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Concept for quality surveillance
exemplary at a shell-and-tube heat
exchanger
ACHEM ASIA 2013Joining in Chemical Apparatus and Plant Construction
May, 13th-16th, 2013, Beijing
BASF SE BASF Company Ltd.
Technical Inspection/Materials Engineering Quality Management/Materials Engineering
Dr. Rainer Eckrich Dr. Guang BinRao
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Requirements of the "Internal Tightness"
of shell-and-tube heat exchangers
Possible impact of presumed leakage:
1) - No impact on "SHE" and environment
- Impact on product quality is not relevant
2) - No immediate impact on "SHE"
- Product contamination is relevant
3) - Immediate impact on "SHE"
- Product contamination is unacceptableOperator must define additional measurements
SHE: = Safety, Health and Environment
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Requirements of tube-tube-sheet joints
(load criteria and tightness requirements)
-Design (minimum tube wallthickness)
-Manufacturing process
(rolling/expanding, welding,
number of layers)
- Type and scope of non-destructive testing
-Quality surveillance/
inspections during fabrication
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Requirements of tube-tube-sheet joints
(load criteria and tightness requirements)
Load criteria A, B, C, D
Tightness requirement(impact of a presumed
leakage)1: No impact
2: No immediate impact
3: immediate impact
Example C3:
s = 2 mm; 2 layers
Including RT testing
In-fabrication inspection
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Recommended weld preparation and
execution
Throat thickness shall be greater
than tube wall thickness (a ≥ t)
Deviating weld preparation
is possible but approval
is required
a
a
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Implementing quality surveillance (1)
Measures before fabrication
Measures before fabrication starts
Advising the requisitioner/orderer
Inspection of the technicaldocumentation
Actions before beginning thetube-to-tube-sheet welding
“Mock-up” welding/procedurequalification
Monitoring of test welding/welders
Evaluation of the test samples AchemAsia 2013 - Joining in Chemical Apparatus and Plant Construction
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Implementing quality surveillance (2)
Fabrication and testing
Measures during welding – in-
fabrication inspections
Weld preparation
Cleanliness
Executing the tube-to-tube-sheet
welding (skills/welding parameters)
Measures after welding – " final
inspection"
Visual inspection Manufacturer tests and inspections
(VT, PT, MT, LT)
RT inspection for heat exchangers
with tightness requirement "3"
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Pores in tube-to-tubesheet welding
Result of radiographic test on tube-to-tube-sheet
joints
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Inspection of shell-and-tube heat exchangers
Test equipment RT – “Back Radiation Technique
with Gammamat B3”
Test setup w ith isotope Ir 192
Additional inspection
Scope of inspection graduated by the
number of tubes and test result
(1st/2nd sample 100% or new)
Gammamat B3, 1 x 0.5 mm
source, activity max. 110 GBq Film C3, 10 x 12 cm, Pb 0.02 /
0.02, with holes
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Improved Radiation-test-system (x-ray)
Anode grounded tubes, Warrikhoff, Berlin
Metal-ceramic tube MCTS 130 - 0.6
130 kV, 300 W, focal spot 0.6 mm
Emission angle 168 x 360°
Rod anode (Diameter 6 mm)
Transformer unit
Operating unit
kV cable
Film-based application / detector
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Limits of application lr 192:
Dimensions tube-to-tubesheet joints
from 16 x 1.5 mm to 76 x 4 mm Carbon steel, high-alloy steel,
Ni-basis materials,
Tube-to-tubesheet joints with up to
15 mm projection
Oval tubes
Areas of application of x-ray tube:
From 8 mm inner tube diameter
Carbon steel, high-alloy steel,nickel and titanium
For customized design (projection
of tubes, material) - test piece
required
Limits of application
Gammamat B3 versus Grounded tube
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Radiographic testing of the
tube-to-tube-sheet joints
1. With gamma ray source (Ir192)
Back-radiation technique
(d = 1 x 0.5 mm) or forward-radiation technique (d = 2 x 1 mm)
2. With x-ray tubes
(grounded anode tubes, d = 1mm )
back-radiation technique on filmbasis
3. With x-ray tube (grounded anode
tube) – back-radiation with CdTe
detector
Detectabili ty of irregularities
D e t e c t a b l e s
i z e o f f l a w ( m
m
)
0.5
1.0
1. Ir192
2. Rod anode on film basis
3. Rod anode with detector
0.3
0.2
Detectabili ty of irregularit ies
Comparison of test systems
mm
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RT scope of inspection of the tube-to-tube-
sheet joints as per table 6.3.1, BASF E-S-
MC 331
RT scope of inspection and evaluation criteria
(E-S-MC331)
Evaluation criteria as per table 6.3.2.1
!Evaluation and acceptance
criteria do not depend on
test-system
!
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Improved RT test system
Comparison of tests systems
Ir192 + film Rod anode + film Rod anode + detector
85 GBq, 1 x 0.5, film C3,
2 x 0.02 Pb film
tB
= 1 min
130 kV, 0.5 mA, film C3,
1 mm Sn pre-filter, 2 x 0.02 Pb
tB = 0.5 min
75 kV, 0.5 mA,
tB = 0.5 min
High pass filter
0.8 mm
0.5 mm
0.3 mm
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Improved RT test system
x-ray film / detector pictures
Tube dimension Ø 25 x 2 mm, exposure data: 80 kV/ 0.5 mA / 30 sec
Detector picture
Pore
and
tungsten
inclusion
X-ray film
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Improved RT test system
Tube dimension Ø 25 x 2 mm
X-ray film PT Inspection Detector picture
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Comparison of RT-test systems
Summary
Isotope Ir192 –
film-based
X-ray tube –
film-based
X-ray tube -
detector-based
Advantage:
• large scope of object
• easy to use
Disadvantage:
• permanent source ofradiation
• disintegration of theisotope
• reduced detectability of
details
Advantage:
• high detectability of details
• fixed recording parameters
• simple transport
Disadvantage:
• lower scope of object
Advantage:
• see x-ray tubes
• lower radiation exposure
• immediate evaluationpossible
Disadvantage:
• sensitive technology
• high investment cost
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Classif ication of shell-and-tube heat exchangers
purchased in 2012
Q u a n t i t y
Classification
Total: 342
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Summary and Outlook
Number of leakages in shell-and-tube heat exchangers due to
fabrication-related errors substantially reduced
Wide acceptance of this BASF standard in projects and while procuring
heat-exchangers
Procedure successfully implemented in Europe, Asia and in the US
Inclusion of heat exchanger tubes in this quality surveillance concept
Application of “Risk based quality assurance (RisQ)” to further welded
constructions and standards
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