ICP Test Report Certification Packet/media/files/littelfuse... · 2013-10-12 · 2 . Table 1: List...

1

ICP Test Report Certification Packet

Company name : Littelfuse, Inc. Product Series: 3AB FUSE Product #: 324xxxP Series Issue Date: April 10, 2013 It is hereby certified by Littelfuse, Inc. that there is neither RoHS (recast 2011/65/EU of R0HS Directive 2002/95/EC)-restricted substance nor such use, for materials to be used for unit parts, for packing/packaging materials, and for additives and the like in the manufacturing processes. In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing processes, are all composed of the following components.

Issued by:

<Global EHS Specialist> (1) Parts, sub-materials and unit parts

This document covers the 3AB Fuse RoHS-Compliant series products manufactured by Littelfuse, Inc. ＜ Raw Materials Used

Please see Table 1 (2) The ICP data on all measurable substances Please see appropriate pages as identifed in Table 1

Remarks：

Form 585-047 Rev. A 2/21/06

2

Table 1: List of Raw Materials covered by this report

Total Parts Raw Material Part Number Raw Material Description Page(s)

1 3M 3779-PG (087244) HMA 3-15 2 910-005/ 910-282 Cap 16-19 3 917-481****-P1 Element – Zinc alloy 20-23 4 (917-445*****-P / 917-48*****-P) Element – Brass Cu 24-27

5 910-054/910-055/

910-061/910-068/ 934-055 Overcap 28-31 6 C610 (909-162/909-165) Ceramic Body 32-60 7 YTW206 (692529) Solder 61-65

8 AIM230 Fast Core H RSA605

(692539-003) Solder 66-70 9 425901 Ink - red 71-81

10 425-907 Ink - green 82-92 11 082xxx Element –Ag Cu plated 93-97 12 11-1175 (497xxx/ 497xxx-001) Element – Ni42Fe58MCu 98-103 13 EP608 (087355) Glue 104-107 14 090184 Filler 108-115 15 090187 Filler 116-122 16 091254 Sand 123-129 17 082xxx-001/ 082xxx Tinned wire 130-137 18 YTW108 (692535-003) Solder 138-142

Test Repott No. SHAECl219975401 Date: 19 Nov 2012 Page 1 of 7

3M CHINA LII,lITED

222# T|AN LIN ROAD, SHANGHAI (200233)

The following sample(s) was^lve€ submitted and identified on behalfofthe clients as: 3M 3779-PG

SGS Job No. :

Date of Sample Rec€ivecl

Testing Period :

Test Requested :

Test Method :

Test Results :

Conclusion :

sP12-033081 - SH'14 Nov 2012

14 Nov 2012 - 19 Nov 2012

Selecled test(s) as requested by client

Please refer to next Page(s)

Please refer to next page(s).

Based on the pedormed tests on submitted samples' the results of Lead,

Mercury, Cadmium, Hexavalent cfi romjum, Polybrominated biphenyls (PBB)'

Polybominated diphenyl ether (PBDE) comply with the limits as set by RoHSDireclive 201'1/65/EU Annex ll; recasting 2002/95/EC.

Signed for and on behalf ofSGS-CSTC Ltd.

7QvJJ FanApproved Signatory

nyrbr.d6nrG'drc.dud!or.3sjqql|.!.1e!:1i.-{1tFl|9!':I:?:r,::1::llL:lLryHl*,'xiffi;T;tli#sJ$'iry lbl.d h rlcddr c.idridr ol sxr4 Dritd o6i'rl t'lhlb q ncu

iH;;i-iru;L-,;l;,;;;i.;q+,! t€!,:".s$*.T].":i"j.:,?1i.J:,:t,***H#":f;ffiI1;."*",.,,*,"0..,*'-',

;si'l '.*b $k bd{!drb.srtbnr.sr.l.)r6L.

tl&Jtle.|tiibatrrhlEt{5h'd'lcfl! 2!0r2!aSl .!a .*trqltltrB|l3t|l l* 2r@

iEtEt6?06110245! lE!Et&?l)ol9B6AH!{t-21)G14@4 fLts-21)615063

M€nbor ora€ scs GtoqP lsGS E )

Test Report No. SHAECl219975401 Dater 19 Nov 2012 Page 2 ol7

Test Results :

Test Part Descriotion :

sp€dm€n No. SGS gampls lD Ds.tiption1 SHA12-199754.001 Brown solid

Rematks :(1 )1mg/kg= I PPm = 0 0001%(2) MDL = lrlethod Oeteclion Limit

(3) ND = Not Detecled ( < MDL )(4) ''' = Not Regulated

RoHS Dirbdive 201 1,/65/EU

Test Method : With reference to IEC 6232'1:2008(1) Determination of Cadmium by ICP'OES.(2) Determination of Lead by ICP-OES(3) Determination of Mercury by ICP-OES(4) Determination of Hexavalent Chromium by Colorimetric lvethod using UV-Vis(5) Determination of PBBS / PBDES c.ntent by GC'NIS

Test ltem(s)

Cadmium (Cd)

Lead (Pb)lrercury (Hg)

Hexavalent Chrcmium (Cr(Vl))

Sum of PBBSMonobrcmobiphenylDibromobiphsnylTribromobiphenylTeAabromobiphenylPentabromobiPhenYlHexabromobiphenylHeptabromobiphenylOclabromobiphenylNonabromobiphenylOecabromobiPhenylSum of PBDESMonobromodiPhenyl ethet

Limit Udt100 mg/kg1000 mg/kg1000 ms/kg1000 mg/kg1000 mSikg

- mgKg, mg/Kg- ms/Ks- mg/kg- mg/Kg- mg/Kg_ mg/Kg- mg/Kg- mg/Kg- mg/Kg

1000 mdKs- mg/Kg

MB! @12 N D2 N D2 N D2 N D, N D

5 N D5 N D5 N D5 N D5 N D5 N D5 N D5 N D5 N D5 N O- N D

5 N D

**xmil.xwJri*:1""uw.&:Js-llx""it1!:l#s$ffi---,ffi ffi ffimffi$g j****mui:'xpslti#r,ffi '"i'e'.u;s^T

iffi ffi;*ffi si*rm.fi sm*m:mn***'xmli$:'ffi liii{ilF.ffi.##**'ii,ii lnm s * rr -part' -

Mombgl ol th. sGS GlouP (sca 8A)

fBllrbeYdtuto d)Olrr|Hd,lt tlo,r zrXzl3+l.Ii.*iEEl{rl68tqstl ll:2(t!.3

lE!EPG-n)64$04?9 ls63!.6fLl&'l|5a6dE! .€:d'nc!*6

r EtE &-?r) 61{66!tlj (6+l)611@a{

Test Report

Test ltem(s)

Oibromodiphenyl ethorTribromodiphenyl etherTetrabromodiphenyl etherPentabromodiphenyl elherHexabromodiphenyl elherHeptabromodiphenyl etherOctabromodiphenyl etherNonabromodiphenyl etherD€cabromodiphenyl ether

Notes :

No. SHAEC1219975401

tilnil

Date: 19 Nov 2012

ud! ua! p01mg/kg 5 NDmg/kg 5 NDmdkg 5 NDmg/kg 5 NDmsikg 5 NDmS/kS 5 NOmg/kg 5 NDms/kg 5 NDmdks 5 ND

ulnmg/kg

MDt 0!.11 0 N D

Page 3 of 7

(1) The maximum permissible limit i6 quoted from the directive 2011/65/EU, Annex ll

Ho€brcrno.i dodod€cano (HBCDDI

Test Method : Determination of HBCDD by GC-MS based on IEC 6232112008.

Test ltem(s)Hexabromocydododecane (HBCDD)

Notes :(1) Refurence Information: Directive 2011/65/EU recasting RoHS diredive 200295/EC:

Hexabromocyclododec€ne (HBCDD) is considered as a priority for dsk evaluation and substanc€restriction.

PhttElatc

Test Method : Determination of phthalates by GC-llS bas€d on EN 14372-2004.

Test ltem(sl

Dibutyl Phthalale (DBP)

Benzylbutyl Phthalate (BBP)

Bis-(2-ethylhexyl) Phthalate (DEHP)

Notes :

ud!

%

%

lIpL p!1

0.003 ND0.003 ND0.003 ND

(1) Referenc€ Informationr Direclive 201 t/65/Eu recasting RoHS direclive 200295/EC:Bis (2-ethylhexyl) phthalate (DEHP), Butvl benzyl phthalate (BBP) and Dibutvl phthalate (DBP) are

considered as a pdotity for dsk evaluation and substance restnction.

I bv rh 6tr{t r!16 b r otd !prs!!!' 6fr*tr!+i! 6drqt

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;;;;;-;-d.tbi;tibatird'It b tu.sir.(.|.rbd

ir.,nb.r dl th, AOS Olouo (9CS SA)

t'gtEl$loYtrDto dlrrie!.tlatroa. 20@+1..tl'*iE8tuft3e53Cl ll:2M3

r€lE(6-al6r.rP56! lErEFtl)6tF5!6'9 *4{3dfli|e.a1!611&iaa tiLls"a$a$a ..s.-d)lro!'m

Test Report No. SHAEC1219975401 Date: 19 Nov 2012 Page 4 of 7

ATTACHMENTSRoHS Testlng Flow Chart

1) Name of the person veho made testing: Jan Shi/Yoyo wang/Allen Xiao/Gary xu2) Name of lhe person in cha€e of testing: Jeff Zhang/Georg€ xLu Linda Li3) Thes€ eemples were di$olved totally by preconditioning method according to below flow chart

(Cr6' and PBBS/PBDES test method excluded)

Sample P€paration

Sample Measurement

concentration/Dilution of

extraction solution

1) Alkali Fusion /DryAshing

2) Acid to di6solve Adding 1,$diphenylcarbazid

e for colorclevelopment

Filtration andpH adiustment

Adding 1,5-diphenylcarbazide

development

A red colorindicatesthe

presence of cf'.lf necessary,confirm with

PBBSTPBDE9

.nf,ffi;; l;; ; ;;-a'-vti"ir.mpr.<.tr.oa.

f ucElnlGl|a bdrrri0f.{Eqrtoh 2,@st 'H.*[atar889+3*t! l* r@3

rE€(5-2!)6r{G6i lEl€s-a)6*st9 ls..rqp.6HLlir?r1614&5ea Hj{&-€lFie63 .lF.ftd}r@

ir.ftbor ol th. SOs Gn uP (SGs sA)

Test Report No. SHAEC1219975401 Date:

Phthalates Testing Flovv chart

19 Nov 20'12 Page 5 of 7

'1 ) Name of the person who made testing: Elyn Yao2) Name of the person in charge of testing: Rachel Zhang

Sample measurcment

sffi*'[farncltraYrotodxd luAlrdtoh @+t'II.*,ral&188e+sal ||:2@

rE!E6-aJ0 653 lElE 641l66ttHlj0i-Al)a1il@94 tii{&aFe!

i rmb.r ol lho Sqg Gloot (sGS SA)

Te€t Report No. SHAEC'1219975401 Date: 19 Nov 2012 P€ge 6 of 7

HBCDD Testing Flow Chart

'1) Name of the person who made testingr Gary Xu2) Name ofthe person in charge of tesling: Jessy Huang

ybr[nnrr.{.)r..bd

Sample cutting/preparation

t'AtEls&.t| na&rhloaldslsgloai ?!Cu30+1.-tl.lltr6ttl€30lt3ft|l ll: 2@3

r EtE (ft-zr)6110e,$Hr {[email protected]

rE!€ &a)6€5619HU W-a)Sr60d!0

Momb.tolrho SGs Gmup(sqss )

Test Report No. SHAEC1219975401 Date: 19 Nov 2012 Page 7 of 7

Sample photo:

sHA12- 199754.001

SGS authenticate the photo on originalreport only

"* End of Report "'

iysbrd b(. cm.n condrtlBors!yqerlf!"1:I"l!1139:11-111^qlx'.1*.'l?illlji.lli:;";i d;;s'il*id b b-. m

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r i y&t&'lotasYdlnRoadxtl$adr496r0rlroD 200133

ll!i+!rt4 gB!!9cr!qj!' 1*"tE&8t86-?1t6.1€53679 M.i.sqscomNtj€6-a)s4500qa . s€sd,@g6lsd

r E3E (0&a )61!€2553

Msmberolth6scs Grclp(sGssA)

Test Report No. sHAEc1219975401

3M CHINA LIIVITED

222$ T|AN LtN ROAD, SHANGHAI (200233)

Date: 19 Nov 2012 Page 1 of 6

The following sample(s) was/were submitt€d and identifed on b€half of the clients as : 3M 3779-PG

SGS Job No. I sP12-033081 - SH

Date ofSamole Received : 14 Nov 2012

T€sting Period :

Test Requested :

Test llethod :

Test Resulb :

14 Nov 2012 - 19 Nov 2012

Selected test(s) as requested by client

Please reier to ne)d page(s).

Pleas€ refer to next page(s).

Signed for and on behalf ofsc$csTc Ltd.

,zQr,-'JJ FanApproved Signatory

ryarhdr.r!chdr9!i!lio.ot3$4Fpir1*eqi.lt1-.F-yl-?l'l!:?l.a':!::i*.'":llyP*!-,*#q!a* *!#ffiHii#ffiil[i6;ff"';ii;;;i;;;; l*ffi;ffi;;dM*Fd"ioinr'. "fuo.

riry nrco.Frr F,. dNb'rr bor'c drdfrr4"."*M-nd'-mrn!'!+1P-'-q!]'3a

Itbh.str.G)hnd

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Monb orth.scsGmuo(scsa )

Te6{ Report No. SHAEC1219975401 Date: 1 I Nov 201 2 Page 2 of 6

Test Results :

Test Part D€scriotion :

Sp€d[€nNo. scssamdelD O€€cripdon1 SHA12-1S9754.001 Brown solid

Remarks :(1 ) 1 mg ikg= 1 PPm=00001%(2) MDL = Method Detedion Limit

(3) ND = Not Detected ( < MDL )(4) '-' = Not Regulated

Haloo€n

Test Method : With reference to EN 14582: 2007, analysis was performed by lon Chromatograph (lC)

Test ltem{s)

Fluodne (F)

Chlorine (Cl)

Bromine (Bt)

lodine (l)

UnitmgxgmgKgmgKgm9Kg

MDL OOI

50 ND50 ND50 ND50 ND

r aE leal61.G5lN!(E-t1)6 @9r

rElE p5-a)Ea$6nHjlE-a)ta$5!

n, aq.dbr.oddlGo.drst.ts.t 6;;?r$iU;;l;;;;;"L;iF.ii;. d cod-.E €hd.oo"lll93!-EFg*49:*gg*L"*-..

"*.- .,-'-"

n,aq.dbr.oddrco.drs'!d3fu E4"'rileJlHHrffi#Hilil'

l'iir-Ji&1ii1i;id?i;A;;i.,i;;;i;-1iii,;;;n;"ot'l"io'u'c" de'' n Mr'r F dFdl ; ;-- 'M-r"^d,b.dd-deiMhdL{.de6 tb'h rnP'.lt ' ..bd

t'urErtlpra'.itud&ni&tl5addc'ii ala3+1.-tf

ttdn!.r ot th! aos Golt ISGE sA)

Test Report

ATTACHMENTSRoHS Tosiing Flow Chart

'l) Name of the pe6on who madetesting: Jan Shil/oyo Wang/Allen Xiao/Gary Xu2) Nam€ of the pe6on in charge of te€ting: Jeff Zhang/George Xu/ Linda Li3) These samples were dissolved totally by preconditioning method according to below flow chan

(Cr8' and PBBS/PBDEStest method excluded)

tuodmd r e.d6r lE A.iFryati*rb tu o.ndr c.dtmo, s.tv6,fuE wht Mr.u..i r4rr.' Easb nher!*rlr 6r4!t!:.+!idisr,

l@ffi*ffi *ffi '#fr'n*H#r$Hfi '$ffidi'ffi H#ffi

No. SHAEC1219975401 Date: 19 Nov 2012 Page 3 of 6

Pb/cdrHg PBBsTPBDES

Positive

Sample Measurement

Acid digestion withmicrowave/ hotplate

Concentration/Dilution of

extraction solution

Adding 1,sdiphenylcarbazid

e for colordevelopment

Filtration anclpH adjustment

Adding 1,Sdiphenylcarbazide

for colordevelopment

A red colorindicates th€

presence of Cf'.lf necessary,confirm wth

fhaqlnefirl ht&n BaBtudioa. 2!@'Fl '-tl.*lcaltl3.o]3il l* 2@3

tEtE6-a)€1aaAt$ lEa$-21tr46$70 m..i4!.mH!tt-?[G1,r&50. n!{f-a)am! .rl.ddoe.@

l&hb!. ol th3 SGS G6!p {SGs sa)

Te6t Report No. SHAEC1219975401

Phthalatea Testing Flow chart

1) Name of lhe person who made testing: Elyn Yao2) Name of the pe6on in charge of testing: RachelZhang

D a t e : 1 I N o v 2 0 1 2 Page 4 of 6

rh!@d're.dbr'br.r'.nruldebr.ormico6bd.o'6 'idt6r|d'ni*rtw'lt 6d1!4. rt-o6im',

i&:ffi kffi nl*'**m ,c,'tffi ;,rff '.:t':lffi *'***ffi ffi ---"-@*E&'T4,?gf rffi {dd'|.{sd.nF.hlh'^^'''ox.;i-bdc!'rl rd@"-. t6r rn c.Mt. sr. .o.rb'it I x!rn'dbr!!i!dm'iir-,ffi rffl i;,ffi i-;a-it-iid;;d nia dt"*n oior b.if;-ri-i?i iJr,i; ar; *o -

- i . imsmu.rs* .

tArEPs8nsho(dJdsi49staori a,@sl.ll.*trart|3rld+3ql ll 2@.

tErE6-A)6€596'r Md!..MHLl$-2ll6r66! . €.dn rFdi

l Et€ (6+11R1{!563

M.mb6. olthE 9Os Groop(SSss )

Test Report

1) Name of the Person2) Name of the pe6on

No. SHAEC'1219975401 Date: 1 I Nov 201 2 Page 5 of 6

HBCDD Testing Flow Chart

who made testing: GarY Xuin charge of testing: Jessy Huang

irb'br.6ir(r)r..bd

Sample cuttingy'prepa€tion

Sample measuremeat

tr!-t]se$lsto OOriucl4s||ldChr ?@33+l.It.*iEAt0l88e!tSt fi:2@

IE f,16-a)flrq63fi! (t-2tn14@ct

rElE p6-a)06'19Hr&AF|.M3

Motnb.' ot $o SGS Gm{P lgqs S,A)

tGsTest Report

Sample photo:

'ElF@2)6 a02553 IE&E 186-2 6!9536?9ttLl33-211614691 Nlj(3521)$5na05x . s!sd'@@ts.m

No. SHAEC1219975401 Oate: 19 Nov 2012 Page 6 of6

SGS authenticate the photo on o ginal report only

t"&sBr$.d9Ysh&F@dxlr LHi!.sturcu_cnd 2@233lFt ..t'*.*icEBtt339t3+& It: 2os3

Membat ol lno SGs Giouo {SGs sA)

Customer: Suzhou FuHong Electronjc InduslrialCo., Lld.

Addres!: NO.89 WEIDU ROAD, WANGTINGTOWN, XIANGCHENG DlsTRlCT, SUZHOU, CHINA

Report on ths submitred s.mplesald to be

S.mple name: CoppeJ,shell

Mod€h/

Item/LoiNo.:/

Metar lal : / ,

Buyer: / ,

Suppli€r: /

Samplo recaivsd d.te: Ocl. 08. 2012

Testins period: Ffom oct os, 20!€ 1o'O4r'10, 2012 . . ,,' \ l '

E9S!.s-Ecs!ed9!f

NO.: 4002R12100802+1 R02

As specified by dient, to determine ihe Lead, cadmlun,

accordance with Dircctive 2002/95/EC {RoHS).

AOV"BPFS,U

LiTingting, Maggie

Chemic€l Test Direcror

TEST REPORTDare: ocr.10, 2012

Mercury & Hexavalent Chrcmium content in the submitled sample in

Ylan Qi, lrickey

Ec!!!s-ee$9!.:Testing ltem Measunng instrumeni I\4QL

Lead (Pb) IEC 62321: 2008, s€ction 9 ICP€ES 2-'nglkg

Cadmium (cd) |EC62321: 2008, seclion I ICP-OES 2 mg/kg

[4ercury (Hg) lEc 62321 2008, seclron 7 tcP-oEs 2 mg/kg

Chromum (Cr\rl) IEC 62321 2008 Annex B 0.02m9/k9'

Ieqr 0.02 mg/kg reE|s to the MQL ofsample extfaction liquid

SsElcge!:-when tesled as speci{i€d the submitted sample complied with the requirements of commission Decision ol 18 Aug 2005

amending Directjve 2002/95/Ec noiilied under document 2005/618/Ec

ILS, PLEASE REFER TOTHE FOLLOWNG PAGE(S)***

signed lor and on behalfof

Shenzhen AOV Tesling Technology Co., Ltd, Kunshan Brcncn

caeateaaer: /blfil **n*"oor, We-r k] n ooo,',*or44.

SI tEN2HEN AOV Tf S I ING T€CHNOI ,O6Y CO. , I "TO.KUNSNAN BRANCTI /// \ Noll ne, J a,t 7tt) 9€'t'o

AOV'*F#S,[

NO.: 4002R121008024-1 R02

TEST REPORTOate :Od.10,2012

Content i|retb.r sulit€le). \ .

Cooling the vess€|, nlter;washed and

Rlled 10 the mark with distill€d wat€r.

The sample is digested in the

microwave oven following a specific

decomposrlon program

Test the sample solution and lhe 0.02

ng/kg standard solltion by uv-vls.F;;1.-

SH€NZH€N AOV TESTITIG lCCINOLOGY CO.,LTD.KUNSIIAN BSANCH( :

H o t l r n e'tL)0 700 8600

1. To Determiney'.ead, C€dmium Contenli (Metal subslrate)

I*redby (y'a04*

Add ihe digestion solulioni the

vessel is heated unlil the sampleWeigh ihe sample into

Add HrOruntilthe sample is clear

To Dete

Weigh ihe sample

Cooling the vessel, tiltei washed and

filled lothe maiK wilh dislilled water.Tested by lcP-oES

Chromium Contenl (boiling- wat€F €xtlaclion): ([4etal Eubstrate)

Remove lhe sample, and cool

the beak€r to room temperature,

and do the color reaction

Take the (50i5) cm,

sample in the beaker.Heat 50 mL of Olwater in

the be6ker to boiling for 1o

nov'Bpf,F,il

NO.: 4002R121008024-1R02

5. To oetemine Hexavalenl Chromium Contonl in_ .. -i\

: va'hu't'

TEST REPORTDaie: Ocl.10, 2012

colorless and colored chromate coating on metats: iPtating)

5.2 Boiling-wateF enradion

lfthe lest result is positive,

the sample is considered to

have hexavalent chmmium

Place 1-5

and the 0.02 mg/kg

Boiling- water- extraotionprocedu€ shall be used to

lflhee is interference or it is hard to decide

whetherlhe sample have lhe hexavalent

Remove the sample, and coolthe beaker lo room temperalure,and do lhe color reaction

sample in the beaker.Heat 50 mlof Dlwaier in the

beaker to boiling for 10 min

Test tne sample solution and lhe 0.02mg/kg standad solulion by UV-VIS.

Sample Delcriptlon:

Code Sample Descndion

1-1 Substrate

Plating

Te3t R63ulb:

Unit RoHS Limit

Lead (Pb) msfts 1000 N.D. 1 0

Cadmium (Cd) mg/K9 100 N.D. N.O.Merorry (Hg) ms/Kg 1000 N.D, N.D.

Chromium {Crl,ll) m9/kg 1000 Negative Negative

s8€NZh€N AOV T€SrtNG TECHNOlOSY CO,,tTD,TUNSHAI!ARANCH H ot l in e.100 700 B6a0

,.r

nov'F"Ff"qn

No.: A002R1210o602:L1 R02

neoatve.,-"The te8t is bas€d on lhe followins d!!{mplifi:

maybe cannot stand lor the physical lrdh 6t s€r

TEST REPORT

Coppershell

-The new RoHS dircclive 2011/6tEU, on Jul. 21, 2011 come into forc€, on Jan. 03, 2013lhe formal implementation, Direclive

2002r'95/EC ahall be repealed simultaneously.

Sp€cimens, which r€Slested lo detemine Lead, Cadmium and Mercury Content, have been dissolved completely,-mg/kg=ppm ,-N.D.=not

i",, ,,,,( The iested sample result is uncertain or

SH€NZII AOVTIST|n|G TECHNOIOCV CO.,ITD.KUNSHAN AFANCH H ot l in e400 /00 8600

Pony Testing lntemslional CrouP

&tnE fifi6€, H01252016704D 8S.2013.01 .30

* f t .+Fl , i , ' | | f f+) t€ &ABCAat

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T€st Method :

Test Result6 :

Conclusion :

No. SHAECl215842621 Date: 13 Sep 2012 Page 1 of4

CHINALO LUOYANG COPPER CO., LTD.

NO,50.JIANSHE ROAD,LUOYANG.HENAN PROVINCE

The following sample(s) was6^/ere submitted and identfred on behalf of the clienb as : C10100(Tul)

SGS Job No. : sP12-027024 - SH

Date of Samole Received : 1 0 SeD 201 2

10 Seo 2012 - 13 SeD 2012

Selected tast(s) as requested by client.


Plea66 refer to next page(s).

Bas€d on the performed tesb on 6ubmitted samples, the resulb of Lead,I\rercury, Cadmium, Hexavalent chromium comply wth the limits as set by RoHSDiredive 2011/65/EU Annex ll; recasting 200295/EC.

Signed for and on behalf ofscs-csrc Ltd.

,zQr"-Fan Jingjie, JJApproved Signatory

ryr{xrbrro-n'cFddd.ors{ "d *dn'bh rrbdsrh {r'@'f!qqrird-:miEr-

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IEIE{6-g1)0L660 lE{E(6-il)610536D ffi 6.!..d

NrlE-21)614@4 HL(F21)t$qS3 .llidtEe.S@

Menb6. oi rh€ scs grouD lSGs s.{)

T€6t Report No. SHAEC1215842621 Date: 13 Sep 2012 Page2d4

Test R€sults :

Test Part Descaiption :

Sp€dmonNo. SGSS€mPlolD D6qiDdon1 SHA'12-158426 015 Copper metalsheet

Rema*s :(1) 1 mg/kg= 1 PPm=00001%(2) MDL = Method Detec{ion Limit

(3) ND = Not o€teded ( < MoL )(4) "'' = Not Regulated

Rolls Oil€ ive 201 1r85/EU

Test Method: With reference to IEC 6232'1:2008(1) Determination of Cadmium by ICP-OES(2) Determination of Lead bv ICP-OES'(3) Determination of Mercury by ICP-OES'(4) Determination of Hexavaler{ Chromium by Spot t€€t / Colodmetric lvelhod using Uv-vis

Te6t ltem{s)

Cadmium (Cd)

Lead (Pb)

Merdry (Hg)

Hexavalent Chrornium (Cr(Vl))

Notes :(1) The maximum permissible limit is quoted from direciive 2011/65/EU Annex ll

(2) osPot-test:N;gative = Absence of Cr(Vl) coating, Positive = Presenc€ of Cr(Vl) coating;.

Oh-e tested sample should be fufte; verified by boiling-wateFertrac'tion method if the spot test resuft

is Negative or cannot be confmed )o goiling-water-extraction:Negative = Absence of Cr(Vl) coatingpositive = presence of Cr(vt) coating; the detected conc€ntration in boiling-water-extraction solution is

equal or greater than O.O2 mg/kg with 50 cm" sample surface area

For conilon proteclion coating; on metals: Information on storage @nditions and prcducton date of

the tested sample is unavailable and thus results of Cr(Vl) rspres€nt status of the sample at the time

of testing-

t!nj! Ud! MpL pE

10O mSikS 2 ND1OOO msftg 2 ND1O0O mS/kS 2 ND

Negative

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r ElE {*-er)etoanrr j (i-a!1614s04

Test Report No. SHAEC121584262'1 Date: 13 Sep 2012 Page 3 of 4

ATTACHMENTS

RoHs Testing Flow chart

1) Name of the p€rson who made testing: Jan Shi^/oyo Wangy'Allen xiao2t Name oI the person in charge of testing: Jeff Zhang/George Xusiil;;;;;;;;; tisioiilo totarrv o'v pr*conditionrng methoo accordrng ro oero/ now chart (cf*

test method excluded)

Sample Preparation

Heating to g0-95cfor extraction


2) Acid to dissolve

Adding'1,5-diphenylcarbazide


A red color indicatesthe presence of cf'lf nec€ssary, confirm

PbrcdrHg

Positive

Negative

i'r4db rqshd g:dt:l. o' *rij91l#;Ygl'3'liii"lii-riifii"ir.r$a ;r;r u. c-1*.g cil!gTi.*3::::|.:: ;ac'@ri i"rhe. .thfrdi;;:;id1i;;.r,'d-"'d. @ih'k 4idllrr

ur tltrcolrytr d. ntdsrEfi [ffiiHffi #ffi ":ffi i##;?s'"r'f s&s*$ili:rm'""n'r'*m*.6i14t6mrHff #ffi.:ffiff H##ff**#rfficlms#î:*""i';l**rhlrr'x;try'i'f,$:igiii io lim s * ta -la rt' -rr b tu.str.(.) r6bd

f a-flt&Yrrib.a&nc|l4ar9tcnE 5@+t.tt.*iEEi|llt$e!3r}l l*2@3

rE!€6-erF6Il w.i,.at.mdj{&a)5l@3 . rsdh€4@

r EtE (*-?1)6r1@5tH!o-er)€ @e4

M.mDd ol6e sGs goup (sGss )

Test Report

Sample photo:

No. SHAEo1215842621 Date: 13 Sep 2012 Page 4 of 4

SGS adhenticate the photo on odginal repod only

"' End of Report *'

yg&rt&Lrbrt&irrfal|ldlctrs 2m3+l.It.tiE8lfi ft.ort39l al: ?@l

r ElF i6-2r)611G63HU (6-21t61{6el

tEtE {E+r)0KI9{:(e-aF|e3

M.nb.r ot tr scs Grouo lsGs &r)

Cuslomer: Suzhou FuHong Electronic IndustriatCo., 16.

Addr6s: NO.89 \/ElDU ROAD, WANGTING TOVIN, XTANGCHENG DISTR|CI SUZHOU. CHINARepod on the submltted samrl€ said to be

sample name: Lead wife coppershell

Modol:/

Itefi/Lot Io.: /Matonal:/Buyen/ :S u p p l i e r : / ,

l i lanufacturE:/- . _ - i

- fSample recelved date: Gq _08, 2012 :t*,tn o"n.o, t.. o".;;,,013

"."r.-,.,,613, 1 ,]

&glirs-Bgsccsgq i

As specifed by dienl, to determine the L€ad, Cadrium, l,tercury & tiexayabntChrcmium conle in the 6ubmitted sampte inaccodance with Directive 2OO2I95/EC {RoHS). j

l\OV'BF.F.q,A

TEST REPORTNO.: 4002R121008024-2R02 Oate: Oct.1 0, 2012

Testing ltem Measufing instrument ,MQL

Lead (Pb) IEC 62321:2008. section I rcP-oEs a!gagcadmium (Cd) IEC 62321:2008, s€ction 9 tcP-oEs 2 mg/kg

[,lercury (Hg) IEC 62321r2008, s€ction 7 rcP-oEs 2 mg/kg

Chromium (CrM) IEC 62321: 2008, Annex B 0.02mg/kg*

Testino method:

lsqj 0.02 mg/tg rcturs to the MQL olsample exlraction liquid.

Conclu3ion:-\ryhen tested as specified lhe submilied sample compried with th€ requircments of commission D€cision of 18 Aug 2005

amending Dircctive 2002/95/EC notilied under docum€nt 2005/618/EC.

LiTingting, Maggie

Chemical Test Direclor

Yuan Qi, l,lickey

LabManager

Sign€d ior and on behallol

Shenzhen AOV Testing Technology Co., Ltd, Kunshan 8ran6h

ea"arc"a"r, A?1 W a l b n OrO."*0r44

."*FOR FURTHER DETAILS, PLEASE REFERTOT

Technical Di€clor

STIENZIIEN AOVTE$Tl'{G I€CHI!OLOGY CO,.I.TD,KUNSHAN BRANCI]

(,10",'ll,,u*

l\ov"BF,?sn

NO.: A0O2R12100802+2R02

T63l Flow:

Cooling the vessel, fiitei washed and

fllled lo the mafK with distilled waler.

Add the digestion solulionj thevess€l is heated until the sample

TEST REPORTDate Oci .10,2012

L To Detemine/lead, Cldmium Content (Metal substrale)lestedbY

L7.ôtq,

-*".irl,"*J "r,to,"t|,

Add lhe digestion soluUon, closelhe microwave vessel.

f---- -].-

(Plating)

The sample is digested in the

micrcwave oven tollowing a specinc

deoomposilion progrcm.

Test the sample solulion and ihe 0.02

mg/kg slandard solution by uv-vls.

' H o t l r n e40a 700 8600

Cooling the vessel, frller;washed and

filled to the maft wilh dislilled waler.

Remove lhe sample, and cool

the beak€r lo room temperature,

and do the color reaclion

______-l "*rn nrte,.washedand l_____*p;-r, f;;-1

I rilled lo$e mark with Dlwaler I

ShENZH€N AOV I6STII {G T 'C NOIOGY CO.. ITD.XUNSHAN OEANCH

/\OV"BF#,HN

NO.i A002R121008024-2R02

Sample Doscripilon:

TEST REPORTOate :Oc l10 2012

5. To Deiermine Hexavalent Chromium Content in colorless and colorcd chromate coaling on metals: (Plating)

r e s t e d b v : l ) ^ ,' L/AÛ,4.

5.1 Spotlesl (

f l;"')l;**SN€$ZHEN AOVI :STING T€C NOIOGY CO' ' ITD.XUNSI lAN BBANCI I

lf the lest result is posiiive,

ihe sample is considered lo

have hexavalenl chromium

Place 1-5

and the 0.02 mg/kg

Boiling- water- extracton

procedurc shall be us€d tolf the test reslrlt

lltherc is intederence or it is had to decide

whetherlhe sample have the hexavalent

5.2 Boilin9- water- enractronRemove the sample, and cool

the beaker to rcom temperalu€,

and do the color rcaolion

Take the (50i5)cm2

sample in the beaker.Heat 50 ml ol Dl waler in the

beak€r to boiling lof 10 min

Code Sample Desc{iplion Code

copper shell subslfate

Lead wire Plating 24 Copper shell Platng

Unit RoHS Limit Result

2-3

Lead {Pb) mg/l(g 1000 N.D. N.D. N.D. N.O

Cadmium (Cd) mg/k9 100 N.D. N.D. N.D, N.D.

Meroury (Hg) mg/kg 1000 N.D. N.D. N.D, N D .

Chromum (Crl'I) mg/K9 1000 Negalive Negalrve Negaliv€ Negative

TEST REPORToare: oct.10,2012

-:fh€ new RoHS di€ctive 2011/65/EU, on Jul. 21,2011 come inlo force, on Jan. 03, 2013 ths formal implementation, Direcliv€

200295/EC ahall be repeal€d simultaneously-

Sp€cimens, which ggqeted to d€temine Lead, Cadmium and Mercury conient have been dissolved completelv.

NO.: A0O2R12100802+2R02

-mg/Kg=ppm

--The iest is bas€d on the following

ce of C_rl\,I)lif"veiry/y6hetp ttef.limere sr{.q!.be/rurTr v ii'iffyiT-''

*'q:*lhe spot test result is uncertain or

each pad is unifom. The tesl rcsult

maybe cannot stand for the physical truth-Photo is included

Lead wir€ copper shell

"'End of Repod""

sHEI\tZH:ir AOVrlsrr'tc IECNl'lO!OeY CO.,ITD KUNSHAN SRANCIi

r.r i35.1J:55i0eo0o Fd.3F1t?55roEr$ hrr ,w.d{.di' Fodrdo 1r.r00/ , Hot l rne

I , 400 700 8600

Signature plidForQueslionPlease Qltwith SGSwww.tw.sal-om

rtlt[tll][]|lt

Test Report No.: CE/20't3l/13191 Dale 2013101121 Page: 1 of 29

CERAMTEC GMBHGESCHAFTSBEREICH IJULTIFUNKTIONSKEMMIK,LUITPOLDSTRABE'I5. 91207 LAUF

The following sample(s) was/werc submitted and identified by/on behatf of the client as:

Sample DesoriptionStyle/ltem No.Sample Receiving DateTesting Period

CERAMICc6102013t1tl42013t1tl4 10 2013tO1n1

Test Re3ult(s)

Conclusion

: Please lefer to next page(s).

: Based on the pedomed test6 on 6ubmitted 6amples, the test results of Cadmium, Lead,I\rercury, Hexavalent Chromium Cr(Vl), PBBS and PBDES comply with tho limits as set byRoHS Dircctive 201'1/65/EU Annex ll; recasting 2002/95/EC.

Efnrd fr. aod

Chqdcd frbot bry-Trlgd

tHl5";vtr^:,)n*$i"d h8 T.u:lM

I d!'€'' ledn'"Jg onr oi.-i"oiji.--," **o o n"c.ru rcele o1r{ o'd.r'"€.o*or

f';;il*-fl9#'i"15;; d;hd,"...bndd;cmsns. E-i '.r ' i ' 'r s.rd bndid roE. .1Yand{o1ouon! (

; -to;;'; ;;:' de. rdd a- i {d d s'***d $;i-.h'';l:*l;-*.":*:;;*|'!6;, .,1;TtydT PJ.;1ii:;;T*.iiift i;;5#;i"'":1'"p,;ilbe tme or E fleiEdm onry ad s

t";!i;y1;;*"*#:;;lim:r"r"*li:;.::ir*"'r;fff";ffij'i"""ffi'13il*:#ift'r-"-".ff'""1;",1#,;1""H{i;:i""'ri"rl,1;ii , : : : n r . l l i r i l l i

Test Report No. : CE/2013/13191 DaIe :2013101121 Page: 2ol 29

CERAMTEC GMBHGESCHAFTSBEREICH MULTIFUNfiIONSKERAMIK,LUITPOLDSTRABE 15, 91207 LAUF

l[]t tt][ttttlt

Test Result(s)

PART I{AME No.1 : CREAM CERAirlC

Test ltem(s) Unit Method MDLReault

LimitNo.t

Cadmium (Cd) mg/Kg with reference to lEc 62321: 2008 andperformed by ICP-AES.

2 n.d. '100

Lead (Pb) mdkg With reference to IEC 62321: 2008 andperformed by lCPiEs.

2 204 1000

Mercury (Hg) mg/Kg With reference to IEC 6232 1 : 2008 andperformed by ICP-AES.

2 n.d. 1000

Hexavalent Chromium cr(Vl) msyKg With reference to IEC 62321: 2008 andperfonned by UV-VIS.

2 n.d. 1000

BBP (Benzyl butyl phthalate) (CASNo. : 85-68-7)

With reference to EN 14372. Analysis,ras performed by GC/MS.

0.003 n.d.

DEHP (Di- (2-ethylhexyl)phthalate) (CAS No.: 117-81-7)

o/. With reference to EN 14372. Analysiswas perfomed by GC/MS.

0.003 n.d.

DIDP (Di-i6odecyl phthalate) (CASNo. : 26761 -4O0)

% With reference to EN 14372. Analysis,,,€s p€rformed by GC/|\4S.

0.01 n.d.

DINP (Di-isononyl phthalate) (CASNo.:28553-12-0)

o/o With reference to EN 14372. AnalysiswEs perfomed by GC/MS.

0.01 n.d.

DNOP (Di-n-octyl phthalate) (CASNo.: 117-84-0)

o/o With reference to EN 14372. Analysisw€s perfomed by Gc/Ms.

0.003 n.d.

DBP (Dibutyl phthalate) (CAS No.u-7+2\

% With feference to EN 14372. Analysiswas performed by GC/MS.

0.003 n.o.

Perf luotooctane sulf onates(PFOS-Acid, Metal Salt, Amide)

mg/kg With reference to US EPA 3550C;2007. Analysis was performed byLC/MS.

1 0 n_o.

PFOA (CAS No.; 33S7-1) mg/Kg With reference to Us EPA 355ocl2007. Analysi6 was pedomed byLC/MS.

1 0 n.d,

Polychlorinated Biphenyls (PCBS)(CAS No.r '133,S36-3)

mg/kg with referenc€ to us EPA 3540cmethod. Analysis was perfomed byGC/MS.

0.5 n.d.

Test Report No. I CE/2013/13191Oate | 2013101121Page :3o f29

CERAI,ITEC GMBHGESCHAFTSBEREICH MULTIFUNKTIONSKERA[/|IK,LUITPOLDSTMBE 15. 9'1207 LAUF

tl|||tt lttlul

Test ltem(s) Unit Method MDLR€6ult

LimitNo.'l

Polychlorinat€d Terphenyls(PCTs)

mS/kg With reference to US EPA 3540Cmethod. Analysis\ ras perfomed byGC/MS.

0.5 n . d .

Polychlorinat€d Naphthalene(PCNs)

mgKg Wth reference to US EPA 3540Cmethod. Analysis\ ras performed byGC/MS.

5 n.d.

Alkanes, C10-13, chloro (ShortChain Chlorinated Paraffins) (CASNo. : 85535-84-8)

mg/Kg With reference to US EPA 3540Cmethod. Analysis was performed byGC/l\rs.

'100 n.d.

PVC Analysis was performed by FTIR andFLAME Te6t.

Negative

Formaldehyde (CAS No.: 50{0-0) mg/Kg With reference to ISO 17226-1(2008).Analysis was performed by HPLC/DAD.

3 n.d.

Monomethyl dibromodiphenylmethane (DBBT)

mg/Kg With reference to uS EPA 8270Dmethod. Analysis was performed byGC/MS.

0.5 n.d.

Monomethyl dichlorodiphenylmethane (Ugilec121)

mg/Kg With refefence to US EPA 8270Dmethod. Analysis was performed byGC/MS.

0.5 n.d.

[4onomethyl tetrachlorodiphenylmethane (Ugilec141)

mg/kg With reference to US EPA 8270Dmethod. Analysis was performed byGC/rlts.

0.5 n.d.

HalogenHalogen-Fluodne (F) (CAs No.:14762444\

mg/Kg

Wilh €fe.ence to BS EN USA2:20O7.Analysis was p€rfomed by lC.

50 n.d.

Halogen-Chlorine (Cl) (CAS No.:22537-15-1)

mg/Kg 50 n . d .

Halogen-Bromine (Br) (CAS No.:1OO97-32-2)

mg/Kg 50 n.d.

Halogenlodine (l) (CAS No.:1436244-8)

mg/Kg 50 n.d.

Oryanic.tin compoundaTdbuvl Tin (TBT) mg/Kg With reference to DIN 38407-13.

Analysis was pertormed bY GC/FPD.0.03 n .d .

rriphenylTin (TphT) me/Kg 0.03 n.d.

TestReport No.:CE/201:r/13191 Date:2013t01t21 pase:4of2s

CERAI,TEC GI,BH |I]|||tt][tt rlGESCHAFTSBEREICH MULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE 15, 91207 LAUF

Test ltem(s) Unit method MDLResult

LimitNo.l

AabestosActinolite (CAS No.: 77536-66-4)

Wilh reference to EPA 600/R-93'/1 I 6method. Analysis was performed byStereo l\Iicroscope (SM), DispersionStaining Polarized Light Microscope(DS-PLlr) and X-ray DiffractionSpectrometef (XFID).

NegativeAmosite (CAS No.: 12172-73-5) o/o NegativeAnthophyllite (CAS No.: 77536-67-5)

% Negative

Chrysotjle (CAS No.: 12001-29-5) NegativeCrocidolite (CAS No.: 12OU-2a4\ ok NegaliveTremolile (CAS No.: 7753e68$) % Negative,zo1): 4-AMINODIPHENYL (CAS No.:92-67-1)

mg/Kg With reference to LFGB 82.02-2.Analysis uras performed by cC/lVS.

3 n.d,

BENZIDINE (CAS No.: 92-87- mg/Kg With feference to LFGB 82.02-2.Analysis was performed by GC/IVIS.

3 n.d.

3): 4.cHLORO-O-TOLUIDINE(CAS No.: 9569-2)

mg/Kg With reference to LFGB 82.02-2.Analysis u/as performed by GC/MS.

3 n.d.

4)r 2-NAPHTHYLAMINE (cASNo.r91-59-8)

mg/Kg With reference to LFGB 82.02-2.Analysis w€s performed by GC/MS.

3 n.d.

5): O-AMINOAZOTOLUENE (CASNo.:97-56-3)

mg/kg With reference to LFGB 82.02-2.Analysis was performed by GC/tu|S.

3 n .d .

6): 2-AMlNO.4-NITROTOLUENE(CAS No.: 99-55-8)

mgikg With reference to LFGB 82.02-2.Analysis was performed by GC/MS.

n.o.

7): P-CHLOROANILINE (CAS No.:10647-8)

mg/Kg With referenc€ to LFGB 82.02-2.Analysis wEs performed by GC/MS.

n.d.

8): 2,4-DIAMINOANISOLE (CASNo.:6'15-05-4)

m9Kg With reference to LFGB 82.02-2.Analysis was performed by GC/[,!S.

3 n.d.

9'):4,4-DIAMINODIPHENYLI\4ETHANE(CAS No.: 101-77-9)

mg/Kg With reference to LFGB 82.02-2.Analysis was performed by Gc/Ms.

3 n.d.

10): 3,3'-DICHLOROBENZIDINE(CAS No.: 91-9+1)

mg/Kg with reference to LFGB 82.02-2.Analysis was performed by GC/MS.

3 n.d.

1 1)r 3,3'-DIMETHOXYBENzIDINE(cAS No.r 11$9&)

mgftg With roference to LFGB 82.02-2.Analysis w€s perfomed by GC/MS.

3 n.o,

'1 2): 3,3'-DII,iIETHYLBENZIDINE(CAS No.: 119-93-7)

m9Kg With reference to LFGB 82.02-2.Analy6is was performed by GC/lltS.

3 n.d.

fi ' ' !,"l;*'"*.;*.-".:;". ' ' ' ,.""""...].,";..":"'.s"*"...*"-':.."'"."."-, i l ; , .n i ' jn . i , .n t tomaroi - . "* . -d€o6|er ,ardcotro|3|oLeiii, iil.-niiniiv-iiiiiinnn-in,ii^?,aitd;*uBdlin6dthe;;î i i i i i i"i,i ir,i*o' -ry-"*ri tr. -'borc ctihqrudm' Ir'l -tcomdars ea s!oo!oi,.i"*.i- m * os no a i r.' q*

" o o'qa'o* -0.'- nino;r'doe-44 n s do' -d -moin. ?erc!L("d P e0

li;fiii rii;" r;;a; tao: b's;t "abi"r.d*

oJ rhe @;;;;;i;;;;;i $ n@*i' "

*h*tu sa otundds mai be prcsdcd b '

, " , . , , , . : i l i i ; i l . r , qno*' t r"aFt i r i . l i . { rrr * f : rr}L s d ..::i-:-1' 9P !.ll!!.r.1

Test Report No. : CE/2013/13191 Dale:2013101121 Paqe | 5 of 29

CERAI\4TEC GMBHGESCHAFTSBEREICH MULTIFUNKTIONSKERA[IIK,LUITPOLDSTMBE 15, 91207 LAUF

Il]mttfittltl

Test ltem(s) Unit lrethod MDLR€ult

LimitNo.l

1 3): 3,3!DIMETFIYL-4,4-DIAIJINODIPHENYLMETHANE(CAS No.: 838-88-0)

mg/Kg With reference to LFGB 82.m-2.Analysis was performed by GC/lrS.

3 n.ct.

14)r P-CRESIDINE (2-IUETHOXY-s-METHYLANILINE) (CAS No. I120-71-8)

msasWith reference to LFGB 82.02-2.Analysis was performed by GC/MS.

3 n.d.

'1 5): 4,4.-METI-IYLENE-BIS- (2-CHLOROANILINE) (CAS No.:101-144)

m!/(g With reference to LFGB 82.02-2.Analysis was performed by GC/MS_

3 n.d.

16): 4,4'-OXYDIANILINE (CASNo.r 101-80-4)

mg/Kg With reference to LFGB 82.02-2.Analysjs wEs p€rfomed by GC/MS-

3 n.d.

17): 4,4'-THIODIANILINE (CASNo.: 139€5-1)

mg/Kg With reference to LFGB 82.02-2.Analysis w€s perfomed by GC/MS.

3 n.d.

1E): O-TOLUIDINE (CAS No : 95-s34)

mg/Kg With reference to LFGB 82.02-2.Analysis was performed by GC/MS.

3 n.d.

'1 9): 2,4-TOLUYLENEDIAMINE(CAS No.: 95-80-7)

mg/Kg With reference to LFGB 82.02-2.Analysis wa6 performed by GC/MS.

3 n . d .

20): 2,4,5-TRIMETHYLANILINE(CAS No.: 137-17-7)

mdkg With reference to LFGB 82.02-2.Analysis\ ras performed by co/l\rs.

3 n.d.

21): O-ANISIDINE (CAS No.:90-04-0)


3 n.d.

22): P-AMINOAZOBENZENE(CAS No.r 6M9-3)

mg/Kg With reference to LFGB 82.02-2.Analysis was perfomed by GC/MS.

3 n.d.

23): 2,4-XYLIDINE (CAS No.r95-68-1)

mg/kg With reference to LFGB 82.02-2.Analysis was performed by GC/IVS.

3 n.d.

24): 2,6-XYLIDINE (CAS No.: 87-62-7)


3 n.d.

CFC's (Chlorofl uorocarbons)Group IChlorofluorocabon-1 1 (CAS No.l75€9-4)

mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.

n .d .

Chlorof luorocarbon-1 2 (CAS No. :75-714]


n-d.

;ii; i;i;;; ; ,!,.i .d '; ri. c.-,;;' ',ti; b iL; &ne'ar condi om d;; ;;;;i i;; d;-tu:â 3uh;ed b rem! ano co.o @ns h' rrqd. b;{.I d{w.{s.o- e.i ; ; d ; l a ' ' h " i j . ' i - * ' ; . d i $a fnn ' 3 . "dddh .F 'ha rme or i! 'meilerton onrv and -; ; ; ; - ; ; h : ; . ; n . d J , ' i . i ' . c ' o i d 0 a f ; i " ' d f u r 1 a " .

Nev tdiFi .ir r.iws / I -: .'. qi i ni {li3rrL

Test Report No. : CE/2013/13191 Date: 2013t01t21 Paoe : 6of 29

CERAMTEC GMBHGESCHAFTSBEREICH MULTIFUNKTIONSKERAMIK,LUITPOLDSTMBE 15. 91207 LAUF

rlfll tlt! ttt]l

lest ltem(s) Unit Me{hod MDL R€6ultLimitNo.1

Chlorof luorocarbon-1 13 (CAS No.:76-13-1)

mg/Kg With reference to US EPA 502 1method. Analysis was performed byGC/t S.

1 n.d.

Chlorcfluorocarbon-1 14 (CAS No.l7efi-2)


1 n.o.

Chlorotluorocarbon-l 15 (CAS No.:76-15-3)

msasWith reference to US EPA 5021method. Analysis was performed byGC/MS,

1 n . d .

Group lllChlorof luoroca6on-1 3 (CAS No.:75-72-9)

mg/kg With reference to US EPA 502 1method. Analysis wEs perfomed byGC/MS.

1 n.d-

Chlorof luoroca6on-'1 1 1 (CAS No.:354-56-3)


1 n.d-

Chlorofluoroc€rbon-'112 (CAS No.:76-12-O)

mlyKg With reference to US EPA 5021method. Analysis was performed byGC/MS.

'I n . d .

Chlorof luorocarbon-2l 1 (CAS No.:422-78-8)

mgikg With reference to US EPA 5021method. Analysis was pertormed byGC/MS.

'I n.d.

Chlorof luorocarbon-21 2 (CAS No. :3182-%-1)

mg/Kg With refefence to US EPA 5021method. Analysis wEs performed byGC/MS.

1 n.d.

Chlorof luoocarbon-21 3 (CAS No.:2354{6-5)

mg/kg With reference to US EPA 5021method- Analysis was performed byGC/[rS.

1 n.d.

Chlorof luoroca6on-214 (CAS No.:29255-31-0)

mgKg With reference to US EPA 5021method. Analysis was performed byGC/MS.

n.d.

Chlorof luorocarbon-215 (CAS No.:425943-2)

mgi Kg With reference to US EPA 5021method. Analysis w€s performed byGC/MS.

n .d .

. ! . .;

"'.i;-.. ; *d b' h6 cmou

,no b' e€dM c romar dnoments rd pd 6 hr3 and cot ions b' Lrecl;;;;tmh ;A;ii-6; md :.$-r,sr3ne . reo rE 'n r . ne f l ono -vdFowt i n ' h . 'mbo rca -s iF taon< 3 l ponqb f t v ' r o c iP "d t r sdo* *o , j " t ' o . i * - " " 0 a i r

" mo l imdmb- i 5doo - t ' a t b pno ' l de roo t l a o . i c

( omod i Mv r s ! o zao arasrca o's.ry o' r;sfr-ton ol I e d+n d

.-""'.,ii::lliiillr: r l Y"!:1t]:rt"pjrtrg:.11':11j'-

Test Report No.: CE/201313191 DaIe 2013101121 Paoe 7 of 29

CERAMTEC GMBHGESCHAFTSBEREICH MULIIFUNKTIONSKERA[TIK,LUITPOLDSTMBE 15, 91207 LAUF

r[|||tt]llttI|

Test ltem(e) unit Method I'DLResult

LimitNo.l

Chlorof luoroc€6on-216 (CAS No.l661-97-2)

mg/Kg With reference to US EPA 5021method. Analysis was perfomed byGC/tUS.

1 n.d.

Chlorof luoroca6on-217 (CAS No.:422-E&6)

mg/kg With referenc€ to US EPA 5021method. Analysis was performed byGC/t S.

1 n.d.

HCFCa(Hydrochlorofl uorocalbons)HCFC-21 (CAS No.: 75434) mg/Kg With reference to US EPA 5021

method. Analy6is was performed byGC/MS.

I n.o,

HCFC-22 (CAS No.: 75-45$) mg/Kg Wilh reference to US EPA 502'1method. Analysis was pertormed byGC/MS.

'I n.d.

HCFC-31 (CAS No.: 593-70-4) mg/Kg With reference to US EPA 5021method. Analysis u/as performed byGC/MS.

'I n.d.

HCFC-121 (CAS No.: 354-14-3) mg/Kg With refefence to US EPA 5021method. Analysis was performed byGC/MS.

'I n.d.

HCFC-122 (CAS No.: 354-21-2) m!/Kg With reference to uS EPA 5021method. Analysi6 was pedormed byGC/MS.

1 n.d.

HCFC-123 {CAS No.: 306-83-2) mg/Kg With refere.ce to US EPA 502 1method. Analysis was performed byGC/rVlS.

1 n.d.

HCFC-124 (CAS No.: 2837-89-0) mg/Kg With reference to US EPA 5021method. Analysis rvas performed byGC/tVS.

n.d.

HCFC-13'1 (CAS No.r 359-28.4) mg/Kg With reference to US EPA 5021method. Analysis was pedormed byGC/tVS.

n.d.

HCFC-132b (CAS No.: 1649-08-7)mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.

n.d.

-nn.'"iJ'""r

" **o

"iuie coma;";b,*

"iGa*eft codod'"s"1eor'sode' .s5i-ier-'-,nd rtro 5b

i J6 i i " oJ . i t i j a ' . i ' . n " , ' " ' , qa i 6 re - , ddod id ' b 'F3ad i , { do ' *La€ - . d t ?n &

rhermed b deiudio onl! d{sh F. aborc ens'n{rdo'' ' l;;;;" b; ;;-ii!i;,;. ilis i; ;'q;,r"";, iir" r*a;m;ry ay lmdb';d *sdon. ro@ery o, disddoi dr he 6n,ent o

Test Report No.: CE/2013/13191 Date:2013101121 Page: 8 of 29

CERAMTEC GMBHGESCHAFTSBEREICH MULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE 15, 91207 LAUF

rll |ltt][ttllll

Test liem(s) Unit Method MDLResult

LimitNo.'l

HCFC-133a (CAS No.: 75-88-7) mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/t S.

n.cl.

HCFCI4lb (CAS No.: 1717-00€) mgKg With reference to US EPA 5021method. Anaiysis was performed byGC/MS.

I n.d.

HCFC-142b (CAS No.: 75-68-3) mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.

1 n-d.

HCFC-221 (CAS No.: 422-264) mg/kg With reference to US EPA 502 1method. Analysis was performed byGC/l\rs.

1 n.d.

HCFC-222 (CAS No.r 422-49-1) mg/Kg With reference to US EPA 5021melhod. Analysis was performed byGC/MS.

1 n.d-

HCFC-223 (cAs No.: 422-526) mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.

'I n.d.

HCFC-224 (CAS No.: 422-54-8) mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.

1 n.d.

HCFC-22sca (CAS No.: 422-56-0) mg/Kg With reference to US EPA 502'lmethod. Analysis u/as performed byGC/MS.

1 n.d.

HCFC-22scb (CAS No.i 507-55-1) mg/Kg With reference to US EPA 5021method. Analysis was perfomed byGC/MS.

n.d.

HCFC-226 (CAS No.: 431-87-8) mg/Kg With reference to US EPA 502'1method. Analysis wes performed byGC/MS.

n.d.

HCFC-231 (CAS No.r 421-94-3) m9Kg With reference to tJS EPA 502'1method. Analysis was Performed bYGC/[iS.

't n.d.

HCFC-232 (CAS No.: 460-89-9) mg/Kg With reference to US EPA 502 1method. Analysis was Performed bYGC/MS.

1 n.d.

ow. m h's 3s B@. FF ul b ne 3

.;;.";;-", is ,rd b, h c-ps y sD.eq,o 6 Gr6rcdoj:i.,.*,pffii;F"1;f;*&,;:,#"r,,!;ri:\t,itr,:xi{.y;%1"iffT"1_i;j ?;:jli:i:",Sblecl lo rems and @ndhons ftr.,m. o. ar .* dstrnra,o, nd.inedd 'nu*"- "t:lll.lj;;1.;:t*"*;,f;:::*i;;fjl,,". if;ti* ilf,;'"-;le:'i:";i;; -?":ig:";',?lli0,:"ii

* * " " "a - , * ' - " - , - . J i i - a ; l ,mom.EF .do - -a ' 6 fdc r e . , & y l 1 a n 1 o n z e d " s d d , . - ' # i ; ; ; ; : ; ; i ; ; * : l i " ^ r ' r o b r o - d i b ' r e * d b r r l l e ' " ' { r o L h e b n

r\eift peicivft rs/:r";iii i ) i il i i 4firb

Test Report No- : CE/201313191 Date:2013101121 Paoe i gof 29

CERAMTEC GMBHGESCHAFTSBEREICH

rllllllat][ ttltMULTIFUNKTIONSKERAMIK,LUITPOLDSTRAEE 15. 91207 LAUF

Te6t ltem(a) Unit method MDL Re€ultLimit

No.1HCFC-233 (CAS No.: 7125-84-0) mg/Kg With reference to US EPA 5021

method. Analysis wa6 performed byGC/MS.

'I n.d.

HCFC-234 (CAS No.: 425-94-5) mg/Kg With reference to US EPA 5021method. Analysis was perlormed byGC/MS.

1 n.d.

HCFC-235 (CAS No.: 450-92-4) rnglkg With reference to US EPA 5021method. Analysis wEs perfomed byGC/MS.

1 n . d .

HCFC-241 (CAS No.: 666-27-3) mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.

1 n . d .

HCFC-242 (CAS No.r 46063-9) mgag With reference to US EPA 5021method. Analysi6 was performed byGC/MS.

1 n .d .

HCFC-243 (CAS No.: 460$9-5) mgKg With reference to US EPA 502 1melhod. Analysis was perfomed byGC/MS.

1 n.d-

HCFC-244 mg/Kg With reference to US EPA 5021method. Analysis w€s performed byGC/MS.

1 n .d .

HCFC-251 (CAS No.: 421-41-0) mg/Kg With reference to US EPA 502 1method. Analysis was pertormed byGC/MS.

1 n.d.

HCFC-252 {CAS No.: 819-00-1) mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/MS.

'I n.d.

HCFC-253 (CAS No.: 460-35-5) mdkg With reference to US EPA 5021method. Analysis was performed byGC/MS.

n.d.

HCFC-261 (CAS No.: 420-97-3) mg/Kg With reference to US EPA 5021method. Analysis w€s perfomed byGC/MS.

n.d.

HCFC-262 (CAS No.: 421-m-03) mdkg With reference to IJS EPA 5021method. Analysis was performed byGC/MS.

n.d.

I i B . I I l !anv5ub ] . db tGE la | cond lonso ' sed@prn iedowdca i ' ava iab |eon r€

qedb ams sr co-o m\!o' ehdd rinsdidon 'sEs ddd rhere n 6y io &r of b s eumd ; adv 3ad Lh be company s {indino! ar

Test Report No. : CE/201313191 Dale 2013t01t21 paoe | 10 of 29

CERAIVTEC G[/lBHGESCHAFTSBEREICH MULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE 15. 91207 LAUF

rtrr lrt][ttt||l

Tegt ltem(s) unit Method MDL ResultLimitNo.1

HCFC-271 (CAS No.r 430-55-7) mg/Kg With reference to US EPA 5021method. Analysis was perfomed byGC/MS.

1 n .d .

HalonsHalon-1211 (CAS No.: 353-59-3) mg/Kg With reference to US EPA 5021

method. Analysis wEs performed byGC/MS.

1 n.d.Halon-1301 (CAS No.: 75-63-8) mg/Kg 1 n.d.Halon-2402 (CAS No.: 124-73-2) mg/Kg 1 n.d.CHCs (Chlorinate hydrocarbon)1, 1, 1,2-Tetrachloroelhane (CASNo.:630-206)

mg/Kg With reference to US EPA 5021melhod. Analysi6 w€s performed byGC/MS.

1 n.d.

'1 , 1 ,'1 -Trichloroethane (CAS No. :71-55€)

mdkg With reference to US EPA 5021method. Analysis w€s performed byGC/MS.

1 n . d .

'1, 1,2,2-Tetrachloroethane (CASNo.:79-34-5)

mgKg With reference to US EPA 5021method. Analysis wa6 perforned byGC/MS.

1 n . d .

1,1,2-Trichloroethane (CAS No.:79-00-s)

mg/Kg With reference to US EPA 5021method. Analysis $/as performed byGC/t\rs.

I n.d.

1,1-Dichloroethane (CAS No.: 7$34-3)

mgKg With reference to US EPA 5021method. Analysis was performed byGC/MS,

,| n .d .

't ,1-Dichloroethene (CAS No.: 75-354)


1 n.d.

1,1-Dichloropropene (CAS No.:5695&6)

mg/Kg With reference to US EPA 5021method- Analysis was performed byGC/tVS.

n.d.

1,2,3-Tichloropropane (CAS No.:96-184)

mdks With reference to US EPA 5021method. Analysis was pedormed byGC/tVlS.

n.d.

'1,2-Dichloroethane (CAS No.:107-06-2)

mgftg With reference to US EPA 5021method. Analysis was performed byGC/l\,!S.

n.d.

LN4r : i F (V r r iw in rn 1 . 1 ' n i l r i i f r : t { J

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CERAMTEC GMBHGESCTIAFTSBEREICH MULTIFUNKTIONSKERAI\4IK,LUITPOLDSTMBE .l 5, 91 207 LAUF

lfl tl|[ tllttl

Test lt€m(s) Unit Method i,DLRegult

LimitNo.l

1,2-Dichloroprcpane (CAS No.:78-87-5)

mg/kg With reference to US EPA 5021method. Analysis wEs perfomed byGC/MS.

1 n.d.

'l,}Dichloropropane (CAS No. :142-2&9)-

mg/Kg With referenc€ to US EPA 5021method. Analysis was performed byGC/MS.

1 n.o.

z,2-Dichloropropane (CAS No.:53+20-7',)

mg/Kg with reference to us EPA 5021method. Analysis wa6 performed byGC/MS.

I n.d.

Carbon tetrachloride (CAS No.i56-23-5)

mgikg Wath reference to US EPA 5021method. Analysis was pertormed byGC/MS.

1 n . d .

Chloroethane (CAS No.: 7$00-3) mg/Kg With reference to US EPA 502 1method. Analysis was porformed byGC/MS.

1 n.d.

Chlorofom {CAS No.: 67-66-3) mg/Kg With reference to US EPA 5021method. Analysis was performed byGC/[rS.

1 n.o.

Chloromethane (CAS No.: 74-87-3)

mg/Kg With reference to US EPA 5021method. Analysis wEs performed byGC/MS.

1 n.d.

cis-1,2-Dichloroethene (CAS No.:15G59-2)

mdkg With reference to uS EPA 5021method. Analysis\ ras pertormed byGC/MS.

1 n . d .

ci6-l,3-Dichloropropene (CAS No.l10061-01-5)

mg/Kg with reference to us EPA 502 1method. Analysis was performed byGC/MS,

1 n.d.

Hexachlorobutadiene (CAS No.i8768-3)


'I n-d.

Methylene Chloride (CAS No.: 75-09-2)

mg/kg With referenc€ to US EPA 5021method. Analysis was performed byGC/MS.

n.d.

Tetrachloroethene (CAS No.: 127-184)

mgI(g With reference to uS EPA 5021method. Analysis was performed byGC/MS,

n.d.

s r lEk t repo ld - r t bs ' s

i ;T f t :k" ' ' ' , . " " " "* - , " . " . " " . " - ; - . " ' " " ' " : . . i " , ' i ' . "s . . *p**"" . i .a 'a-uu"" ' l .osdo!esbA-"e!o 'o 'i * i i " i

" an ' i n t ma r ; i e r c i . r i d . db -em, ' bco r ' . " r ' ' edonLOo@f t1Rd"ms { ' , o -

a1 eas , dco ,d tuo s r8Tseooai ; ; ; ; j b ; i i ; # ; i i " ; ; i ; ; . i " " " ; . ^ d ' * h . * , e ' ' d o . t r | ' 0 r ' a ' ' a d . gh " | - . d k FE ; \ ed on odv and w ,h i d he im so c rems nsMros ' L r v i b i s r r . l a d lF tum"d6;;;(-;;;;;;-;;;;6;i;;oi:a ;; ;;J;, . ;. :ie r,..obidd-.-d -n, oo@r1 d "o 0- re o! @o "oo;#ffi;:p;;;;,-,i;;;:d i;i,;: i;a;t ;iai,n-i;";i h" -"bd

"; r . : r i r ! r ' i ' i t - l r .

Test Report No.:CE/2013/13191 Dale 201310121 Paoe:12 ot 29

CERAMTEC GMBHGESCI-I,AFTSBEREICH

tl| |l lrtl]lIVULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE 15, 91207 LAUF

T€6r ltem(s) Unii method MDLResult

LimitNo.1

trans-1,2-Dichloroethene (CASNo. : 1 56-60-5)


'I n.d.

trans-1,3-Dichloropropene (CASNo.: 10061-02€)

mg/Kg With reference to US EPA 502'method. Analysis was performed byGC/MS.

1 n.d.

Trichloroethylene (CAS No.: 7$.01€)

mg/Kg With refefence to US EPA 5021method. Analysis was performed byGC/US.

'I n.o,

Sum of PBBS mg/Kg

With reference to lEc 62321: 2008 andoertormed bv GC/I\IS.

n.d. 1000lMonobromobiphenyl mg,iKg 5 n.d.Dibromobiphenyl mdkg 5 n .d .Tribromobiphenyl mg/kg 5 n.d.Tetrabromobiphenyl mg/Kg n.o,Pentabromobiphenyl mg/Kg n.d.Hexabromobiphenyl mg/Kg 5 n.d.

Heptabromobiphenyl mgKg 5 n .d .Octabromobiphenyl mg/kg 5 n.d.Nonabomobiphenyl mg/Kg n.d.Decabromobiphenyl mg/Kg 5 n . d .

Sum of PBOE5 mg/Kg n.d. 1000Monobromodiphenyl ether mg/Kg 5 n.d.

Dibromodiphenyl ether mgikg 5 n.d.

Tribromodiphenyl ether mg/Kg 5 n.d.Tetrabromodiphenyl ether mg/Kg 5 n.d.

Pentabromodiphenyl ether mg/Kg 5 n.d.

Hexabromodiphenyl ether mg/kg 5 n.d.

Heptabromodiphenyl ether mg/Kg 5 n.d.

Octabromodiphenyl ether mgKg 5 n.d.

Nonabromodiphenyl ether mg/Kg 5 n.o.

oecabromodiphenyl ether mg/Kg 5 n.d.

i . , ; j i t r : l e t . r \ i

Test Report No. I CE/2013/13191Dale | 2013101121Page : 13 ot 29

CERAMTEC GMBHGESCI-I,AFTSBEREICH iNULTIFUNKTIONSKERAMIK,LUITPOLDSTMBE 15, 9.1207 LAUF

lm[llt rt]I

Not. :'1. mg/kg = ppm | 0.1wt% = loooppm2. n.d. = Not Detecled3. MDL = Method Detection Limit4. "-"= Not Regulated5. - = Qualitative analysis (No Unit)6. N€gative = Undet€ctable / Positive = DetectableT Testing range of asbestos qualitative analysis is from less than 0.1% to 1OO%. The judgment crjterion: asbestos fibers

being found is shown as "Positive'; asbeslos fibers not being found is shown as,'Negative..

PFOS Refe.ence Intormetion : POPS - (EU) 757m10Outlawing PFOS as substances or preparations in concentrations above O.OOl% (lOppm), in s€mi-finished products ofarticle6 or parts at a level above 0.1%(1000ppm), in textiles or other coated materials above 1pg/m,.

3liffJ*:"iT,:'?jil\"ri+iTi:?i,iii)i:;::ii:?i"T::i:rl'!{i'iili:r!':ti,li;'rflf'l"1-'e@rcd@d eed rtur Mhdrp

ii":l"H*;:;rls,:iixs'.9"r;i"'t*;:ffagfi"u;::"^'J:rffis#j:r,x*ir5'Lri!tr:"i3;xlf;,i:;-x'#;%1:"#il";: rd,rll,l'Ti"'4ri,:"-..r-o'in|;n,*..neo,-d .<-'.*"a,doids";, ti;o; tr: dMm{ F;dre 'edsI e (omLnr\ihdin$''iiiiilni.l *'r"i'*ro" on" a"o *ti".m rns or ce.' +.*"i ';q Fe.d",p".v"d"."po"'blv ' 'o r! LrPl' . t r ' ood ̂ " diliil;a; i."- d*o.ri+e

"e;fi;;l!;;;'.;-*o;;&;1.;i;;: 6;s;t ;iaianai,* .r h. -dei, (

Test Report No.:CEl2013l13191 DaIe:2013101121 Page: 14 of 29

CERA['TEC GI,lBHGESCHAFTSBEREICH MULTIFUNKTIONSKERAMIK.LUITPOLDSTRABE'15, 9'1207 LAUF

1 ) These samples were dissolved toblly by pretonditioning method according to belolt/ flow chart.( Cf' te€t method excluded )

Name of the person who made measurement Climbgleat YangName of the person in charge of measurement: Troy Chang

2)3)

SamDle Mderial DioestionAcid

S'teel, copper, aluminum, solder Aqua reqia, HNOr, HCl, HE HzO:

Glass HNOy'HF

Gold, platinum, palladium, ce€mic Aqua regia

Silver HN03

Plastic H,SO., H,O,, HNO3, HCI

Others Added appropriate reagent to totaldiOe6tion

Note- : (1) For non{netallic material, add alkaline digestion reagent and heat to 90'95f(2) For metallic material, add pure water and heat to bdling.

r ! { e * h p e . 4 f t t $ / i i : l i i i r d r i r : l i i 4 3 \ 1

Cutting / Preparation

Sample Measurement

Add appropriate amountof digestion reagent

Acid dige6tion by suitable aciddeoended on different samolematedal (as below table)

Microv/ave digestion withHN03/HCI/HF

Heat to appropriatetemperatuae to erdr€ct

1) Alkal iFusion2) HClto dissolve

Add d iphenyltarbazidefor color development

measute the absotbanceat 540 nm by UV-VIS

Test Report No. ICE/2013i/13191Dele :2013101121Page : 15 of 29

CERAMTEC GMBHGESCHAFTSBEREICH MULTIFUNKTIONSKERAMIK.LUITPOLDSTMBE 1 5. 91 207 LAUF

]tI|tt][tttutl

PFOA/PFOS analytical flow chart of Ultrasonic extraction (LC/MS) procedure

r Name of the person who made me€surement: Roman WongI Name ofthe person in chaqe of measurement Troy Chang

ffi um*m,1*ffit*'r,*ffi*#iHl*gl+rsirti*ffikNdrripd.tvlriw:i/li: ' n ] ': Iiriti33li

r+elo2)r4rD ||e6Orlr??1 ?1

Test Report No. : CE2013l'13'191 Date 201?,10121 Paoe: 16of 29

CERAMTEC GMBHGESCHAFTSBEREICH MULTIFUNKTIONSKERAMIK.LUITPOLDSTRABE 15, 91207 LAUF

lm[tr|| ||tt]t

Data

PCTS analytical flow chert

t Name ofthe petson who made measurement Barry T6engr Name ofthe per6on in charge of measurement: Troy Chang

. i r i { r i c f n r \ i

Test Report No. : CE/2013/13191 Dale : 2013101121 Page : 17 of 29

CEMMTEC GMBHGESCFI,AFTSBEREICH MULTIFUNKTIONSKERA[/lIK,LUITPOLDSTMBE 1 5, 91 207 LAUF

ll] ttJflllafll

PBB/PBDE analytical FLOW CHART

I Name ofthe person who made measurement Roman Wongr Name of the person in charge of measurement Troy Chang

First testing process -----'

Optional screen proce6s ....

Confirmation procegs -.>

[J-"'d;---l--------r-------[s-"-lrj--jr"t""t.-tl-T-

Screen analysis

Sample e)draction/Soxhlet method

Concentrate./DiluteExtEcted solution

Filter

Analysis by GC/lvlS

lssue Report

" " " " " " ' f " " " " " "

a;; . : : ' ' . <we p" 'ed owtd ars dbir oll, :T i ;e1d; : - . ;F ; l ;u . ; " ;o€ ; '6hr 'mdcordb4u i ;n rc : .oo . - . ' l dMa ' jdq |

" ' , , . . - ' * * . . " ' , , " , , " ;r i , i j t i i o is ; ; l *m, - rv - " - ' . ,n " . ,uo |cs '+n ' .d ;n i; a ; i i i i ' . i # a j g . * , g , ' r - ' g t : T o o ] g ! j l o B J n d e l ' 9 ? n % d f ' @ o - 4 k T i 3 d o (

u ' { i;:;; ;;;;r;;: : 'oeft | s 5d|" oo'arc"a -dib'

l i i i ,: r !l I {lii:rri

Test Report No. : CE/2013/13191 Dale:20131O1n1Page : 18 of 29

CERAI,TTEC GI,/lBHGESCHAFTSBEREICH MULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE 15. 91207 LAUF

PCBe analytical flow chart

r Name ofthe person who made measurement Bafiy Tsengr Nameoftheperson incharge of measurcment: Troy Chang

Data

lll |ltt][ttlllt

M ti rhlsresr €Don rerer ont ro be tpdorMtbpembsondrE

rhsiftinmr'a €sid b! lh€ cmoanv eubEci ro 'ls Gne'arcndiions orseruie or ed o6'ldat a$ abeonie ms .M,@iditons lrhand ror € adrof, c romd dntum.nb e 6 e d 6 re' ms and C.d ton s lo' Ered msad.Cond( ons/rerm* Dotuft

d u'is. dion isues derned bere i tuv s Ihe companvs nnd'nqs ari heheo ib i n l e iwn1ono i vandw id i n l he ] im$o l c i e i 1sns1 rc i ons f ; nyTheco Inpas$ |e Iespon3b |ftnsdon rrom err"vnq ri h., adFioftJml' hEoodm"lrConprnJ diy iaLtdzeo arleu on

Test Report No. : CE/2013i13191Dale:2013101121Page : 19 of 29

CERAMTEC GMBHGESCHAFTSBEREICH [/|ULTIFUNKTIONSKERAMIK,LUITPOLDSTMBE 1 5, 91 207 LAUF

Chlorinated Paraffins analytical flow chart

r Name oflhe person who made measurement: Bary Tsengr Nam€ of the person in charge of measuremenl Troy Chang

Data

tl][ || t|:ll]I

a m o € ' : e e e d I i ' 6 r ? o o ' € o' , t . - I . t i ,

i i i i i . i . * . " * . * o " o e c o . o a ; ' ' o d b ' i c s t . | L d d ' o ' ' d . o l , o ' 3 e e * o A d e 3 s 9 J - l;; ;i; ;.;;; ;;;' ;r;. ;;;B &;ed b rems rm cdiGmb 0 Eranrcn( ooom.{ . ar "B {- "o_ .innn;iiri,h ,omnta;.; d :1d'do sr! d,,rd h.r,he ru or r 'n,ei!en, on oi v dnd dbinher+aorcrcn \'ran01"; ; ; ; ; ; ; ; ' ; " ^ n ; ; i ; ; i o i " * o o t a " . ' ' c . * . u " ' * . ' o , ' o o J m ' 6 i I o o J - e { o ' '( dmoa., hr ,rd bo zen ,n4no'

N€r tdFi.[r ri iwri / i i-: ' !: ]. ' i : . r {iLli! l i

Test Report No. : CE/2013/13191D?[e:2013101121Page:20 ol 29

CERAMTEC GMBHGESCHAFTSBEREICH MULTIFUNKTIONSKERAIV]IK,LUITPOLDSTMBE 1 5. 91 207 LAUF

Analysis flow cha.t for determination of Asbe6tos

I Name ofthe person who made measuremenl: Victor KaoI Name of the person in charge of measurementt Wendy Wei

( Reie.ence method: EPA 600/R-93/l 16l

Sampling

Contai ning AsbestovPositive Not conhining Asbesto6/ N€gative

!]l[ttt ltt]l

" i t , 1rh6 do.irm.m E Lsusd s rha com"nd b . l . {on . r .mar o@merb . . ' iF - d re- 'dndco ld ro 's ro Fsa vdm(odor - " -3€Dor_ena

ndemnrca( on and 'LlNd d6 6su6rheriftdl6 d.iwi{on otrlv a qsi r;nrTh?com0anyssercspoi5br'ry'' 'o Lsc'en and'hsdocum.ndt r sdo hma . G ro a r i t e nConpaiy ay unauhdzad a lsrdion

k { 4 r t P ( r y r . e d / i . l : i . i 1 1 i t * j : t j r

Continue when probl€rnsarc encournefed withDS-PLM and/or for quality assurance pufposes

Asbestos identifc€lion by dispetsion stainingpola zed light micrcscope (DS-PLM)

Asbe€tos idenlifcation by X-faydiff raclion speclrometer (XRD)

Test Report No. : CEl2013i/13191 Date : 2013101121 Paae : 21 of 29

CERAI,iITEC GMBHGESCHAFTSBEREICH

!

I

Analytical flow chan of Organic-Tin content

Name ofthe person who made measurement: Ginny ChenName ofthe person in charge of measuremenl Troy Chang

It] tttI[ltr tMULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE 15, 91207 LAUF

ui4s dheNs sbcd hs e$ 6 s,o!.n ,n h'' '6d rcpoi erer o'u.bri€ 3aT?fFr,!".i:i .iii:iif...;r':pd

**d b

"K1 i l ; "1 . , . " ; , , " . * . *# ; " , " . * ' " " ; ' * , . J , * * . '9 {ep ' ' coo ' " l "a ] ' .€ ,bPo1 'a;;.rii;etu .-d oie.- ',oFc6 krsmd hthE,o L] . i i i ' i " ' i n * l "nd6mnid lo ,a t '1 r$oo '9ae ' *nare6 ' : , i , i i "nnn.s i io ; { ' , i .Nsddd'r. t-n:

"i s l;* m. -rv,

" w

3'Ji;::i:,m^'tf:3.'illli'i*:?fJliP','€*":ii#l;iik"," '""doneid-" *vbfi;;;;ih;i6.1eiii"brih" ""

Test Report No.:CE201?'13191 Date:2013101121 Page: 22 of 29

CEMMTEC GIVBHGESCHAFTSBEREICH

rtl ltrt ttlllllMULTIFUNKTIONSKERAI/|IK,LUITPOLDSTRABE 15, 91207 LAUF

PCNS analytical flow chart

r Name ofthe person who made measurement: BarryTsengI Name of the person in charge of measurement; Troy Chang

Data

Test Report No.: CE/201313191 DaIe 2013101121 Paqe: 23 of 29

CERAMTEC GMBHGESCHAFTSBEREICH IVULTIFUNKTIONSKERAMIK.LUITPOLDSTMBE 15. 91207 LAUF

tn[lnl|l l|l]t]

Analytical flow chad of phthalate content

I Name of the person who made measufementr Roman Wongr Name of the pe6on in charge of measurement: Troy Chang

Data

' ' r i n l ! r i r r f t i3 r l ' i

Concentrate./Dilute Extracted solution

An€lysis was perfomed by GC/MS

Test Report No. : CE/2013/13191 Dale : 2013101121

CERAMTEC GMBHGESCIIAFTSBEREICH

Page:24 ol 29

91207 LAUFll| |l!] |lttl

I,IULTIFUNKTIONSKERAMIK,LUITPOLDSTMBE 1 5,

I

I

Formaldehyde analytical flow chart

Name of the pe6on who made measurement: Scott KuN€me of the person in charge of measurement: Troy Chang

I Test Method : US EPA 83154 ' ISO 17226-1 ]

Dala

Derived by DNPH ConcentrateJDilute Extractedsolution

Test Report No. :CE/2013 /13191Dale'.2013101121Page : 25 of 29

Analyais flow chart for determination of PVC In material

CERAMTEC GMBHGESCHAFTSBEREICH MULTIFUNKTIONSKERAI,!IK.LUITPOLDSTMBE 1 5. 9'1 207 LAUF

||]tIltt][t [Il

I

I

Name ofthe person who made measurement: Ginny ChenName of the person in charge of measurement: Troy Chang

Sample analyzed by FTIR

Check wave-number of c-cl bonding

Test Report No. CE2013,/13191 Dale:2O1AO1121 Page : 26 of 29

CERAMTEC GMBHGESCHAFTSBEREICH

|ln[ t][tll]rMULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE 15, 91207 LAUF

II

DBBT analytical flow chart

Name ofthe pe6on who made me€surement Roman WongName ofthe person in charge of measurement: Troy Chang

Dala

. i : r , i l r 1 i l i t - l j

Sample pretreatmenvseparation

Sample extraction by 6oxhlet method

Test Report No.:CEl2013/13191Dale: 2o13lo1nl Page 27 ot 29

CERAI.TTEC GI,/IBHGESCHAFTSBEREICH MULTIFUNKTIONSKERAI/|IK,LUITPOLDSTRABE'1 5, 9'1 207 LAUF

Analytical flow chart of halogen content'1) Name of the oerson vt/t|o made measurement: Rita Chen2) Name of the person in charge of measurement: Troy Chang

||l ||tt]tI|tttll

9fj] iH*"", ';:* ' ' ,*.- '"], ' ' , ;;"...""*.l"i"".-".n.*,." ' '-"*"'.n-.*'."1' ; ; t i ; d f u .bmddmmmE' *oFdhh rsmdcodbn 'b ; ; i . nn . cDo6m{ | J# { , od 'ri,:"luri6'in

'rn,r Ardbs; ;jlnri'n dhatu-.in in i

" l " d* . " - , , " * i ' r . . , so - t "n .c i " . , ; ' ; ' : ;a ; . ; ; ; ' - ; - "F*br ' rv rb c* r id ' '<dc ' -c

r i in i i , " j r . * lo i rua i r " monoodm. . ' i ' doo .ne1rcomoanv try unau,tu'z& abad.,-q.ry * I'kh*- drb-tu;it;iFt€ne or th sdturud smawtu

i. ., + i _ri;\l

lFli33!1

Sample pretreatment / separation

Wdghting and putting sample in cell

Oxygen Bomb Cornbustion / Absorption

Dilution to fixed volume

Analysis was performed by lC

Test Report No. : CE/20'13/13191Dai'e : 2O13101n1 Page : 28 of 29

CERAMTEC GMBHGESCHAFTSBEREICH l/TULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE 1 5, 91207 LAUF

Analytical flow chart ofvolatile organic compounds (VOCS)

I Name ofthe oe6on who made measurement : Chun WuI Name of the person in charge of measurernent : Shinjyh Chen

(Reference method : US EPA 5021)

lfl||tt][ttl||ll

Sample pretreatment

Take sample and put it intoheadspace glassware.

Analy6is was per{ormed by GCYlrs

Test Report No. : CE2013/13191D e: 2013101121Page : 29 of 29

cERAlilTEC GIVBHGESCHAFTSBEREICH MULTIFUNKTIONSKERA[/|IK,LUITPOLDSTRABE 15, 91207 LAUF

'The tested sample/ part is ma*ed by an arrow if ifs shown on lhe photo.'

'* End of Repod "

ll]t ttflll0llll

kNewr i t s i . i vL {$ i , : - : ' . ! r , d r i i i l i l f n r \ i

T€st Report No. SHAEC1216714738 Date: 25 Sep 201 2 Page 1 ol5

ZHEJIANG ASIA GENERAL SOLDERING&BRAZING MATERIAL CO., LTD

XIHU INDUSTRIAL PARK, SANDUN, HANGZHOU CIry' ZHEJIANG, PROVINCE' CHINA

The following 6ample(s) was/were submitted and identified on behalf of the clients as : LEAD-FREE SoLDER

WIRE

SGS Job No. :

Part No. (PN) :

Compositlon :

Date of Sampl€ Received :

Testing Period :

Test R€quested :

Test Method :

T€st Resulb :

Condusion :

Signed for and on b€half ofscs-csTc Ltd.

sP12-028285 - SH

YTW2O6

sno.3Ag0.7ouce

21 Sep 2012

21 s,ep 2012 - 25 SeP 2012

Selected test(s) as requested by client

Please refer to next Page(s)

Please refer to next Page(s).Baa€d on the perfomed tests on submitted samples' the results of Lead'I\rercury, Cadmium, Hexavalent chomium, Polybrorninated biphenyls (PBB)'

Polybrominated diphenyl ethe6 (PBDE) comply with the limits as set by RoHS

Di.ective 201 1/65/EU Annex ll; recasting 200295/EC

/Qv''Fan Jingiie, JJApproved Signatory

.n#ffiffiirmr r* u-ra -td *vot rmrr.t.t t*

tirtDafi$EE|ihtltrorr zxtaoil.t.|.*f,Ertr€€.lt$l ll@3

tErEl@llitldt6!E{ti"clt06t'9 ffior*ofrxr.c+rti el Kr(,-tt)Eaffi 1j!ltor-

iLnlirotllt SOS Otbt4 (aGS 8A)

T€6t Report

Test Results :

Test Pert De€criotion ;

S@rn6n No, SGS Sampl€ lD D6ctiptioi1 SHA12-167147.035 Silvery wire

Rgmarks :(1) 1 mg/kg= I PPm=00001%(2) MDL = Method Deteclion Limit

(3) ND = Not D€teded ( < lrDL )(4) '-' = Not Regulated

RoHS DllBdivs 201 l/85/EU

Test Llethod

No. SHAEC1216714734 Date: 25 Sep 2012 Page 2 o15

with reference to lEc 6232 1 :2008(1) Determination of cadmium by ICP-oEs.(2) Dete.mination of Lead by ICP-oEs(3) Determination of Mercrlry by ICP-OES.(4) Determination of Hexavalent Chromium by Spot test / Colorimetric l\,ethod using UV-Vis(5) Detemination of PBBS i PBoES by GC-[IS.

Test ltem{s)

Cadmium (Cd)

Lead (Pb)

Mercury fig)Hexavalent Chromium (Ci(VD)

Sum of PBBSMonobromobiphenylDibromobiphenylTribromobiph€nylTetrabrornobiphenylPentabromobiPhenYlHe/€bromobiphenylHeptabromobiPhenylOctabromobiphenylNonabromobiPhenylDecabromobiPhenYlSum oI PBDESMonobromodiphenyl ether

Limit UlE l\rDL

100 mdkg 2

1000 ms/kg 2

1000 ms/kS 2o

1000 mS.ftS- mS/kS 5- mdkg 5- mdkS s- mSikS 5- mdks 5- ms/kg 5- mg/kg 5- mdkS 5- msikg 5- mdks 5

1m0 mgftS- mg/KS 5

Ij*tffib D.r. na co{d6 *r I ffi*,Hffi !#,g;"EHT* ###f g"fff ffi Stift Ufiffiffi:ffi

Sffi *ff rffi #ffi*,rx*$'#'ffi *lvl*sm.1m*ts""nr*

ND50ND

N€gativeNDNDNDNDNDNDNDNDNDNDNDNDND

;;bii*hEni-.6fr d tbtk r6tr.{.)r-H

tt-ErrlFYasft.cxd|lt.9|dlcrn zfrlr3 rd€6+1)6r.@ tElEF{lF6tlHit!-2l164@raa it{&aFl@+l -l|.*tr[lt|fte||6+l lr:2@

lr.nD.t o1$.8Gg OrouP (8cgs )

Tes{ Report

Test ltem(s)Dibromodiphenyl etherTribromodiphenyl etherTetrabromodiphenyl etherPentabromodiphenyl elherHexabromodiphenyl etherHeptabromodiphenyl etherOc-tabromodiphenyl etherNonabro.nodiphenyl etherD€cabromodiphenyl ether

thi!

t'ilt,b.aYrbto drchrbrd,Swaon !e3a+1

No. SHAEC1216714738 Date: 25 Sep 2012

UdT MDt @mdkS 5 NDmdkS 5 NDmdkS 5 NDmdkg 5 NOmS/kg 5 NDmSikS 5 NDmg/kg 5 NDmS/kS 5 NDmgkg 5 ND

I ErE {O-Zr)OtrOO*FA)ala@!.a

Page 3 of 5

raEFaFffiTl|{j{l.?J)6r@

Notes :(1) The maximum permissible limit is quoted from diredive 2011/65/EU, Annex ll(2) ospot{est:

Negative = Absence of Cr(Vl) coating, Positive = Presence of Cr(Vl) coating;CIhe tested sample should be fudher verifed by boiling-waterextraction method if the spot test resultis Negative or cannot be confirmed.)oBoiling-wateFextraction:Negative = Ahsence of Cr(Vl) coatingPositive = Pesence of Cr(Vl) coating; the detected concentration in boiling-water-ext€ction solution isequal or greater than 0.02 mgl(q with 50 cm'z sample surtace area.For corrosion protection coatings on metals: Information on storage conditions and produclion date ofthe tested sample is unavailable and thus results of Cr(Vl) represent status of lhe sample at the timeof testing.

M.m!.rorh.scsGtuc(acgs )

Test Report No. SHAEC1216714734 Date: 25 S€p 2012 Page 4 of 5

' l ' ;-;Ltidbd$rffi '-d6.h*lhE.,nrdri*6

ATTACHMENTS

RoHS Te€ting Flow Chart

1) Name of the person who madetesting: Jan Shi/Yoyo Wang/Allen Xiao/Gary xu2i Name of the berson in charge of testing: Jeff Zhang/George Xu/ Linda Liiiiii,"i !!rir!!,i. aissoried totarry 6'y pre-condit-roningherhod accorcting to berowflow chart. (Cf '

and PBBdPBDES test method excluded)

tr

Sample Prcparation

Sample Measurement

Acid digestion withmicrow€ve/ hotplate

Concentration/Dilution of extraclion

solution

'1) Alkali Fusion /DryAshing

2) Acid to dissolve

Adding 1,sdiphenylcarbazide


A red colorindicatesthe

presence of cP'.neceas€ry,confirm with

Pbrcd,Hg PB86fPBDE8

tilairl$gYb.rto dErloat4ltrtracnr 20(43fl..tjt.*Iqldl|6els+l a|lM

rEtE Fzr)0tac53l+{a-a)dlqaa

rE&&4lrsartjF.?1)6@

$6nb.fol th.ao6 GlDlD {8oas )

Test Report

Sample photo:

No. SHAECl2'16714738 Date: 25 Sep 201 2 Page 5 of 5

sHA12-167147.035

SGS authenticato the photo on original report only'* End of Report ""

(d-l!r. .Dor d6.ccil-iibhihr.ldcn.h,

' | l ! !a|i!!{ l |ddbd',td.lwb|||d4ded

tLlliDl! Bftfiufition 2dEs rElE[6-eDdag6l lElfF2l!ffia *6r*.&rr{&a1}ara@a ttF+lFN .,9d'rt.l.-tr.tl.*tr6l||,|rF|6r+l ll: @3

l|.fiDcrolm. SOS Gtu,D |SOSS ]

SGS Job No. :

oate of sample R€ceived :

T€sting Pedod I

Test Requested i

Test Method :

Test Results :

Conclusion :

Test Report No. CANEC1208305601 Date: 02 Jul 2012 Page 1 ot 5

AIM SOLDER (SHEN ZHEN) CO,,LTD.

BLOCK69.THIRD INDUSTRIAL ZONE,LUOTIAN VILLAGE,SONGGANG TOWN'BAOAN DISTRICT'SZCHINA

The fo owing sampte(s) wasl/verc submitted and identified on behalf of the clients as: soLoER wlRE AlM230

FA.ST CORE H RSA6O5

cP12-030363 - SZ

26 Jun 2012

26 Jun 2012 - 02 Jul 2012

Selected test(s) as requested by client.

Pleasg refer to next page(s).

Please r€fer to next page(s).

Bas€d on the oedormed lests on submitted sampl€s' the results of Lead'Mercury, Cadmium, Hexavalent ctromium, Polybrominated biph€nyls (PBB)'Potybrominated dipheny' ethels (PSDE) comply with the limits as set by RoHSDireclive 2011/65/EU Annex ll; recasting 2002/95/EC

behalf of

Kenny WangApproved Signatory

r"1,"'ii,::r*H.:lili::lli'i.".aI:',1:s*.:,n3!;i?fi1i1':jii:'y:::1si#*ii*eHi"#1#Hlffi:fi:;lji;.ruT1-nffid.'.';rliSlilil{ml:;iin:,trili..rA,'qr.f i'-. j'jgr;'Sr'i**funi:;'lh;il}ir*:id:E"r.*ii-ri"- G.- 'ii"i;iai -' .fi,*ti:jilfl$fr':f*:i#'lt'1'hi'llt#,ff+d#il}i$,fi'$*iqffi}il'l*:}iil*rd"jr":ii'r"'ir*ilj-'

stdltRe(srtdrPrrotsd EoEildridi.srioidot9dpD 510€53 r (35-2013?i5lt55 I 136-20 32015113

Test Report

Test Results :

No. CANECl208305601 Date: 02 Jul2012 Page 2 ol5

Test Pat Desciotion :

Sp6dmo.r iao, SGS Sampl€ lD1 CAN12-083056.001

Remaaks :

D6qidionSilvery metal wire

(1) I mg/kg= 1 PPm =00001%

(2) MDL = Method Deteclion Limit

(3) ND = Not Detected ( < MDL )(4) 1' = Not Rogulated

Rol{S Dlrc.ft o 201 1/86/EU

TestMethod: With refefence to IEC 62321:2008(1) Determination ofCadmium by ICP-OES.(2) Determination of Lead by ICP-OES.(3) Determination of Mercury by ICP-OES.(4) Determination of Hexavalent Chromium by Spot test / Colodmetric Method using UV-Vis'(5) Determination of PBBS/ PBoEs by GC-MS

Test ltemls)Cadmium (Cd)Lead (Pb)Merc.ury (Hg)Hexavalent Chromium (C l)

Sum ol PBBSMonobromobiphenylDibromobiphenylTribromobiphenylTetrabromobiphenylPentabromobiphenylHexabromobiphenylHeptabromobiphenylOctabromobiphenylNonabrcmobiphenYlDecabromobiphenylSum of PBDESMonobromodiphenyl elher

!!ni! uli!100 mgfts

1,000 mg/kg''y '.tn1,m0 mg/kg

, mg/Kg- mgkg- mg/Kg- ms&g_ mg/Kg- mgKg- mg/Kg- mgKg- mgfts_ mg/Kg

1,0OO mglkg- mg/Kg

**:5yvr;ir'""^'."1.',r.Ti."":l;:R.:L*i::iif,ffj:ii."il*':.1'^:1::?fi'l#i1;;'*l!:11'd#"iliiffi:i:::*"*[$]ns:'uljillfi-f,-':*nii:;Ti;::.i:.'#1i::ii"-,;Iiizffi;;;:i;;;..;-..":^.t,Ti:fiH#;i.:'::J1'";.,"::'J;::.':;i;:;i",,"..,."",:.::; ,::'i1r":,1:r il.1"j'iil lli,i;^;'.1"'i":::ii::;;1T.'i:'J:! ;,:r' :; i] : ":;":;;; ; " " .ii; ^':::1 "";'i:"':. ""'"il;J :;ii;;;;;ii$,r.T#l'* *:*;i;i*xEiiti:it:tll*.*""*::'":x li:r:fi '.': i: ; iii"'j,'lil'rif,,"iijiTli#*:1'Hi.s1'"J;.1r3"i{ii"Tfs'l'ri*l';:rj::ia*:i:*j,r;9,:::ilsr;:ruil*r:';:1,','."llnl'*'

'oos, on.brriciion or,h. codlnr o

iiili"iri'icu', .. -am r.ry r-

r c a i r ; d ^ m h b b d ^ i o d r o 6 , m

MDL22

901ND78ND

NegativeNDNDNDNDNDNDN DNDN DNDNDNDND

2

;555555555

5

' f 6 {& r5d !5 l f i ! 320 : r .wcs$M

Te61 Report

Test ltem(s)

Dibromodaphenyl etherTribromodiphenyl etherTelrabromodiphenyl etherPenlabromodaphenyl etherH€xabromodaphenyl etherHeptabromodiphenyl etherOclabromodiphenyl etherNonabromodiphenyl ethorDecabromodaphenyl ether

Notes :

No. CANEC1208305601 Date:02 Jul2012 Page 3 ot 5

tiEi! @1NDNDN DN DNDNDNDN DND

!d! t\rplmg/kg 5msiks 5mdkg 5mdks 5mgiks 5mg/kg 5mdts 5mdkg 5mg/kg 5

(1) Tho maximum permissibl€ limit is quoted lrom the directive 2011/65/EU, Annex ll(2)oSPottest:Negative = Absenc€ ofCrVlcoating, Positive = Presence ofCNlcoating;(The tested sample should be tudher verified by boiling'water'enraciion m€thod if the spot test result isNegative or cannot bo @nfimed.)oBoiling-water-e)draction:Negative = Absenoe of CrVl coatingPositive = Presence of CrVl coating; the detected concentEtion in boiling'water-extraction solution asequal or greater than 0.02 mg/Kg with 50 ctn2 s€nple surfaoe a.eaFor corrosion prctection coatings on metals: Information on stoEge conditions and produclion date of thelested sample is unavailable and thus resulls of Cr(Vl) represent status ofthe sample atthe time oftesting.

ffiDtu!'m'tu 5t0€61 teo )0 P t66. 16 20 3.4_i: 3

Test Report No. CANEC1208305601 Dale: 02 Jul2012 Page 4 of 5

ATTACHMENTSRoHS Tesiing FlowChart

1) Name of the person who made testing: Bella Wang / Cutey Yu2) Name of the person in charge oftesting:Adams Yu / Ryan Yang3) These samples were dissolved totally by preronditioning method according to below flow chart

(Cf'and PBBS/PBDEs test method excluded).

;ffi]"'t;lfl[;#;:;i";;;i]ffi;i":]ifil";;i;,;;:;];;;c;;:;ilrv.r"*o*t*lt"a*'.-.o; ' ; ; k . ; i ^ ' n " d h ^ . - i d h . k a i ! r d D ; d o c q n . d 5 : h s d o . ! n e d . a i - i i . - p . o d ! . ' d - c . o l i f u;l,'l:'i:lT;i;;i"J'i;d:i'i'"ii]:;;i;;i l;;;;ii1i,:,i.:;i";:;;i l;::i,::li::-"-:t:::ll':l:.1:::l.l::.'l^:l:?1,".?i.".i:i::ii:.'liFrr.tliror nc''i.llr,eh ! a { od

#r;;;J;"*-h\" -s'ry.;hb'6h"dh.*"b"ro'

Sample Measurement

Nonmetallicmaterial

'l) Alkali Fusion /Dry Ashing

2) Acid tiodissolve

Filtration andpH adjustment

Adding 1,5-diphenylcarbazidefor colordevelopment

Adding 1,5-diphenylcarbazidefor colordevelopment

A red colorindicates thepresence of cpr.lf necessary,crnfirm with

Pb/CdtHg PBBS,PBDEs

Positive

r!0&r!R€(serdrf$orlddEdmrlclteb.4d0ddstdqor 510{63 I 136-20}321t5555 rl3t20)3A7t13

Test Report No. CANEC1208305601 Date: 02 Jul 2012 Page 5 of 5

Sample photo:

cAN12-083056.001

SGS authenticat€ the photo on odginal report only*" End of Report "'

dyr6i6droiscei.,.rcoidtriF:ds w4d&6$bldtrhpraw{5@nrqrnr l id-ondiq!omar .o.!n!nb &bld b fumi.idsd utrddbits$e;drrdhdoh A nhkim.noicork i.d hr8oiai.d5

hiiharmGorcri.d! hnrucronr :idd&id.t.eaiG!b!'!md6irhii ha rmGorcri.d! hnruclonr'hu";ddi, ' '-3s6'h.'s-dddeun.n;rfu.oaren€iadi.cPrcdude{6'lf i i ' ] '*sod

l*dhod;db-h\ii,q.ry.ndw')

TEST REPORT NUMBER: SH AH00346635

AUTHORIZED BY： FOR INTERTEK TESTING SERVICES LTD., SHANGHAI

JACOB LIN GENERAL MANAGER

PAGE 1 OF 11 Intertek Testing Services Ltd., Shanghai

Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233 上海天祥質量技術服務有限公司

上海市宜山路 801 號金陵商務廣場 B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740

www.intertek.com www.intertek.com.cn

APPLICANT: LITTELFUSE,INC. DATE: OCT 29, 2012 800 E. NORTHWEST HWY ATT N: A.DIVIETRO/D.UNTIEDT

SAMPLE DESCRIPTION: ONE (1) SUBMITTED SAMPLE SAID TO BE RED INK. PART DESCRIPTION : INK-RED. PART NUMBER : 425901. DATE SAMPLE RECEIVED : OCTOBER.19, 2012. DATE TEST STARTED : OCTOBER.19, 2012.

***************************************************************************************************************************************************** TESTS CONDUCTED: AS REQUESTED BY THE APPLICANT, FOR DETAILS REFER TO ATTACHED PAGE(S) *****************************************************************************************************************************************************

TO BE CONTINUED


TESTS CONDUCTED





1 ( Ⅰ) Test Result Summary :

Testing Item Result (ppm) Heavy Metal

Cadmium (Cd) content ND Lead (Pb) content ND Mercury (Hg) content ND Chromium VI (Cr6+) content ND

Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND

Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND

(Ⅲ) Test Method:

Testing Item T esting Method R eporting Limit

Cadmium (Cd) content With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Lead (Pb) content With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Mercury (Hg) content With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Chromium VI (Cr6+) content With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer. 1 ppm

Polybrominated Biphenyls (PBBs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MSD and further HPLC confirmation when necessary.

5 ppm

Polybrominated Diphenyl Ethers (PBDEs)


5 ppm

Remark: Reporting limit = Quantitation limit of analyte in sample

************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED





(Ⅳ) Measurement Flowchart:

Test For Cd/Pb/Hg/Chromium (VI)/PBBs/PBDEs Contents Reference Standard: IEC 62321 edition 1.0:2008

REMARKS:

*1: List of appropriate acid： Material Acid added for digestion

Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO 3,HCl,HF Electronics H NO3,HCl,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as detected.

************************************************************************************************************************************************** TO BE CONTINUED

sampling/grinding or cutting

weigh sample and for different

material, digest the sample with

make up with deionized water

Cd/Pb/Hg

analyzed by ICP-OES

weigh sample and add alkaline solution

definite temp.

make up with deionized water and add diphenyl-

carbazide solution

Cr6+

weigh sample and add organic

soxhlet extraction or

solvent extraction

concentrate the extract and make up with organic

PBBs/PBDEs

analyzed by UV-VIS

analyzed by GC-MSD

spot test

get 50cm2 samples

boiling water extraction

metalpolymers / electronics

negative*2

confirm the tested samples are totally

dissolved No

cool and filter the extract


TESTS CONDUCTED





2 ( ) Ⅰ Test Result Summary :

Testing Item Result (ppm) Halogen Content

Fluorine (F) ND Chlorine (Cl) 1000 Bromine (Br) ND Iodine (I) ND

Remarks: ppm = Parts per million = mg/kg ND = Not detected

Responsibility Of Chemist : Leaf Liu

(Ⅲ) Test Method:


Halogen Content With reference to EN 14582:2007 by combustion flask with oxygen and determined by ion chromatography 50 ppm


************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED






Test For Halogen Content Reference Standard： EN 14582

**************************************************************************************************************************************************

TO BE CONTINUED

add absorbent in a combustion flask & place weighed sample in equipment

fill the combustion flask with oxygen

ignite then leave the flask at room temperature

transfer the absorbent into a volumetric flask



analyzed by ion chromatography


TESTS CONDUCTED





3 (A) TEST RESULT SUMMARY:

TESTING ITEM R ESULT(ppm) HBCD (HEXABROMOCYCLODODECANE) ND

REMARKS: ppm = PARTS PER MILLION = mg/kg ND = NOT DETECTED (B) TEST METHOD :

TESTING ITEM TE STING METHOD REPORTING LIMIT

HBCD (HEXABROMOCYCLODODECANE) WITH REFERENCE TO USEPA 3540C, BY SOLVENT EXTRACTION AND DETERMINED BY GC/MS

10 ppm

************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED





MEASUREMENT FLOWCHART:

TEST FOR HBCD (HEXABROMOCYCLODODECANE) CONTENT

************************************************************************************************************************************************** TO BE CONTINUED

WEIGH SAMPLE AND PLACE INTO A THIMBLE

SOXHLET EXTRACTION WITH ORGANIC SOLVENT

CONCENTRATE THE EXTRACT

ANALYZE BY GC-MSD

MAKE UP WITH ORGANIC SOLVENT

TRANSFER THE EXTRACT INTO A VOLUMETRIC FLASK


TESTS CONDUCTED





4 PHT HALATE CONTENT TEST

WITH REFERENCE TO EN14372, BY GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS) ANALYSIS.

LIMIT(%,W/W) TESTED COMPOUND R ESULT (%,W/W) (MAX.)

DIBUTYL PHTHALATE (DBP) ND --- DI(2-ETHYL HEXYL) PHTHALATE(DEHP) ND --- BENZYL BUTYL PHTHALATE (BBP) ND --- SUM OF THREE PHTHALATES ND 0.1

REMARK：THE ABOVE LIMIT WAS QUOTED ACCORDING TO ANNEX XVII ITEMS 51 & 52 OF THE REACH

REGULATION (EC) NO. 1907/2006 & AMENDENT NO.552/2009 FOR PHTHALATE CONTENT IN TOYS AND CHILDREN CARE ARTICLES.

DETECTION LIMIT = 0.01%(W/W) ND = NOT DETECTED


WITH REFERENCE TO CPSC-CH-C1001-09.3, BY GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS) ANALYSIS.

LIMIT(%,W/W) TESTED COMPOUND R ESULT (%,W/W)

(MAX.) DI-BUTYL PHTHALATE (DBP) ND 0.1 DI(2-ETHYL HEXYL) PHTHALATE(DEHP) ND 0.1 BENZYL BUTYL PHTHALATE (BBP) ND 0.1

REMARK：THE ABOVE LIMIT WAS QUOTED ACCORDING TO US CONSUMER PRODUCT SAFETY

IMPROVEMENT ACT 2008 & AMENDMENT H.R.2715 FOR PROHIBITION ON SALE OF CERTAIN PRODUCTS CONTAINING SPECIFIED PHTHALATES.


DATE SAMPLE RECEIVED : OCT.19, 2012 TESTING PERIOD : OCT.19, 2012 TO OCT.23, 2012

************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED





MEASUREMENT FLOWCHART: TEST FOR PHTHALATES CONTENTS (EN14372)

************************************************************************************************************************************************** TO BE CONTINUED

WEIGH SAMPLE AND PLACE IN A THIMBLE

EXTRACTED BY SOXHLET EXTRACTION WITH ORGANIC SOLVENT


ANALYZE BY GC-MSD


Transfer the extract into a volumetric flask


TESTS CONDUCTED





MEASUREMENT FLOWCHART: TEST FOR PHTHALATES CONTENTS (CPSC-CH-C1001-09.3)

************************************************************************************************************************************************** TO BE CONTINUED


EXTRACTED WITH ORGANIC SOLVENT BY ULTRASONIC WATER BATH

ANALYZE BY GC-MSD


TESTS CONDUCTED





**************************************************************************************************************************************************

END OF REPORT This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.








APPLICANT: LITTELFUSE,INC. DATE: OCT 29, 2012 800 E. NORTHWEST HWY ATT N: A.DIVIETRO/D.UNTIEDT

SAMPLE DESCRIPTION: ONE (1) SUBMITTED SAMPLE SAID TO BE GREEN INK. PART DESCRIPTION : INK-GREEN. PART NUMBER : 425907. DATE SAMPLE RECEIVED : OCTOBER.15, 2012. DATE TEST STARTED : OCTOBER.15, 2012.

************************************************************************************************************************************************** TESTS CONDUCTED: AS REQUESTED BY THE APPLICANT, FOR DETAILS REFER TO ATTACHED PAGE(S)

************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED





1 ( Ⅰ) Test Result Summary :

Testing Item Result (ppm) Heavy Metal

Cadmium (Cd) content ND Lead (Pb) content ND Mercury (Hg) content ND Chromium VI (Cr6+) content ND

Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND

Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND

(Ⅲ) Test Method:


Cadmium (Cd) content With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Lead (Pb) content With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Mercury (Hg) content With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Chromium VI (Cr6+) content With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer. 1 ppm

Polybrominated Biphenyls (PBBs)


5 ppm

Polybrominated Diphenyl Ethers (PBDEs)


5 ppm


************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED






Test For Cd/Pb/Hg/Chromium (VI)/PBBs/PBDEs Contents Reference Standard: IEC 62321 edition 1.0:2008

REMARKS:

*1: List of appropriate acid： Material Acid added for digestion

Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO 3,HCl,HF Electronics H NO3,HCl,H2O2,HBF4


************************************************************************************************************************************************** TO BE CONTINUED


weigh sample and for different

material, digest the sample with


Cd/Pb/Hg

analyzed by ICP-OES

weigh sample and add alkaline solution

definite temp.

make up with deionized water and add diphenyl-

carbazide solution

Cr6+

weigh sample and add organic

soxhlet extraction or

solvent extraction

concentrate the extract and make up with organic

PBBs/PBDEs

analyzed by UV-VIS

analyzed by GC-MSD

spot test

get 50cm2 samples

boiling water extraction

metalpolymers / electronics

negative*2

confirm the tested samples are totally

dissolved No

cool and filter the extract


TESTS CONDUCTED





2 ( ) Test Result Summary :Ⅰ

Testing Item Result (ppm) Halogen Content

Fluorine (F) 200 Chlorine (Cl) 650 Bromine (Br) ND Iodine (I) ND


Responsibility Of Chemist : Leaf Liu

(Ⅲ) Test Method:




************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED







**************************************************************************************************************************************************

TO BE CONTINUED









TESTS CONDUCTED





3 (A) TEST RESULT SUMMARY:

TESTING ITEM R ESULT(ppm) HBCD (HEXABROMOCYCLODODECANE) ND

REMARKS: ppm = PARTS PER MILLION = mg/kg ND = NOT DETECTED (B) TEST METHOD :

TESTING ITEM TE STING METHOD REPORTING LIMIT

HBCD (HEXABROMOCYCLODODECANE) WITH REFERENCE TO USEPA 3540C, BY SOLVENT EXTRACTION AND DETERMINED BY GC/MS

10 ppm

************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED





MEASUREMENT FLOWCHART:

TEST FOR HBCD (HEXABROMOCYCLODODECANE) CONTENT

************************************************************************************************************************************************** TO BE CONTINUED

WEIGH SAMPLE AND PLACE INTO A THIMBLE

SOXHLET EXTRACTION WITH ORGANIC SOLVENT


ANALYZE BY GC-MSD


TRANSFER THE EXTRACT INTO A VOLUMETRIC FLASK


TESTS CONDUCTED






WITH REFERENCE TO EN14372, BY GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS) ANALYSIS.

LIMIT(%,W/W) TESTED COMPOUND R ESULT (%,W/W) (MAX.)

DIBUTYL PHTHALATE (DBP) ND --- DI(2-ETHYL HEXYL) PHTHALATE(DEHP) ND --- BENZYL BUTYL PHTHALATE (BBP) ND --- SUM OF THREE PHTHALATES ND 0.1

REMARK：THE ABOVE LIMIT WAS QUOTED ACCORDING TO ANNEX XVII ITEMS 51 & 52 OF THE REACH

REGULATION (EC) NO. 1907/2006 & AMENDENT NO.552/2009 FOR PHTHALATE CONTENT IN TOYS AND CHILDREN CARE ARTICLES.



WITH REFERENCE TO CPSC-CH-C1001-09.3, BY GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS) ANALYSIS.

LIMIT(%,W/W) TESTED COMPOUND R ESULT (%,W/W)

(MAX.) DI-BUTYL PHTHALATE (DBP) ND 0.1 DI(2-ETHYL HEXYL) PHTHALATE(DEHP) ND 0.1 BENZYL BUTYL PHTHALATE (BBP) ND 0.1

REMARK：THE ABOVE LIMIT WAS QUOTED ACCORDING TO US CONSUMER PRODUCT SAFETY

IMPROVEMENT ACT 2008 & AMENDMENT H.R.2715 FOR PROHIBITION ON SALE OF CERTAIN PRODUCTS CONTAINING SPECIFIED PHTHALATES.


DATE SAMPLE RECEIVED : OCT.15, 2012 TESTING PERIOD : OCT.15, 2012 TO OCT.18, 2012

************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED





MEASUREMENT FLOWCHART: TEST FOR PHTHALATES CONTENTS (EN14372)

************************************************************************************************************************************************** TO BE CONTINUED


EXTRACTED BY SOXHLETEXTRACTION WITH ORGANIC SOLVENT


ANALYZE BY GC-MSD

MAKE UP WITH ORGANICSOLVENT

Transfer the extract into a volumetric flask


TESTS CONDUCTED





MEASUREMENT FLOWCHART: TEST FOR PHTHALATES CONTENTS (CPSC-CH-C1001-09.3)

************************************************************************************************************************************************** TO BE CONTINUED

Weigh sample and place in a tube

Extracted with organic solvent by ultrasonic water bath

Analyze by GC-MSD


TESTS CONDUCTED





**************************************************************************************************************************************************


Test Report Number： SHAH0036227401

Authorized by： For intertek testing services Ltd., Shanghai

Jacob Lin General Manager

Page 1 Of 5 Intertek Testing Services Ltd., Shanghai




Applicant： ELSCHUKOM ELEKTROSCHUTZKOMPONENTENBAU Date： JAN 18, 2013 GMBH

GEWERBESTRASSE 87,D-98669 VEILSDORF, GERMANY

Sample Description： Two(2) pieces of submitted samples said to be ： (1) Mixed all kinds of metal substrates. (2) Mixed all kinds of plating layers. Item Name ： Silver Plated & Pure Silver Wires. Item No. ： (B-1) 101.014 -. ----

– silver plated copper wire – Cu, Ag--% (B-2) 101.0131.---- – pure silver wire – Ag 1000 (B-3) 101.0123.0--- – silver plated purest nickel wire – Ni99.98%, Ag1% (B-4) 101.0182.0--- – silver-copper alloy plated copper plated iron nickel alloy wire – ElconD, AgCu5% (B-5) 101.0120.0--- – silver plated constantan wire – CuNi44, Ag5% (B-6) 101.0151.0--- – silver plated copper - nickel 44 alloy wire – CuNi44, Ag10% (B-7) 1050--31.-------- – pure silver strips – Ag 1000 pure

Country Of Origin ： Germany. ************************************************************************************************************************************************************ Tests Conducted：

As requested by the applicant, for details refer to attached page(s). ************************************************************************************************************************************************************

To Be Continued


Tests Conducted





(A) Test result of RoHS Directive： Result

Testing item (1)

Cadmium (Cd) content (mg/kg) ND

Lead (Pb) content (mg/kg) ND

Mercury (Hg) content (mg/kg) ND Chromium (VI)(Cr6+) result (by boiling water extraction on metal) (mg/kg with 50cm2) ND

Result

Testing item (2)

Cadmium (Cd) content (mg/kg) /Plating ND

Lead (Pb) content (mg/kg) /Plating ND

Mercury (Hg) content (mg/kg) /Plating ND

Chromium (VI)(Cr6+) result (by boiling water extraction on metal) (mg/kg with 50cm2) /Plating ND

Remark：mg/kg with 50cm2 = milligram per kilogram with 50 square centimeter

ND = not detected (B) RoHS Requirement：

Restricted substances Limits Cadmium (Cd) 0.01% (100 mg/kg) Lead (Pb) 0.1% (1000 mg/kg) Mercury (Hg) 0.1% (1000 mg/kg) Chromium (VI) (Cr6+) 0.1% (1000 mg/kg)

The above limits were quoted from RoHS Directive 2011/65/EU for homogeneous material.

(C) Test method： Testing item Testing method Reporting limit

Cadmium (Cd) content With reference to IEC 62321 Edition 1.0: 2008, by acid digestion until the tested sample was totally dissolved, and determined by ICP-OES.

2 mg/kg

Lead (Pb) content With reference to IEC 62321 Edition 1.0: 2008, by acid digestion until the tested sample was totally dissolved, and determined by ICP-OES.

2 mg/kg

Mercury (Hg) content With reference to IEC 62321 Edition 1.0: 2008, by acid digestion until the tested sample was totally dissolved, and determined by ICP-OES.

2 mg/kg

Chromium (VI) (Cr6+) content (for metal)

With reference to IEC 62321 Edition 1.0: 2008, by boiling water extraction and determined by UV-VIS Spectrophotometer.

0.02mg/kg with 50cm2

(in testing solution)

Date sample received： Jan.14, 2013 Testing period： Jan.14, 2013 To Jan.17, 2013

************************************************************************************************************************************************************ To Be Continued


Tests Conducted





(D) Measurement flowchart：

Test for Cd/Pb/Hg/Cr (VI)/PBBs/PBDEs contents Reference standard: IEC 62321 Edition 1.0: 2008

Remarks： *1: list of appropriate acid：

Material Acid added for digestion Polymers HNO3,HCL,HF,H2O2,H3BO3 Metals HNO3,HCL,HF Electronics HNO3,HCL,H2O2,HBF4


************************************************************************************************************************************************************ To Be Continued

Sampling/grinding or cutting

Weigh sample and for different material, digest

the sample with appropriate acid*1

Make up with deionized water

Cd/Pb/Hg

Analyzed by ICP-OES

Weigh sample and add alkaline

solution

Definite temp. Extraction

Make up with deionized waterand add diphenyl-carbazide

solution

Cr6+

Weigh sample and add organic

solvent

Soxhlet extractionor

Solvent extraction

Concentrate the extract and make up with organic

solvent

PBBs/PBDEs

Analyzed by UV-VIS

Analyzed by GC-MSD

Spot test

Get 50cm2 samples

Boiling water extraction

Metal Polymers / electronics

Positive*2

Confirm the tested samples are totally

dissolved

No

Cool and filter the extract

Yes


Tests Conducted





************************************************************************************************************************************************************

To Be Continued


Tests Conducted





************************************************************************************************************************************************************

End Of Report This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.

Intertek Consumer Goods GmbH · Würzburger Straße 152 · 90766 Fürth ·

Durch die DAkkS nach DIN EN ISO/IEC 17025 akkreditiertes Prüflaboratorium Die Akkreditierung gilt für die in der Urkunde aufgeführten Prüfverfahren.

Intertek Consumer Goods GmbH Tel.: +49 911 74075 0 Sitz Fürth Geschäftsführer Würzburger Straße 152 Fax: +49 911 74075 30 Amtsgericht Fürth, HRB 5756 Kay Grönhardt 90766 Fürth, Germany [email protected] USt-IdNr. DE169317871 Rainer Mast

Polyfil AG Gina Gregorio Oberallmendstrasse 20A 6300 Zug / Switzerland

Fürth, 2012-12-19 Test report No. FUHL1236936 Testing of a material sample according to the RoHS directive 2011/65/EC Sample description: Ni42Fe58MCu wire; part no. 4500173056; batch 0380.6017 Arrival in lab: 2012-012-04; Period of XRF analysis incl. sample preparation and photo documentation: 2012-12-07 – 2012-12-10 Head of Inorganic Lab: Claudia List Copying this test report is permitted only in agreement with the contracted lab. The test results refer only to the tested item. This report consists of 6 page(s). The test methods signed with * are not listed in the attachment of the accreditation certificate.

Conclusion based on tested item Test order Status testing according to the RoHS directive 2011/65/EC conform° ° Please see overview of test results - Test results see next pages -

Page 2 of 6 page(s) of our test report No. FUHL1236936 dated 2012-12-19

Sample description: Ni42Fe58MCu wire; part no. 4500173056; batch 0380.6017

Intertek Consumer Goods GmbH Tel.: +49 911 74075 0 Sitz Fürth Geschäftsführer Würzburger Straße 152 Fax: +49 911 74075 30 Amtsgericht Fürth, HRB 5756 Kay Grönhardt 90766 Fürth, Germany [email protected] Ust-IdNr. DE169317871 Rainer Mast

nM = non Metal M = Metal cM = composite Material List of component parts:

Sample No. Part No. Material Description

236936 1 M Ni42Fe58MCu wire; part no. 4500173056; batch 0380.6017




Comment

LOD = Limit of Detection

BL = Below Limit OL = Over Limit X = Inconclusive, further test necessary σ = Standard deviation CS = Composite sample

Remark: Results were obtained by EDXRF for primary screening. Additional chemical testing using ICP (for Cd, Pb), AAS (for Hg), IC-UC/VIS (for CrVI) and GC/MS (for PBBs/PBDEs) are recommended, if the concentration exceeds the below warning value according to IEC 62321. Element Unit non - metal metal

Cd mg / kg BL ≤ (70-3σ) < X < (130+3σ) ≤ OL BL ≤ (70-3σ) < X < (130+3σ) ≤ OL Pb mg / kg BL ≤ (700-3σ) < X < (1300+3σ) ≤ OL BL ≤ (700-3σ) < X < (1300+3σ) ≤ OL Hg mg / kg BL ≤ (700-3σ) < X < (1300+3σ) ≤ OL BL ≤ (700-3σ) < X < (1300+3σ) ≤ OL Br mg / kg BL ≤ (300-3σ) < X -- Cr mg / kg BL ≤ (700-3σ) < X BL ≤ (700-3σ) < X

Element Unit composite material

Cd mg / kg LOD < X < (150+3σ) ≤ OL Pb mg / kg BL ≤ (500-3σ) < X < (1500+3σ) ≤ OL Hg mg / kg BL ≤ (500-3σ) < X < (1500+3σ) ≤ OL Br mg / kg BL ≤ (250-3σ) < X Cr mg / kg BL ≤ (500-3σ) < X




1. XRF screening Method: XRF according to IEC 62321:2008*

Sample No. Part No. Pb Hg Cd Crtotal Br Status 236936 1 BL BL BL BL -- conform

Comment: Elements RoHS-limit value Lead (Pb) 1000 mg/kg Mercury (Hg) 1000 mg/kg Cadmium (Cd) 100 mg/kg Chromium VI (Cr VI) 1000 mg/kg Polybrominated Biphenyle (PBBs) 1000 mg/kg Polybrominated Diphenyl ether (PBDEs) 1000 mg/kg

- Flow charts see next page(s) -

Page 5 of 6 page(s) Test procedure


YES

YES

YES

YES

YES

NO

NO NO

NO

NO

samples

metallic materials,

polymer materials,

electronics (PCB / component)

mechanical

sample preparation

mechanical

sample preparation

screening by XRF ?

sample uniform ?

screening procedure

by XRF

chemical test procedure (verification)

various methods (please see verification test

procedure below)

meets limits ?

further testing ?

meets limits ?

pass

entity based conforming

sample

fail

entity based non conforming

sample

pass

entity based conforming

sample

fail

entity based non conforming

sample

non-destructive

sample preparation

Page 6 of 6 page(s) Verification test procedure


Sample Preparation

Sample Measurement

Sample solvent extraction

Concentration/ Dilution of extraction

solution

Filtration

GC/MS

DATA

Acid digestion with microwave / hotplate

Filtration

Residue

Total digestion

Solution

ICP-OES/AAS

DATA

Non-metallic material

Alkaline extraction Adding extraction

solution

Alkaline extraction Heating to 90~95°C

for extraction

Filtration and pH adjustment


for color development

UV-VIS or IC-UV/VIS

DATA

Metallic material

Spot test



for color development

A red color indicates the presence of Cr6+ If necessary, confirm

with UV-VIS or IC-UV/VIS

DATA

Pb/Cd/Hg PBBs/PBDEs Cr6+

Positive

Negative

TEST REPORT NUMBER: SHAH00355836







APPLICANT: LITTELFUSE,INC. DATE: DEC 13, 2012 800 E. NORTHWEST HWY ATTN: A.DIVIETRO/D.UNTIEDT

SAMPLE DESCRIPTION: ONE(1) SUBMITTED SAMPLE SAID TO BE BEIGE POWDER. ITEM NAME : FILLER. PART NO. : 090184. ******************************************************************************************************************************************************

TESTS CONDUCTED: AS REQUESTED BY THE APPLICANT, FOR DETAILS REFER TO ATTACHED PAGE(S)

****************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED





1 (Ⅰ) Test Result Summary：

TESTING ITEM RESULT (ppm)

HEAVY METAL CADMIUM (Cd) CONTENT ND LEAD (Pb) CONTENT ND MERCURY (Hg) CONTENT ND CHROMIUM VI (Cr6+) CONTENT ND POLYBROMINATED BIPHENYLS (PBBs) MONOBROMINATED BIPHENYLS (MonoBB) ND DIBROMINATED BIPHENYLS (DiBB) ND TRIBROMINATED BIPHENYLS (TriBB) ND TETRABROMINATED BIPHENYLS (TetraBB) ND PENTABROMINATED BIPHENYLS (PentaBB) ND HEXABROMINATED BIPHENYLS (HexaBB) ND HEPTABROMINATED BIPHENYLS (HeptaBB) ND OCTABROMINATED BIPHENYLS (OctaBB) ND NONABROMINATED BIPHENYLS (NonaBB) ND DECABROMINATED BIPHENYL (DecaBB) ND POLYBROMINATED DIPHENYL ETHERS (PBDEs) MONOBROMINATED DIPHENYL ETHERS (MonoBDE) ND DIBROMINATED DIPHENYL ETHERS (DiBDE) ND TRIBROMINATED DIPHENYL ETHERS (TriBDE) ND TETRABROMINATED DIPHENYL ETHERS (TetraBDE) ND PENTABROMINATED DIPHENYL ETHERS (PentaBDE) ND HEXABROMINATED DIPHENYL ETHERS (HexaBDE) ND HEPTABROMINATED DIPHENYL ETHERS (HeptaBDE) ND OCTABROMINATED DIPHENYL ETHERS (OctaBDE) ND NONABROMINATED DIPHENYL ETHERS (NonaBDE) ND DECABROMINATED DIPHENYL ETHER (DecaBDE) ND

REMARKS：ppm = PARTS PER MILLION = mg/kg

ND = NOT DETECTED

RESPONSIBILITY OF CHEMIST: DENT FANG / LEAF LIU (Ⅱ) ROHS REQUIREMENT：

RESTRICTED SUBSTANCES LIMITS

CADMIUM (Cd) CONTENT 0.01% (100ppm) LEAD (Pb) CONTENT 0.1% (1000ppm) MERCURY (Hg) CONTENT 0.1% (1000ppm) CHROMIUM VI (Cr6+) CONTENT 0.1% (1000ppm) POLYBROMINATED BIPHENYLS (PBBs) 0.1% (1000ppm) POLYBROMINATED DIPHENYL ETHERS (PBDEs) 0.1% (1000ppm)

THE ABOVE LIMITS WERE QUOTED FROM ROHS DIRECTIVE 2002/95/EC AND AMENDMENT 2005/618/EC FOR HOMOGENEOUS MATERIAL.

****************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED





(Ⅲ) TEST METHOD：

TESTING ITEM TESTING METHOD REPORTING LIMIT

CADMIUM (Cd) CONTENT

WITH REFERENCE TO IEC 62321 EDITION 1.0:2008 IN CLAUSE 8/9/10, BY MICROWAVE DIGESTION UNTIL THE TESTED SAMPLES ARE TOTALLY DISSOLVED AND DETERMINED BY ICP-OES.

2 ppm

LEAD (Pb) CONTENT


2 ppm

MERCURY (Hg) CONTENT WITH REFERENCE TO IEC 62321 EDITION 1.0:2008 IN CLAUSE 7, BY MICROWAVE DIGESTION UNTIL THE TESTED SAMPLES ARE TOTALLY DISSOLVED AND DETERMINED BY ICP-OES.

2 ppm

CHROMIUM VI (CR6+) CONTENT

WITH REFERENCE TO IEC 62321 EDITION 1.0:2008 IN ANNEX C, BY ALKALINE DIGESTION AND DETERMINED BY UV-VIS SPECTROPHOTOMETER.

1 ppm

POLYBROMINATED BIPHENYLS (PBBs)

WITH REFERENCE TO IEC 62321 EDITION 1.0:2008 IN ANNEX A, BY SOLVENT EXTRACTION AND DETERMINED BY GC-MSD AND FURTHER HPLC CONFIRMATION WHEN NECESSARY.

5 ppm

POLYBROMINATED DIPHENYL ETHERS (PBDEs)


5 ppm

REMARK：REPORTING LIMIT = QUANTITATION LIMIT OF ANALYZE IN SAMPLE

****************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED





(Ⅳ) MEASUREMENT FLOWCHART: TEST FOR Cd/ Pb/ Hg/Cr (VI)/ PBBS/PBDES CONTENTS REFERENCE STANDARD: IEC 62321 EDITION 1.0:2008

REMARKS： *1: LIST OF APPROPRIATE ACID： MATERIAL ACID ADDED FOR DIGESTION POLYMERS HNO3,HCL,HF,H2O2,H3BO3 METALS HNO3,HCL,HF ELECTRONICS HNO3,HCL,H2O2,HBF4

*2: IF THE RESULT OF SPOT TEST IS POSITIVE, CHROMIUM (VI) WOULD BE DETERMINED AS DETECTED.

****************************************************************************************************************************************************** TO BE CONTINUED


Weigh sample and for different material,

digest the sample with appropriate acid*1


Cd/Pb/Hg

Analyzed by ICP-OES


solution


Make up with deionized water and add Diphenyl-

carbazide solution

Cr6+

Weigh sample andadd organic

solvent


Solvent extraction


solvent

PBBs/PBDEs

Analyzed by UV-VIS

Analyzed by GC-MSD

Spot test

Get 50cm2 samples



Positive*2


dissolved

No


Yes


TESTS CONDUCTED





(Ⅴ) MEASUREMENT FLOWCHART： TEST FOR HALOGEN CONTENT REFERENCE STANDARD： EN 14582

****************************************************************************************************************************************************** TO BE CONTINUED

Add absorbent in a combustion flask & place weighted sample in equipment

Fill the combustion flask with Oxygen

Ignite then leave the flask at room temperature

Transfer the absorbent into a volumetric flask



Analyzed by Ion Chromatography


TESTS CONDUCTED





2 ( ) Ⅰ Test Result Summary :

Testing Item Result (ppm)

Halogen Content Fluorine (F) ND Chlorine (Cl) 100 Bromine (Br) ND Iodine (I) ND


Responsibility Of Chemist : Grace Wang

(Ⅲ) Test Method:

Testing Item Testing Method Reporting Limit



Date Sample Received : Dec.5, 2012 Testing Period : Dec.5, 2012 To Dec.11, 2012

****************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED







****************************************************************************************************************************************************** TO BE CONTINUED









TESTS CONDUCTED





******************************************************************************************************************************************************










SAMPLE DESCRIPTION: ONE (1) SUBMITTED SAMPLE SAID TO BE WHITE POWDER. ITEM NAME : FILLER. PART NO. : 090187.

***************************************************************************************************************************************************** TESTS CONDUCTED: AS REQUESTED BY THE APPLICANT, FOR DETAILS REFER TO ATTACHED PAGE(S) *****************************************************************************************************************************************************

TO BE CONTINUED


TESTS CONDUCTED







HEAVY METAL CADMIUM (Cd) CONTENT ND LEAD (Pb) CONTENT ND MERCURY (Hg) CONTENT ND CHROMIUM VI (Cr6+) CONTENT ND POLYBROMINATED BIPHENYLS (PBBs) MONOBROMINATED BIPHENYLS (MonoBB) ND DIBROMINATED BIPHENYLS (DiBB) ND TRIBROMINATED BIPHENYLS (TriBB) ND TETRABROMINATED BIPHENYLS (TetraBB) ND PENTABROMINATED BIPHENYLS (PentaBB) ND HEXABROMINATED BIPHENYLS (HexaBB) ND HEPTABROMINATED BIPHENYLS (HeptaBB) ND OCTABROMINATED BIPHENYLS (OctaBB) ND NONABROMINATED BIPHENYLS (NonaBB) ND DECABROMINATED BIPHENYL (DecaBB) ND POLYBROMINATED DIPHENYL ETHERS (PBDEs) MONOBROMINATED DIPHENYL ETHERS (MonoBDE) ND DIBROMINATED DIPHENYL ETHERS (DiBDE) ND TRIBROMINATED DIPHENYL ETHERS (TriBDE) ND TETRABROMINATED DIPHENYL ETHERS (TetraBDE) ND PENTABROMINATED DIPHENYL ETHERS (PentaBDE) ND HEXABROMINATED DIPHENYL ETHERS (HexaBDE) ND HEPTABROMINATED DIPHENYL ETHERS (HeptaBDE) ND OCTABROMINATED DIPHENYL ETHERS (OctaBDE) ND NONABROMINATED DIPHENYL ETHERS (NonaBDE) ND DECABROMINATED DIPHENYL ETHER (DecaBDE) ND

REMARKS： ppm = PARTS PER MILLION = mg/kg

ND = NOT DETECTED

(Ⅱ) ROHS REQUIREMENT： RESTRICTED SUBSTANCES LIMITS



***************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED







HALOGEN CONTENT FLUORINE (F) ND CHLORINE (Cl) ND BROMINE (Br) ND IODINE (I) ND

REMARKS： ppm = PARTS PER MILLION = mg/kg

ND = NOT DETECTED



HALOGEN CONTENT WITH REFERENCE TO EN 14582:2007 BY COMBUSTION FLASK WITH OXYGEN AND DETERMINED BY ION CHROMATOGRAPHY 50 ppm

***************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED









2 ppm

LEAD (Pb) CONTENT


2 ppm


2 ppm



1 ppm



5 ppm



5 ppm


***************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED








***************************************************************************************************************************************************** TO BE CONTINUED





Cd/Pb/Hg

Analyzed by ICP-OES


solution



carbazide solution

Cr6+

Weigh sample andadd organic

solvent


Solvent extraction


solvent

PBBs/PBDEs

Analyzed by UV-VIS

Analyzed by GC-MSD

Spot test

Get 50cm2 samples



Positive*2


dissolved

No


Yes


TESTS CONDUCTED





(Ⅴ) MEASUREMENT FLOWCHART： TEST FOR HALOGEN CONTENT REFERENCE STANDARD： EN 14582

*****************************************************************************************************************************************************

TO BE CONTINUED

Add absorbent in a combustion flask & place weighted sample in equipment

Fill the combustion flask with Oxygen

Ignite then leave the flask at room temperature

Transfer the absorbent into a volumetric flask



Analyzed by Ion Chromatography


TESTS CONDUCTED





*****************************************************************************************************************************************************

END OF REPORT

This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.









SAMPLE DESCRIPTION: ONE(1) SUBMITTED SAMPLE SAID TO BE WHITE SAND. ITEM NAME : SAND. PART NO. : 091254.

************************************************************************************************************************************************** TESTS CONDUCTED: AS REQUESTED BY THE APPLICANT, FOR DETAILS REFER TO ATTACHED PAGE(S)

************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED





1 (Ⅰ) TEST RESULT SUMMARY：


HEAVY METAL CADMIUM (Cd) CONTENT ND LEAD (Pb) CONTENT ND MERCURY (Hg) CONTENT ND CHROMIUM VI (Cr6+) CONTENT ND POLYBROMINATED BIPHENYLS (PBBs) MONOBROMINATED BIPHENYLS (MonoBB) ND DIBROMINATED BIPHENYLS (DiBB) ND TRIBROMINATED BIPHENYLS (TriBB) ND TETRABROMINATED BIPHENYLS (TetraBB) ND PENTABROMINATED BIPHENYLS (PentaBB) ND HEXABROMINATED BIPHENYLS (HexaBB) ND HEPTABROMINATED BIPHENYLS (HeptaBB) ND OCTABROMINATED BIPHENYLS (OctaBB) ND NONABROMINATED BIPHENYLS (NonaBB) ND DECABROMINATED BIPHENYL (DecaBB) ND POLYBROMINATED DIPHENYL ETHERS (PBDEs) MONOBROMINATED DIPHENYL ETHERS (MonoBDE) ND DIBROMINATED DIPHENYL ETHERS (DiBDE) ND TRIBROMINATED DIPHENYL ETHERS (TriBDE) ND TETRABROMINATED DIPHENYL ETHERS (TetraBDE) ND PENTABROMINATED DIPHENYL ETHERS (PentaBDE) ND HEXABROMINATED DIPHENYL ETHERS (HexaBDE) ND HEPTABROMINATED DIPHENYL ETHERS (HeptaBDE) ND OCTABROMINATED DIPHENYL ETHERS (OctaBDE) ND NONABROMINATED DIPHENYL ETHERS (NonaBDE) ND DECABROMINATED DIPHENYL ETHER (DecaBDE) ND HALOGEN CONTENT FLUORINE (F) ND CHLORINE (Cl) ND BROMINE (Br) ND IODINE (I) ND

REMARKS：ppm = PARTS PER MILLION = mg/kg

ND = NOT DETECTED

RESPONSIBILITY OF CHEMIST: DENT FANG / LEAF LIU

(Ⅱ) ROHS REQUIREMENT： RESTRICTED SUBSTANCES LIMITS



************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED









2 ppm

LEAD (Pb) CONTENT


2 ppm


2 ppm



1 ppm



5 ppm



5 ppm


************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED








************************************************************************************************************************************************** TO BE CONTINUED





Cd/Pb/Hg

Analyzed by ICP-OES


solution



carbazide solution

Cr6+

Weigh sample and add organic

solvent


Solvent extraction


solvent

PBBs/PBDEs

Analyzed by UV-VIS

Analyzed by GC-MSD

Spot test

Get 50cm2 samples



Positive*2


dissolved

No


Yes


TESTS CONDUCTED





2 ( ) Ⅰ TEST RESULT SUMMARY :

TESTING ITEM RESULT (ppm) HALOGEN CONTENT FLUORINE (F) ND CHLORINE (Cl) ND BROMINE (Br) ND IODINE (I) ND

REMARKS: ppm = PARTS PER MILLION = mg/kg ND = NOT DETECTED

RESPONSIBILITY OF CHEMIST : GRAVE WANG

(Ⅲ) TEST METHOD:


HALOGEN CONTENT WITH REFERENCE TO EN 14582:2007 BY COMBUSTION FLASK WITH OXYGEN AND DETERMINED BY ION CHROMATOGRAPHY

50 ppm

REMARK: REPORTING LIMIT = QUANTITATION LIMIT OF ANALYTE IN SAMPLE

DATE SAMPLE RECEIVED : DEC.5, 2012 TESTING PERIOD : DEC.5, 2012 TO DEC.7, 2012

************************************************************************************************************************************************** TO BE CONTINUED


TESTS CONDUCTED





(Ⅳ) MEASUREMENT FLOWCHART:

TEST FOR HALOGEN CONTENT REFERENCE STANDARD： EN 14582

**************************************************************************************************************************************************

TO BE CONTINUED









TESTS CONDUCTED





**************************************************************************************************************************************************

END OF REPORT


Test Report Number : TWNC00296620

Authorized by: On Behalf of Intertek Testing Services Taiwan Limited

K. Y. Liang Director

*THJ0296620* Page 1 of 8

Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.

全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

Applicant: Elschukom Elektroschutzkomponentenbau Date : Jan 30, 2013 GmbH

Gewerbestrasse 87, D-98669 Veilsdorf, Germany

Sample Description: One (1) group of submitted samples said to be : Sample Description :Tin plated Wires Style / Item No. :Please see page two to three. Country of Origin :Germany Date Sample Received :Jan 23, 2013 Date Test Started :Jan 23, 2013

Test Conducted :

As requested by the applicant, for details please refer to attached pages.




*THJ0296620* Page 2 of 8



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

Sample Description: Style / Item No. :(A-1)101--271.0---

– tin plated copper wire – Cu, Sn--% (A-2)101--283.0--- – tin plated, copper plated copper nickel alloy wire – Elcon30, Sn--% (A-3)101--272.0--- – tin plated, copper plated steel wire – ElconF, Sn--% (A-4)101--281.0--- – tin plated, copper plated iron nickel alloy wire – ElconD, Sn--% (A-5)101--221.0--- – tin plated copper nickel alloy wire - CuNi44, Sn--% (A-6)101--24-.0--- – tin plated, silver plated copper wire – Cu, Ag--%, Sn--% (A-7)101--257.0--- – tin plated brass wire – Cu80Zn20, Sn--%




*THJ0296620* Page 3 of 8



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

Sample Description: Style / Item No. :(A-9)101--234.0---

- tin plated silver copper alloy wire – AgCu90, Sn--% (ElCu90, Sn--%) (A-10)101--255.---- – tin plated copper zinc alloy wire – Cu70Zn30, Sn--% (A-11)101--229.---- – tin plated copper nickel alloy wire – CuNi12, Sn--% (A-12)101--235.---- – tin plated silver copper alloy wire – Ag72Cu28, Sn--% (A-13)101--231.---- – tin plated silver wire – Ag1000, Sn--% (A-14)101--236.---- – tin plated silver copper alloy wire – Ag45Cu55, Sn--%(AgCu55, Sn) (A-15)101--266.---- – tin plated silver copper alloy wire – AgCu70, Sn--%(ElCu70, Sn) (A-16)101--238.---- – tin plated silver copper alloy wire – AgCu80, Sn--%(Elcu80, Sn) (A-17)101--228.0--- – tin plated tungsten wire – W, Sn

Number : TWNC00296620

Test Conducted

*THJ0296620* Page 4 of 8



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

(Ⅰ) Test Result Summary: Result

Test Item Unit Test Method Mixed all kinds of metal wire

RL

Heavy Metal

Cadmium (Cd) content ppm

With reference to IEC 62321: 2008, by microwave digestion and determined by ICP-OES.

ND 2

Lead (Pb) content ppm


37 2

Mercury (Hg) content ppm


ND 2

Chromium VI (Cr6+) content mg/kg with 50 cm2

With reference to IEC 62321: 2008, by boiling water extraction and determined by UV-Vis Spectrophotometer.

Negative (#)

0.02

Remarks: ppm = parts per million based on weight of tested sample = mg/kg

ND = Not detected

RL = Reporting Limit, Quantitation limit of analyte in sample mg/kg with 50cm2 = milligram per kilogram with 50 square centimeter

Negative = A negative test result indicated positive observation was not found at the time of Test. When the spot test showed a negative result, the boiling water extraction procedure shall be used to verify the result.

# = Due to the insufficient sample area, reduced total sample surface of10 cm2 was used and the dilution factor was adjusted accordingly.

Responsibility of Chemist: Kevin Liu/ Irene Chiou Date Sample Received : Jan 23, 2013 Test Period : Jan 23, 2013 To Jan 29, 2013


Test Conducted

*THJ0296620* Page 5 of 8



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

(Ⅱ) RoHS Limits: Restricted Substances Limits

Cadmium (Cd) content 0.01% (100ppm)

Lead (Pb) content 0.1% (1000ppm)

Mercury (Hg) content 0.1% (1000ppm)

Chromium VI (Cr6+) content 0.1% (1000ppm) The above limits were quoted from Annex II of 2011/65/EU for homogeneous material.


Test Conducted

*THJ0296620* Page 6 of 8



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

(Ⅲ) Measurement Flowchart:

Test for Cd/Pb/Hg/Chromium (VI) Reference Standard：IEC 62321 edition 1.0:2008


For different material, digest the sample with appropriate acid*1


Cd/Pb/Hg

Analyzed by ICP-OES

Weigh sample and add alkaline solution

Definite temp. extraction

Make up with deionized water and add diphenyl-carbazide solution


Cr6+

Analyzed by UV-VIS

By spot test

Get 50cm2 sample


Metal Polymers / Electronics

Negative*2 Confirm the tested samples are totally dissolved


Test Conducted

*THJ0296620* Page 7 of 8



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

Remarks: *1: List of Appropriate Acid：

Material Acid Added for Digestion

Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as

detected.

End of Report



Test Conducted

*THJ0296620* Page 8 of 8



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

Photo

Test Report No. SHAECl216714748 Date: 25 Sep 20 1 2 Page 1 of 5

ZHEJIANG ASIA GENERAL SOLDERING&BRAZING MATERIAL CO'' LTD

XIHU INDUSTRIAL PARK, SANDUN, HANGZHOU CITY, ZHEJIANG, PROVINCE' CHINA

The follorving sample(s) wasl/verc submitted and identified on behalf of the clienb as : LEAD'FREE SOLOER

WIRE

sGS Job No. :

Part No. (P/N) :

Composition :

Date ol Sample Received :

Testing Period :

Test Reqlested :

Test Method :

Test Resulb :

Condusion :

sP12-028285 - SH

YTW1o8 (692535-001' 692535-003 )

Sn3.0CuRE21 gep 2012

21 Sep 2012 - 25 seq 20 12

Seleded test(s) as requested by client.


Ple€se refer to next Page(s)Based on the perfrcrmed tests on submitted samples, the results of Lead'

Mercury, cadmium, Hexavalent chromium, Polybrominated biphenyls (PBB)' -Polybrominatecl diphenylethe6 (PBDE) comply with the limits as set by RoHS

Direciive 2011/6tEu Annex lli recasting 200295/EC.

Signed for and on behalf ofsc$csrc Ltd.

,zQv"-Fan Jingjie, JJApproved Signatory

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Teet Report

Test Resufts :

No. SHAEC1216714748 Date; 25 Sep 2012 Page 2 of 5

Test Part Desc.iption :

SpodmqrNo. SGSSandolD D*qiptlon1 SHA'12167147.041 Silvery wire

Rema*€ :(1 ) I mg /kg= 1 PPm=00001%(2) MDL = Method Detedion Limit

(3) ND = Not Detected ( < NIDL )(4)

"" = Not Regulated

RoHS Diradv€ 201 1/65/EU

Test Method : with reference to lEc 62321i2008(1) Determination of Cadmium by ICP-OES.(2) Oetemination of Lead by ICP-oES(3) Determination of Merdiry bv ICP'OES(4) Determination of Hexavalent Chromium by Spot test / Colorimetric Method using UV-Vis

(5) Determination of PBBS / PBDES by GC-MS'

Test ltem(s)

Cadmium (Cd)

Lead (Pb)

Mercury (Hs)

Hexavalent Chromium (Cr(Vl))

Sum ol PBBSMonobrcmobiphenylDibrcmobiphenylTribromobiphenylTetrabromobiPhenylPentabromobiphenYlHexabromobtphenylHeptabromobiPhenylOctabromobiphenylNonabromobiphonylDecabromobiPhenylSum of PBDESMonobromodiphenyl ether

Limit ud! M0!100 mg/kS 2

1000 mSftS 2

1000 mS/kg 2o

1000 mgkg- mSikS 5- mdkS 5- mS/kS 5- ms/ks 5- mdkS 5- mg/kg 5- mg/kg 5- mgftS 5

mdkg 5- mS/kg 5

1000 mS/kg- mdkg 5

@1ND55ND

NegativeNDNDNDNDNDNDNDNDNDNDNONDND

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sGqTest Report

Test ltem{s)

Dibromodiphenyl etherTribromodiphenyl etherTelrabromodiphenyl elherPentabrcmodiphenyl etherHexabromodiphenyl etherHeptabromodiphenyl elherOctabromodiphenyl elherNonabromodiphenyl ethetDecabromodiphenyl ether

Notes :(1) The maximum permissible limit is quoted ffom direclive 2011/65/EU' Annex ll(2) ospoltest:

Negative = Absence of Cr(Vl) coating, Positive = Presence of Cr(Vl) coating;

Ohe tested sample should be further vedfied by boiling-wateFexlraction method if the spot test result

is Negative or cannot be confimed-)oBoiling-wateFextraction:Negative = Absence of Cr(Vl) coatingpositive = Presence of Cr(Vl) coating; the detected concentration in boiling-wateFextraction solution is

equal or greater than O.O2 mg/kg with 50 crn" sample surface areaForcorosionprotectioncoatingsonmeta|s:|nformationonstorageconditionsandproducliondateofthe tested sample is unavailable and thus results of Cr(Vl) represent status of the sample at the time

of testing.

No. SHAEC1216714748 Date: 25 Sep 2012

ud! Mot @1mg/kS 5 NDmS/kS 5 NDmdks 5 NDmSikS 5 NDmg/kS 5 NDmSftS 5 NDmdkS 5 NDmS/kS 5 NDmdkS 5 ND

Page 3 of 5

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Test R€port No. SHAECl216714748 Date: 25 Sep 2012 Pag€ 4 of 5

ATTACHMENTS

RoHS Testing Flow Chart

1) Name of the person who made testing: Jan Shi/Yoyo Wangr'Allen XiaolGaryXu2) Name of the person in charge of testing: Jeff Zhanglceorge Xu/ Linda Li3) These sampleswere dissolved lotally by pre-conditioning method according to betow flow chart. (Cf'

and PBB!,/PBDES test method excluded)

Sample PrepaEtion


2) Acid to dissolve

Heating to 90-957for extraction

Adding 1,5-diphenylcalbaAde


Adding 1,5-diphenylcarbaade


A rcd colorindicatesthe

presence of cr8t.necessary,

Pb/CdHg PBBs/PBDES

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Teet Report

Sample photo:

No. SHAEC1216714748 Oate: 25 Sep 2012 Page 5 of 5

sHA12-167147.041

SGS authenticate the photo on odginal report only

". End of Report '_

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