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Innovations in Home Care - DKSH...2017/04/28  · B1 Bioterge AS 40 Alpha olefin sulphonate -----...

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Page 1: Innovations in Home Care - DKSH...2017/04/28  · B1 Bioterge AS 40 Alpha olefin sulphonate ----- 3.0 B2 Ammonyx LMDO Lauramidopropylamine Oxide STEPAN 5.0 B3 CAPB Coco Amido Propyl

© DKSHPage 1

Innovations in Home Care

Page 2: Innovations in Home Care - DKSH...2017/04/28  · B1 Bioterge AS 40 Alpha olefin sulphonate ----- 3.0 B2 Ammonyx LMDO Lauramidopropylamine Oxide STEPAN 5.0 B3 CAPB Coco Amido Propyl

© DKSHPage 2

• Premium car wash shampoo

• High gloss car polish

• Leather and vinyl conditioner

• Car freshner gel

• Home Care

• Liquid dish wash detergent

• Dishwash gel

• Bathroom cleaner

• Fabric softener

• Liquid fabric detergent

• Multipurpose cleaner

• Stain remover

• Phenyl white cleaner

Prototypes display at CosmoTech Expo 2019

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© DKSHPage 3

Liquid dishwash detergent

• DKSH key ingredients:

➢ Ammonyx LMDO

(Stepan)

• Key product benefits:

➢ Removes oil and dirt

➢ Controls odor

➢ Deep cleaning

➢ Rich lather

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© DKSHPage 4

Liquid dishwash detergent

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© DKSHPage 5

Ammonyx LMDO

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© DKSHPage 6

Ammonyx LMDO

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© DKSHPage 7

Dishwash gel

• DKSH key ingredients:

➢ Ammonyx LMDO

(Stepan)

➢ Dermothix 100 (Alzo)

• Key product benefits:

➢ Removes oil and dirt

➢ Removes toughest

grease

➢ Easy to use

➢ Deep cleaning

➢ Rich lather

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© DKSHPage 8

All data, formulations and information provided herein have not been comprehensively tested and are not represented as suitable for any particular uses. Statement concerning possible or suggested uses made herein may not be relied upon or be construed as a guaranty of no patent infringement. Users have the sole responsibility and obligation for making preliminary tests to determine the suitability of the sample formulations described herein for any application, to make tests before use in any specific applications, and to confirm the performance, efficacy, safety and regulatory compliance of such products for their particular use.

DKSHIN # DG 12122018

Phase Ingredient INCI Supplier %

A1 Distilled water Water ---- Qs

A2 SLES 28 % Sodium lauryl ether sulphate ----- 75.0

A3 Dermothix 100 Disteareth-100 IPDI Alzo 4

B1 Bioterge AS 40 Alpha olefin sulphonate ----- 3.0

B2 Ammonyx LMDO Lauramidopropylamine Oxide STEPAN 5.0

B3 CAPB Coco Amido Propyl Betain ----- 6.0

B4 CDEA Coco Diethanol amide ----- 1.5

C1 Citric acid Citric acid ---- Qs

C2 Perfume Fragrance ----- 75.0

Description:

Transparent clear viscous thick gel

✓ Removes Oil and Dirt

✓ Controls odour

✓ Deep Cleaning

✓ Rich lather

Key ingredients:

Ammonyx LMDO It is an amine oxide suitable for Cleaning formulations. It is a good Foam booster, grease remover and viscosity builder.

Dermothix 100 It is water soluble dimeric urethane where alcohol is a 100 mole ethoxylated stearyl alcohol. It is non – ionic thickener and rheology modifier.

Procedure:

1 Take total quantity of water, SLES in beaker & add Dermothix- 100 and heat upto 65 degree C

2 Add Bioterge AS 40, Ammonyx LMDO, CAPB & CDEA one by one, stir until all the ingredients are dissolved.

3 Adjust the pH of final product 8 to 9.

4 Pour the product in suitable packaging in liquid stage & keep the product @ RT for setting.

Specification

pH = 8.0

Appearance – Transparent clear viscous thick gel

Stability test : Product has Successfully completed 3 month stability @ 25 deg RT & ETC conditions i.e. 40 deg temp. & 75 % RH as per

Indian standards

DKSH India June 2019

Formulation number:

DKSHIN # DG 12122018

Dishwash gel

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© DKSHPage 9

Ammonyx LMDO

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© DKSHPage 10

Dermothix 100

.AJLZ{)International Inc.

TM75 and DERMDTHIJI™1DD

Solid Solutions forViscosity Control FEATURES • A::>lyurethane A::>lymers

• Broad pHEffectiveness

• Unique RheologyandTexture

• Chemical&ThermalStability

Structure

'

CH

(H

HC IPOI 110

• Exceptional Emulsification

• Solubilizingand Coupling

• EaseofUse

Viscosity Builder for Surfactant Systems

DEBMDIHDI 75

• INCJName: Disteareth-75 lPDI

• Unique o/WEmulsifier

• Water Dispersible Flake

• I00% Active

• Forms Clear to Hazy Solutions

• Soluble in Anionics, Nonionics and cationics

R OCH D1 I 0 C N H C I'> C 01 CH CH 0 R

Oh

Thickening Effects of DERMOTHIX 75 on Common Shampoo Systems

VISCO$ity (cps)

50,000

45,000

40,000

35,000

30,000

25,000

20,POO ---------

15,000

10,000

5,000

Percentage of Emulsifier Versus Percentage of OilPhase

•Conventional Emulsions

• INCJName:Disteareth-100 IPDI

• Water Soluble F1ake

• Nonionic

• Clear VISCous Solutions

• Solublein Anionics.

Emulsifier

15

10

5

0

8DERMOTHIX100 Emulsions

Nonionics and cationics

• Pigment Suspension

• Stable High InternalPhaseo/W Emulsifier

APPUCATIONS

• Shampoos

5 10 15 20 25 30

O Phase

'Y15cosi1Yilulcin& 1 7 1 -

• Sulfate Free Products X + lJrrired

• Conditionersc.taa.tly X X X X

Surfaaont Compaljblicy

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© DKSHPage 11

Bathroom cleaner

• DKSH key ingredients:

• Ammonyx LOA (Stepan)

• Key product benefits:

➢Removes tough stains

➢Removes oïl and grease

➢Disinfectant

➢Controls odor

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© DKSHPage 12

Bathroom cleaner

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© DKSHPage 13

Ammonyx LOA

Page 14: Innovations in Home Care - DKSH...2017/04/28  · B1 Bioterge AS 40 Alpha olefin sulphonate ----- 3.0 B2 Ammonyx LMDO Lauramidopropylamine Oxide STEPAN 5.0 B3 CAPB Coco Amido Propyl

© DKSHPage 14

Multipurpose cleaner

• DKSH key ingredients:

➢ Ammonyx LOA (Stepan)

➢ Ammonyx LMDO

(Stepan)

• Key product benefits:

➢ Removes tough stains

➢ Removes oil and

gease

➢ Gives shine to floor

➢ Disinfectant and

controls odor

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© DKSHPage 15

Multipurpose Cleaner

Multipurpose Cleaner DKSHIN # MC 30082016

All data, formulations and information provided herein have not been comprehensively tested and are not represented as suitable for any particular uses. Statement concerning possible or suggested uses made herein may not be relied upon or be construed as a guaranty of no patent infringement. Users have the sole responsibility and obligation for making preliminary tests to determine the suitability of the sample formulations described herein for any application, to make tests before use in any specific applications, and to confirm the performance, efficacy, safety and regulatory compliance of such products for their particular use.

DKSHIN # MC 30082016

Phase Ingredient INCI Supplier %

A1 Aqua _____ --------- Q.S.

B1 Ammonyx LOA Lauramine

Oxide Stepan 15.0

B2 Ammonyx LMDO Lauramidopropyl

Amine Oxide Stepan 15.0

B3 SLES (28%) Sodium Lauryl

Ether Sulphate --------- 6.0

B4 Sodium Hypochlorite

(4%)

Hypochlorous

Acid, Sodium Salt --------- 6.3

C1 NaOH Sodium Hydroxide --------- 0.1

C2 Nacl Sodium Chloride --------- 0.5

C3 Perfume --------- --------- QS

C4 Color Color Coloring agent QS

Description:

Green Coloured Transparent Clear Liquid

✓ Removes Tough Stains

✓ Removes Oil and Grease

✓ Gives shine to Floor

✓ Disinfectant and controls odour

Key ingredients:

Ammonyx LMDO. It is an amine oxide suitable for cleaning formulations. It is a good Foam booster, grease remover and viscosity builder.

Ammonyx LOA It is a an amphoteric surfactant used in Home Care cleaning applications. It is a good foam enhancer, viscosity builder.

Procedure:

1 Initially take total quantity water & add Ammonyx LOA, Ammonyx LMDO, SLES, Sod.Hypochlorite, in manufacturing vessel

2 Then add NaOH to adjust the pH upto 12.0

3 Then add Nacl to increase product Viscosity

4 Finally add Colour and perfume to above with stirring

Specification

pH = 12.0

Appearance – Gtreen coloured Transparent clear liquid.

Stability test : Product has successfully completed 3 month stability @ 25 deg RT & ETC conditions i.e. 40 deg temp. & 75 % RH as per Indian

standards

DKSH India June 2018

Formulation number:

DKSHIN # MC 30082016

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© DKSHPage 16

Ammonyx LOA and Ammonyx LMDO

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© DKSHPage 17

Stain remover

• DKSH key ingredients:

➢ Steposol Citrimet

(Stepan)

• Key product benefits:

➢ Removes tough stains

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© DKSHPage 18

Stain remover

Stain Remover DKSHIN # SR 13042018

All data, formulations and information provided herein have not been comprehensively tested and are not represented as suitable for any particular uses. Statement concerning possible or suggested uses made herein may not be relied upon or be construed as a guaranty of no patent infringement. Users have the sole responsibility and obligation for making preliminary tests to determine the suitability of the sample formulations described herein for any application, to make tests before use in any specific applications, and to confirm the performance, efficacy, safety and regulatory compliance of such products for their particular use.

DKSHIN # SR 13042018

Phase Ingredient INCI Supplier %

A1 Aqua _____ --------- Q.S.

B2 Steposol Citrimet Steposol Met 10 U, Natural terpene,

emulsifier Stepan 6.67

Description:

Orange Coloured Transparent Clear Liquid

✓ Dissolves wide variety of stains

✓ Cleans glass, carpet & multiple surfaces

✓ Ready for dilution

✓ Household ti industrial applications

Key ingredients:

Steposol Citrimet

Patented technology comes to ready for dilution o meet customer’s specific product needs. It is derived from bio-based sources to provide a greener profile. It covers broad range of applications from household to industrial to institutional.

Procedure:

Firstly weigh water in manufacturing vessel & ass steposol Citrimet with stirring to mixed well.

Specification

pH = 10.1

Appearance – orange coloured Transparent clear liquid.

Stability test : Product has successfully completed 3 month stability @ 25 deg RT & ETC conditions i.e. 40 deg temp. & 75 % RH as per Indian

standards.

DKSH India Dec 2018

Formulation number:

DKSHIN # SR 13042018

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© DKSHPage 19

Steposol Citrimet

STEPOSOL® CITRI-MET is a revolutionary

fully formulated solution that dissolves a

wide variety of stains and provides a

greener clean in both household and

industrial environments.

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© DKSHPage 20

Liquid fabric detergent

• DKSH key ingredients:

➢ Bioterge EC 690

(Stepan)

➢ Stepantex SXS (Stepan)

➢ MEL (Advanced

Enzymes)

• Key product benefits:

➢Dissolves in water

completely

➢Excellent cleaning even

on all types of stains

➢Can be used as a pre

treat stain

➢Much more compact

and easier to use

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© DKSHPage 21

All data, formulations and information provided herein have not been comprehensively tested and are not represented as suitable for any particular uses. Statement concerning possible or suggested uses made herein may not be relied upon or be construed as a guaranty of no patent infringement. Users have the sole responsibility and obligation for making preliminary tests to determine the suitability of the sample formulations described herein for any application, to make tests before use in any specific applications, and to confirm the performance, efficacy, safety and regulatory compliance of such products for their particular use.

DKSHIN # LFD 02042019

Phase Ingredient INCI Supplier %

A1 Aqua _____ --------- Q.S.

A3 NaOH Sodium Hydroxide --------- 1.6

A4 LABSA 90% Alkyl benzene

Sulphonic acid --------- 5,7

B1 Bioterge EC 690 Lauryl alcohol ethoxylate, POE - 7 Stepan 10.0

B2 SLES (28%) Sodium Lauryl

Ether Sulphate --------- 20.0

B3 Stepantex SXS Sodium xylène sulphonater Stepan 1.75

B4 MEL Enzyme blend Advanced enzymes 0.5

B5 NaCl Sodium Chloride ------- 1.0

C1 Perfume Fragrance --------- QS

C2 Color Color --------- QS

Description:

Orange Coloured Transparent Clear Viscous Liquid

✓ Dissolves in water completely

✓ Excellent cleaning even on all stains

✓ Can be used as a pre treat stain

✓ Much more compact & easier to use

Key ingredients:

MEL Blend of enzymes which works on all types of stains.

Stepantex SXS Anionic surfactant used in liquid detergent. It is used as a solubilizer, coupling agent & cloud point dispersant.

Procedure:

1 First add NaOH in water and stir to dissolve it. Then add LABSA With continous stirring, adjust the pH NaoH, Until all nuetralized. ( Buffer solution may vary while adjusting the PH of LABSA solution) to PH-7

2 Add Boterge EC 690, SLES, Stepantex SXS one by one, stir until all ingredients are dissolved

3 Add MEL, Color &stir to Mix well. & adjust the final viscosity with NaCl.

4 Finally add Colour and perfume to above with stirring

Specification

pH = 11.34, Brookfield DV-II+Pro # RV, Viscosity - 408 cps, Spindle -02, Speed - 20 rpm

Appearance – Orange coloured Transparent clear liquid.

Stability test : Product has Successfully completed 3 month stability @ 25 deg RT & 2 weeks @ ETC conditions i.e. 40 deg temp. & 75 % RH

as per Indian standards

DKSH India Apr 2019

Formulation number:

DKSHIN # LDD31012014

Liquid fabric detergent

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© DKSHPage 22

Adclean ME L

AETL/DET/RT/055

AETL/DET/F/003

Detergent Lab Trial Results

Objective:

STUDY OF ADDCLEAN ME L (AETL CUSTOMISED ENZYME BLEND) ON MARKET LIQUID

DETERGENT

Samples: MARKET LIQUID DETERGENT

ADDCLEAN ME L

(MFG. AETL CUSTOMISED ENZYME BLEND)

Treatment Fabric:

(A) EMPA* standard (EMPA soiled fabrics)

Article/Stain code Type

164 Grass

116 Blood/Milk/Ink

106 Carbon / Mineral oil

160 Chocolate

118 Sebum

167 Tea

*EMPA: The Swiss Federal Laboratories for Materials Science and Technology (EMPA, German acronym for

Eidgenössische Materialprüfungs- und Forschungsanstalt) is an interdisciplinary Swiss research institute for applied

materials sciences and technology

Washing parameters:

Parameter Machine wash

Equipment Tergotometer

Detergent dose, g 10.0 & 8.0

Temperature, 0C Room temperature

Time, min. 30

Water, lt. 1.0

Washing Process:

Machine wash 1. Prepare the bath with desired quantity of water and add laundry detergent

2. Start the machine rotor for mixing before adding fabrics

3. Immerse EMPA soiled fabric and run the machine for 30 minutes

4. After 30 minutes remove the fabric from the bath

5. Rinse in clean water for 5 minutes and drain

6. Air dry the fabric and take reading with spectrophotometer

Understanding of CIE L*

& Y color space:

L* is an international standard for color measurements,

adopted by the Commission Internationale d’Eclairage

(CIE) in 1976.

▪ L*

is the luminance or lightness component,

which ranges from 0 (Black) to 100 (White),

▪ Y gives significant value of luminance (Y

ranges from 1 to 100 indicates brightest white)/

directly related to stain removing efficiency.

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© DKSHPage 23

Adclean ME L

AETL/DET/RT/055

AETL/DET/F/003

BLOOD/ MILK/ INK

A) CONTROL

B) MARKET LIQUID

DETERGENT

C) MARKET LIQUID

DETERGENT (100%) + 0.50

% ADDCLEAN ME L

D) MARKET LIQUID

DETERGENT (80%) + 0.50

% ADDCLEAN ME L

Parameter L* Y

Whiteness

(CIE)

Brightnes

s (%ISO)

Control 43.92 13.78 -26.03 12.37

Market Liquid Detergent 72.21 43.97 37.02 43.12

Market Liquid Detergent

(100%) + 0.50 % Addclean

ME L

77.37 52.15 43.03 50.82

Market Liquid Detergent

(80%) + 0.50 % Addclean ME L

75.41 48.94 39.65 47.68

AETL/DET/RT/055

AETL/DET/F/003

TEA

A) CONTROL

B) MARKET LIQUID

DETERGENT

C) MARKET LIQUID

DETERGENT (100%) + 0.50 % ADDCLEAN ME L

D) MARKET LIQUID

DETERGENT (80%) + 0.50 % ADDCLEAN ME L

Parameter L*

Y Whiteness

(CIE)

Brightnes

s (%ISO)

Control 72 43.66 -69.23 29.05

Market Liquid Detergent 79 54.92 -17.34 42.89

Market Liquid Detergent

(100%) + 0.50 % Addclean

ME L

77.89 53.02 -27.24 40.18

Market Liquid Detergent

(80%) + 0.50 % Addclean

ME L

78.05 53.3 -23.53 40.94

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© DKSHPage 24

Fabric softener

• DKSH key ingredients:

➢ Stepantex SP 90

(Stepan)

• Key product benefits:

➢Excellent softening effect

➢ It gives cloth fresh scent

➢Makes the cloth easier to

iron

➢Provides anti static and

rewetting effect

➢Makes fabric smoother

and fresh

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© DKSHPage 25

Fabric softenerFabric softener DKSHIN # FS 02032016

All data, formulations and information provided herein have not been comprehensively tested and are not represented as suitable for any particular uses. Statement concerning possible or suggested uses made herein may not be relied upon or be construed as a guaranty of no patent infringement. Users have the sole responsibility and obligation for making preliminary tests to determine the suitability of the sample formulations described herein for any application, to make tests before use in any specific applications, and to confirm the performance, efficacy, safety and regulatory compliance of such products for their particular use.

DKSHIN # MC 30082016

Phase Ingredient INCI Supplier %

A1 Distilled water Water --------- Q.S.

B1 Stepanex SP 90 (Esterquat)

Dialkylester ammonium methosulphate

Stepan 7.0

B2 Belsil ADM 22 Amodimethicone, Laureth - 6, Trideceth -6, Trideceth - 3

Wacker 2,0

B3 Flosoft FS 222 Cationinc acrylamide SNF 0,5

C3 Perfume --------- --------- QS

C4 Color Color --------- QS

Description:

Light blue translucent Liquid

➢ Excellent softening effect

➢ It gives cloth fresh scent

➢ Makes the cloth easier to iron

➢ Makes fabric smoother & fresh

Key ingredients:

Steopantex SP 90 It is a cationinc surfactant for used in fabric softeners. It provides good softening, antistatic & rewetting properties.

Procedure:

1 Add Stepanex SP 90 part by part into DM water with continuos stirring at 50 deg C to make a homogeneous mixture.

2 Cool it down to 25 deg C. Add & gently stir with Belsil ADM 22.

3 Finally add, Flosoft FS 222 & Fragrance with continuos stirring.

4 Finally add Colour and perfume to above with stirring

Specification

pH = 3.4, , Brookfield DV-II+Pro # RV, Viscosity - 556 cps, Spindle -02, Speed - 10 rpm

Appearance – Light blue translucent Liquid

Stability test : Product has successfully completed 3 month stability @ 25 deg RT & ETC conditions i.e. 40 deg temp. & 75 % RH as per Indian

standards

DKSH India Mar 2016

Formulation number:

DKSHIN # FS 02032016

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© DKSHPage 26

Stepantex SP 90 and Belsil ADM 22

Stepan Fabric Softeners Stepantex Series Fabric Softener

Main Benefits

Chemical name

TEA Ester Quaternaries

Chemical structure

Best for

household

use

Typical properties

Good re-wetting

Good static control

Good non-yellowing Readily biodegradable

Most

environmental

-friendly fabric

softener

chemistry Widest

softening

performance

range-does

not turn waxy

easily

STEPANTEX TEA Ester Quat Phase

@ 25°C

% Quat

Solids Solvent

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© DKSHPage 27

Phenyl white cleaner

• DKSH key ingredients:

➢ Ammonyx LO – A

(Stepan)

➢ Makon 12 (Stepan)

• Key product benefits:

➢Surface cleaner

and disinfectant

➢ It removes tough oil,

grease, stains

➢ It kills the germs

➢Removes odorr and

leaves pleasant frag

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© DKSHPage 28

Phenyl white cleaner

Phenyl white cleaner DKSHIN # PWC 10072017

All data, formulations and information provided herein have not been comprehensively tested and are not represented as suitable for any particular uses. Statement concerning possible or suggested uses made herein may not be relied upon or be construed as a guaranty of no patent infringement. Users have the sole responsibility and obligation for making preliminary tests to determine the suitability of the sample formulations described herein for any application, to make tests before use in any specific applications, and to confirm the performance, efficacy, safety and regulatory compliance of such products for their particular use.

DKSHIN # PWC 10072017

Phase Ingredient INCI Supplier %

A1 Pine oil Pine oïl ---- 60

B1 Makon 12 Nonyl Phenol Ethoxylate ----- 30.0

B2 Ammonyx LO - A Lauramine Oxide ------ 10.0

Description:

Yellow transparent liquid conc.

➢ Surface cleaner & disinfectant

➢ It removes tough oil, grease, stains

➢ It kills the germs

➢ Removes odour & leaves pleasant frag

Key ingredients:

Ammonyx LO - A Amphoteric surfactant used as a foam enhancer, viscosity builder and emulsifier. It gas excellent gloss on tiles when used in phenyl.

Procedure:

Take all the ingredients one by one in a manufacturing vessel, & mix it properly.

Specification

Appearance – Yellow transparent liquid conc.

Stability test : Product has successfully completed 3 month stability @ 25 deg RT & ETC conditions i.e. 40 deg temp. & 75 % RH as per Indian

standards

DKSH India Jun 2016

Formulation number:

DKSHIN # FS 02032016

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Ammonyx LO – A & Makon 12

Product MAKON®

8, 10 and 12 Name

Chemical Structure

AGRICULTURE

C9H19 (OCH2CH2 )n OH

Chemical Nonylphenol Ethoxylate Description

CAS 127087-87-0 Registry No.

Applications The MAKON series of surfactants is nonionic in nature; they neither ionize in water nor hydrolyze in aqueous acid or alkaline solutions. Chemically, they are the reaction products of nonylphenol and ethylene oxide. They differ in the mole ratio of hydrophilic ethylene oxide to hydrophobic nonylphenol. The MAKON surfactants are high active products that offer a broad range of properties. Because of this versatility, MAKON products find application in a number of different industries and in a multitude of products including agricultural emulsions, detergents, sanitizers, industrial cleaners, metal cleaners, textiles, paper de-inking and drilling products.

Typical MAKON 8 MAKON 10 Properties Appearance at 25°C............................................................................ Clear liquid Clear liquid

pH, 5% 1:1 IPA:H2O ........................................................................................ 7.5 ---

pH, 10% aqueous.............................................................................................. --- 6.3 Actives, % ....................................................................................................... 99.8 99.8 Color, APHA ..................................................................................................... 54 29 Pour Point, °C (°F) ...................................................................................... 6 (43) 4 (42) Freeze Point, °C (°F)................................................................................... 3 (37) 1 (34) Cloud Point, 1% in water, °C (°F) .............................................................. 24 (75) 54 (129) Hydroxyl Number .............................................................................................. 95 88 Approximate HLB .............................................................................................. 12 13 Average Moles of EO .......................................................................................... 8 10 Viscosity, cps at 25°C ..................................................................................... 240 240 Flash Point, PMCC, °C (°F)................................................................. >94 (>201) >94 (>201) Density, g/ml (lbs/U.S. gal).................................................................... 1.04 (8.7) 1.06 (8.8) RVOC, U.S. EPA, % ........................................................................................... 0 0

MAKON 12 Appearance at 25°C............................................................................ Hazy liquid pH, 5% 1:1 IPA:H2O ........................................................................................ 7.5

pH, 10% aqueous.............................................................................................. --- Actives, % ...................................................................................................... 99.8 Color, APHA ....................................................................................... .... 100 max Pour Point, °C (°F) ..................................................................................... 14 (57) Freeze Point, °C (°F)................................................................................. 11 (52) Cloud Point, 1% in water, °C (°F) ............................................................ 81 (178) Hydroxyl Number .............................................................................................. 76 Approximate HLB .............................................................................................. 14 Average Moles of EO ........................................................................................ 12 Viscosity, cps at 25°C ..................................................................................... 280 Flash Point, PMCC, °C (°F)................................................................ >94 (>201) Density, g/ml (lbs/U.S. gal).................................................................... 1.06 (8.8) RVOC, U.S. EPA, % ........................................................................................... 0

Oct. 2015 Supersedes: Oct. 2014 Page 1 of 2

MAKON®

is a registered trademark of Stepan Company.

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Premium car wash shampoo

• DKSH key ingredients:

➢ Ammonyx LMDO

(Stepan)

• Key product benefits:

➢ Removes tough stains

➢ Removes oil and

grease

➢ Imparts shine and

lustre

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© DKSHPage 31

Premium car wash shampoo

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Ammonyx LMDO

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High gloss car polish

• DKSH key ingredients:

➢ Wacker E 87 (Wacker)

➢ Sabowax FL 65 K (Sabo)

➢ Carbomer 980 (Ashland)

➢ Kaolin Opaque (Imerys)

• Key product benefits:

➢ Provides gloss and

smear

➢ Removes grit and grime

from paint

➢ Reduces paint oxidation

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High Gloss Car Polish

High Gloss Car Polish DKSHIN # HGCP20062017

All data, formulations and information provided herein have not been comprehensively tested and are not represented as suitable for any particular uses. Statement concerning possible or suggested uses made herein may not be relied upon or be construed as a guaranty of no patent infringement. Users have the sole responsibility and obligation for making preliminary tests to determine the suitability of the sample formulations described herein for any application, to make tests before use in any specific applications, and to confirm the performance, efficacy, safety and regulatory compliance of such products for their particular use.

DKSHIN # HGCP20062018

Phase Ingredient INCI Supplier %

A1 Aqua _____ --------- Q.S.

A2 Carbomer

980 Carbomer Ashland 0.3

A3 TEA Triethanolamine ______ QS

B2 Carnabua Wax Carnabua Wax ______ 1.5

B3 SabowaxFL65K

Glyceryl

stearate,

PEG -100

stearate

Sabo 2.0

C1 Belsil E87 Silicone Emulsion Wacker 10.0

C2 Kaolin Kaolin Imerys 8.0

C3 Nipaguard

DMDMH DMDMH ____ 0.4

Description:

White Liquid

✓ Provides Gloss and Smear

✓ Removes grit and grime from

Paint.

✓ Reduces paint oxidation

Key ingredients:

Belsil E87

SLM E 87 emulsion is a 60% active non-ionic emulsion Formulated with a polydimethylsiloxane. SLM E 87 can be Used both in concentrated as well as diluted form. It has been Specially formulated for use as polish ingredient .This Emulsion is used to provide good gloss and minimum smear in car polish formulation

Procedure:

1

Take 2/3rd qty of water in a manufacturing vessel & heat it upto 75 - 80 deg C. Add carbomer 980 to it under constant stirring. Allow it to completely dissolve and neutralize with TEA

2

In another beaker heat Carnauba wax & Sabowax FL 65 K, heat it upto 75 - 80 deg C.

3

Add oil phase to water phase under continuous stirring with proper emulsification.

4 Add Kaolin with continous stirring in it

5

At 45 deg Celsius add Belsil E87, and preservative.

Specification

pH = 6.2

Appearance – White liquid

Stability test : Product has Successfully completed 3 month stability @ 25 deg RT & ETC conditions i.e. 40 deg temp. & 75 % RH as per

indian standards

DKSH India June 2018

Formulation number:

DKSHIN # HGCP20062017

Image

Image

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Wacker E 87 and Kaolin Opaque

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Sabowax FL 65 K and Ashland 980 Carbomer

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Car freshener gel

• DKSH key ingredients:

➢ AL-TH Gel (Taiyo

Corp.)

• Key product benefits:

➢ Designed to mask

unpleasant odor

➢ Mild aroma

➢ Long lasting fragrance

➢ Good relaxing and

healing properties

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Car freshener gelCar freshener gel DKSHIN # CFG 10082015

All data, formulations and information provided herein have not been comprehensively tested and are not represented as suitable for any particular uses. Statement concerning possible or suggested uses made herein may not be relied upon or be construed as a guaranty of no patent infringement. Users have the sole responsibility and obligation for making preliminary tests to determine the suitability of the sample formulations described herein for any application, to make tests before use in any specific applications, and to confirm the performance, efficacy, safety and regulatory compliance of such products for their particular use.

DKSHIN # FO 05072018

Phase Ingredient INCI Supplier %

A1 OCTOPE ALTH ALTH Taiyo Corp. 3

B1 Isopar G Synthetic Isoparaffin fluid ------ Q.S.

B2 BHT Butylated Hydroxytoluene ------ 0.5

B4 Perfume - Mon Fragrance ------ 10.0

Description:

Transparent Clear Gel

✓ Designed to mask Unpleasant Odour.

✓ Mild aroma✓ Long lasting fragrance✓ Good relaxing and Healing properties

Key ingredients:

SEBS GP 7550 Procedure:

1 In a beaker add ALTH slowly in 2/3 rd qty of Isopar G at 50 deg C for 5 min.

2 In a separate beaker, take balance qty Isopar G, BHT & fragrance & stir at 50 deg C for 5 min.

3 Mix both the phases & stir for 5 min at 50 deg C.

4 Pour the phase in liquid state in a filling kettle & fill in a suitable container.

Specification

Appearance – Transparent clear Gel.

Stability test : Product has successfully completed 15 days stability @ 25 deg RT & ETC conditions i.e. 40 deg temp. & 75 % RH as per Indian

standards

DKSH India Aug 2015

Formulation number:

DKSHIN # CFG 10082015

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AL – TH gel

・ AL-TH gel air freshener (for cars/home use )

It is the most popular air freshener of gel type especially in air freshener for cars sold in Japan. The greatest features are heat resistance and cold resistance. It does not melt at 100 ℃ and does not freeze at the freezing point either. The gel is transparent and has beautiful appearance. It will be back in original shape even if its form changes temporarily since it has liquidity. The characteristic of AL-TH gel has the high compatibility with tropical climate of Thailand since inside of a car becomes high temperature.

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© DKSHPage 40

Leather and vinyl conditioner

• DKSH key ingredients:

➢AK 1000 Silicon Fluid

(Wacker)

➢AK 12500 Silicon Fluid

(Wacker)

➢Wacker E 87 (Wacker)

➢Saboderm HE (Sabo)

• Key product benefits:

➢Non greasy formula

makes leather supple,

shine and vinyl surface

soft

➢Rehydrates, restores

and protects all of your

leather and vinyl

surfaces

➢Great as a leather polish

for furniture, car seats,

shoes, bags and more

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Leather and vinyl conditioner

Procedure:

1 Initially take total quantity water ,DEDTA in manufacturing vessel & heat upto 70 – 75 deg C

2 In another beaker take oil phase & heat it up to 70 – 75 deg C.

3 Then add Weigh Carboner 980 to the water phase to mixed well with contineous stirring.

4 Then add oil phase to water phase under continuos stirring to get an emulsion.

5 At 50 deg C, add Preservative with stirring.

6 Finally add perfume with stirring & adjust the product pH 5.5 - 6.5

Specification

pH = 5.5, Brookfield DV-II+Pro # RV, Viscosity – 28000 cps, Spindle - 05, Speed -10 rpm

Appearance – White smooth cream

Stability test : Product has Successfully completed 3 months stability @ 25 deg RT & ETC conditions i.e. 40 deg temp. & 75 % RH as per

Indian standards

DKSH India July 2019

Formulation number:

DKSHIN # LVC 12092018

Leather & vinyl conditionerDKSHIN # LVC 12092018

All data, formulations and information provided herein have not been comprehensively tested and are not represented as suitable for any particular uses. Statement concerning possible or suggested uses made herein may not be relied upon or be construed as a guaranty of no patent infringement. Users have the sole responsibility and obligation for making preliminary tests to determine the suitability of the sample formulations described herein for any application, to make tests before use in any specific applications, and to confirm the performance, efficacy, safety and regulatory compliance of such products for their particular use.

DKSHIN # AASM 09072019

Phase Ingredient INCI Supplier %

A1 Aqua Water ----- Q.S.

A2 Carbomer 980 Carbomer Ashland 0.5

A3 D. EDTA D.EDTA ----- 0.1

A4 TEA Triethanol amine 0.5

B1 Saboderm HE POE-7 Glyceryl cocoate Sabo 2.0

B2 Makon 12 Nonyl phenol ethoxylate Stepan 1,0

B3 AK 1000 silicone fluid Silicone fluid Wacker 5.0

B4 AK 12500 silicone fluid Silicone fluid Wacker 3.0

B5 Belsil E 87 Silicone emulsion for car care Wacker 10.0

B6 Escalol 775 Octyl methoxy cinnamate Ashland 1,0

B7 DMDMH DMDMH Etser india 0.5

B8 Perfume Perfume ------- Q.S.

Description:

White smooth cream

➢ Non greasy formula makes leather supple, shine & vinyl surface soft

➢ Rehydrates, restores & protects all of your leather & vinyl surfaces

➢ Great as a leather polish for furniture, car seats, shoes, bags & more

Key ingredients:

AK 1000 Silicone fluid It is linear, non – reactive polydimethylsiloxane with viscosity of approximately 1000 mm2/s. It is used as a polish additive,

AK 12500 Silicone fluid It is linear, non – reactive polydimethylsiloxane with viscosity of approximately 12500 mm2/s. It is used as a polish additive,

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Wacker AK 1000 and 12500

Technical data sheet for WACKER® AK 1 000 / Version: 1.5 / Date of last alteration: 28.04.2017 1 / 2

WACKER® AK 1 000 S I L I C O N E F L U I D

Product description

Structural formula:

WACKER® AK 1 000 is a linear, non-reactive

polydimethylsiloxane with a viscosity of

approx. 1 000 mm²/s. Due to its chemical structure,

WACKER® AK 1 000 has an outstanding property

profile, which sets it apart from organic materials such

as mineral oils.

Properties

WACKER® AK 1 000 is a clear, odorless and colorless

liquid.

Special features

- minimal change in physical properties over a broad

temperature range

- excellent water-repellent properties

- good dielectric properties

- low surface tension and thus high surface activity

- chemically highly unreactive

- low solidifying point

- high flash point

- high heat resistance

- good solubility in a wide range of solvents

Application

- release agent

- lubricant

- hydraulic fluid

- antifoam agent

- water-repellent agent

- liquid dielectric for electrical and electronic

equipment

- heat-transfer oil

- polish additive

- plastics additive

- additive for textile and fiber auxiliaries

For pharmaceutical applications, we recommend

specialty silicone fluids from our SILFAR ® line.

Silicone fluids from our BELSIL® line are available for

the cosmetic sector. Whenever particularly high heat

and shear resistance is required, we recommend

silicone fluids from our AK stab, AK visc and AKC

product lines. Specialty grades of the product

(available as WACKER® PLASTICIZER) will be

needed for use as a silicone plasticizer in RTV-1

sealants.

Processing

Due to WACKER® AK 1 000 many diverse

applications, no general processing information can be

provided. Parameters will vary from application to

application.

Available in a range of viscosities,

WACKER® SILICONE FLUIDS AK are miscible with

each other in any ratio. The standard product's

viscosity can thus be altered to suit your individual

needs.

WACKER® AK 1 000 is a non-polar liquid and is

immiscible with polar solvents such as water or short -

chain alcohols. In aliphatic and aromatic hydrocarbons,

chlorohydrocarbons, ethers, esters, ketones and

higher alcohols, WACKER® AK 1 000 is soluble in any

proportion.

Before the product is used with solvents for the first

time, it is advisable to perform a lab-scale test.

When solvents are used, please remember to read the

appropriate hazard information.

Technical data sheet for WACKER® AK 12 500 / Version: 1.3 / Date of last alteration: 06.11.2014 1 / 2

WACKER® AK 12 500 S I L I C O N E F L U I D

Product description

Structural formula:

WACKER® AK 12 500 is a linear, non-reactive

polydimethylsiloxane with a viscosity of

approx. 12 500 mm²/s. Due to its chemical structure,

WACKER® AK 12 500 has an outstanding property

profile, which sets it apart from organic materials such

as mineral oils.

Properties

WACKER® AK 12 500 is a clear, odorless and

colorless liquid.

Special features

- minimal change in physical properties over a broad

temperature range

- excellent water-repellent properties

- good dielectric properties

- low surface tension and thus high surface activity

- chemically highly unreactive

- low solidifying point

- high flash point

- high heat resistance

- good solubility in a wide range of solvents

Application

- release agent

- lubricant

- hydraulic fluid

- antifoam agent

- water-repellent agent

- liquid dielectric for electrical and electronic

equipment

- polish additive

- plastics additive

- additive for textile and fiber auxiliaries

- damping medium

For pharmaceutical applications, we recommend

specialty silicone fluids from our SILFAR ® line.

Silicone fluids from our BELSIL® line are available for

the cosmetic sector. Whenever particularly high heat

and shear resistance is required, we recommend

silicone fluids from our AK stab, AK visc and AKC

product lines.

Processing

Due to WACKER® AK 12 500 many diverse

applications, no general processing information can be

provided. Parameters will vary from application to

application.

Available in a range of viscosities,

WACKER® SILICONE FLUIDS AK are miscible with

each other in any ratio. The standard product's

viscosity can thus be altered to suit your individual

needs.

WACKER® AK 12 500 is a non-polar liquid and is

immiscible with polar solvents such as water or short-

chain alcohols. In aliphatic and aromatic hydrocarbons,

chlorohydrocarbons, ethers, esters, ketones and

higher alcohols, WACKER® AK 12 500 is soluble in

any proportion.

Before the product is used with solvents for th e first

time, it is advisable to perform a lab-scale test.

When solvents are used, please remember to read the

appropriate hazard information.

Storage

Maximum temperature allowed during storage and

transportation:

50 °C

The 'Best use before end' date of each batch is shown

on the product label.

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Wacker E 87

WACKER E 87 Silicone emulsion for Car Care

Characteristics

SLM E 87 emulsion is a 60% active non-ionic emulsion formulated with a polydimethylsiloxane. SLM E 87 can be used both in concentrated as well as diluted form. It has been specially formulated for use as polish ingredient .This emulsion is used to provide good gloss and minimum smear in car polish formulation.

Application

Use clean water to dilute the Wacker E 87 and a standard dilution of 1: 10 to 1:30 is recommended for best results. An optimum dilution of 1 : 20 is recommended for excellent result, if it is to be used in the diluted form. But, obviously the ratio varies from applica- tion to application.

Storage and Shelf Life

Wacker E 87 has a shelf life of at least 6 months when stored at 25 °C in the tightly closed original container. The 'Best use before end' date of each batch appears on the product label. Emulsions showing signs of creaming should be agitated before use to assure uniform consistency.

Storage beyond the date specified on the label does not nec- essarily mean that the product is no longer usable. In this case however, the properties required for the intended use must be checked for quality assurance reasons.

Product Safety

Detailed safety information is contained in each material data safety sheet, which can be obtained from our sales offices.

Eigenschaften / Product data

Typical general characteristics Inspection Method Value

Appearance visual White liquid

Nonvolatile content, approx., % 64-66

pH,approx 6-9

These figures are intended as a guide and should not be used in preparing specifications.

Kolkata, 2015

The data presented in this leaflet are in accordance with the present state of

our knowledge, but do not absolve the user from carefully checking all

supplies immediately on receipt. We reserve the right to alter product con-

stands within the scope of technical progress or new developments. The

recom-mendations made in this leaflet should be checked by preliminary trials

because of conditions during processing over which we have no con- trol,

especially where other companies' raw materials are also being used. The

recommendations do not absolve the user from the obligation of investi-

gating the possibility of infringement of third parties' rights and, if necessary,

clarifying the position. Recommendations for use do not constitute a warran-

ty, either express or implied, of the fitness or suitability of the product for a

particular purpose.

An ISO 9001:2008 & ISO 14001-2004

& ISO 22716-2007 certified company

Wacker Metroark

Chemicals Pvt. Limited

Diamond Harbour Road Chandi, 24 Par (S) W.Bengal 743 503, India

Tel: + 91 33 24072 101 Fax: + 91 33 24072 502

Seite 1 von 1

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Disclaimer

.DKSH

Due care has been used in preparation of this presentation and DKSH makes every effort to

provide accurate and up-to-date information. Nlevertheless, this presentation may be subject

to technical ,inaccuracies, information that is not up-to-date or typographical errors.

DKSH does not assume liabili1ty for relevance, accuracy and co:mpleteness of the information

provided. DKSH reserves the right to change, supplement, or-delete some or all of the

information on this presentation without notice.

The layout, graphics and other contents in this presentation are protected by copyright law

and should not be reproduced or used without DKSH's written permission.

Think Asra. Think DKSH. Page 16 © DKSH 2018


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