OrgoniCB Anolvaia Data Sheet.Data Reporting Oualifiarn T" — " '"
Conaral Dnta
Valuo - iConcentrat'ion Found (Value •> D L > ;D L . ' '0 -- Anaiyzed.for but hot detected '(Reported Value" la Detection Li.it)J . - Eitlkated Value: Target Compound -0< Value < DL; or
Tent. ID'o - A 1:1 reoponmo i« aaauaed for Quantisation.
• Adiuat6dVcc/Hs'ADLv iijfo&tad^^?g£u&.•-:•/;x"---. ;: ' .%^~- >.•«.>?;*••-•::->-.•..•".. ^' - ' •• '- Lont^-In^DiiOit < o n f - S«Bnl A - u « a — H < 1 nfraH-««--i«t.~k— *-Kii—"nj Wi.4. ;.i- i.i.'i^—:'_-j-j-.LID - Loot* In-Dilutidn>- SaBple -waa-diluted^oo -nuch~that Dibutyi" chlorendotew a o Loot I n Dilution. . ,
SEMIVOLATILE COMPOUNDS(ALL SOLID RESULTS REPORTED ON A DRY WEIGHT BASIS)
LEVEL: : - • • • • "DATE EXT/PREP:DATE ANALYZED:SPL—>EX TRACT:PH:X MOISTURE (NOT DEC. ):'/. MOISTURE (DEC. ):'"--•'.'STANDARD/I i>:- "•.•• .~:~.CTKIC T TT T I J T TV/ -^ T r\ . ••"•• ' 'OC.lMw 1 I I y i t .Y--*i- 1 U . -"-' .-e»H^.;
Value - Concentration Found (Value >, DL)DL - Detection Li»itU - Analyzed for but not detected (Reported Valuoi la Detection Licit;3 - Estimated Value: Target Conpound - 0 < Valua < DL; or
Tsnt. ID's - A 1:1 response is onounod for Quantitation.D - Conppund found in Blank. Ssnple results oro not Blank Corrected.K/A - Hot AnalyzedHR - Hot;ReportedMS - Hot'fSpiked,;.— .,;
Pesticide Qualifiers:
C - Confirmed by GC/HS; GC Ousntitotion Reported•o - Detected end Confirned by GC below GC/HS DL;
GC Guontitation Reportedi; - Hot Confiraod by GC/ttS; Atteeptod and unsucceauful*ot< - GC/HS Confiraation attempted and uneucceaaful because concentraticti
ia < GC/MJS DL;vGC Ouantitation reportedUN - GC/MSConfir'satibnattenpted and,,unaucceooful although nuopoct
Note: This section lists compounds on the HSL which were found in the Sample, MS, and/or MSD. It does notinclude Tentatively Identified compounds which may have been found in the, Sample.
Mr. Paul KefauverPedco EnvironmentalBox 11499 Chester RoadCincinnati, Ohio 45246
Dear Mr. Kefauver:
Please find enclosed the analytical reports for the samplessubmitted to Gulf Coast Laboratories on September 15, 1986.They were identified with our GCLfts 91469 and 91470.
If you have any further questions please contact ourlaboratories.
Sincerely,
GOLF COAST LABORATORIES, INC.
John Boudreau
JPB/sj
cc: Mr. Steve FaryenU.S. EPA
000185
GULF COAST LABORATORIES, INC.
2417 Bond St., University Park, Illinois 60466
Phones (312) 534-5200 (219)885-7077 (815)723-7533
The following is a list of flags that Gulf Coast Laboratoriesfrequently uses on our anlytical reports. All flags nay notbe applicable for the enclosed reports.
V
B - Indicates the compound was found in the blank as well asthe sample, it indicates possible/probable blank contamin-ation and warns the data user to take appropriate action.
E - Severe matrix interference
D - Result is on a dry weight basis
J - Indicates an estimated value
P - Peaks present but do not appear to be PCBs
U - Indicates compound was analyed for but not detected
Mr. Paul KefauverPedco EnvironmentalBOM 11499 Chester Road 46100Cincinnati, Ohio 45246
Dear Mr. Kefauveri
Please find enclosed method references for the EP Taxicitytesting procedures.
On May 19, 1980, the EPA published in the Federal Register thefirst phase of the RCRA Laws. It defines four characteristics ofhazardous waste to be used by persons handling solid waste todetermine if that waste is a hazardous waste. RCRA defines ahazardous waste as a solid waste that may cause or significantlycontribute to serious- illness or death, or that poses asubstantial threat to human health or the environment whenimproperly managed. EPA has listed four characteristics, any ofwhich would characterize it as a hazardous waste. They are;
1) IGNITABILITY - Identifies wastes that pose a fire hazardduring routine management. Fires not only present immediatedangers of heat and smoke but also are capable of spreadingharmful particulate matter over large areas. In general, thefollowing criteria establish ignitabilitya
Liquids - A flash point temperature below 60 C (140 F.)
Solids - Capable of causing fire through friction, absorption ofmoisture or spontaneous chemical reactions. When ignited burnsvigorously.
*Methodology - SU-846 Method 1010. A solid sample is prepared asa 50% suspension with Ethylene Glycol. The suspension is analyzedper SW-846, Method 1010.
2) CORROSIVITY - Identifies wastes requiring special containersbecause of their ability to corrode standard materials, orrequiring segregation from other wastes because of their abilityto dissolve toxic contaminants. The following criteria establishcorrosivity:
Liquids - A pH less than or equal to 2.0 or greater than or equalto 12.5. i
Solids — Any solids that exhibits corrosive properties.
•Methodology — A 1031 suspension of a solid sample is prepared -foranalysis by SW-846, Method 9040.
3) REACTIVITY - Identities wastes that during routine management,tend to react spontaneously, react vigorously with air or water,are unstable to shock or heat, generate toxic gases or areexplosive. Criteria that establish reactivity are any substancethat!
a) Is unstable and readily undergoes violent change withoutdetonation.
b) Reacts violently with water.
c) Forms potential explosive mixtures with water.
d) When mixed with water -forms toxic gases, vapors or -fumes inquantities that present danger to human health or theenvironment.
e) Is a cyanide or sul-fides bearing waste that can generate atoxic gases when exposed to pH conditions between 2 and 12.5units.
f) Is capable o-f detenation i-f subjected to a strong initiatingsource.
g) Is readily capable o-f detonation or explosive decompositionat standard temperature and pressure.
h) Is a -forbidden explosive as defined in 49 CFR 173.51, is aClass A explosive as de-fined by 49 CFR 173.88.
Reactive Cyanides is quantitated by determining the di-f-ferencebetween total cyanide content and the cyanide content o-f aportion o-f the same sample that is suspended in approximately 400mis o-f del an i zed water and the pH adjusted to 2 with 50% Aceticacid. The sample is stirred -for 24 hours and then analyzed -fortotal cyanides. The difference between the original result andthe treated results is reported as Reactive Cyanides.
Reactive Sulfides is quantitated by determining the differencebetween total sulfides content and the sulfides content of aportion of the same sample that is suspended in approximately 400mis of deionized water and the pH adjusted to 2 with 50% Aceticacid. The sample is stirred for 24 hours and then analyzed fortotal sulfides. The difference between the original result andthe treated results is reported as Reactive Sulfides.
TOXICITY - Identifies wastes that, when improperly managed, may,release toxicants in sufficient quantities to pose a substantialhazard to human health or the environment. A waste exhibits thecharacteristics of EP Toxicity if the extract, following theextraction procedure as described in Appendix II of 45 CFR 261,contains concentrations equal to or greater than the levelslisted below:
*Methodology - SW-846 Method 1310. All parameters aboveare referenced upon the attached Laboratory Summary.
*Methodology - SW-846 Method 1330. All parameters aboveare referenced upon the attached Laboratory Summary.
The other charts and graphs included with this report are thedata generated during the analysis of the sample and are includedfor your inspection. Analyses for Copper, Nickel, Iron and Zincare also included, but threshold values have not been establishedat this time. These probably will be included in the near futureand are now requested by some landfills, before they will accepta waste for disposal.
If you have any further questions please contact ourlaboratories.
EXTRACTION - Samples are prepared in accordance with SV846, Kethod1310. The extractor used is a 29 RPK multiple extraction unit, perSV-846, Method 1310, Figure 3. A picture is enclosed.
ANALYSIS - A summary of instrumentation, methodology, and specificwavelength is provided below. All analysis are conducted by StandardAddition per SV-846 methodology. A correlation coefficient of 0.095or greater is required by GULF COAST LABORATORIES, INC. QualityControl Protocol for all analysis which contain significant amounts ofthe parameter of Interest or contain a value greater than one-tenth ofthe maximum value established by EPA, per the May 19, 1980 FederalRegister.
For more specific Information, please refer to the attached benchsheets. A copy of each chromatogram for each parameter is enclosedfor your reference.
GULF COAST
2417 Bond St. Unb«nhy r«
MtonM O12) 534*200 Ulflj' "
::••.<*!*'& •.•;••••_.».,-;..«",.... • ' '-?• ..
(815)723-71
! EXTRACTION PROCEDURE TOXICITY
METHOD 1310 KEY
A. Gulf Coast Laboratories, Inc. Log Number
8. Sample Description
Sample Weight
D. Filtration Procedure for Liquid - Solid Separation
E. Volume of Mother Liquid
F. Method of Preservation of Mother Liquid
G. Grams of Solid Material
H. Sample Size Specifications (<9.5 mm)
I. Volume of Deionised Water for Extraction
J. pH Ledger
K. Volume of 0.5 N Acetic Acid Used to Adjust pH
Volume of Deionized Water Added Following Extraction
M. Final Volume of Combined Filtrates
N. Filtration Procedure of Solid Leachate
0. Verification of the Addition of Mother Liquid to Solid Phase Extract
P. Verification of Temperature Control (20 - 40 degrees C)
Q. Time Procedure was Started
aULF COAST LABORATORIES, INC.2417 Bond ft, Park Fomt South, Mneto 604M
994-ttOO
EXTRACTION DATA
Gulf Coast Laboratories NumberVolume of Mother Liquid A///\Mass of Solid Material Extracted I DP gDescription of Solid Phase >/ <9.5 mm >9.5 mmVolume of 0.5 N Acetic Acid to Extractor (^^ mlFinal Volume of Combined Filtrates c3Q£)(J mlFor specific pH data throughout the test, refer to attached extractiontoxicity key and the extraction raw data.
EXTRACTION DATA
Gulf Coast Laboratories Number. Q 1{(QVolume of Mother Liquid fj/A mlMass of Solid Material Extracted inO gDescription of Solid Phase \f <9.5 mm >9.5 mmVolume of 0.5 N Acetic Acid io Extractor ^QO mlFinal Volume of Combined Filtrates rvnnQmlFor specific pH data throughout the test, refer to attached extractiontoxicity key and the extraction raw data.
EXTRACTION DATA
Gulf Coast Laboratories Number . . ..,Volume of Mother Liquid AJ/r\ mlMass of Solid Material Extracted |D£) gDescription of Solid Phase y <9.5 mm >9.5 mmVolume of 0.5 N Acetic Acid to Extractor { 6£L mlFinal Volume of Combined FiltratesZ3QQT} mlFor specific pH data throughout the test, refer to attached extractiontoxicity key and the extraction raw data.
EXTRACTION DATA
Gulf Coast Laboratories NumberVolume of Mother Liquid • mlMass of Solid Material ExtractedDescription of Solid Phase <9.5 mm >9.5 mmVolume of 0.5 N Acetic Acid to Extractor mlFinal Volume of Combined Filtrates mlFor specific pH data throughout the test, refer to attached extractiontoxicity key and the extraction raw data.
EXTRACTION DATA
Gulf Coast Laboratories NumberVolume of Mother Liquid mlMass of Solid Material Extracted gDescription of Solid Phase <9.5 mm >9.5 mmVolume of 0.5 N Acetic Acid to Extractor mlFinal Volume of Combined Filtrates _ mlFor specific pH data throughout the test, refer to attached extractiontoxicity key and the extraction raw data.
162 TITLE PROJECT NO. V~T [
» BOOK NO. /3/0
I
ICIENDFIC IINDERY PSODUCTS CMICACO tOUA
DISCLOSED TO AND UNDERSTOOD BY
PROJECT NO.
BOOK NO. I3/O163,:->«!
SCIENTIFIC IINOERY PflODUCTS CHICAGO W6M
Sfc
164 TITLE
«?-3oO.T<4>'
* 'D>3
/*./??
L
/
5.0
s.t
3-r0.33.3
^•33'V'Y
/
/r
33/ "^'-^M*' >
•e.otl
,0H (,
•', Vix £?•'•'
34
I* • (
'
h.C L 0 .
. or
-o
•6>>'f
x
f.f-(** .f?
164 TITLE PROJECT NO.
BOOK NO.
.f '>.
DISCLOSED TO AND UNDERSTOOD BY
J J J JCHART NO. LIC-0100-C025
J J J J ] J J J J J J .
PRINTED IN USA.
CHART NO. L
, ) J J J J : J J J ] J J J J
.;!:> |l:;!_[.r;
i i r I i - i- !--• f •L! I.: -r<.. >.'LlLJ J.U- L:
H h i i i ! i -
I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I
CHA3T NO. LlC-0100-0025
L._-L. .4: . ij..ofi-i^-
I | I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I
3O
A*
x-%
—•».«•» 3- o • "C- J
00 \
. 250
£0-0 [
0-0(0
' %Li/^•* ''t '"'l** ifi'
;-.li",? ^•;^fe%.-•^i.'- ' '*?"
^•r:.*.
**/•
/L
/•rf.
31
I- 0 <><
/*•.i
C-L-
Z . J
t.t
o.
2V
i.
I I I I I I I I |
CHART NO. LIC-0100-0025
I I I I I I I I I I I I I I | I I I I I I I I <
I II I I
CHART NO. UC-01CO-0025 PRINTED l« US A.
I I I I I I
11111111111
CHART NO. LIC 0100-0025
/
•#£//£/
/.£H>t>
tf,ef.l
o.l
3.0
I- ~/.
5. b, ^
3Vt- -e,
5:?- i •-*-
/ 'Y -A
-«»«/
I II I
I I
._• ..-. _ ~7 ; | i . 1 • iT ~' • n—T—
' TTV n i f t r rn> iTV- j*-\- -i I , ; ' . ; ! - , . |^»
J^. , . - . . i , ; . i ; ; f . \?
r31
f ft /*>.?** t+j far*
t.i-
i -- o-
to-lit—0.01-
/>-/d < > . \tt 0-441
L
f-
32
•
1
i
,
•
!
I
1
.
i
1
1I
1
j
t ,
1
i
!iiiii
•
i
!ji
ii
i .c:!'C
D\u
. ; I . : i.. i . 1\.\ \ •. L ' ; L . J . : L.
I ' I !
Mr. i ./- -
11111111
4*4
r/7/
/u
HOt . t
36
CHART NO. LIC-0100-0025
I t I I I I I I I I I I I I I I I I t I I I I I t I I I I I | |
POINTED IN US A.
ART NO. LIC-0100-0025
I I I I I I I
PRINTED IN u 5 A. 11 III'
35
Al/3
(V
E-f«-Af,r
£7"
er"I*
t-l
l.f
• (
I (.if (- -o.-o-o*-
0.1
f > • ->
CHART NO. LIC-0100-0025 PR
I I I I I I I I I I I I I I I I I I I I I I I I I
3Of • •"> /">, <~v /I »-»
01C- ~o>{
t- ^D.
Cc (.* »<'
v.•i.,
fl?£*
tf./ ^'0
^ /•'«"' .
A ^. «A
•OO
A*/'/*
CHART NO. LIC-0100-0025 ^HINTED IN U S-*,
I I I • I I I I I
•*• .'V^-^^^^i*
1111111111111 1111 11111111 •
C > r- *-. n ,
2,oo fa* X(j^?* -*. * '.'•• •—L«i __---''""_
•_;.. ..A./..
1.0
.v-
t- -o tftf
2-52/zJ/
*•*!/,>-»
C.C
lie.
/ •••»
['too
^ ^p ./*
A^ /.^oo
^ /-^»
'*!/V
'£~ *~) /C
3O
35
36
4
' D / T L
PRINTED IN U 3 ACHART NO. LIC-0100-0025
I I I I I I I I I I I I I I I I I I I I I I I I I C I I I I I I I I I I I I I I •
30
).•
_s L ^o.vjf
7-.(
o.n(-0-ots
t>
O.T- - 6
£77- *- ^
Mt>
-0 /O
Ir
Mtf>
(
*•{••
/-/r
. 00
MsjJJk*
' ' 3*t>tn*in-^ *>A.fi
61 */w ^//-r ^*4£-1 ufr.4 ^/^-r ir
0-t
€>
/*•</0-/2-
6-llb
31
• >
CHART NO. LIC-0100-0025
( f • • ~- r~-r~i
CHART 1
111111111111 f 11111111111111111111111111111
1 'I • • ; i.:_i . . ! : ' : . , i il: i
12 TITLE I0
S PROJECT NO.
BOOK NO.
DISaOSEC TO AND UNDERSTOOD 6V
11 rut
Z/
/
/ i
J u
1 T
tKJNATURE DATE
6t$dOSED TO AND UNDERSTOOD BY DATE WITNESS DATE '
too r- 90 ' 80 ' 70 : CO • SO
zr—^J .:=rr-r:1
ir—!— ~ * " * ' '
?" i I =Ei
too
f '• «•"•"•
f/^N SPECIAL WASTE ANALYSIS REPORT /t\\Jjy This Report is intended for the sole use and benefit of Waste Management and its companies. N^^^^gK/
1 >^^^ Ho representation concerning significance of the reported data is made to any other person or entity, ^fyV x
r
LABORATORY NAME:
WASTE PROFILE !
COL , b,'
>HEET CODE ^
/,o,^-p, 1FROM SAMPLE CONTAINER 1
Adams Center Landfill (219) 447-5585 ^
AOHR^S . 4636 Adams Center Rd., Ft. Wayne, IN 46806 ,_.„„.,/ ^ / . ii
DATE SAMPLE RECEIVED AT IAB ., [3 > 3 1 •> ' DATE SAME TAKEN : /'•> I f '<- ' *^>
LAB SAMPLE NUMBER ASSIGNED:. •'j/i C" 0"n
CERTIFICATION Eicepi as explicitly noted, all analytical canalydca: equipment specified or approved in the most reellaboratory follows a quality assurance control program, inc
nATE OF RCPOHT- .. / _L
^ LAB MANAGER NAME: ^*"lfcOCA/ C,
ata reported below were obtained under my dir>nl "Test Methods lor the Evaluation ol Solid Wuding a sample chain of custody procedure.
SIGNATURE
l*^/\j tl.'v' T\,*—
r.FRTIFir ATinn OFection and supervision, using samasle. Physical/Chemical Methods.'
yl~r7 £~
REP SAMPLE OBTAINED?pie preparation and analytiSW 846. USEPA Office ol £
&.C?
PHYSICAL CHARACTERISTICS OF WASTE
SAMPLE VOLUME
/OfV
COLOR ODOR:
I-,/? /) iyV^t \. T
DESCRIBE
^^ Test
Specific Gravity
PH s. u . y^%Acidity % as
Alkalinity % as
C.O.D. mg/l
B.O.D. mg/l
Total Solids @ 105'C
Total Dissolved Solids mg/l
Residue on Evaporation @ 180*C
Flash Point F* (closed cup)
Ash Content, on ignition (%)
Heating Value, BTU/lb
"Acid Scrub." gNaOH/g
Arsenic, as As, mg/l
rd iumTaTBarmfl'V^Bromium as Br, mg/l
Cad"mu7tTi »Cd, mV/l
Chromium. Total as Cr, mg/l
Hexavalent Chromium as Cr, mg/l
Copper, as Cu, mg/l
Iron, Total as Fe. mg/l
lron..dissolved, as Fe, mg/l
Lead, aTpbTmfl'l ^^
Manganese, as Mn, mg/l
Maon- sium, as Mg, mgfl
Mercury, as Hg. mg/l
Nickel, as Ni, mg/l
Selenium, as Se, mg/l
Silver as Ag, mg/l
Zinc, as Zn, mg/l
Bicarbonates, as HCO,. mg/l
Carbonates, as CO,, mg/l
Chlorides, as Cl. mg/l
Flourides. as F, mg/
Nitrates, as NO,, mg/l
Nitrite, as NO. mg/l
Phosphate, as P. mg/l
Suilate. as SO., mg/lc..,«:^r r -,r C fnn'l
AsReceived
i -^fS- .2-
£7. 6l2
^7 7^
ExtractionProcedure
i
i
D NONE -9 MILD
D STRONG
^rtuJ&A'X'
Date ofAnalysis
i
i
PHYSICAL STATE « 70 'F
H] SOLID D SEMI-SOLID
D LIQUID Cl POWDER
Test
Radiation Screen
Penelrometer
Phenols, mg/l
Cyanides, as CN Total mg/l
Cyanides, as CN Free mg/l
Nitrogen Ammonia, as N mg/l
Total Kjeldahl Nitrogen as N mgfl
Total Alkalinity, P as CaCO, mg/l
Total Alkalinity M as CaCO,, mg/t
Total Hardness as CaCO,, mg/l
Calcium Hardness, as CaCO mg/l
Magnesium Hardness, as CaCO, mg/l
Oil and Grease, mg/l
LAYERS
G MULTILAYERED
Cl BI-LAYERED
Gr SINGLE PHASED
AsReceived/OO,
,/<TTd*l
Aldrin. mg/l
Chlorides.mg/l :
DDT , mg/l
Dieldrin, mg/l
Endrin, mg/l
Heptachlor, mg/l
Lindane, mg/l
Methoxychlor, mg/l
Toxaphene, mg/l
Parathion, mg/l
2,4, D, mg/l2, 4, 5 TP (Sllvex), mg/l
PCBs, mg/l
2,3,7,8 TCOD, u.g/1
tjQ jS/r-mf ^^ j* i~^f^*~•/ r
**n V W ' JfJ *9"\?
^volatile 0 /7;?
%Ash j_ /*"") -y '/<'/
*"*'«,« <5"-So-<
E YES 11 NOcal methods andolid Waste This
>
FREE LIQUIDS
VOLUME '''
ExtractionProcedure
'rsX-r/*"'
Date ofAnalysis
i
y/<D-J4-e61
'gnilab,,,,,, AJ^V
c""'*Scr«ii i ^viV/D ,--**
s"""V^reen -< AO^p^*
.Waste Management, Inc.' '. . ,. . . _..
GENERATOR'S WASTE MATERIAL PROFILE SHEET
WASTE PROFILE SHEET CODE
A GENERAL INFORMATION
GENERATOR NAME: I t/. J. C, T/3
FACILITY ADDRESS: L
pa-J TRANSPORTER: L TO
TRANSPORTER PHONE: I
GENERATOR USEPA I.D.
GENERATOR STATE I.D.
•
TECHNICAL CONTACT: 1_
NAME OF WASTE:' i -
TITLE: PHONE:
PROCESS GENERATING WASTE:
B PHYSICAL CHARACTERISTICS OF WASTE
CHEMICAL COMPOSITION (TOTALS MUST ADD TO 100".) JD METALS U TOTAL (PPM)
ARSENIC (As)
l& EPA EXTRACTION PROCEDURE (fng/L)
SELENIUM (Se)
COPPER (Cu) I
NICKEL (Ni)
ZINC (Zn)
THALLIUM (Tl)
F SHIPPING INFORMATION
D O.T. HAZARDOUS MATERIAL?
HAZARDOUS CHARACTERISTICS
REACTIVITY: IX NONE I I PYROPHORIC
D EXPLOSIVE CD WATER REACTIVE
OTHER HAZARDOUS CHARACTERISTICS.
NONE O RADIOACTIVE D ETIOLOGICAL
D PESTICIDE MANUFACTURING WASTE D OTHER I
USEPA HAZARDOUS WASTE? D YES D NO
USEPA HAZARDOUS CODE(S)
STATE HAZARDOUS WASTE? D YES D NO
STATE CODE(S) I
D SHOCK SENSITIVE
D OTHERPROPER SHIPPING NAME
HAZARD CLASS , O
METHOD OF SHIPMENT: D BULK LIQUID
D DRUM (TYPEJSIZE) I
ANTICIPATED VOLUME: I I GALS.
ONE TIME
D QUARTER
H SPECIAL HANDLING INFORMATION .
. DADDITIONAL PAGE(S) ATTACHED
I HEREBY CERTIFY THAT ALL INFORMATION SUBMITTED INSUSPECTED HAZARDS HAVE BEEN DISCLOSED.AUTHORIZED SIGNATURE
THIS AND ALL ATTACHED DOCUMENTS IS COMPLETE AND ACCURATE. AND THAT ALL KNOWN OR
TITLE DATE
of Suite 1501, Northbrook Office Courtf\\ 666 West Dundee Road, Northbrook, IL 60062 • (312) 498-909-1
TECHNICAL ASSISTANCE TEAM FOR EMERGENCY RESPONSE REMOVAL AND PREVENTIONEPA CONTRACT 68-01-6669 ' ^ . •.. • :$. . • •:
Re: Disposal Analysis for Belvidere Landfill Drums
f,
October 9, 1986
Dear Mr. Ewen:
Enclosed is the Generator's Waste Profile Sheet, Certification ofRepresentative Sample, and disposal analysis of composites of thedrum sludges. The Purchase Order Number for the waste acceptanceanalysis is PEI-86-2084-1083. If you have any questions aboutthe billing, please contact Paul Kefauver of PEI Associates,Inc., at (513) 782-4700. For any other matters, I may be reachedat (312) 498-9090.
I would appreciate if you could send copies of the profile sheet,certificate of representative sample, lab analysis, and disposaldecision to Sara Walton at the Chem Waste facility in Emelle,Alabama.
Thank you very much for your help.
Sincerely yours,
William H. ScovilleEnvironmental Engineer
Roy l ;. Westoii j Inc.SPILL PREVENTION & EMERGENCY RESPONSE DIVISIONIn A s s o c i i i i i o n w i t h 1CI? Inc. , Jacobs Eng inee r ing Group Inc., C.C.Johnson & Associates, Inc., and Tctra Tech, Inc.
••'•\^/tt^7&&?fi!r&$f&;&i!\-'
A GENERAL INFORMATION
, U. 5. £GENERATOR NAME:
FACILITY ADDRESS:
GENERATOR USEPA I.D. '
j GENERATOR STATE I.D. l
TECHNICAL CONTACT:
NAME OF WASTE I ^
PROCESS GENERATING WASTE
B PHYSICAL CHARACTERISTICS OF WASTE
EPA EXTRACTION PROCEDURE (mg/L)
i SELENIUM fS. 1 <*O«'
COPPER (Cu) I
NICKEL (Ni)
ZINC (Zn)
THALLIUM fTI)
CHROMIUM-HEX (Cr + 6) I
%VE OTHER COMPONENTS - TOTAL (PPM)
HAZARDOUS CHARACTERISTICS
REACTIVITY: C3 NONE ED PYROPHORIC ED SHOCK SENSITIVE
ED EXPLOSIVE ED WATER REACTIVE ED OTHER
OTHER HAZARDOUS CHARACTERISTICS:
NONE D RADIOACTIVE ED ETIOLOGICAL
ED PESTICIDE MANUFACTURING WASTE ED OTHER I
USEPA HAZARDOUS WASTE? BU YES ED NO
USEPA HAZARDOUS CODE(S)
STATE HAZARDOUS WASTE? B YI.S ED NO
CODES) I
Rl ONE TIME
LJ QUARTER
SPECIAL HANULING INFORMATION
ADDITIONAL PAGE(S) ATTACHEB
l Ml.HLUi' C t H T i r I MAT ALL INFORMATION SUBMITTED IN THIS AND ALL ATTACHED DOCUMENTS IS COMPLETE AND ACCURATE, AND THAT ALL KNOWN ORSUSI'F.CTCO HAZARDS HAVE BEEN DISCLOSED'•uiHOHiztu 'J i3f,JTuRE TITLE DATF
-•vo
CERTIFICATION OF REPRESENTATIVEGENERAL DIRECTIONS: IN ORDER TO DETERMINE WHETHER WE CAN ACCEPT THE SPECIAL WASTE DEIN THE ABOVE NUMBERED PROFILE SHEET, WE MUST OBTAIN A REPRESENTATIVE SAMPLE OF THE WAWILL ANALYZE THE SAMPLE TO VERIFY THE INFORMATION,;YOU HAVE PROVIDED US.'SOJT IS PARTKIMPORTANT THAT THE SAMPLE BE TRULY REPRESENTATIVE?^ MOST CIRCUMSTANCES YOU'WILL BE OETHE SAMPLE. HOWEVER, IN THOSE CASES IN WHICH WE OBTAIN THE SAMPLE, WE MUST ASK THATYOUR EMPLOYEES BE PRESENT TO DIRECT THE PARTICULAR SOURCE TO BE SAMPLED AND TO WITNSAMPLING. IN SUCH CASE, YOUR EMPLOYEE MUST SIGN THIS CERTIFICATION A3 A WITNESS.
' ' - • : - , ' '• - « • < % :- '-'« •- ''• '-V •.•"..•-..-"-.< ,i'..:i:',;'T,visf --:l:. -. . , - •THIS CERTIFICATION MUST BE RETURNED, WITH THE REPRESENTATIVE WASTE SAMPLE. TO:
THE UNDERSIGNED CERTIFIES THAT HE/SHE OBTAINED A REPRESENTATIVE SAMPLE OF THEMATERIAL DESCRIBED IN THE "GENERATOR'S WASTE MATERIAL PROFILE SHEET1' ABOVE REFERENCTHAT THE FOLLOWING REPRESENTATIONS ARE TRUE AND CORRECT:
/2.1. HOUR AND DATE OF SAMPLING:.
2. SOURCE FROM WHICH SAMPLE TAKEN:. ?XLl»v» -fi jUftoftl
EQUIPMENT AND SAMPLING METHOD USED:.
r/v-rfV« javyi
3.
4. AMOUNT OF SAMPLE OBTAINED: 2>
5. TYPE OF CONTAINER INTO WHICH SAMPLE WAS PLACED:_£a
/£>/*> /fit
6. THE SAMPLING EQUIPMENT USED, AND THE CONTAINER INTO WHICH THE SAMFPLACED, WERE THEMSELVES UNCONTAMINATED BEFORE USE.
7. AT THE TIME OF SAMPLING I AFFIXED A LABEL TO THE CONTAINER IN THE FOLFORM WITH THE FOLLOWING INFORMATION (FILL IN THIS PORTION, INCLUDINSIGNATURE, JUST AS IT APPEARS ON THE LABEL YOU PREPARED):
WITNESS VERIFICATION: I WAS PERSONALLY PRES-ENT DURING THE SAMPLING DESCRIBED; I DIRECTEDTHE WASTE SOURCE TO BE SAMPLED; AND I VERIFYTHE INFORMATION ABOVE NOTED.
WITNESS:
SIGNATURE:
TITLE:
EMPLOYER:
DATE:.
SAMPLER NAME:
SIGNATURE:.
TITLE: JEs
EMPLOYER: fo-i P.
DATE: /
_^V2feal*2fiJ
/ -.
FORM WMI-51 (R«v. 12/84)« 1980 WASTE MANAGEMENT. INC.
