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Improving Asphalt Content Determination Through Ignition Testing Wednesday, December 6, 2017 2:00-3:30PM ET TRANSPORTATION RESEARCH BOARD
Transcript
Page 1: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

Improving Asphalt Content Determination Through Ignition Testing

Wednesday, December 6, 2017

2:00-3:30PM ET

TRANSPORTATION RESEARCH BOARD

Page 2: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

The Transportation Research Board has met the standards and requirements of

the Registered Continuing Education Providers Program. Credit earned on

completion of this program will be reported to RCEP. A certificate of completion

will be issued to participants that have registered and attended the entire session.

As such, it does not include content that may be deemed or construed to be an

approval or endorsement by RCEP.

Page 3: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

Purpose

Discuss NCHRP Report 847. Learning Objectives

At the end of this webinar, you will be able to: • Identify factors that affect asphalt correction factors • Describe the consequences of sharing correction factors • Identify ways to minimize variability in asphalt correction

factors

Page 4: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

NCHRP Research Report 847: Variability of Ignition Furnace Correction Factors NCHRP Project 09-56

Page 5: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

NCHRP is a State-Driven Program

– Suggest research of national interest

– Serve on oversight panels that guide the research.

• Administered by TRB in cooperation with the Federal Highway Administration.

• Sponsored by individual state DOTs who

Page 6: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

Practical, ready-to-use results • Applied research aimed at

state DOT practitioners • Often become AASHTO

standards, specifications, guides, syntheses

• Can be applied in planning, design, construction, operations, maintenance, safety, environment

Page 7: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

Today’s Speakers

• Carolina Rodezno, Auburn University • E. Ray Brown, Auburn University • Ed Harrigan, Transportation Research Board

Page 8: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

1

Dr. Carolina Rodezno Dr. Ray Brown

December 6, 2017

NCHRP Project 9-56

Page 9: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

2

Outline Project Scope Objectives Background Methodology Results Conclusions Recommendations/Further Research

Page 10: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

3

Project Scope • Literature Review • DOT’s/Industry Survey • Experimental Plan

Phase I

• Conduct Experimental Plan Phase II

• AASHTO Practice • Final Report Phase III

Page 11: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

4

Project Objectives • Determine significant factors that affect asphalt

correction factors (CF) for ignition furnaces to minimize their variability

Evaluate effect of sharing CFs between units • Develop guidelines for installation, operation,

and maintenance of ignition furnaces

Page 12: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

5

Background Accurate determination of AC and aggregate gradation

critical in control of quality of asphalt mixtures during construction

Ignition method per AASHTO T 308 is widely used to determine AC and gradation

Basic Procedure: Oven uses high temp. to burn asphalt off aggregate Procedure terminates when weight of sample stabilizes-

indicating there is no more binder to ignite CF needed to account for difference between known

binder content and ignition test results

Page 13: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

6

Background Types of Ignition Ovens

Convection Units Chamber heated using radiant heat

source-electric heating element-heat air, then sample

Asphalt ignites-blower pulls air into chamber to maintain ignition

Released gases further oxidized while passing out through a secondary chamber

Exhaust is cooled by mixing with air Ovens may have internal balance or

not

Page 14: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

7

Background Types of Ignition Ovens

Infrared Units Infrared heating element to heat

sample Electromagnetic energy waves to

transfer heat energy to sample-stimulating molecules in mix- sample heats furnace by conduction/convection

Troxler units: 3 burning profiles: default, option 1-soft aggregates, option 2-high AC, stone matrix or modifiers

Page 15: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

8

Background Most research studies conducted in mid to late 1990s

and early to mid 2000s during its implementation Evaluated effectiveness, accuracy of new method

(compared to extraction and compared units/brands available)

Studies focused on evaluating variables related with the mix components and not operation

Page 16: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

9

Background Temperature effect (Kowalski et al, 2010) High temp. during ignition produced decomposition

which causes mass loss to continue after binder is burned off

Mass loss f(test temp), higher loss as temp. increases Higher test temperature, sooner oven temperature

exceeded target and sooner temperature peaked Decreasing temperature has a significant effect on mass

loss and rate of mass loss

Page 17: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

10

Background Lime effect (Prowell and Youtcheff, 2000) Hydrated lime has a significant effect on CF Lime addition decreases CF; CF varied from 0.64 with no

hydrated lime to 0.13 with 2% hydrated lime Variability reported large enough to cause non-compliance

with quality control tests according to VDOT’s specifications Description Average CF

Control 5.84 0.64 +0.5% hydrated lime 5.64 0.44 +1 % hydrated lime 5.47 0.27 +2% hydrated lime 5.33 0.13

Page 18: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

11

Background Ignition method (AASHTO T 308) and solvent extraction

(AASHTO T 164) most common methods to measure AC

Condition Standard Deviation

Acceptable Range of Two Tests

T 308 T 164 T 308 T 164 Single Operator

Precision: AC (%) 0.069 0.18 0.196 0.52

Multilaboratory Precision: AC (%)

0.117 0.29 0.33 0.81

Page 19: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

12

Background Share CFs is a practice by some agencies Approach violates AASHTO T 308 which indicates CF

must be established for each mix and ignition unit Some states have aggregates with high mass loss and

don’t allow use of ignition test States like Indiana and Wisconsin have reported

problems with aggregates such as dolomites High CFs result in more variability in measured AC

content

Page 20: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

13

Agency/ Contractor Survey Insight and concerns regarding use of ignition

test 60 agency responses representing 42/50 US

states, 7/10 Canadian provinces and federal lands Additional 37 responses from contractors and 7

responses from testing labs Most respondents use AASHTO T 308 or agency

modification

Page 21: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

14

Ignition Furnace Types

93.3% - use internal balances 56.3% indicated differences in CF with different brands,

models or locations

68.5% 20.2%

5.6%

18.0%

6.7%

2.2%

Thermolyne Series 859/945

Fisher Thermo/Thermolyne Series1087/1275

Troxler 4155 Asphalt Analyzer

Troxler 4730/4731 NTO

Gilson HM-378

Carbolite Asphalt Binder Analyzer

Page 22: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

15

Ages of Furnaces Operated

26.4%

37.4%

51.7%

38.5%

18.7%

< 2 years old

2 - 5 years old

5 - 10 years old

10 - 15 years old

> 15 years old

Range of furnace ages appears to be normally distributed with a median age of 5-10 years

Page 23: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

16

Factors Affecting Ignition Furnace CF 92.2% aggregate type

significant, follow by test temperature, AC content and use of hydrated lime

Samples with higher AC/larger samples →more asphalt to burn → higher peak test temperature

Other factors : RAP/RAS; length of vent pipe, cleanliness of oven, how basket are loaded

92.2%

37.8%

21.1%

14.4%

Aggregate type

Test temperature

Asphalt content

Hydrated lime

Page 24: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

17

Typical Asphalt Content CF Range

Majority indicated CF <1 Some agencies identified CF >1 is common Granite, gravel and limestone most common aggregates

67.4%

49.4%

6.7%

3.4%

<= 0.50

0.51 - 1.00

1.00 - 2.00

> 2.00

Page 25: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

18

Frequency at which CF are Determined/Reevaluated

17.4%

7.0%

8.1%

48.8%

18.6%

Correction factors are not reevaluated

Longer than two years

Once every two years

Once a year

More than once a year

Page 26: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

19

Typical Sample Burn Times

0.0%

9.4%

90.6%

7.1%

> 1 hour 30 minutes

1 hour - 1 hour 30 minutes

30 minutes - 1 hour

< 30 minutes

Page 27: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

20

Installation, Maintenance and Cleaning Issues

2-1200 samples per year-average=285

90 degree elbows avoided, average slightly less than 1

13% hooked multiple furnace to same ductwork

Number of Samples Tested per Year

40.7% 17.3%

21.0%

7.4%

3.7%

8.6%

1.2%

< 100

100 - 200

200 - 400

400 - 600

600 - 800

800 - 1000

> 1000

Page 28: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

21

Areas of Concern with Test Procedure

Only 56/106 respondents answered question; 26 provided comments that range from no problems (majority) to issues with dolomites →Missouri→ no constant mass even at lower temperature

42.9%

39.3%

46.4%

44.6%

35.7%

Long burn times

Smoke from furnace entering lab

Residual asphalt on burned sample

Inconsistent test results

High correction factors

Page 29: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

22

Experimental Plan Objective: Determine significant influences affecting variability of asphalt correction factors Three studies: • Sensitivity Study at NCAT Lab • Round Robin Study(RRS) • Troubleshooting Outliers from RRS

Page 30: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

23

Sensitivity Study at NCAT Lab Objective: Examine different factors to determine which factors influence ignition test results • Identify materials • Identify factors and levels • Display of treatment combination • Conduct tests and statistical analysis

• Linear regression analysis • If p-value≤0.10 regression coefficient is statistically

significant -factor has an effect on test results

Page 31: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

24

Aggregates/Mixes Four Aggregates/Mixes, 12.5mm NMAS; PG 67-22

Aggregate/ Mix

Aggregate Description

Source Expected CF Range

1 Limestone and Granite

Calera, AL – Vulcan Materials

0.0 - 0.5

2 Limestone and Granite with 1% Lime

Calera, AL – Vulcan Materials

0.0 - 0.5

3 Limestone Barbeau, MI – Payne and Dolan

0.5 - 1.0

4 Dolomite Delphi, IN ---USA Aggregates

1.0 - 3.0

Page 32: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

25

Sensitivity Study at NCAT Lab Factors Levels

Ovens Thermolyne, Troxler, Gilson

Test Temperature 800°F, 1000°F (Default, Option 1 for Troxler)

Air Flow 30% Open, 100% Open

Sample Mass 1500 , 2000 grams

AC Content Optimum AC -1%, Optimum AC +1%

Burning Profile (Troxler Only) Default, Option 1, Option 2

Page 33: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

26

Sensitivity Study Results

Page 34: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

27

Mix # Variable Levels Average CF

Statistically Significant

(Y/N)

Practically Significant

(Y/N)

Mix 1

Ignition Unit Thermolyne 0.07

Y Y Troxler 0.12 Gilson -0.03

Temperature 800°F -0.02 Y Y 1000°F 0.12

AC Content Opt. AC -1% 0.10 Y N Opt. AC +1% 0.00 Air Flow, Sample Weight N -

Mix 2

Ignition Unit Thermolyne -0.26

Y N Troxler -0.21 Gilson -0.36

Temperature 800°F -0.33 Y N 1000°F -0.23 Air Flow, AC Content, Sample Weight N -

Factors Affecting Asphalt CF-Mix 1 and 2

Page 35: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

28

Factors Affecting Asphalt CF • Type of oven and test temperature were statistically

and practically significant for mixes 1, 3 and 4 • Reducing test temperature from 1000°F to 800°F

resulted in a lower CF for all mixes except Mix 2 • Air flow was found to be statistically and practically

significant only for Mix 4 • Sample weight and AC content not significant • For Mixes 1, 3 and 4, Gilson resulted in lowest

average CF

Page 36: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

29

Factors Affecting Asphalt CF Test Temperature: Affects AC CF for 7/12 combinations Effect more significant for convection units Decreasing test temperature decreases aggregate

mass loss for all mixes Air Flow (Damper Opening): Affects AC CF for 4/12 combinations Restriction in air flow may cause an increase of

asphalt CF Effect more significant for Troxler

Page 37: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

30

Factors Affecting Asphalt CF

Asphalt Content: Affects AC CF for 3/12 combinations( Mix 3 and 4) Both combinations with Troxler unit Sample Weight: Not significant

Page 38: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

31

Temperature Effect by Mix Type

AC content =Optimum - 1% AC content =Optimum +1%

0.0

-0.5

0.5

1.5

2.5

3.5

Mix 1 Mix 2 Mix 3 Mix 4

800°F 1000°F

-0.5

0.5

1.5

2.5

3.5

Mix 1 Mix 2 Mix 3 Mix 4

800°F 1000°F

Page 39: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

Troxler Only-Burning Profiles Mix # Variable Levels Average CF

Statistically Significant

(Y/N)

Practically Significant

(Y/N)

Mix 1 Profile Default, Option 1,

Option 2 0.11, -0.04,

0.17 Y Y

Mix 2 Burning Profile, AC Content, Sample Weight N ---

Mix 3 Profile Default, Option 1,

Option 2 0.70, 0.64, 0.92 Y Y

Mix 4 Profile Default, Option 1,

Option 2 1.59, 1.27, 2.15 Y Y

• For mixes 1, 3 and 4, Option 2 yielded highest asphalt CF • For mixes 1, 3 and 4 Option 1 resulted in lowest asphalt CF • Change in asphalt CF caused by changing burning profiles was

more pronounced for mix 4

Page 40: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

33

Average Test Time by Mix Type and Test Temperature -Thermolyne

0

20

40

60

80

100

120

140

160

Mix 1 Mix 2 Mix 3 Mix 4 Mix 1 Mix 2 Mix 3 Mix 4

800°F 1000°F

Aver

age

Test

Tim

e (m

in)

Page 41: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

34

Average Test Time by Mix Type and Test Temperature -Troxler

0

20

40

60

80

100

120

140

160

Mix 1 Mix 2 Mix 3 Mix 4 Mix 1 Mix 2 Mix 3 Mix 4

Option 1 Default

Aver

age

Test

Tim

e (m

in)

Page 42: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

35

Average Test Time by Mix Type and Test Temperature -Gilson

0

20

40

60

80

100

120

140

160

Mix 1 Mix 2 Mix 3 Mix 4 Mix 1 Mix 2 Mix 3 Mix 4

800°F 1000°F

Aver

age

Test

Tim

e (m

in)

Page 43: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

36

RRS Experimental Plan

Labs 18 DOT agencies; 5 Contractors/Research

Oven brand 17 Thermolyne, 8 Troxler, 3 Gilson Multi-labs 5 labs with two different oven brands

Number of Mixes Four mixes at their optimum asphalt content

Test temperature 538°C (mixes 1-3) and 482°C (mix 4) for

convection units (Thermolyne, Gilson); default and option 1 for infrared unit(Troxler)

Total Number of Specimens

4 samples x 4 mixes x ( 28 units) = 448 samples; 1500 grams each

Replicates 3 per mix

Objective: Identify CF outliers for further investigation

Page 44: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

37

RRS Results

Page 45: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

38

Data Analysis Test results analyzed per ASTM E 691 k and h statistics to evaluate consistency of results

and possible outliers k=indicator of how laboratory variability compared with that of other labs h=indicator of how laboratory average compared with that of other labs

Critical k and h values recommended in standard Each mix test results analyzed separately

Page 46: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

Asphalt Content CF RRS -Mix 1

-0.8

-0.6

-0.4

-0.2

0

0.2

0.4

0.6

0.8La

b 1-

THLa

b 2-

THLa

b 3-

THLa

b 4-

THLa

b 5-

THLa

b 6-

THLa

b 7-

THLa

b 8-

THLa

b 9-

THLa

b 10

-TH

Lab

11-T

HLa

b 12

-TH

Lab

13-T

HLa

b 14

-TH

Lab

15-T

HLa

b 16

-TH

Lab

17-T

H

Lab

16-G

SLa

b 18

-GS

Lab

19-G

S

Lab

10-T

XLa

b 20

-TX

Lab

17-T

XLa

b 4-

TXLa

b 21

-TX

Lab

22-T

XLa

b 12

-TX

Lab

23-T

X

Thermolyne Gilson Troxler

Asph

alt C

onte

nt C

F

Average=0.11MIn. =-0.66Max.=0.62

Page 47: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

Asphalt Content CF RRS -Mix 2

-0.8

-0.7

-0.6

-0.5

-0.4

-0.3

-0.2

-0.1

0.0

0.1

0.2

0.3La

b 1-

THLa

b 2-

THLa

b 3-

THLa

b 4-

THLa

b 5-

THLa

b 6-

THLa

b 7-

THLa

b 8-

THLa

b 9-

THLa

b 10

-TH

Lab

11-T

HLa

b 12

-TH

Lab

13-T

HLa

b 14

-TH

Lab

15-T

HLa

b 16

-TH

Lab

17-T

H

Lab

16-G

SLa

b 18

-GS

Lab

19-G

S

Lab

10-T

XLa

b 20

-TX

Lab

17-T

XLa

b 4-

TXLa

b 21

-TX

Lab

22-T

XLa

b 12

-TX

Lab

23-T

X

Thermolyne Gilson Troxler

Asph

alt C

onte

nt C

F

Average= -0.23MIn. = -0.67Max.= 0.18

Page 48: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

Asphalt Content CF RRS -Mix 3

0

0.2

0.4

0.6

0.8

1

1.2

1.4

1.6

1.8La

b 1-

THLa

b 2-

THLa

b 3-

THLa

b 4-

THLa

b 5-

THLa

b 6-

THLa

b 7-

THLa

b 8-

THLa

b 9-

THLa

b 10

-TH

Lab

11-T

HLa

b 12

-TH

Lab

13-T

HLa

b 14

-TH

Lab

15-T

HLa

b 16

-TH

Lab

17-T

H

Lab

16-G

SLa

b 18

-GS

Lab

19-G

S

Lab

10-T

XLa

b 20

-TX

Lab

17-T

XLa

b 4-

TXLa

b 21

-TX

Lab

22-T

XLa

b 12

-TX

Lab

23-T

X

Thermolyne Gilson Troxler

Asph

alt C

onte

nt C

F

Average=0.92MIn. =0.55Max.=1.51

Page 49: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

Asphalt Content CF RRS -Mix 4

-2-1.5

-1-0.5

00.5

11.5

22.5

33.5

4La

b 1-

THLa

b 2-

THLa

b 3-

THLa

b 4-

THLa

b 5-

THLa

b 6-

THLa

b 7-

THLa

b 8-

THLa

b 9-

THLa

b 10

-TH

Lab

11-T

HLa

b 12

-TH

Lab

13-T

HLa

b 14

-TH

Lab

15-T

HLa

b 16

-TH

Lab

17-T

H

Lab

16-G

SLa

b 18

-GS

Lab

19-G

S

Lab

10-T

XLa

b 20

-TX

Lab

17-T

XLa

b 4-

TXLa

b 21

-TX

Lab

22-T

XLa

b 12

-TX

Lab

23-T

X

Thermolyne Gilson Troxler

Asph

alt C

onte

nt C

F

Average=1.25MIn. =-1.57Max.=3.58

Page 50: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

k Statistics-Mix 3 (ASTM E 691)

43

Lab 17-TH k value = 2.4> k critical=2.22

0

0.5

1

1.5

2

2.5

3La

b 1-

THLa

b 2-

THLa

b 3-

THLa

b 4-

THLa

b 5-

THLa

b 6-

THLa

b 7-

THLa

b 8-

THLa

b 9-

THLa

b 10

-TH

Lab

11-T

HLa

b 12

-TH

Lab

13-T

HLa

b 14

-TH

Lab

15-T

HLa

b 16

-TH

Lab

17-T

H

Lab

16-G

SLa

b 18

-GS

Lab

19-G

S

Lab

10-T

XLa

b 20

-TX

Lab

17-T

XLa

b 4-

TXLa

b 21

-TX

Lab

22-T

XLa

b 12

-TX

Lab

23-T

X

Thermolyne Gilson Troxler

k St

atis

tics

Critical value =2.22

Page 51: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

h Statistics-Mix 3 (ASTM E 691)

44

-3

-2

-1

0

1

2

3

4

Lab

1-TH

Lab

2-TH

Lab

3-TH

Lab

4-TH

Lab

5-TH

Lab

6-TH

Lab

7-TH

Lab

8-TH

Lab

9-TH

Lab

10-T

HLa

b 11

-TH

Lab

12-T

HLa

b 13

-TH

Lab

14-T

HLa

b 15

-TH

Lab

16-T

HLa

b 17

-TH

Lab

16-G

SLa

b 18

-GS

Lab

19-G

S

Lab

10-T

XLa

b 20

-TX

Lab

17-T

XLa

b 4-

TXLa

b 21

-TX

Lab

22-T

XLa

b 12

-TX

Lab

23-T

X

Thermolyne Gilson Troxler

h St

atis

tics

Critical value =2.63

Critical value =-2.63

Page 52: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

45

Precision Statistics-RRS

Mix # Actual AC%

Average Measured

AC%

Average AC CF

Standard Deviation

W/L B/L

1 5.2 5.32 0.12 0.097 0.117

2 5.2 4.97 -0.23 0.086 0.102

3 6.2 7.08 0.88 0.197 0.212

4 6.1 7.31 1.21 0.345 0.370

AASHTO T 308 0.069 0.117

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46

Troubleshooting Outliers from Round Robin Study

Objective: Team visit labs to conduct additional testing, document specifics about tests to determine reasons for the differences in CF

Mix Lab k-value h-value

1 Lab 4-TX Lab 21 TX

3.4 3.2

3.9 1.7

2 Lab 4-TX Lab 21 TX

4.1 0.4

-2.8 2.66

3 Lab 17-TH 2.4 1.69

4 Lab 16 -GS Lab 21-TX Lab 23-TX

4.6 3.1 1.1

-4.1 4.3 3.0

Critical values 2.22 2.59

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47

TROUBLESHOOTING -LAB VISITS

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48

Lab 4 -Troxler • Results significantly different for Mix 1 and 2 • CF from oven tickets were significantly different from

external weighing • Results obtained from external weighing were found

to be similar to results for other labs

Mix # Average Lab

AC from RRS

Average AC from RRS for Lab 4

AC Average (Manually

weighing on scales outside the

furnace) by NCAT 1 5.32 4.54 5.52 2 4.97 4.53 4.92

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49

Lab 16-Gilson • Higher CF for Lab 16 than for average of all labs for Mix 4 • Gilson unit required to program “preheat” and “burnout”

temperatures. It was suspected that only “preheat” temp. was changed to 482°C and left “burnout” temp. set to 538°C when testing Mix 4

• After adjustments NCAT tests more in line with average lab results Mix #

Measured Average Lab AC

from RRS

Average AC from RRS Lab 16

Average AC Measured During

Lab Visit

Measured AC Average During NCAT Lab Visit

Furnace Set to Incorrect Burnout

Temp

Furnace Set to Correct Burnout

Temp 3 7.08 6.95 NA 6.98 4 7.31 8.80 8.81 7.00

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50

Lab 17-Thermolyne CF Results were higher for Mix 4 than for average of all

labs NCAT results more in line with mean for all labs High results attributed to test error because no issues

with the equipment were found

Mix Average Lab measured AC

from RRS

Average AC measured from

RRS

Average AC Measured During

NCAT Lab Visit

3 7.08 7.08 6.95 4 7.31 7.61 7.30

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51

Lab 19-Gilson • CF Results lower for Mixes 3 and 4 than for average of

all labs • Input parameter for the afterburner temperature was

set to 1000°F, instead of 1562°F • After adjustments NCAT tests yielded higher results

more in line with average of all labs but still low

Mix #

Average Lab measured AC

from RRS

Average measured AC

from RRS for Lab 19

Average AC Measured During NCAT Lab Visit

Afterburner at 1000°F

Afterburner at 1562°F

3 7.08 6.75 6.76* 6.95 4 7.31 6.56 - 6.78

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52

Lab 21-Troxler CF results higher for Mix 3 and 4 than for average of all

labs After results submitted, this lab decided to replace the

unit due to malfunction NCAT tests using new Troxler unit more in line with

results for average of all labs

Mix # Average Lab AC

from RRS

Average AC from RRS for

Lab 21

Average AC Measured

During Lab Visit

3 7.08 7.71 7.12 4 7.31 4.53 7.55

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53

Lab 23-Troxler • CF results for Mix 4 significantly higher than average of

all labs • Programmed “Default” burn profile was incorrect • Research team adjusted burning profile to match factory

profile • NCAT test results using new burning profile much more

in line with average results from all labs.

Mix #

Average Lab AC from RRS

Average AC from RRS for Lab 23

Average AC Measured During NCAT Lab Visit

Original Profile New Profile

3 7.08 7.64 7.76 6.85 4 7.31 9.68 9.93 7.06

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54

Observations from Outlier Study • Equipment was not functioning correctly • Equipment was not set up correctly or test procedures

not followed • Need good procedure to validate proper equipment

operation • Need good guidance for when and how to properly

maintain equipment • Need to participate in routine round robin testing

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55

Installation, Operation, and Maintenance of Ignition Furnace

• Follow Manufacturer’s recommendations for installation, operation, and maintenance

• Very high test temperatures so be safe • Situate furnace so that adequate space for hot baskets • Minimize length of vent (less than 10 feet if possible) • Leaking smoke can be caused by improper seals,

negative pressure in room (caused by hoods), etc • Moisture in mix affects measured asphalt content

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56

Installation, Operation, and Maintenance of Ignition Furnace (Cont’d)

• Allow sample to cool before measuring weight externally • Lime affects the correction factor • Be careful with high AC content mixes such as fine RAP,

RAS, etc. Sample size will likely need to be reduced to prevent overheating furnace once burn begins

• Perform round robin testing to ensure accuracy of measured AC content. This can be done within one lab with multiple pieces of equipment or between multiple labs. Accurately measuring the CF is a bigger problem with high mass loss aggregates

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57

Conclusions • Although not recommended, sharing CF may be possible

when low CF aggregates (say 0.1 to 0.2% or less) are used

Amount of lime has to be closely controlled during production otherwise this will affect the CF and result in incorrect measurement of AC content

For mixes that do not contain lime, test conducted at 800°F significantly reduced asphalt CF, particularly for high mass loss aggregates

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58

Conclusions • Study suggested that different precision statements may

be necessary for aggregates with higher CFs • For mixes 1 and 2 within-lab and between-lab σ

similar to AASHTO T 308 • For mixes 3 and 4 as CF increased σ also increased

It also suggests that precision statement in AASHTO T 308 was developed with low mass loss aggregates and are not applicable to aggregates with higher mass loss

Causes of differences in CF from troubleshooting study were primarily related to wrong equipment settings or other equipment issues

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59

Recommendations/Further Work

Conducting ignition test for RAP materials at 800°F, will allow more accurate determination of the RAP asphalt content which can be difficult since the CF is not known

Key product of this research is a Proposed Standard Practice for Installation, Operation, and Maintenance of Ignition Furnaces

Additional work currently in progress to evaluate effect of reducing test temperature including mixes that contain recycled materials

Page 67: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

60 Courtesy of Timothy Ramirez

Page 68: Improving Asphalt Content Determination Through Ignition ...onlinepubs.trb.org/onlinepubs/webinars/171206.pdf · Improving Asphalt Content Determination Through Ignition Testing Wednesday,

Today’s Participants

• Ed Harrigan, Transportation Research Board, [email protected]

• Carolina Rodezno, Auburn University, [email protected]

• E. Ray Brown, Auburn University, [email protected]

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Get Involved with TRB • Getting involved is free! • Join a Standing Committee (http://bit.ly/2jYRrF6) • Become a Friend of a Committee

(http://bit.ly/TRBcommittees) – Networking opportunities – May provide a path to become a Standing Committee

member • For more information: www.mytrb.org

– Create your account – Update your profile 97th TRB Annual Meeting: January 7-11, 2018

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Get involved with NCHRP

• Suggest NCHRP research topics • Volunteer to serve on NCHRP panels • Lead pilot projects and other

implementation efforts at your agency • For more information:

http://www.trb.org/nchrp/nchrp.aspx

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Take Part in the Careers in Motion Networking Fair

http://bit.ly/CareersInMotionFair


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