11
High sensitivity imaging by using secondary electrons in a VP-mode
Environmental Secondary Electron Detector II, ESED II (Option)
The ESED II detects a signal that is the result of thesecondary electrons interacting with the gas in thechamber. The resultant image has all the characteris-tics and topographical information of a traditional sec-ondary electron image.
A comparison of the ESED II and BSE images in VP-mode
A complemental use of the ESED II with the standard BSE detector allows a comparison of two images. BSEimages show sample compositions while ESED II images show surface topography of a sample closely.
Typical applications of the ESED II detector
BSE image ESED II imageSample: LLP (Long-Lasting Phosphor)
Sample: Rubber roller Sample: IC on a printed circuit board
A general view of the ESED II mounted on the S-3700N
The same field of view
12
For observation of wet samples for a long time
Cooling stage (Option)
Cooling stage can be used to image hydrated samples such as biological material, plants, food products and emul-sions as the vaporization of water content can be minimized by keeping the sample between 0 to –20°C. It allowsobservation and analysis of water-containing samples for a few tens of minutes to a couple of hours without causingdeformation of samples. This is recommended to observe beam sensitive samples as well.
Typical applications of a cooling stage
Sample shrinkage is seen after 10 minutes. Sample shrinkage is not seen after 10 minutes.Sample: Plum petal
A general view of a cooling stage
A relation of water and its vapor pressure
Pressure (Pa)
Tem
pera
ture
(°C
)
Variable pressure range of the S-3700N
A cooling stage
A water (ice) vapor pressure curve
Evaporation
Freezing
Freezing
At an ambient temperature At –20°C (A cooling stage was used.)
30
0
–606 10 102 103 104
13
For convenient and comfortable operations
Operation guide
This software helps the operator select the optimumoperating conditions applicable to the user’s application.By simply following the instructions the S-3700N will beset to the proper operating conditions.
Customizing the GUI
The S-3700N allows the operator to customize the GUI to suite their applications, samples or their personal prefer-ence.
Operation panel
The S-3700N can be controlled either by mouse andsoftware or by rotary controls on a separate opera-tion panel which is equipped as standard. The lay-out of rotary controls is common with many otherHitachi SEM’s such as S-5500, S-4800 and S-3400N.
14
Image data management (SEM data manager)
The SEM data manager is an original soft-ware of Hitachi PC-SEMs. It allows auto-matic registration of stored images in thedatabase by the user name. It allows usersto select any one of registered images bydate, operating conditions, size of images,keywords, folders, etc. It also allows grayscale controls, image processing, free-lay-out and print out images.
Free-layout printing
Selected images or thumbnail images can be sorted and pasted into print layout image. The pasted images can bemanipulated prior to saving as an HTML, transferring to MS Word* or printing.
* Microsoft Word
Transfer toMicrosoft® Word.
Microsoft® Word is a registered trademark of Microsoft Corp., U. S. A.
15
Simple maintenance
3D animated maintenance guide
Auto Beam Setting
After the installation of a new filament, it is necessary to adjust the filament current, electron beam alignment,focus brightness and contrast. This can all be achieved automatically with the click of a single button.
Pre-centered cartridge filament
There is no need for the operator to perform complicated and deli-cate alignment procedures. The filaments for the S-3700N are pre-aligned at the factory so there is no need to perform centering inthe field.
Condenser lens apertures (Column liner design)
The condenser lens fixed apertures are all located within the linertube and can be simply removed through the gun chamber. It isnot necessary to disassemble the column to gain access to theaperture assembly. 3D animated maintenance guide providesusers with step by step instructions on how to replace the aper-tures.
The S-3700N has a 3D animated maintenance guide that shows the procedure for routine tasks such as to replace afilament.
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Optional software for extended data analyses
3D View software (Option)
Using the BSE detector equipped as standard the 3D software generates surface roughness measurements and aninteractive 3D model display of the sample.
Critical Dimension measurement function (Option)
The critical dimension measurement function allows measurements of dimensions and angles of a specific point of inter-est on an SEM image. This function includes manual/auto-measurements, sequential measurements and simultaneousmeasurements of width and pitch. Users may select any one of these measurements to suite their specific purposes.
A result of angle measurements
A result of simultaneous width and pitch (2µm)measurements
A 3D-model and a sectional profile
17
Sample holders
Multi sample holders (Option)
Special holders (Option)
Here are sample holders prepared for some specific purposes.
Wafer holders (Option)
Here are sample holders for wafers of 2 to 8 inches (SEMI compatible). These holders allow loading/unloading wafers at one touch.
Multi sample holders for 14 and 33 (15mm stubs) samples are available. All of the stubs are indexed in software andby selecting the required stub on the holder layout the stage can be driven to the center of that stub.
Multiple sample holder with samples of 15mm dia. × 14 pcs Multiple sample holder with samples of 15mm dia. × 33 pcs
Sample holder for resin embedded samples
Wafer holders for 4, 6, and 8 inch wafers
Sample holder for EBSP work Sample holder for square samples
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Specifications
Items
Resolution SE
BSE
Magnification
Accelerating voltage
Low vacuum range
Image shift
Maximum specimen size
Specimen stage
X
Y
Z
R
T
Observable area
Maximum height
Stage control
Electron optics
Electron gun
Objective aperture
Gun bias
Detectors
Analytical position
Display
Controls
Monitor
Auto alignment
Auto image adjustment
Image data saving
Filing format
Image display mode
Evacuation system
Operation
Turbo molecular pump
Rotary pump
Protection
Auxiliary functions
Description
3.0nm at 30kV (High vacuum mode)
10nm at 3kV (High vacuum mode)
4.0nm at 30kV (Low vacuum mode)
×5 – ×300,000
0.3 – 30kV
6 – 270Pa through graphic menu
±50µm (WD= 10mm)
300mm in diameter
150mm
110mm
5 – 65mm
360°
–20° – 90°
203mm in diameter (with rotation)
110mm (WD= 10mm)
Computer eucentric 5-axis motorization
Precentered cartridge filament
5-position, click stop objective aperture
Quad bias with variable bias control
Everhart thornley secondary electron detector
High sensitivity semiconductor BSE detector, five segments, fully selectable
WD = 10mm, TOA = 35°
Joystick, keyboard and rotary knob set
19.1 LCD flat panel monitor (subject to change without notice)
Auto beam setting, auto axial alignment,
Auto focus, auto stigmator/focus, Auto brightness & contrast
640 × 480 pixels, 1,280 × 960 pixels
2,560 × 1,920 pixels, 5,120 × 3,840 pixels
BMP,TIFF,JPEG
Full screen display: 1,280 × 960 pixels
Small screen display: 640 × 480 pixels
Dual image display: 640 × 480 pixels × 2
Signal Mixing
Full automatic sequence
210L/sec. × 1
135L/min. (162L/min. with 60Hz) × 1
Power failure and vacuum failure
Raster rotation, dynamic stigma-monitor
Dynamic focus/tilt compensation
Free layout print function, alphanumeric function
3D animation maintenance guide
Navigation, Easy measurement, Oblique image
Specifications Optional accssoriesDetector and analytical tool
Environmental secondary electron detector(ESED-II)
Energy dispersive X-ray spectrometer (EDS) made by third party vender
Wavelength dispersive X-ray spectrometer (WDS) made by third party vender
Electron backscattered diffraction analyzer (EBSD) made by third party vender
Cathode luminescence spectrometer (CL) made by third party vender
Specimen stage and holder
Multiple specimen holder
Plastic embedded specimen holder
Wafer holders (for 3", 4", 5", 6" and 8")
Special specimen holder for EBSD
Specimen exchange device
Cool stage made by third party vender
Software
CD measurement
Hi-mouse (One keyboard, one mouse)
Consecutiveimage recording function (Zigzag capture function)
Stitch
3D View Software
Interface
External communication interface
SCSI
DBC
Others
Chamberscope made by third party vender
Dimensions & weightItems Dimension/weight
Colum unit 780(W) × 850(D) × 1,600(H) mm, 550kg
Display unit 850(W) × 800(D) × 1,200(H) mm, 120kg
Rotary pump 526(W) × 225(D) × 306(H) mm, 28kg
Air compressor 400(W) × 230(D) × 550(H) mm, 18kg
Weight 200(W) × 180(D) × 160(H) mm, 40kg
Installation requirements
Typical installation room layout
Items Description
Room temperature 15 – 30°C
Humidity 70% RH or less
Power supply Single phase AC 110, 115, 200, 220 or 240V(±10%), 2.0kVA
Power cable 10meters long with M5 crimp-type terminal
Grounding 100Ω or better
Unit: mm
850
526400
850
800
225
230
780
1,630
Doorway 850 or greater
400 or greater500 or greater
2,600 or greater
2,25
0 or
gre
ater
Weight
Air compressor
Rotary pump
Display unit
500
or g
reat
er
Column unit
NOTICE: For proper operation, follow the instruction manual when using the instrument.
Specifications in this catalog are subject to change with or without notice, as Hitachi High-Technologies Corporation continues to develop the latest technologies and products for our customers.
Tokyo, Japanhttp://www.hitachi-hitec.com/em/world/24-14 Nishi-Shimbashi 1-chome, Minato-ku, Tokyo, 105-8717, Japan
Printed in Japan (H) HTD-E134P 2010.4