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Copyright by Daejong Kim 2004
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Page 1: kimd042.pdf

Copyright

by

Daejong Kim

2004

Page 2: kimd042.pdf

Design and Fabrication of Sub-Millimeter Scale Gas Bearings

with Tungsten-Containing Diamond Like Carbon Coatings

by

Daejong Kim, B.S.; M.S.

Dissertation

Presented to the Faculty of the Graduate School of

The University of Texas at Austin

in Partial Fulfillment

of the Requirements

for the Degree of

Doctor of Philosophy

The University of Texas at Austin

May, 2004

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The dissertation Committee for Daejong Kim certifies that this is the approved version of the following dissertation:

Design and Fabrication of Sub-Millimeter Scale Gas Bearings

with Tungsten-Containing Diamond Like Carbon Coatings

Committee:

Michael D. Bryant, Supervisor

Frederick F. Ling

Wenjin Meng

Li Shi

Shaochen Chen

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Dedication

To my parents and family who endlessly loved and supported me

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v

Acknowledgements

I am grateful to all the people who were with me throughout the PhD program. Most

special appreciation goes to my advisor, Dr. Michael D. Bryant, for helping me and

guiding me to accomplish this work. I was very fortunate to have him as an advisor. He

has always motivated me, gave emotional support to overcome every difficulty

encountered during the work and led me to be a good researcher. Another special

appreciation goes to Dr. Frederick F. Ling, co-advisor, for leading me to this exciting

area and all his emotional support. I appreciate Dr. Wenjin Meng, Louisiana State

University for valuable advice and support for coating. I also appreciate Dr. Shaochen

Chen and Dr. Li Shi for their valuable advice and help to finish my PhD work.

Special thanks go to Yohannes Desta, Yoonyoung Jin, and Dr. Jost Goettert for their

help during the fabrication of gas bearings. Additionally, I thank Don Artieschoufsky,

Curtis Johnson, Danny Jares and John Pedrachine for their technical support for

machining parts and other staffs in the department. Partial support from NSF is also

acknowledged.

Special thanks go to Byungsoon Kim, Myungjin Kim and their family, who shared

happy and exciting life in Austin. Thanks to office mates, Jihoon, Sanghoon, Huijie and

other Korean graduate students in the department. Our family will miss all the wonderful

memories of neighbors and families in Brackenridge apartments. Finally, this work was

not possible without endless love and emotional support of my wife Donghee, my

children, Yushin and Edward, and my parents, brothers and sisters in Korea.

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vi

Design and Fabrication of Sub-Millimeter Scale Gas Bearings with

Tungsten-Containing Diamond Like Carbon Coatings

Publication No._____________

Daejong Kim, PhD

The University of Texas at Austin, 2004

Supervisor: Michael D. Bryant

Micro gas bearings of sub millimeter size (diameter of 500µm and length of

300µm) with micron clearances were designed and fabricated through X-ray lithography

and Ni electroplating. Details of the fabrication processes for the micro gas bearings are

described. Procedures to make X-ray mask and technical issues are discussed. Static and

dynamic hydrodynamic characteristics of the micro gas bearings were assessed using

Molecular Gas Lubrication (MGL) theory. Fabricated micro gas bearings had lower

stability than plain circular gas bearings due to lower load capacity and poor gas

damping. Improved bearing designs having non-symmetrical step geometry with deep

axial groove were suggested. These bearings were predicted to have much higher load

capacities and dynamic stabilities than the fabricated micro gas bearings.

Micro gas bearings were tested via an air jet-driven micro turbine made of SU-8,

press-fitted onto the shaft. A self-aligning assembly technique for the micro gas bearings

(using capillary action of photo resist) was developed and proved to be very effective.

Successful operation of micro gas bearings at 60,000 rpm was demonstrated under

limited operating conditions.

Tribological characteristics of Ni micro bearings and amorphous tungsten

hydrocarbon (W-C:H) coated micro bearings were investigated in dry friction mode,

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vii

using a newly designed micro tribo tester. 900nm thick uniform conformal coatings were

deposited onto the inner surface of micro bearings. Chemical and mechanical

microstructures were studied via X-ray Photoelectron Spectroscopy (XPS), Raman micro

spectroscopy. Wear rates, mechanical and material properties, and other tribological

characteristics of W-C:H coated Ni micro bearings were investigated and compared to

those of uncoated Ni micro bearings.

Uncoated Ni micro bearings, as deposited and annealed at 800oC, experienced

severe wear and appeared inadequate for tribological applications. Micro bearings with

low tungsten-containing (5% wt) hydrocarbon had higher wear resistance than micro

bearings with high tungsten-containing (11% wt) hydrocarbon. During the wear test of

the W-C:H coated micro bearings, a transfer layer formed on the counter steel shaft even

under very small contact pressure, leading to low steady state friction and high wear

resistance.

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viii

Table of Contents

List of Tables .................................................................................................................... xii

List of Figures .................................................................................................................. xiii

Chapter 1 Introduction .........................................................................................................1 1.1 Reliability Issue on MEMS...................................................................................1 1.2 Micro Gas Bearings ..............................................................................................2

1.2.1 Operating Principle of Gas Bearings ...........................................................2 1.2.2 Past Research on Micro Gas Bearings .........................................................4

1.3 Mechanism of Stiction of Two Surfaces in MEMS..............................................6 1.3.1 Capillary Force ............................................................................................6 1.3.2 Van der Waals Force....................................................................................8 1.3.3 Electrostatic Force .......................................................................................9

1.4 Review of Nano Scale Friction Study via AFM .................................................10 1.5 Past Studies on Coatings for MEMS devices .....................................................14

1.5.1 Chemisorbed Monolayer............................................................................15 1.5.2 Hydrocarbon Based Coatings ....................................................................16

1.6 Overview of Dissertation ....................................................................................18

Chapter 2 Fabrication Processes of Micro Gas Bearings...................................................19 2.1 Introduction.........................................................................................................19 2.2 Fabrication Processes of Micro Gas Bearings ....................................................20 2.3 X-ray Lithography on PMMA ............................................................................21

2.3.1 Substrate Preparation .................................................................................21 2.3.2 Material Selection for X-ray Mask ............................................................22 2.3.3 Fabrication Processes of X-ray Mask ........................................................24 2.3.4 X-ray Exposure and Development.............................................................26

2.4 Post Processes .....................................................................................................26 2.4.1 Electroplating.............................................................................................26 2.4.2 Processes to Form Thrust Bearings............................................................31

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ix

2.4.3 Sacrificial Layer Etching to Release Bearings...........................................32

Chapter 3 Static Performance of Micro Gas Bearings.......................................................35 3.1 Theory .................................................................................................................35

3.1.1 Journal Bearing ..........................................................................................39 3.1.2 Thrust Bearing ...........................................................................................43

3.2 Numerical Method ..............................................................................................46 3.3 Static Analysis ....................................................................................................47

3.3.1 Journal Bearing ..........................................................................................47 3.3.2 Thrust Bearing ...........................................................................................54 3.3.3 Rotational Friction Factor..........................................................................54

Chapter 4 Dynamic Performance of Micro Gas Bearings .................................................56 4.1 Approach.............................................................................................................56

4.1.1 Scheme for Numerical Integration.............................................................58 4.1.2 Stability Analysis: Threshold Speed..........................................................59

4.2 Discussion on the Whirl Instability.....................................................................64 4.2.1 Quasi-Stable Behavior of Stepped Bearings..............................................64 4.2.2 Threshold Rotor Mass................................................................................67

4.3 Design Improvement of Stepped Micro Gas Bearings .......................................69 4.3.1 Static Analysis of Improved Design ..........................................................70 4.3.2 Dynamic Analysis of Improved Design.....................................................73 4.3.3 Four-stepped Bearings with Axial Grooves...............................................76

4.4 Discussions from Stability Analyses ..................................................................84 4.5 Feasibility Study of Meso Scale Gas Bearing.....................................................84

4.5.1 Fabrication Processes of Meso Scale Gas Bearings ..................................84 4.5.2 Applications of Meso Scale Gas Bearings.................................................85 4.5.3 Three-Dimensional Imbalance Response ..................................................88

Chapter 5 Testing of Gas Bearings ....................................................................................97 5.1 Issues on Gas Bearing Tests ...............................................................................97 5.2 Testing of Micro Gas Bearings .........................................................................99

5.2.1 Assembly of micro gas bearings ..............................................................100

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x

5.2.2 Test Results..............................................................................................102

Chapter 6 Tribological Study of Micro Bearings ..........................................................112 6.1 Introduction.......................................................................................................112 6.2 Coating Process of W-C:H on Micro Sleeve bearings......................................115

6.2.1 Process conditions of W-C:H coatings ....................................................116 6.2.2 Material Properties of W-C:H coatings ...................................................117

6.3 Micro Tribo Tester ............................................................................................119 6.4 Results and Discussions....................................................................................123

6.4.1 Nickel Bearings........................................................................................123 6.4.2 W-C:H Coated Micro Bearings ...............................................................127

6.5 Summary and Conclusions of the Experiments ................................................132

Chapter 7 Future Work and Conclusions.........................................................................133 7.1 Future Works ....................................................................................................133

7.1.1 Hydrostatic Meso Scale Gas Bearing ......................................................133 7.1.2 Meso Scale Foil Gas Bearing...................................................................134 7.1.3 New Software for Performance Analyses of Gas Bearings .....................136 7.1.4 Advanced Testing Method of Gas Bearings ............................................137 7.1.5 Improvement of Micro Tribo Tester ........................................................139 7.1.6 Tribological Characteristics at Various Environments ............................139 7.1.7 Other Suggestions ....................................................................................139

7.2 Contributions and Conclusions of Dissertation ................................................140

Appendix A Discretization of the Gas Film Equation .....................................................143

Nomenclature...................................................................................................................149

References........................................................................................................................155

Vita ...............................................................................................................................162

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List of Tables

Table 2.1: Chemical composition of Ti oxidation solution............................................22

Table 2.2: Chemical composition of PMMA bonding epoxy ........................................22

Table 2.3: Chemical compositions of G-G developer and rinse ....................................26

Table 2.4: Chemical composition of Ni sulfamate solution and the process condition.29

Table 3.1: Numerical resolution for various grid schemes ( Λ=1, θR =-15o) .................48

Table 4.1: ω* and m* for stepped bearing with axial grooves (θS/θP =0.5, θR=0o) ....74

Table 4.2: ω* and m* for different θS/θP, the number of steps (θR=0o, ε=0.6, Λ=1) ...74

Table 4.3: Threshold speed ω* and rotor mass m* for four-stepped gas bearings with

axial grooves; C=1µm, step height=1µm, θS/θP =0.333 (θS =30o) ...............79

Table 4.4: Design parameters of LSU rotor ...................................................................88

Table 4.5: Design parameters of HDD rotor ................................................................88

Table 5.1: Load capacity and threshold rotor mass of plain micro gas bearings .........108

Table 5.2: Load capacity and threshold rotor mass of stepped micro gas bearings.....108

Table 6.1: Chemical composition and mechanical properties of 900nm thick W-C:H

coating.........................................................................................................117

Table 6.2: Wear rates of Ni bearings ...........................................................................124

Table 6.3: Wear rates of W-C:H coated micro bearings..............................................128

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List of Figures

Figure 1.1: Stiction failure of surface micro machined micro cantilever beam array

[Maboudian and Howe, 1997] ........................................................................2

Figure 1.2: Failure of poly silicon joint by surface friction [Tanner, 2000] .....................2

Figure 1.3: Operating principles of gas journal bearings ..................................................3

Figure 1.4: Micro fabricated micro gas bearing test rig [Lin, 1999].................................5

Figure 1.5: Capillary condensations around spherical asperity.........................................7

Figure 1.6: Surface energy balance at interface of three media ........................................7

Figure 1.7: Deformation of elastic sphere on rigid surface [Israelachvili, 1992]............13

Figure 1.8: Friction coefficients of 250nm thick DLC on glass: (a) Friction coefficient-

tip radius (b) Friction coefficient-applied load (contact pressure) [Bandorf et

al, 2003] ........................................................................................................14

Figure 1.9: Friction coefficient in (a) vacuum / ambient (b) dry N2 / ambient [Donnet et

al 1994] : Test conditions :contact pressure 1GPa ,sliding speed 1.7mm/s,

Ra=0.28nm, Steel ball on DLC.....................................................................17

Figure 2.1: Micro gas bearing design, the heights of steps and recesses are exaggerated,

and the overall diameter is 2mm: (a) Dimensions of journal bearings, (b)

Dimensions of thrust bearings ......................................................................19

Figure 2.2: Overall fabrication processes of micro gas bearings: (a) X-ray lithography,

(b) Ni plating/polishing, (c) SU-8 photolithography, (d) Ni plating/polishing,

(e) Photolithography/etching, (f) Releasing..................................................21

Figure 2.3: Absorption contrast of 3µm Ti membrane mask versus Au thickness with

various PMMA thicknesses ..........................................................................23

Figure 2.4: SEM image of patterned 13µm thick SPR: (a) overall image of bearings, (b)

near perfect vertical sidewall ........................................................................25

Figure 2.5: SEM images of Ti-membrane X-ray mask with 8µm thick Au absorber: (a)

Top view, (b) 2µm step in journal bearings..................................................25

Figure 2.6: Ti membrane X-ray mask with Au absorber.................................................25

Figure 2.7: Reaction in the Ni electroplating bath ..........................................................27

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xiii

Figure 2.8: Contamination of Ni electro deposit surface by nickel sulfide particles,

shown as small black dots on white Ni electro deposit ................................28

Figure 2.9: Non uniform current density at the edge of patterned plating mold cause non

uniform deposit thickness [Judy, 1996] ........................................................30

Figure 2.10: High magnification SEM image of bearing sidewall: cavity formed by air

bubbles attached to PMMM..........................................................................30

Figure 2.11: SEM images of bearing surface after different sacrificial layer etching time:

(a) Bearing surface after 2 days release (× 2K), (b) Bearing surface after 2

weeks release (× 2K).....................................................................................33

Figure 2.12: Higher magnification of Figure 2.11: (a) Bearing surface after 2 days release

(× 10K), (b) Bearing surface after 2 weeks release (× 10K).........................33

Figure 2.13: Micro gas bearing: (a) SEM images of overall bearing, (b) SEM images of

2µm steps on journal bearings before processing thrust bearings, (c)

Magnified image of 2µm step.......................................................................34

Figure 2.14: Surface morphology of bearing surface measured from AFM (scan length

10µm×10µm) and SEM: (a) AFM topography, (b) High magnification SEM

images ...........................................................................................................34

Figure 3.1: Journal bearing in normal operating condition .............................................36

Figure 3.2: Comparison of shear stress factor by Couette flow for fully diffusive walls;

database from Kang [Kang, 1997] and first order slip model.......................43

Figure 3.3: Grid scheme for control volume method ......................................................47

Figure 3.4: Stepped bearing configuration ......................................................................48

Figure 3.5: Static performance of stepped micro gas bearings (θR =5o) .........................50

Figure 3.6: Static performance of plain micro gas journal bearings ...............................50

Figure 3.7: Pressure profiles (Λ=1, ε=0.4) of fabricated stepped gas bearing ................51

Figure 3.8: Load parameters and attitude angles of stepped micro gas journal bearing at

ε=0.8 for different θR ....................................................................................52

Figure 3.9: Load parameters of stepped micro gas journal bearing at ε=0.6 and ε=0.98

for different θR ..............................................................................................53

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Figure 3.10: Circumferential pressure profile at the bearing center (Λ=0.2, θR= 25o)......53

Figure 3.11: Direction of load capacity vector F for the conditions in Figure 3.10 with

ε=0.98, Λ=0.2, and θR= 25o. ζX = 0.0318 and ζY = 0.0156............................54

Figure 3.12: Load capacity as a function of step height for thrust bearings .....................55

Figure 3.13: Non-dimensional rotational friction of micro gas bearing (θR =5o for stepped

journal bearings, step height 3µm for thrust bearings) .................................55

Figure 4.1: Journal bearing operating at an equilibrium point with eccentricity e, where

F is bearing reaction force represented as integral term in Equation (4.1)...57

Figure 4.2: Converging orbit from origin (stepped gas journal bearing, Λ=0.6, ε0=0.6,

ω*=0.4, C=1µm) .........................................................................................61

Figure 4.3: Diverging orbits Plain bearing: (a) Λ=1, ω*=1.6, ε0=0.6, (b) Stepped

bearing, Λ=3, ω*=2.7, ε0=0.8 .......................................................................62

Figure 4.4: Converging orbit (stepped gas journal bearing, Λ=2, ω*=1.5, ε0=0.8) ..62

Figure 4.5: Threshold speed map for plain gas bearings.................................................63

Figure 4.6: Threshold speed map for stepped gas bearings.............................................63

Figure 4.7: Stabilizing motion of journal to (εX,εY) =(0.694,0.547) by small disturbance

at (εX0,εY0)=(0.8,0), with Λ=0.6, ω*=0.9 ......................................................65

Figure 4.8: Motion of journal to (εX,εY) =(0.694,0.547) from origin for static loading

corresponding to (εX0,εY0)=(0.8,0) with Λ=0.6, ω*=0.9. The angle between

external load and eccentricity vector is attitude angle ..................................65

Figure 4.9: Pressure profile at (εX,εY)=(0.694,0.547) ......................................................66

Figure 4.10: Pressure profile at (εX,εY)=(0.8,0.0) ..............................................................66

Figure 4.11: Self sustained vibration by perturbation, 50 cycles, ε=0.8, Λ=1, ω*=1.7,

stepped gas journal bearing...........................................................................66

Figure 4.12: Stability chart of plain gas journal bearing given as non-dimensional

threshold speed m*........................................................................................68

Figure 4.13: Stability chart of stepped gas journal bearing given as non-dimensional

threshold speed m*........................................................................................68

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Figure 4.14: Axial grooves formed at the beginning of every step. Axial grooves supply

gas with ambient pressure to minimize high negative pressure and decrease

attitude angles ...............................................................................................69

Figure 4.15: Static performance for stepped gas journal bearings with axial grooves (θR=

0o): (a) Λ=1, (b) Λ=10...................................................................................71

Figure 4.16: Load parameter and attitude angle of six-stepped bearings without axial

grooves for various step configurations (θR=0o, ε=0.6, and Λ=1) ................72

Figure 4.17: Load parameter and attitude angle of four-stepped bearings without axial

grooves for various step configurations for (θR=0o, ε=0.6, and Λ=1) ..........72

Figure 4.18: Orbit for 50 cycles for four stepped bearing without axial grooves, θS/θP

=0.333, Λ=1, ε=0.6, step height 2µm, and ω*=6 (m*=1.5022, m=0.12g)....75

Figure 4.19: Four-stepped micro gas bearings with axial grooves....................................76

Figure 4.20: Static performance of four-stepped micro gas journal bearings with axial

grooves: (a) C=1µm, step height 2µm, (b) C=1µm, step height 1µm ..........77

Figure 4.21: Pressure profiles (Λ=1, ε=0.4) of four-stepped micro gas bearings with axial

grooves..........................................................................................................78

Figure 4.22: Orbit for 100 cycles of four-stepped gas bearings with axial grooves, Λ=1,

ε=0.6, and ω*=15: (a) Orbit for step height 1µm, (b) Orbit for step height

2µm ...............................................................................................................80

Figure 4.23: Orbit for 400 cycles of four-stepped gas bearings with axial grooves, Λ=1,

ε=0.6, step height 2µm, and ω*=40. Very slow chaotic motion initiates and

does not converge or diverge ........................................................................81

Figure 4.24: Orbit for four-stepped gas bearings with axial grooves, Λ=5, ε=0.6, ω*=5,

and step height 1µm: (a) Orbit for total 200 cycles, (b) Orbit for last 10

cycles.............................................................................................................82

Figure 4.25: Orbit for 200 cycles of four-stepped gas bearings with axial grooves, Λ=5,

ε=0.8, and step height 1µm: (a) Orbit for ω*=1, (b) Orbit for ω*=5, (c) Orbit

for ω*=10, (d) Orbit for ω*=20 ....................................................................83

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Figure 4.26: Conceptual figure of meso scale gas bearing with spiral grooved thrust

bearings, D=L=2mm.....................................................................................85

Figure 4.27: Laser scanner: (a) Assembled unit, (b) Rotor. The X-Y-Z is a fixed reference

frame and x-y-z is a rotational coordinate attached to rotor center ...............87

Figure 4.28: HDD spindle rotor: The X-Y-Z is a fixed reference frame and x-y-z is a

rotational coordinate attached to rotor center. y(Y) axis is into the plane....87

Figure 4.29: Rotor with angular rotation and eccentricity: The X-Y-Z is a fixed reference

frame with origin at the center of bearing and x-y-z is a rotational coordinate

attached to rotor center..................................................................................89

Figure 4.30: Three-dimensional imbalance response of HDD rotor, 50 cycles: (a) Orbit at

Z=0, (b) Stable rotor from initial misalignment (ψX0=0.2, ψY0=0.2),

Imbalance force: 0.56N, Speed: 15,000 RPM ..............................................93

Figure 4.31: Three-dimensional imbalance response of HDD rotor, 50 cycles: (a) Orbit at

Z=0, (b) Stable rotor from initial misalignment (ψX0=0.2, ψY0=0.2),

Imbalance force: 0.033N, Speed: 15,000 RPM ............................................93

Figure 4.32: Rotor orbits of Laser scanner rotor, 30 cycles; (a) 100,000rpm (b) 200,000

rpm (c) 300,000 rpm (d) 400,000rpm (e) 440,000rpm (f) 500,000 rpm (g)

600,000 rpm (h) 700,000 rpm (i) 800,000 rpm (j) 860,000 rpm...................95

Figure 4.33: Frequency spectrum of Laser scanner rotor orbit; (a) 660,000 rpm (b)

680,000 rpm (c) 700,000 rpm (d) 800,000 rpm ............................................96

Figure 4.34: Trace of misalignment of Laser scanner rotor at 860,000 rpm from initial

misalignment.................................................................................................96

Figure 5.1: Description of rotor running at certain eccentricity under given external

load................................................................................................................98

Figure 5.2: Macro scale gas bearing tester [Wilde and Andres, 2003] ...........................98

Figure 5.3: Meso scale turbo jet simulator supported by foil gas bearings [Heshmat,

2003] .............................................................................................................99

Figure 5.4: Photo of gas bearing tester; (a) Description of gas bearing tester (b) Photo of

assembled gas bearing tester (c) Capacitance sensor and drive shaft with

press-fitted SU-8 turbine.............................................................................101

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Figure 5.5: Assembly procedures of micro gas bearings; (a) Pre-assembly (b) Photo

resist dispensing (c) Soft baking (d) Anchoring to base (e) Release .......102

Figure 5.6: Photonic sensor signal measuring rotor speeds; (a) Supply pressure 35psi

(b) Supply pressure 50psi............................................................................102

Figure 5.7: Impulse turbine with open air jet ................................................................103

Figure 5.8: Simulated speed of dental drill turbine .......................................................105

Figure 5.9: Vibration signal from bearings with 2.3mg rotor; (a) Vibration signal from

plain bearing, speed 8890 rpm (b) Vibration signal from step bearing ......106

Figure 5.10: SEM images after operation for 1 hour with repeated start/stops every 5 to

10 minutes...................................................................................................107

Figure 5.11: New gas bearing tester with machined shroud to drive micro turbine; (a)

Shroud (b) Enlarged image of circled region in (a) (c) Photo of assembled

new gas bearing tester.................................................................................109

Figure 5.12: Photonic sensor signal measuring rotor speeds with new gas bearing tester

shown in Figure 5.11, supply pressure 35psi, plain gas bearing.................110

Figure 5.13: Simulated orbit of 2.3mg rotor supported by plain gas bearing at 60,000 rpm

with combined load of rotor mass and preload (7.4mg) .............................111

Figure 5.14: SEM image of plain gas bearing surface after test with new test rig shown in

Figure 5.11 ..................................................................................................111

Figure 6.1: Ni micro bearing: (a) Photograph of micro sleeve bearings, (b) SEM image

of Ni micro sleeve bearing surface before coating, the lower arc is the inner

diameter.......................................................................................................113

Figure 6.2: Microstructure of sidewall of electroplated Ni, as deposited and annealed

[Hemker et al, 2001; Cho et al, 2003].........................................................115

Figure 6.3: Fixture to coat W-C:H coatings on the micro bearings: (a) 1mm thick

stainless steel sheet with holes to hold micro bearings (b) Conformal coating

process of bearing surfaces .........................................................................116

Figure 6.4: Photo of W-C:H coated micro bearings......................................................117

Figure 6.5: Raman spectrum of new W-C:H.................................................................118

Figure 6.6: 900 nm thick uniform coating thickness on the bearing surface ................118

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Figure 6.7: SEM images of W-DLC2 coated bearing surface: (a) Low magnification

SEM image of W-DLC2 coated surface (b) High magnification SEM image

of W-DLC2 coated surface (×40K) ............................................................119

Figure 6.8: Micro wear tester: (a) Overview, (b) Detailed view within dotted circle in

(a), (c) Photo of micro wear tester ..............................................................121

Figure 6.9: Micro friction tester: (a) Schematic diagram, (b) Principle of friction

measurement (side view), (c) Photo of friction tester.................................122

Figure 6.10: Wear characteristics of as-deposited Ni bearings: (a) Top view, worn

materials moved along the axial direction and accumulated at the thrust

surface of the bearing (b) Inner bearing surface after test ..........................125

Figure 6.11: Wear characteristics of annealed (at 800oC for 1h) Ni bearings: (a) Top

view, worn materials moved along the axial direction and accumulated at

the thrust surface of the bearing as multiple layers (b) Inner bearing

surface after test ..........................................................................................126

Figure 6.12: SEM images of shaft tested against (a) As-deposited Ni bearing (b)

Annealed Ni bearings. No noticeable wear was observed..........................126

Figure 6.13: RPM-time relation of the W-C:H coated micro bearings ...........................128

Figure 6.14: SEM images of W-C:H coated micro bearing surfaces after wear test: (a) W-

DLC1 coated micro bearing (b) W-DLC2 coated micro bearing ...............128

Figure 6.15: Voltage signal from capacitance sensor and converted rotational angle of

horizontal bar attached to bearing holder with W-DLC1 coated bearing...130

Figure 6.16: Evolution of friction coefficient of W-C:H coated micro bearing..............130

Figure 6.17: Raman spectrum on the wear scar on the steel shaft tested with W-DLC2

coated bearing .............................................................................................131

Figure 6.18: SEM images of shaft tested against W-DLC2 coated bearing after 2hour

continuous wear test....................................................................................131

Figure 7.1: Conceptual design of hydrostatic micro gas bearing ..................................134

Figure 7.2: Detail fabrication processes of hydrostatic micro gas bearings..................135

Figure 7.3: Principle of foil gas bearings ......................................................................135

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Figure 7.4: Fabrication process of micro stamping mold for foil; (a) X-ray lithography

(b) Stacking (c) Solid micro stamping mold (d) Coated micro stamping

mold ............................................................................................................136

Figure 7.5: Gas bearing tester using reaction turbine....................................................138

Figure 7.6: Auxiliary devices for gas bearing tester in Figure 6.3: (a) Radial impulse

turbine (b) Centrifugal pump ......................................................................138

Figure A.1: Control volume (Figure 3.3 is repeated) ..................................................143

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1

Chapter 1

Introduction

The first part of this chapter addresses reliability issues of micro electro

mechanical systems (MEMS). The second part introduces the gas bearing, reviews

operating principles of gas bearings and past research on micro gas bearings. Various

surface forces causing stiction failures in MEMS devices and past nano scale tribological

studies via Atomic Force Microscopy (AFM) are reviewed. Finally, past tribological

studies on MEMS surfaces are reviewed, and the dissertation is overviewed.

1.1 Reliability Issue on MEMS

In physical systems, the surface area to volume ratio is inversely proportional to

L, the characteristic dimension of the system [Drexler, 1992]. Therefore, as a 3-D

structure is miniaturized, surface effects become very important in characterizing the

behavior of micro scale systems. Common failures of IC-processed MEMS are stiction,

during the release and operation in humid environment [Maboudian et al, 2000;

Mastrangelo, 1997; Ashurst, 2001]. In Figure 1.1, the low two micro machined

cantilevers failed via stiction to the bottom surface.

In the case of micro mechanical systems with a relative sliding contact, friction

and wear at the contact surface are critical factors for reliability and long-term

performance [Bhushan, 1996; Tanner, 2000; Beerschwinger, 1997]. Figure 1.2 shows

catastrophic failure of a polysilicon joint fabricated through surface and bulk micro

machining.

Bearing systems in micro rotating machinery should have sufficient load carrying

capacity, low friction and high wear resistance for continuous operation. Small bearing

friction can cause severe power loss.

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2

Figure 1.1 Stiction failure of surface micro machined micro cantilever beam

array [Maboudian and Howe, 1997]

Figure l.2 Failure of poly silicon joint by surface friction [Tanner, 2000]

1.2 Micro Gas Bearings To avoid wear and failure, frictionless bearings are needed. In practice, micro gas

bearings come close to this ideal.

1.2.1 Operating Principle of Gas Bearings Figure 1.3 explains the operating principle of gas journal bearings. The clearance

C between bearing and shaft was exaggerated. Pressure within the bearing clearance, to

support an external load, is generated via two mechanisms. One is a wedge effect

between the two converging surfaces. When a bearing is stationary and the journal shaft

rotates at a constant speed ω with eccentricity e, the converging wedge (at θ=0o ~180o) is

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3

formed. The pressure builds between the two converging surfaces to maintain gas flow

continuity at the inlet (θ=0o) and outlet (θ=180o), assuming no side leakage. When there

is side leakage (that is, for actual bearings), the pressure from the wedge effect is smaller.

The other mechanism is the squeeze film effect. When the gas film in the bearing

clearance is squeezed suddenly, escaping gas molecules feel resistance from surrounding

gas molecules, and a positive pressure is generated. The pressure profile in a journal

bearing causes the journal shaft to orient with attitude angle φ with respect to the load

direction. The main advantages of gas bearings over high precision ball bearings are

frictionless operation, negligible thermal degradation, and ultra high precision. Macro

scale gas journal bearings have been used for high precision and high speed rotating

machinery for decades.

Chapters 3 and 4 present a detailed mathematical model, to estimate the pressure

distribution in the bearing clearance, and numerical analyses of the static and dynamic

performance of the micro gas bearings.

Figure 1.3 Operating principles of gas journal bearings

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4

1.2.2 Past Research on Micro Gas Bearings Extensive research on micro gas bearings was performed at Massachusetts

Institute of Technology (MIT). Lin [Lin, 1999] demonstrated a test rig, with maximum

design speed of 2.4M rpm, shown in Figure 1.4. Deep Reactive Ion Etching (DRIE)

process was used to separate a rotor from bearing, resulting in a bearing clearance (C) of

about 10µm. The rotor diameter (D) and bearing length (L) were 4mm and 300µm

respectively, which resulted in L/D ratio of 0.0075 and C/D ratio of 0.003. Piekos &

Breuer [Piekos & Breuer, 1999], at MIT, performed hydrodynamic analyses of the micro

gas bearings embedded in the test rig. Orr Jr [Orr Jr, 2000] constructed a macro scale gas

bearing test rig with similar bearing geometry with the DRIE-processed micro gas

bearings, to validate the hydrodynamic analyseis of [Piekos & Breuer, 1999]. Frechette et

al [Frechette et al, 2001] demonstrated an electrostatic induction motor supported by the

DRIE-processed micro gas bearings.

The gas bearing test rig [Lin, 1999] was operated both in hydrostatic and

hydrodynamic modes. In the hydrostatic mode, compressed air was blown into the

bearing clearance from thrust side (along axial direction, see Figure 1.4), to generate a

fully developed journal bearing sump flow, and to levitate the rotor in the radial

direction1. Maximum speed was 110,000 rpm, far below the initial design speed (2.4M

rpm) in hydrostatic mode. In a hydrodynamic mode, 70,000 rpm was achieved for only

0.5 sec (total 500 rev). By continuous improvements (precision, supply pressure, etc) of

the test rig, they reached maximum 296,000 rpm in a hydrostatic mode [Lin, 1999].

In the macro scale, gas bearings are fabricated as separate components and

assembled to the system. However, in micro scale devices, assembly procedures are

known to be very tedious and time consuming. This led other researchers in micro gas

bearings to pursue single material monolithic structures. Problems of the silicon micro

gas bearings were, among others, use of limited micro machining process (DRIE), which

led to relatively a large bearing clearance, comparable to clearances of macro scale gas

1 In common hydrostatic gas bearings, air is supplied along the radial direction through small orifices or capillary tubes formed at the bearing surface.

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5

bearings with rotor diameters 50-100mm. Whirl instability due to the large bearing

clearance, and catastrophic failure of the silicon rotor upon touch-down to bearing (made

of silicon, too) resulted.

Rotor

Figure 1.4 Micro fabricated micro gas bearing test rig [Lin, 1999]

This work pursued new approaches. Micro gas bearings were fabricated as a

single component through X-ray lithography and electroplating. A stainless steel gauge

pin machined to ultra precision (±0.25µm), served as a journal shaft. Simple and very

easy assembly processes using self-aligning concepts (such as surface tension or

precision dowel pins) were developed. Detailed specifications and fabrication processes

will be discussed in Chapter 2.

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6

1.3 Mechanism of Stiction of Two Surfaces in MEMS As discussed earlier, one of the failure mechanisms of IC-processed MEMS

devices is stiction caused by strong surface forces, generated during release and/or

operation of the devices. Stiction also causes high friction in MEMS devices. In this

section, various surface forces are reviewed, and methods to minimize these surface

forces and friction are suggested.

1.3.1 Capillary Force When a microscopic asperity is close to a flat surface in a humid environment as

in Figure1.5, water vapor undergoes capillary condensation and forms a liquid meniscus.

The Kelvin radius of the meniscus rk is defined [Israelachvili, 1992] as

21

21

rrrr

rk += (1.1)

where r1 and r2 are radii of the meniscus curvature in principle directions. In a spherical

meniscus, r1=r2=rK. In a cylindrical meniscus, r2=∞. The Kelvin radius, derived from

equilibrium of the chemical potential across the meniscus surface, is given by

[Israelachvili, 1992] as

)100/log(%ˆ RHTR

r LVk

νγ= (1.2)

where, RH is relative humidity (%), γLV and v are surface tension and molar volume of

water, respectively, and R is the ideal gas constant.

The adhesion force associated with liquid condensation arises from pressure

differences across the meniscus is given by [Israelachvili, 1992]

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7

θγπ cos4 LVcap RF = (1.3)

Here, θ is the water contact angle on the solid surface, determined from a force balance

at the interface between water droplet, the vapor phase and the solid surface as in

Figure1.6. The force balance equation is called Young’s equation [Meyer et al, 2000],

given as

SVSLLV γγθγ =+cos (1.4a)

or

LV

SLSV

γγγ

θ−

=cos (1.4b)

r1

R

x y

φ

θ

θ r1cosθ r1

(a) (b)

Figure 1.5 Capillary condensations around spherical asperity

γSV

γSL

γLV

θ

Figure1.6 Surface energy balance at interface of three media

When a sphere and a flat surface are separated by a distance d, the capillary

attractive force can be derived by minimizing the surface free energy, keeping constant

liquid volume, as

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8

drRr

dyyRdF

K

LVKLVcap +

=+

θγπθγπ

cos2cos8

cos4)(2

(1.5)

From equation (1.5), the capillary force depends on the water contact angle θ, and

the relative humidity of the environment.

When the surface energy of solid γSV exceeds the solid-liquid interfacial energy

γSL, i.e., θ <90 o, the surface is hydrophilic and attractive. When γSV is smaller than γSL,

i.e., θ >90o, the surface is hydrophobic, making the capillary force repulsive. Minimizing

the surface energy γSV and increasing the water contact angle θ for a given relative

humidity can reduce capillary attractive forces.

1.3.2 Van der Waals Force Van der Waals force originates from dipole-dipole interaction between molecules.

There are three kinds of dipole-dipole interactions: permanent dipole-permanent dipole

(between polar molecules, called Keesom type); permanent dipole-induced dipole (Debye

type); and induced dipole-induced dipole (called London dispersion force). The

interaction energy W(r) between two molecules (dipoles) can be represented as

[Israelachvili, 1992],

6)(rCrW −= (1.6)

for all the three types of dipole-dipole interactions. Here, C is a constant for given

temperature, depending on the type of dipole interaction and r is distance between the

molecules.

Adhesion forces by van der Waals interaction between macroscopic particles

result from integration of the interaction energy, given by equation (1.6), over all atoms

or molecules that constitute the two surfaces. For a macroscopic sphere of radius R and a

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9

flat surface separated by d, the adhesion force due to the van der Waals interaction can be

derived as [Israelachvili, 1992]

d

HRdFwdw 6)( = (1.7)

Here, H is called Hamaker constant, a property depending on the materials of the two

surfaces. The adhesion force per unit area between two flat surfaces becomes

36)(

dHdfwdw π

= (1.8)

Equations (1.8) and (1.9) are not valid for d=0 because the interaction potential,

equation (1.6), accounts for only attraction energy when the distance is larger than

intermolecular or inter atomic distance.

1.3.3 Electrostatic Force

When electric field is applied between two surfaces, static surface charges build

up on the surface and electrostatic forces arise by Coulom attraction. When a sphere and

a flat surface are close compared with the radius of the sphere, the electrostatic attractive

force is given by [Arai et al, 1996]

εεσπσ

0

221)( RdFelec = (1.9)

Here, σ1 andσ2 are charge densities of the two surfaces,ε0 is the permittivity of free space,

and ε is dielectric constant of the media between the sphere and flat surface. For two flat

surfaces, the electrostatic attraction per unit area becomes

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10

20

21

4)(

ddfelec επε

σσ= (1.10)

From the above, van der Waals forces are unavoidable. Electrostatic force is

generated only when an electric field is applied. However to minimize electrostatic

attractions after an electric field is removed, the charges trapped on the surface should be

quickly dissipated. Highly conductive materials help dissipate surface charge. Reducing

surface energy of the material can minimize capillary attractive forces in humid

environments. By choosing adequate materials and surface modification processes, it is

possible to reduce stiction failures and friction in MEMS devices.

1.4 Review of Nano Scale Friction Study via AFM Dry friction without liquid lubricants can be classified into adhesion-controlled

and load-controlled friction [Meyer et al, 2000]. In adhesion-controlled friction, the load

is usually small enough for the contact deformation to be elastic (usually with no wear).

The friction force depends on the interfacial properties such as surface energy and

presence of boundary lubricants. In load-controlled friction, the friction force is less

sensitive to interfacial properties or environmental factors such as humidity, and depends

more on bulk mechanical properties such as hardness, Young’s modulus, and toughness.

High stress, concentrated at the local contact, causes wear and damage to the surface

layers. The dry friction force at the macro scale can be interpreted as a summation over

the adhesion-controlled and load-controlled friction force.

Very light loads usually characterize working conditions of MEMS surfaces.

Therefore, studies on tribological characteristics of MEMS surface employed AFM or

Surface Force Apparatus (SFA) to simulate single asperity contact under very light load

[Lu and Komvopoulos, 2001; Schwarz et al, 1997; Enachescu et al, 1998]. Typical nano

tribological studies using AFM had contact load of 10~100µN, sliding speed of ~µm/s,

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11

and tip radius of 20~100nm. In this section, issues on nano scale study on adhesion-

controlled friction (under elastic contact), are investigated.

Modern theory of adhesion-controlled friction employs Bowden and Tabor’s

adhesion model [Meyer et al, 2000], in which the friction force

Rf SAF = (1.11)

is proportional to real contact area AR and the interfacial shear strength S, dependent on

the interfacial conditions such as surface energy and lubrication. The dependence on load

is contained in the real contact area AR. Nano tribological studies of different carbon

based coatings [Schwarz et al, 1997; Lu and Komvopoulos, 2001] and diamond and WC

interfaces [Enachescu et al, 1998], showed that S is nearly constant, and the friction force,

between a single asperity and a smooth surface at the atomic level, is proportional to the

contact area predicted by Johnson, Kendal and Roberts (JKR) or Derjaguin, Muller and

Toporov (DMT) contact model (explained later). They used accurately manufactured

nano scale tips (17~58nm radius) to simulate single spherical asperity contact.

A simple contact model to estimate the contact area for single asperity contact is

Hertzian [Johnson, 1985], in which the deformation of two spherical surfaces is assumed

elastic. The contact area follows from elastic theory is given by

3/2

=

KFR

A eeπ (1.12)

where 1

2

22

1

21 11

34

−+

−=

EEK

νν (1.13)

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12

is an effective elastic modulus based on Young’s modulus E1, E2 and Poison’s ratio ν1, ν2

for the contacting surfaces and Fe is an external force. In the foregoing, an effective

radius Re of the two contacting curved surfaces becomes

21

21

RRRRRe +

= (1.14)

If surface energy effects and elastic deformations are considered, the JKR model

predicts contact area well for materials with high surface energy and low stiffness

[Schwarz et al, 1997; Enachescu et al, 1998]. The DMT model accurately predicts the

contact area for materials with low surface energy and high stiffness.

The contact area between two spheres, when adhesion force Fa is considered, is

given by, from equation (1.12), 3/2)(

+

=K

FFRA aeeπ (1.15)

Here 2)3(63 adeeadeadea WRFWRWRF πππ ++= for JKR model

eada RWF π= for DMT model

where Wad is work of adhesion, given by [Israelachvili, 1992],

1221 γγγ −+=daW (1.16)

Here, 1γ and 2γ are surface energy of two surfaces and 12γ is an interfacial surface energy

between surface 1 and surface 2. When two surfaces consist of the identical material,

12γ=daW . The contact area A increases with the surface energy of the solid surface. As

seen in Figure 1.7, in the presence of surface energy, two surfaces tend to adhere even

without external force.

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13

Figure 1.7 Deformation of elastic sphere on rigid surface [Israelachvili, 1992]

Putting the contact area predicted by JKR or DMT model into the adhesion-

controlled friction equation (1.11) yields

( ) 3/23/2aeef FFCRF += , where

3/2KSC π

≡ (1.17)

Because C is constant (S is constant as assumed earlier), the friction force depends on the

radius of asperity, the surface energies of the two surfaces, and external force. The

friction force depends on the AFM tip radius, surface energies of the two surfaces, and

external force. If surface energies are very small, Fa can be neglected and Ff is

proportional to R2/3.

Another noticeable fact is that the equation (1.17) is only true for very small

sliding speed, where relaxation time of the atoms experiencing elastic deformation during

the scanning of AFM tip is much smaller than the inter atomic distance divided by the

scanning speed. Figure 1.8 shows the tendency of nano scale friction, where nano scale

friction coefficients of DLC coatings on a glass wafer increased, as AFM tip radius and

applied load (contact pressure) increased [Bandorf et al, 2003].

Tip radius, surface energy, and scanning speed-dependent behavior of friction

forces makes comparison of measured nano scale friction coefficients, to friction

coefficients measured by other methods, difficult, especially if the test environment and

tip radius are not known exactly, or the tip is not perfectly spherical.

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14

Surfaces of micro mechanical systems possess multiple nano meter scales

asperities and follow fractal geometry characterized by self-affinity over a wide range of

length scales [Ling, 1990]. Even if the load is very small and the macroscopic contact

pressure is far below the elastic limit of the materials, some local asperities will

plastically deform because of concentrated loads on those spots. Therefore, wear can be

induced even under an extremely small load, which complicates investigation of

frictional behavior of actual MEMS surface and also makes it difficult to estimate a real

friction from nano scale friction via AFM.

In this work, direct characterization of the working surface of the micro bearings

(sidewalls), under similar working conditions of the micro bearings, was pursued via

specially designed tribo tester. Detailed investigation and test results are presented in

Chapter 6.

(a) Friction coefficient-tip radius (b) Friction coefficient-contact pressure

Figure 1.8 Friction coefficients of 250nm thick DLC on glass: (a) Friction

coefficient-tip radius (b) Friction coefficient-contact pressure [Bandorf et al, 2003]

1.5 Past Studies on Coatings for MEMS devices In this section, past research on tribological coatings for MEMS devices,

chemisorbed monolayers on hydrophilic silicon oxide surfaces, and DLC coatings are

reviewed.

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15

1.5.1 Chemisorbed Monolayer The chemisorbed monolayer, well known for nano scale thin anti-stiction coatings,

modifies hydrophilic oxide surfaces to hydrophobic surface by long chain molecules with

non-polar end groups. The attractive force an atom has for shared electrons in a molecule

is its electro negativity. The polarity of end groups forming long chain molecules is

determined by the difference of electro negativities of constituent atoms. The larger the

difference, the larger the polarity of the end group. End groups such as –OH (hydroxyl), -

COOH (carboxyl), -SH (thiol), -SiCl3 (trichlorosilane) with strong polarity, can anchor

the molecule to the surface. Non-polar end groups such as -CH3 (methyl), -CF3

(trifluoromethyl) can decrease surface energy and form hydrophobic end groups.

Octadecyl-Trichloro-Silane (C18H37SiCl3) monolayer (OTS) coatings [Maboudian

and Howe, 1997; Ashurst, 2001], have -CH3 end groups to lower surface energy.

Compared to physisorbed Langmuir-Blodgett monolayers formed by weak van der Waals

bonds, OTS molecules have strong covalent bonds to the oxide surface and show high

durability even under large load [Berman et al, 1998; Ruhe et al, 1993; DePalma and

Tillman, 1989]. The chain length of one OTS molecule determines the coating thickness.

The OTS has 18 carbons, rendering a thickness of 2.5nm.

Friction coefficient of OTS coating on SiO2 wafer, measured via pin-on disc test,

was 0.07 under various loads and sliding speeds [Bhushan et al, 1995; DePalma and

Tillman, 1989]. Xiao et al [Xiao et al, 1996] and Israelachvili [Israelachvili, 1992]

showed that attractive van der Waals force between molecules plays an essential role in

ensuring good close packing and self-organization of the molecules. They also showed

that alkylsilane molecules having -CH3 end group should have more than 10 carbon

atoms to have high packing density and low friction.

Perfluorodecyltrichlorosilane (CF3(CF2)7(CH2)2SiCl3) monolayers (FDTS) seems

to be more promising compared to OTS [Srinivasan et al, 1998]. FDTS has -CF3 end

groups, with lower surface energy (6mJ/m2) than OTS (22 mJ/m2). FDTS shows more

stable characteristics at high temperature. OTS degraded above 150oC but FDTS could

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16

withstand up to 400oC in air. Electrical properties are also important reducing permanent

stiction in MEMS device. FDTS has much lower resistivity than OTS, which leads to less

surface charge accumulation and low stiction. A FDTS coated cantilever actuator showed

far superior performance over 40 million cycles without failure compared to an OTS

coated actuator [Srinivasan et al, 1998].

Teflon-like fluorinated hydrocarbon coatings (FC) consisting of CFx chains,

grown commonly by plasma polymerization [Yasuda, 1985], also show very low surface

energy of 7mJ/m2 and high durability in wear tests (collapse cycles of cantilever) even at

400oC [Mastrangelo, 1997]. Periodic contact tests with an actuated cantilever showed 108

collapse cycles at 150oC without any degradation of 20nm thick FC films [Mastrangelo,

1997].

Despite very low surface energy and high reliability, during repeated collapse

cycles in certain conditions, sliding wear resistance and long-term reliability of these

chemisorbed monolayer coatings are questionable, especially in harsh environments.

1.5.2 Hydrocarbon Based Coatings

Carbon based films such as graphite, polycrystalline diamond, amorphous hydro

carbon (a-C:H or DLC), and metal containing hydrocarbon (Me-C:H) are widely used for

low friction surfaces in macro scale applications. Various techniques have studied

microstructure, mechanical properties, and tribological characteristics of these films

[Koskinen et al, 1998; Donnet. and Grill, 1997; Erdemir et al, 2000; Liu et al, 1997; Shi

et al, 2000; Cao et al, 2001].

In the macro-scale pin-on disc tests, steel or ceramic balls are rubbed against flat

surface with DLC coatings. Adsorbates such as oxygen or moisture affect the result

significantly, especially at low speed tests [Donnet et al 1994]. Typical friction

coefficients versus time in ultra high vacuum (UHV), in dry nitrogen and ambient are

shown in Figure 1.9. Initially the friction coefficient is high, but after a break in period,

lower steady state values appear in UHV and dry nitrogen environments.

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17

Feasible theory for low friction in UHV or inert environment is graphitization of

the sp3 carbon structure (diamond phase) during the initial break in period suggested by

several researchers [Liu et al, 1996; Liu et al, 1997, Donnet et al, 1994; Koskinen et al,

1998]. Hydrogen within DLC is released from sp3 carbon at about 450oC, which leads to

collapse of sp3 carbon to sp2 carbon. Frictional heating and sliding-induced strain energy

in the surface layer seems to cause extensive graphitization [Liu et al, 1996].

(a) (b)

Figure 1.9 Friction coefficient in: (a) Vacuum / ambient (b) Dry N2 / ambient [Donnet et al 1994] ; Test conditions :contact pressure 1GPa ,sliding speed 1.7mm/s,

Ra=0.28nm, Steel ball on DLC

Recent research on highly hydrogenated DLC [Erdemir et al, 2000] revealed the

importance of hydrogen to very low friction in vacuum or dry nitrogen environment.

Erdemir [Erdemir et al, 2000] suggested the passivation of dangling bonds of surface

carbon by continuously released hydrogen atoms from bulk DLC, and strong repulsion

between the surface hydrogen atoms, to be the main cause of ultra low friction.

Despite promising tribological characteristics and proven performance of DLC in

macro scale applications, direct applications to MEMS have been limited. Beerschwinger

et al [Beerschwinger et al, 1995] measured friction of DLC coating on flat silicon surface,

via surface micro machined small friction tester. Bandorf et al [Bandorf et al, 2003]

showed that DLC on soft polymer surface had better wear resistance than DLC on silicon

wafer. Mousinho et al [Mousinho et al, 2003] demonstrated microstructures made with

DLC film, deposited by RF magnetron sputtering. Cao et al [Cao et al, 2003] coated Ti-

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containing DLC (Ti-C:H) on Ni micro mold insert, fabricated by X-ray lithography and

electroplating. However, applications of DLC coatings to the sidewall of micro scale

mechanical parts, that experience sliding contacts (bearings, gears, etc), have not been

reported.

1.6 Overview of Dissertation This chapter briefly reviewed reliability of past micro rotating machinery

including benefits of micro gas bearings and current research. Various surface forces, and

related failures were introduced. Nano scale friction studies via AFM, and limitations

interpreting the results were addressed. Also reviewed were tribological studies on

chemisorbed monolayers for oxide surfaces and hydrocarbon (DLC) for macro scale

applications.

Chapter 2 will present fabrication processes for micro gas bearings. Procedures to

make an X-ray mask and technical issues will be discussed. Finally, SU-8 lithography,

electroplating principles, and other issues will be addressed.

Chapter 3 and 4 will investigate static and dynamic performance of the fabricated

micro gas bearings using Molecular Gas Lubrication (MGL) theory and improved

designs will be suggested in terms of load capacity and dynamic stability. Fabrication

methods of meso scale gas bearings, via X-ray lithography and precision assembly

techniques will be proposed. Performance analyses of the meso scale gas bearings will be

presented in terms of three-dimensional imbalance response.

Chapter 5 will give test results of micro gas bearings with a simple air jet driven

turbine configuration. Technical issues involved in the testing will be also addressed.

Chapter 6 will present tribological characteristics of tungsten containing

hydrocarbon (W-C:H) coated micro bearings, compared with uncoated micro bearings.

Finally, chapter 7 will suggest future work and summarize contributions and conclusions

of the dissertation.

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Chapter 2

Fabrication Processes of Micro Gas Bearings

In this chapter, detailed fabrication processes of micro gas bearings are described.

Procedures to make X-ray mask and technical issues are discussed. Finally SU-8

lithography, electroplating principle, and other issues are addressed.

2.1 Introduction

Figure 2.1 shows the configuration and dimensions of fabricated micro gas

journal bearings with thrust pads. The journal bearings have several evenly distributed

recesses 2µm deep along the circumferential direction, to control inherent whirl

instability [Cheng and Pan 1965; Castelli and Elrod, 1965]. Thrust bearings with 4 thrust

pads, 3µm high with an angular width of 30o, were integrated with the journal bearing.

Radial grooves with an angular width of 20o and a 100µm depth were formed at the end

of every thrust pad to present atmospheric pressure to the beginnings and ends of thrust

pads. The inner and outer diameters of the thrust pads are 0.6mm and 1.5mm respectively.

2µm step

300µm

φ 500µm

20o

30o

3µm step

φ 1.5mm

φ 600µm

100µm deep groove

Figure 2.1 Micro gas bearing design, the heights of steps and recesses are

exaggerated, and the overall diameter is 2mm

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20

2.2 Fabrication Processes of Micro Gas Bearings

The design specifications of the micro gas bearings require a high degree of

circumferential roundness and limit the deviation from a perfect vertical sidewall to

within 0.5µm, to maintain the nominal clearance of 1µm between the bearing and shaft.

The bearing surfaces must have a surface roughness less than 50nm to ensure

hydrodynamic operation. To meet these very strict geometrical tolerances, unique

fabrication processes were developed that combined X-ray lithography, electroplating,

and wet etching.

The sequence of fabrication processes (shown in Figure 2.2) to make the micro

gas bearings (Figure 2.1) include the following steps: (a) bonding of 2mm thick PMMA

(polymethylmethacrylate) sheet atop a TiO sacrificial layer and fly cut to a 320µm thick

layer, followed by X-ray exposure and developing with a G-G solution; (b) Ni

electroplating and polishing down to the PMMA layer; (c) spin coating of a 100µm-thick

SU-8 layer, followed by UV lithography to pattern a mold for electroplating thrust pads;

(d) a second Ni electroplating and polishing down to the SU-8 layer; (e) a photo resist

spin, photolithography, and wet etching of the Ni to make 3µm steps; (f) removal of all

photo resists, and a sacrificial layer etching to release the bearings. The detail procedures

of each process are explained in the following sections.

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21

(a) X-ray lithography (b) Ni plating/polishing (c) SU-8 photolithography

(d) Ni plating/polishing (e) Photolithography/etching (f) Releasing

Figure 2.2 Overall fabrication processes of micro gas bearings: (a) X-ray lithography, (b) Ni plating/polishing, (c) SU-8 photolithography, (d) Ni

plating/polishing, (e) Photolithography/etching, (f) Releasing

2.3 X-ray Lithography on PMMA

2.3.1 Substrate Preparation

A layer of 2µm thick Ti was evaporated onto a 1mm thick Alumina ceramic wafer,

which becomes a substrate for subsequent processes. The Ti was partially oxidized in

sodium hydroxide and hydrogen peroxide solutions at 65 °C to improve adhesion of the

PMMA sheet. The partially oxidized Ti layer has very low electrical resistivity and serves

as a seed layer for subsequent Ni plating (Figure 2.2b) and also as the sacrificial layer

when making the final Ni bearing in Figure 2.2(f). The detailed composition of the Ti

oxidation solution is given in Table 2.1.

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22

A commercially available 2mm-thick PMMA sheet of CQ grade2 was bonded on

top of the ceramic substrate with the partially oxidized Ti layer. Detailed information on

bonding epoxy for the PMMA sheet is given in Table 2.2

Table 2.1 Chemical composition of Ti oxidation solution

Chemical Quantity Hydrogen peroxide (H2O2) 30% solution 2.04g Sodium hydroxide (NaOH) 2.0g DI water Up to 100ml

Table 2.2 Chemical composition of PMMA bonding epoxy

Chemical Amount Purpose MEMO3 0.10g Resist adhesion promoter BPO4 0.15g Catalyst as hardener (radical builder) DMA5 0.10g Polymerization Initiator MMA6(85%)/PMMA(15%) 10.0g Bulk resin

To reduce the stress of the bond resin and increase the molecular weight, >1%

BPO was used to minimize the monomer content below 0.5% [Madou, 2002]. The

prepared epoxy resin was placed in the vacuum oven for 3 minutes to remove air bubbles

in the resin. The PMMA sheet was bonded under constant pressure (20psi) for 8 hours to

allow complete polymerization of the bonding epoxy. The bonded PMMA sheet was cut

to 350µm thickness with a fly cutter.

2.3.2 Material Selection for X-ray Mask

To make high aspect ratio structures using X-ray lithography, the Au absorber

must be thick to increase contrast and to minimize fluorescence from the Au absorber

2 CQ grade is a particular cast sheet of PMMA for X-ray lithography that is additive-free and is the highest molecular weight grade of PMMA available. It contains a minimum UV absorber. 3 MEMO: 3-Methacryloxypropyltrimethoxysilane 4 BPO: Benzoyl peroxide 5 DMA: Dimethylaniline 6 MMA: Methylmethacrylate Monomer

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23

itself. A 3µm Ti film was chosen as an X-ray transmitting membrane because of the good

adhesion property of the thick photo resist for Au plating, and the moderate radiation

stability. In the X-ray lithography, contrast refers to absorption contrast, defined as the

ratio of the total dose at the bottom of the resist under the X-ray transparent membrane, to

the total dose below the X-ray absorber. Figure 2.3 plots the absorption contrast for the

3µm Ti membrane mask for various PMMA thicknesses versus the Au absorber thickness,

calculated by dose simulation software from the Center for Advanced Microstructures

and Devices (CAMD), Louisiana State University; here the bottom dose was 2500J/cm3

with a 175µm thick Beryllium window and a 9.5µm thick Al filter.

An acceptable contrast for a process with PMMA combined with a G-G developer

is known to be above 40 to produce good lithographic patterns [Desta et al, 2003]. In this

work, 8µm thick Au was chosen to obtain contrasts of 71. The maximum contrast was

compromised by limitations on the maximum thickness of SPR 220-7 (a positive tone

photo resist from Shipley, Inc. patterned for Au plating on the 3 µm Ti membrane) that

can produce good vertical profiles. The detailed process conditions for the lithography of

SPR 220-7 is explained in the next section.

Figure 2.3 Absorption contrast of 3µm Ti membrane mask versus Au

thickness with various PMMA thicknesses

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24

2.3.3 Fabrication Processes of X-ray Mask

The fabrication processes of the Ti membrane mask are as follows: 3µm Ti was

sputter deposited on to a Si wafer. A 50nm layer of Au was evaporated onto the Ti as a

seed layer for Au electroplating. To improve the adhesion of Au to Ti, 10nm Cr was used

as a bonding layer between the Ti and Au layer. Shipley’s SPR 220-7 was the positive

photo resist used for patterning the Au electroplating mold, where an e-beam photo mask

with critical dimension 0.1µm was used.

Lithographic conditions were carefully optimized to obtain a nearly vertical

sidewall. The process conditions of SPR 220-7 were as follows: it was spin-coated for 40

seconds at 1500 rpm to obtain a 13µm thick layer. To minimize cracking and a build-up

of internal stresses, a soft bake was performed on a contact hot plate in a two-step

process: for 150 seconds at 100oC, followed by 240 seconds at 115oC. The dose was

optimized as 420mJ/cm2 for best contrast and vertical sidewall, using a broadband

(350~550nm) Oriel UV station in CAMD. Any attempt to post-exposure bake resulted in

extensive cracking all over the resist, regardless of baking conditions for the resist thicker

than 10µm. The developer was a 1:1 mixture of MF 321 and MF 322. The developing

condition was very critical to achieve a high-quality photo resist pattern. Even a slight

over-development resulted in rough-edged profiles and blunted corners. Moderate

agitation and careful time control were very important. Figure 2.4 shows the SEM images

of the patterned photo resist.

After the SPR 220-7 was patterned, 8µm Au was electroplated at a current density

of 1mA/cm2 and at a bath temperature of 43oC, resulting in a plating rate of 4µm/hr. SEM

images of the X-ray mask in Figure 2.5 show very smooth circumferential profiles, which

are critical realizing very smooth surface roughness on the final Ni structure. After the

Au was electroplated, the backside of the silicon wafer was etched by 40% KOH at 65oC

to suspend the Au pattern on the Ti membrane. Figure 2.6 shows Ti membrane mask

fabricated through the processes described above.

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25

(a) Overall image of bearings (b) Near perfect vertical sidewall

Figure 2.4 SEM image of patterned 13µm thick SPR: (a) overall image of bearings, (b) near perfect vertical sidewall

(a) Top view (b) 2µm step in journal bearings

Figure 2.5 SEM images of Ti-membrane X-ray mask with 8µm thick Au absorber: (a) Top view, (b) 2µm step in journal bearings

Figure 2.6 Ti membrane X-ray mask with Au absorber

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26

2.3.4 X-ray Exposure and Development

The X-ray source was XRLM3 at CAMD with a 175µm thick beryllium window.

An additional 9.5µm thick Al filter was inserted into the beam line to remove low-energy

photons and to decrease top to bottom dose ratio. The minimum bottom dose below the

Ti membrane was chosen as 2500J/cm3, and the top to bottom dose ratio was 4.84. The

dose below the Au absorber was 34J/cm3.

PMMA was developed in a G-G solution at room temperature to minimize

cracking and to improve the contrast between the exposed and unexposed areas

[Pantenburg et al, 1998]. Higher development temperature can increase development rate

but G-G solution can also develop unexposed area. Table 2.3 shows the chemical

compositions of the G-G developer and rinse solution. One cycle consists of 20 minutes

developing and 40 minutes rinse. Each cycle develops 100µm.

Table 2.3 Chemical compositions of G-G developer and rinse Developer (for 1L solution)

2-(2-Butoxyethoxy)ethanol 600mL Morpholine 200mL 2-aminoethanol 50mL DI water 150mL

Rinse (for 1L solution)

2-(2-Butoxyethoxy)ethanol 800mL DI water 200mL

2.4 Post Processes

2.4.1 Electroplating

The basic procedure of Ni electroplating is similar to other electroplating

processes. In Figure 2.7, the Ni anode is dissolved in a Ni sulfamate solution, where it

replenishes the Ni2+ ions. In the cathode, which is the substrate to be Ni plated, the Ni2+

ions react with two electrons and are deposited on the cathode in a metallic form. Since

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27

3-5% of the current is consumed by reduction of H+ ions in the cathode, cathode

efficiency is 95-97%, depending on the solution conditions [Bari, 1994; Judy, 1996].

The reactions at the cathode and anode are as follows:

Cathode reaction

Ni 2+ + 2e → Ni (main reaction) (2.1a)

2H+ + 2e → H2 (2.1b)

Anode reaction

Ni → Ni 2++ 2e (main reaction) (2.2a)

OH- → ½ O2+ H + +2e (2.2b)

Ni 2+

H+OH -

Ni 2+

Ni

2e

Cathode (substrate

Anode

2eH2

Ni

O2

NH2SO3 -

Figure 2.7 Reaction in the Ni electroplating bath

Under normal operating conditions, there should be no hydroxyl ions (OH-)

dissolved from the water, and the dissolution efficiency of the Ni anode should be 100%.

When there are too many hydroxyl ions (OH-), oxygen is evolved at the anode (Equation

2.2b) instead of the Ni dissolution. In that case, the anode stops dissolving, Ni2+ ions are

exhaused quickly at the cathode, and electroplating stops. To keep the anode efficiency at

100%, chloride ions are added to the Ni sulfamate solution, or an activated Ni anode is

used instead of pure Ni [Bari, 1994]. The activated nickel , which contains about 0.025%

sulfur, is commercially availlable [Online reference 1]. The sulfur forms insoluble black

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28

nickel sulfide residue on the Ni anode surfaces, and the residues should be retained in a

polyprophylene anode bag to prevent contamination on the electroplated Ni surface, as

shown in Figure 2.8. The nickle sulfide also removes unwanted copper impurities from

the plating solution.

Figure 2.8 Contamination of Ni electro deposit surface by nickel sulfide particles,

shown as small black dots on white Ni electro deposit

Table 2.4 shows the chemical composition of the nickel sulfamate solution and

the process conditions. To adjust the pH, diluted sulfamic acid (H3NO3S) was used for

pH>4 and diluted sodium hydroxide (NaOH) was used for pH<3.5. Small amount of

sodium lauryl sulfate was added as a wetting agent (surfactant) to reduce the surface

tension of the Ni sulfamate solution and to permit it to penetrate into small

microstructures.

Faraday’s Law for the Ni plating is expressed by the following equation [Bari,

1994]:

tIFnM

me

cη= (2.3)

, where m is mass of electroplated Ni (g), M is the molecular weight of Ni (58.7g/mol), ne

(=2) is the number of elecrons involved in the reduction of Ni, F is Faraday’s constant

(96488 C/mol), ηc is cathode efficiency (0.95-0.97), t is time, and I is total current.

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29

If the total area to be electroplated is A(cm2) and the thickness is d(µm), Equation

(2.3) becomes

tJFnM

de

c

ρη

= . (2.4)

Here ρ is the density of Ni (=8.9g/cm3) and J is the current density in mA/cm2. Plugging

the values into equation (2.4) gives

Jdd

JMFn

tcc

e

ηηρ

871.925,2== (2.5)

Assuming ηc =1, the total time to electroplate 300µm thick Ni is about 24 hours

(~0.2µm/min). Because the current density is not uniform at the edges of the structures as

sown in Figure 2.9, the patterned PMMA structure was over plated for 30 hours and

polished down to 300µm (Figure 2.2b) for subsequent processes to form the thrust

bearing.

Table 2.4 Chemical composition of Ni sulfamate solution and the process conditions

Component Amount per 1L final solution Nickle sulfamate(Ni(NH2SO3)2) 50% aqueous solution 450ml (78g of Ni2+ ions/L)

Sodium Lauryl Sulfate 1g Boric Acid (H3BO3) 37.5g DI water to 1L final volume pH 3.7 Temperature 50oC Current density 10mA/cm2

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30

Plating mold

Seed layer

Figure 2.9 Non uniform current density at the edge of patterned plating mold cause

non uniform deposit thickness [Judy, 1996]

Important factors, easily overseen in Ni electroplating, are hydrogen evolution in

a cathode (3~5% of total current), and nucleation of air bubbles on a PMMA surface,

when cathode is immersed in electroplating bath. Because electroplating is very fast

process, small air or hydrogen bubbles are easily trapped and form a micro scale cavity

after electroplating is finished. Figure 2.10 is a high magnification SEM image of bearing

surface with cavity formed by air bubble nucleated right after substrate was immersed in

a plating bath. Increasing wetting agent or fast stirring of electroplating solution can

remove air or hydrogen bubble effectively.

Figure 2.10 High magnification SEM image of bearing sidewall: cavity formed by

air bubbles attached to PMMM

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31

2.4.2 Processes to Form Thrust Bearing

A 100µm thick layer of negative photo resist, SU-8 2100 from MicroChem, Inc.,

was spin-coated on top of the polished Ni-PMMA structure (shown in Figure 2.2b) to

pattern the second Ni plating mold for the thrust pads. Spin conditions were 3000 rpm for

30 seconds. SU-8 2100 was selected as a plating mold because of its unique capability to

coat more than 100µm thick layer with a single spin and its high sensitivity to UV (250-

450nm).

The spin coated SU-8 had 10 hours of hold time before the soft bake to relax

stress built up during the spin. Soft baking was performed at 95oC for 30minutes on a

contact hot plate that was partially sealed by a cover to maintain a uniform temperature

over the thickness of the SU-8 layer. During the soft baking, the temperature was

changed slowly to minimize shrinkage and thermal shock. A KARL SUSS UV aligner

was used for the UV exposure and for alignment of the location of the thrust pads with

respect to the journal bearing center. The dose was optimized as 400mJ/cm2 for the best

vertical sidewall. SU-8 is cross-linked in two steps. During the exposure, strong acid is

formed, and the acid initiates a photoreaction to cross link the polymer during the post

exposure bake (PEB). The PEB was performed for 25minutes at 96 °C. Slow cooling to

room temperature after the PEB is very important to prevent resist cracking. Overnight

cooling is recommended for best results. The unexposed area was developed with SU-8

developer from MicroChem, Inc. and rinsed by isopropyl alcohol (IPA).

Before the second Ni layer was electroplated to form the thrust pads, the exposed

Ni surface (polished surface at step (b) in Figure 2.2) was etched by diluted HNO3 for 5

minutes to remove a natural Ni oxide layer on the surface. With the oxide layer, the

adhesion of the second Ni structure on the first Ni structure was poor, and the second Ni

structure was easily peeled off. Ni was electroplated again within the patterned SU-8

mold and polished down to the SU-8 (Figure 2.2d).

Positive i-line (365nm) photo resist AZ 4330 was spin coated on the SU-8 and Ni

structure (Figure 2.2d), to process the final 3µm recesses on the thrust pads. The nitric

acid-based nickel etchant TFB from Transene, Inc. (etch rate of 0.18µm/min at 25oC) was

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32

used to etch the final 3µm recesses. The widely used sulfuric acid based etchant TFG

from the same company reacted with the Ni surface to form presumably black nickel

sulfide, preventing further etching.

2.4.3 Sacrificial Layer Etching to Release Bearings

After steps in thrust bearing were formed, SU-8 and PMMA were removed in a

Dynasolve 165 and chlorobenzene, respectively. The final releasing step of the bearings

from the substrate was performed in diluted (~10%) HF, to etch TiO sacrificial layer on

ceramic wafer. Ni does not dissolve in HF because chemical activity of Ni is very close

to H [Whitten et al, 2004]. Ti and TiO are dissolved very fast in even highly diluted HF.

Etching time depends on the thickness of TiO and size of the structures. Thicker TiO

layer allows better diffusion of diluted HF, leading to shorter release time. Release time is

very important achieving good sidewall roughness.

Figure 2.11 compares SEM images of sidewall generated by different sacrificial

layer etching time; (a) and (b) are surfaces generated by sacrificial layer etching for 2

days and 2 weeks, respectively. Figure 2.12 is a high magnification image of Figure 2.11.

Small cavity in Figure 2.12(a) was formed by an air bubble nucleated on a PMMA

surface when electroplating began. Both samples had the identical process conditions (X-

ray dose, PMMA development and electroplating conditions, etc), except the release time.

Even if activity of Ni with H is negligible, long etching time increase surface roughness

of final Ni microstructure significantly. To minimize etching of Ni during the sacrificial

layer etching, Ti layer should be thick enough to allow diluted HF to diffuse very quickly

or sonic agitation is recommended. Figure 2.13 is SEM images of the final micro gas

bearings with thrust pads, with releasing time of 2 days. The surface roughness of the

bearings was measured by the D-3100 Atomic Force Microscope (AFM) from Digital

Instruments, Inc. in a tapping mode. Instead of the inside surfaces of the bearing, the

outer edges were measured because, in principle, their lithographic conditions are exactly

the same as the inside surfaces, and, in practice, this surface is accessible. Figure 2.14

shows the morphology of the bearing surfaces of dimensions 10µm × 10µm. Both Ra and

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33

RMS values were below 20nm. The surface profiles do not show the noticeable

orientation that is typical in X-ray lithography patterns using graphite mask [Coane,

2000], which means very smooth circumferential profiles of the Au absorber in the

fabricated Ti membrane X-ray mask.

(a) After 2 days release (× 2K) (b) After 2 weeks release (× 2K)

Figure 2.11 SEM images of bearing surface after different sacrificial layer

etching time: (a) After 2 days release (× 2K), (b) After 2 weeks release (× 2K)

(a) After 2 days release (× 10K) (b) After 2 weeks release (× 10K)

Figure 2.12 Higher magnification of Figure 2.11: (a) After 2 days release (×

10K), (b) After 2 weeks release (× 10K)

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34

(a) Overall bearing (b) 2µm steps on journal bearings

(c) Magnified image of 2µm step

Figure 2.13 SEM images of micro gas bearing: (a) Overall bearing, (b) 2µm steps on journal bearings before processing thrust bearings, (c) Magnified image of 2µm step

(a) AFM topography (b) High magnification SEM images

Figure 2.14 Surface morphology of bearing surface measured from AFM (scan

length 10µm×10µm) and SEM: (a) AFM topography, (b) High magnification SEM images

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35

Chapter 3

Static Performance of Micro Gas Bearing

In the Chapter 3, Reynolds Equations for gas journal and thrust bearings, based on

Molecular Gas Lubrication (MGL) theory, are introduced. Numerical analyses results on

static performance and rotational friction factor of the micro gas journal and thrust

bearings are presented.

3.1 Theory Figure 3.1 shows a schematic diagram of the micro gas journal bearing in the

normal operating conditions with eccentricity e of the journal center from the bearing

center. In the figure, ω is the rotational speed of the journal, and θ is the circumferential

coordinate with the same direction as ω. C is the radial clearance between the bearing and

journal. φ is the attitude angle of the journal, which is the angle between the direction of

load capacity F and eccentricity e.

Upon rotation of the journal shaft, the gas between two surfaces of a gas bearing

is pressurized by the squeeze film effect. This generates a hydrodynamic force, lifting the

journal immediately after the initial slip. At steady state, there is no contact between the

two surfaces, and friction approaches zero.

The governing equation for a gas journal bearing was derived from the general

Navier Stoke’s equation, with the assumptions of a thin gas film, negligible curvature

effect, and ideal gas under isothermal equilibrium. Here the local gas film thickness h is

much smaller than the bearing length L and diameter D. The result, Reynolds Equation

for gas film pressure p, was derived using a no slip boundary condition of gas at the

bearing surfaces [Cameron, 1966].

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36

)(12)(6)()( 33 pht

phx

Uzpph

zxpph

x ∂∂

+∂∂

=∂∂

∂∂

+∂∂

∂∂ µµ (3.1)

In the foregoing, x is the direction of linear speed U (=Dω/2), z is the direction of side

flow, and µ is the viscosity of the lubricating gas. The ideal gas law was used to include

the compressible flow effect to change a density to pressure.

x

θ

Χ

ω

e

y r

YYXX iFiFF +=

φ

C(1+ε)

C(1-ε)

Y

Figure 3.1 Journal bearing in normal operating condition

For a micro gas bearing, the slip at the surface should be considered, because the

molecular mean free path of gas molecules is not negligible compared with the bearing

clearance C. An important parameter in a gas kinetic theory is Knudsen number, defined

as Kn = l/h, where l is a molecular mean free path derived from the gas kinetic theory

[Kennard, 1938]7.

pNdTR

A22

ˆ

πλ = (3.2)

The concept of gas kinetic theory was first introduced to a rarefied gas film by

Burgdorfer [Burgdorfer, 1959]. He adopted Maxwell’s wall slip analysis [Kennard, 1938]

7 The mean free path is defined as the average distance that a molecule travels between successive collisions.

Page 56: kimd042.pdf

37

and modified the Poiseuille flow component, using a slip flow velocity boundary

condition for a small Knudsen number (Kn << 1). He assumed the slip is proportional to

the velocity gradient dzdv /0 at the wall. Then the slip velocity us at the wall can be

written as

dzdv

u as0ζ= (3.3)

Maxwell derived the Knudsen layer thickness ζa based on the tangential

momentum transfer ratio of molecules with molecular mean free path λ:

λλα

αζ aca ≡

=22 (3.4)

Here, c is an adjustable parameter with values between 0.491 and 0.499 (such that very

nearly 2c ≈ 1).

The surface accommodation coefficient of the wall α is the energy transfer ratio

defined by Knudsen [Kennard, 1938] as

wi

ri

EEEE

−−

=α (3.5)

In Equation (3.5) Ei denotes the energy of incident molecules, Er denotes the

energy of reflected molecules, and Ew denotes the energy of molecules that reflected

diffusively at the wall. In “diffusive” reflection, the time that a molecule stays at the wall

is long enough for the molecule to absorb sufficient kinetic energy of the wall

temperature and to reflect in a direction independent of the incident direction. In that case,

Er approaches Ew and α=1. When α is zero, the molecules are reflected “specularly” with

no change of their initial kinetic energy. The accommodation coefficient depends on the

surface conditions, such as material, surface roughness, adsorbates on the surface, etc.

Page 57: kimd042.pdf

38

[Kennard, 1938; Rettner, 1997]. Maxwell [Kennard 1938] assumed a fraction φ of the

incident molecules were reflected diffusively with α=1, and the rest were reflected with

α=0. With Maxwell’s assumptions, the total reflected energy will be Er=φEw+(1-φ)Ei .

Since from Equation (3.5), φ and α are governed by the same equation, the

accommodation coefficient represents the fraction of diffusive reflection.

From experiments [Rettner, 1997; Gabis et al, 1996] on the hard disk surfaces,

various real engineering surfaces have α=0.9 -0.95. In this work, the accommodation

coefficients at both walls are assumed to be 1.

Taking account of the wall slip effect, the Reynolds Equation was modified as

[Burgdorfer, 1959]

)(12)(6

))61(())61(( 33

pht

phx

U

zp

haph

zxp

haph

x

∂∂

+∂∂

=

∂∂

+∂∂

+∂∂

+∂∂

µµ

λλ

(3.6)

Fukui and Kaneko [Fukui and Kaneko, 1988] derived a Molecular Gas

Lubrication (MGL) model based on the linearized Boltzmann Equation8, to account for

the molecular slip effect in Poiseuille flow. They rigorously derived a Poiseuille flow

factor PQ , defined as the ratio of the real Poiseuille flow rate PQ in rarefied gas regions

to the continuum flow rate conQ . They created the numerical tabulation of the database

for the flow rate coefficient PQ . Kang [Kang, 1997] improved the database by correcting

PQ at very small Kn numbers and by taking into account of the different accommodation

coefficients at both wall boundaries. One of the key assumptions on the MGL model

from the linearized Bolzmann Equation is that the bulk flow speed is much smaller than

the molecular speed at a given temperature. In this case, the velocity distribution function

of the gas flow within the bearing clearance can be assumed to be almost the same as that

of isotropic equilibrium [Kang, 1997]. Therefore, when bulk flow velocity (∝ sliding

8 Called as the linearized BGK (Bhatnagar, Gross, Krook) model.

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39

speed U of the journal) is comparable to the molecular speed at a given temperature; that

is, as the Mach number is approaches 1, MGL model fails to predict the correct pressure

profile, and direct molecular dynamic simulation or Direct Simulation Monte Carlo

(DSMC) should be used [Alexander, 1994] to calculate the direct momentum change

(pressure) at the wall.

3.1.1 Journal bearing In spite of the limitation of the MGL model explained above, a direct comparison

of the pressure profile from the MGL model with that from DSMC [Alexander, 1994]

and experimental results [Menon, 2000] confirmed the validity of the MGL model with

reasonable accuracy, up to Mach number 0.5 and a bearing clearance as low as 10 nm.

The Equation (3.1) can be non-dimensionalized as

)()()()( 33 PHPHZPPHQ

ZPPHQ PP τ

σθθθ ∂

∂+

∂∂

Λ=∂∂

∂∂

+∂∂

∂∂

(3.7)

where,

appP /= (3.8a)

Rx /=θ (3.8b)

RzZ /= (3.8c)

ChH /= (3.8d)

tωτ = (3.8e)

Ce /=ε (3.8f)

Here pa is atmospheric pressure and R is bearing radius. In the right-hand side of

Equation (3.7), bearing number Λ and squeeze number σ are defined as

26

CR

pa

µω (3.9a)

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40

212

=

CR

pa

µωσ (3.9b)

The Poiseuille flow factor PQ can be

1P =Q for the continuum model

PHKn

aQ a61P += for the first order slip model [Burgdorfer, 1959]

( )α;P KnfQ = for the MGL model [Fukui and Kaneko, 1988]

The non-dimensional gas film thickness H is given by

θεθε sincos1 YXH −−= (3.10a)

θεθε sincos1/ YXR CCH −−+= (3.10b)

for a bearing surface without steps and with steps, respectively. Using Equation (3.8), the

Knudsen number Kn can be represented as follows

PHKn

CPHPCHpNdRT

phNdRT

hKn a

aAA

===== 022 22

λππ

λ (3.11)

where λ0 (≅ 64nm) is a mean free path at atmospheric pressure and 20oC, and Kna is

defined as the characteristic Knudsen number, which is the ratio of λ0 to the bearing

clearance C.

Once the pressure field P(θ, Z) is obtained, the load carrying capacities FX and FY

and the dimensionless load parameters ζX and ζY along X and Y directions become

∫ ∫−= π θθθ20

/0

2 cos),(RLaX dZdZPRpF (3.12a)

∫ ∫−=π

θθθ2

0

/

0

2 sin),(RL

aY dZdZPRpF (3.12b)

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41

RLpF

a

XX 2

=ζ (3.12c)

RLpF

a

YY 2

=ζ (3.12d)

The load parameters ζX and ζY are defined as a load capacity normalized with respect to

the projection area of the bearing multiplied by the ambient pressure. The total bearing

load parameter ζ becomes

22YX ζζζ += (3.13)

The attitude angle φ is the angle between the external load vector and the

eccentricity vector (see Figure 3.1), and is given by

2222

)(cosYX

X

YX

X

FF

FFeFe

ζζ

ζφ+

−=

+

−=

−−⋅

= (3.14)

The friction by air drag at the journal shaft can be calculated from the shear stress.

For fully diffusive reflection at both walls, the local velocity distribution function from

[Burgdorfer, 1959] in the x direction (Figure 3.1) becomes

( )λλλ

µ 2)()(

21 2

++

++−=h

yUhyydxdpu (3.15)

and the shear stress at the journal shaft (y=h) is given as

conccconppcphy

xy WWyu

,, ττττµτ +=+≡∂∂

==

(3.16)

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42

Here, τp is the shear stress by Poiseuille flow, and τc is the shear stress by Couette flow.

Wp and Wc are the shear stress factors for Poiseuille flow and Couette flow, respectively.

The subscript “con” refers to continuum flow. Using gas kinetic theory, Kang [Kang,

1997] derived and tabulated numerically Wc and Wp for an arbitrary Knudsen number and

accommodation coefficients at both walls. Kang [Kang, 1997] showed that Wp is unity

when both walls have identical accommodation coefficients. The Couette shear stress

factor for a fully diffusive wall becomes

KnaPHPH

KnhhWc 221

12 +

=+

=+

(3.17)

Figure 3.2 compares the numerical tabulation Wc by Kang with that by the first

order slip model in Equation (3.17). The maximum error is about 10% at very high Kn

numbers. In this work, Equation (3.17) was used instead of the exact numerical tabulation

in Figure 4.2 to calculate the friction at the journal surface.

The friction torque by air drag becomes

∫ +∫=

∫ +∫∫ ∫ ==

π

ππ

θµ

θτττ

20 0

20 0

20 0

)2

(

)(

dzdRhUW

dxdphR

dzdRWRdART

cL

ccpLL

xyF

(3.18)

Page 62: kimd042.pdf

43

Figure 3.2 Comparison of shear stress factor by Couette flow for fully diffusive

walls; database from Kang [Kang, 1997] and first order slip model

Representing Equation (3.18) with non-dimensional parameters defined in

Equation (3.8), gives

∫ ∫

+= π θµ

θ20

/0

32

2dZd

CUR

HW

ddPH

RCpT RL ca

F (3.19)

By arranging terms, the non-dimensional rotational friction factor βJ for the journal

bearing becomes

∫ ∫

== π θθωµ

β 20

/04

3 dZdH

WddPH

RCT RL cF

J (3.20)

3.1.2 Thrust Bearing The Reynolds Equation given in Equation (3.1) can be transformed to cylindrical

coordinates. The mass fluxes in cylindrical coordinates are

rphmr ∂

∂−=

µρ12

3

& (3.21a)

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44

212

3 hUr

phm θθ

ρθµ

ρ+

∂∂

−=& (3.21b)

Inserting the mass flux into the continuity equation and adopting the ideal gas law gives

tph

rphU

rpph

rrpphr

rr ∂∂

+∂

∂=

∂∂

∂∂

+

∂∂

∂∂ )()(

2121

121 33

θθµθµθ (3.22)

where Uθ=rω. Non-dimensionalizing Equation (3.22) at steady state by

Rr

=η and ChH = (3.23)

yields

θη

θηθηη

η ∂∂

Λ=

∂∂

∂∂

+

∂∂

∂∂ )(33 PHPPHPPH (3.24)

Here r and the gas film thickness h of thrust bearing was non-dimensionalized using

radius R of the journal bearing and the journal bearing clearance C to get the same

bearing number for the same rotational speed.

Taking gas rarefaction effects into consideration, Equation (3.24) becomes

θη

θηθηη

η ∂∂

Λ=

∂∂

∂∂

+

∂∂

∂∂ )(33 PHPPHQPPHQ pp (3.25)

Integration of the pressure distribution over the thrust bearing surface area gives the load

capacity fT and load parameter ζT as

∫ ∫ −= π ηθηηθ20

//

2 )1),((RRRRaT

o

iddPRpf (3.26a)

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45

)( 22ioa

TT RRp

f−

ζ (3.26b)

where Ri and Ro are the inner and outer radii of the thrust bearings.

Rotational friction damping can be calculated the same way as for the journal

bearing. The flow velocity distribution in the θ direction considering first order slip

effects becomes

λλωλ

θµθ 2)())((

21 2

++

++−∂∂

=h

zrhzzr

pu (3.27)

Then, the shear stress at the bearing surface is

ccpz Wh

rrddph

zu

ττλ

ωµθ

µτ θθ +≡

++=

∂∂

=22

(3.28)

Integrating the shear stress over the thrust bearing surface, the total frictional torque

becomes

∫ ∫ +=

∫ +∫∫ ∫ ==

π

ππθ

θωµθ

θτττ

20

2

20

220

)2

(

)(

drdhrW

rddphr

drdWrdArT

RoRi c

ccpRoRi

RoRi zFT

(3.29)

Representing Equation (3.29) with non-dimensional parameters defined at Equation (3.9)

and (3.23) gives

∫ ∫

+= π ηθηωµ

θη2

0/

/

342

2dd

HCRW

ddPH

CRpT RRo

RRica

FT (3.30)

By rearranging Equation (3.30), the non-dimensional rotational friction factor βT for

thrust bearings becomes

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46

∫ ∫

+

Λ== π ηθ

ηθ

ηωµ

β 20

//

3

4

3 ddH

WddPH

RCT RRo

RRicFT

T (3.31)

3.2 Numerical Method The dynamic gas film equation for the journal bearing, Equation (3.7), and the

static gas film equation for the thrust bearing, Equation (3.25), can be rewritten as

)(2 PHQJJ τ∂

∂Λ−=⋅∇ (3.32a)

0=⋅∇TT Q (3.32b)

, where

ZPPJi

ZPPHQiPPHQPHQ

∂∂

−+

∂∂

−Λ= 33θθ

ηθ ηη

θηη iPPHQiPPHQPHQ ppT

∂∂

−+

∂∂

−Λ= 33

Here, subscripts J and T denote journal and thrust bearing, respectively, and

),,( ηθ Zkik = are unit vectors along the θ, Z, and η directions. ∇J and ∇T are gradient

operators. Integrating Equation (3.32) over the control surface SP (shaded in Figure 3.3)

gives

PPSPPS JJ dSPHdSQ ∫∫∂∂

Λ−=∫∫ ⋅∇ )(2τ

(3.33a)

0=⋅∇∫∫ PS TT dSQP

(3.33b)

Applying the divergence theorem to the left-hand sides of Equation (3.33) gives

PPSPJPldSPHdlnQ ∫∫

∂∂

Λ−=⋅∫ )(2τ

(3.34a)

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47

0=⋅∫ Pl TdlnQ

P

(3.34b)

where n is a unit normal vector along line lP, surrounding the control surface SP.

i-1,j i+1,j

i,j-1

i,j+1

i,j

i,j-1/2

i-1/2,j

i,j+1/2

∆θ

∆Z

θ

Z

lP SP

i+1/2,j+θQ−

θQ

+ZQ

−ZQ

SQ

Figure 3.3 Grid scheme for control volume method

The power law schemes [Patankar, 1980] based on the central difference method,

and the Gauss-Seidel iteration were used in the simulation. Details of the discretization of

each flux term and the detail numerical schemes are presented in Appendix A.

3.3 Static analysis

3.3.1 Journal bearings The bearing design parameters and gas properties for a static analysis are diameter

D=500µm, length L=300µm, bearing clearance C=1.0µm, viscosity µ=19.6×10-6 Ns/m2,

and molecular mean free path λo=64nm. Simulations assumed isothermal air at 20oC. The

step configuration on the journal bearings was such that θS/θP =0.5. Here, θS (=30o) is the

angle one step occupies, and θP (=60 o) is 2π divided by the number of steps (see Figure

3.4). In the analysis of stepped micro gas journal bearings, the angular location (θR in

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48

Figure3.4) of the first step was varied with respect to the journal eccentricity (θR =25o, 15

o, 5 o, -5 o, -15 o, -25 o).

The accuracy of the numerical method for high eccentricities with the stepped

bearing geometry was checked for different numbers of grid points, along the

circumferential (n) and axial (m) directions, for Λ=1 and θR =-15o. Table 1 shows the

variations of load parameter ζ (Equation 3.13), and attitude angle φ (Equation 3.14) for

different grid schemes for ε=0.8 and ε=0.9, since numerical stability is more sensitive at

higher ε. Using the most dense grid, 336×36, as a reference, variations of ζ and φ for the

other grid schemes were within 2.3% for ε=0.8 and within 5.8% for ε=0.9. The grid

scheme 180×36 was used in the foregoing analyses.

θS

θP θ

Χ

ω

e

YYXX iFiFF +=

φ

C(1+ε)

C(1-ε)

Y θR

Figure 3.4 Stepped bearing configuration

Table 3.1 Numerical resolution for various grid schemes ( Λ=1, θR =-15o)

n×m 96×24 120×32 180×36 240×36 300×36 336×36

ε=0.8 0.032952 0.033219 0.033228 0.033496 0.033339 0.033424 ζ

ε=0.9 0.057738 0.058588 0.058444 0.059867 0.059344 0.060052

ε=0.8 80.7489 80.4778 81.6499 79.9762 80.8017 79.8424 φ

ε=0.9 78.025 77.0634 79.0161 75.2124 76.7797 74.7021

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49

The specific film thickness 22bss hh σσ += , where σs and σb are RMS surface

roughnesses of the shaft and the bearing, respectively, and h is the local film thickness,

should be larger than 4 for full hydrodynamic lubrication [Pirro, 2001]. Assuming that

the bearings and shafts are fabricated by the same processes (surface roughness with

σs=σb=18.2nm), the minimum film thickness for hydrodynamic lubrication is 103nm,

which is equivalent to an eccentricity ~0.9 with a 1µm bearing clearance. Therefore, the

maximum eccentricity was limited to 0.9 in the analyses.

Figures 3.5 and 3.6 plot the load parameter ζ and attitude angle φ vs. bearing

number Λ for plain micro gas bearings and stepped micro gas bearings with θR=5o. In the

plain journal bearing, ζ monotonically increases for Λ<10, but tends to flatten for Λ>10

due to excessive side leakage by very high pressures generated on the bearing surfaces.

These saturation effects were not observed for the stepped journal bearings because the

maximum pressures were lower compared to those of plain journal bearings. The attitude

angle φ starts at 80-90o for small Λ and tends to decrease with increasing Λ for plain

bearings and step bearings. For a given eccentricity, the stepped bearings have smaller ζ

than plain gas bearings because repeated step geometry produced chain saw-like pressure

profile as shown in Figure 3.7. The chin saw-like pressure profile is generated because

gas is compressible fluid. In a gas or liquid lubricated bearing, high attitude angle results

in large negative cross stiffness and leads to whirl instability. Gas bearings should be

designed to minimize attitude angles at wide operating conditions.

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50

Figure 3.5 Static performance of stepped micro gas bearings (θR =5o)

Figure3.6 Static performance of plain micro gas journal bearings

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51

Figure 3.7 Pressure profiles (Λ=1, ε=0.4) of fabricated stepped gas bearing

A unique characteristic of stepped micro gas bearings is the variation of the

attitude angle φ and the load parameters ζ with the relative position (θR) of the journal

center and steps, when eccentricity is high. Figure 3.8 plots the load parameters ζ and

attitude angles φ vs. the bearing number Λ for eccentricity ε=0.8, with θR as a curve

parameter. The attitude angles φ vary over a wide range from 67 o to 107 o, depending on

θR, and the load parameters also change as a function of θR. This implies that, for a given

external load (load parameter), the journal center can have more than one steady state

position with different eccentricities and attitude angles. However, for small

eccentricities, for example, ε<0.6, the load parameters ζ and attitude angles φ were

almost independent of θR, as shown in Figure 3.9. Also shown in Figure 3.9 is the

simulation at extreme eccentricity (ε=0.98, which may not be a feasible hydrodynamic

region of the fabricated micro gas bearings), where the load parameters showed large

variations depending on θR and showed its maximum at –5<θR<5 over a wide range of

bearing numbers.

Figure 3.10 is a circumferential pressure profile at the bearing center with attitude

angles for ε=0.8 and 0.98. At ε=0.98, the attitude angle φ was larger than 150o, due to

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52

high negative pressure built at the diverging gas film due to the adjacent trailing step. In

this case, the load capacity F (bearing reaction) is directed as in Figure 3.11. It should be

noted that even if the bearing reaction is directed toward the rotor displacement due to

very large attitude angles, the bearings should not be regarded as statically unstable. In

these cases, the external load can be applied in the opposite direction of the bearing

reaction force. The application of the negative pressurized bearing can be found in a hard

disc slider, where the servo actuator lifts the slider arm and the slider is designed such

that negative pressure is built to maintain a very thin gas film at steady state. At the same

token, it is possible to operate the bearings with high attitude angles if the bearings are

dynamically stable.

Figure 3.8 Load parameters and attitude angles of stepped micro

gas journal bearing at ε=0.8 for different θR

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53

Figure 3.9 Load parameters of stepped micro

gas journal bearing at ε=0.6 and ε=0.98 for different θR

Figure 3.10 Circumferential pressure profile at the bearing center

(Λ=0.2, θR= 25o)

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54

θΧ

ω e

φ

25o

Y

F

Figure 3.11 Direction of load capacity vector F for the conditions in Figure 3.10 with

ε=0.98, Λ=0.2, and θR= 25o. ζX = 0.0318 and ζY = 0.0156

3.3.2 Thrust Bearings

Figure 3.12, showing local maxima in ζT vs. step height, indicates the existence of

an optimal step height as a function of thrust bearing clearances CT for a given bearing

number Λ; this optimal step height (which produces the maximum load capacity) is a

weak function of the bearing number. The optimum ratio of bearing clearance to step

height falls between 1.2-1.4, which is similar to the optimal ratio (1.15) for a rectangular

step bearing with fixed pad [Cameron, 1966]. The step height of the thrust bearing was

chosen as 3µm to get as much load capacity as possible over a wide range of bearing

clearances.

3.3.3 Rotational Friction Factor

Rotational friction factors, calculated as shown in Figure 3.13 using a first-order

slip model, were almost constant over a wide range of bearing numbers, for given journal

positions or operational points for the thrust bearings. The simulations suggest that a

stepped gas journal bearing should have much lower rotational friction than plain gas

journal bearings.

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55

Figure 3.12 Load capacity as a function of step height for thrust bearings

Figure 3.13 Non-dimensional rotational friction of micro gas bearing (θR =5o for

stepped journal bearings, step height 3µm for thrust bearings)

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56

Chapter 4

Dynamic Performance of Micro Gas Bearings

In this chapter, dynamic performance of the micro gas bearing is investigated.

Orbit method is employed to simulate a numerical test rig, and to investigate whirl

instability. Improved bearing profiles with higher load capacity and dynamic stability are

suggested. Fabrication methods of meso scale gas bearings are proposed. Performance

analyses of the meso scale gas bearings in terms of two-dimensional imbalance response

are presented.

4.1 Approach We consider stability of micro gas bearings with an assumption of rigid rotor with

perfect alignment with the gas bearing along the axial direction. The equations of motion

for the journal shown in the Figure 4.1 are

∫ ∫ +−= π θθθ

ωε 2

0/

0 22

2

cos),(RL

a

eXaX Rp

FdZdZP

mCRp

&& , (4.1a)

∫ ∫ +−= π θθθ

ωε 2

0/

0 22

2

sin),(RL

a

eYaY Rp

FdZdZP

mCRp

&& , (4.1b)

where m is rotor mass, eF is the total external load ( 5.022 )( eYeXe FFF += ) including rotor

weight, and εX and εY are X and Y components of non-dimensional eccentricity vector ε.

The integral terms represent the components of bearing reaction force F. At equilibrium

operating conditions, the external load eF and bearing reaction F have the same

magnitude and opposite directions.

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57

Χ ω

e

YYXX iFiFF +=

φ

Y

θ Fe

Χ ω

e

YYXX iFiFF +=

φ

Y

θ Fe

Figure 4.1 Journal bearing operating at an equilibrium point with eccentricity e, where F is bearing reaction force represented as integral term in Equation (4.1)

One approach to study the stability of the gas bearings linearizes the dynamic

equation (Equation 4.1) by small perturbations about a steady state position [Cheng and

Pan, 1965; Castelli and Elrod, 1965; Pan et al, 2003]. Corresponding stiffness and

damping matrix of the gas bearing are calculated by perturbation of the Reynolds

Equation (Equation 3.7) [Han et al, 1994; Hwang and Ono, 2003; San Andres and Wilde,

2000]. After stiffness and damping matrix are achieved, the bearing reaction force (the

integral term in Equation 4.1) can be decomposed into the reaction forces due to stiffness

and damping of the gas. Once the Jacobian matrix of the linearized equation has been

obtained, stability is assured if all eigenvalues of the characteristic equation of the

Jacobian matrix are negative.

In the other hand, the orbit method [Fuller, 1969; Piekos and Breuer, 1999; Jang

and Yoon, 2002] can accommodate arbitrary external loading patterns and disturbances

such as forced vibration, step-jump displacement, imbalance forces, various bearing

shapes and external loads. The orbit method traces the path of the journal center over

time, by solving journal dynamics (Equation 4.1) and the unsteady Reynolds Equation

(Equation 3.7) simultaneously, for given external forces and disturbances. Bearing

reaction forces at each time step are calculated by solving the unsteady Reynolds

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58

Equation (Equation 3.7). The orbit method can accommodate molecular rarefaction effect

very easily because non-linear unsteady Reynolds Equation is solved at every time step.

Due to the high non-linearity of the Reynolds Equation, all the previous works

[Cheng and Pan, 1965; Castelli and Elrod, 1965; Han et al, 1994; Piekos and Breuer,

1999; San Andres and Wilde, 2000; Jang and Yoon, 2002; Pan et al, 2003; Hwang and

Ono, 2003] assumed continuum Poiseuille flow ( PQ =1 in Equation 3.7). For the micro

gas bearings with sub micron bearing clearances, the molecular rarefaction effects cannot

be neglected and the perturbation method can not be used unless the Poiseuille flow

factor PQ is expressed in a explicit function of pressure P and gas film thickness H.

Previous studies on the DRIE-processed micro gas bearings, using the orbit

method [Piekos and Breuer, 1999], didn’t include molecular rarefaction effect because of

the relatively large bearing clearance (12-14µm).

4.1.1 Scheme for Numerical Integration If four state variables are defined as,

1XX =ε , (4.2a)

2XX =ε& , (4.2b)

3XY =ε , (4.2c)

4XY =ε& , (4.2d)

then, the Equation (4.1) can be represented as four 1st order differential equations as:

21 XX =& (4.3a)

∫ ∫ +−= π θθθ

ω20

/0 22

2

2 cos),(RL

a

eXa

RpF

dZdZPmC

RpX& (4.3b)

43 XX =& (4.3c)

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59

∫ ∫ +−= π θθθ

ω20

/0 22

2

4 sin),(RL

a

eYa

RpF

dZdZPmC

RpX& . (4.3d)

A fifth order Adams-Bashforth scheme [Nikravesh, 1988] as

)2511274261627741901(720

43211 −−−−+ +−+−∆

+= ni

ni

ni

ni

ni

ni

ni ffffftXX (4.4)

integrated equations (4.3). First five state variables in time domain were obtained by 4th

order Runge Kutta method. The advantage of Adams-Bashforth scheme over Runge

Kutta method is single evaluation of function at each time step instead of four

evaluations.

4.1.2 Stability Analysis: Threshold Speed A non-dimensional threshold speed9 [Cheng and Pan, 1965; Castelli and Elrod,

1965] 5.0

*

e

crit

FCm

ωω , (4.5)

was used to predict the onset of whirl instability, where mcrit is the maximum allowable

rotor mass for stable operation, and external load Fe has the same magnitude but opposite

direction with bearing reaction force at steady state for given operating conditions (ε, Λ),

see Figure 4.1.

The procedure of stability analyses are as follows: 1) Interested operating point (ε, Λ or

ω) 10 for stability check is selected and corresponding bearing reaction force F is

9 The current definition of threshold speed should be distinguished from rotor critical speed, where damped rotor vibration is maximized before reaching the threshold speed.

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60

calculated and external load Fe, in opposite direction to the bearing reaction force F, is

applied numerically, to establish static equilibrium; 2) Select test rotor mass m and give

very small step displacement (perturbation) from the steady state position; 3) Perform

orbit simulation, to check whether the disturbed rotor comes back to the steady state

position (the rotor is stable) or diverges (rotor is unstable); 3) Repeat the procedure

increasing the test rotor mass m until rotor becomes unstable; 4) Upon detection of rotor

instability, the test rotor mass m becomes critical rotor mass mcrit and ω*, the threshold

speed, can be calculated from equation (4.5). In early stages of gas bearing research

[Cheng and Pan, 1965; Castelli and Elrod, 1965], ω* was accepted as a general indicator

of gas bearing performance. The advantage of using ω* instead of critical rotor mass mcrit

is that ω* can be also decided by varying ω, with fixed rotor mass m becauseω* is a non-

dimensional number. In actual gas bearing systems, rotor mass is usually fixed and rotor

dynamics over wide speed ranges are more of interest. Disadvantage of using ω* comes

when plotting ω* versus Λ (or equivalently ω), because rotational speed ω appears at

both axes.

To test the orbit program, journal center was initially positioned at the origin

under external load corresponding to eccentricity (0.6,0) and convergence of journal orbit

to the steady state position (0.6,0) was followed as in Figure 4.2. The stability analyses of

stepped bearings were performed for θR=0o, and external load Fe was oriented such that

the journal was initially on the X-axis. For plain bearings, external load was directed

along –Y and initial journal location was obtained for successive disturbance and orbit

simulation. A step displacement of 0.0005 (0.05%) of the steady state eccentricity was

applied, and the corresponding journal orbits were obtained. Figure. 4.3 shows exemplary

diverging orbits of plain and stepped bearings with whirl frequency 0.465ω and 0.341ω

respectively. Figure 4.4 shows converging orbits for stepped bearing.

10 Note

26

CR

pa

µω and proportional to ω

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61

Figure 4.2 Converging orbit from origin (stepped gas journal bearing, Λ=0.6,

ε0=0.6, ω*=0.4, C=1µm)

The threshold speed maps were constructed by varying the non-dimensional

group on the right hand side of Equation (4.5), to estimate the threshold ω* at which

orbits diverge. Figure 4.5 and Figure 4.6 plot the threshold speeds ω* vs. Λ, with

eccentricity ε as a curve parameter for plain and stepped bearings respectively. Because

of the trial and error based method, the accuracy of ω* values is ±0.05. The general

tendencies of Figure 4.5 are similar to results reported in [Cheng and Panl, 1965; Castelli

and Elrod, 1965], where a peak threshold speed ω* exists around Λ=0.8~2, depending on

the L/D ratio, which indicates a maximum damping. Stepped gas bearings show a more

distinguished peak of ω* around Λ=2, at eccentricity ε=0.8 as shown in Figure 4.6

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62

(a) Plain bearing, Λ=1, ω*=1.6, ε0=0.6 (b) Stepped bearing, Λ=3, ω*=2.7, ε0=0.8

Figure 4.3 Diverging orbits Plain bearing: (a) Λ=1, ω*=1.6, ε0=0.6, (b) Stepped bearing, Λ=3, ω*=2.7, ε0=0.8

Figure 4.4 Converging orbit (stepped gas journal bearing, Λ=2, ω*=1.5, ε0=0.8)

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63

Figure 4.5 Threshold speed map for plain gas bearings

Figure 4.6 Threshold speed map for stepped gas bearings

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64

4.2 Discussion on the Whirl Instability

4.2.1 Quasi-Stable Behavior of Stepped Bearings

Stepped bearings can exhibit peculiar journal orbits for high ε and low Λ. Figure

4.7 shows a journal orbit (Λ=0.6, ω*=0.9) stabilizing at (εX,εY)=(0.694,0.547), after a

small step displacement (of 0.05% eccentricity) disturbed the system from its initial

steady state position, (εX0,εY0)=(0.8,0).

To support the phenomena, another orbit simulation was performed. Journal was

positioned at bearing center at t=0 and external load opposite to the load capacity

corresponding to position (0.8,0) or (0.694, 0.547) was applied and corresponding orbits

were obtained as in Figure 4.8. For given external load, the rotor stabilized at position

(0.694, 0.547) again.

These peculiar phenomena can be explained by the fact that there can be more

than one position (ε, φ, θR) of journal center that produce the same load capacity. From

the static analysis, the journal at (εX,εY)= (0.694,0.547) had the same load parameter

(ζ=0.019) as the journal at (εX0,εY0)=(0.8,0). Interestingly, for given external load, the

position (0.694,0.547) with φ=101.2o (see Fig. 4.8) is preferred to position (0.8,0) with

φ=63.8o. The load vector is tangent to the initial journal orbit, as should be. The location

(0.694,0.547) has θR of 21.76 o from step geometry. The stabilizing motions are

considered phenomena that minimize average pressure inside the bearing. The average

pressure at (0.694,0.547) was lower than at (0.8,0). Figure 4.9 and Figure 4.10 shows the

pressure profiles for the two locations. These stabilizing motions were negligible for Λ>

2 with ε =0.8 (Figure 3b), or ε < 0.8 with all Λ (Figure 4.4), due to smaller variation of

load capacities as discussed earlier.

Another interesting phenomena of step bearings are the initiation of self-sustained

confined orbit shown in Figure 4.11, when rotor is perturbed at equilibrium points for

certain operating conditions (ε=0.8 and Λ ≤1). These self-sustained vibrations did not

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65

progress to half–frequency whirl and did not converge to an equilibrium point either

within 50 cycles. It seems there are certain range of ω* below actual threshold speed (, at

which orbit begin to diverge,) for these self-sustained vibration to persist.

For stepped bearings with ε=0.8 and Λ ≤1, the data points in Figure 4.6 should be

understood as quasi-stable positions that transit to more stable journal positions

minimizing average pressure inside the bearings or that maintain self-sustained confined

vibration.

Figure 4.7 Stabilizing motion of journal to (εX,εY) =(0.694,0.547) by small

disturbance at (εX0,εY0)=(0.8,0), with Λ=0.6, ω*=0.9

external load

eccentricity

Figure 4.8 Motion of journal to (εX,εY) =(0.694,0.547) from origin for static loading corresponding to (εX0,εY0)=(0.8,0) with Λ=0.6, ω*=0.9. The angle between external

load and eccentricity vector is attitude angle

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66

Figure 4.9 Pressure profile at (εX,εY)=(0.694,0.547)

Figure 4.10 Pressure profile at (εX,εY)=(0.8,0.0)

Figure 4.11 Self sustained vibration by perturbation, 50 cycles, ε=0.8, Λ=1, ω*=1.7,

stepped gas journal bearing

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67

4.2.2 Threshold Rotor Mass

As discussed in section 4.1.2, plotting threshold speed ω* versus Λ complicates

understanding physical meaning of threshold speed. Of interest is the maximum

allowable rotor mass for a given operating speed (Λ) and operating position (ε) of the

rotor. Following the definition in [Piekos and Breuer, 1999], equation (4.5) can be

rewritten as a non-dimensional threshold rotor mass11,

25

2

*72

*

Λ=

ωζµ R

CL

pmm acrit . (4.6)

Once ω* is calculated for specific operating conditions (for given Λ and ζ (or Fe)), m*

can be calculated from equation (4.6) and is directly proportional to mcrit , maximum

allowable rotor mass.

Assuming steel, the rotor mass m for L=300µm, and D=500µm is 0.46mg, which

corresponds to m* =5.75×10-3 from Equation (4.6). Stability charts with m* vs. Λ are

plotted in Figure 4.12 and 4.13 for plain and stepped bearings respectively. The dashed

horizontal line marks the minimum mass that the rotor can have, if composed of steel

with the required geometry. The region under the dashed line pertains to a very small

mass, and is not a physically feasible operating condition for a steel rotor.

Fabricated stepped bearings without axial grooves have significantly lower m*

than plain bearings. From Figure 4.5 and 4.6, ω* ranges 0.6~4 for plain gas journal

bearings, and 0.3~2 for stepped gas journal bearings. Assuming ω* is the same order of

magnitude for plain and stepped gas journal bearings for a given Λ, the corresponding

threshold rotor mass m is proportional to load carrying capacities from Equation (4.5). 11 From definitions of load parameter (3.12) and bearing number (3.9), ζRLpF ae 2= ,

2

6

Λ

=RCpa

µω .

Plugging these into equation (4.5) and taking square at both sides,

ζζµζµω

225

2

5

2

222 *

72236* Λ

=

Λ

≡ mRC

Lpm

Lpm

RCp acrit

a

crita , where 5

272*

RC

Lpmm acrit

µ

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68

Stepped micro gas journal bearings have significantly lower load carrying capacities, see

Figure 3.5 and Figure 3.6. Initially, 2µm step was formed to lower load capacity and

allow the bearing to run with high eccentricity. However, due to small load capacities, the

fabricated stepped gas journal bearings show significantly lower threshold rotor mass

than plain micro gas journal bearings.

Figure 4.12 Stability chart of plain gas journal bearing given as non-dimensional

threshold speed m*

Figure 4.13 Stability chart of stepped gas journal bearing given as non-dimensional

threshold speed m*

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69

Micro turbines and engines are designed to be operating at over 1 million rpm

[Frechette et al, 2001b; Epstein et al, 1997] to generate useful power. Λ=10 corresponds

to about 1.3 million rpm. Even if inertia effects are very small, micro gas bearing systems

are highly unstable at high Λ, and require very high eccentricities for stability. Equivalent

rotor mass is the sum of the actual mass plus an additional mass that renders an inertial

load equivalent to the static load capacity. Calculated equivalent rotor mass, assuming

external load is applied only by rotor weight, is much bigger than the threshold rotor

mass (m or m*) even for plain gas journal bearings. This implies significant external load

is needed for the rotor with such a small threshold mass to obtain the necessary

eccentricities and thus stability.

4.3 Design Improvement of Stepped Micro Gas Bearings As discussed above, the fabricated micro gas bearings had low stability. To

improve the design, effects of various step configurations on the static and dynamic

characteristics were investigated. The first approach was to place a deep axial groove at

the beginning of every step, as shown in Figure 4.14. Axial grooves supply gas with

ambient pressure to minimize high negative pressure, shown in Figure 3.7 and decrease

attitude angles.

Χ

θ ω

e

axial groove

Y

Figure 4.14 Axial grooves formed at the beginning of every step. Axial grooves

supply gas with ambient pressure to minimize high negative pressure and decrease attitude angles

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70

The second approach was the variation of the number of steps, step height, and

θS/θP without adopting axial grooves, where θS is the angle one step occupies, and θP is

2π divided by the number of steps as shown in the following figure.

4.3.1 Static Analysis of Improved Design

Figure 4.15 shows ζ and φ vs. step height, for Λ=1 and 10 and θR= 0o. Two grid

points occupied one axial groove (of width 17.5µm) in the simulation. While load

capacity is similar to step bearings without axial grooves for the same step height,

attitude angles are much lower (than step bearings without axial grooves), and minimize

at around 0.75~1.25µm, implying an optimal step height in terms of attitude angles and

cross stiffness.

Figure 4.16 and 4.17 show load parameter ζ and attitude angle φ vs. θS/θP for

micro gas bearings with six steps and four steps respectively, with θR=0o, ε=0.6, and Λ=1.

The load parameter ζ increased as θS/θP decreases and step height decreases for both six-

stepped and four-stepped bearings. The bearings with four steps had larger load

parameter ζ than the bearings with six steps (for the case of the same step height) due to

large bearing land area to build enough hydrodynamic pressure. While, the stepped

bearings with 2µm steps reveal sharp decrease of load capacities as θS/θP increases, the

stepped bearings with 1µm steps had lower sensitivity of load parameters to the θS/θP

ratio, due to relatively small step height. The variation of attitude angles φ is small

compared to the variation of load parameters, as step configuration changes. The

optimum θS/θP was not found in terms of ζ.

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71

(a) Λ=1

(b) Λ=10

Figure 4.15 Static performance for stepped gas journal bearings with axial grooves (θR= 0o): (a) Λ=1, (b) Λ=10

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72

Figure 4.16 Load parameter and attitude angle of six-stepped bearings without

axial grooves for various step configurations (θR=0o, ε=0.6, and Λ=1)

Figure 4.17 Load parameter and attitude angle of four-stepped bearings without

axial grooves for various step configurations for (θR=0o, ε=0.6, and Λ=1)

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73

4.3.2 Dynamic Analysis of Improved Design Orbit simulations were performed for the stepped bearings with axial grooves.

Table 4.1 summarizes the effect of axial grooves on the ω* and m* for θS/θP=0.5. The

values in parenthesis represent the m* ratio of the investigated bearings to the fabricated

stepped bearing (θS/θP =0.5, 2µm steps, no axial grooves). Table 4.1 shows substantial

improvement of stability for low Λ by adopting axial grooves. Table 4.1 also presents

orbit simulations for 1µm step height (considered optimal) with axial grooves. Over the

entire region of operating conditions, threshold mass m* increased with improvements

more prominent at lower Λ. Despite improved stability by adopting axial grooves, overall

performance was inferior to the plain gas bearings, due to similar load capacities with

bearings without axial grooves. However, very high threshold mass (shown as italicized

bold-faced) larger than plain bearings (m*= 2.791 for ε=0.8) was observed at Λ=1, and

ε=0.8, implying very high damping. There were no noticeable stabilizing journal motions

at high eccentricities for step bearings with axial grooves.

Table 4.2 presents the effects of different θS/θP, number of steps, and step height

on theω* and m* for the bearings without axial grooves. As shown in Figure 4.16,

attitude angles of six-stepped bearings are almost the same for different step

configurations; ω* is almost the same (0.9~1.05), and threshold mass m* is directly

proportional to the load capacity (the first two columns of Table. 4.2). However,

noticeable improvement of stability was observed by reducing the number of steps to

four. The italicized bold-faced ω* and m* in Table 4.2, represent the bearings with higher

threshold mass than the plain bearings (m*=0.257 for ε=0.6), even if the load capacity

was lower than the six-stepped bearings with 1µm steps or plain bearings.

When the number of steps is reduced without axial grooves, self-sustained

confined orbit (similar to Figure 4.11 for six stepped bearing without axial groove) was

observed (Figure 4.18) even at low eccentricity (ε=0.6) when Λ≤1. However the

magnitude of the orbits were much smaller compared to the orbits for six-stepped

bearings (Figure 4.11).

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74

Table 4.1. ω* and m* for stepped bearing with axial grooves (θS/θP =0.5, θR=0o) Step height 2µm

ε=0.5 ε=0.6 ε=0.7 ε=0.8

Λ=1 ω*=1.7

m*=0.02778 (3.02)

1.7 0.03869 (2.52)

2.1 0.08722 (2.39)

11 4.09752 (41.2)

Λ=10 1.5

0.00247 (0.68)

1.5 0.00320 (0.75)

1.5 0.00416 (0.80)

1.6 0.00636 (0.90)

Step height 1µm ε=0.5 ε=0.6 ε=0.7 ε=0.8

Λ=1 1.4

0.03451 (3.75)

1.6 0.06140 (3.99)

2.1 0.14960 (4.10)

10 5.36439 (53.93)

Λ=10 1.5

0.00461 (1.27)

1.4 0.00532 (1.25)

1.35 0.00657 (1.26)

1.5 0.01113 (1.58)

Table 4.2. ω* and m* for different θS/θP, the number of steps (θR=0o, ε=0.6, Λ=1)

Bearings with 6 steps Bearings with 4 steps 2µm steps 1µm steps 2µm steps 1µm steps

θS/θP =0.333 ω*=0.95

m*=0.02365 (1.54)

1 0.04059 (2.64)

6 1.50223

(97.71)

1.7 0.15047 (9.79)

θS/θP =0.5 1

0.01537 (1)

1.05 0.03147 (2.05)

3.5 0.30970 (20.14)

1.55 0.08630 (5.61)

θS/θP =0.667 0.9

0.00676 (0.44)

0.9 0.01656 (1.08)

1.3 0.01868 (1.22)

1.4 0.04370 (2.84)

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75

Figure 4.18 Orbit for 50 cycles for four stepped bearing without axial grooves, θS/θP =0.333, Λ=1, ε=0.6, step height 2µm, and ω*=6 (m*=1.5022, m=0.12g)

Whirl instability is often understood as resonance phenomena between journal

motion and circumferential gas flow, at low eccentricity and high attitude angle. From the

orbit simulations for various step geometries, and calculation of circumferential flow

speed, threshold mass was dependent on the load capacity, attitude angle, and how

effectively circumferential gas flow is blocked. For six-stepped bearings, load capacities

are significantly lower than the plain bearings, due to small bearing land area to build

effective hydrodynamic pressure. By adopting axial grooves, attitude angles became

much smaller at low eccentricities, rendering low cross stiffness and improved stability,

even if load capacities did not increase. Four-stepped bearings had much higher load

capacities than six-stepped bearings, permitting higher stability. However, for the four-

stepped bearings with 1µm steps, higher attitude angles (even if load capacities were a

little higher) than the bearings with 2µm steps (Figure 4.17), and insufficient step height

to block the circumferential gas flow effectively (presumably) as 2µm steps, led to lower

threshold mass than the bearings with 2µm steps.

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76

4.3.3 Four-stepped Bearings with Axial Grooves From the previous investigation on the dynamic performance of the micro gas

bearings with various step geometries (with six stepped bearing with axial grooves and

four-stepped gas bearings without axial grooves), the four-stepped micro gas bearing with

axial grooves in Figure 4.19 seems the most effective to increase stability.

Figure 4.19 Four-stepped micro gas bearings with axial grooves

Figure 4.20 presents load parameter ζ and attitude angle φ versus bearing number Λ, for

θS=30o and θR=0o. Both figures have clearance C=1µm. With axial grooves, the bearings

with 1µm step showed lower attitude angle than those with 2µm step. Without axial

grooves, the bearings with 2µm step showed smaller attitude angles as shown in the

Figure 4.17. Figure 4.21 shows pressure profile at the bearing center. Unlike the pressure

profile of six stepped bearing without axial grooves (shown in Figure 3.7), more direct

stiffness and stability can be expected.

Orbit simulation was performed for the bearings with the geometry of Figure

4.19, for ε=0.5 and 0.6. Figures 4.22 to 4.25 display orbits for various operating

conditions. Figure 4.22 with Λ=1, ε=0.6 has converging orbits with chaotic motion, when

ω* is very large (> 15). Notice the different orbits for the different step heights. As ω* is

increased to 40 (see Figure 4.23) with other conditions as in Figure 4.22(b), the orbit

shows chaotic motion without converging or diverging, even after 400 simulated cycles.

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77

(a) C=1µm, step height 2µm

(b) C=1µm, step height 1µm

Figure 4.20 Static performance of four-stepped micro gas journal bearings with axial grooves: (a) C=1µm, step height 2µm, (b) C=1µm, step height 1µm

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78

Figure 4.21 Pressure profiles (Λ=1, ε=0.4) of four-stepped micro gas bearings

with axial grooves

In Figure 24 (with Λ=5, ε=0.6, ω*=5, and step height 1µm), the orbit diverges

initially (by perturbation) but finally becomes a self-sustained stable orbit. This is true for

2.4<ω*<8.5, however, for ω*>8.5, the orbit diverges continuously and becomes unstable

with whirling motion. The magnitude of vibration in the self-sustained stable orbit

increased as ω* increased within its stable range. For both step heights (1µm and 2µm),

there was a range of ω* that initiated the self-sustained stable orbit for ε=0.5 and 0.6.

When eccentricity was increased to 0.8, with the same bearing number (Λ=5), journal

orbit became chaotic (Figure 4.25), instead of a self-sustained finite orbit. The chaotic

characteristics increased as ω* varied from 1 to 20. The chaotic motions along the Y

direction were confined within the same range, and only the amplitude of vibration along

the X-direction increased as ω* increased (see Figures 4.25). However, the journal orbits

did not diverge.

The exact boundaries of eccentricity ε and bearing number Λ, which initiate self-

sustained stable orbit or chaotic motions, are not clear from the limited number of orbit

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79

simulations performed here. Because the ranges of chaotic motions are extremely small

(∆ε~10-3), all orbits were assumed stable because half-frequency whirl was never

observed in the simulations.

Instead of full threshold mass for all operating conditions, threshold speed and

rotor mass at ε=0.5 and ε=0.6, for Λ=1 and Λ=5, were calculated in Table 4.3. Compared

to Table 4.1 and 4.2, the four-stepped bearings with axial grooves appear to be much

more stable than other stepped bearings.

Table 4.3 Threshold speed12 ω* and rotor mass m* for four-stepped gas bearings with axial grooves C=1µm, step height=1µm, θS/θP =0.333 (θS =30o)

Λ=1 Λ=5

Step 1µm Step 2µm Step 1µm Step 2µm

ε=0.5 ω* =3.0 m* =0.2793

2.0 0.1048

3.5 0.0767

2.4 0.0278

ε=0.6 >1513 >10.3495

>15 >8.8486

8.5 0.6408

3.6 0.0892

12 The error of the threshold speed ω* in the Table 4.3 is ±0.2. 13 At ω* =15, the orbit was still stable

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80

(a) Orbit for step height 1µm

(b)

(b) Orbit for step height 2µm

Figure 4.22 Orbit for 100 cycles of four-stepped gas bearings with axial grooves, Λ=1, ε=0.6, and ω*=15: (a) Orbit for step height 1µm, (b) Orbit for step

height 2µm

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81

Figure 4.23 Orbit for 400 cycles of four-stepped gas bearings with axial

grooves, Λ=1, ε=0.6, step height 2µm, and ω*=40. Very slow chaotic motion initiates and does not converge or diverge

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82

(a) Orbit for total 200 cycles

(b) Orbit for last 10 cycles

Figure 4.24 Orbit for four-stepped gas bearings with axial grooves, Λ=5, ε=0.6, ω*=5, and step height 1µm: (a) Orbit for total 200 cycles, (b) Orbit for last 10 cycles

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83

(a) Orbit for ω*=1

(b) Orbit for ω*=5

(c) Orbit for ω*=10

(d) Orbit for ω*=20

Figure 4.25 Orbit for 200 cycles of four-stepped gas bearings with axial grooves, Λ=5, ε=0.8, and step height 1µm: (a) Orbit for ω*=1, (b) Orbit for ω*=5, (c) Orbit

for ω*=10, (d) Orbit for ω*=20

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84

4.4 Discussions of Stability Analyses The foregoing dynamic stability analyses can locate feasible stable operating

points of the micro gas bearing. In a practical sense, a rotor running at a prescribed

eccentricity (high for stable operations), poses difficulties, especially for micro or even

meso scale applications. When the rotor-bearing configuration and operating speed are

given, the eccentricity should be chosen from the stability chart (such as Figure 4.13),

where threshold rotor mass should exceed the given rotor mass. The weight of the rotor

mass should generate the necessary eccentricity, otherwise, additional external load

should be applied. Problems involving additional loading include: difficulties controlling

bearing and rotor orientation in terms of attitude angle and step locations; unavoidable

and very large imbalance force, especially at high rotational speeds; and crash of the rotor

onto the bearing wall, at high eccentricity.

More amenable is an investigation of bearing performance under actual dynamic

load (rotor weight and imbalance force, generated by operating speed). If rotor and

bearing are initially not perfectly aligned, the initial misalignment can become a

disturbance. In the following sections, the fabrication method of meso scale (~mm) gas

bearings using X-ray lithography, and performance of the gas bearings in two application

areas will be investigated, in terms of three-dimensional imbalance response.

4.5 Feasibility Study of Meso Scale Gas Bearing In this section, new fabrication processes for the meso scale gas bearings are

suggested. Two application areas will be introduced and dynamic performance at a

systems level will be investigated.

4.5.1 Fabrication Processes of Meso Scale Gas Bearings Typical electron-beam lithography for initial optical mask to make a final X-ray

mask, provides a maximum resolution of 6nm and a usual beam spot size of 0.1µm.

Theoretically, several identical patterns within the resolution of the initial optical mask

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85

can be transferred to the final parts. These parts are identical within the resolution of the

X-ray mask. The accuracy of pattern transfer from the optical mask to the X-ray mask

depends on process conditions.

The fabrication processes of the meso scale gas bearings are based on stacking

several identical parts, made by X-ray lithography. Due to the in-plane lithographic

technique process, there is no limit on the diameter of the bearings. Figure 4.26

conceptually depicts a meso scale gas bearing of 2mm length, with step geometry shown

in Figure 4.19, made by stacking or fusion bonding of 500 µm thick four identical

bearings. Both end faces have spiral grooves, to serve as thrust bearings. The spiral

grooves14 can be easily formed by single optical lithography and etching process on the

electroplated part.

Figure 4.26 Conceptual figure of meso scale gas bearing with spiral grooved

thrust bearings, D=L=2mm

4.5.2 Applications of Meso Scale Gas Bearings Potential applications of meso scale gas journal bearings include Laser scanner

[Ono and Hwang, 1994; Hwang and Ono, 1996], and hard disc drive (HDD) main spindle

bearings [Hwang and Ono, 2003; Jang and Yoon, 2002]. Other applications may include:

meso scale turbine for micro power generation, dental drills, miniature precision machine

tool, and micro motors. Polygon mirror attached to a high-speed spindle in Laser scanner

14 The spiral grooved thrust bearings have a seal region, which was not described in the Figure 4.25, before the spiral grooves reach journal bearing.

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86

has rotational speed ranging from 30,000 rpm to 50,000 rpm, for Laser printer and photo

printer applications. Another application of Laser scanner is an optical low coherence

reflectometry (OLCR) [Szydlo et al, 1998], an imaging technique, for various science and

engineering field including biological, medical, material growth, optoelectronics, etc.

OLCR consists of a broadband light source and a coherent cross correlation light

detector. Measurements must be performed rapidly, to capture or freeze motion of

moving or live objects. Increasing image acquisition rate and light scanning speed are

crucial. Szydlo et al [Szydlo et al, 1998] demonstrated an air turbine driven gold plated

cubic mirror with rotational speed of 427,000 rpm, equivalent to a scan repetition rate of

28.5kHz. Heshmat [Heshmat, 2003] reported stable operation of mesoscopic turbine

simulator, at 700,000 rpm, using miniature foil gas bearings, made via conventional

precision machining.

Figure 4.27 depicts suggested configuration of Laser scanner, with hydrodynamic

gas bearing suggested in Figure 4.26. The simulation parameters, including dimensions,

are shown in Table 4.4. The rotor mass and moments of inertia were calculated from

solid models and material densities. The origin of the simulation’s coordinate system was

the center of the gas bearing.

To meet high demand for bigger information storage capacity, performance

requirements of hard disc drive (HDD) spindle bearings became more stringent. For

20Gb/in2 HDD, tracks per inch (TPI) is 50000, which requires a non-repeatable run out

(NRRO) of 30nm[Hwang and Ono, 2003]. For 10Gb/in2 HDD, the maximum allowed

NRRO is 0.5µm [Hwang and Ono, 2003]. Figure 4.28 depicts an HDD spindle rotor

consisting of two discs, two clamps, a permanent magnet rotor, and two spacers. Included

in Table 4.5 are the rotor mass and moments of inertia, calculated from solid models and

the material densities. Simulated gas bearing has diameter and length of 6mm and

rotational speed was fixed at 15,000 rpm.

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87

Scanner Mirror

Bearing unitMotor x (X)

y (Y)

z (Z)

(a) Assembled unit (b) Rotor

Figure 4.27 Laser scanner: (a) Assembled unit, (b) Rotor. The X-Y-Z is a fixed reference frame and x-y-z is a rotational coordinate attached to rotor center

Spacer

Clamp Disc

Permanent magnet

Clamp

Shaft x (X)

z (Z)

Figure 4.28 HDD spindle rotor: The X-Y-Z is a fixed reference frame and x-y-z is a

rotational coordinate attached to rotor center. y(Y) axis is into the plane

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88

Table 4.4 Design parameters of Laser scanner rotor

Rotor mass 0.3g Imbalance radius 0.1µm

Ixx = Iyy 1.05x10-9 kgm2 Izz 8.97x10-10 kgm2

Bearing diameter 2mm Bearing length 2mm

Bearing clearance 1µm Rotational speed 100,000-1,000,000rpm

Working temperature 20oC Air viscosity 1.79x10-5 Ns/m2

Molecular mean free path 64nm

Table 4.5 Design parameters of HDD rotor

Rotor mass 57.3g Imbalance radius 4µm

Ixx =Iyy 2.18x10-5 kgm2 Izz 4.25x10-5 kgm2

Bearing diameter 6mm Bearing length 6mm

Bearing clearance 1µm Rotational speed 15,000 rpm

Working temperature 50oC Air viscosity 1.92x10-5 Ns/m2

Molecular mean free path 70nm

4.5.3 Three-Dimensional Imbalance Response In this section, three-dimensional imbalance responses of Laser scanner and HDD

rotors, including gyroscopic effects, are investigated. In Equation (4.1), Fe can

accommodate any time varying external force. Assuming gravity is directed along x-

direction, with imbalance radius a, equation (4.1) for the systems shown in the Figure

4.27 and 4.28 becomes

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89

∫ ∫

++−= π τωθθθ

ωε 2

0/

0 2

2

2

2 coscos),(RL

a

aX Rp

mamgdZdZPmC

Rp&& , (4.7a)

∫ ∫ +−= π τωθθθ

ωε 2

0/

0 2

2

2

2 sinsin),(RL

a

aY Rp

madZdZPmC

Rp&& . (4.7b)

Here, dot means derivative with respective to tωτ = . Figure 4.29 shows a rotor (at

eccentricity e) with angular rotational speed xϕ& and yϕ& along the x- and y-axis,

respectively. X-Y-Z is a fixed reference frame with origin at the bearing center and x-y-z

is a rotational coordinate attached to the rotor center. The moment due to imbalance force

becomes

jmazimazM uuu τωτω cossin 22 +−= (4.8)

where zu locates the imbalance mass along the z direction. i and j are unit vectors along

the x and y direction, respectively.

Xx

Y

Z

e

y

yϕ&

Figure 4.29 Rotor with angular rotation and eccentricity: The X-Y-Z is a

fixed reference frame with origin at the center of bearing and x-y-z is a rotational coordinate attached to rotor center.

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90

When there are instantaneous rotational speeds xϕ& and yϕ& , the angular momentum

vector G and instantaneous angular rotation vector Ω of the rotor with the spin speed ω,

become

kIjIiIG zzyyyxxx ωϕϕ ++= && (4.9)

kji yx ωϕϕ ++=Ω && (4.10)

respectively. The relation between the change of angular momentum and the total

external moment M due to the imbalance force and bearing reaction force, becomes

MdtGd

= (4.11)

By inserting equation (4.9) into equation (4.11), incorporating equation (4.10), the

equations describing the conical motion of the spinning rotor can be derived as,

uxiuxyzzyyyxxx MMIII +=+− ϕωϕωϕ &&&& (4.12a)

uyiuyxzzxxxyyy MMIII +=−+ ϕωϕωϕ &&&& (4.12b)

where Miux and Miuy are reaction moment from gas bearings calculated via integration of

moment by dynamics pressure. Note equation (4.12) pertains to the rotating coordinate

systems x-y-z, attached to the rotor. The equation should be referenced to the fixed X-Y-Z

coordinate.

The relation between instantaneous rotational speed about x-y-z coordinate and X-

Y-Z coordinate becomes, from [Nelson, 1976]

[ ]

Ω=

Y

Xy

x

Tψψ

ωψψ

&

&&

&

or [ ]

=

Ω−

ωψψ

ψψ y

x

Y

X T &

&

&

& 1 (4.13a)

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91

[ ]

−=

XXY

XXY

Y

Tψψψ

ψψψψ

sin0coscoscos0sincos

01sin (4.13b)

where Ω is rotation speed of rotor with respect to fixed X-Y-Z coordinate. Using relation

(4.13), equation (4.12) becomes

uXRLRLaYzzXxx MdZdZZPRpII +∫ ∫=+ −

π θθθϕωϕ 20

2/2/

3 sin),(&&& (4.14a)

uYRLRLaXzzYyy MdZdZZPRpII +∫ ∫−=− −

π θθθϕωϕ 20

2/2/

3 cos),(&&& (4.14b)

Now external moment uXM and uYM are for fixed reference frame X-Y-Z, attached to

bearings, and bearing reaction moments are expressed as integration terms of pressure

field at the bearing surfaces. Due to the gyroscopic effect of the spinning rotor,

Xϕ& and Yϕ& generate moments along Y- and X- directions in addition to those by the

imbalance force and bearing reaction force. Non-dimensionalizing equation (4.14) using

RCϕψ = and τ =ω t,

+∫ ∫+−= − 3

20

2/2/2

4

sin),(Rp

MdZdZZP

CIRp

II

a

uXRLRL

xx

aY

xx

zzX

π θθθω

ψψ &&& (4.15a)

+∫ ∫−+= − 3

20

2/2/2

4

cos),(Rp

MdZdZZP

CIRp

II

a

uYRLRL

yy

aX

yy

zzY

π θθθω

ψψ &&& (4.15b)

Here, dot means derivative with respective to τ. Equation (4.15) with equation (4.7), can

simulate complete 3-D imbalance responses. In a strict sense, the imbalance forces, in

equation (4.7), should be transformed to those with respect to the fixed bearing

coordinates X-Y-Z. However due to very small bearing clearance, compared to bearing

radius or length, the numerical error is negligible.

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92

To calculate pressure field at bearing surface when journal has eccentricities εX, εY

and misalignment angles ψX, ψY, local gas film thickness H should be expressed as a

function of εX , εY , ψX ,and ψY . Gas film thickness H for Reynolds Equation becomes

θψεθψε sin2

cos2

1

+−−−

+−+−= Z

RLZ

RLH XYYX (4.16)

In the simulations of Laser scanner, imbalance mass was assumed as 0.01%15 of

rotor mass, located on the outer surface of rotor shaft, giving imbalance radius of 0.1µm.

For HDD spindle rotor, imbalance mass was 0.13% of rotor mass, to give the imbalance

radius and imbalance force of 4µm and 0.56N, respectively, at 15,000RPM, which are

typical operating conditions of HDD spindles [Hwang and Ono, 2003; Jang and Yoon,

2002]. The air viscosity and molecular mean free path were adjusted according to the

working temperatures as shown in Tables 4.4 and 4.5.

To investigate conical stability of the gas bearings, the rotor was given initial

misalignment angles (ψX0, ψY0)=(0.2,0.2), and trace of the misalignment angles was

simulated. In the simulation, zu=0 (the location of imbalance force in axial direction) to

eliminate a moment by imbalance force in equation (4.8).

Figures 4.30 and 4.31 are orbits for the HDD spindle rotor with imbalance forces

of 0.033N and 0.56N, respectively. For the meso scale gas bearing (with dimensions

given in Table 4.5) to be used for an HDD spindle with area density of 20Gb/in2, the

imbalance force should be reduced below 0.033N.

Figure 4.32 and Figure 4.33 shows series of rotor orbits and their frequency

spectrum for Laser scanner at different rpm. As rotational speed increased, vibrations

increased and reached its maximum at around 440,000 rpm, which was a first critical

speed. At the critical speed, the phase angle of rotor with respect to imbalance force was

109.5o. Above the first critical speed, the bearing was stable until above 600,000rpm. At 15 The small imbalance was chosen to excite an imbalance force, which is within the limit of load capacity of the bearing when rotor passes through the first critical speed.

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93

around 660,000 rpm, half-frequency whirling initiated, indicating the bearing’s maximum

allowable speed. Figure 4.34 shows trace of misalignment angles from initial disturbance

at 860,000 rpm.

From the dynamic analyses, the meso scale gas bearings had adequate load capacities

and dynamic stabilities, over wide operating ranges.

(a) (b)

Figure 4.30 Three-dimensional imbalance response of HDD rotor, 50 cycles: (a)

Orbit at Z=0, (b) Stable rotor from initial misalignment (ψX0=0.2, ψY0=0.2), Imbalance force: 0.56N, Speed: 15,000 RPM

(a) (b)

Figure 4.31 Three-dimensional imbalance response of HDD rotor, 50 cycles: (a) Orbit at Z=0, (b) Stable rotor from initial misalignment (ψX0=0.2, ψY0=0.2),

Imbalance force: 0.033N, Speed: 15,000 RPM

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94

(a) 100,000 rpm (b) 200,000 rpm

(c) 300,000 rpm (d) 400,000 rpm

(e) 440,000 rpm (f) 500,000 rpm

Figure 4.32 Rotor orbits of Laser scanner rotor, 30 cycles; cont.

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95

(g) 600,000 rpm (h) 700,000 rpm

(i) 800,000 rpm (j) 860,000 rpm

Figure 4.32 Rotor orbits of Laser scanner rotor, 30 cycles; (a) 100,000rpm (b) 200,000 rpm (c) 300,000 rpm (d) 400,000rpm (e) 440,000rpm (f) 500,000 rpm (g)

600,000 rpm (h) 700,000 rpm (i) 800,000 rpm (j) 860,000 rpm

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96

(a) 640,000 rpm (b) 660,000 rpm

(c) 700,000 rpm (d) 800,000 rpm

Figure 4.33 Frequency spectrum of Laser scanner rotor orbit; (a) 640,000 rpm (b) 660,000 rpm (c) 700,000 rpm (d) 800,000 rpm

Figure 4.34 Trace of misalignment of Laser scanner rotor at 860,000 rpm from

initial misalignment

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97

Chapter 5

Testing of Micro Gas Bearing

In this chapter, test results are presented, and technical issues involved in the test

are discussed.

5.1 Issues on Gas Bearing Tests Figure 5.1 depicts a stable rotor running at eccentricity e under a given external

load. For the rotor to run at the given eccentricity, several ideal conditions should exist:

the rotor mass should be smaller than the threshold rotor mass for dynamic stability; there

should be no imbalance force; and an external load (including rotor weight),

corresponding to the eccentricity, should be applied along correct direction. Among the

conditions listed above, the most difficult to fulfill is avoiding imbalance force,

practically impossible in rotating machinery. Imbalance force, which depends on the

imbalance radius and imbalance mass, is usually much larger than the static load, at very

high rotating speeds.

Figure 5.2 depicts the macro scale gas bearing test rig from [Wilde and San

Andres, 2003]. Two three-lobe hybrid gas bearings support the rotor, driven by an

electric motor located at the center of the rotor. Radial run out was measured using an

eddy current sensor. Figure 5.3 depicts the meso scale turbo jet simulator [Heshmat,

2003], using foil gas bearings of 6mm diameter. Here an impulse turbine, formed directly

on the rotor surface, with multiple nozzles around the shroud, drove the rotor. With

choked conditions at the nozzles, stable operation at 700,000rpm was reported. Silicon

micro turbine from MIT [Lin, C.C., 1999] also embedded centrifugal reaction turbine to

drive a rotor with 4mm diameter (see Figure 1.4).

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98

θΧ ω

e

φ

θR

Y

Reaction

External load

Figure 5.1 Description of rotor running at certain eccentricity under given

external load

Figure 5.2 Macro scale gas bearing tester [Wilde and Andres, 2003]

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99

Figure 5.3 Meso scale turbo jet simulator supported by foil gas bearings

[Heshmat, 2003]

The macro or meso scale gas bearing test rig could use an electric motor or an

impulse turbine as a drive, supplying direct torque to the rotor. In general, a gas bearing

tester should be very similar to the actual system, where the gas bearings will be used.

Drives for high-speed spindles or turbo compressor, which use gas bearings, should be

engineered very carefully, to match the embedded gas bearings. The static and dynamic

stability analyses in previous chapters give a sanity check for basic performance,

including maximum load and allowable rotor mass that a specific bearing can support.

5.2 Testing of Micro Gas Bearings For testing of the fabricated micro gas bearings, the small shaft (0.5mm)

complicates embedding of the electric drive, or formation of the impulse turbine on the

shaft directly. First test rig is shown in Figure 5.4. Here, small turbine with diameter

1.6mm made of SU-8 was assembled onto the shaft, made of bearing steel SAE 52100

with diametral tolerance ±0.25µm, using the large thermal expansion coefficient of SU-8

at 50oC to aid an interference fit. Total rotor mass was measured as 2.3mg per bearing.

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100

Two identical circular nozzles with 0.3mm diameter drove the turbine at offset locations

to cancel radial force16 and deliver only torque. Capacitance sensor with 25nm resolution

from MTi, inc., which is the smallest commercially available sensor, measured vibrations

of the test bearing (not on rotor shaft), because direct measurement of shaft vibrations

was not possible due to very small size of the shaft.

The first criterion of successful operation at gas bearing mode, was near zero

vibration signal from the bearings, because once the rotor took off, the vibration of the

bearing would nearly vanish. The second criterion was SEM image of tested bearing. In a

gas bearing mode, the bearing surface should be almost free of scratch. To identify

scratch easily after the test, uncoated bearings were used.

Due to the uncertainty of air jet forces from nozzles and the imbalance force,

precise quantification of the total external load was not possible.

5.2.1 Assembly of Test Rigs To assemble two micro gas bearings with shaft, simple and effective self-aligning

method was developed as described in Figure 5.5. In step (a), two bearings are put onto

rotor (shaft and turbine assembly). Photo resist is dispensed in step (b), allowing photo

resist to seep into bearing clearance by capillary action. In step (c), residual photo resist is

wiped out and soft baking follows. Then two gas bearings are fixed to the bearing

housing structure using epoxy in step (d). Photo resist inside the gap is dissolved in

acetone to release the rotor in step (e). In step (d), the epoxy should be chemically

resistant to acetone.

16 Eliminating radial load could lead to instability because rotor eccentricity could be very small with only rotor weight.

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101

Nozzle

Capacitance sensor

Nozzle

Nozzle

(a) Description of gas bearing tester

(b) Photo of assembled gas bearing tester

(c) Capacitance sensor and drive shaft with press-fitted SU-8 turbine

Figure 5.4 Photo of gas bearing tester with open air jet; (a) Description of gas bearing tester (b) Photo of assembled gas bearing tester (c) Capacitance sensor and

drive shaft with press-fitted SU-8 turbine

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102

(a) (b) (c) (d) (e)

Figure 5.5 Assembly procedures of micro gas bearings; (a) Pre-assembly (b) Photo resist dispensing (c) Soft baking (d) Anchoring to base (e) Release

5.2.2 Test Results Preliminarily measured speeds17 of 2.3mg rotor with plain gas bearings were

around 8,890 rpm as shown in Figure 5.6, far below the expected speed. Rotational speed

was measured by counting the number of peaks in certain time interval or taking FFT of

the voltage signal.

(a) Supply pressure 35psi (b) Supply pressure 50psi

Figure 5.6 Photonic sensor signal measuring rotor speeds; (a) Supply pressure 35psi (b) Supply pressure 50psi

To investigate the very low speed, a simple turbine model was developed. From

Figure 5.7, using control volume method, torque by air jet becomes

17 Because the photonic sensor had much larger diameter than width of single turbine blade, the photonic sensor measured averaged oscillating signal with frequency of rotating speed of turbine, which is not perfectly symmetrical.

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103

( )2ωρη jjnajeffjet ruarT −= (5.1)

where ηeff is an overall turbine efficiency considering all geometric factors of nozzle and

turbine blades, ρa is an air density, an is nozzle area, uj is air jet speed, rj is the radius of

air jet action, and ω is a rotational speed of the turbine. Windage friction torque is

αωρ ⋅⋅≅ jjbabw rrANT 2)( (5.2)

where α is a windage loss factor, Nb is number of blade, Ab is blade area. When α=1, all

the air in front of each blade is assumed stationary and windage loss is maximum.

ρaanuj

ω

rj

Figure 5.7 Impulse turbine with open air jet

Bearing friction torque bT is

( ) RWruaRRFTT Rjjnaeffbbb µωρηµµ 2221 +−==+ (5.3)

where µ is a friction coefficient at the bearing surface, Fb is a summation of two bearing

forces, WR is a rotor weight per bearing, and R is radius of the bearing. From torque

equilibrium,

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104

21 bbwjet TTTT ++= (5.4)

Rearranging equation (5.4) for ω gives

( )( )

( )

( )0

12

2

122

22

2 =+−

+−

++−

−−

αµη

ρµ

ωµη

ωαµη

ωµηω

jn

bjeff

jna

Rmjeff

jn

bjeff

mjeff

raA

rR

raRW

rR

raA

rR

rR (5.5a)

or

( )( ) ( ) ( ) ( )

−+

−+

+

+−

−=

RrarA

RraA

rraRrRW

raArR

rR

jneff

jb

jneff

b

jjnamjeff

R

jn

bjeff

mjeff

µηα

µηα

ρωµηµ

αµη

ωµηω 121212

1

12 2

(5.5b)

where jjm ru /=ω . Equation (5.5) was plotted for a dental drill turbine (for given speed

400,000 rpm@ 35 psi, assuming air jet speed 200 m/s), as a function of friction

coefficient of the bearing, as shown in Figure 5.8. From given speed information, turbine

efficiency ηeff and windage loss factor α were estimated as 0.6 and 0.1, respectively.

Surprisingly, turbine speed is almost independent of bearing friction 18 until bearing

friction reaches 0.2~0.3 (typical friction coefficients of low friction coatings). From the

figure, turbine speed is a strong function of windage loss and turbine efficiency, and a

very weak function of bearing friction.

With, ηeff =0.6 and α =0.1, the speed of SU-8 micro turbines was estimated to

be around 900,000 rpm. However, as shown in Figure 5.6, measured turbine speed was

far below the expected speed. Even under choked conditions of the nozzles, the turbine

speed did not reach over 20,000 rpm. In an open air jet configuration without properly

designed shroud, negative pressure at trailing edge of the turbine generated presumably

18 However, it should be noted that thermal heat generation is directly proportional to friction coefficient, and bearing performance deteriorates very quickly at dry friction region if adequate cooling is not available in actual rotating machinery

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105

high negative pressure, rendering windage loss factor α >> 1 and turbine efficiency ηeff

<<1, and prevented the turbine from rotating fast.

Figure 5.8 Simulated speed of dental drill turbine

Figure 5.9 contains vibration signals from plain and step gas bearings (not from

rotor), measured by capacitance sensor with 25nm resolution. For step bearing19, 2.3 mg

rotor appeared unstable, causing large vibration at the bearing. The amplitude of the

vibration for plain gas bearing was estimated about 0.3µm. To check whether the plain

gas bearings were operated as gas bearing or dry friction bearing, SEM images were

taken from the bearing operated for 1 hour with repeated start/stops every 5 to 10 minutes.

Figure 5.10 shows such a SEM image on the bearing surface after the test. The picture

shows slight wear at both ends of the bearing during the repeated start/stops.

19 Note the stepped gas bearings in this section are fabricated six stepped gas bearing without axial grooves

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(a) Vibration signal from plain bearing, speed 8890 rpm

(b) Vibration signal from step bearing

Figure 5.9 Vibration signal from bearings with 2.3mg rotor; (a) Vibration

signal from plain bearing, speed 8890 rpm (b) Vibration signal from step bearing

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Figure 5.10 SEM images after operation for 1 hour with repeated start/stops

every 5 to 10 minutes

Tables 5.1 and 5.2 show simulated load capacities and threshold rotor masses of

plain and stepped micro gas bearings at low speed ranges. The table predicts the plain gas

bearing to be stable with 2.3mg rotor, if operated at eccentricity above 0.5. From the

simulated results and visual inspection of the tested gas journal bearings, the plain micro

gas journal bearings appeared to have been operated at gas bearing mode. When two

nozzles are used (to minimize radial force to the bearings), bearing load becomes ideally

zero, leading to low eccentricity and high vulnerability of instability, from basic gas

bearing theory. However, from the test, the plain gas bearing was considered to be stable.

Possible reasons include remnant imbalance force of the SU-8 micro turbine or

unbalanced air jet force (probably due to different air jet speeds of two nozzles, slightly

different distance of nozzle center from bearing center, etc).

To improve turbine performance, a simple shroud was machined as in Figure 5.11.

The radius of the shroud was 1.7mm, rendering about 50µm clearance between the

turbine blades and shroud housing. Only one nozzle was used to preload bearings. One

side was an air input and the other side was connected to vacuum. The arrow in Figure

5.11(b) indicates the direction of air jet flow through the shroud. Top of the turbine was

not covered with shroud to measure the speed and bearing vibration. Supply pressure was

35 psi, identical to the pressure at previous tests, with air jet speeds of 223.7m/s. Air jet

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108

speed was measured by strain gauge signals attached to a slender cantilever20, onto which

air jet momentum was directly applied. With the simple shroud, turbine speed increased

to 60,000 rpm as in Figure 5.12, indicating that the open air jet caused very poor turbine

performance, preventing fast rotation.

Table 5.1 Load capacity and threshold rotor mass of plain micro gas bearings

Threshold rotor mass (mg) Load capacity (mg)

RPM e=0.5 e=0.6 e=0.7 e=0.8 ε=0.5 ε=0.6 ε=0.7 ε=0.8

5,266 9.8 19.9 62.4 175.6 4.3 6.0 8.3 12.2

7,899 10.1 20.9 65.6 180.2 6.5 9.0 12.5 18.4

10,532 10.5 22.1 70.5 190.3 8.8 12.0 16.8 24.5

13,165 11.2 23.2 77.3 200.5 11.0 15.1 21.0 30.7

26,329 12.3 25.7 81.1 214.5 22.6 31.1 43.7 65.0

Table 5.2 Load capacity and threshold rotor mass of stepped micro gas bearings

Threshold rotor mass (mg) Load capacity (mg)

RPM ε=0.5 ε=0.6 ε=0.7 ε=0.8 ε=0.5 ε=0.6 ε=0.7 ε=0.8

5,266 0.28 0.58 1.6 3.3 0.6 0.8 1.2 1.8

7,899 0.3 0.62 1.8 3.7 0.9 1.3 1.8 2.8

10,532 0.35 0.75 1.9 4.2 1.3 1.7 2.5 3.8

13,165 0.38 0.82 2 4.5 1.6 2.2 3.1 4.8

26,329 0.4 0.9 2.1 4.7 3.3 4.5 6.4 10.2

20 For the cantilever, 2.4mm wide, 0.2mm thick, 45mm long stainless steel sheet was used.

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109

(a) Shroud

(b) Enlarged image of circled region in (a)

(c) Photo of assembled new gas bearing tester

Figure 5.11 New gas bearing tester with machined shroud to drive micro turbine; (a) Shroud (b) Enlarged image of circled region in (a) (c) Photo of

assembled new gas bearing tester

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110

From the turbine model, equations (5.1) to (5.5), preload by single air jet was

estimated as 7.4mg in horizontal direction. Using combined load of rotor mass and the

preload, orbit simulation were performed with imbalance radius of 5µm, as shown in

Figure 5.13. The imbalance radius was estimated from the accuracy (5µm) of stepper,

which fabricated the mask pattern for the SU-8 turbine. As seen from the orbit simulation,

tested plain gas bearing was predicted stable. The SEM image of bearing surface, shown

in Figure 5.14, after test for 1 hour with frequent start/stops every 5 to 10 minutes,

confirms the gas bearing operation. Slight scratch during the start/stops was observed on

the bearing surface.

Figure 5.12 Photonic sensor signal measuring rotor speeds with new gas bearing

tester shown in Figure 5.11, supply pressure 35psi, plain gas bearing

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111

Figure 5.13 Simulated orbit of 2.3mg rotor supported by plain gas bearing at 60,000

rpm with combined load of rotor mass and preload (7.4mg)

Figure 5.14 SEM image of plain gas bearing surface after test with new test rig shown in Figure 5.11

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Chapter 6

Tribological Study of Micro Bearings

In this chapter, tribological characteristics of tungsten containing hydrocarbon

(W-C:H) coated micro sleeve bearings are discussed and compared with uncoated Ni

micro bearings.

6.1 Introduction Micro gas bearings are ideal for micro rotating machinery. Nevertheless, wide

application of the micro gas bearings in micro systems is limited, due to the following

reasons: high rotational speed is required to ensure sufficient load capacity; aligning the

bearing with the rotor is difficult; extensive engineering is needed to design proper rotor-

bearing configuration, to guarantee stable operation; the gas bearings are vulnerable to

dust particles, and need a clean environment; and wear during repeated start-stop and/or

unexpected touch down onto bearing surface increases bearing clearance, leading to

smaller load capacity and changing bearing characteristics. Even with negligible friction

at normal operating conditions, initial high static friction can be problematic when the

actuator lacks enough power to overcome the static friction.

Dry friction bearings with very low friction and high wear resistance can be

alternatives to gas bearings, due to easy of use and assembly. As discussed in Chapter 1,

surface modification can reduce static friction and surface energies of sliding surfaces.

Nickel micro sleeve bearings, shown in Figure 6.1 with nominal inner diameters

ranging from 500µm to 506µm, and length of 300µm, were fabricated via the X-ray

lithography and electroplating processes introduced in Chapter 2. A uniform 900nm thick

W-C:H was coated on the bearing surfaces using an ICP assisted, hybrid CVD/PVD tool.

Mechanical properties of these coating were studied via nano indentation. Hydrocarbon

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113

containing metal showed better adhesion [Meng, 2003] to metal surfaces than a-C:H, i.e.,

amorphous hydro carbon.

Very light loads usually characterize working conditions of MEMS surfaces.

Therefore, studies on tribological characteristics of MEMS surface employed AFM or

Surface Force Apparatus (SFA) to simulate a single asperity contact under very light load

[Lu and Komvopoulos, 2001; Schwarz et al, 1997; Enachescu et al, 1998]. Typical nano

tribological studies using AFM had contact load of 10~100µN, sliding speed of ~µm/s,

and tip radius of 20~100nm.

However, as discussed in detail in Chapter 1, tip radius, surface energy, and

scanning speed-dependent behavior of friction forces makes comparison of measured

nano scale friction coefficients, to friction coefficients measured by other methods,

difficult, especially if the test environment and tip radius are not known exactly, or the tip

is not perfectly spherical.

(a) Photograph of micro sleeve bearings (b) SEM image of Ni micro bearing

Figure 6.1 Ni micro bearing: (a) Photograph of micro sleeve bearings, (b)

SEM image of Ni micro bearings

Surfaces of micro mechanical systems possess multiple nano meter scales

asperities and follow fractal geometry characterized by self-affinity over a wide range of

length scales [Ling, 1990]. Even if the load is very small and the macroscopic contact

pressure is far below the elastic limit of the materials, some local asperities will

plastically deform because of concentrated loads on those spots. Wear can be induced,

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114

even under extremely small load, which complicates investigation of frictional behavior

of actual MEMS surface, and makes estimating real friction from nano scale friction via

AFM difficult.

Despite promising tribological characteristics and proven performance of DLC in

macro scale applications, direct application to MEMS have been limited. Beerschwinger

et al [Beerschwinger et al, 1995] measured friction of DLC coatings on flat silicon

surfaces, via a surface micro machined small friction tester. Bandorf et al [Bandorf et al,

2003] showed that DLC on a soft polymer surface had better wear resistance than DLC

on silicon wafer. Mousinho et al [Mousinho et al, 2003] demonstrated microstructures

made with DLC film, deposited by RF magnetron sputtering. Cao et al [Cao et al, 2003]

coated Ti-containing DLC (Ti-C:H) on Ni micro mold insert, fabricated by X-ray

lithography and electroplating. However, applications of DLC coatings to the sidewall of

micro scale mechanical parts, that experience sliding contacts (bearings, gears, etc), have

not been reported.

Working surfaces of these micro bearings were characterized using a newly

designed micro tribo tester. Wear rates, mechanical and material properties, and other

tribological characteristics of W-C:H coated Ni micro bearings are presented and

compared to uncoated Ni micro bearings.

Electroplated Ni has unique sidewall characteristics and mechanical properties,

compared to bulk Ni, as shown in Figure 6.2. The yield stress and ultimate tensile

strength of a nickel sample, deposited via the identical process conditions as the Ni

bearings of this work, were 360MPa and 535MPa, respectively [Hemker et al, 2001; Cho

et al, 2003]. After annealing the electroplated Ni at 800oC for 1 hour, the yield stress and

ultimate tensile strength reduced to 180MPa and 200MPa, respectively [Hemker et al,

2001; Cho et al, 2003]. The microstructure of as-deposited Ni had a columnar grain

structure with 2~4µm size, but the grain size increased to about 24µm with an equitaxial

direction after annealing [Hemker et al, 2001; Cho et al, 2003].

Tribological characteristics of annealed Ni micro bearings are important because

of potential high temperature applications. Because the microstructures and mechanical

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115

properties changed after annealing, the tribological characteristics of annealed Ni micro

bearings should differ from as-deposited Ni bearings. In this work, tribological

characteristics of three micro bearings (as-deposited and annealed Ni micro bearings,

tungsten hydrocarbon coated micro bearings) were investigated via a new micro tribo

tester.

800oC 1hr

Grain size 2~4 µm (columnar)

Grain size ~ 24µm (equitaxial)

As-deposited Annealed

Figure 6.2 Microstructure of sidewall of electroplated Ni, as deposited and annealed

[Hemker et al, 2001; Cho et al, 2003]

6.2 Coating Process of W-C:H on Micro Sleeve bearings To deposit a conformal W-C:H coating on the bearing inner surfaces, multiple

bearings were fixed within the holes of two thin stainless steel sheets, as depicted in

Figure 6.3. The stainless steel sheets were Ni plated, in a Ni sulfamate solution, to

prevent cross contamination during coating. The entire assembly with bearings was

placed in a plasma deposition chamber. Plasma reached both sides of the bearing

surfaces.

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116

plasma species

plasma species

plasma species

plasma species

(a) 1mm thick stainless steel sheet (b) Conformal coating process

with holes to hold micro bearings of bearing surfaces

Figure 6.3 Fixture to coat W-C:H coatings on the micro bearings: (a) 1mm thick stainless steel sheet with holes to hold micro bearings (b) Conformal coating process

of bearing surfaces

6.2.1 Process conditions of W-C:H coatings The deposition of W-C:H thin films on the bearings was carried out in an ICP

assisted, hybrid CVD)/PVD tool, with a base pressure ~ 4.7×10−6 Pa. Details are given in

reference [Shi et al, 2000; Meng et al, 2000]. The sequences of the deposition are: 10

minutes etching in a 0.23 Pa Ar (99.999+%) plasma with 1000 W total ICP input power;

pure tungsten interlayer deposition in the PVD mode for 10 minutes, wherein two

magnetron sources sputtered two pure W cathodes (99.99+%); and W-C:H deposition in

the hybrid mode for 41 minutes, with the same W cathodes in an Ar/C2H2 ICP plasma at

a fixed flow rate ratio (10:1) of Ar/C2H2(99.99+%), to achieve a coating thickness of

about 1µm.

During the pure W interlayer, the tungsten cathode current was fixed at 0.5A. W-

C:H was deposited at the tungsten cathode current of 0.15A for the first series of micro

bearings, and 0.1A for the second series of micro bearings. The total ICP power and total

pressure were 1000W and ~0.23 Pa, respectively. The bias voltage applied to the bearing

was fixed at -100V during etching, and -50V during the interlayer and W-C:H

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117

depositions. No intentional heating was applied to the bearing during the deposition.

Figure 6.4 is a photograph of W-C:H coated micro bearings

Figure 6.4 Photo of W-C:H coated micro bearings

6.2.2 Material Properties of W-C:H Coatings

Shown in Table 6.1 are X-ray Photoelectron Spectroscopy (XPS) analysis results

of the chemical compositions of the coatings and mechanical properties. In-plane

Young’s modulus E/(1-ν2) and hardness H of the W-C:H coatings deposited on the

silicon wafer were measured by nano indentation using Digital Instrument Dimension

3100 AFM. Indentation depth was carefully controlled to minimize the substrate effect.

The in-plane Young’s modulus was used to calculate contact pressure during the wear

test.

Table 6.1 Chemical composition and mechanical properties of 900nm thick W-C:H coating

Coating name

Chemical composition (W/C ratio)

W current Hardness H

In-plane Young’s modulus E/(1-ν2)

W-DLC1 11/89 0.15A 8.4 GPa 99 GPa W-DLC2 5/95 0.1A 11 GPa 68 GPa

Figure 6.5 shows a Raman spectrum of a new W-C:H coating, measured with a

Renishaw Micro Raman Microscope with 784nm He-Cd Diode Laser source and input

power 30W. Exposure time was 30 sec, to maximize signal to noise ratio. The diamond to

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118

graphite phase intensity ratios for the two coatings were almost identical at 1.17, because

the flow rate ratio of Ar/C2H2 was the same for the two coatings. The microstructure of

the coating appears to be amorphous from the Raman spectrum. The SEM photos of

Figure 6.6 suggest that uniform conformal coatings with thickness of about 900nm were

achieved by the coating method of Figure 6.3. The SEM image of W-DLC2 coated micro

bearing is shown in Figure 6.7.

Figure 6.5 Raman spectrum of new W-C:H

Figure 6.6 900 nm thick uniform coating thickness on the bearing surface

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119

(a) Low magnification SEM image of W-DLC2 coated surface

(b) High magnification SEM image of W-DLC2 coated surface (×40K)

Figure 6.7 SEM images of W-DLC2 coated bearing surface: (a) Low magnification SEM image of W-DLC2 coated surface (b) High magnification SEM image of W-

DLC2 coated surface (×40K)

6.3 Micro Tribo Tester

Micro bearings made via X-ray lithography have sidewalls with non-symmetrical

fractal geometry. These sidewalls as working surfaces may experience very low contact

pressure during operation. Direct characterization of the sidewall (as-made & coated)

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120

appears to be the best way to assess the microscopic tribological characteristics (and

performance) of the micro bearings. A new micro tribo tester was developed to measure

friction and wear characteristics of the as-made, annealed and coated micro bearings

A miniature impulse turbine with 5mm diameter and 2mm thickness was

fabricated by stacking (on the same shaft) four separate 0.5mm thick electroplated Ni

turbines. SU-8 2100 from MicroChem, Inc., was a photo resist used for plating mold for

0.5mm thick Ni turbines. A micro nozzle with cross section of 0.2mm height and 1.8mm

width and pressurized air at 50 psi drove the turbine. A gauge pin of diameter 500µm

(±0.25µm) composed of SAE 52100 bearing steel (1% C, 1.5% Cr, 0.1% Si) with surface

roughness Ra 50nm served as a driving shaft. Figure 6.8 shows the wear tester for the

micro bearings. The turbine was assembled onto the shaft using epoxy. Two micro

bearings (identical to the test bearings) supported the rotor. Air jetting from the nozzle

applied torque to the turbine. The air jetting also applied an external force to the bearings,

which was measured via the strain gauge attached at the bottom of the cantilever. A

photonic sensor measured the rotational speed stroboscopically.

Maximum Hertzian contact pressure Pmax between the bearing and shaft is given

by [Johnson, 1985] 5.0

max 488.0

=

LRKF

Pe

e (6.1a)

CR

RRRR

R B

SB

SBe

2

≅−

= (6.1b)

122 1134

−+

−=

S

S

B

B

EEK

νν (6.1c)

Here L is the length of the bearing, RB and RS are radii of the bearing and shaft,

respectively, Re is equivalent radius, K is equivalent elastic modulus and C is the

clearance between the bearing and shaft.

Figure 6.9 shows the micro friction tester. An air driven dental drill drove a test

shaft. Two W-C:H coated micro bearings supported the test shaft, to permit ultra-

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121

precision operation. The friction tester consisted of precision and non-precision parts. A

flexible rubber tube coupled the dental drill to the precision test shaft. The coupling

isolated radial vibrations from the dental drill. Moving the stage deflected the cantilever

(Figure 6.9a), which applied and controlled the external load to the test bearings. This

load was measured via a strain gauge attached to the cantilever. The bearing holder with

the test bearing was connected to the cantilever by a flexible cotton string (Figure 6.9b).

The configuration is similar to a macro scale pin-on disc machine. Here the circular steel

shaft and bearing, which replaced the pin and disc, simulated extremely small contact

stress.

Cantilever sensor tomeasure bearing force directly

Strain gauge

Air nozzle Test bearing Micro turbine

Counter shaft: SAE 52100 bearing steel Diameter=500µm; Ra=50nm

(a) Overview of micro wear tester Detailed view within dotted circle in (a)

(b) Photo of micro wear tester

Figure 6.8 Micro wear tester: (a) Overview, (b) Detailed view within dotted circle in

(a), (c) Photo of micro wear tester

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Capacitance probe

Test bearing Dental drill

turbine Rubber tube

Micro Bearing

Moving stage

Strain gauge

Precision Non-precision

String

(a) Schematic diagram

L

TF

T

Test bearing with bearing holder

θ

φ

D

Capacitance probe to measure θ

Cantilever

String

(b) Principle of friction measurement (side view)

(c) Photo of friction tester

Figure 6.9 Micro friction tester: (a) Schematic diagram, (b) Principle of friction

measurement (side view), (c) Photo of friction tester

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123

The kinetic friction coefficient µk of the bearing surface can be calculated from

the static equilibrium (see Figure 6.9b) between friction torque TF and the restoring

torque TR from the external force T,

RTTTLT kFR µφθ ===+ )sin( (6.2)

Giving

RL

k)sin( φθµ +

= (6.3)

In the foregoing, R is the radius of the test bearing (250µm), and deflection angle θ of the

bearing from the vertical (Figure 6.9b) was calculated by measuring the displacement of

the end of the horizontal bar, attached to the bearing holder, via the capacitance probe.

The capacitance probe was calibrated with a micrometer, to compensate errors due to its

non-perpendicular facing with the horizontal bar. The angle φ (Figure 6.9b) was

calculated by trigonometry after θ was measured.

6.4 Results and Discussions

6.4.1 Nickel Bearings

The elastic modulus of electroplated Ni under the plating conditions described

earlier was 163±14GPa [Hemker et al, 2001; Cho et al, 2003]. From this, the equivalent

elastic modulus K=134.5GPa, via equation (6.1c) and material properties of the bearing

and shaft. The initial clearances between the test bearing and shaft was1µm. Bearings

were tested for 1hour, and diameters were measured using SEM. The shapes of the

bearings after the test were not circular, and the diameters in the vertical and horizontal

direction were averaged to calculate wear volume. The wear rates, averaged from four

test bearings, are summarized in Table 6.2. Because of slightly different assembly

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124

conditions of the wear tester for each test (i.e., location of nozzle relative to the turbine),

the load and speed were slightly different for each test.

The annealed Ni bearings had about three-fold higher wear rate than as-deposited

Ni bearings, likely due to smaller yield stress and ultimate tensile strength after

annealing.

Figure 6.10 and 6.11 show the bearing surfaces of as-deposited and annealed Ni

bearings after testing. The lower images magnify the enclosed rectangular frame. Worn

materials were transferred along the axial direction, by axial movements of the turbine

rotor within the clearances between the bearings and turbine. There materials

accumulated on the thrust surfaces. Electroplated Ni bearings were soft, and suffered

severe plastic deformation presumably due to high impacts of the turbine rotor on to the

bearing surface. Even if the initial bearing clearance was 1µm, high impact load could be

expected because of looser clearances caused by rapid wear of the Ni bearings. Figure

6.12 shows SEM images of steel shafts, tested against the as-deposited and annealed Ni

bearings. Both shafts had slight scratching marks without any noticeable wear.

Table 6.2 Wear rates of Ni bearings

Wear rate (×10-3 mm3/Nm)

Bearing load (µN)

Contact pressure (MPa)

Speed (RPM)

As-deposited Ni bearing 0.54~0.96 15500 5.8~29.1 8000~9000

Annealed Ni bearing 1.25~2.98 17250 4.9~27.2 9000~12000

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(a) (b)

Figure 6.10 Wear characteristics of as-deposited Ni bearings: (a) Top view, worn materials moved along the axial direction and accumulated at the thrust surface of

the bearing (b) Inner bearing surface after test

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(a) (b)

Figure 6.11 Wear characteristics of annealed (at 800oC for 1h) Ni bearings: (a) Top view, worn materials moved along the axial direction and accumulated at the thrust surface of the bearing as multiple layers (b) Inner bearing surface after test

(a) (b)

Figure 6.12 SEM images of shaft tested against (a) As-deposited Ni bearing (b) Annealed Ni bearings. No noticeable wear was observed

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127

6.4.2 W-C:H Coated Micro Bearings Contact pressure Pmax of the W-C:H coated bearings, calculated via equations

(6.1), employed the measured in-plane elastic modulus E/(1-ν2) (to estimate K), see Table

6.1. Challenging for the wear test was detection of when the coating was completely

worn, exposing the bare underlying Ni surface to rub against the steel shaft. Due to the

very small bearing size and inaccessibility to surfaces, there was no direct way to monitor

the conditions of the coatings during tests. Unlike Ni micro bearings, the wear tests

monitored rotational speed and shaft vibration every five minutes. Upon a sudden change

of rotational speed, it was assumed that the bearing experienced a sudden change of

coating conditions. Figure 6.13 records rotational speed vs. testing time. Initial turbine

speeds were around 3500 rpm for both bearings. The speed increased slowly until

reaching steady state. Initial slow speed was considered as a break-in period, for typical

hydrocarbon coatings. The turbine speed was steady for certain periods, but increased

suddenly to over 10000 rpm, suggesting a dramatic change of coating conditions. At

these transitions, the coating was considered worn, exposing the underlying Ni surface to

wear. W-DLC1 coated bearing had shorter break-in period, lower steady state RPM, and

reached coating failure earlier than the W-DLC2 coated bearing.

Figure 6.14 shows SEM images of W-C:H coated micro bearings after the wear

test. Here wear of the underlying Ni was assumed to begin after the coating was

completely worn. At this time, the wear tests were stopped. The small particles are stray

epoxy particles that fell off the wear tester when the test bearings were disassembled.

Table 6.3 summarizes the test conditions and the wear rates. The total sliding distance

was estimated from turbine speed, integrated up to the sudden speed increase. The wear

rate of W-DLC2 (high W composition, see Table 6.1) coated micro bearings was about

32% smaller than W-DLC1 (low W composition) coated micro bearings.

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128

Table 6.3 Wear rates of W-C:H coated micro bearings

Coating Wear rate (×10-5 mm3/Nm)

Bearing load (µN)

Contact pressure (MPa)

Speed (RPM)

W-DLC1 1.11~1.43 40461 6.84 3400~10910 W-DLC2 0.75~0.96 44668 6.27 3582~13000

Figure 6.13 RPM-time relation of the W-C:H coated micro bearings

(a) (b)

Figure 6.14 SEM images of W-C:H coated micro bearing surfaces after wear test: (a) W-DLC1 coated micro bearing (b) W-DLC2 coated micro bearing

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129

Direct friction measurements of W-C:H coatings using the micro friction tester

shown in Figure 6.9, were not successful, due to large run outs of the test shaft,

transmitted from dental drill turbine despite flexible rubber coupling. Even very small

shaft vibrations caused severe stick slip and rotational vibration of the bearing holder.

Instead, the turbine was stopped every three minutes and the test shaft was rotated

manually in both clockwise and counter clockwise directions, at slow speed (~5mm/s).

While the test shaft was rotating, deflection angle θ of the bearing holder was measured

via the displacement of the horizontal bar attached to the bearing holder. Figure 6.15 is an

exemplary signal from the capacitance sensor and converted deflection angle θ, in

degrees. Once θ and φ (from trigonometry, Figure 6.9) were measured, the friction

coefficient was calculated using equation (6.3).

Figure 6.16 shows the evolution over time of the friction coefficients of W-C:H

coated micro bearings. From a relatively high initial value, friction coefficient reached at

very low steady state value of about 0.12. Although failure of the rubber coupling

prevented friction measurement over longer periods, a low steady state friction is

suggested by the steady RPM (Figure 6.13), and the Raman spectrum of the wear scar on

the steel test shaft (Figure 6.17), where a transfer layer of W-C:H coating formed. Figure

6.18 is a SEM image of the steel shaft ran against the W-DLC2 coated micro bearing. No

noticeable wear was observed. The shaft tested against the W-DLC1 coated bearing

showed a similar pattern, with no noticeable wear on the shaft.

Low friction of amorphous hydrocarbon coatings at steady state is usually

initiated by a transfer layer formed on the counter surface at very high contact pressure

[Liu et al, 1996; Liu et al, 1997, Donnet et al, 1994; Koskinen et al, 1998]. Even if the

contact pressure is very small during the wear test of the W-C:H coated micro bearings, a

transfer layer formed on the counter surface, leading to low friction and high wear

resistance of both bearing and shaft.

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130

Figure 6.15 Voltage signal from capacitance sensor and converted rotational

angle of horizontal bar attached to bearing holder with W-DLC1 coated bearing

Figure 6.16 Evolution of friction coefficient of W-C:H coated micro bearing

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131

Figure 6.17 Raman spectrum on the wear scar on the steel shaft tested with W-

DLC2 coated bearing

Figure 6.18 SEM images of shaft tested against W-DLC2 coated bearing after 2hour continuous wear test

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132

6.5 Summary and Conclusions of the Experiments

Micro bearings, with and without W-C:H coatings, were introduced and tested. A

deposition process of W-C:H coatings on the micro bearings was developed and

mechanical properties and tribological response of these films were measured. For this, a

micro tribo tester, to directly characterize the sidewall of the micro bearings, was

designed. From this article, the following can be concluded: 1) Ni micro bearings (as

deposited and annealed), without coatings, experienced severe wear and appear

inadequate for tribological applications. 2) Uniform conformal W-C:H coatings, achieved

by the deposition process discussed, proved very efficient tribological coatings for micro

bearings. 3) W-DLC2 (with low W composition) coated micro bearings had higher wear

resistance than W-DLC1 coated micro bearings. 4) During the wear test of the W-C:H

coated micro bearings, a transfer layer formed on the counter steel shaft even under very

small contact pressure, leading to low steady state friction and high wear resistance.

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Chapter 7

Future Work and Conclusions

In this chapter, future research related to this dissertation will be suggested, and

conclusions will be made.

7.1 Future Work This section suggests future research work to improve the micro scale 21 gas

bearings, and experimental methods to characterize gas bearing characteristics and

tribological performance.

7.1.1 Hydrostatic Meso Scale Gas Bearing Figure 7.1 suggests a conceptual design for hydrostatic meso scale gas bearings.

Upper and lower parts can be fabricated separately and fusion bonded together as

suggested in section 4.4.1. Details to form a gas channel are described in Figure 7.2. In

step (a), the negative image of gas channels are formed on a substrate using SU-8, and Cr

(or adhesion layer with good electrical conductivity) is evaporated on the structure to

serve as an electroplating seed layer for later electroplating. A PMMA sheet is bonded on

the structure using PMMA bonding epoxy (see Table 2.2) in step (b). Because negative

images of gas channels have been already formed on the substrate, thick epoxy is

required to avoid damage during bonding. X-ray lithography is performed on PMMA to

make negative image of final bearing part as in step (c), and electroplating and polishing

are followed in step (d), to complete the part as in step (e). Once final part is fabricated,

two identical parts can be stacked or fusion bonded to make a complete hydrostatic meso

scale gas bearings

21 Here, micro scale ranges from sub millimeter to millimeter scale.

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134

7.1.2 Meso Scale Foil Gas Bearing

Foil gas bearings (Figure 7.3) have been known as very stable gas bearings

because foil can accommodate local film thickness variation and minimizes negative

pressure at diverging land, leading to minimum negative cross stiffness [Heshmat, 2000].

Spring alloy Inconel X750® Ni Alloy is widely used to make foils. In Figure 7.3, the foil

should be designed to have highly non-linear stiffness and damping characteristics. Foil

can have non- uniform geometry along axial direction to trap working gas at bearing

center and maximize damping. Despite the high performance, high manufacturing cost

limited their wide application. For meso scale application, manufacturing process of foil

poses additional difficulty. Figure 7.4 suggests fabrication process of micro stamping

mold to process Inconel. In steps (a) and (b), multiple layers consisting micro stamping

mold are processed via X-ray lithography and stacked to make single solid micro

stamping mold as shown in steps (c) and (d). Stamped foils can be wrapped in cylindrical

form and fitted into bearings.

Due to line of sight process of lithography technique, arbitrary circumferential

profile in stamping mold can be processed to tailor stiffness and damping of foil structure.

Changing dimensions of each layer with sub micron resolutions can easily process non-

homogeneous foil structure along axial direction.

Figure 7.1 Conceptual design of hydrostatic meso scale gas bearing

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135

(a) (b) (c)

(d) (e) (f)

Figure 7.2 Detail fabrication processes of hydrostatic meso scale gas bearings; (a) SU-8 pattern with seed layer (b) PMMA bonding (c) X-ray lithography on PMMA

(d) Electroplating (e) Release (f) Final Part

Figure 7.3 Principle of foil gas bearings [Heshmat, 2000]

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136

(a) X-ray lithography (b) Stacking

(c) Solid micro stamping mold (d) Coated micro stamping mold

Figure 7.4 Fabrication process of micro stamping mold for foil; (a) X-ray

lithography (b) Stacking (c) Solid micro stamping mold (d) Coated micro stamping mold

7.1.3 New Software for Performance Analyses of Gas Bearings

Detailed numerical performance analyses are required for optimal design of the

proposed hydrostatic and foil meso scale gas bearings. For the foil gas bearings, new

software should be developed to solve gas lubrication and non-linear elastic deformation

of the foil structure simultaneously.

Due to highly non-linear characteristics of Reynolds Equation (with molecular gas

rarefaction effects) and complicated bearing geometry, orbit method was used in the

dynamic analyses. More time efficient perturbation methods should be developed to

estimate stiffness and damping coefficients of meso scale gas bearings.

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137

In Chapter 4, three-dimensional dynamic analyses were performed for meso scale

applications, such as Laser scanner and HDD spindle. Complete dynamic analyses

including thrust bearings will better predict maximum allowable speed and performance

of the meso scale gas bearings.

7.1.4 Advanced Testing Method of Gas Bearings Difficulties in performance testing of micro scale gas bearings were pointed out in

chapter 5. To facilitate testing and performance investigation, under similar operating

conditions, advanced experimental testing method is suggested.

Figure 7.5 is a turbine-driven gas bearing tester. The shaded part in the right hand

side is a rotor composted of drive shaft, reaction turbine and centrifugal pump. The detail

configuration of reaction turbine and pump are described in Figure 7.6. The reaction

turbine and pump can be built by two-step lithography technique using X-ray or/and UV

lithography. The turbine can be driven with compressed air to test the bearing. The main

purpose of the proposed micro turbine is to measure maximum operating speed and long-

term reliability of the meso scale gas bearings (proposed in section 4.4), meso scale

hydrostatic and foil gas bearings (introduced in sections 7.1.1 and 7.1.2). Another

purpose is to investigate performance of the centrifugal pump as a reliable auxiliary

device, with very low power consumption (through gas bearing), for other types of power

generation system such as thermoelectric power generator and micro fuel cell. Past

research on thermoelectric power generator [Stark and Stordeur, 1999] and/or micro fuel

cell [Hahn et al, 2003] assume the existence of a reliable auxiliary device, with very low

power consumption, to supply pressurized air, hydrogen gas, or hydrocarbon

continuously to main power generation modules such as combustor, electrode-membrane

module, etc. Development of reliable auxiliary devices (with very low power

consumption) is challenging and very important for the micro power generation system to

work as an independent power generation unit.

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138

Turbine nozzle

Pump housing

Gas bearing

Figure 7.5 Gas bearing tester using reaction turbine

(a) Radial impulse turbine (b) Centrifugal pump

Figure 7.6 Auxiliary devices for gas bearing tester in Figure 6.3: (a) Radial impulse

turbine (b) Centrifugal pump

Small size complicates performance testing of the gas bearings. Direct

measurement of states can be very difficult or costly: typically, only one or two states can

be observed with off-the-shelf or even specially developed sensors. This necessitates

models to interpret measured data. Detailed model of rotor dynamics including micro gas

journal bearing and thrust bearing, and simulations will be used to estimate internal states

and parameters that cannot be measured.

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139

7.1.5 Improvement of Micro Tribo Tester Micro wear tester, developed in this work needs further improvement. External

load to the micro bearing and driving speed are determined by single air nozzle. Ideally,

rotational speed and external load to the test bearings should be controlled independently.

Micro electric drive with reliable flexible coupling would be a choice. External loading

can be controlled by air jet independently. Indirect in-situ monitoring technique of

coatings should be employed to decide a moment of coating failure accurately. Viable

techniques would include: monitoring transition of acoustic noise from total system;

monitoring vibration of bearing; measuring rotor run out with specially designed micro

capacitance sensor; combination of the suggested methods, etc.

7.1.6 Tribological Characteristics at Various Environments Limited number of fabricated micro bearings and a shortage of necessary

equipment prohibited further investigation of tribological characteristics of W-C:H

coated micro bearings in various environments, such as dry nitrogen, vacuum and high

temperature. To drive wear tester or friction tester in vacuum, electric drive should be

developed instead of air jet driven turbine.

7.1.7 Other Suggestions

In addition to the proposed future research, the following are suggested.

Statistical investigation on accuracy of dowel pin-based assembly for meso scale gas

bearings: suggested fabrication method of mesocale gas bearings is based on

assumption of exact pattern transfer and repeatability of X-ray lithography process.

However, uncertainties involved in every unit process conditions require statistical

approach to estimate assembly accuracy using dowel pins.

Investigation of tribological characteristics of different solid thin film coatings (such

as CrN, TiN, organic thin films, etc) for other MEMS and biomechanical systems.

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140

Tribological characteristics of thin solid film on soft substrate, such as micro

structures made of SU-8

Improvement of electroplating conditions to minimize micro scale cavity due to

hydrogen reduction and air bubble

7.2 Contributions and Conclusions of Dissertation The purpose of this work was to develop highly reliable micro bearings for micro

rotating machinery. Main contributions and conclusions of this dissertation are

summarized as follows.

1. Reviewed in chapter1 were reliability issues concerning past micro rotating

machinery, and benefits and current research on the micro gas bearings. Various

surface forces arising in MEMS devices, and related failures were introduced,

with their origins. Nano scale friction studies via Atomic Force Microscopy

(AFM), and limitations interpreting results were addressed. Also reviewed were

tribological studies on chemisorbed monolayers for oxide surfaces, and

hydrocarbon (DLC) for macro scale applications.

2. New integrated fabrication process of micro gas journal bearings with thrust

bearings was developed using X-ray lithography and electroplating. In chapter 2,

detailed procedures to make an X-ray mask and other technical issues were

discussed. By precise control and optimization of critical process parameters for

X-ray mask fabrication, a very smooth sidewall (Ra and RMS below 20nm) with

a near perfect vertical sidewall could be achieved. Very long sacrificial layer

etching (for 2 weeks) in diluted HF for final release from substrate, increased

surface roughness dramatically. To achieve a very smooth bearing surface,

sacrificial layer etching time should be minimized.

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141

3. Software to predict hydrodynamic performance of micro gas bearings, including

molecular gas rarefaction effects in sub micron bearing clearances, were

developed. The orbit method, which solves non-linear transient Reynolds

Equation and rotor dynamics in time domain, was very effective for predicting

whirl instability of the micro gas bearings, and for simulating rotor dynamics

under various loading patterns. Chapter 3 and chapter 4 investigated and

summarized hydrodynamic performance of the fabricated micro gas journal, and

thrust bearing, using the software. Fabricated micro gas bearings had lower

stability than plain circular gas bearings due to lower load capacity and poor

system damping characteristics of the original step geometry. Improved bearing

designs having non-symmetrical step geometry with deep axial grooves were

suggested. These bearings were predicted to have much higher load capacities and

dynamic stabilities than the fabricated micro gas bearings.

4. A fabrication process combining X-ray lithography and precision assembly

technique was suggested to make meso scale gas bearings for various

applications. The meso scale gas bearings, applied to Laser scanner and HDD

spindle bearings, were predicted to be very stable over wide operating conditions.

5. A self-aligning assembly technique for micro gas bearings (using capillary action

of photo resist) was developed and proved to be a very effective assembly method

for performance testing of the micro gas bearings. Chapter 5 presented the test

results of the micro gas bearings. Successful operations of micro gas bearings at

60,000 rpm were demonstrated via an air jet-driven turbine under limited

operating conditions. Due to a very small shaft diameter (500µm), employing an

electric drive or a direct formation of an impulse turbine on the shaft, was not a

viable method for the micro gas bearing test. A small micro turbine made of SU-

8, press-fitted onto the shaft, was an alternative.

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142

6. Hybrid CVD/PVD tools with a specially designed bearing holder was very

effective for achieving 900nm thick uniform conformal W-C:H coatings on the

micro bearings. New micro wear and friction testers were designed to characterize

bearing sidewalls directly. Tribological characteristics of as-made Ni micro

bearings, annealed Ni micro bearings, and W-C:H coated micro bearings, were

measured with the micro wear and friction tester. Chapter 6 investigated and

summarized tribological characteristics of Ni micro bearings and amorphous

tungsten hydrocarbon (W-C:H) coated micro bearings in dry friction mode, using

the micro wear and friction tester. Chemical and mechanical microstructures were

studied via X-ray Photoelectron Spectroscopy (XPS), Raman micro spectroscopy

and nano indentation. Wear rates, mechanical and material properties, and other

tribological characteristics of W-C:H coated Ni micro bearings were investigated

and compared to uncoated Ni micro bearings. Uncoated Ni micro bearings, as

deposited and annealed at 800oC, experienced severe wear and appeared

inadequate for tribological applications. Micro bearings with low tungsten-

containing (5% wt) hydrocarbon had higher wear resistance than micro bearings

with high tungsten-containing (11% wt) hydrocarbon. During the wear test of the

W-C:H coated micro bearings, a transfer layer formed on the counter steel shaft

even under very small contact pressure, leading to low steady state friction and

high wear resistance.

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143

Appendix A.

Discretization of the Gas Film Equation

Journal Bearings

i-1,j i+1,j

i,j-1

i,j+1

i,j

i,j-1/2

i-1/2,j

i,j+1/2

∆θ

∆Z

θ

Z

lP SP

i+1/2,j+θQ−

θQ

+ZQ

−ZQ

SQ

Figure A.1 Control volume (Figure 3.3 is repeated)

Performing integral of the left hand side in equation (3.33a), along the control

boundary lP, in Figure A.1, and discretizating of each flux terms using a central

difference scheme, the mass flux term through the each face surrounding control surface

SP in Figure A.1 becomes

( )

( ) ( )

jijiji

jijiji

jijijijijiji

jijiji

jijiji

ji

PDF

PDF

PPDPPF

ZPP

PHQZPP

H

ZPPHQPHQ

,,2/1,2/1

,1,2/1,2/1

,,1,2/1,,1,2/1

,,1,2/1

3P

,,1,2/1

,2/1

3P

22

2

2

++

−=

−−+=

∆∆

−−∆

+Λ=

∂∂

−Λ=

+

+++

+

++++

++

++

+

+

θθ

θ

θ

θ

θ

(A.1a)

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144

( )

( ) ( )

jijiji

jijiji

jijijijijiji

jijiji

jijiji

ji

PDF

PDF

PPDPPF

ZPP

PHQZPP

H

ZPPHQPHQ

,,2/1,2/1

,1,2/1,2/1

,1,,2/1,,1,2/1

,1,,2/1

3P

,,1,2/1

,2/1

3P

22

2

2

−+

+=

−−+=

∆∆

−−∆

+Λ=

∂∂

−Λ=

−−−

−−−−

−−

−−

θθ

θ

θ

θ

θ

(A.1b)

( )

( )jijiZ

ji

jijiji

jiZ

PPD

ZPP

PHQZPPHQQ

,1,2/1,

,1,2/1,

3P

2/1,

3P

−−=

∆∆

−−=∆

∂∂

−=

++

++

+

+ θθ (A.1c)

( )

( )1,,2/1,

1,,2/1,

3P

2/1,

3P

−−

−−

−−=

∆∆

−−=∆

∂∂

−=

jijiZ

ji

jijiji

jiZ

PPD

ZPP

PHQZPPHQQ θθ

(A.1d)

where convection term ZHF jiji ∆Λ= ,, , diffusion term along θ direction,

( )θ

θ

∆∆

=ZPHQD jiji ,

3P, , and diffusion term along Z direction ( )

ZPHQD ji

Zji ∆

∆=

θ,

3P, .

Squeeze term PPS dSPH∫∫∂∂

Λ )(2τ

can be treated as source term Qs and integrated

over the control surface SP to get

( ) ( )[ ]1,,,,

,, 2)(2

)(2

−−∆

∆Λ∆≅∆∆

∆Λ≅

∫∫∂∂

Λ=

nAVjijiAVjiji

AVjiji

PPSs

HPHPZZHP

dSPHQ

τθθ

τ

τ , (A.2)

where 1,

−njiP is the pressure at time grid n-1. Subscript AV denotes the average value.

Applying continuity equation on the control volume in Figure A.1, gives

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145

0=+−+− −+−+sZZ QQQQQ θθ (A.3)

Inserting (A.1) and (A.2) into (A.3), and rearranging gives

0,1,1,1,1,,1,1,1,1,, =−+++++ −−++−−++ jijijijijijijijijijiji bPaPaPaPaPa (A.4)

where

( )

( ) 1,

1,,

2/1,1,

2/1,1,

,2/1,2/1

,1

,2/1,2/1,

,2/1,2/1

,2/1,2/1

,

,2/1,2/1

,1

2

2

222

2

−−

−−

++

−−

−+

−−

++

++

+

∆∆Λ∆

=

−=

−=

−−=

∆∆Λ∆

+++

−−

+=

−=

nji

nAVjiji

Zjiji

Zjiji

jiji

ji

AVjiZ

jiZ

ji

jiji

jiji

ji

jiji

ji

PHZb

Da

Da

DF

a

HZDD

DF

DF

a

DF

a

τθ

τθ

θ

θθ

θ

(A.5)

Using definition of Peclet number Pe [Patankar, 1980] for θ and Z direction, given as

θθ

ji

jiji D

FPe

,

,, = (A.6a)

Zji

jiZji D

FPe

,

,, = (A.6b)

and rearranging (A.5) gives,

Page 165: kimd042.pdf

146

( )

( ) 1,

1,,

2/1,1,

2/1,1,

,2/1,2/1,1

,,2/1,2/11,1,,1,1,

,2/1,2/1,1

2

21

2

21

−−

−−

++

−−−

−+−+−+

+++

∆∆Λ∆

=

−=

−=

+−=

∆∆Λ∆

+−+−−−−=

−−=

nji

nAVjiji

Zjiji

Zjiji

jijiji

AVjijijijijijijiji

jijiji

PHZb

Da

Da

PeDa

HZFFaaaaa

PeDa

τθ

τθ

θθ

θθ

(A.7)

The Scarborough criterion is a sufficient condition for the convergence of the

Gauss-Seidel iteration method:

<≤

=+++∑

=∑ −+−+

equation oneleast at for 1 equations allfor 1

,

1,1,,1j1,i

,

pointsneighber

ji

jijiji

ji a

aaaa

a

a

Patankar [Patankar, 1980] provided the basic rules of convergence of central

difference schemes. For a high bearing number Λ such that 2or ,, >Zjiji PePeθ , a basic

rule that all coefficients must always be positive, is violated. Patankar [Patankar, 1980]

suggested various hybrid convection-diffusion schemes to meet the Scarborough criterion

and to improve numerical stability.

Yum [Yum, 2002] showed the power-law scheme yielded the best stability for

large bearing numbers and coarse grids. Gauss-Seidel iteration method with power-law

scheme was used to get pressure profiles. A more general form of the discretization

equations can be written as

Page 166: kimd042.pdf

147

( )

( )( )[ ]

( ) 1,

1,,,2/1,2/1,

2/1,1,

2/1,1,

,/1,/1,2/1,1

,,2/1,2/1

1,1,,1,1,

,/1,2/1,1

2),0max(

2),0max(

−−−+

−−

++

−−−−

−+

−+−+

+++

∆∆Λ∆

++−=

−=

−=

+−=∆

∆Λ∆+−+

−−−−=

−=

nji

nAVjijijijiji

Zjiji

Zjiji

jsijsijiji

AVjijiji

jijijijiji

jsijiji

PHZPFFb

Da

Da

PePeADa

HZFF

aaaaa

PeADa

τθ

τθ

θθθ

θθ

(A.8)

where ( ) ( )

−≡

5

,, 5.01,0max jiji PePeA and jiP , is the latest value of jiP , in the

iteration.

Thrust Bearing

The same procedures adopted for the journal bearing are applied. Equation

(3.32b) is integrated over the control boundary lP, in Figure A.1, where Z is replaced to η.

( )

( ) ( )

jijiji

jijiji

jijijijijiji

ji

jijiji

jijijiji

ji

PDF

PDF

PPDPPF

PPPHQ

PPH

PPHQPHQ

,,2/1,2/1

,1,2/1,2/1

,,1,2/1,,1,2/1

,2/1

,,1,2/1

3P

,,1,2/1,2/1

,2/1

3P

22

2

2

++

−=

−−+=

∆∆

−−∆

+Λ=

∂∂

−Λ=

+

+++

+

++++

+

++

+++

+

+

θθ

θ

θ

ηθη

ηη

ηθη

η

(A.9a)

Page 167: kimd042.pdf

148

( )

( ) ( )

jijiji

jijiji

jijijijijiji

ji

jijiji

jijijiji

ji

PDF

PDF

PPDPPF

PPPHQ

PPH

PPHQPHQ

,,2/1,2/1

,1,2/1,2/1

,1,,2/1,,1,2/1

,2/1

,1,,2/1

3P

,,1,2/1,2/1

,2/1

3P

22

2

2

−+

+=

−−+=

∆∆

−−∆

+Λ=

∂∂

−Λ=

−−−

−−−−

−−

−−−

θθ

θ

θ

ηθη

ηη

ηθη

η

(A.9b)

( )

( )jijiji

jijiji

ji

PPD

PPPHQPPHQQ

,1,2/1,

,1,2/1,

3P

2/1,

3P

−−=

∆∆

−−=∆

∂∂

−=

++

++

+

+

η

η θη

ηθη

η (A.9c)

( )

( )1,,2/1,

1,,2/1,

3P

2/1,

3P

−−

−−

−−=

∆∆

−−=∆

∂∂

−=

jijiji

jijiji

ji

PPD

PPPHQPPHQQ

η

η θη

ηθη

η (A.9d)

where convection term ηη ∆Λ= jijiji HF ,,, , diffusion term along θ direction,

θη

ηθ

∆∆

=

jiji

PHQD

,

3P

, , and diffusion term along η direction ( )ηθηη

∆∆

= jiji PHQD ,3

P, .

Following the same argument for journal bearings without source term,

0,1,1,1,1,,1,1,1,1,, =−+++++ −−++−−++ jijijijijijijijijijiji bPaPaPaPaPa (A.10)

with

( )

( )[ ]

jijijiji

jiji

jiji

jsijsijiji

jijijijijijiji

jsijiji

PFFb

Da

Da

PePeADa

FFaaaaa

PeADa

,,2/1,2/1,

2/1,1,

2/1,1,

,/1,/1,2/1,1

,2/1,2/11,1,,1,1,

,/1,2/1,1

),0max(

),0max(

−+

−−

++

−−−−

−+−+−+

+++

+−=

−=

−=

+−=

−+−−−−=

−=

η

η

θθθ

θθ

(A.11)

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149

Nomenclatures

Chapter 3

H Local gas film thickness

C Nominal clearance of journal bearing

L Bearing length

D Bearing diameter (=2R)

CT Nominal clearance of thrust bearing

Ri Inner radius of thrust pad

Ro Outer radius of thrust pad

e Journal eccentricity

ε Non-dimensional eccentricity (=e/C)

p Pressure

P Non-dimensional pressure (=p/pa)

pa Atmospheric pressure

U Surface velocity (U=Rω)

ω Angular velocity

µ Viscosity of gas

X, Y, Z Defined in Figure 3.1

x, y, z Defined in Figure 3.1

θ Angular coordinate (=x/R)

Z Non-dimensional axial coordinate (=z/R)

r Radial coordinate in thrust bearing

η Non-dimensional radial coordinate in thrust bearing (=r/R)

l Molecular mean free path of air

lo Molecular mean free path of air in atmospheric pressure

Page 169: kimd042.pdf

150

Kn Knudsen number (=l / h)

Kna Characteristic Knudsen number (=lo / C)

NA Abogadro’s number

d Diameter of gas molecules

T Absolute temperature (K)

us Slip velocity

ζa Knudsen layer thickness

α Surface accommodation coefficient of the wall

PQ Poiseuille flow rate in rarefied gas regions

conQ Poiseuille flow rate in continuum flow regions

PQ Poiseuille flow factor (= PQ / conQ )

Λ Bearing number

σ Squeeze number

H Non-dimensional local gas film thickness (=h/C)

CR Bearing clearance at steps

F Load capacity )( 22YX FF +=

ζ Load parameter )( 22YX ζζ +=

φ Attitude angle

u Local velocity distribution in x direction

τp Shear stresses by Poiseuille flow in rarefied region

τc Shear stresses by Couette flow in rarefied region

τp,con Shear stresses by continuum Poiseuille flow

τc,con Shear stresses by continuum Couette flow

Wp Shear stress factor for Poiseuille flow (=τp/τp,con )

Wc Shear stress factor for Couette flow (=τc/τc,con )

τxy Shear stress at wall of journal shaft

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151

TF Friction torque of journal bearing

βJ Non-dimensional rotational friction factor of journal bearing

rm& Mass flux along r direction

θm& Mass flux along θ direction

FT Load carrying capacity of thrust bearing

ζT Load parameter of thrust bearing

TFT Friction torque of thrust bearing

βT Non-dimensional rotational friction factor of thrust bearing

τθz Shear stress at wall of journal shaft

uθ Local velocity distribution in θ direction

∇k Gradient operators (k=J for journal bearing, k=T for thrust bearing)

ki Unit vectors along the θ, Z, and η directions ),,( ηθ Zk =

SP Control surface

lP Line surrounding control surface SP

θs Angle of one recess

sh

Specific film thickness

σs RMS surface roughness of shaft

σb RMS surface roughness bearing

θR Location of first recess from the line of eccentricity

Chapter 4

eF Total external load (5.022 )( eYeXe FFF += )

Xk State variables (k=1,2,3,4)

ω* Non-dimensional threshold speed

m* Non-dimensional threshold mass

x,y,z Rotational coordinate attached to rotor center

X,Y,Z Fixed reference frame attached to bearing center

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152

a Imbalance radius

ϕx Misalignment of journal along x

ϕy Misalignment of journal along y

uF Imbalance force

i , j Unit vectors along the -x and -y direction

uM Imbalance moment by imbalance force

zu Location of imbalance mass along the -z direction

G Angular momentum vector of journal

Ω Instantaneous angular rotation vector of journal

ψ Non-dimensional misalignment of journal

ψ0 Initial non-dimensional misalignment of journal

Chapter 5

jetT Torque by air jet

Tw Windage loss

Tb Friction torque at bearings

Fb Friction force at bearings

ηeff Turbine efficiency

ρa Density of air

an Nozzle cross section area

Nb Number of turbine blades

Ab Frontal area of one turbine blade

α Windage loss factor

uj Air jet speed

rj Distance of nozzle from bearing center

ω Rotational speed of turbine (rad/s)

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153

R Radius of sotor shaft

µ Friction coefficient of bearing and rotor shaft pair

WR Rotor weight per bearing

Chapter 6 E Young’s modulus

ν Poissson’s ratio

H Hardness

K Equivalent Young’s modulus

Re Equivalent contact radius

C Clearance of test bearing

RB Radius of bearing

RS Radius of shaft

µk Kinetic friction coefficient of the bearing surface

TF Friction torque

TR Restoring torque

T External force

R Radius of test bearing

θ Deflection angle of test bearing

Appendix A +θQ Flow out of control volume in θ direction

−θQ Flow into control volume in θ direction +ZQ Flow out of control volume in Z direction

−ZQ Flow into control volume in Z direction

jiF , Convection term at grid point (i, j)

Page 173: kimd042.pdf

154

θjiD , Diffusion term along θ direction

ZjiD , Diffusion term along Z direction

Qs Source term integrated over the control surface

Pe Peclet number

Page 174: kimd042.pdf

155

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Tanner, D.M. (2000), “Reliability of Surface Micromachined Micro Electro Mechanical Actuators”, Invited Keynote at the 22nd International Conference in Microelectronics, Nis, Yugoslavia, pp 97-1043 Whitten, K. W., Davis, R. E., Peck, M. L., Stanley, G. G. (2004), General Chemistry, 7th edition, Brooks/Cole-Thomson Learning, pp152-153 Wilde, D. A., San Andres, L. (2003), “Experimental lift off characteristics and the effect of a low friction coating on the startup response of simple gas hybrid bearings for oil-free turbo machinery”, Proceedings of STLE/ASME 2003 Intl. Joint Tribology Conference Oct. 2003, Ponte Vedra, FL, USA Xiao, X., Hu, J., Charych, D. H., Salmeron, M. (1996), “Chain length dependence of the frictional properties of alkylsilane molecules self-assembled on mica studied by atomic force microscopy”, Langmuir, vol.12, pp 235-237 Yasuda, H., Plasma polymerization, Academic press, 1985 Yum, K. (2002), Numerical simulation of micro air-lubricated journal bearings for 3-D micro actuators, MS Thesis, Mechanical Engineering, UT-Austin Zhu, X., San Andres, L. (2004), “Rotordynamic Performance of flexure pivot hydrostatic gas bearings for oil-free turbomachinery”, Proceedings of ASME Turbo Expo 2004 Power for Land, Sea and Air, June 14-17, Vienna, Austria

Page 181: kimd042.pdf

162

Vita

Daejong Kim was born in Puan, Korea, on December 02, 1969. He earned his Bachelor

of Science and Master of Science degree in Mechanical Design and Production

Engineering at the Seoul National University in 1991 and 1993, respectively. He entered

doctoral program in Mechanical Engineering at the University of Texas at Austin in

2000.

Permanent address: 1161 DeokLim-Ri, Jusan-Myun, Puan-Kun, Jeonbuk, 579-920,

Korea

This dissertation was typed by author.


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