Disclosure to Promote the Right To Information Whereas the Parliament of India has set out to provide a practical regime of right to information for citizens to secure access to information under the control of public authorities, in order to promote transparency and accountability in the working of every public authority, and whereas the attached publication of the Bureau of Indian Standards is of particular interest to the public, particularly disadvantaged communities and those engaged in the pursuit of education and knowledge, the attached public safety standard is made available to promote the timely dissemination of this information in an accurate manner to the public. इंटरनेट मानक “!ान $ एक न’ भारत का +नम-ण” Satyanarayan Gangaram Pitroda “Invent a New India Using Knowledge” “प0रा1 को छोड न’ 5 तरफ” Jawaharlal Nehru “Step Out From the Old to the New” “जान1 का अ+धकार, जी1 का अ+धकार” Mazdoor Kisan Shakti Sangathan “The Right to Information, The Right to Live” “!ान एक ऐसा खजाना > जो कभी च0राया नहB जा सकता ह ै” Bhartṛhari—Nītiśatakam “Knowledge is such a treasure which cannot be stolen” IS 1115 (1986): cutting oil, soluble [PCD 3: Petroleum, Lubricants and their Related Products]
Transcript
Disclosure to Promote the Right To Information
Whereas the Parliament of India has set out to provide a practical regime of right to information for citizens to secure access to information under the control of public authorities, in order to promote transparency and accountability in the working of every public authority, and whereas the attached publication of the Bureau of Indian Standards is of particular interest to the public, particularly disadvantaged communities and those engaged in the pursuit of education and knowledge, the attached public safety standard is made available to promote the timely dissemination of this information in an accurate manner to the public.
इंटरनेट मानक
“!ान $ एक न' भारत का +नम-ण”Satyanarayan Gangaram Pitroda
“Invent a New India Using Knowledge”
“प0रा1 को छोड न' 5 तरफ”Jawaharlal Nehru
“Step Out From the Old to the New”
“जान1 का अ+धकार, जी1 का अ+धकार”Mazdoor Kisan Shakti Sangathan
“The Right to Information, The Right to Live”
“!ान एक ऐसा खजाना > जो कभी च0राया नहB जा सकता है”Bhartṛhari—Nītiśatakam
“Knowledge is such a treasure which cannot be stolen”
“Invent a New India Using Knowledge”
है”ह”ह
IS 1115 (1986): cutting oil, soluble [PCD 3: Petroleum,Lubricants and their Related Products]
ISrlll5-4986
tndian Standard (Itdfhedl~)
SPECIFICATION FOR GENERAL PURPOSE CUTTING OIL, SOLUBLE
( Second Revision )
Second Reprint JANUARY 1998
UDC 621.892.6
@ Copyrikht 1986
BUFAU OF INDIAN STANDARDS MANAK BHAVAN, 9 BAHADUR SHAH ZAFAR MARG
NEW DELHI ~K100i
Cr 3 Ninwmbm 1986
IS t 1115 - 1996 ( Reaairmd 1996 )
Indian Standard SPECIFICATION FOR
GENERAL PURPOSE CU’ITING OIL,
( Second Revision )
SOLUBLE
Lubricants and Related Products Sectional Committee, PCDC 4
Chaimuzn SEW P. K. GOEL
JZ+r#Wt&llg Petroleum Conservation Raearcb AIIociation, New
SHRI I. CHANDBA ( Altmutr ) SERI P. K. GUPTA SHRI J. D. HANDAS
SFIRI B. GOSWAMI ( AI&m& )
Naval Headquarters, New Delhi Assam Oil Dlviaion, Bombay
Hindustan Fertilizers Cqporation Ltd, New Delhi Tata Engineering dt Locomotive Co Ltd.
Jamsbedpur
Q Ce@ghr 1966
BUREAU OF, INDIAN STANDARDS Thii publication b protected under tbe IndEw CopJrilirt Act ( XIV of 1957 ) *ad teprohtion in whole or in part by any means except witb written pertnirion of tbs Dublirber &all be deemed to be an infringement of copyright under the rid Act.
18 t 1115 l 1986
( Gmtindffem pug0 1 )
MOlllbWS R@wnting SERI Ii. JAFFBEY
S-I M. A. Pans ( .4lternato ) Pttrodl Oil Co Ltd. Bombay
JIB G. JAYARAXA RAO Ministry of Petroleum KU~ARI RAJIALAPSHYI ( Al&rxatr )
Saar 0. K. JIJN~~A Bharat Petroleum Corporation Ltd, Bombay SEBI I. M. MEWEAXT ( Ahmatr )
SHRI S. K. KALB Soar J. L. G~ovaa ( Alterme. )
Bhilai Steel Plant, Bhilai
SEW R. KU~A~IIXABA~P SERI R. N. PADEY ( Atfmatr )
Ministry of Defence ( R & D )
SRRIV. LOB0 Oil Co-ordination Committee, New Delhi SBR~ S. N. MATEUX ( Afkrnorr )
Smtx R. MUxIiERJ1PE SHEI M. J. SHAE ( Allrmofr)
Indian Oil Blending Ltd, Bombay
DR P. K. MUKHOP.+DEYAY Indian Oil Corporation Ltd ( Research & Develop-
SEW K. C. MEHTA ( Altmatr ) ment Centre ) , Paridabad
SHRI J. P. NI~AM Development Commissioner, Small Scale Induatriet, New Delhi
SHRI J. C. PAS~IJA ( Altamut~) Snnr RAJSXD- Surua Indian Oil Corporation Ltd ( Refinery & Pipeline
Sasr D. K. DA~QUPTA ( Ahmatu ) Division ), New Delhi
SHRI T. R. RAMAKR~~HNAN SRRI C. MIEHRA ( Akrnek )
Tata Iron & Steel Co Ltd, Jamahedpur
SHSI R. A. RAO Lubrixol India Ltd, Bombay SERI K. L. MALLIK ( Ahudr )
Saran S. V. SASTRY The Automotive Research Association of India, Pune SERI B. Grtoan ( Aftumet# )
SRRI v. R. SESHU Hindustan Petroleum Corporation Ltd, Bombay SHRI P. M. RAO ( Altmutr )
SERI D; K. SJNQR Bharat Heavy Electricals Ltd, Bhopal SHRI R. K. GUF-TA ( Aknutr I ) SERI T. v. SUnDEnnAJan ( AkmetU II )
SERI SIJDEIR SINWAL Indian Institute of Petroleum, Debra Dun DR A. SETEURAYIAA ( Alfmmtr )
SHRI T. V. VARCWESE Madras Refine&r Ltd, Madras SHRI V. K. GOPINATE ( Aflnnotr )
DR P. S. VEX~ITARAMANI Ministry of Defence ( DM & SR & DE ) DR R. D. SRIVA~TA~A ( Al&m& )
SHRI M. S. SAXENA, Director General, IS1 ( Ex-o&cio Mm&n ) Director ( P & C )
SIcrrkr~ SERI M. A. U..KHAN
Joint Director ( P & C ), IS1
(conlhwdonp8g8 11)
2
IS : 1115 - 1986
Indian Standard SPECIFICATION FOR
GENERAL PURPOSE CUTTING OIL, SOLUBLE
( Second Revision )
0. FOREWORD
0.1 This Indian Standard ( Second Revision ) was adopted by the Indian Standards Institution on 3 March 1986,‘after the draft finalized by the Lubricants and Related Products Sectional Committee had been appro- ved by the Petroleum, Coal and Related Products Division Council. 0.2 This Indian Standard was first published in 1957. It was subsequently revised in 1973. In the first revision the requirements for emulsion and frothing test copper strip corrosion test and low temperature stability test were modified. The standard was also amended twice in 1975 and 1977. 0.3 The present revision has been prepared as a result of a review of the standard by the Ad-hoc study group especially set up for this purpose as we11 as by the concerned technical committee in the.light of the current requirements of cutting oils and advancement in the field of lubrication technology in the country. In this revision the title of the standard has been changed and the requirements for emulsion, frothing and high temperature stability tests have been modified as per the latest test methods being followed by the industry. 0.4 In the preparation of this standard considerable assistance has been derived from the following publications:
i) 3-GP-334 4 Oil, cutting, soluble. Canadian Government Specification Board; and
ii) INDjSL 3626 ( a )-1951 Oil, 2x-l. Ministry of Defence, Government of India.
0.5 For the purpose of deciding whether a particular requirement of this standard is complied with, the final value, observed or calculated, expressing the result of a test or analysis, shall be rounded off in accord- ance with IS : 2-1960’. The number of significant places retained in the rounded off value should be the same as that of the specified value in this standard.
*Rules for rounding off numerical values ( reuisud ).
3
IS:1115-1986
1. SCOPE
1.1 This standard sampling and test
prescribes the requirements and the methods of
_ _ for general purpose cutting oil, soluble intended for use in machines where the use of a suitable cutting oil giving a non- transparent aqueous emulsion.is permissible as coolant and lubricant for cutting tools.
2. REQUIREMENTS
2.1 General Requirements
2.1.1 The material shall be prepared from mineral lubricating oil having a flash point of 15O”C, Min when tested by IS : 1448 ( P : 69 )*, together with emulsifiers, bactericides, stabilizers and other additives, if necessary.
2.1.2 The oil shall be clear, homogeneous and free from foreign matter, sediment and visible impurities. It shall not contain any ingredients injurious to persons using or handling it either in the original state or in the form of an emulsion. The oil should be free from any pungent or unpleasant odour.
2.2 Specific Requirements - The material shall comply with the. requirements prescribed in Table 1 when tested according to the methods prescribed in the relevant appendix to this standard and ‘P :’ series of IS : 1448t. Reference to the relevant methods of test is given in Table 1.
3. PACKING AND MARKING
3.1 Packing - The material shall be packed in securely closed metal drums or any other suitable containers of appropriate size and strength as agreed to between the purchaser and the supplier.
3.2 Marking - information:
Each container shall be marked with the following
a) Name of the material;
b) Manufacturer’s name, initials or his trade-mark, if any;
c) Quantity of the content; and
d) Batch number and year of manufacture.
*Determination of flash and iire point by Cleveland ( open) cup. tMethods of test for petroleum and itsproducts.
4
L
iS:lllS-‘1986
(1)
i) ii)
iii)
iv)
v)
vi)
vii)
viii)
ix)
x)
TABLE 1 REQUIREMENTS FOR GENERAL PURPOSE CUTTING OIL, SOLUBLE
( Clauses 2.2, 4.1 anu 5.2 )
RLQUIREMENXS
(2) Aah, percent by mass, Max
Water, percent by mass, Max
Emulsion test, 5 : 1 and 20 : I ratio in water of 400 ppm hardness ( as CaCO, )
Cast iron corrosion test, 20 : 1 ratio emulsion with 400 ppm hard water ( as CaCO, ), Max
Copper strip corrosion teat at 100% for 3 hours
Thermal stability teat
Flash point, COC, “C, Min
+%scodty at 40°C, CSt, Mitt
*Volatile matter at 100°C for 16 h, percent by mass, Max
(3)
3.5
10’0
0-l ml oil and 0.2 ml cream permitted
No froth after 15 minutes
Oil-1
Not worse than No. 1
Shall pass the test
150
20
20
METHOD OF TEST, REFTO
~__-_*----~ Appendix
(4)
-
-
-
-
A
-
-
-
IB
P:ofIS:’ 1448+
(5)
P:4
P:ul
P : 98
P : 99
-
P: 15
P: 100
P : 69 ( sac Note )
P : 25
NOTE -- Take 200 g of soluble oil teat sample. Add 25 to 30 g of anhydrous sodium sulphate. Stir thoroughly for 5 minutes, keep it in the oven at 40% for one hour. Decant tile oil and subject it to,flaah point determination by Cleveland ( open ) cup method.
*Methods of teat for petroleum and ita products. tl’hese tests are applicable only for defence requirements.
3.2.1 The container may also be marked with Standard mark.
3.2.2 The use of the Standard Mark is govered by the provisions of the Bureau of Indian Standards Act, 1986 and the Rules and Regulations made thereunder. The details of conditions under which the Iicence for the use of Standard Mark may be granted to manufrcturenr or producc~ may be obtained from the Bureau of Indian Standards.
5
D
IS I 1115 - 1986
4. KEEPING PROPERTIES
4.1 The material when stored in original sealed containers under ambient temperature conditions in shade shall retain the properties described in Table 1 for a period of not less than 6 months after the date of delivery.
5. SAMPLING
5.1 Representative samples of the material shall be drawn as prescribed in IS : 1447-1966*.
5.2 Number of Tests and Criteria for Conformity - Tests for emulsion, frothing, cast iron corrosion and thermal stability shall be conducted on three of the individual samples each, and there shall be no failure if the lot is to be accepted as satisfactory in respect of the above characteristics. For the remaining characteristics prescribed in Table 1 the tests shall be conducted on the composite sample prepared according to IS : 1447-1966’ and no failure shall be reported for the acceptance of the lot.
APPENDIX A [ Tublc 1, Item (v) ]
CAST IRON CORROSION TEST
( Adapted with permission from the Institute of Petroleum, Standard No. IP 125/77 Aqueous cutting fluid, corrosion of cast iron )
A-l. SCOPE
A-l.1 Cutting oils which are used in the form of aqueous dispersions or solutions should not readily permit corrosion of equipment with which they come into contact. This method is accordingly designed to assess the behaviour of such fluids in contact with a typical metal, such as cast iron; and is applicable to samples submitted either in the form of an aqueous fluid as used in practice or as a concentrate requiring dilution with water.
A-2. OUTLINE OF THE METHOD
A-2.1 Steel millings are placed on the cleaned surface of a cast-iron plate and emulsion of the cutting oil under test is poured on to them. After 24 hours the millings are removed and the surface of the plate ia examined for corrosion.
*Methodr of sampling of petroleum and its products.
6
A-3. APPARATUS
Ab3.1 Teat Plate - Conforming to Grade 15 of IS’: 210-1978+; 10 cm x 10 cm: x 6 mm ( originally ) of grey cast iron, the surface being ground to a smooth finish free from chatter marks and burniahings ( CLA 025 to 0.38 pm ).
A-3.2 Steel Millinga - Approximately 6 mm long and 1’5 to 3 mm width prepared by dry-milling the steel conforming to IS : 226-1975t.
A-3.3 Test Chamber - No dimensional limits are prescribed 6~ the chamber. The temperature shall be maintained at 27 & 2°C. and the humidity at 52 f 5 per&m’. The required le.vel of humidity can be obtained by placing at the bottom of the cabinet at least one open dish, not Iess than 15 mm diameter, containing a-saturated solution of sodium bisulphate in contact with an excess of solid bisulphate which give a humidity of 52 percent at 20°C. Lumps ‘of solid bisulphate should stand out of the liquid. If a large chamber is used with several platea under test, several dishes may be desirable. Alternatively, separate chambers, each with a dish of bisulphate, can be used one for each test plate.
A-3.4 Pipette - Calibrated to deliver 2 ml of the fluid.
A-4. PRErARATION OF SAMPLE
A-4.1 For carrying out this test the 2O:l ratio emulsion shall be prepared with 400 ppm hard water in accordance with the method given for emulsion and frothing tests.
A-5. PREPARATION OF APPARATUS
A-5.1 If the surface of any plate is corroded or pitted, regrind the plate to a smooth surface. Do not allow the plate to become burnished.
A-5.2 If the thickness of. the plate is reduced to 3 mm, discard it.
A-5.3 Immediately prior to test, prepare the ground surface of the test plate as follows and do not touch the surface subsequently, Carry out this procedure irrespective of whether or not the plate has been used before, and whether or not it is new or reground:
a) Wipe with cotton wool soaked in toluene;
b) Wash with acetone from a wash-bottle;
c) Wipe dry with cotton wool; -.
*Specification fix grey iron castings. (Udrd rmi~bn ).
tSpecification for rtructural ateel ( standard quality ) (&IA mision j.
7
.
i
- .
I
IS t 1115 - 1986
4
4 f)
Rub the plate on a new piece of No. 0 emery cloth placed on flat surface ( plate glass for example ), rubbing heavily by bar for 30 double-stokes without lifting in each of two directions right angles. A hand magnet may be found convenient to ho the plate for this operation. If .stain marks are still apparet treat. the plate.as pitted and regrind it; Wipe with clean filter Paper soaked in acetone; and
Rub with successive pieces of dry clean filter paper until I marks are apparent on the paper.
A-6. PROCEDURE
Ad.1 Make the test in a room free from corrosive fumes.
A-6.2 Take the millings and sieve with a standard 710-micron IS siel [ sss IS : 460 ( Part 1 )-1985* 3. Discard the dust and retain the m: lings. Discard all the millings if any rust is present.
A-6.5 Wash the millings in acetone and allow to dry in air. Thereafts the millings should remain untouched by hand.
A-6.4 With the aid of a spatula, place 4 portions each of approximate 2 g of steel millings in a single layer each centrally in a quarter of tl prepared surface of the plate. Each portion shall be so disposed th the edges are not in contact either with adjacent portions or the edges the plate.
A-g.5 Pipette the fluid to be tested on the each portion of millings, ; that the millings are thoroughly wetted. The fluids on adjacent portio! shall not run together. About.2 ml of the fluid will be required PI portion of millings. If testing several fluids at once, put the 4 portio; on different plates as far as possible, so that each plate has several fluic on it. This minimizes error due to possible variations in plates.
A-6.6 Transfer the plate to the test chamber, the temperature am humidity of which is maintained as specified in A-3.3.
A-6.7 After 24 hours, remove the plate from the cabinet, remove tl millings from the plate and discard them. Wash the surface of the pla with acetone then with toluene and finally rub gently with a filter pap1 soaked in toluene.
A-6.8 Inspect the surface areas of the plate for corrosion, and recoi pittings and staining results separately for each test area, for exampl the areas previously covered by 2 g of steel millings as follows:
Pitting - Record the number of pits present.
l Specificatiim for test sieves : Part 1 Wire cloth test sievea ( &rd reuitin ).
8
IS t 1115 - 1996
Staining - Record the extent and intensity of staining using the following numbers.
ProQortioas of Test Arta Staintd Inttnsity of Staining
0 Nil 0 Nil
1 Less than 10 percent ! Hardly perceptible
2 Between 10 and 25 percent 2 Slight staining
3 Between 25 and 50 percent 3 Heavy staining
4 Between 50 and 75 percent 4 Surface damage ( not including pits )
5 Over 75 percent
NOTE - If staining ia not uniform record the maximum intensity observed.
A-7. REPORTING
A-7.1 Report the results by three numbers, the first being the number of pits, followed by an oblique stroke; the second, the area of staining followed by a hyphen; and the third, the maximum intensity of staining ( for example: O/l-l, S/O-O, O/3-2, etc ).
A-7.1.1 Also report’relevant test details, as follows:
a) Nature of added water used; and
b) Dilutian if known and method of preparation, if relevant.
A-8. PRECISION
A-8.1 The precision cannot be expressed in a useful form to cover all cases. Extensive investigations have shown that it is very poor when the corrosion probability is of the order of 50 percent, but that it is better when either very little or considerable corrosion occurs. The use of statistically designed programmes are recommended whenever compara- tive tests are to be made.
PS:1115 - 1986
APPENDIX B [ z-able 1, Item (x) ]
DETERMINATION OF VOLATILE MATTER
B-l. PROCEDURE
B-l.1 Place 10 f 0.1 g of the sample in a clean, dried and weighed petri dish of 100 mm diameter and weigh to the nearest 0.01 g.
B-1.2 Place the sample in the petri dish in an oven maintained at 100 5 1°C for 16 h.
B-l.3 At the end of the heating period remove the petri dish from the oven, cool to room temperature and weigh to nearest 0.01 g.
B-l.4 Calculate the volatile matter as percent by mass.
I
10
IS : 1115 - 1996
( Continfud from pub’ 2 )
Metal working Products Subcommittee, PCDC 4 : 13
c.hwma BERI K. C. MEHTA
Rrpmmling
Indian Oil Corporation Ltd ( Research & Develop ment Centre ), Faridabad
SHRI FAIURA Smoa ( Ahmatr to Shri K. C. Mehta )
SHRI A. K. ARORA Rourkela Steel Plant, Rourkela Da N. T. BADDI Association of Manufacturers of Petroleum Specia-
SARI R. CHAKRAVARTY ( Ahnatr ) lities, Bombay
SERI M. K. BHARQAVA Petroleum Re-Refiners Association of India, Madras SH~I SHANTILAL DAYA ( A&em& )
SHRI S. R. BHATWAOAB Indrol Lubricants & Specialities Ltd, Bombay SHRI N. SETHURUAN ( Altematc )
SHBI A. K. CAPRIHAN Indian Aluminium Co Ltd, Calcutta SHRI A. K. HAJARA ( A&n& )
SARI C. V. CHANDEASEEHAB Balmer Lawire St Co Ltd, Bombay SHRI R. R. SARAN ( AI&n& )
TEE CEEXIST & METALLURQIST Railway Board ( Ministry of Railways ) ASSTT RESEARCH OBBICER
( Came ), RDSO, LUCXNOW ( Altemats ) SHRI S. GHOSE National Test House, Calcutta
SHRI P. K. CEAKRABORTY ( Alternafe ) SHRI H. JA~EY Petrosil Oil Co Ltd, Bombay
SHRI M. A. PAES ( Alternate ) SHRI V. K. JAIN Indian Institute of Petroleum, Debra Dun
SHRI B. R. CHADHA ( Alternate ) SHRI 0. K. JUN~EJA Bharat Petroleum Corporation Ltd, Bombay
SERI P. P. NACURKAR ( Altcmak ) SHRI B. LAKSHMINARAYAN Indian Oil Corporation Ltd ( Marketing Division ),
Bombay SHRI M. Q. KHAN ( Alt.matc )
SHRI A. K. MISRA Bokaro Steel Plant, Bokaro SERI M. P. PATHAK ( Alternats )
SHRI M. RADHAERIBHNAN Central Machine Tool Institute, Bangalore SBRI S. HANUMANTHA RAO ( Al&mats )
SERI B. SAN~HAVI Lubrizol India Ltd, Bombay SHRI R. R. PARMAR ( Altarnate )
SHRI S. P. SARMA Hindustan Petroleum Corporation Ltd, Bombtiy SERI’D. W. RAUT ( Alternate )
SH~I S. SATHPATHY Bharat Aluminium Co Ltd, Korba SHRI S. C. VARBHNEY ( Altcrnatr )
SHRI M. J. SHAH SHRI S. P. PERE~A ( Ahnate)
Indian Oil Blending Ltd, Bombay
SHRI K. B. SHRIVASTAVA Tide Water Oil Co ( India ) Ltd, Calcutta SHRI J. NAIK ( Altematr I ) SHRI N. C. MITTAL ( Altmats II )
SEEI R. V. SINQH Hindustan Aluminium Corporation, Renukoot SERI 0. P. GUPTA ( Altmuztr )
