1HNMR Spectrum of Stage-1

Electronic Supplementary Material (ESI) for RSC Advances.This journal is © The Royal Society of Chemistry 2018

13CNMR Spectrum of Stage-1

Mass spectrum of Stage-1

DSC Thermogram of Stage-1

HPLC Chromatogram of Stage-1

1HNMR Spectrum of Stage-2

13CNMR Spectrum of Stage-2

Mass Spectrum of Stage-2

DSC Thermogram of Stage-2

HPLC Chromatogram of Stage-2

1HNMR Spectrum of Stage-3

13 CNMR Spectrum of Stage-3

Mass Spectrum of Stage-3

DSC Thermogram of Stage-3

HPLC Chromatogram of Stage-3 (Chemical purity)

HPLC Chromatogram of Stage-3 (Chiral purity)

1HNMR Spectrum of stage-4

13CNMR Spectrum of stage-4

Mass Spectrum of stage-4

DSC Thermogram of stage-4

HPLC Chromatogram of stage-4

1HNMR Spectrum of stage-5/ Idelalisib

13CNMR Spectrum of stage-5/ Idelalisib

Mass Spectrum of stage-5/ Idelalisib

DSC Thermogram of stage-5/ Idelalisib

HPLC Chromatogram of stage-5/ Idelalisib (Chemical purity)

HPLC Chromatogram of stage-5/ Idelalisib

(Chiral purity)