 2.3º C.

GC Semi VOA Method 8082: The following samples required a tetrabutylammonium sulfite (TBA) clean-up to reduce matrix interferences caused by

sulfur: PCB-100 (720-78005-1), PCB-101 (720-78005-2), (LCS 720-218954/2-A) and (MB 720-218954/1-A), PCB-102 (720-78005-3),

PCB-104 (720-78005-5), (720-78005-A-5-A MS) and (720-78005-A-5-B MSD).

Method 8082: The following sample contained more than one Aroclor with insufficient separation to quantify individually. The PCBs present are quantified as the predominant Aroclor: PCB-101 (720-78005-2).

Method 8082: The following sample contained more than one Aroclor with insufficient separation to quantify individually. The PCBs present are quantified as the predominant Aroclor: PCB-103 (720-78005-4).

Method 8082: The following sample was diluted due to the abundance of non-target analytes: PCB-102 (720-78005-3) and PCB-104 (720-78005-5). Elevated reporting limits (RLs) are provided.

Method 8082: The following samples required a dilution due to the nature of the sample matrix: PCB-102 (720-78005-3), PCB-104 (720-78005-5), (720-78005-A-5-A MS) and (720-78005-A-5-B MSD). Because of this dilution, the surrogate spike concentration in the sample was reduced to a level where the recovery calculation does not provide useful information.

Method 8082: The following sample appears to contain polychlorinated biphenyls (PCBs); however, due to weathering or other environmental processes, the PCBs in the sample do not closely match any of the laboratory's Aroclor standards used for instrument calibration: PCB-101 (720-78005-2). The sample has been quantified and reported as Aroclor 1248. Due to the poor match with the Aroclor standard, there is increased qualitative and quantitative uncertainty associated with this result.

Method 8082: The following sample appears to contain polychlorinated biphenyls (PCBs); however, due to weathering or other environmental processes, the PCBs in the sample do not closely match any of the laboratory's Aroclor standards used for instrument

calibration: PCB-103 (720-78005-4). The sample has been quantified and reported as Aroclor 1248. Due to the poor match with the Aroclor standard, there is increased qualitative and quantitative uncertainty associated with this result.

No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

Organic Prep

No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.

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Detection SummaryTestAmerica Job ID: 720-78005-1Client: Ninyo & Moore

Project/Site: EVC/ROBLE

Client Sample ID: PCB-100 Lab Sample ID: 720-78005-1

No Detections.

Client Sample ID: PCB-101 Lab Sample ID: 720-78005-2

PCB-1248

RL

700 ug/Kg

MDLAnalyte Result Qualifier Unit Dil Fac D Method Prep Type

Total/NA1980 8082

Client Sample ID: PCB-102 Lab Sample ID: 720-78005-3

No Detections.

Client Sample ID: PCB-103 Lab Sample ID: 720-78005-4

PCB-1248

RL

680 ug/Kg

MDLAnalyte Result Qualifier Unit Dil Fac D Method Prep Type

Total/NA11100 8082

Client Sample ID: PCB-104 Lab Sample ID: 720-78005-5

No Detections.

TestAmerica Pleasanton

This Detection Summary does not include radiochemical test results.

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Client Sample ResultsTestAmerica Job ID: 720-78005-1Client: Ninyo & Moore

Project/Site: EVC/ROBLE

Lab Sample ID: 720-78005-1Client Sample ID: PCB-100Matrix: SolidDate Collected: 03/01/17 00:00

Date Received: 03/02/17 15:30

Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas ChromatographyRL MDL

PCB-1016 ND 680 ug/Kg 03/08/17 14:25 03/08/17 23:48 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

680 ug/Kg 03/08/17 14:25 03/08/17 23:48 1PCB-1221 ND

680 ug/Kg 03/08/17 14:25 03/08/17 23:48 1PCB-1232 ND

680 ug/Kg 03/08/17 14:25 03/08/17 23:48 1PCB-1242 ND

680 ug/Kg 03/08/17 14:25 03/08/17 23:48 1PCB-1248 ND

680 ug/Kg 03/08/17 14:25 03/08/17 23:48 1PCB-1254 ND

680 ug/Kg 03/08/17 14:25 03/08/17 23:48 1PCB-1260 ND

Tetrachloro-m-xylene 79 32 - 112 03/08/17 14:25 03/08/17 23:48 1

Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery

DCB Decachlorobiphenyl 74 03/08/17 14:25 03/08/17 23:48 12 - 122

TestAmerica Pleasanton

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Client Sample ResultsTestAmerica Job ID: 720-78005-1Client: Ninyo & Moore

Project/Site: EVC/ROBLE

Lab Sample ID: 720-78005-2Client Sample ID: PCB-101Matrix: SolidDate Collected: 03/01/17 00:00

Date Received: 03/02/17 15:30

Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas ChromatographyRL MDL

PCB-1016 ND 700 ug/Kg 03/08/17 14:25 03/09/17 00:04 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

700 ug/Kg 03/08/17 14:25 03/09/17 00:04 1PCB-1221 ND

700 ug/Kg 03/08/17 14:25 03/09/17 00:04 1PCB-1232 ND

700 ug/Kg 03/08/17 14:25 03/09/17 00:04 1PCB-1242 ND

700 ug/Kg 03/08/17 14:25 03/09/17 00:04 1PCB-1248 980

700 ug/Kg 03/08/17 14:25 03/09/17 00:04 1PCB-1254 ND

700 ug/Kg 03/08/17 14:25 03/09/17 00:04 1PCB-1260 ND

Tetrachloro-m-xylene 83 32 - 112 03/08/17 14:25 03/09/17 00:04 1

Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery

DCB Decachlorobiphenyl 103 03/08/17 14:25 03/09/17 00:04 12 - 122

TestAmerica Pleasanton

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Client Sample ResultsTestAmerica Job ID: 720-78005-1Client: Ninyo & Moore

Project/Site: EVC/ROBLE

Lab Sample ID: 720-78005-3Client Sample ID: PCB-102Matrix: SolidDate Collected: 03/01/17 00:00

Date Received: 03/02/17 15:30

Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas ChromatographyRL MDL

PCB-1016 ND 14000 ug/Kg 03/08/17 14:25 03/09/17 10:15 20

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

14000 ug/Kg 03/08/17 14:25 03/09/17 10:15 20PCB-1221 ND

14000 ug/Kg 03/08/17 14:25 03/09/17 10:15 20PCB-1232 ND

14000 ug/Kg 03/08/17 14:25 03/09/17 10:15 20PCB-1242 ND

14000 ug/Kg 03/08/17 14:25 03/09/17 10:15 20PCB-1248 ND

14000 ug/Kg 03/08/17 14:25 03/09/17 10:15 20PCB-1254 ND

14000 ug/Kg 03/08/17 14:25 03/09/17 10:15 20PCB-1260 ND

Tetrachloro-m-xylene 0 X D 32 - 112 03/08/17 14:25 03/09/17 10:15 20

Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery

DCB Decachlorobiphenyl 0 X D 03/08/17 14:25 03/09/17 10:15 202 - 122

TestAmerica Pleasanton

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Client Sample ResultsTestAmerica Job ID: 720-78005-1Client: Ninyo & Moore

Project/Site: EVC/ROBLE

Lab Sample ID: 720-78005-4Client Sample ID: PCB-103Matrix: SolidDate Collected: 03/01/17 00:00

Date Received: 03/02/17 15:30

Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas ChromatographyRL MDL

PCB-1016 ND 680 ug/Kg 03/08/17 14:25 03/09/17 11:15 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

680 ug/Kg 03/08/17 14:25 03/09/17 11:15 1PCB-1221 ND

680 ug/Kg 03/08/17 14:25 03/09/17 11:15 1PCB-1232 ND

680 ug/Kg 03/08/17 14:25 03/09/17 11:15 1PCB-1242 ND

680 ug/Kg 03/08/17 14:25 03/09/17 11:15 1PCB-1248 1100

680 ug/Kg 03/08/17 14:25 03/09/17 11:15 1PCB-1254 ND

680 ug/Kg 03/08/17 14:25 03/09/17 11:15 1PCB-1260 ND

Tetrachloro-m-xylene 85 32 - 112 03/08/17 14:25 03/09/17 11:15 1

Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery

DCB Decachlorobiphenyl 85 03/08/17 14:25 03/09/17 11:15 12 - 122

TestAmerica Pleasanton

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Client Sample ResultsTestAmerica Job ID: 720-78005-1Client: Ninyo & Moore

Project/Site: EVC/ROBLE

Lab Sample ID: 720-78005-5Client Sample ID: PCB-104Matrix: SolidDate Collected: 03/01/17 00:00

Date Received: 03/02/17 15:30

Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas ChromatographyRL MDL

PCB-1016 ND 37000 ug/Kg 03/08/17 14:25 03/09/17 11:15 50

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

37000 ug/Kg 03/08/17 14:25 03/09/17 11:15 50PCB-1221 ND

37000 ug/Kg 03/08/17 14:25 03/09/17 11:15 50PCB-1232 ND

37000 ug/Kg 03/08/17 14:25 03/09/17 11:15 50PCB-1242 ND

37000 ug/Kg 03/08/17 14:25 03/09/17 11:15 50PCB-1248 ND

37000 ug/Kg 03/08/17 14:25 03/09/17 11:15 50PCB-1254 ND

37000 ug/Kg 03/08/17 14:25 03/09/17 11:15 50PCB-1260 ND F1

Tetrachloro-m-xylene 0 D X 32 - 112 03/08/17 14:25 03/09/17 11:15 50

Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery

DCB Decachlorobiphenyl 0 D X 03/08/17 14:25 03/09/17 11:15 502 - 122

TestAmerica Pleasanton

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Surrogate SummaryTestAmerica Job ID: 720-78005-1Client: Ninyo & Moore

Project/Site: EVC/ROBLE

Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas ChromatographyPrep Type: Total/NAMatrix: Solid

Lab Sample ID Client Sample ID (32-112) (2-122)

TCX1 DCB1

79 74720-78005-1

Percent Surrogate Recovery (Acceptance Limits)

PCB-100

83 103720-78005-2 PCB-101

0 X D 0 X D720-78005-3 PCB-102

85 85720-78005-4 PCB-103

0 D X 0 D X720-78005-5 PCB-104

0 D X 0 D X720-78005-5 MS PCB-104

0 D X 0 D X720-78005-5 MSD PCB-104

54 88LCS 720-218954/2-A Lab Control Sample

45 84MB 720-218954/1-A Method Blank

Surrogate Legend

TCX = Tetrachloro-m-xylene

DCB = DCB Decachlorobiphenyl

TestAmerica Pleasanton

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QC Sample ResultsTestAmerica Job ID: 720-78005-1Client: Ninyo & Moore

Project/Site: EVC/ROBLE

Method: 8082 - Polychlorinated Biphenyls (PCBs) by Gas Chromatography

Client Sample ID: Method BlankLab Sample ID: MB 720-218954/1-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 218913 Prep Batch: 218954

RL MDL

PCB-1016 ND 50 ug/Kg 03/08/17 14:25 03/08/17 22:24 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

ND 50 ug/Kg 03/08/17 14:25 03/08/17 22:24 1PCB-1221

ND 50 ug/Kg 03/08/17 14:25 03/08/17 22:24 1PCB-1232

ND 50 ug/Kg 03/08/17 14:25 03/08/17 22:24 1PCB-1242

ND 50 ug/Kg 03/08/17 14:25 03/08/17 22:24 1PCB-1248

ND 50 ug/Kg 03/08/17 14:25 03/08/17 22:24 1PCB-1254

ND 50 ug/Kg 03/08/17 14:25 03/08/17 22:24 1PCB-1260

Tetrachloro-m-xylene 45 32 - 112 03/08/17 22:24 1

MB MB

Surrogate

03/08/17 14:25

Dil FacPrepared AnalyzedQualifier Limits%Recovery

84 03/08/17 14:25 03/08/17 22:24 1DCB Decachlorobiphenyl 2 - 122

Client Sample ID: Lab Control SampleLab Sample ID: LCS 720-218954/2-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 218913 Prep Batch: 218954

PCB-1016 133 87.1 ug/Kg 65 55 - 112

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

PCB-1260 133 110 ug/Kg 83 65 - 120

Tetrachloro-m-xylene 32 - 112

Surrogate

54

LCS LCS

Qualifier Limits%Recovery

88DCB Decachlorobiphenyl 2 - 122

Client Sample ID: PCB-104Lab Sample ID: 720-78005-5 MSMatrix: Solid Prep Type: Total/NAAnalysis Batch: 218998 Prep Batch: 218954

PCB-1016 ND 1920 ND ug/Kg NC 69 - 120

Analyte

MS MS

DUnitResult Qualifier %Rec

Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

PCB-1260 ND F1 1920 ND F1 ug/Kg 0 73 - 114

Tetrachloro-m-xylene D X 32 - 112

Surrogate

0

MS MS

Qualifier Limits%Recovery

0 D XDCB Decachlorobiphenyl 2 - 122

Client Sample ID: PCB-104Lab Sample ID: 720-78005-5 MSDMatrix: Solid Prep Type: Total/NAAnalysis Batch: 218998 Prep Batch: 218954

PCB-1016 ND 1900 ND ug/Kg NC 69 - 120 NC 20

Analyte

MSD MSD

DUnitResult Qualifier %Rec

Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

PCB-1260 ND F1 1900 ND F1 ug/Kg 0 73 - 114 NC 20

Tetrachloro-m-xylene D X 32 - 112

Surrogate

0

MSD MSD

Qualifier Limits%Recovery

0 D XDCB Decachlorobiphenyl 2 - 122

TestAmerica Pleasanton

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QC Association SummaryTestAmerica Job ID: 720-78005-1Client: Ninyo & Moore

Project/Site: EVC/ROBLE

GC Semi VOA

Analysis Batch: 218913

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid 8082 218954720-78005-1 PCB-100 Total/NA

Solid 8082 218954720-78005-2 PCB-101 Total/NA

Solid 8082 218954MB 720-218954/1-A Method Blank Total/NA

Solid 8082 218954LCS 720-218954/2-A Lab Control Sample Total/NA

Prep Batch: 218954

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid 3550B720-78005-1 PCB-100 Total/NA

Solid 3550B720-78005-2 PCB-101 Total/NA

Solid 3550B720-78005-3 PCB-102 Total/NA

Solid 3550B720-78005-4 PCB-103 Total/NA

Solid 3550B720-78005-5 PCB-104 Total/NA

Solid 3550BMB 720-218954/1-A Method Blank Total/NA

Solid 3550BLCS 720-218954/2-A Lab Control Sample Total/NA

Solid 3550B720-78005-5 MS PCB-104 Total/NA

Solid 3550B720-78005-5 MSD PCB-104 Total/NA

Analysis Batch: 218998

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid 8082 218954720-78005-3 PCB-102 Total/NA

Solid 8082 218954720-78005-5 PCB-104 Total/NA

Solid 8082 218954720-78005-5 MS PCB-104 Total/NA

Solid 8082 218954720-78005-5 MSD PCB-104 Total/NA

Analysis Batch: 218999

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid 8082 218954720-78005-4 PCB-103 Total/NA

TestAmerica Pleasanton

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Lab ChronicleClient: Ninyo & Moore TestAmerica Job ID: 720-78005-1Project/Site: EVC/ROBLE

Client Sample ID: PCB-100 Lab Sample ID: 720-78005-1Matrix: SolidDate Collected: 03/01/17 00:00

Date Received: 03/02/17 15:30

Prep 3550B 03/08/17 14:25 JEV218954 TAL PLS

Type

Batch Batch

MethodPrep Type LabAnalystRun

Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Analysis 8082 1 218913 03/08/17 23:48 DCH TAL PLSTotal/NA

Client Sample ID: PCB-101 Lab Sample ID: 720-78005-2Matrix: SolidDate Collected: 03/01/17 00:00

Date Received: 03/02/17 15:30

Prep 3550B 03/08/17 14:25 JEV218954 TAL PLS

Type

Batch Batch

MethodPrep Type LabAnalystRun

Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Analysis 8082 1 218913 03/09/17 00:04 DCH TAL PLSTotal/NA

Client Sample ID: PCB-102 Lab Sample ID: 720-78005-3Matrix: SolidDate Collected: 03/01/17 00:00

Date Received: 03/02/17 15:30

Prep 3550B 03/08/17 14:25 JEV218954 TAL PLS

Type

Batch Batch

MethodPrep Type LabAnalystRun

Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Analysis 8082 20 218998 03/09/17 10:15 DCH TAL PLSTotal/NA

Client Sample ID: PCB-103 Lab Sample ID: 720-78005-4Matrix: SolidDate Collected: 03/01/17 00:00

Date Received: 03/02/17 15:30

Prep 3550B 03/08/17 14:25 JEV218954 TAL PLS

Type

Batch Batch

MethodPrep Type LabAnalystRun

Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Analysis 8082 1 218999 03/09/17 11:15 DCH TAL PLSTotal/NA

Client Sample ID: PCB-104 Lab Sample ID: 720-78005-5Matrix: SolidDate Collected: 03/01/17 00:00

Date Received: 03/02/17 15:30

Prep 3550B 03/08/17 14:25 JEV218954 TAL PLS

Type

Batch Batch

MethodPrep Type LabAnalystRun

Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Analysis 8082 50 218998 03/09/17 11:15 DCH TAL PLSTotal/NA

Laboratory References:

TAL PLS = TestAmerica Pleasanton, 1220 Quarry Lane, Pleasanton, CA 94566, TEL (925)484-1919

TestAmerica Pleasanton

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Certification SummaryClient: Ninyo & Moore TestAmerica Job ID: 720-78005-1Project/Site: EVC/ROBLE

Laboratory: TestAmerica PleasantonUnless otherwise noted, all analytes for this laboratory were covered under each certification below.

Authority Program EPA Region Certification ID Expiration Date

California 24969State Program 01-31-18

Analysis Method Prep Method Matrix Analyte

TestAmerica Pleasanton

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Method SummaryTestAmerica Job ID: 720-78005-1Client: Ninyo & Moore

Project/Site: EVC/ROBLE

Method Method Description LaboratoryProtocol

SW8468082 Polychlorinated Biphenyls (PCBs) by Gas Chromatography TAL PLS

Protocol References:

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

Laboratory References:

TAL PLS = TestAmerica Pleasanton, 1220 Quarry Lane, Pleasanton, CA 94566, TEL (925)484-1919

TestAmerica Pleasanton

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Sample SummaryTestAmerica Job ID: 720-78005-1Client: Ninyo & Moore

Project/Site: EVC/ROBLE

Lab Sample ID Client Sample ID ReceivedCollectedMatrix

720-78005-1 PCB-100 Solid 03/01/17 00:00 03/02/17 15:30

720-78005-2 PCB-101 Solid 03/01/17 00:00 03/02/17 15:30

720-78005-3 PCB-102 Solid 03/01/17 00:00 03/02/17 15:30

720-78005-4 PCB-103 Solid 03/01/17 00:00 03/02/17 15:30

720-78005-5 PCB-104 Solid 03/01/17 00:00 03/02/17 15:30

TestAmerica Pleasanton

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Login Sample Receipt Checklist

Client: Ninyo & Moore Job Number: 720-78005-1

Login Number: 78005

Question Answer Comment

Creator: Arauz, Dennis

List Source: TestAmerica Pleasanton

List Number: 1

N/ARadioactivity wasn't checked or is </= background as measured by a survey meter.

N/AThe cooler's custody seal, if present, is intact.

N/ASample custody seals, if present, are intact.

TrueThe cooler or samples do not appear to have been compromised or tampered with.

TrueSamples were received on ice.

TrueCooler Temperature is acceptable.

TrueCooler Temperature is recorded.

TrueCOC is present.

TrueCOC is filled out in ink and legible.

TrueCOC is filled out with all pertinent information.

TrueIs the Field Sampler's name present on COC?

TrueThere are no discrepancies between the containers received and the COC.

TrueSamples are received within Holding Time (excluding tests with immediate HTs)

TrueSample containers have legible labels.

TrueContainers are not broken or leaking.

TrueSample collection date/times are provided.

TrueAppropriate sample containers are used.

TrueSample bottles are completely filled.

N/ASample Preservation Verified.

TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs

TrueContainers requiring zero headspace have no headspace or bubble is <6mm (1/4").

TrueMultiphasic samples are not present.

TrueSamples do not require splitting or compositing.

N/AResidual Chlorine Checked.

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Lab Sample ID Client Sample ID Matrix Sample Type Collection Date Percent Moisture Analysis Method Dilution Factor Analysis Date

720-78005-1 PCB-100 Solid 3/1/2017 0:00 8082 1 3/8/2017 23:48

720-78005-1 PCB-100 Solid 3/1/2017 0:00 8082 1 3/8/2017 23:48

720-78005-1 PCB-100 Solid 3/1/2017 0:00 8082 1 3/8/2017 23:48

720-78005-1 PCB-100 Solid 3/1/2017 0:00 8082 1 3/8/2017 23:48

720-78005-1 PCB-100 Solid 3/1/2017 0:00 8082 1 3/8/2017 23:48

720-78005-1 PCB-100 Solid 3/1/2017 0:00 8082 1 3/8/2017 23:48

720-78005-1 PCB-100 Solid 3/1/2017 0:00 8082 1 3/8/2017 23:48

720-78005-1 PCB-100 Solid 3/1/2017 0:00 8082 1 3/8/2017 23:48

720-78005-1 PCB-100 Solid 3/1/2017 0:00 8082 1 3/8/2017 23:48

720-78005-2 PCB-101 Solid 3/1/2017 0:00 8082 1 3/9/2017 0:04

720-78005-2 PCB-101 Solid 3/1/2017 0:00 8082 1 3/9/2017 0:04

720-78005-2 PCB-101 Solid 3/1/2017 0:00 8082 1 3/9/2017 0:04

720-78005-2 PCB-101 Solid 3/1/2017 0:00 8082 1 3/9/2017 0:04

720-78005-2 PCB-101 Solid 3/1/2017 0:00 8082 1 3/9/2017 0:04

720-78005-2 PCB-101 Solid 3/1/2017 0:00 8082 1 3/9/2017 0:04

720-78005-2 PCB-101 Solid 3/1/2017 0:00 8082 1 3/9/2017 0:04

720-78005-2 PCB-101 Solid 3/1/2017 0:00 8082 1 3/9/2017 0:04

720-78005-2 PCB-101 Solid 3/1/2017 0:00 8082 1 3/9/2017 0:04

720-78005-3 PCB-102 Solid 3/1/2017 0:00 8082 20 3/9/2017 10:15

720-78005-3 PCB-102 Solid 3/1/2017 0:00 8082 20 3/9/2017 10:15

720-78005-3 PCB-102 Solid 3/1/2017 0:00 8082 20 3/9/2017 10:15

720-78005-3 PCB-102 Solid 3/1/2017 0:00 8082 20 3/9/2017 10:15

720-78005-3 PCB-102 Solid 3/1/2017 0:00 8082 20 3/9/2017 10:15

720-78005-3 PCB-102 Solid 3/1/2017 0:00 8082 20 3/9/2017 10:15

720-78005-3 PCB-102 Solid 3/1/2017 0:00 8082 20 3/9/2017 10:15

720-78005-3 PCB-102 Solid 3/1/2017 0:00 8082 20 3/9/2017 10:15

720-78005-3 PCB-102 Solid 3/1/2017 0:00 8082 20 3/9/2017 10:15

720-78005-4 PCB-103 Solid 3/1/2017 0:00 8082 1 3/9/2017 11:15

720-78005-4 PCB-103 Solid 3/1/2017 0:00 8082 1 3/9/2017 11:15

720-78005-4 PCB-103 Solid 3/1/2017 0:00 8082 1 3/9/2017 11:15

720-78005-4 PCB-103 Solid 3/1/2017 0:00 8082 1 3/9/2017 11:15

720-78005-4 PCB-103 Solid 3/1/2017 0:00 8082 1 3/9/2017 11:15

720-78005-4 PCB-103 Solid 3/1/2017 0:00 8082 1 3/9/2017 11:15

Lab Sample ID Client Sample ID Matrix Sample Type Collection Date Percent Moisture Analysis Method Dilution Factor Analysis Date

720-78005-4 PCB-103 Solid 3/1/2017 0:00 8082 1 3/9/2017 11:15

720-78005-4 PCB-103 Solid 3/1/2017 0:00 8082 1 3/9/2017 11:15

720-78005-4 PCB-103 Solid 3/1/2017 0:00 8082 1 3/9/2017 11:15

720-78005-5 PCB-104 Solid 3/1/2017 0:00 8082 50 3/9/2017 11:15

720-78005-5 PCB-104 Solid 3/1/2017 0:00 8082 50 3/9/2017 11:15

720-78005-5 PCB-104 Solid 3/1/2017 0:00 8082 50 3/9/2017 11:15

720-78005-5 PCB-104 Solid 3/1/2017 0:00 8082 50 3/9/2017 11:15

720-78005-5 PCB-104 Solid 3/1/2017 0:00 8082 50 3/9/2017 11:15

720-78005-5 PCB-104 Solid 3/1/2017 0:00 8082 50 3/9/2017 11:15

720-78005-5 PCB-104 Solid 3/1/2017 0:00 8082 50 3/9/2017 11:15

720-78005-5 PCB-104 Solid 3/1/2017 0:00 8082 50 3/9/2017 11:15

720-78005-5 PCB-104 Solid 3/1/2017 0:00 8082 50 3/9/2017 11:15

720-78005-5 MS PCB-104 Solid MS 3/1/2017 0:00 8082 50 3/9/2017 11:32

720-78005-5 MS PCB-104 Solid MS 3/1/2017 0:00 8082 50 3/9/2017 11:32

720-78005-5 MS PCB-104 Solid MS 3/1/2017 0:00 8082 50 3/9/2017 11:32

720-78005-5 MS PCB-104 Solid MS 3/1/2017 0:00 8082 50 3/9/2017 11:32

720-78005-5 MSD PCB-104 Solid MSD 3/1/2017 0:00 8082 50 3/9/2017 11:48

720-78005-5 MSD PCB-104 Solid MSD 3/1/2017 0:00 8082 50 3/9/2017 11:48

720-78005-5 MSD PCB-104 Solid MSD 3/1/2017 0:00 8082 50 3/9/2017 11:48

720-78005-5 MSD PCB-104 Solid MSD 3/1/2017 0:00 8082 50 3/9/2017 11:48

LCS 720-218954/2-A Solid LCS 8082 1 3/8/2017 22:41

LCS 720-218954/2-A Solid LCS 8082 1 3/8/2017 22:41

LCS 720-218954/2-A Solid LCS 8082 1 3/8/2017 22:41

LCS 720-218954/2-A Solid LCS 8082 1 3/8/2017 22:41

MB 720-218954/1-A Solid MB 8082 1 3/8/2017 22:24

MB 720-218954/1-A Solid MB 8082 1 3/8/2017 22:24

MB 720-218954/1-A Solid MB 8082 1 3/8/2017 22:24

MB 720-218954/1-A Solid MB 8082 1 3/8/2017 22:24

MB 720-218954/1-A Solid MB 8082 1 3/8/2017 22:24

MB 720-218954/1-A Solid MB 8082 1 3/8/2017 22:24

MB 720-218954/1-A Solid MB 8082 1 3/8/2017 22:24

MB 720-218954/1-A Solid MB 8082 1 3/8/2017 22:24

MB 720-218954/1-A Solid MB 8082 1 3/8/2017 22:24

Lab Sample ID CAS Analyte Result Unit Flag High Limit High Limit Type Low Limit Low Limit Type

720-78005-1 2051-24-3 DCB Decachlorobiphenyl 170 ug/Kg 680 RL

720-78005-1 12674-11-2 PCB-1016 ND ug/Kg 680 RL 140 MDL

720-78005-1 11104-28-2 PCB-1221 ND ug/Kg 680 RL 140 MDL

720-78005-1 11141-16-5 PCB-1232 ND ug/Kg 680 RL 140 MDL

720-78005-1 53469-21-9 PCB-1242 ND ug/Kg 680 RL 140 MDL

720-78005-1 12672-29-6 PCB-1248 ND ug/Kg 680 RL 140 MDL

720-78005-1 11097-69-1 PCB-1254 ND ug/Kg 680 RL 140 MDL

720-78005-1 11096-82-5 PCB-1260 ND ug/Kg 680 RL 27 MDL

720-78005-1 877-09-8 Tetrachloro-m-xylene 180 ug/Kg 680 RL

720-78005-2 2051-24-3 DCB Decachlorobiphenyl 240 ug/Kg 700 RL

720-78005-2 12674-11-2 PCB-1016 ND ug/Kg 700 RL 140 MDL

720-78005-2 11104-28-2 PCB-1221 ND ug/Kg 700 RL 140 MDL

720-78005-2 11141-16-5 PCB-1232 ND ug/Kg 700 RL 140 MDL

720-78005-2 53469-21-9 PCB-1242 ND ug/Kg 700 RL 140 MDL

720-78005-2 12672-29-6 PCB-1248 980 ug/Kg 700 RL 140 MDL

720-78005-2 11097-69-1 PCB-1254 ND ug/Kg 700 RL 140 MDL

720-78005-2 11096-82-5 PCB-1260 ND ug/Kg 700 RL 28 MDL

720-78005-2 877-09-8 Tetrachloro-m-xylene 190 ug/Kg 700 RL

720-78005-3 2051-24-3 DCB Decachlorobiphenyl 0 ug/Kg X D 14000 RL

720-78005-3 12674-11-2 PCB-1016 ND ug/Kg 14000 RL 2700 MDL

720-78005-3 11104-28-2 PCB-1221 ND ug/Kg 14000 RL 2700 MDL

720-78005-3 11141-16-5 PCB-1232 ND ug/Kg 14000 RL 2700 MDL

720-78005-3 53469-21-9 PCB-1242 ND ug/Kg 14000 RL 2700 MDL

720-78005-3 12672-29-6 PCB-1248 ND ug/Kg 14000 RL 2700 MDL

720-78005-3 11097-69-1 PCB-1254 ND ug/Kg 14000 RL 2700 MDL

720-78005-3 11096-82-5 PCB-1260 ND ug/Kg 14000 RL 550 MDL

720-78005-3 877-09-8 Tetrachloro-m-xylene 0 ug/Kg X D 14000 RL

720-78005-4 2051-24-3 DCB Decachlorobiphenyl 190 ug/Kg 680 RL

720-78005-4 12674-11-2 PCB-1016 ND ug/Kg 680 RL 130 MDL

720-78005-4 11104-28-2 PCB-1221 ND ug/Kg 680 RL 130 MDL

720-78005-4 11141-16-5 PCB-1232 ND ug/Kg 680 RL 130 MDL

720-78005-4 53469-21-9 PCB-1242 ND ug/Kg 680 RL 130 MDL

720-78005-4 12672-29-6 PCB-1248 1100 ug/Kg 680 RL 130 MDL

Lab Sample ID CAS Analyte Result Unit Flag High Limit High Limit Type Low Limit Low Limit Type

720-78005-4 11097-69-1 PCB-1254 ND ug/Kg 680 RL 130 MDL

720-78005-4 11096-82-5 PCB-1260 ND ug/Kg 680 RL 27 MDL

720-78005-4 877-09-8 Tetrachloro-m-xylene 190 ug/Kg 680 RL

720-78005-5 2051-24-3 DCB Decachlorobiphenyl 0 ug/Kg D X 37000 RL

720-78005-5 12674-11-2 PCB-1016 ND ug/Kg 37000 RL 7200 MDL

720-78005-5 11104-28-2 PCB-1221 ND ug/Kg 37000 RL 7200 MDL

720-78005-5 11141-16-5 PCB-1232 ND ug/Kg 37000 RL 7200 MDL

720-78005-5 53469-21-9 PCB-1242 ND ug/Kg 37000 RL 7200 MDL

720-78005-5 12672-29-6 PCB-1248 ND ug/Kg 37000 RL 7200 MDL

720-78005-5 11097-69-1 PCB-1254 ND ug/Kg 37000 RL 7200 MDL

720-78005-5 11096-82-5 PCB-1260 ND ug/Kg F1 37000 RL 1500 MDL

720-78005-5 877-09-8 Tetrachloro-m-xylene 0 ug/Kg D X 37000 RL

720-78005-5 MS 2051-24-3 DCB Decachlorobiphenyl 0 ug/Kg D X 36000 RL

720-78005-5 MS 12674-11-2 PCB-1016 ND ug/Kg 36000 RL 7100 MDL

720-78005-5 MS 11096-82-5 PCB-1260 ND ug/Kg F1 36000 RL 1400 MDL

720-78005-5 MS 877-09-8 Tetrachloro-m-xylene 0 ug/Kg D X 36000 RL

720-78005-5 MSD 2051-24-3 DCB Decachlorobiphenyl 0 ug/Kg D X 36000 RL

720-78005-5 MSD 12674-11-2 PCB-1016 ND ug/Kg 36000 RL 7100 MDL

720-78005-5 MSD 11096-82-5 PCB-1260 ND ug/Kg F1 36000 RL 1400 MDL

720-78005-5 MSD 877-09-8 Tetrachloro-m-xylene 0 ug/Kg D X 36000 RL

LCS 720-218954/2-A 2051-24-3 DCB Decachlorobiphenyl 14.7 ug/Kg 50 RL

LCS 720-218954/2-A 12674-11-2 PCB-1016 87.1 ug/Kg 50 RL 9.9 MDL

LCS 720-218954/2-A 11096-82-5 PCB-1260 110 ug/Kg 50 RL 2 MDL

LCS 720-218954/2-A 877-09-8 Tetrachloro-m-xylene 8.92 ug/Kg 50 RL

MB 720-218954/1-A 2051-24-3 DCB Decachlorobiphenyl 13.9 ug/Kg 50 RL

MB 720-218954/1-A 12674-11-2 PCB-1016 ND ug/Kg 50 RL 9.9 MDL

MB 720-218954/1-A 11104-28-2 PCB-1221 ND ug/Kg 50 RL 9.9 MDL

MB 720-218954/1-A 11141-16-5 PCB-1232 ND ug/Kg 50 RL 9.9 MDL

MB 720-218954/1-A 53469-21-9 PCB-1242 ND ug/Kg 50 RL 9.9 MDL

MB 720-218954/1-A 12672-29-6 PCB-1248 ND ug/Kg 50 RL 9.9 MDL

MB 720-218954/1-A 11097-69-1 PCB-1254 ND ug/Kg 50 RL 9.9 MDL

MB 720-218954/1-A 11096-82-5 PCB-1260 ND ug/Kg 50 RL 2 MDL

MB 720-218954/1-A 877-09-8 Tetrachloro-m-xylene 7.49 ug/Kg 50 RL

Lab Sample ID Percent Recovery Lower Recovery Limit Upper Recovery Limit RPD RPD Limit Receipt Lab Project Description

720-78005-1 74 2 122 TestAmerica San Francisco EVC/ROBLE

720-78005-1 TestAmerica San Francisco EVC/ROBLE

720-78005-1 TestAmerica San Francisco EVC/ROBLE

720-78005-1 TestAmerica San Francisco EVC/ROBLE

720-78005-1 TestAmerica San Francisco EVC/ROBLE

720-78005-1 TestAmerica San Francisco EVC/ROBLE

720-78005-1 TestAmerica San Francisco EVC/ROBLE

720-78005-1 TestAmerica San Francisco EVC/ROBLE

720-78005-1 79 32 112 TestAmerica San Francisco EVC/ROBLE

720-78005-2 103 2 122 TestAmerica San Francisco EVC/ROBLE

720-78005-2 TestAmerica San Francisco EVC/ROBLE

720-78005-2 TestAmerica San Francisco EVC/ROBLE

720-78005-2 TestAmerica San Francisco EVC/ROBLE

720-78005-2 TestAmerica San Francisco EVC/ROBLE

720-78005-2 TestAmerica San Francisco EVC/ROBLE

720-78005-2 TestAmerica San Francisco EVC/ROBLE

720-78005-2 TestAmerica San Francisco EVC/ROBLE

720-78005-2 83 32 112 TestAmerica San Francisco EVC/ROBLE

720-78005-3 0 2 122 TestAmerica San Francisco EVC/ROBLE

720-78005-3 TestAmerica San Francisco EVC/ROBLE

720-78005-3 TestAmerica San Francisco EVC/ROBLE

720-78005-3 TestAmerica San Francisco EVC/ROBLE

720-78005-3 TestAmerica San Francisco EVC/ROBLE

720-78005-3 TestAmerica San Francisco EVC/ROBLE

720-78005-3 TestAmerica San Francisco EVC/ROBLE

720-78005-3 TestAmerica San Francisco EVC/ROBLE

720-78005-3 0 32 112 TestAmerica San Francisco EVC/ROBLE

720-78005-4 85 2 122 TestAmerica San Francisco EVC/ROBLE

720-78005-4 TestAmerica San Francisco EVC/ROBLE

720-78005-4 TestAmerica San Francisco EVC/ROBLE

720-78005-4 TestAmerica San Francisco EVC/ROBLE

720-78005-4 TestAmerica San Francisco EVC/ROBLE

720-78005-4 TestAmerica San Francisco EVC/ROBLE

Lab Sample ID Percent Recovery Lower Recovery Limit Upper Recovery Limit RPD RPD Limit Receipt Lab Project Description

720-78005-4 TestAmerica San Francisco EVC/ROBLE

720-78005-4 TestAmerica San Francisco EVC/ROBLE

720-78005-4 85 32 112 TestAmerica San Francisco EVC/ROBLE

720-78005-5 0 2 122 TestAmerica San Francisco EVC/ROBLE

720-78005-5 TestAmerica San Francisco EVC/ROBLE

720-78005-5 TestAmerica San Francisco EVC/ROBLE

720-78005-5 TestAmerica San Francisco EVC/ROBLE

720-78005-5 TestAmerica San Francisco EVC/ROBLE

720-78005-5 TestAmerica San Francisco EVC/ROBLE

720-78005-5 TestAmerica San Francisco EVC/ROBLE

720-78005-5 TestAmerica San Francisco EVC/ROBLE

720-78005-5 0 32 112 TestAmerica San Francisco EVC/ROBLE

720-78005-5 MS 0 2 122 EVC/ROBLE

720-78005-5 MS NC 69 120 NC 20 EVC/ROBLE

720-78005-5 MS 0 73 114 NC 20 EVC/ROBLE

720-78005-5 MS 0 32 112 EVC/ROBLE

720-78005-5 MSD 0 2 122 EVC/ROBLE

720-78005-5 MSD NC 69 120 NC 20 EVC/ROBLE

720-78005-5 MSD 0 73 114 NC 20 EVC/ROBLE

720-78005-5 MSD 0 32 112 EVC/ROBLE

LCS 720-218954/2-A 88 2 122 EVC/ROBLE

LCS 720-218954/2-A 65 55 112 EVC/ROBLE

LCS 720-218954/2-A 83 65 120 EVC/ROBLE

LCS 720-218954/2-A 54 32 112 EVC/ROBLE

MB 720-218954/1-A 84 2 122 EVC/ROBLE

MB 720-218954/1-A EVC/ROBLE

MB 720-218954/1-A EVC/ROBLE

MB 720-218954/1-A EVC/ROBLE

MB 720-218954/1-A EVC/ROBLE

MB 720-218954/1-A EVC/ROBLE

MB 720-218954/1-A EVC/ROBLE

MB 720-218954/1-A EVC/ROBLE

MB 720-218954/1-A 45 32 112 EVC/ROBLE

Lab Sample ID SDG Lab Job ID COC IDSample Type DescReceive Date Total Sample Amount Total Sample Amount Units Leach Batch

720-78005-1 720-78005-1 174430 3/2/2017 15:30

720-78005-1 720-78005-1 174430 3/2/2017 15:30

720-78005-1 720-78005-1 174430 3/2/2017 15:30

720-78005-1 720-78005-1 174430 3/2/2017 15:30

720-78005-1 720-78005-1 174430 3/2/2017 15:30

720-78005-1 720-78005-1 174430 3/2/2017 15:30

720-78005-1 720-78005-1 174430 3/2/2017 15:30

720-78005-1 720-78005-1 174430 3/2/2017 15:30

720-78005-1 720-78005-1 174430 3/2/2017 15:30

720-78005-2 720-78005-1 174430 3/2/2017 15:30

720-78005-2 720-78005-1 174430 3/2/2017 15:30

720-78005-2 720-78005-1 174430 3/2/2017 15:30

720-78005-2 720-78005-1 174430 3/2/2017 15:30

720-78005-2 720-78005-1 174430 3/2/2017 15:30

720-78005-2 720-78005-1 174430 3/2/2017 15:30

720-78005-2 720-78005-1 174430 3/2/2017 15:30

720-78005-2 720-78005-1 174430 3/2/2017 15:30

720-78005-2 720-78005-1 174430 3/2/2017 15:30

720-78005-3 720-78005-1 174430 3/2/2017 15:30

720-78005-3 720-78005-1 174430 3/2/2017 15:30

720-78005-3 720-78005-1 174430 3/2/2017 15:30

720-78005-3 720-78005-1 174430 3/2/2017 15:30

720-78005-3 720-78005-1 174430 3/2/2017 15:30

720-78005-3 720-78005-1 174430 3/2/2017 15:30

720-78005-3 720-78005-1 174430 3/2/2017 15:30

720-78005-3 720-78005-1 174430 3/2/2017 15:30

720-78005-3 720-78005-1 174430 3/2/2017 15:30

720-78005-4 720-78005-1 174430 3/2/2017 15:30

720-78005-4 720-78005-1 174430 3/2/2017 15:30

720-78005-4 720-78005-1 174430 3/2/2017 15:30

720-78005-4 720-78005-1 174430 3/2/2017 15:30

720-78005-4 720-78005-1 174430 3/2/2017 15:30

720-78005-4 720-78005-1 174430 3/2/2017 15:30

Lab Sample ID SDG Lab Job ID COC IDSample Type DescReceive Date Total Sample Amount Total Sample Amount Units Leach Batch

720-78005-4 720-78005-1 174430 3/2/2017 15:30

720-78005-4 720-78005-1 174430 3/2/2017 15:30

720-78005-4 720-78005-1 174430 3/2/2017 15:30

720-78005-5 720-78005-1 174430 3/2/2017 15:30

720-78005-5 720-78005-1 174430 3/2/2017 15:30

720-78005-5 720-78005-1 174430 3/2/2017 15:30

720-78005-5 720-78005-1 174430 3/2/2017 15:30

720-78005-5 720-78005-1 174430 3/2/2017 15:30

720-78005-5 720-78005-1 174430 3/2/2017 15:30

720-78005-5 720-78005-1 174430 3/2/2017 15:30

720-78005-5 720-78005-1 174430 3/2/2017 15:30

720-78005-5 720-78005-1 174430 3/2/2017 15:30

720-78005-5 MS 720-78005-1 174430 Matrix Spike 3/2/2017 15:30

720-78005-5 MS 720-78005-1 174430 Matrix Spike 3/2/2017 15:30

720-78005-5 MS 720-78005-1 174430 Matrix Spike 3/2/2017 15:30

720-78005-5 MS 720-78005-1 174430 Matrix Spike 3/2/2017 15:30

720-78005-5 MSD 720-78005-1 174430Matrix Spike Duplicate3/2/2017 15:30

720-78005-5 MSD 720-78005-1 174430Matrix Spike Duplicate3/2/2017 15:30

720-78005-5 MSD 720-78005-1 174430Matrix Spike Duplicate3/2/2017 15:30

720-78005-5 MSD 720-78005-1 174430Matrix Spike Duplicate3/2/2017 15:30

LCS 720-218954/2-A 720-78005-1 Lab Control Sample

LCS 720-218954/2-A 720-78005-1 Lab Control Sample

LCS 720-218954/2-A 720-78005-1 Lab Control Sample

LCS 720-218954/2-A 720-78005-1 Lab Control Sample

MB 720-218954/1-A 720-78005-1 Method Blank

MB 720-218954/1-A 720-78005-1 Method Blank

MB 720-218954/1-A 720-78005-1 Method Blank

MB 720-218954/1-A 720-78005-1 Method Blank

MB 720-218954/1-A 720-78005-1 Method Blank

MB 720-218954/1-A 720-78005-1 Method Blank

MB 720-218954/1-A 720-78005-1 Method Blank

MB 720-218954/1-A 720-78005-1 Method Blank

MB 720-218954/1-A 720-78005-1 Method Blank

Lab Sample ID Leach Date Prep Batch Prep Method Prep Date Prep Type Initial Amount Initial Amount Unit Final Amount

720-78005-1 720-218954 3550B 3/8/2017 14:25 Total/NA 2.19 g 10

720-78005-1 720-218954 3550B 3/8/2017 14:25 Total/NA 2.19 g 10

720-78005-1 720-218954 3550B 3/8/2017 14:25 Total/NA 2.19 g 10

720-78005-1 720-218954 3550B 3/8/2017 14:25 Total/NA 2.19 g 10

720-78005-1 720-218954 3550B 3/8/2017 14:25 Total/NA 2.19 g 10

720-78005-1 720-218954 3550B 3/8/2017 14:25 Total/NA 2.19 g 10

720-78005-1 720-218954 3550B 3/8/2017 14:25 Total/NA 2.19 g 10

720-78005-1 720-218954 3550B 3/8/2017 14:25 Total/NA 2.19 g 10

720-78005-1 720-218954 3550B 3/8/2017 14:25 Total/NA 2.19 g 10

720-78005-2 720-218954 3550B 3/8/2017 14:25 Total/NA 2.15 g 10

720-78005-2 720-218954 3550B 3/8/2017 14:25 Total/NA 2.15 g 10

720-78005-2 720-218954 3550B 3/8/2017 14:25 Total/NA 2.15 g 10

720-78005-2 720-218954 3550B 3/8/2017 14:25 Total/NA 2.15 g 10

720-78005-2 720-218954 3550B 3/8/2017 14:25 Total/NA 2.15 g 10

720-78005-2 720-218954 3550B 3/8/2017 14:25 Total/NA 2.15 g 10

720-78005-2 720-218954 3550B 3/8/2017 14:25 Total/NA 2.15 g 10

720-78005-2 720-218954 3550B 3/8/2017 14:25 Total/NA 2.15 g 10

720-78005-2 720-218954 3550B 3/8/2017 14:25 Total/NA 2.15 g 10

720-78005-3 720-218954 3550B 3/8/2017 14:25 Total/NA 2.2 g 10

720-78005-3 720-218954 3550B 3/8/2017 14:25 Total/NA 2.2 g 10

720-78005-3 720-218954 3550B 3/8/2017 14:25 Total/NA 2.2 g 10

720-78005-3 720-218954 3550B 3/8/2017 14:25 Total/NA 2.2 g 10

720-78005-3 720-218954 3550B 3/8/2017 14:25 Total/NA 2.2 g 10

720-78005-3 720-218954 3550B 3/8/2017 14:25 Total/NA 2.2 g 10

720-78005-3 720-218954 3550B 3/8/2017 14:25 Total/NA 2.2 g 10

720-78005-3 720-218954 3550B 3/8/2017 14:25 Total/NA 2.2 g 10

720-78005-3 720-218954 3550B 3/8/2017 14:25 Total/NA 2.2 g 10

720-78005-4 720-218954 3550B 3/8/2017 14:25 Total/NA 2.22 g 10

720-78005-4 720-218954 3550B 3/8/2017 14:25 Total/NA 2.22 g 10

720-78005-4 720-218954 3550B 3/8/2017 14:25 Total/NA 2.22 g 10

720-78005-4 720-218954 3550B 3/8/2017 14:25 Total/NA 2.22 g 10

720-78005-4 720-218954 3550B 3/8/2017 14:25 Total/NA 2.22 g 10

720-78005-4 720-218954 3550B 3/8/2017 14:25 Total/NA 2.22 g 10

Lab Sample ID Leach Date Prep Batch Prep Method Prep Date Prep Type Initial Amount Initial Amount Unit Final Amount

720-78005-4 720-218954 3550B 3/8/2017 14:25 Total/NA 2.22 g 10

720-78005-4 720-218954 3550B 3/8/2017 14:25 Total/NA 2.22 g 10

720-78005-4 720-218954 3550B 3/8/2017 14:25 Total/NA 2.22 g 10

720-78005-5 720-218954 3550B 3/8/2017 14:25 Total/NA 2.05 g 10

720-78005-5 720-218954 3550B 3/8/2017 14:25 Total/NA 2.05 g 10

720-78005-5 720-218954 3550B 3/8/2017 14:25 Total/NA 2.05 g 10

720-78005-5 720-218954 3550B 3/8/2017 14:25 Total/NA 2.05 g 10

720-78005-5 720-218954 3550B 3/8/2017 14:25 Total/NA 2.05 g 10

720-78005-5 720-218954 3550B 3/8/2017 14:25 Total/NA 2.05 g 10

720-78005-5 720-218954 3550B 3/8/2017 14:25 Total/NA 2.05 g 10

720-78005-5 720-218954 3550B 3/8/2017 14:25 Total/NA 2.05 g 10

720-78005-5 720-218954 3550B 3/8/2017 14:25 Total/NA 2.05 g 10

720-78005-5 MS 720-218954 3550B 3/8/2017 14:25 Total/NA 2.08 g 10

720-78005-5 MS 720-218954 3550B 3/8/2017 14:25 Total/NA 2.08 g 10

720-78005-5 MS 720-218954 3550B 3/8/2017 14:25 Total/NA 2.08 g 10

720-78005-5 MS 720-218954 3550B 3/8/2017 14:25 Total/NA 2.08 g 10

720-78005-5 MSD 720-218954 3550B 3/8/2017 14:25 Total/NA 2.1 g 10

720-78005-5 MSD 720-218954 3550B 3/8/2017 14:25 Total/NA 2.1 g 10

720-78005-5 MSD 720-218954 3550B 3/8/2017 14:25 Total/NA 2.1 g 10

720-78005-5 MSD 720-218954 3550B 3/8/2017 14:25 Total/NA 2.1 g 10

LCS 720-218954/2-A 720-218954 3550B 3/8/2017 14:25 Total/NA 30 g 10

LCS 720-218954/2-A 720-218954 3550B 3/8/2017 14:25 Total/NA 30 g 10

LCS 720-218954/2-A 720-218954 3550B 3/8/2017 14:25 Total/NA 30 g 10

LCS 720-218954/2-A 720-218954 3550B 3/8/2017 14:25 Total/NA 30 g 10

MB 720-218954/1-A 720-218954 3550B 3/8/2017 14:25 Total/NA 30 g 10

MB 720-218954/1-A 720-218954 3550B 3/8/2017 14:25 Total/NA 30 g 10

MB 720-218954/1-A 720-218954 3550B 3/8/2017 14:25 Total/NA 30 g 10

MB 720-218954/1-A 720-218954 3550B 3/8/2017 14:25 Total/NA 30 g 10

MB 720-218954/1-A 720-218954 3550B 3/8/2017 14:25 Total/NA 30 g 10

MB 720-218954/1-A 720-218954 3550B 3/8/2017 14:25 Total/NA 30 g 10

MB 720-218954/1-A 720-218954 3550B 3/8/2017 14:25 Total/NA 30 g 10

MB 720-218954/1-A 720-218954 3550B 3/8/2017 14:25 Total/NA 30 g 10

MB 720-218954/1-A 720-218954 3550B 3/8/2017 14:25 Total/NA 30 g 10

Lab Sample ID Final Amount Unit Re-Analysis Type Analysis Batch Analysis Lab Instrument ID Column_Detector ID Basis

720-78005-1 mL 720-218913 TestAmerica Pleasanton CHPCB # 2 1C WET

720-78005-1 mL 720-218913 TestAmerica Pleasanton CHPCB # 2 1C WET

720-78005-1 mL 720-218913 TestAmerica Pleasanton CHPCB # 2 1C WET

720-78005-1 mL 720-218913 TestAmerica Pleasanton CHPCB # 2 1C WET

720-78005-1 mL 720-218913 TestAmerica Pleasanton CHPCB # 2 1C WET

720-78005-1 mL 720-218913 TestAmerica Pleasanton CHPCB # 2 1C WET

720-78005-1 mL 720-218913 TestAmerica Pleasanton CHPCB # 2 1C WET

720-78005-1 mL 720-218913 TestAmerica Pleasanton CHPCB # 2 1C WET

720-78005-1 mL 720-218913 TestAmerica Pleasanton CHPCB # 2 1C WET

720-78005-2 mL 720-218913 TestAmerica Pleasanton CHPCB # 2 1C WET

720-78005-2 mL 720-218913 TestAmerica Pleasanton CHPCB # 2 1C WET

720-78005-2 mL 720-218913 TestAmerica Pleasanton CHPCB # 2 1C WET

720-78005-2 mL 720-218913 TestAmerica Pleasanton CHPCB # 2 1C WET

720-78005-2 mL 720-218913 TestAmerica Pleasanton CHPCB # 2 1C WET

720-78005-2 mL 720-218913 TestAmerica Pleasanton CHPCB # 2 1C WET

720-78005-2 mL 720-218913 TestAmerica Pleasanton CHPCB # 2 1C WET

720-78005-2 mL 720-218913 TestAmerica Pleasanton CHPCB # 2 1C WET

720-78005-2 mL 720-218913 TestAmerica Pleasanton CHPCB # 2 1C WET

720-78005-3 mL 720-218998 TestAmerica Pleasanton CHPCB # 2 1C WET

720-78005-3 mL 720-218998 TestAmerica Pleasanton CHPCB # 2 1C WET

720-78005-3 mL 720-218998 TestAmerica Pleasanton CHPCB # 2 1C WET

720-78005-3 mL 720-218998 TestAmerica Pleasanton CHPCB # 2 1C WET

720-78005-3 mL 720-218998 TestAmerica Pleasanton CHPCB # 2 1C WET

720-78005-3 mL 720-218998 TestAmerica Pleasanton CHPCB # 2 1C WET

720-78005-3 mL 720-218998 TestAmerica Pleasanton CHPCB # 2 1C WET

720-78005-3 mL 720-218998 TestAmerica Pleasanton CHPCB # 2 1C WET

720-78005-3 mL 720-218998 TestAmerica Pleasanton CHPCB # 2 1C WET

720-78005-4 mL 720-218999 TestAmerica Pleasanton CHPCB # 2 1C WET

720-78005-4 mL 720-218999 TestAmerica Pleasanton CHPCB # 2 1C WET

720-78005-4 mL 720-218999 TestAmerica Pleasanton CHPCB # 2 1C WET

720-78005-4 mL 720-218999 TestAmerica Pleasanton CHPCB # 2 1C WET

720-78005-4 mL 720-218999 TestAmerica Pleasanton CHPCB # 2 1C WET

720-78005-4 mL 720-218999 TestAmerica Pleasanton CHPCB # 2 1C WET

Lab Sample ID Final Amount Unit Re-Analysis Type Analysis Batch Analysis Lab Instrument ID Column_Detector ID Basis

720-78005-4 mL 720-218999 TestAmerica Pleasanton CHPCB # 2 1C WET

720-78005-4 mL 720-218999 TestAmerica Pleasanton CHPCB # 2 1C WET

720-78005-4 mL 720-218999 TestAmerica Pleasanton CHPCB # 2 1C WET

720-78005-5 mL 720-218998 TestAmerica Pleasanton CHPCB # 2 1C WET

720-78005-5 mL 720-218998 TestAmerica Pleasanton CHPCB # 2 1C WET

720-78005-5 mL 720-218998 TestAmerica Pleasanton CHPCB # 2 1C WET

720-78005-5 mL 720-218998 TestAmerica Pleasanton CHPCB # 2 1C WET

720-78005-5 mL 720-218998 TestAmerica Pleasanton CHPCB # 2 1C WET

720-78005-5 mL 720-218998 TestAmerica Pleasanton CHPCB # 2 1C WET

720-78005-5 mL 720-218998 TestAmerica Pleasanton CHPCB # 2 1C WET

720-78005-5 mL 720-218998 TestAmerica Pleasanton CHPCB # 2 1C WET

720-78005-5 mL 720-218998 TestAmerica Pleasanton CHPCB # 2 1C WET

720-78005-5 MS mL 720-218998 TestAmerica Pleasanton CHPCB # 2 1C WET

720-78005-5 MS mL 720-218998 TestAmerica Pleasanton CHPCB # 2 1C WET

720-78005-5 MS mL 720-218998 TestAmerica Pleasanton CHPCB # 2 1C WET

720-78005-5 MS mL 720-218998 TestAmerica Pleasanton CHPCB # 2 1C WET

720-78005-5 MSD mL 720-218998 TestAmerica Pleasanton CHPCB # 2 1C WET

720-78005-5 MSD mL 720-218998 TestAmerica Pleasanton CHPCB # 2 1C WET

720-78005-5 MSD mL 720-218998 TestAmerica Pleasanton CHPCB # 2 1C WET

720-78005-5 MSD mL 720-218998 TestAmerica Pleasanton CHPCB # 2 1C WET

LCS 720-218954/2-A mL 720-218913 TestAmerica Pleasanton CHPCB # 2 1C WET

LCS 720-218954/2-A mL 720-218913 TestAmerica Pleasanton CHPCB # 2 1C WET

LCS 720-218954/2-A mL 720-218913 TestAmerica Pleasanton CHPCB # 2 1C WET

LCS 720-218954/2-A mL 720-218913 TestAmerica Pleasanton CHPCB # 2 1C WET

MB 720-218954/1-A mL 720-218913 TestAmerica Pleasanton CHPCB # 2 1C WET

MB 720-218954/1-A mL 720-218913 TestAmerica Pleasanton CHPCB # 2 1C WET

MB 720-218954/1-A mL 720-218913 TestAmerica Pleasanton CHPCB # 2 1C WET

MB 720-218954/1-A mL 720-218913 TestAmerica Pleasanton CHPCB # 2 1C WET

MB 720-218954/1-A mL 720-218913 TestAmerica Pleasanton CHPCB # 2 1C WET

MB 720-218954/1-A mL 720-218913 TestAmerica Pleasanton CHPCB # 2 1C WET

MB 720-218954/1-A mL 720-218913 TestAmerica Pleasanton CHPCB # 2 1C WET

MB 720-218954/1-A mL 720-218913 TestAmerica Pleasanton CHPCB # 2 1C WET

MB 720-218954/1-A mL 720-218913 TestAmerica Pleasanton CHPCB # 2 1C WET

Lab Sample ID Analyte Type Result Status TPU TPU Sigma Decision Level Retention Time Spike Amount Expected Amount RER

720-78005-1 Surrogate PRIMARY 11.14 228 228

720-78005-1 Target PRIMARY

720-78005-1 Target PRIMARY

720-78005-1 Target PRIMARY

720-78005-1 Target PRIMARY

720-78005-1 Target PRIMARY

720-78005-1 Target PRIMARY

720-78005-1 Target PRIMARY

720-78005-1 Surrogate PRIMARY 3.323 228 228

720-78005-2 Surrogate PRIMARY 11.137 233 233

720-78005-2 Target PRIMARY

720-78005-2 Target PRIMARY

720-78005-2 Target PRIMARY

720-78005-2 Target PRIMARY

720-78005-2 Target PRIMARY

720-78005-2 Target PRIMARY

720-78005-2 Target PRIMARY

720-78005-2 Surrogate PRIMARY 3.323 233 233

720-78005-3 Surrogate PRIMARY 227 227

720-78005-3 Target PRIMARY

720-78005-3 Target PRIMARY

720-78005-3 Target PRIMARY

720-78005-3 Target PRIMARY

720-78005-3 Target PRIMARY

720-78005-3 Target PRIMARY

720-78005-3 Target PRIMARY

720-78005-3 Surrogate PRIMARY 227 227

720-78005-4 Surrogate PRIMARY 11.14 225 225

720-78005-4 Target PRIMARY

720-78005-4 Target PRIMARY

720-78005-4 Target PRIMARY

720-78005-4 Target PRIMARY

720-78005-4 Target PRIMARY

Lab Sample ID Analyte Type Result Status TPU TPU Sigma Decision Level Retention Time Spike Amount Expected Amount RER

720-78005-4 Target PRIMARY

720-78005-4 Target PRIMARY

720-78005-4 Surrogate PRIMARY 3.315 225 225

720-78005-5 Surrogate PRIMARY 244 244

720-78005-5 Target PRIMARY

720-78005-5 Target PRIMARY

720-78005-5 Target PRIMARY

720-78005-5 Target PRIMARY

720-78005-5 Target PRIMARY

720-78005-5 Target PRIMARY

720-78005-5 Target PRIMARY

720-78005-5 Surrogate PRIMARY 244 244

720-78005-5 MS Surrogate PRIMARY 240 240

720-78005-5 MS Spike PRIMARY 1920 1920

720-78005-5 MS Spike PRIMARY 1920 1920

720-78005-5 MS Surrogate PRIMARY 240 240

720-78005-5 MSD Surrogate PRIMARY 238 238

720-78005-5 MSD Spike PRIMARY 1900 1900

720-78005-5 MSD Spike PRIMARY 1900 1900

720-78005-5 MSD Surrogate PRIMARY 238 238

LCS 720-218954/2-A Surrogate PRIMARY 11.14 16.7 16.7

LCS 720-218954/2-A Spike PRIMARY 133

LCS 720-218954/2-A Spike PRIMARY 133

LCS 720-218954/2-A Surrogate PRIMARY 3.322 16.7 16.7

MB 720-218954/1-A Surrogate PRIMARY 11.141 16.7 16.7

MB 720-218954/1-A Target PRIMARY

MB 720-218954/1-A Target PRIMARY

MB 720-218954/1-A Target PRIMARY

MB 720-218954/1-A Target PRIMARY

MB 720-218954/1-A Target PRIMARY

MB 720-218954/1-A Target PRIMARY

MB 720-218954/1-A Target PRIMARY

MB 720-218954/1-A Surrogate PRIMARY 3.324 16.7 16.7


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