Lead in Drinking Water Testing Report Jefferson Jr. High ...

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ENVIRONMENTAL

GEOTECHNICAL

MATERIALS

FORENSICS

Lead in Drinking Water Testing Report Jefferson Jr. High School 1200 W. 26th St. Minneapolis, MN 55405

AET Project No. 03-06427

Date:

January 27, 2017

Prepared for:

Minneapolis Public Schools Capital Planning and Project Development (CPPD) 1250 West Broadway 4th Floor North Building Minneapolis, MN 55411

550 Cleveland Avenue North St. Paul, MN 55114Phone 651-659-9001 Toll Free 800-972-6364 Fax 651-659-1379 www.amengtest.com AA/EEO

This document shall not be reproduced, except in full, without written approval from American Engineering Testing, Inc.

CONSULTANTS

ENVIRONMENTAL

GEOTECHNICAL

MATERIALS

FORENSICS

January 27, 2017

Minneapolis Public Schools Capital Planning and Project Development (CPPD) 1250 West Broadway 4th Floor North Building Minneapolis, MN 55411

Attn: Ms. Amy Ennen [email protected]

RE: Lead in Drinking Water Assessment Report Jefferson Jr. High School 1200 W. 26th St. Minneapolis, MN 55405 AET Project No. 03-06427

Dear Ms. Ennen:

American Engineering Testing, Inc. (AET) has completed the Lead in Drinking Water Testing at the Jefferson Jr. High School and the results are presented in the attached report. Our services were conducted on December 22, 2016 and performed according to AET’s Proposal No. 03-06427.

We appreciate your business and the opportunity to have been of service to you. If you have any questions regarding the information in this report or if we can be of additional service, please do not hesitate to contact me.

Sincerely,

Bruce A. Boehm Carlson Senior Environmental Project Manager

Direct: (651) 999-1387 Email: [email protected]

mailto:[email protected]

mailto:[email protected]

Lead in Drinking Water Testing Jefferson Jr. High – Minneapolis, MN January 27, 2017 AET Project No. 03-06427

AMERICAN ENGINEERING TESTING, INC.

TABLE OF CONTENTS

Page

TABLE OF CONTENTS ................................................................................................................. i EXECUTIVE SUMMARY ........................................................................................................... iii 1.0 INTRODUCTION .................................................................................................................... 1

1.1 BACKGROUND................................................................................................................. 1 1.2 SITE DESCRIPTION ......................................................................................................... 2 1.3 SCOPE OF SERVICES ....................................................................................................... 2 1.4 SAMPLING AND ANALYTICAL METHODOLOGIES ................................................. 2 1.5 REGULATORY REQUIREMENTS .................................................................................. 2

2.0 ANALYTICAL RESULTS ...................................................................................................... 3 2.1 LEAD DRINKING WATER SAMPLE RESULTS ............................................................ 3

3.0 CONCLUSIONS....................................................................................................................... 4 4.0 RECOMMENDATIONS .......................................................................................................... 5 5.0 STANDARD OF CARE ........................................................................................................... 6 APPENDICES A. Diagrams for Samples of Concern B. Analytical Results Summary C. Analytical Laboratory Reports and Chain of Custody D. Laboratory Accreditation, Personnel Certifications E. Sampling Methodologies and Analysis F. Supporting Documents

Page i



EXECUTIVE SUMMARY

American Engineering Testing (AET) was authorized by Ms. Amy Ennen, Planning Design Manager for Minneapolis Public Schools (Client), to conduct lead in drinking water testing at the Jefferson Jr. High School located at 1200 W. 26th Street in Minneapolis, Minnesota (the Site). Services were performed according to AET’s Proposal No. 03-06427, dated October 24, 2016. Todd Lewis, Lead Risk Assessor, and Jake Langstaff, Environmental Technician, conducted the lead inspection and testing on December 22, 2016. The purpose for the lead in drinking water testing was to determine lead concentrations in the drinking water throughout the school, determine a potential source(s) for any lead identified in the system, and recommend methods for reducing the lead exposure. This assessment was limited to the faucets and fountains within the school building. AET collected a total of 204 samples, which were broken down between 122 first-draw and 82 second-draw potable drinking water samples. Laboratory analytical results are provided in Appendix C. Based on the analytical results, a concern for lead exposure exists in some faucets/fountains due to first-draw concentrations above the regulated limit of 20 parts per billion (ppb), or 20 micrograms per liter (µg/L). One faucet/fountain is a concern for lead exposure due to a second-draw concentration above the regulated limit of 20 ppb. AET recommends the following corrective actions to be taken to reduce the potential exposure to lead:

• Continue to follow the twice daily Flush Program.

• Remove/replace the faucets/fountains/fixtures for the following locations:

o Sample 9, Cafeteria Kitchen sink faucet with a concentration of 20.1 ppb.

o Sample 15, Community Partners classroom, left sink faucet with a concentration of 52.7 ppb.

o Sample 17, Community Partners classroom, right sink faucet with a concentration of 22.9 ppb.

o Sample 23, Music Room Office bathroom sink with a concentration of 18.1 ppb.

o Sample 25, Music Room Classroom utility sink faucet with a concentration of 84.9 ppb.

o Sample 33, Classroom 116 bathroom sink faucet with a concentration of 20.1 ppb.

o Sample 34, Classroom 116 bathroom pipes leading to the sink (second draw/flush sample) with a concentration of 38.4 ppb.

Page ii



o Sample 53, Room 102 (Main Office) right bathroom sink faucet with a concentration of 19.1 ppb.

o Sample 66, Classroom 138 sink faucet with a concentration of 63.9 ppb.


o Sample 80, Classroom 127 Restroom sink faucet with a concentration of 23.6 ppb.

o Sample 116, Room 204, Media Room sink faucet with a concentration of 66.7 ppb.

o Sample 120, Classroom 208 sink faucet with a concentration of 21 ppb.



o Sample 142, Room 329, Girl’s Restroom handwashing sink faucet with a concentration of 21.1 ppb.

o Sample 144, Classroom 334 middle faucet for the south sink with a concentration of 28 ppb.

o Sample 145, Classroom 334 right faucet for the south sink with a concentration of 25.5 ppb.

• Consider removing/replacing the faucet/fountain/fixture for the following location:

o Sample 54, Hallway Utility Closet Outside Room 102, utility sink faucet with a concentration of 15.5 ppb.

• Consider replacing all faucets/fountains/fixtures throughout the building and the pipes

leading to the bathroom in Classroom 116 to further reduce potential lead in drinking water exposures.

• If any of the above mentioned fixtures are replaced, conduct additional testing following replacement to document and confirm lead in drinking water concentration reduction.

Page iii



1.0 INTRODUCTION

American Engineering Testing (AET) was authorized by Ms. Amy Ennen, Planning Design Manager for Minneapolis Public Schools (Client), to conduct lead in drinking water testing at the Jefferson Jr. High School located at 1200 W. 26th Street in Minneapolis, Minnesota (the Site). Services were performed according to AET’s Proposal No. 03-06427, dated October 24, 2016. Todd Lewis, Lead Risk Assessor, and Jake Langstaff, Environmental Technician, conducted the lead inspection and testing on December 22, 2016. The purpose for the lead in drinking water testing was to determine lead concentrations in the drinking water throughout the school, determine a potential source(s) for any lead identified in the system, and recommend methods for reducing the lead exposure. This assessment was limited to the faucets and fountains within the school building. This report includes analytical results, conclusions, and recommendations. Refer to the Appendices for an introduction to lead, methodologies for lead sampling and analysis, diagrams, laboratory reports, and other supporting documents.

1.1 BACKGROUND

Background information was obtained from an interview and information provided by the Client. Information provided by other parties is assumed accurate unless determined otherwise. The Client provided the last lead in drinking water test results, which were collected by the Minneapolis Environmental Health and Safety and Plumbing Departments on September 26, 1998. They collected samples from 17 locations, following the first-draw protocol, throughout the school and found that 13 of the 17 samples contained lead above the Environmental Protection Agency (EPA) Action Level of 20 parts per billion (ppb). Based on the results they determined that the School needed to remain in the “Flushing Program”, which is an internally developed program, following EPA guidelines, for flushing the drinking water system at the school twice daily in an attempt to reduce lead in drinking water exposures. This program must remain in place until further testing shows a reduction in the first draw lead in drinking water concentrations. At the time of our testing, the Client indicated that they were still following the twice daily flushing program. The Client also indicated that the drinking water system had not been used since the night before, which resulted in the drinking water system being left for a minimum of six hour stagnation, as required by the EPA lead in drinking water sampling guidelines.

Page 1 of 6



1.2 SITE DESCRIPTION

The Jefferson Jr. High School building is a four-story building. AET identified approximately 128 fountains, faucets, and fixtures, which would require sampling and testing as part of this project. 1.3 SCOPE OF SERVICES

AET’s project scope of work includes the following items:

• Collect two water samples at each location; a first draw sample and a flush sample.

• Collect two samples from a faucet, sink or exterior spigot near where the water enters the building to evaluate the lead concentration in the pipe leading from the street to the building.

• Submit the water samples to an accredited laboratory for analyses utilizing appropriate analytical methods.

• Prepare a sample/site diagram.

• Prepare a written report describing our sampling process, outlining the sampling locations, discussing the locations with elevated lead concentrations and identify the source of the contamination based on the analytical results.

1.4 SAMPLING AND ANALYTICAL METHODOLOGIES

Information on sampling methodologies and laboratory analyses are provided in Appendix E. 1.5 REGULATORY REQUIREMENTS

A summary of relevant EPA regulatory requirements are provided in each section. Additional information on lead is available in Appendix F. 1.5.1 Lead in Drinking Water

EPA regulates lead in drinking water in residential buildings and schools. The Occupational Safety and Health Administration (OSHA) or the EPA regulates lead in drinking water in commercial buildings. However, lead in residential potable water sources is used as a guideline in determining if lead in drinking water is acceptable and the basis for recommending corrective actions to reduce lead levels in the drinking water source. EPA recommends lead in residential drinking water be less than 15 ppb or 15 µg/L. In schools, the EPA recommends lead in drinking water to be less than 20 ppb or 20 µg/L. The maximum contaminant level goal (MCLG) is zero. These are the levels determined to be safe by toxicological and biomedical considerations, independent of feasibility.

Page 2 of 6



2.0 ANALYTICAL RESULTS

Analytical results are summarized in this section and in Appendix B. Laboratory reports, analytical results, and chain of custodies are provided in Appendix C. Laboratory accreditation and MN Lead Inspector/Risk Assessor licenses are provided in Appendix D. 2.1 LEAD DRINKING WATER SAMPLE RESULTS

The samples of concern are discussed below. Appendix A contains figures showing the locations of the samples of concern, which are discussed below. The EPA regulates lead levels in school buildings with an Action Level of 20 ppb. Results that exceed 20 ppb require corrective action and results below 20 ppb can be inferred to acceptable based on the EPA regulated limits. However, attention should be paid to samples with results that are approaching 20 ppb as well as to those that exceed 20 ppb. The following first draw samples were found to exceed the EPA Action Level of 20 ppb:

• Sample 9, Cafeteria Kitchen sink faucet with a concentration of 20.1 ppb.

• Sample 15, Community Partners classroom, left sink faucet with a concentration of 52.7 ppb.

• Sample 17, Community Partners classroom, right sink faucet with a concentration of 22.9 ppb.

• Sample 25, Music Room Classroom utility sink faucet with a concentration of 84.9 ppb.

• Sample 33, Classroom 116 bathroom sink faucet with a concentration of 20.1 ppb.

• Sample 66, Classroom 138 sink faucet with a concentration of 63.9 ppb.

• Sample 78, Classroom 128 sink faucet with a concentration of 29.6 ppb.

• Sample 80, Classroom 127 Restroom sink faucet with a concentration of 23.6 ppb.

• Sample 116, Room 204, Media Room sink faucet with a concentration of 66.7 ppb.

• Sample 120, Classroom 208 sink faucet with a concentration of 21 ppb.



• Sample 142, Room 329, Girl’s Restroom handwashing sink faucet with a concentration of 21.1 ppb.

• Sample 144, Classroom 334 middle faucet for the south sink with a concentration of 28 ppb.

Page 3 of 6



• Sample 145, Classroom 334 right faucet for the south sink with a concentration of 25.5 ppb.

The following second draw sample was found to exceed the EPA Action Level of 20 ppb:

• Sample 34, Classroom 116 bathroom pipes leading to the sink (second draw/flush sample) with a concentration of 38.4 ppb.

The following first draw samples were just below the EPA Action Level of 20 ppb and should likely be included as faucets/fixtures that exceed 20 ppb:

• Sample 23, Music Room Office bathroom sink with a concentration of 18.1 ppb.

• Sample 53, Room 102 (Main Office) right bathroom sink faucet with a concentration of 19.1 ppb.

The following sample exceeded the EPA regulated level for residential drinking water, which is 15 ppb. This is a faucet/fixtures that should be evaluated periodically as it is approaching the EPA Action Level of 20 ppb.

• Sample 54, Hallway Utility Closet Outside Room 102, utility sink faucet with a concentration of 15.5 ppb.

Results for samples collected from other sample locations were below the EPA threshold limit of 15.0 ppb. 3.0 CONCLUSIONS

The conclusions in this report are based on information obtained from the Client and the interpretation of the sample results. AET reached the following conclusions:

• The source of the lead, which is causing the elevated lead in drinking water concentrations, appears to be in the fixtures as the samples with results exceeding the EPA Action Level of 20 ppb were all first-draw samples.

• One location, Classroom 166 Bathroom, revealed a source of lead, which is causing the elevated lead in drinking water concentrations, to be in the pipes leading to the bathroom fixture as sample 34, which exceeded the EPA Action Level of 20 ppb, was a second draw/flush sample.

• The samples which exceed 20 ppb appear to be scattered throughout the building.

• All other potable water sources tested below the 15 ppb EPA regulatory level for residential buildings.

Page 4 of 6



4.0 RECOMMENDATIONS

The recommendations provided in this report are limited to available information and the interpretation of the sample results. AET recommends the following:

• Continue to follow the twice daily Flush Program.

• Remove/replace the faucets/fountains/fixtures for the following locations:

o Sample 9, Cafeteria Kitchen sink faucet with a concentration of 20.1 ppb.

o Sample 15, Community Partners classroom, left sink faucet with a concentration of 52.7 ppb.

o Sample 17, Community Partners classroom, right sink faucet with a concentration of 22.9 ppb.

o Sample 23, Music Room Office bathroom sink with a concentration of 18.1 ppb.

o Sample 25, Music Room Classroom utility sink faucet with a concentration of 84.9 ppb.

o Sample 33, Classroom 116 bathroom sink faucet with a concentration of 20.1 ppb.

o Sample 34, Classroom 116 bathroom pipes leading to the sink (second draw/flush sample) with a concentration of 38.4 ppb.

o Sample 53, Room 102 (Main Office) right bathroom sink faucet with a concentration of 19.1 ppb.



o Sample 80, Classroom 127 Restroom sink faucet with a concentration of 23.6 ppb.

o Sample 116, Room 204, Media Room sink faucet with a concentration of 66.7 ppb.




o Sample 142, Room 329, Girl’s Restroom handwashing sink faucet with a concentration of 21.1 ppb.

o Sample 144, Classroom 334 middle faucet for the south sink with a concentration of 28 ppb.

Page 5 of 6



o Sample 145, Classroom 334 right faucet for the south sink with a concentration of25.5 ppb.

• Consider removing/replacing the faucet/fountain/fixture for the following location:

o Sample 54, Hallway Utility Closet Outside Room 102, utility sink faucet with aconcentration of 15.5 ppb.

• Consider replacing all faucets/fountains/fixtures throughout the building and the pipesleading to the bathroom in Classroom 116 to further reduce potential lead in drinkingwater exposures.

• If any of the above mentioned fixtures are replaced, conduct additional testing followingreplacement to document and confirm lead in drinking water concentration reduction.

5.0 STANDARD OF CARE

The Standard of Care for all professional services performed or furnished by AET are at the level and care used ordinarily exercised by members of the profession practicing under similar conditions at the same time, locality, and cost constraints. The results, findings, conclusions, and recommendations expressed in this report are based on conditions observed during the building survey. The information contained in this report is relevant to the date on which this service was performed. AET provides no warranty, expressed or implied, in connection with the services.

If you have questions about this report or would like to discuss the assessment in more detail, please do not hesitate to contact me at 651-999-1387 or at [email protected].

Sincerely, American Engineering Testing, Inc. American Engineering Testing, Inc.

Bruce A. Boehm Carlson Tyler Boley, GIT Senior Environmental Project Manager Geologist

Page 6 of 6

Appendix A Diagrams for Samples of Concern


Figure 1Ground Floor – Sample of Concern Location Diagram

Lead in Drinking Water Testing

Date: 1/23/17 AET Project No.: 03-06427

Jefferson Jr. High School

1200 W. 26th

St.

Minneapolis, MN

Scale: Not to Scale

Legend

### – Sample of Concern

9

15

17

2325

Figure 2First Floor – Sample of Concern Location Diagram




1200 W. 26th

St.

Minneapolis, MN

Scale: Not to Scale

Legend


33,

34

53

54

66

78

80

Figure 3Second Floor – Sample of Concern Location Diagram




1200 W. 26th

St.

Minneapolis, MN

Scale: Not to Scale

Legend


116120122

124

Figure 4Third Floor – Sample of Concern Location Diagram




1200 W. 26th

St.

Minneapolis, MN

Scale: Not to Scale

Legend


142

144,

145

Appendix B Analytical Results Summary


ResultsLab

NumberLocation/Room Draw Fixture

Location Description Room Type Draw Type of Fixture

Plumbing Concern

ug/L (ppb) Limit is 20 ppb

1 M FD S Mechanical Rm. Bathroom first draw sink Fixture 0.21

2 M SD S Mechanical Rm. Mechanical Rm.second draw sink

Street to Building Pipe 0.19

3 B FD S Boiler Rm. Main first draw faucet Fixture 0.86

4 B SD S Boiler Rm. Mainsecond draw faucet

Pipes to Fixture 0.5

5 BW FD F Boiler Rm. Main first draw wash station Fixture 1.5

6 BW SD F Boiler Rm. Mainsecond draw wash station


7 M FD UF Mechanical Rm. Utility Rm. first draw utility faucet Fixture 0.85

8 M SD UF Mechanical Rm. Utility Rm.second draw utility faucet


9 C FD S Cafeteria Main first draw sink Fixture 20.1

10 C SD S Cafeteria Mainsecond draw sink


11 C FD DF Cafeteria Main first drawdrinking fountain Fixture 1.2

12 C SD DF Cafeteria Mainsecond draw

drinking fountain


13 C FD 2S Cafeteria Main first draw second sink Fixture 3.1

14 C SD 2S Cafeteria Mainsecond draw second sink


15 CP FD FLCommunity Partners classroom first draw left faucet Fixture 52.7

16 CP FD FMCommunity Partners classroom first draw middle faucet Fixture 5.4

17 CP FD FRCommunity Partners classroom first draw right faucet Fixture 22.9

Sample Descripton Sample NumberJefferson Jr. High Lead Assessment Data

AET Project No. 03-06427 Page B1 of 16

ResultsLab



Plumbing Concern


Sample Descripton Sample Number

18 CP SD FRCommunity Partners classroom

second draw right faucet


19 CP FD SACommunity Partners bathroom first draw faucet for sink Fixture 2.1

20 MU FD S Music Rm. classroom first draw faucet for sink Fixture 6.121 MU FD SF Music Rm. classroom first draw sink fountain Fixture 2.2

22 MU SD SF Music Rm. classroomsecond draw sink fountain


23 MUO FD SA Music Rm. Office bathroom first draw faucet for sink Fixture 18.1

24 MUO SD SA Music Rm. Office bathroomsecond draw faucet for sink


25 MU FD US Music Rm. classroom first draw utility sink Fixture 84.9

26 MU SD US Music Rm. classroomsecond draw utility sink


27 122 FD SA 122 bathroom first draw faucet for sink Fixture 14.8

28 122 SD SA 122 bathroomsecond draw faucet for sink


29 120 FD S 120 classroom first draw faucet for sink Fixture 4.5

30 120 SD S 120 classroomsecond draw faucet for sink







ResultsLab



Plumbing Concern







Pipes to Fixture 2










43 108 FD S 108 classroom first draw faucet for sink Fixture 15


Pipes to Fixture 1




47 H106 FD DF Outside 106 hallway first drawdrinking fountain Fixture 0.14

48 H106 SD DF Outside 106 hallwaysecond draw

drinking fountain

Pipes to Fixture

None Detect (ND)


ResultsLab



Plumbing Concern






51 102 FD SA 102 (Main Off.) left bathroom first draw faucet for sink Fixture 9.6

52 102 SD SA 102 (Main Off.) left bathroomsecond draw faucet for sink


53 102 FD SB 102 (Main Off.) right bathroom first draw faucet for sink Fixture 19.154 H102 FD US Outside 102 hallway first draw utility sink Fixture 15.5

55 H102 SD US Outside 102 hallwaysecond draw utility sink


56 H102 FD DF Outside 102 hallway first drawdrinking fountain Fixture 0.33

57 H102 SD DF Outside 102 hallwaysecond draw

drinking fountain


58 102C FD S 102C classroom first draw faucet for sink Fixture 5.4

59 102C SD S 102C classroomsecond draw faucet for sink


60 TRH106 FD S Teachers RR bathroom first draw faucet for sink Fixture 0.54

61 TRH106 SD S Teachers RR bathroomsecond draw faucet for sink


62 101 FD S 101 (Health Off.) main first draw faucet for sink Fixture 6.6

63 101 SD S 101 (Health Off.) Mainsecond draw faucet for sink


64 101 FD SA 101 (Health Off.) bathroom first draw faucet for sink Fixture 7.2


ResultsLab



Plumbing Concern



65 101 SD SA 101 (Health Off.) bathroomsecond draw faucet for sink







Pipes to Fixture 2




72 130 FD DF 130 classroom first drawdrinking fountain Fixture 9.7

73 130 SD DF 130 classroomsecond draw

drinking fountain


74 H129 FD DFHallway Outside

129 hallway first drawdrinking fountain Fixture 2.1

75 H129 SD DFHallway Outside

129 hallwaysecond draw

drinking fountain


76 129 FD HWA 129 girls restroom first drawhand washing

station Fixture 0.98

77 129 SD HWA 129 girls restroomsecond draw

hand washing station




ResultsLab



Plumbing Concern





80 127 FD SA 127 classroom w/ rr first draw faucet for sink Fixture 23.6

81 127 SD SA 127 classroom w/ rrsecond draw faucet for sink


82 H127 FD US H127 janitors closet first draw utility sink Fixture 0.55

83 H127 SD US H127 janitors closetsecond draw utility sink

Pipes to Fixture ND

84 123 FD SA 123 classroom w/ rr first draw faucet for sink Fixture 0.41

85 123 SD SA 123 classroom w/ rrsecond draw faucet for sink


86 121 FD HWA 121 boys restroom first drawhand washing

station Fixture 2.6

87 121 SD HWA 121 boys restroomsecond draw



88 H121 FD DF1Hallway Outside

121 hallway

first draw (sample 87 is second draw as these are back to

back)

lower drinking fountain Fixture 0.15


121 hallway


back)

upper drinking fountain Fixture ND

90 H221 FD DF1Hallway Outide

221 hallway first drawlower drinking

fountain Fixture 0.47


ResultsLab



Plumbing Concern



91 H221 FD DF2Hallway Outide

221 hallway first drawupper drinking


92 H221 SD DF1Hallway Outide


lower drinking fountain


93 221 FD HWA 221 room 128


back)

hand washing station Fixture 1.8

94 223 FD SA 223 workroom rr first draw faucet for sink Fixture 1.4

95 223 SD SA 223 workroom rrsecond draw faucet for sink


96A H225 FD USHallway Outside

225 hallway first draw utility sink Fixture 1.5

96B H225 SD USHallway Outside

225 hallwaysecond draw utility sink

Pipes to Fixture ND







99 H229 SD DF2Hallway Outside


upper drinking fountain


100 229 FD HWA 229 girls restroom


back)



ResultsLab



Plumbing Concern



101 228 FD S 228 staff room first draw faucet for sink Fixture 3

102 228 SD S 228 staff roomsecond draw faucet for sink


103 228 FD HWA 228 staff room first drawhand washing

station Fixture 2.5

104 228 SD HWA 228 staff roomsecond draw



105 234 FD S 234 classroom first draw faucet for sink Fixture 0.61106 234 FD SF 234 classroom first draw sink fountain Fixture 0.12













drinking fountain


116 204 FD S 204 media room first draw faucet for sink Fixture 66.7


ResultsLab



Plumbing Concern



117 204 SD S 204 media roomsecond draw faucet for sink


118 H207 FD DFHallway Across

From 207 hallway first drawdrinking fountain Fixture 0.56

119 H207 SD DFHallway Across

From 207 hallwaysecond draw

drinking fountain





















ResultsLab



Plumbing Concern






132 H321 SD DF2Hallway Outside


upper drinking fountain


133 321 FD HWA 321 classroom


back)


134 TRH321 FD S TRH321 teachers rr first draw faucet for sink Fixture 0.57

135 TRH321 SD S TRH321 teachers rrsecond draw faucet for sink









329 hallway first drawdrinking fountain




drinking fountain Fixture 4.1

142 329 FD HWA 329 girls restroom


back) faucet for sink Fixture 21.1


ResultsLab



Plumbing Concern



143 334 FD SSL 334 classroom first drawleft faucet for south sink


144 334 FD SSM 334 classroom first drawmiddle faucet for south sink Fixture 28

145 334 FD SSR 334 classroom first drawright faucet for south sink Fixture 25.5

146 334 FD SNL 334 classroom first drawleft faucet for north sink Fixture 8.4

147 334 FD SNM 334 classroom first drawmiddle faucet for north sink Fixture 9.9

148 334 FD SNR 334 classroom first drawright faucet for north sink Fixture 6.9

149 334 SD SNR 334 classroomsecond draw

right faucet for north sink


150 336 FD SSL 336 classroom first drawleft faucet for south sink


151 336 FD SSM 336 classroom first drawmiddle faucet for south sink Fixture 2.8

152 336 FD SSR 336 classroom first drawright faucet for south sink Fixture 3.2

153 336 FD SNL 336 classroom first drawleft faucet for north sink Fixture 1.3

154 336 FD SNM 336 classroom first drawmiddle faucet for north sink Fixture 0.9

155 336 FD SNR 336 classroom first drawright faucet for north sink Fixture 1.3


ResultsLab



Plumbing Concern



156 336 SD SNR 336 classroomsecond draw

right faucet for north sink


157 302 FD SSWW 302 classroom first drawwest faucet for southwest sink Fixture 0.86

158 302 FD SSWE 302 classroom first draweast faucet for southwest sink Fixture 2

159 302 SD SSWE 302 classroomsecond draw

east faucet for southwest sink


160 302 FD SWW 302 classroom first drawwest faucet for

west sink Fixture 1.9

161 302 FD SWE 302 classroom first draweast faucet for


162 302 SD SWW 302 classroomsecond draw

west faucet for west sink


163 302 FD SNWW 302 classroom first drawwest faucet for northwest sink Fixture 0.98

164 302 FD SNWE 302 classroom first draweast faucet for northwest sink Fixture 2.9


ResultsLab



Plumbing Concern



165 302 SD SNWE 302 classroomsecond draw

east faucet for northwest sink


166 302 FD SSEW 302 classroom first drawwest faucet for southeast sink Fixture 1.1

167 302 FD SSEE 302 classroom first draweast faucet for southeast sink Fixture 1.4

168 302 SD SSEE 302 classroomsecond draw

east faucet for southeast sink


169 302 FD SEW 302 classroom first drawwest faucet for south sink Fixture 1.4

170 302 FD SEE 302 classroom first draweast faucet for south sink Fixture 1.9

171 302 SD SEE 302 classroomsecond draw

east faucet for south sink


172 302 FD SNEW 302 classroom first drawwest faucet for northeast sink Fixture 5.1

173 302 FD SNEE 302 classroom first draweast faucet for northeast sink Fixture 4.1

174 302 SD SNEE 302 classroomsecond draw

east faucet for northeast sink


175 302 FD SE 302 classroom first drawfaucet for east

sink Fixture 0.2


ResultsLab



Plumbing Concern



176 302 SD SE 302 classroomsecond draw

faucet for east sink

Pipes to Fixture ND

177 302 FD SN 302 classroom first drawfaucet for north sink Fixture 1

178 302 SD SN 302 classroomsecond draw

faucet for north sink


179 302 FD SNN 302 classroom first drawnorth faucet for north sink Fixture 2.6

180 302 FD SNS 302 classroom first drawsouth faucet for north sink Fixture 11.9

181 302 SD SNS 302 classroomsecond draw

south faucet for north sink


182 302PREP FD S 302PREP prep room first draw sink Fixture 4.1

183 302PREP SD S 302PREP prep roomsecond draw sink

Pipes to Fixture 1

184 304 FD SNWW 304 classroom first drawwest faucet for northwest sink Fixture 1.6

185 304 FD SNWE 304 classroom first draweast faucet for northwest sink Fixture 1.1

186 304 SD SNWE 304 classroomsecond draw

east faucet for northwest sink


187 304 FD SWW 304 classroom first drawwest faucet for


188 304 FD SWE 304 classroom first draweast faucet for



ResultsLab



Plumbing Concern



189 304 SD SWE 304 classroomsecond draw

east faucet for west sink


190 304 FD SSWW 304 classroom first drawwest faucet for southwest sink Fixture 1.5

191 304 FD SSWE 304 classroom first draweast faucet for southwest sink Fixture 2.3

192 304 SD SSWE 304 classroomsecond draw

east faucet for southwest sink


193 304 FD SEW 304 classroom first drawwest faucet for

east sink Fixture 1.1

194 304 FD SEE 304 classroom first draweast faucet for

east sink Fixture 0.8

195 304 SD SEE 304 classroomsecond draw

east faucet for southeast sink


196 304 FD SSN 304 classroom first drawnorth faucet for south sink Fixture 2.5

197 304 FD SSS 304 classroom first drawsouth faucet for south sink Fixture 1.4

198 304 SD SSS 304 classroomsecond draw

south faucet for south sink


199 304 FD SS 304 classroom first drawfaucet for south sink Fixture 0.36

200 304 SD SS 304 classroomsecond draw

faucet for south sink



ResultsLab



Plumbing Concern



201 304 FD SE 304 classroom first drawfaucet for east

sink Fixture 0.97

202 304 SD SE 304 classroomsecond draw

faucet for east sink




204 H306 SD DFHalway Outside


drinking fountain


A ‐ Bathroom 1HW ‐ Handwashing

B ‐ Bathroom 2

LEGENDFD ‐ First DrawSD ‐ Second Draw/Flush Sample

FM ‐ Faucet MiddleFL ‐ Faucet LeftUS ‐ Utility SinkUF ‐ Utility Faucet (no sink)SA‐ Bathroom Sink

F‐ FountainDF ‐ Drinking FountainM ‐ Mechanical RoomB ‐ Boiler RoomC ‐ CafeteriaCP ‐ Community Partners

FR ‐ Faucet RightS ‐ Sink Faucet


Appendix C Analytical Laboratory Reports and Chain of custody


#=CL#

December 30, 2016

LIMS USE: FR - BRUCE CARLSON

LIMS OBJECT ID: 10374222

10374222

Project:

Pace Project No.:

RE:

Bruce Boehm CarlsonAmerican Engineer Testing550 Cleveland Avenue NorthSaint Paul, MN 55114

03-06427 Jefferson Pb Water

Dear Bruce Carlson:

Enclosed are the analytical results for sample(s) received by the laboratory on December 23, 2016.The results relate only to the samples included in this report. Results reported herein conform to themost current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,where applicable, unless otherwise noted in the body of the report.

If you have any questions concerning this report, please feel free to contact me.

Sincerely,

Kabor Xiong

[email protected]

Project Manager

Enclosures

cc: Todd Lewis, American Engineering Testing

REPORT OF LABORATORY ANALYSIS

This report shall not be reproduced, except in full,

without the written consent of Pace Analytical Services, LLC.

Pace Analytical Services, LLC

1700 Elm Street - Suite 200

Minneapolis, MN 55414

(612)607-1700

Page 1 of 245

AET Project No.03-06427 Page C1 of 245

bboehmcarlson

Reviewed

#=CP#

CERTIFICATIONS

Pace Project No.:

Project:

10374222


Minnesota Certification IDs

1700 Elm Street SE Suite 200, Minneapolis, MN 55414

Alaska Certification UST-107

525 N 8th Street, Salina, KS 67401

A2LA Certification #: 2926.01

Alaska Certification #: UST-078

Alaska Certification #MN00064

Alabama Certification #40770

Arizona Certification #: AZ-0014

Arkansas Certification #: 88-0680

California Certification #: 01155CA

Colorado Certification #Pace

Connecticut Certification #: PH-0256

EPA Region 8 Certification #: 8TMS-L

Florida/NELAP Certification #: E87605

Guam Certification #:14-008r

Georgia Certification #: 959

Georgia EPD #: Pace

Idaho Certification #: MN00064

Hawaii Certification #MN00064

Illinois Certification #: 200011

Indiana Certification#C-MN-01

Iowa Certification #: 368

Kansas Certification #: E-10167

Kentucky Dept of Envi. Protection - DW #90062

Kentucky Dept of Envi. Protection - WW #:90062

Louisiana DEQ Certification #: 3086

Louisiana DHH #: LA140001

Maine Certification #: 2013011

Maryland Certification #: 322

Michigan DEPH Certification #: 9909

Minnesota Certification #: 027-053-137

Mississippi Certification #: Pace

Montana Certification #: MT0092

Nevada Certification #: MN_00064

Nebraska Certification #: Pace

New Jersey Certification #: MN-002

New York Certification #: 11647

North Carolina Certification #: 530

North Carolina State Public Health #: 27700

North Dakota Certification #: R-036

Ohio EPA #: 4150

Ohio VAP Certification #: CL101

Oklahoma Certification #: 9507

Oregon Certification #: MN200001

Oregon Certification #: MN300001

Pennsylvania Certification #: 68-00563

Puerto Rico Certification

Saipan (CNMI) #:MP0003

South Carolina #:74003001

Texas Certification #: T104704192

Tennessee Certification #: 02818

Utah Certification #: MN000642013-4

Virginia DGS Certification #: 251

Virginia/VELAP Certification #: Pace

Washington Certification #: C486

West Virginia Certification #: 382

West Virginia DHHR #:9952C

Wisconsin Certification #: 999407970







(612)607-1700

Page 2 of 245


#=SS#

SAMPLE SUMMARY

Pace Project No.:

Project:

10374222


Lab ID Sample ID Matrix Date Collected Date Received

10374222001 1 Water 12/22/16 00:00 12/23/16 12:15

10374222002 2 Water 12/22/16 00:00 12/23/16 12:15

10374222003 3 Water 12/22/16 00:00 12/23/16 12:15

10374222004 4 Water 12/22/16 00:00 12/23/16 12:15

10374222005 5 Water 12/22/16 00:00 12/23/16 12:15

10374222006 6 Water 12/22/16 00:00 12/23/16 12:15

10374222007 7 Water 12/22/16 00:00 12/23/16 12:15

10374222008 8 Water 12/22/16 00:00 12/23/16 12:15

10374222009 9 Water 12/22/16 00:00 12/23/16 12:15

10374222010 10 Water 12/22/16 00:00 12/23/16 12:15

10374222011 11 Water 12/22/16 00:00 12/23/16 12:15

10374222012 12 Water 12/22/16 00:00 12/23/16 12:15

10374222013 13 Water 12/22/16 00:00 12/23/16 12:15

10374222014 14 Water 12/22/16 00:00 12/23/16 12:15

10374222015 15 Water 12/22/16 00:00 12/23/16 12:15

10374222016 16 Water 12/22/16 00:00 12/23/16 12:15

10374222017 17 Water 12/22/16 00:00 12/23/16 12:15

10374222018 18 Water 12/22/16 00:00 12/23/16 12:15

10374222019 19 Water 12/22/16 00:00 12/23/16 12:15

10374222020 20 Water 12/22/16 00:00 12/23/16 12:15

10374222021 21 Water 12/22/16 00:00 12/23/16 12:15

10374222022 22 Water 12/22/16 00:00 12/23/16 12:15

10374222023 23 Water 12/22/16 00:00 12/23/16 12:15

10374222024 24 Water 12/22/16 00:00 12/23/16 12:15

10374222025 25 Water 12/22/16 00:00 12/23/16 12:15

10374222026 26 Water 12/22/16 00:00 12/23/16 12:15

10374222027 27 Water 12/22/16 00:00 12/23/16 12:15

10374222028 28 Water 12/22/16 00:00 12/23/16 12:15

10374222029 29 Water 12/22/16 00:00 12/23/16 12:15

10374222030 30 Water 12/22/16 00:00 12/23/16 12:15

10374222031 31 Water 12/22/16 00:00 12/23/16 12:15

10374222032 32 Water 12/22/16 00:00 12/23/16 12:15

10374222033 33 Water 12/22/16 00:00 12/23/16 12:15

10374222034 34 Water 12/22/16 00:00 12/23/16 12:15

10374222035 35 Water 12/22/16 00:00 12/23/16 12:15

10374222036 36 Water 12/22/16 00:00 12/23/16 12:15

10374222037 37 Water 12/22/16 00:00 12/23/16 12:15







(612)607-1700

Page 3 of 245


#=SS#

SAMPLE SUMMARY

Pace Project No.:

Project:

10374222



10374222038 38 Water 12/22/16 00:00 12/23/16 12:15

10374222039 39 Water 12/22/16 00:00 12/23/16 12:15

10374222040 40 Water 12/22/16 00:00 12/23/16 12:15

10374222041 41 Water 12/22/16 00:00 12/23/16 12:15

10374222042 42 Water 12/22/16 00:00 12/23/16 12:15

10374222043 43 Water 12/22/16 00:00 12/23/16 12:15

10374222044 44 Water 12/22/16 00:00 12/23/16 12:15

10374222045 45 Water 12/22/16 00:00 12/23/16 12:15

10374222046 46 Water 12/22/16 00:00 12/23/16 12:15

10374222047 47 Water 12/22/16 00:00 12/23/16 12:15

10374222048 48 Water 12/22/16 00:00 12/23/16 12:15

10374222049 49 Water 12/22/16 00:00 12/23/16 12:15

10374222050 50 Water 12/22/16 00:00 12/23/16 12:15

10374222051 51 Water 12/22/16 00:00 12/23/16 12:15

10374222052 52 Water 12/22/16 00:00 12/23/16 12:15

10374222053 53 Water 12/22/16 00:00 12/23/16 12:15

10374222054 54 Water 12/22/16 00:00 12/23/16 12:15

10374222055 55 Water 12/22/16 00:00 12/23/16 12:15

10374222056 56 Water 12/22/16 00:00 12/23/16 12:15

10374222057 57 Water 12/22/16 00:00 12/23/16 12:15

10374222058 58 Water 12/22/16 00:00 12/23/16 12:15

10374222059 59 Water 12/22/16 00:00 12/23/16 12:15

10374222060 60 Water 12/22/16 00:00 12/23/16 12:15

10374222061 61 Water 12/22/16 00:00 12/23/16 12:15

10374222062 62 Water 12/22/16 00:00 12/23/16 12:15

10374222063 63 Water 12/22/16 00:00 12/23/16 12:15

10374222064 64 Water 12/22/16 00:00 12/23/16 12:15

10374222065 65 Water 12/22/16 00:00 12/23/16 12:15

10374222066 66 Water 12/22/16 00:00 12/23/16 12:15

10374222067 67 Water 12/22/16 00:00 12/23/16 12:15

10374222068 68 Water 12/22/16 00:00 12/23/16 12:15

10374222069 69 Water 12/22/16 00:00 12/23/16 12:15

10374222070 70 Water 12/22/16 00:00 12/23/16 12:15

10374222071 71 Water 12/22/16 00:00 12/23/16 12:15

10374222072 72 Water 12/22/16 00:00 12/23/16 12:15

10374222073 73 Water 12/22/16 00:00 12/23/16 12:15

10374222074 74 Water 12/22/16 00:00 12/23/16 12:15







(612)607-1700

Page 4 of 245


#=SS#

SAMPLE SUMMARY

Pace Project No.:

Project:

10374222



10374222075 75 Water 12/22/16 00:00 12/23/16 12:15

10374222076 76 Water 12/22/16 00:00 12/23/16 12:15

10374222077 77 Water 12/22/16 00:00 12/23/16 12:15

10374222078 78 Water 12/22/16 00:00 12/23/16 12:15

10374222079 79 Water 12/22/16 00:00 12/23/16 12:15

10374222080 80 Water 12/22/16 00:00 12/23/16 12:15

10374222081 81 Water 12/22/16 00:00 12/23/16 12:15

10374222082 82 Water 12/22/16 00:00 12/23/16 12:15

10374222083 83 Water 12/22/16 00:00 12/23/16 12:15

10374222084 84 Water 12/22/16 00:00 12/23/16 12:15

10374222085 85 Water 12/22/16 00:00 12/23/16 12:15

10374222086 86 Water 12/22/16 00:00 12/23/16 12:15

10374222087 87 Water 12/22/16 00:00 12/23/16 12:15

10374222088 88 Water 12/22/16 00:00 12/23/16 12:15

10374222089 89 Water 12/22/16 00:00 12/23/16 12:15

10374222090 90 Water 12/22/16 00:00 12/23/16 12:15

10374222091 91 Water 12/22/16 00:00 12/23/16 12:15

10374222092 92 Water 12/22/16 00:00 12/23/16 12:15

10374222093 93 Water 12/22/16 00:00 12/23/16 12:15

10374222094 94 Water 12/22/16 00:00 12/23/16 12:15

10374222095 95 Water 12/22/16 00:00 12/23/16 12:15

10374222096 96 (A) Water 12/22/16 00:00 12/23/16 12:15

10374222097 97 Water 12/22/16 00:00 12/23/16 12:15

10374222098 98 Water 12/22/16 00:00 12/23/16 12:15

10374222099 99 Water 12/22/16 00:00 12/23/16 12:15

10374222100 100 Water 12/22/16 00:00 12/23/16 12:15

10374222101 101 Water 12/22/16 00:00 12/23/16 12:15

10374222102 102 Water 12/22/16 00:00 12/23/16 12:15

10374222103 103 Water 12/22/16 00:00 12/23/16 12:15

10374222104 104 Water 12/22/16 00:00 12/23/16 12:15

10374222105 105 Water 12/22/16 00:00 12/23/16 12:15

10374222106 106 Water 12/22/16 00:00 12/23/16 12:15

10374222107 107 Water 12/22/16 00:00 12/23/16 12:15

10374222108 108 Water 12/22/16 00:00 12/23/16 12:15

10374222109 109 Water 12/22/16 00:00 12/23/16 12:15

10374222110 110 Water 12/22/16 00:00 12/23/16 12:15

10374222111 111 Water 12/22/16 00:00 12/23/16 12:15







(612)607-1700

Page 5 of 245


#=SS#

SAMPLE SUMMARY

Pace Project No.:

Project:

10374222



10374222112 112 Water 12/22/16 00:00 12/23/16 12:15

10374222113 113 Water 12/22/16 00:00 12/23/16 12:15

10374222114 114 Water 12/22/16 00:00 12/23/16 12:15

10374222115 115 Water 12/22/16 00:00 12/23/16 12:15

10374222116 116 Water 12/22/16 00:00 12/23/16 12:15

10374222117 117 Water 12/22/16 00:00 12/23/16 12:15

10374222118 118 Water 12/22/16 00:00 12/23/16 12:15

10374222119 119 Water 12/22/16 00:00 12/23/16 12:15

10374222120 120 Water 12/22/16 00:00 12/23/16 12:15

10374222121 121 Water 12/22/16 00:00 12/23/16 12:15

10374222122 122 Water 12/22/16 00:00 12/23/16 12:15

10374222123 123 Water 12/22/16 00:00 12/23/16 12:15

10374222124 124 Water 12/22/16 00:00 12/23/16 12:15

10374222125 125 Water 12/22/16 00:00 12/23/16 12:15

10374222126 126 Water 12/22/16 00:00 12/23/16 12:15

10374222127 127 Water 12/22/16 00:00 12/23/16 12:15

10374222128 128 Water 12/22/16 00:00 12/23/16 12:15

10374222129 129 Water 12/22/16 00:00 12/23/16 12:15

10374222130 130 Water 12/22/16 00:00 12/23/16 12:15

10374222131 131 Water 12/22/16 00:00 12/23/16 12:15

10374222132 132 Water 12/22/16 00:00 12/23/16 12:15

10374222133 133 Water 12/22/16 00:00 12/23/16 12:15

10374222134 134 Water 12/22/16 00:00 12/23/16 12:15

10374222135 135 Water 12/22/16 00:00 12/23/16 12:15

10374222136 136 Water 12/22/16 00:00 12/23/16 12:15

10374222137 137 Water 12/22/16 00:00 12/23/16 12:15

10374222138 138 Water 12/22/16 00:00 12/23/16 12:15

10374222139 139 Water 12/22/16 00:00 12/23/16 12:15

10374222140 140 Water 12/22/16 00:00 12/23/16 12:15

10374222141 141 Water 12/22/16 00:00 12/23/16 12:15

10374222142 142 Water 12/22/16 00:00 12/23/16 12:15

10374222143 143 Water 12/22/16 00:00 12/23/16 12:15

10374222144 144 Water 12/22/16 00:00 12/23/16 12:15

10374222145 145 Water 12/22/16 00:00 12/23/16 12:15

10374222146 146 Water 12/22/16 00:00 12/23/16 12:15

10374222147 147 Water 12/22/16 00:00 12/23/16 12:15

10374222148 148 Water 12/22/16 00:00 12/23/16 12:15







(612)607-1700

Page 6 of 245


#=SS#

SAMPLE SUMMARY

Pace Project No.:

Project:

10374222



10374222149 149 Water 12/22/16 00:00 12/23/16 12:15

10374222150 150 Water 12/22/16 00:00 12/23/16 12:15

10374222151 151 Water 12/22/16 00:00 12/23/16 12:15

10374222152 152 Water 12/22/16 00:00 12/23/16 12:15

10374222153 153 Water 12/22/16 00:00 12/23/16 12:15

10374222154 154 Water 12/22/16 00:00 12/23/16 12:15

10374222155 155 Water 12/22/16 00:00 12/23/16 12:15

10374222156 156 Water 12/22/16 00:00 12/23/16 12:15

10374222157 157 Water 12/22/16 00:00 12/23/16 12:15

10374222158 158 Water 12/22/16 00:00 12/23/16 12:15

10374222159 159 Water 12/22/16 00:00 12/23/16 12:15

10374222160 160 Water 12/22/16 00:00 12/23/16 12:15

10374222161 161 Water 12/22/16 00:00 12/23/16 12:15

10374222162 162 Water 12/22/16 00:00 12/23/16 12:15

10374222163 163 Water 12/22/16 00:00 12/23/16 12:15

10374222164 164 Water 12/22/16 00:00 12/23/16 12:15

10374222165 165 Water 12/22/16 00:00 12/23/16 12:15

10374222166 166 Water 12/22/16 00:00 12/23/16 12:15

10374222167 167 Water 12/22/16 00:00 12/23/16 12:15

10374222168 168 Water 12/22/16 00:00 12/23/16 12:15

10374222169 169 Water 12/22/16 00:00 12/23/16 12:15

10374222170 170 Water 12/22/16 00:00 12/23/16 12:15

10374222171 171 Water 12/22/16 00:00 12/23/16 12:15

10374222172 172 Water 12/22/16 00:00 12/23/16 12:15

10374222173 173 Water 12/22/16 00:00 12/23/16 12:15

10374222174 174 Water 12/22/16 00:00 12/23/16 12:15

10374222175 175 Water 12/22/16 00:00 12/23/16 12:15

10374222176 176 Water 12/22/16 00:00 12/23/16 12:15

10374222177 177 Water 12/22/16 00:00 12/23/16 12:15

10374222178 178 Water 12/22/16 00:00 12/23/16 12:15

10374222179 179 Water 12/22/16 00:00 12/23/16 12:15

10374222180 180 Water 12/22/16 00:00 12/23/16 12:15

10374222181 181 Water 12/22/16 00:00 12/23/16 12:15

10374222182 182 Water 12/22/16 00:00 12/23/16 12:15

10374222183 183 Water 12/22/16 00:00 12/23/16 12:15

10374222184 184 Water 12/22/16 00:00 12/23/16 12:15

10374222185 185 Water 12/22/16 00:00 12/23/16 12:15







(612)607-1700

Page 7 of 245


#=SS#

SAMPLE SUMMARY

Pace Project No.:

Project:

10374222



10374222186 186 Water 12/22/16 00:00 12/23/16 12:15

10374222187 187 Water 12/22/16 00:00 12/23/16 12:15

10374222188 188 Water 12/22/16 00:00 12/23/16 12:15

10374222189 189 Water 12/22/16 00:00 12/23/16 12:15

10374222190 190 Water 12/22/16 00:00 12/23/16 12:15

10374222191 191 Water 12/22/16 00:00 12/23/16 12:15

10374222192 192 Water 12/22/16 00:00 12/23/16 12:15

10374222193 193 Water 12/22/16 00:00 12/23/16 12:15

10374222194 194 Water 12/22/16 00:00 12/23/16 12:15

10374222195 195 Water 12/22/16 00:00 12/23/16 12:15

10374222196 196 Water 12/22/16 00:00 12/23/16 12:15

10374222197 197 Water 12/22/16 00:00 12/23/16 12:15

10374222198 198 Water 12/22/16 00:00 12/23/16 12:15

10374222199 199 Water 12/22/16 00:00 12/23/16 12:15

10374222200 200 Water 12/22/16 00:00 12/23/16 12:15

10374222201 201 Water 12/22/16 00:00 12/23/16 12:15

10374222202 202 Water 12/22/16 00:00 12/23/16 12:15

10374222203 203 Water 12/22/16 00:00 12/23/16 12:15

10374222204 204 Water 12/22/16 00:00 12/23/16 12:15

10374222205 96(B) Water 12/22/16 00:00 12/23/16 12:15







(612)607-1700

Page 8 of 245


#=SA#

SAMPLE ANALYTE COUNT

Pace Project No.:

Project:

10374222


Lab ID Sample ID Method

Analytes

Reported LaboratoryAnalysts

10374222001 1 EPA 200.8 1 PASI-MTT3

10374222002 2 EPA 200.8 1 PASI-MTT3

10374222003 3 EPA 200.8 1 PASI-MTT3

10374222004 4 EPA 200.8 1 PASI-MTT3

10374222005 5 EPA 200.8 1 PASI-MTT3

10374222006 6 EPA 200.8 1 PASI-MTT3

10374222007 7 EPA 200.8 1 PASI-MTT3

10374222008 8 EPA 200.8 1 PASI-MTT3

10374222009 9 EPA 200.8 1 PASI-MTT3

10374222010 10 EPA 200.8 1 PASI-MTT3

10374222011 11 EPA 200.8 1 PASI-MTT3

10374222012 12 EPA 200.8 1 PASI-MTT3

10374222013 13 EPA 200.8 1 PASI-MTT3

10374222014 14 EPA 200.8 1 PASI-MTT3

10374222015 15 EPA 200.8 1 PASI-MTT3

10374222016 16 EPA 200.8 1 PASI-MTT3

10374222017 17 EPA 200.8 1 PASI-MTT3

10374222018 18 EPA 200.8 1 PASI-MTT3

10374222019 19 EPA 200.8 1 PASI-MTT3

10374222020 20 EPA 200.8 1 PASI-MTT3

10374222021 21 EPA 200.8 1 PASI-MTT3

10374222022 22 EPA 200.8 1 PASI-MTT3

10374222023 23 EPA 200.8 1 PASI-MTT3

10374222024 24 EPA 200.8 1 PASI-MTT3

10374222025 25 EPA 200.8 1 PASI-MTT3

10374222026 26 EPA 200.8 1 PASI-MTT3

10374222027 27 EPA 200.8 1 PASI-MRJS

10374222028 28 EPA 200.8 1 PASI-MTT3

10374222029 29 EPA 200.8 1 PASI-MTT3

10374222030 30 EPA 200.8 1 PASI-MTT3

10374222031 31 EPA 200.8 1 PASI-MTT3

10374222032 32 EPA 200.8 1 PASI-MTT3

10374222033 33 EPA 200.8 1 PASI-MTT3

10374222034 34 EPA 200.8 1 PASI-MTT3

10374222035 35 EPA 200.8 1 PASI-MTT3

10374222036 36 EPA 200.8 1 PASI-MTT3

10374222037 37 EPA 200.8 1 PASI-MTT3







(612)607-1700

Page 9 of 245


#=SA#


Pace Project No.:

Project:

10374222



Analytes


10374222038 38 EPA 200.8 1 PASI-MTT3

10374222039 39 EPA 200.8 1 PASI-MTT3

10374222040 40 EPA 200.8 1 PASI-MTT3

10374222041 41 EPA 200.8 1 PASI-MTT3

10374222042 42 EPA 200.8 1 PASI-MTT3

10374222043 43 EPA 200.8 1 PASI-MTT3

10374222044 44 EPA 200.8 1 PASI-MTT3

10374222045 45 EPA 200.8 1 PASI-MTT3

10374222046 46 EPA 200.8 1 PASI-MTT3

10374222047 47 EPA 200.8 1 PASI-MTT3

10374222048 48 EPA 200.8 1 PASI-MTT3

10374222049 49 EPA 200.8 1 PASI-MTT3

10374222050 50 EPA 200.8 1 PASI-MTT3

10374222051 51 EPA 200.8 1 PASI-MTT3

10374222052 52 EPA 200.8 1 PASI-MTT3

10374222053 53 EPA 200.8 1 PASI-MTT3

10374222054 54 EPA 200.8 1 PASI-MTT3

10374222055 55 EPA 200.8 1 PASI-MTT3

10374222056 56 EPA 200.8 1 PASI-MTT3

10374222057 57 EPA 200.8 1 PASI-MTT3

10374222058 58 EPA 200.8 1 PASI-MTT3

10374222059 59 EPA 200.8 1 PASI-MTT3

10374222060 60 EPA 200.8 1 PASI-MTT3

10374222061 61 EPA 200.8 1 PASI-MTT3

10374222062 62 EPA 200.8 1 PASI-MTT3

10374222063 63 EPA 200.8 1 PASI-MTT3

10374222064 64 EPA 200.8 1 PASI-MTT3

10374222065 65 EPA 200.8 1 PASI-MTT3

10374222066 66 EPA 200.8 1 PASI-MRJS

10374222067 67 EPA 200.8 1 PASI-MTT3

10374222068 68 EPA 200.8 1 PASI-MTT3

10374222069 69 EPA 200.8 1 PASI-MTT3

10374222070 70 EPA 200.8 1 PASI-MTT3

10374222071 71 EPA 200.8 1 PASI-MTT3

10374222072 72 EPA 200.8 1 PASI-MTT3

10374222073 73 EPA 200.8 1 PASI-MTT3

10374222074 74 EPA 200.8 1 PASI-MRJS







(612)607-1700

Page 10 of 245


#=SA#


Pace Project No.:

Project:

10374222



Analytes


10374222075 75 EPA 200.8 1 PASI-MTT3

10374222076 76 EPA 200.8 1 PASI-MTT3

10374222077 77 EPA 200.8 1 PASI-MTT3

10374222078 78 EPA 200.8 1 PASI-MTT3

10374222079 79 EPA 200.8 1 PASI-MTT3

10374222080 80 EPA 200.8 1 PASI-MTT3

10374222081 81 EPA 200.8 1 PASI-MTT3

10374222082 82 EPA 200.8 1 PASI-MTT3

10374222083 83 EPA 200.8 1 PASI-MTT3

10374222084 84 EPA 200.8 1 PASI-MTT3

10374222085 85 EPA 200.8 1 PASI-MTT3

10374222086 86 EPA 200.8 1 PASI-MTT3

10374222087 87 EPA 200.8 1 PASI-MTT3

10374222088 88 EPA 200.8 1 PASI-MTT3

10374222089 89 EPA 200.8 1 PASI-MTT3

10374222090 90 EPA 200.8 1 PASI-MTT3

10374222091 91 EPA 200.8 1 PASI-MTT3

10374222092 92 EPA 200.8 1 PASI-MTT3

10374222093 93 EPA 200.8 1 PASI-MTT3

10374222094 94 EPA 200.8 1 PASI-MTT3

10374222095 95 EPA 200.8 1 PASI-MTT3

10374222096 96 (A) EPA 200.8 1 PASI-MTT3

10374222097 97 EPA 200.8 1 PASI-MTT3

10374222098 98 EPA 200.8 1 PASI-MTT3

10374222099 99 EPA 200.8 1 PASI-MTT3

10374222100 100 EPA 200.8 1 PASI-MTT3

10374222101 101 EPA 200.8 1 PASI-MTT3

10374222102 102 EPA 200.8 1 PASI-MTT3

10374222103 103 EPA 200.8 1 PASI-MTT3

10374222104 104 EPA 200.8 1 PASI-MTT3

10374222105 105 EPA 200.8 1 PASI-MTT3

10374222106 106 EPA 200.8 1 PASI-MTT3

10374222107 107 EPA 200.8 1 PASI-MTT3

10374222108 108 EPA 200.8 1 PASI-MTT3

10374222109 109 EPA 200.8 1 PASI-MTT3

10374222110 110 EPA 200.8 1 PASI-MTT3

10374222111 111 EPA 200.8 1 PASI-MTT3







(612)607-1700

Page 11 of 245


#=SA#


Pace Project No.:

Project:

10374222



Analytes


10374222112 112 EPA 200.8 1 PASI-MTT3

10374222113 113 EPA 200.8 1 PASI-MTT3

10374222114 114 EPA 200.8 1 PASI-MTT3

10374222115 115 EPA 200.8 1 PASI-MTT3

10374222116 116 EPA 200.8 1 PASI-MTT3

10374222117 117 EPA 200.8 1 PASI-MTT3

10374222118 118 EPA 200.8 1 PASI-MTT3

10374222119 119 EPA 200.8 1 PASI-MTT3

10374222120 120 EPA 200.8 1 PASI-MTT3

10374222121 121 EPA 200.8 1 PASI-MRJS

10374222122 122 EPA 200.8 1 PASI-MRJS

10374222123 123 EPA 200.8 1 PASI-MRJS

10374222124 124 EPA 200.8 1 PASI-MRJS

10374222125 125 EPA 200.8 1 PASI-MRJS

10374222126 126 EPA 200.8 1 PASI-MRJS

10374222127 127 EPA 200.8 1 PASI-MRJS

10374222128 128 EPA 200.8 1 PASI-MRJS

10374222129 129 EPA 200.8 1 PASI-MRJS

10374222130 130 EPA 200.8 1 PASI-MRJS

10374222131 131 EPA 200.8 1 PASI-MRJS

10374222132 132 EPA 200.8 1 PASI-MRJS

10374222133 133 EPA 200.8 1 PASI-MRJS

10374222134 134 EPA 200.8 1 PASI-MRJS

10374222135 135 EPA 200.8 1 PASI-MRJS

10374222136 136 EPA 200.8 1 PASI-MRJS

10374222137 137 EPA 200.8 1 PASI-MRJS

10374222138 138 EPA 200.8 1 PASI-MRJS

10374222139 139 EPA 200.8 1 PASI-MRJS

10374222140 140 EPA 200.8 1 PASI-MRJS

10374222141 141 EPA 200.8 1 PASI-MRJS

10374222142 142 EPA 200.8 1 PASI-MRJS

10374222143 143 EPA 200.8 1 PASI-MRJS

10374222144 144 EPA 200.8 1 PASI-MRJS

10374222145 145 EPA 200.8 1 PASI-MRJS

10374222146 146 EPA 200.8 1 PASI-MRJS

10374222147 147 EPA 200.8 1 PASI-MRJS

10374222148 148 EPA 200.8 1 PASI-MRJS







(612)607-1700

Page 12 of 245


#=SA#


Pace Project No.:

Project:

10374222



Analytes


10374222149 149 EPA 200.8 1 PASI-MRJS

10374222150 150 EPA 200.8 1 PASI-MRJS

10374222151 151 EPA 200.8 1 PASI-MRJS

10374222152 152 EPA 200.8 1 PASI-MRJS

10374222153 153 EPA 200.8 1 PASI-MRJS

10374222154 154 EPA 200.8 1 PASI-MRJS

10374222155 155 EPA 200.8 1 PASI-MRJS

10374222156 156 EPA 200.8 1 PASI-MRJS

10374222157 157 EPA 200.8 1 PASI-MRJS

10374222158 158 EPA 200.8 1 PASI-MRJS

10374222159 159 EPA 200.8 1 PASI-MRJS

10374222160 160 EPA 200.8 1 PASI-MRJS

10374222161 161 EPA 200.8 1 PASI-MTT3

10374222162 162 EPA 200.8 1 PASI-MTT3

10374222163 163 EPA 200.8 1 PASI-MTT3

10374222164 164 EPA 200.8 1 PASI-MTT3

10374222165 165 EPA 200.8 1 PASI-MTT3

10374222166 166 EPA 200.8 1 PASI-MTT3

10374222167 167 EPA 200.8 1 PASI-MTT3

10374222168 168 EPA 200.8 1 PASI-MTT3

10374222169 169 EPA 200.8 1 PASI-MTT3

10374222170 170 EPA 200.8 1 PASI-MTT3

10374222171 171 EPA 200.8 1 PASI-MTT3

10374222172 172 EPA 200.8 1 PASI-MTT3

10374222173 173 EPA 200.8 1 PASI-MTT3

10374222174 174 EPA 200.8 1 PASI-MTT3

10374222175 175 EPA 200.8 1 PASI-MTT3

10374222176 176 EPA 200.8 1 PASI-MTT3

10374222177 177 EPA 200.8 1 PASI-MTT3

10374222178 178 EPA 200.8 1 PASI-MTT3

10374222179 179 EPA 200.8 1 PASI-MTT3

10374222180 180 EPA 200.8 1 PASI-MRJS

10374222181 181 EPA 200.8 1 PASI-MTT3

10374222182 182 EPA 200.8 1 PASI-MTT3

10374222183 183 EPA 200.8 1 PASI-MTT3

10374222184 184 EPA 200.8 1 PASI-MTT3

10374222185 185 EPA 200.8 1 PASI-MTT3







(612)607-1700

Page 13 of 245


#=SA#


Pace Project No.:

Project:

10374222



Analytes


10374222186 186 EPA 200.8 1 PASI-MTT3

10374222187 187 EPA 200.8 1 PASI-MTT3

10374222188 188 EPA 200.8 1 PASI-MTT3

10374222189 189 EPA 200.8 1 PASI-MTT3

10374222190 190 EPA 200.8 1 PASI-MTT3

10374222191 191 EPA 200.8 1 PASI-MTT3

10374222192 192 EPA 200.8 1 PASI-MTT3

10374222193 193 EPA 200.8 1 PASI-MTT3

10374222194 194 EPA 200.8 1 PASI-MTT3

10374222195 195 EPA 200.8 1 PASI-MTT3

10374222196 196 EPA 200.8 1 PASI-MTT3

10374222197 197 EPA 200.8 1 PASI-MTT3

10374222198 198 EPA 200.8 1 PASI-MTT3

10374222199 199 EPA 200.8 1 PASI-MTT3

10374222200 200 EPA 200.8 1 PASI-MTT3

10374222201 201 EPA 200.8 1 PASI-MTT3

10374222202 202 EPA 200.8 1 PASI-MTT3

10374222203 203 EPA 200.8 1 PASI-MTT3

10374222204 204 EPA 200.8 1 PASI-MTT3

10374222205 96(B) EPA 200.8 1 PASI-MTT3







(612)607-1700

Page 14 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222


Sample: 1 Lab ID: 10374222001 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water

Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit

Analytical Method: EPA 200.8200.8 MET ICPMS, DW

Lead 0.21 ug/L 12/27/16 14:01 7439-92-10.10 1



without the written consent of Pace Analytical Services, LLC.Date: 12/30/2016 09:19 AM




(612)607-1700

Page 15 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.19 ug/L 12/27/16 14:05 7439-92-10.10 1







(612)607-1700

Page 16 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.86 ug/L 12/27/16 14:06 7439-92-10.10 1







(612)607-1700

Page 17 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.50 ug/L 12/27/16 14:07 7439-92-10.10 1







(612)607-1700

Page 18 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 1.5 ug/L 12/27/16 14:08 7439-92-10.10 1







(612)607-1700

Page 19 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.86 ug/L 12/27/16 14:12 7439-92-10.10 1







(612)607-1700

Page 20 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.85 ug/L 12/27/16 14:13 7439-92-10.10 1







(612)607-1700

Page 21 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.86 ug/L 12/27/16 14:14 7439-92-10.10 1







(612)607-1700

Page 22 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 20.1 ug/L 12/27/16 14:15 7439-92-10.10 1







(612)607-1700

Page 23 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 4.6 ug/L 12/27/16 14:16 7439-92-10.10 1







(612)607-1700

Page 24 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 1.2 ug/L 12/27/16 14:17 7439-92-10.10 1







(612)607-1700

Page 25 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 1.3 ug/L 12/27/16 14:19 7439-92-10.10 1







(612)607-1700

Page 26 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 3.1 ug/L 12/27/16 14:20 7439-92-10.10 1







(612)607-1700

Page 27 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 3.2 ug/L 12/27/16 14:21 7439-92-10.10 1







(612)607-1700

Page 28 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 52.7 ug/L 12/27/16 14:27 7439-92-10.10 1







(612)607-1700

Page 29 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 5.4 ug/L 12/27/16 14:28 7439-92-10.10 1







(612)607-1700

Page 30 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 22.9 ug/L 12/27/16 14:29 7439-92-10.10 1







(612)607-1700

Page 31 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 1.5 ug/L 12/27/16 14:30 7439-92-10.10 1







(612)607-1700

Page 32 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 2.1 ug/L 12/27/16 14:32 7439-92-10.10 1







(612)607-1700

Page 33 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 6.1 ug/L 12/27/16 14:33 7439-92-10.10 1







(612)607-1700

Page 34 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 2.2 ug/L 12/27/16 14:34 7439-92-10.10 1







(612)607-1700

Page 35 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 4.3 ug/L 12/27/16 14:40 7439-92-10.10 1







(612)607-1700

Page 36 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 18.1 ug/L 12/27/16 14:41 7439-92-10.10 1







(612)607-1700

Page 37 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 5.3 ug/L 12/27/16 14:42 7439-92-10.10 1







(612)607-1700

Page 38 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 84.9 ug/L 12/27/16 14:43 7439-92-10.10 1







(612)607-1700

Page 39 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 5.3 ug/L 12/27/16 14:44 7439-92-10.10 1







(612)607-1700

Page 40 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222




Analytical Method: EPA 200.8 Preparation Method: EPA 200.8200.8 MET ICPMS

Lead 14.8 ug/L 12/29/16 22:05 7439-92-112/29/16 09:360.10 1







(612)607-1700

Page 41 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.26 ug/L 12/27/16 14:45 7439-92-10.10 1







(612)607-1700

Page 42 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 4.5 ug/L 12/27/16 14:47 7439-92-10.10 1







(612)607-1700

Page 43 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.27 ug/L 12/27/16 14:48 7439-92-10.10 1







(612)607-1700

Page 44 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 11.9 ug/L 12/27/16 14:51 7439-92-10.10 1







(612)607-1700

Page 45 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 2.2 ug/L 12/27/16 14:52 7439-92-10.10 1







(612)607-1700

Page 46 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 20.1 ug/L 12/27/16 14:54 7439-92-10.10 1







(612)607-1700

Page 47 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 38.4 ug/L 12/27/16 14:55 7439-92-10.10 1







(612)607-1700

Page 48 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 12.8 ug/L 12/27/16 14:56 7439-92-10.10 1







(612)607-1700

Page 49 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 2.0 ug/L 12/27/16 14:57 7439-92-10.10 1







(612)607-1700

Page 50 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 3.6 ug/L 12/27/16 14:59 7439-92-10.10 1







(612)607-1700

Page 51 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.78 ug/L 12/27/16 15:00 7439-92-10.10 1







(612)607-1700

Page 52 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 3.4 ug/L 12/27/16 15:01 7439-92-10.10 1







(612)607-1700

Page 53 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 1.5 ug/L 12/27/16 15:06 7439-92-10.10 1







(612)607-1700

Page 54 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.82 ug/L 12/27/16 15:07 7439-92-10.10 1







(612)607-1700

Page 55 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.75 ug/L 12/27/16 15:11 7439-92-10.10 1







(612)607-1700

Page 56 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 15.0 ug/L 12/27/16 15:12 7439-92-10.10 1







(612)607-1700

Page 57 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 1.0 ug/L 12/27/16 15:14 7439-92-10.10 1







(612)607-1700

Page 58 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 1.5 ug/L 12/27/16 15:18 7439-92-10.10 1







(612)607-1700

Page 59 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.22 ug/L 12/27/16 15:19 7439-92-10.10 1







(612)607-1700

Page 60 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.14 ug/L 12/27/16 15:20 7439-92-10.10 1







(612)607-1700

Page 61 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead ND ug/L 12/27/16 15:21 7439-92-10.10 1







(612)607-1700

Page 62 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.56 ug/L 12/27/16 15:22 7439-92-10.10 1







(612)607-1700

Page 63 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.20 ug/L 12/27/16 15:23 7439-92-10.10 1







(612)607-1700

Page 64 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 9.6 ug/L 12/27/16 15:24 7439-92-10.10 1







(612)607-1700

Page 65 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 2.1 ug/L 12/27/16 15:26 7439-92-10.10 1







(612)607-1700

Page 66 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 19.1 ug/L 12/27/16 15:27 7439-92-10.10 1







(612)607-1700

Page 67 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 15.5 ug/L 12/27/16 15:33 7439-92-10.10 1







(612)607-1700

Page 68 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.65 ug/L 12/27/16 15:34 7439-92-10.10 1







(612)607-1700

Page 69 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.33 ug/L 12/27/16 15:35 7439-92-10.10 1







(612)607-1700

Page 70 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.11 ug/L 12/27/16 15:36 7439-92-10.10 1







(612)607-1700

Page 71 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 5.4 ug/L 12/27/16 15:37 7439-92-10.10 1







(612)607-1700

Page 72 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 1.3 ug/L 12/27/16 15:38 7439-92-10.10 1







(612)607-1700

Page 73 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.54 ug/L 12/27/16 15:39 7439-92-10.10 1







(612)607-1700

Page 74 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.34 ug/L 12/27/16 15:40 7439-92-10.10 1







(612)607-1700

Page 75 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 6.6 ug/L 12/27/16 15:46 7439-92-10.10 1







(612)607-1700

Page 76 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 1.2 ug/L 12/27/16 15:47 7439-92-10.10 1







(612)607-1700

Page 77 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 7.2 ug/L 12/27/16 15:49 7439-92-10.10 1







(612)607-1700

Page 78 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 2.1 ug/L 12/27/16 15:50 7439-92-10.10 1







(612)607-1700

Page 79 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 63.9 ug/L 12/29/16 22:17 7439-92-112/29/16 09:360.10 1







(612)607-1700

Page 80 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 1.1 ug/L 12/27/16 15:51 7439-92-10.10 1







(612)607-1700

Page 81 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 14.2 ug/L 12/27/16 15:52 7439-92-10.10 1







(612)607-1700

Page 82 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 2.0 ug/L 12/27/16 15:53 7439-92-10.10 1







(612)607-1700

Page 83 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 8.4 ug/L 12/27/16 16:47 7439-92-10.10 1







(612)607-1700

Page 84 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.96 ug/L 12/27/16 16:48 7439-92-10.10 1







(612)607-1700

Page 85 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 9.7 ug/L 12/27/16 16:49 7439-92-10.10 1







(612)607-1700

Page 86 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 1.5 ug/L 12/27/16 16:51 7439-92-10.10 1







(612)607-1700

Page 87 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 2.1 ug/L 12/29/16 22:20 7439-92-112/29/16 09:360.10 1







(612)607-1700

Page 88 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.74 ug/L 12/27/16 16:52 7439-92-10.10 1







(612)607-1700

Page 89 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.98 ug/L 12/27/16 16:53 7439-92-10.10 1







(612)607-1700

Page 90 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.69 ug/L 12/27/16 16:54 7439-92-10.10 1







(612)607-1700

Page 91 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 29.6 ug/L 12/27/16 16:55 7439-92-10.10 1







(612)607-1700

Page 92 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 4.4 ug/L 12/27/16 16:56 7439-92-10.10 1







(612)607-1700

Page 93 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 23.6 ug/L 12/27/16 17:02 7439-92-10.10 1







(612)607-1700

Page 94 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 1.8 ug/L 12/27/16 17:03 7439-92-10.10 1







(612)607-1700

Page 95 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.55 ug/L 12/27/16 17:07 7439-92-10.10 1







(612)607-1700

Page 96 of 245


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Pace Project No.:

Project:

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Lead ND ug/L 12/27/16 17:08 7439-92-10.10 1







(612)607-1700

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Pace Project No.:

Project:

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Lead 0.41 ug/L 12/27/16 17:09 7439-92-10.10 1







(612)607-1700

Page 98 of 245


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ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.16 ug/L 12/27/16 17:13 7439-92-10.10 1







(612)607-1700

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ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 2.6 ug/L 12/27/16 17:14 7439-92-10.10 1







(612)607-1700

Page 100 of 245


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ANALYTICAL RESULTS

Pace Project No.:

Project:

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Lead 1.5 ug/L 12/27/16 17:15 7439-92-10.10 1







(612)607-1700

Page 101 of 245


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ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.15 ug/L 12/27/16 17:16 7439-92-10.10 1







(612)607-1700

Page 102 of 245


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Pace Project No.:

Project:

10374222





Lead ND ug/L 12/27/16 17:17 7439-92-10.10 1







(612)607-1700

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Pace Project No.:

Project:

10374222





Lead 0.47 ug/L 12/27/16 17:18 7439-92-10.10 1







(612)607-1700

Page 104 of 245


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Pace Project No.:

Project:

10374222





Lead 0.54 ug/L 12/27/16 17:19 7439-92-10.10 1







(612)607-1700

Page 105 of 245


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Pace Project No.:

Project:

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Lead 0.12 ug/L 12/27/16 17:21 7439-92-10.10 1







(612)607-1700

Page 106 of 245


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ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 1.8 ug/L 12/27/16 17:22 7439-92-10.10 1







(612)607-1700

Page 107 of 245


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ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 1.4 ug/L 12/27/16 17:27 7439-92-10.10 1







(612)607-1700

Page 108 of 245


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ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.64 ug/L 12/27/16 17:29 7439-92-10.10 1







(612)607-1700

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Pace Project No.:

Project:

10374222


Sample: 96 (A) Lab ID: 10374222096 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water



Lead 1.5 ug/L 12/27/16 17:30 7439-92-10.10 1







(612)607-1700

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Pace Project No.:

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Lead 1.3 ug/L 12/27/16 17:31 7439-92-10.10 1







(612)607-1700

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Pace Project No.:

Project:

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Lead 0.91 ug/L 12/27/16 17:32 7439-92-10.10 1







(612)607-1700

Page 112 of 245


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ANALYTICAL RESULTS

Pace Project No.:

Project:

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Lead 0.54 ug/L 12/27/16 17:33 7439-92-10.10 1







(612)607-1700

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Pace Project No.:

Project:

10374222





Lead 1.1 ug/L 12/27/16 17:34 7439-92-10.10 1







(612)607-1700

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Pace Project No.:

Project:

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Lead 3.0 ug/L 12/27/16 17:35 7439-92-10.10 1







(612)607-1700

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Pace Project No.:

Project:

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Lead 1.3 ug/L 12/27/16 17:41 7439-92-10.10 1







(612)607-1700

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Pace Project No.:

Project:

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Lead 2.5 ug/L 12/27/16 17:42 7439-92-10.10 1







(612)607-1700

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Pace Project No.:

Project:

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Lead 2.2 ug/L 12/27/16 17:43 7439-92-10.10 1







(612)607-1700

Page 118 of 245


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Pace Project No.:

Project:

10374222





Lead 0.61 ug/L 12/27/16 17:45 7439-92-10.10 1







(612)607-1700

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Pace Project No.:

Project:

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Lead 0.12 ug/L 12/27/16 17:46 7439-92-10.10 1







(612)607-1700

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Pace Project No.:

Project:

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Lead 0.18 ug/L 12/27/16 17:47 7439-92-10.10 1







(612)607-1700

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Pace Project No.:

Project:

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Lead 0.42 ug/L 12/27/16 17:48 7439-92-10.10 1







(612)607-1700

Page 122 of 245


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Pace Project No.:

Project:

10374222





Lead 0.78 ug/L 12/28/16 07:39 7439-92-10.10 1







(612)607-1700

Page 123 of 245


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Pace Project No.:

Project:

10374222





Lead 0.31 ug/L 12/28/16 07:41 7439-92-10.10 1







(612)607-1700

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Pace Project No.:

Project:

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Lead 0.48 ug/L 12/28/16 07:42 7439-92-10.10 1







(612)607-1700

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Pace Project No.:

Project:

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Lead 0.65 ug/L 12/28/16 07:45 7439-92-10.10 1







(612)607-1700

Page 126 of 245


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Pace Project No.:

Project:

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Lead 0.35 ug/L 12/28/16 07:46 7439-92-10.10 1







(612)607-1700

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Pace Project No.:

Project:

10374222





Lead 0.41 ug/L 12/28/16 07:47 7439-92-10.10 1







(612)607-1700

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Pace Project No.:

Project:

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Lead 0.16 ug/L 12/28/16 07:48 7439-92-10.10 1







(612)607-1700

Page 129 of 245


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Pace Project No.:

Project:

10374222





Lead 66.7 ug/L 12/28/16 07:49 7439-92-10.10 1







(612)607-1700

Page 130 of 245


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Pace Project No.:

Project:

10374222





Lead 10.8 ug/L 12/28/16 07:50 7439-92-10.10 1







(612)607-1700

Page 131 of 245


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Pace Project No.:

Project:

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Lead 0.56 ug/L 12/27/16 16:35 7439-92-10.10 1







(612)607-1700

Page 132 of 245


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Pace Project No.:

Project:

10374222





Lead 0.19 ug/L 12/27/16 16:36 7439-92-10.10 1







(612)607-1700

Page 133 of 245


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ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 21.0 ug/L 12/27/16 16:37 7439-92-10.10 1







(612)607-1700

Page 134 of 245


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ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 2.4 ug/L 12/29/16 18:52 7439-92-10.10 1







(612)607-1700

Page 135 of 245


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Pace Project No.:

Project:

10374222





Lead 25.0 ug/L 12/29/16 19:04 7439-92-10.10 1







(612)607-1700

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Pace Project No.:

Project:

10374222





Lead 5.2 ug/L 12/29/16 19:07 7439-92-10.10 1







(612)607-1700

Page 137 of 245


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Pace Project No.:

Project:

10374222





Lead 586 ug/L 12/29/16 19:10 7439-92-10.10 1







(612)607-1700

Page 138 of 245


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ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 11.1 ug/L 12/29/16 19:13 7439-92-10.10 1







(612)607-1700

Page 139 of 245


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Pace Project No.:

Project:

10374222





Lead 8.5 ug/L 12/29/16 19:22 7439-92-10.10 1







(612)607-1700

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Pace Project No.:

Project:

10374222





Lead 0.80 ug/L 12/29/16 19:25 7439-92-10.10 1







(612)607-1700

Page 141 of 245


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Pace Project No.:

Project:

10374222





Lead 9.0 ug/L 12/29/16 19:28 7439-92-10.10 1







(612)607-1700

Page 142 of 245


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Pace Project No.:

Project:

10374222





Lead 0.65 ug/L 12/29/16 19:31 7439-92-10.10 1







(612)607-1700

Page 143 of 245


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Pace Project No.:

Project:

10374222





Lead 0.48 ug/L 12/29/16 19:34 7439-92-10.10 1







(612)607-1700

Page 144 of 245


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Pace Project No.:

Project:

10374222





Lead 0.37 ug/L 12/29/16 19:37 7439-92-10.10 1







(612)607-1700

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Pace Project No.:

Project:

10374222





Lead 0.13 ug/L 12/29/16 19:40 7439-92-10.10 1







(612)607-1700

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Pace Project No.:

Project:

10374222





Lead 2.1 ug/L 12/29/16 19:43 7439-92-10.10 1







(612)607-1700

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Pace Project No.:

Project:

10374222





Lead 0.57 ug/L 12/29/16 19:46 7439-92-10.10 1







(612)607-1700

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Pace Project No.:

Project:

10374222





Lead 0.20 ug/L 12/29/16 19:49 7439-92-10.10 1







(612)607-1700

Page 149 of 245


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Pace Project No.:

Project:

10374222





Lead 2.1 ug/L 12/29/16 20:04 7439-92-10.10 1







(612)607-1700

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Pace Project No.:

Project:

10374222





Lead 2.2 ug/L 12/29/16 20:07 7439-92-10.10 1







(612)607-1700

Page 151 of 245


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Pace Project No.:

Project:

10374222





Lead 8.1 ug/L 12/29/16 20:10 7439-92-10.10 1







(612)607-1700

Page 152 of 245


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Pace Project No.:

Project:

10374222





Lead 1.1 ug/L 12/29/16 20:13 7439-92-10.10 1







(612)607-1700

Page 153 of 245


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Pace Project No.:

Project:

10374222





Lead 5.3 ug/L 12/29/16 20:16 7439-92-10.10 1







(612)607-1700

Page 154 of 245


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Pace Project No.:

Project:

10374222





Lead 4.1 ug/L 12/29/16 20:22 7439-92-10.10 1







(612)607-1700

Page 155 of 245


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Pace Project No.:

Project:

10374222





Lead 21.1 ug/L 12/29/16 20:41 7439-92-10.10 1







(612)607-1700

Page 156 of 245


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ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 6.9 ug/L 12/29/16 20:44 7439-92-10.10 1







(612)607-1700

Page 157 of 245


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ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 28.0 ug/L 12/29/16 20:47 7439-92-10.10 1







(612)607-1700

Page 158 of 245


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ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 25.5 ug/L 12/29/16 20:50 7439-92-10.10 1







(612)607-1700

Page 159 of 245


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ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 8.4 ug/L 12/29/16 20:53 7439-92-10.10 1







(612)607-1700

Page 160 of 245


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ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 9.9 ug/L 12/29/16 20:56 7439-92-10.10 1







(612)607-1700

Page 161 of 245


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ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 6.9 ug/L 12/29/16 20:59 7439-92-10.10 1







(612)607-1700

Page 162 of 245


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ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 5.8 ug/L 12/29/16 21:01 7439-92-10.10 1







(612)607-1700

Page 163 of 245


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ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 3.7 ug/L 12/29/16 21:11 7439-92-10.10 1







(612)607-1700

Page 164 of 245


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ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 2.8 ug/L 12/29/16 21:14 7439-92-10.10 1







(612)607-1700

Page 165 of 245


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ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 3.2 ug/L 12/29/16 21:16 7439-92-10.10 1







(612)607-1700

Page 166 of 245


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ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 1.3 ug/L 12/29/16 21:20 7439-92-10.10 1







(612)607-1700

Page 167 of 245


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ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.90 ug/L 12/29/16 21:23 7439-92-10.10 1







(612)607-1700

Page 168 of 245


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ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 1.3 ug/L 12/29/16 21:26 7439-92-10.10 1







(612)607-1700

Page 169 of 245


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ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.36 ug/L 12/29/16 21:29 7439-92-10.10 1







(612)607-1700

Page 170 of 245


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ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.86 ug/L 12/29/16 21:32 7439-92-10.10 1







(612)607-1700

Page 171 of 245


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ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 2.0 ug/L 12/29/16 21:35 7439-92-10.10 1







(612)607-1700

Page 172 of 245


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ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.27 ug/L 12/29/16 21:38 7439-92-10.10 1







(612)607-1700

Page 173 of 245


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ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 1.9 ug/L 12/29/16 21:47 7439-92-10.10 1







(612)607-1700

Page 174 of 245


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ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 4.6 ug/L 12/28/16 08:22 7439-92-10.10 1







(612)607-1700

Page 175 of 245


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ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.40 ug/L 12/28/16 08:27 7439-92-10.10 1







(612)607-1700

Page 176 of 245


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ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.98 ug/L 12/28/16 08:28 7439-92-10.10 1







(612)607-1700

Page 177 of 245


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ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 2.9 ug/L 12/28/16 08:29 7439-92-10.10 1







(612)607-1700

Page 178 of 245


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ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.46 ug/L 12/28/16 08:32 7439-92-10.10 1







(612)607-1700

Page 179 of 245


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ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 1.1 ug/L 12/28/16 08:33 7439-92-10.10 1







(612)607-1700

Page 180 of 245


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ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 1.4 ug/L 12/28/16 08:34 7439-92-10.10 1







(612)607-1700

Page 181 of 245


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ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.41 ug/L 12/28/16 08:35 7439-92-10.10 1







(612)607-1700

Page 182 of 245


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ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 1.4 ug/L 12/28/16 08:36 7439-92-10.10 1







(612)607-1700

Page 183 of 245


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ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 1.9 ug/L 12/28/16 08:37 7439-92-10.10 1







(612)607-1700

Page 184 of 245


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ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.30 ug/L 12/28/16 08:38 7439-92-10.10 1







(612)607-1700

Page 185 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 5.1 ug/L 12/28/16 08:40 7439-92-10.10 1







(612)607-1700

Page 186 of 245


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ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 4.1 ug/L 12/28/16 08:41 7439-92-10.10 1







(612)607-1700

Page 187 of 245


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ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.73 ug/L 12/28/16 08:47 7439-92-10.10 1







(612)607-1700

Page 188 of 245


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ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.20 ug/L 12/28/16 08:48 7439-92-10.10 1







(612)607-1700

Page 189 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead ND ug/L 12/28/16 08:49 7439-92-10.10 1







(612)607-1700

Page 190 of 245


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ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 1.0 ug/L 12/28/16 08:50 7439-92-10.10 1







(612)607-1700

Page 191 of 245


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ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.26 ug/L 12/28/16 08:51 7439-92-10.10 1







(612)607-1700

Page 192 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 2.6 ug/L 12/28/16 08:52 7439-92-10.10 1







(612)607-1700

Page 193 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 11.9 ug/L 12/29/16 22:23 7439-92-112/29/16 09:360.10 1







(612)607-1700

Page 194 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.22 ug/L 12/28/16 08:53 7439-92-10.10 1







(612)607-1700

Page 195 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 4.1 ug/L 12/28/16 09:00 7439-92-10.10 1







(612)607-1700

Page 196 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 1.0 ug/L 12/28/16 09:01 7439-92-10.10 1







(612)607-1700

Page 197 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 1.6 ug/L 12/28/16 09:02 7439-92-10.10 1







(612)607-1700

Page 198 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 1.1 ug/L 12/28/16 09:03 7439-92-10.10 1







(612)607-1700

Page 199 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.37 ug/L 12/28/16 09:04 7439-92-10.10 1







(612)607-1700

Page 200 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.50 ug/L 12/28/16 09:05 7439-92-10.10 1







(612)607-1700

Page 201 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 1.1 ug/L 12/28/16 09:06 7439-92-10.10 1







(612)607-1700

Page 202 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.46 ug/L 12/28/16 09:07 7439-92-10.10 1







(612)607-1700

Page 203 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 1.5 ug/L 12/28/16 09:10 7439-92-10.10 1







(612)607-1700

Page 204 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 2.3 ug/L 12/28/16 09:11 7439-92-10.10 1







(612)607-1700

Page 205 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.64 ug/L 12/28/16 09:14 7439-92-10.10 1







(612)607-1700

Page 206 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 1.1 ug/L 12/28/16 09:15 7439-92-10.10 1







(612)607-1700

Page 207 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.80 ug/L 12/28/16 09:16 7439-92-10.10 1







(612)607-1700

Page 208 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.27 ug/L 12/28/16 09:17 7439-92-10.10 1







(612)607-1700

Page 209 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 2.5 ug/L 12/28/16 09:18 7439-92-10.10 1







(612)607-1700

Page 210 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 1.4 ug/L 12/28/16 09:19 7439-92-10.10 1







(612)607-1700

Page 211 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.38 ug/L 12/28/16 09:20 7439-92-10.10 1







(612)607-1700

Page 212 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.36 ug/L 12/28/16 09:25 7439-92-10.10 1







(612)607-1700

Page 213 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.12 ug/L 12/28/16 09:26 7439-92-10.10 1







(612)607-1700

Page 214 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.97 ug/L 12/28/16 09:27 7439-92-10.10 1







(612)607-1700

Page 215 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.31 ug/L 12/28/16 09:31 7439-92-10.10 1







(612)607-1700

Page 216 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.28 ug/L 12/28/16 09:33 7439-92-10.10 1







(612)607-1700

Page 217 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222





Lead 0.18 ug/L 12/28/16 09:36 7439-92-10.10 1







(612)607-1700

Page 218 of 245


#=AR#

ANALYTICAL RESULTS

Pace Project No.:

Project:

10374222


Sample: 96(B) Lab ID: 10374222205 Collected: 12/22/16 00:00 Received: 12/23/16 12:15 Matrix: Water



Lead ND ug/L 12/28/16 09:37 7439-92-10.10 1







(612)607-1700

Page 219 of 245


#=QC#

QUALITY CONTROL DATA

Pace Project No.:

Project:

10374222


Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.

QC Batch:

QC Batch Method:

Analysis Method:

Analysis Description:

453250

EPA 200.8

EPA 200.8

ICPMS Metals, Drinking Water

Associated Lab Samples: 10374222001, 10374222002, 10374222003, 10374222004, 10374222005, 10374222006, 10374222007,10374222008, 10374222009, 10374222010, 10374222011, 10374222012, 10374222013, 10374222014,10374222015, 10374222016, 10374222017, 10374222018, 10374222019, 10374222020

Parameter Units

Blank

Result

Reporting

Limit Qualifiers

METHOD BLANK: 2481496


Matrix: Water

Analyzed

Lead ug/L ND 0.10 12/27/16 13:59

Parameter Units

LCS

Result

% Rec

Limits Qualifiers% RecConc.

2481497LABORATORY CONTROL SAMPLE:

LCSSpike

Lead ug/L 101100 101 85-115

Parameter Units

MS

Result

% Rec

Limits Qual% RecConc.

2482275MATRIX SPIKE & MATRIX SPIKE DUPLICATE:

MSSpike

Result

10374222001

2482276

MSD

Result

MSD

% Rec RPD RPD

Max

MSDMS

Spike

Conc.

Lead ug/L 100 96 70-13096 0 201000.21 96.7 96.5

Parameter Units

MS

Result

% Rec


2482277MATRIX SPIKE SAMPLE:

MSSpike

Result

10374222011

Lead ug/L 113100 112 70-1301.2







(612)607-1700

Page 220 of 245


#=QC#


Pace Project No.:

Project:

10374222



QC Batch:

QC Batch Method:

Analysis Method:


453251

EPA 200.8

EPA 200.8


Associated Lab Samples: 10374222021, 10374222022, 10374222023, 10374222024, 10374222025, 10374222026, 10374222028,10374222029, 10374222030, 10374222031, 10374222032, 10374222033, 10374222034, 10374222035,10374222036, 10374222037, 10374222038, 10374222039, 10374222040

Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Water

Analyzed

Lead ug/L ND 0.10 12/27/16 14:25

Parameter Units

LCS

Result

% Rec



LCSSpike

Lead ug/L 99.2100 99 85-115

Parameter Units

MS

Result

% Rec



MSSpike

Result

10374222021

2482311

MSD

Result

MSD

% Rec RPD RPD

Max

MSDMS

Spike

Conc.

Lead ug/L 100 100 70-13098 2 201002.2 102 100

Parameter Units

MS

Result

% Rec



MSSpike

Result

10374222032

Lead ug/L 110100 108 70-1302.2







(612)607-1700

Page 221 of 245


#=QC#


Pace Project No.:

Project:

10374222



QC Batch:

QC Batch Method:

Analysis Method:


453252

EPA 200.8

EPA 200.8



Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Water

Analyzed

Lead ug/L ND 0.10 12/27/16 15:04

Parameter Units

LCS

Result

% Rec



LCSSpike

Lead ug/L 102100 102 85-115

Parameter Units

MS

Result

% Rec



MSSpike

Result

10374222041

2482327

MSD

Result

MSD

% Rec RPD RPD

Max

MSDMS

Spike

Conc.

Lead ug/L 100 98 70-130101 2 201000.82 99.3 102

Parameter Units

MS

Result

% Rec



MSSpike

Result

10374222051

Lead ug/L 112100 103 70-1309.6







(612)607-1700

Page 222 of 245


#=QC#


Pace Project No.:

Project:

10374222



QC Batch:

QC Batch Method:

Analysis Method:


453253

EPA 200.8

EPA 200.8


Associated Lab Samples: 10374222061, 10374222062, 10374222063, 10374222064, 10374222065, 10374222067, 10374222068,10374222069, 10374222070, 10374222071, 10374222072, 10374222073, 10374222075, 10374222076,10374222077, 10374222078, 10374222079, 10374222080

Parameter Units

Blank

Result

Reporting

Limit Qualifiers


Associated Lab Samples: 10374222061, 10374222062, 10374222063, 10374222064, 10374222065, 10374222067, 10374222068,10374222069, 10374222070, 10374222071, 10374222072, 10374222073, 10374222075, 10374222076,10374222077, 10374222078, 10374222079, 10374222080

Matrix: Water

Analyzed

Lead ug/L ND 0.10 12/27/16 15:30

Parameter Units

LCS

Result

% Rec



LCSSpike

Lead ug/L 104100 104 85-115

Parameter Units

MS

Result

% Rec



MSSpike

Result

10374222061

2482356

MSD

Result

MSD

% Rec RPD RPD

Max

MSDMS

Spike

Conc.

Lead ug/L 100 98 70-13096 1 201000.34 97.9 96.6

Parameter Units

MS

Result

% Rec



MSSpike

Result

10374222072

Lead ug/L 108100 98 70-1309.7







(612)607-1700

Page 223 of 245


#=QC#


Pace Project No.:

Project:

10374222



QC Batch:

QC Batch Method:

Analysis Method:


453254

EPA 200.8

EPA 200.8



Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Water

Analyzed

Lead ug/L ND 0.10 12/27/16 17:00

Parameter Units

LCS

Result

% Rec



LCSSpike

Lead ug/L 101100 101 85-115

Parameter Units

MS

Result

% Rec



MSSpike

Result

10374222081

2482371

MSD

Result

MSD

% Rec RPD RPD

Max

MSDMS

Spike

Conc.

Lead ug/L 100 102 70-13099 2 201001.8 103 101

Parameter Units

MS

Result

% Rec



MSSpike

Result

10374222091

Lead ug/L 99.5100 99 70-1300.54







(612)607-1700

Page 224 of 245


#=QC#


Pace Project No.:

Project:

10374222



QC Batch:

QC Batch Method:

Analysis Method:


453255

EPA 200.8

EPA 200.8



Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Water

Analyzed

Lead ug/L ND 0.10 12/27/16 17:25

Parameter Units

LCS

Result

% Rec



LCSSpike

Lead ug/L 102100 102 85-115

Parameter Units

MS

Result

% Rec



MSSpike

Result

10374222101

2482413

MSD

Result

MSD

% Rec RPD RPD

Max

MSDMS

Spike

Conc.

Lead ug/L 100 98 70-130101 3 201003.0 101 104

Parameter Units

MS

Result

% Rec



MSSpike

Result

10374222111

Lead ug/L 96.7100 96 70-1300.48







(612)607-1700

Page 225 of 245


#=QC#


Pace Project No.:

Project:

10374222



QC Batch:

QC Batch Method:

Analysis Method:


453256

EPA 200.8

EPA 200.8



Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Water

Analyzed

Lead ug/L ND 0.10 12/29/16 18:46

Parameter Units

LCS

Result

% Rec



LCSSpike

Lead ug/L 104100 104 85-115

Parameter Units

MS

Result

% Rec



MSSpike

Result

10374222121

2482589

MSD

Result

MSD

% Rec RPD RPD

Max

MSDMS

Spike

Conc.

Lead ug/L 100 100 70-13099 1 201002.4 103 101

Parameter Units

MS

Result

% Rec



MSSpike

Result

10374222140

Lead ug/L 103100 97 70-1305.3







(612)607-1700

Page 226 of 245


#=QC#


Pace Project No.:

Project:

10374222



QC Batch:

QC Batch Method:

Analysis Method:


453257

EPA 200.8

EPA 200.8



Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Water

Analyzed

Lead ug/L ND 0.10 12/29/16 19:58

Parameter Units

LCS

Result

% Rec



LCSSpike

Lead ug/L 106100 106 85-115

Parameter Units

MS

Result

% Rec



MSSpike

Result

10374222141

2483481

MSD

Result

MSD

% Rec RPD RPD

Max

MSDMS

Spike

Conc.

Lead ug/L 100 99 70-13097 1 201004.1 103 101

Parameter Units

MS

Result

% Rec



MSSpike

Result

10374222160

Lead ug/L 103100 101 70-1301.9







(612)607-1700

Page 227 of 245


#=QC#


Pace Project No.:

Project:

10374222



QC Batch:

QC Batch Method:

Analysis Method:


453258

EPA 200.8

EPA 200.8



Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Water

Analyzed

Lead ug/L ND 0.10 12/28/16 08:20

Parameter Units

LCS

Result

% Rec



LCSSpike

Lead ug/L 99.7100 100 85-115

Parameter Units

MS

Result

% Rec



MSSpike

Result

10374222161

2482572

MSD

Result

MSD

% Rec RPD RPD

Max

MSDMS

Spike

Conc.

Lead ug/L 100 99 70-13095 4 201004.6 103 99.2

Parameter Units

MS

Result

% Rec



MSSpike

Result

10374222171

Lead ug/L 95.9100 96 70-1300.30







(612)607-1700

Page 228 of 245


#=QC#


Pace Project No.:

Project:

10374222



QC Batch:

QC Batch Method:

Analysis Method:


453259

EPA 200.8

EPA 200.8



Parameter Units

Blank

Result

Reporting

Limit Qualifiers



Matrix: Water

Analyzed

Lead ug/L ND 0.10 12/28/16 08:45

Parameter Units

LCS

Result

% Rec



LCSSpike

Lead ug/L 96.2100 96 85-115

Parameter Units

MS

Result

% Rec



MSSpike

Result

10374222181

2482577

MSD

Result

MSD

% Rec RPD RPD

Max

MSDMS

Spike

Conc.

Lead ug/L 100 90 70-13095 5 201000.22 90.1 95.0

Parameter Units

MS

Result

% Rec



MSSpike

Result

10374222191

Lead ug/L 94.7100 92 70-1302.3







(612)607-1700

Page 229 of 245


#=QC#


Pace Project No.:

Project:

10374222



QC Batch:

QC Batch Method:

Analysis Method:


453260

EPA 200.8

EPA 200.8


Associated Lab Samples: 10374222201, 10374222202, 10374222203, 10374222204, 10374222205

Parameter Units

Blank

Result

Reporting

Limit Qualifiers


Associated Lab Samples: 10374222201, 10374222202, 10374222203, 10374222204, 10374222205

Matrix: Water

Analyzed

Lead ug/L ND 0.10 12/28/16 09:23

Parameter Units

LCS

Result

% Rec



LCSSpike

Lead ug/L 97.5100 98 85-115

Parameter Units

MS

Result

% Rec



MSSpike

Result

10374222201

2482586

MSD

Result

MSD

% Rec RPD RPD

Max

MSDMS

Spike

Conc.

Lead ug/L 100 96 70-13096 1 201000.97 97.4 96.6







(612)607-1700

Page 230 of 245


#=QC#


Pace Project No.:

Project:

10374222



QC Batch:

QC Batch Method:

Analysis Method:


453517

EPA 200.8

EPA 200.8

200.8 MET

Associated Lab Samples: 10374222027, 10374222066, 10374222074, 10374222180

Parameter Units

Blank

Result

Reporting

Limit Qualifiers


Associated Lab Samples: 10374222027, 10374222066, 10374222074, 10374222180

Matrix: Water

Analyzed

Lead ug/L ND 0.10 12/29/16 21:59

Parameter Units

LCS

Result

% Rec



LCSSpike

Lead ug/L 106100 106 85-115

Parameter Units

MS

Result

% Rec



MSSpike

Result

10374222027

2482632

MSD

Result

MSD

% Rec RPD RPD

Max

MSDMS

Spike

Conc.

Lead ug/L 100 105 70-130105 0 2010014.8 120 120







(612)607-1700

Page 231 of 245


#=QL#

QUALIFIERS

Pace Project No.:

Project:

10374222


DEFINITIONS

DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.

ND - Not Detected at or above adjusted reporting limit.

J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.

MDL - Adjusted Method Detection Limit.

PQL - Practical Quantitation Limit.

RL - Reporting Limit.

S - Surrogate

1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte isa combined concentration.

Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.

LCS(D) - Laboratory Control Sample (Duplicate)

MS(D) - Matrix Spike (Duplicate)

DUP - Sample Duplicate

RPD - Relative Percent Difference

NC - Not Calculable.

SG - Silica Gel - Clean-Up

U - Indicates the compound was analyzed for, but not detected.

N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.

Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.

TNI - The NELAC Institute.

LABORATORIES

Pace Analytical Services - MinneapolisPASI-M







(612)607-1700

Page 232 of 245


#=CR#

QUALITY CONTROL DATA CROSS REFERENCE TABLE

Pace Project No.:

Project:

10374222


Lab ID Sample ID QC Batch Method QC Batch Analytical Method

Analytical

Batch

10374222001 4532501 EPA 200.8

10374222002 4532502 EPA 200.8

10374222003 4532503 EPA 200.8

10374222004 4532504 EPA 200.8

10374222005 4532505 EPA 200.8

10374222006 4532506 EPA 200.8

10374222007 4532507 EPA 200.8

10374222008 4532508 EPA 200.8

10374222009 4532509 EPA 200.8

10374222010 45325010 EPA 200.8

10374222011 45325011 EPA 200.8

10374222012 45325012 EPA 200.8

10374222013 45325013 EPA 200.8

10374222014 45325014 EPA 200.8

10374222015 45325015 EPA 200.8

10374222016 45325016 EPA 200.8

10374222017 45325017 EPA 200.8

10374222018 45325018 EPA 200.8

10374222019 45325019 EPA 200.8

10374222020 45325020 EPA 200.8

10374222021 45325121 EPA 200.8

10374222022 45325122 EPA 200.8

10374222023 45325123 EPA 200.8

10374222024 45325124 EPA 200.8

10374222025 45325125 EPA 200.8

10374222026 45325126 EPA 200.8

10374222028 45325128 EPA 200.8

10374222029 45325129 EPA 200.8

10374222030 45325130 EPA 200.8

10374222031 45325131 EPA 200.8

10374222032 45325132 EPA 200.8

10374222033 45325133 EPA 200.8

10374222034 45325134 EPA 200.8

10374222035 45325135 EPA 200.8

10374222036 45325136 EPA 200.8

10374222037 45325137 EPA 200.8

10374222038 45325138 EPA 200.8

10374222039 45325139 EPA 200.8

10374222040 45325140 EPA 200.8

10374222041 45325241 EPA 200.8

10374222042 45325242 EPA 200.8

10374222043 45325243 EPA 200.8

10374222044 45325244 EPA 200.8

10374222045 45325245 EPA 200.8

10374222046 45325246 EPA 200.8

10374222047 45325247 EPA 200.8

10374222048 45325248 EPA 200.8

10374222049 45325249 EPA 200.8







(612)607-1700

Page 233 of 245


#=CR#


Pace Project No.:

Project:

10374222



Analytical

Batch

10374222050 45325250 EPA 200.8

10374222051 45325251 EPA 200.8

10374222052 45325252 EPA 200.8

10374222053 45325253 EPA 200.8

10374222054 45325254 EPA 200.8

10374222055 45325255 EPA 200.8

10374222056 45325256 EPA 200.8

10374222057 45325257 EPA 200.8

10374222058 45325258 EPA 200.8

10374222059 45325259 EPA 200.8

10374222060 45325260 EPA 200.8

10374222061 45325361 EPA 200.8

10374222062 45325362 EPA 200.8

10374222063 45325363 EPA 200.8

10374222064 45325364 EPA 200.8

10374222065 45325365 EPA 200.8

10374222067 45325367 EPA 200.8

10374222068 45325368 EPA 200.8

10374222069 45325369 EPA 200.8

10374222070 45325370 EPA 200.8

10374222071 45325371 EPA 200.8

10374222072 45325372 EPA 200.8

10374222073 45325373 EPA 200.8

10374222075 45325375 EPA 200.8

10374222076 45325376 EPA 200.8

10374222077 45325377 EPA 200.8

10374222078 45325378 EPA 200.8

10374222079 45325379 EPA 200.8

10374222080 45325380 EPA 200.8

10374222081 45325481 EPA 200.8

10374222082 45325482 EPA 200.8

10374222083 45325483 EPA 200.8

10374222084 45325484 EPA 200.8

10374222085 45325485 EPA 200.8

10374222086 45325486 EPA 200.8

10374222087 45325487 EPA 200.8

10374222088 45325488 EPA 200.8

10374222089 45325489 EPA 200.8

10374222090 45325490 EPA 200.8

10374222091 45325491 EPA 200.8

10374222092 45325492 EPA 200.8

10374222093 45325493 EPA 200.8

10374222094 45325494 EPA 200.8

10374222095 45325495 EPA 200.8

10374222096 45325496 (A) EPA 200.8

10374222097 45325497 EPA 200.8

10374222098 45325498 EPA 200.8

10374222099 45325499 EPA 200.8







(612)607-1700

Page 234 of 245


#=CR#


Pace Project No.:

Project:

10374222



Analytical

Batch

10374222100 453254100 EPA 200.8

10374222101 453255101 EPA 200.8

10374222102 453255102 EPA 200.8

10374222103 453255103 EPA 200.8

10374222104 453255104 EPA 200.8

10374222105 453255105 EPA 200.8

10374222106 453255106 EPA 200.8

10374222107 453255107 EPA 200.8

10374222108 453255108 EPA 200.8

10374222109 453255109 EPA 200.8

10374222110 453255110 EPA 200.8

10374222111 453255111 EPA 200.8

10374222112 453255112 EPA 200.8

10374222113 453255113 EPA 200.8

10374222114 453255114 EPA 200.8

10374222115 453255115 EPA 200.8

10374222116 453255116 EPA 200.8

10374222117 453255117 EPA 200.8

10374222118 453255118 EPA 200.8

10374222119 453255119 EPA 200.8

10374222120 453255120 EPA 200.8

10374222121 453256121 EPA 200.8

10374222122 453256122 EPA 200.8

10374222123 453256123 EPA 200.8

10374222124 453256124 EPA 200.8

10374222125 453256125 EPA 200.8

10374222126 453256126 EPA 200.8

10374222127 453256127 EPA 200.8

10374222128 453256128 EPA 200.8

10374222129 453256129 EPA 200.8

10374222130 453256130 EPA 200.8

10374222131 453256131 EPA 200.8

10374222132 453256132 EPA 200.8

10374222133 453256133 EPA 200.8

10374222134 453256134 EPA 200.8

10374222135 453256135 EPA 200.8

10374222136 453256136 EPA 200.8

10374222137 453256137 EPA 200.8

10374222138 453256138 EPA 200.8

10374222139 453256139 EPA 200.8

10374222140 453256140 EPA 200.8

10374222141 453257141 EPA 200.8

10374222142 453257142 EPA 200.8

10374222143 453257143 EPA 200.8

10374222144 453257144 EPA 200.8

10374222145 453257145 EPA 200.8

10374222146 453257146 EPA 200.8







(612)607-1700

Page 235 of 245


#=CR#


Pace Project No.:

Project:

10374222



Analytical

Batch

10374222147 453257147 EPA 200.8

10374222148 453257148 EPA 200.8

10374222149 453257149 EPA 200.8

10374222150 453257150 EPA 200.8

10374222151 453257151 EPA 200.8

10374222152 453257152 EPA 200.8

10374222153 453257153 EPA 200.8

10374222154 453257154 EPA 200.8

10374222155 453257155 EPA 200.8

10374222156 453257156 EPA 200.8

10374222157 453257157 EPA 200.8

10374222158 453257158 EPA 200.8

10374222159 453257159 EPA 200.8

10374222160 453257160 EPA 200.8

10374222161 453258161 EPA 200.8

10374222162 453258162 EPA 200.8

10374222163 453258163 EPA 200.8

10374222164 453258164 EPA 200.8

10374222165 453258165 EPA 200.8

10374222166 453258166 EPA 200.8

10374222167 453258167 EPA 200.8

10374222168 453258168 EPA 200.8

10374222169 453258169 EPA 200.8

10374222170 453258170 EPA 200.8

10374222171 453258171 EPA 200.8

10374222172 453258172 EPA 200.8

10374222173 453258173 EPA 200.8

10374222174 453258174 EPA 200.8

10374222175 453258175 EPA 200.8

10374222176 453258176 EPA 200.8

10374222177 453258177 EPA 200.8

10374222178 453258178 EPA 200.8

10374222179 453258179 EPA 200.8

10374222181 453259181 EPA 200.8

10374222182 453259182 EPA 200.8

10374222183 453259183 EPA 200.8

10374222184 453259184 EPA 200.8

10374222185 453259185 EPA 200.8

10374222186 453259186 EPA 200.8

10374222187 453259187 EPA 200.8

10374222188 453259188 EPA 200.8

10374222189 453259189 EPA 200.8

10374222190 453259190 EPA 200.8

10374222191 453259191 EPA 200.8

10374222192 453259192 EPA 200.8

10374222193 453259193 EPA 200.8

10374222194 453259194 EPA 200.8

10374222195 453259195 EPA 200.8







(612)607-1700

Page 236 of 245


#=CR#


Pace Project No.:

Project:

10374222



Analytical

Batch

10374222196 453259196 EPA 200.8

10374222197 453259197 EPA 200.8

10374222198 453259198 EPA 200.8

10374222199 453259199 EPA 200.8

10374222200 453259200 EPA 200.8

10374222201 453260201 EPA 200.8

10374222202 453260202 EPA 200.8

10374222203 453260203 EPA 200.8

10374222204 453260204 EPA 200.8

10374222205 45326096(B) EPA 200.8

10374222027 453517 45379227 EPA 200.8 EPA 200.8

10374222066 453517 45379266 EPA 200.8 EPA 200.8

10374222074 453517 45379274 EPA 200.8 EPA 200.8

10374222180 453517 453792180 EPA 200.8 EPA 200.8







(612)607-1700

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12/23/16

Temperature ok for metals.

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Appendix D Laboratory Accreditation, Personnel Certifications


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for fields of accreditation listed on the laboratory's accompanying Scope of Certification

in accordance with the provisions in Minnesota Laws and Rules.

Continued accreditation is contingent upon successful on-going compliance with Minnesota Statutes 144.97 to 144.98, 2009 TNI

Standard and applicable Minnesota Rules 4740.2010 to 4740.2120. The laboratory's Scope of Certification cites the specific

programs, methods, analytes and matrices for which MDH issues this accreditation.

This certificate is valid proof of accreditation only when associated with its accompanying Scope of Certification.

The Scope of Certification and reports of on-site assessments are on file at the Minnesota Department of Health,

601 Robert Street North, Saint Paul, Minnesota. Customers may verify the laboratory's accreditation status in

Minnesota by contacting MNELAP at (651) 201-5324.

Minnesota Department of Health

Environmental Laboratory Accreditation Program

Issues accreditation to

State Laboratory ID: 027-053-137

EPA Lab Code: MN00064

Pace Analytical Services, LLC. - Minneapolis MN

1700 Elm Street SE, Suite 200


Effective Date: 12/22/2016

Expires: 12/31/2017

Certificate Number: 1179284

Issued under the authoritydelegated by theCommissioner of Health,State of Minnesota

AET Project No. 03-06427 Page D3 of 90

Printed on 12/22/2016

THIS LISTING OF FIELDS OF ACCREDITATION MUST BE

ACCOMPANIED BY CERTIFICATE NUMBER: 1179284

Pace Analytical Services, LLC. - Minneapolis MN

1700 Elm Street SE, Suite 200


EPA 3C Preparation Techniques: N/A

EPA Method 23 Preparation Techniques: N/A

Environmental Laboratory Accreditation Program

Scope of Certification

State Laboratory ID: 027-053-137 EPA Lab Code: MN00064 Issue Date: 12/22/2016

Expiration Date: 12/31/2017

Clean Air Act

Program Method Analyte Matrix Primary SOP

CAA EPA 3C Carbon dioxide AIR MN

CAA EPA 3C Carbon monoxide AIR MN

CAA EPA 3C Methane AIR MN

CAA EPA 3C Nitrogen AIR MN

CAA EPA 3C Oxygen AIR MN


CAA EPA Method 23 1,2,3,4,6,7,8,9-Octachlorodibenzo-p-dioxin (OCDD)

AIR MN

CAA EPA Method 23 1,2,3,4,6,7,8,9-Octachlorodibenzofuran(OCDF)

AIR MN

CAA EPA Method 23 1,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin (1,2,3,4,6,7,8-hpcdd)

AIR MN

CAA EPA Method 23 1,2,3,4,6,7,8-Heptachlorodibenzofuran(1,2,3,4,6,7,8-hpcdf)

AIR MN

Page 1 of 87



EPA RSK-175 (GC/FID) Preparation Techniques: N/A

EPA TO-13A Preparation Techniques: N/A


CAA EPA Method 23 1,2,3,4,7,8,9-Heptachlorodibenzofuran(1,2,3,4,7,8,9-hpcdf)

AIR MN

CAA EPA Method 23 1,2,3,4,7,8-Hexachlorodibenzo-p-dioxin(1,2,3,4,7,8-Hxcdd)

AIR MN

CAA EPA Method 23 1,2,3,4,7,8-Hexachlorodibenzofuran(1,2,3,4,7,8-Hxcdf)

AIR MN


AIR MN


AIR MN


AIR MN


AIR MN

CAA EPA Method 23 1,2,3,7,8-Pentachlorodibenzo-p-dioxin(1,2,3,7,8-Pecdd)

AIR MN

CAA EPA Method 23 1,2,3,7,8-Pentachlorodibenzofuran(1,2,3,7,8-Pecdf)

AIR MN

CAA EPA Method 23 2,3,4,6,7,8-Hexachlorodibenzofuran AIR MN

CAA EPA Method 23 2,3,4,7,8-Pentachlorodibenzofuran AIR MN

CAA EPA Method 23 2,3,7,8-Tetrachlorodibenzo- p-dioxin(2,3,7,8-TCDD)

AIR MN

CAA EPA Method 23 2,3,7,8-Tetrachlorodibenzofuran AIR MN


CAA EPA RSK-175 (GC/FID) Ethane AIR MN

CAA EPA RSK-175 (GC/FID) Ethene AIR MN

CAA EPA RSK-175 (GC/FID) Methane AIR MN

CAA EPA RSK-175 (GC/FID) n-Propane AIR MN


CAA EPA TO-13A 2-Methylnaphthalene AIR MN

CAA EPA TO-13A Acenaphthene AIR MN

CAA EPA TO-13A Acenaphthylene AIR MN

Page 2 of 87





CAA EPA TO-13A Anthracene AIR MN

CAA EPA TO-13A Benzo(a)anthracene AIR MN

CAA EPA TO-13A Benzo(a)pyrene AIR MN

CAA EPA TO-13A Benzo(e)pyrene AIR MN

CAA EPA TO-13A Benzo(g,h,i)perylene AIR MN

CAA EPA TO-13A Benzo(k)fluoranthene AIR MN

CAA EPA TO-13A Benzo[b]fluoranthene AIR MN

CAA EPA TO-13A Chrysene AIR MN

CAA EPA TO-13A Dibenz(a,h) anthracene AIR MN

CAA EPA TO-13A Fluoranthene AIR MN

CAA EPA TO-13A Fluorene AIR MN

CAA EPA TO-13A Indeno(1,2,3-cd) pyrene AIR MN

CAA EPA TO-13A Naphthalene AIR MN

CAA EPA TO-13A Phenanthrene AIR MN

CAA EPA TO-13A Pyrene AIR MN


CAA EPA TO-14A 1,1,1-Trichloroethane AIR MN

CAA EPA TO-14A 1,1,2,2-Tetrachloroethane AIR MN

CAA EPA TO-14A 1,1,2-Trichloro-1,2,2-trifluoroethane(Freon 113)

AIR MN

CAA EPA TO-14A 1,1,2-Trichloroethane AIR MN

CAA EPA TO-14A 1,1-Dichloroethane AIR MN

CAA EPA TO-14A 1,1-Dichloroethylene AIR MN

CAA EPA TO-14A 1,2,4-Trichlorobenzene AIR MN

CAA EPA TO-14A 1,2,4-Trimethylbenzene AIR MN

CAA EPA TO-14A 1,2-Dibromoethane (EDB, Ethylenedibromide)

AIR MN

CAA EPA TO-14A 1,2-Dichloro-1,1,2,2-tetrafluoroethane(Freon-114)

AIR MN

CAA EPA TO-14A 1,2-Dichlorobenzene AIR MN

CAA EPA TO-14A 1,2-Dichloroethane (Ethylene dichloride) AIR MN

CAA EPA TO-14A 1,2-Dichloroethene (total) AIR MN

CAA EPA TO-14A 1,2-Dichloropropane AIR MN

Page 3 of 87



EPA TO-17




CAA EPA TO-14A Benzene AIR MN

CAA EPA TO-14A Benzyl chloride AIR MN

CAA EPA TO-14A Bromoform AIR MN

CAA EPA TO-14A Bromomethane AIR MN

CAA EPA TO-14A Carbon tetrachloride AIR MN

CAA EPA TO-14A Chlorobenzene AIR MN

CAA EPA TO-14A Chloroethane (Ethyl chloride) AIR MN

CAA EPA TO-14A Chloroform AIR MN

CAA EPA TO-14A cis-1,2-Dichloroethylene AIR MN

CAA EPA TO-14A cis-1,3-Dichloropropene AIR MN

CAA EPA TO-14A Dichlorodifluoromethane (Freon-12) AIR MN

CAA EPA TO-14A Ethylbenzene AIR MN

CAA EPA TO-14A Hexachloro-1,3-butadiene AIR MN

CAA EPA TO-14A Hexachlorobutadiene AIR MN

CAA EPA TO-14A m+p-xylene AIR MN

CAA EPA TO-14A Methyl chloride (Chloromethane) AIR MN

CAA EPA TO-14A Methyl tert-butyl ether (MTBE) AIR MN

CAA EPA TO-14A Methylene chloride (Dichloromethane) AIR MN

CAA EPA TO-14A n-Hexane AIR MN

CAA EPA TO-14A o-Xylene AIR MN

CAA EPA TO-14A Styrene AIR MN

CAA EPA TO-14A Tetrachloroethene AIR MN

CAA EPA TO-14A THC as Gas AIR MN

CAA EPA TO-14A Toluene AIR MN

CAA EPA TO-14A trans-1,2-Dichloroethylene AIR MN

CAA EPA TO-14A trans-1,3-Dichloropropylene AIR MN

CAA EPA TO-14A Trichloroethene (Trichloroethylene) AIR MN

CAA EPA TO-14A Trichlorofluoromethane(Fluorotrichloromethane, Freon 11)

AIR MN

CAA EPA TO-14A Vinyl chloride AIR MN

CAA EPA TO-14A Xylene (total) AIR MN

Page 4 of 87



Preparation Techniques: N/A


CAA EPA TO-17 1,1,1-Trichloroethane AIR MN

CAA EPA TO-17 1,1,2,2-Tetrachloroethane AIR MN

CAA EPA TO-17 1,1,2-Trichloro-1,2,2-trifluoroethane(Freon 113)

AIR MN

CAA EPA TO-17 1,1,2-Trichloroethane AIR MN

CAA EPA TO-17 1,1-Dichloroethane AIR MN

CAA EPA TO-17 1,1-Dichloroethylene AIR MN

CAA EPA TO-17 1,2,4-Trichlorobenzene AIR MN

CAA EPA TO-17 1,2,4-Trimethylbenzene AIR MN

CAA EPA TO-17 1,2-Dibromoethane (EDB, Ethylenedibromide)

AIR MN

CAA EPA TO-17 1,2-Dichlorobenzene AIR MN

CAA EPA TO-17 1,2-Dichloroethane (Ethylene dichloride) AIR MN

CAA EPA TO-17 1,2-Dichloropropane AIR MN


CAA EPA TO-17 1,3-Butadiene AIR MN



CAA EPA TO-17 1,4-Dioxane (1,4- Diethyleneoxide) AIR MN

CAA EPA TO-17 2-Butanone (Methyl ethyl ketone, MEK) AIR MN

CAA EPA TO-17 2-Hexanone AIR MN

CAA EPA TO-17 4-Ethyltoluene AIR MN

CAA EPA TO-17 4-Methyl-2-pentanone (MIBK) AIR MN

CAA EPA TO-17 Acetone AIR MN

CAA EPA TO-17 Acrolein (Propenal) AIR MN

CAA EPA TO-17 Acrylonitrile AIR MN

CAA EPA TO-17 Benzene AIR MN

CAA EPA TO-17 Benzyl chloride AIR MN

CAA EPA TO-17 Bromodichloromethane AIR MN

CAA EPA TO-17 Bromoform AIR MN

CAA EPA TO-17 Bromomethane AIR MN

CAA EPA TO-17 Carbon disulfide AIR MN

CAA EPA TO-17 Carbon tetrachloride AIR MN

CAA EPA TO-17 Chlorobenzene AIR MN

CAA EPA TO-17 Chloroethane (Ethyl chloride) AIR MN

Page 5 of 87




CAA EPA TO-17 Chloroform AIR MN

CAA EPA TO-17 cis-1,2-Dichloroethylene AIR MN

CAA EPA TO-17 cis-1,3-Dichloropropene AIR MN

CAA EPA TO-17 Cyclohexane AIR MN

CAA EPA TO-17 Dibromochloromethane AIR MN

CAA EPA TO-17 Dichlorodifluoromethane (Freon-12) AIR MN

CAA EPA TO-17 Dichlorotetrafluoroethane AIR MN

CAA EPA TO-17 Ethanol AIR MN

CAA EPA TO-17 Ethyl acetate AIR MN

CAA EPA TO-17 Ethylbenzene AIR MN

CAA EPA TO-17 Hexachloro-1,3-butadiene AIR MN

CAA EPA TO-17 Isopropyl alcohol (2-Propanol,Isopropanol)

AIR MN

CAA EPA TO-17 Isopropylbenzene AIR MN

CAA EPA TO-17 m+p-xylene AIR MN

CAA EPA TO-17 Methyl chloride (Chloromethane) AIR MN

CAA EPA TO-17 Methyl tert-butyl ether (MTBE) AIR MN

CAA EPA TO-17 Methylene chloride (Dichloromethane) AIR MN

CAA EPA TO-17 n-Butylbenzene AIR MN

CAA EPA TO-17 n-Heptane AIR MN

CAA EPA TO-17 n-Hexane AIR MN

CAA EPA TO-17 n-Propylbenzene AIR MN

CAA EPA TO-17 Naphthalene AIR MN

CAA EPA TO-17 o-Xylene AIR MN

CAA EPA TO-17 sec-Butylbenzene AIR MN

CAA EPA TO-17 Styrene AIR MN

CAA EPA TO-17 Tetrachloroethene AIR MN

CAA EPA TO-17 Tetrahydrofuran (THF) AIR MN

CAA EPA TO-17 Toluene AIR MN

CAA EPA TO-17 trans-1,2-Dichloroethylene AIR MN

CAA EPA TO-17 trans-1,3-Dichloropropylene AIR MN

CAA EPA TO-17 Trichloroethene (Trichloroethylene) AIR MN

CAA EPA TO-17 Trichlorofluoromethane(Fluorotrichloromethane, Freon 11)

AIR MN

CAA EPA TO-17 Vinyl acetate AIR MN

CAA EPA TO-17 Vinyl chloride AIR MN

Page 6 of 87



EPA TO-3 Preparation Techniques: N/A




CAA EPA TO-3 Benzene AIR MN

CAA EPA TO-3 Ethane AIR MN

CAA EPA TO-3 Ethene AIR MN

CAA EPA TO-3 Ethylbenzene AIR MN

CAA EPA TO-3 m+p-xylene AIR MN

CAA EPA TO-3 Methane AIR MN

CAA EPA TO-3 Methyl tert-butyl ether (MTBE) AIR MN

CAA EPA TO-3 n-Hexane AIR MN

CAA EPA TO-3 o-Xylene AIR MN

CAA EPA TO-3 THC as C1-C4 AIR MN

CAA EPA TO-3 THC as Gas AIR MN

CAA EPA TO-3 Toluene AIR MN

CAA EPA TO-3 Total BTEX AIR MN

CAA EPA TO-3 Xylene (total) AIR MN


CAA EPA TO-9A 1,2,3,4,6,7,8,9-Octachlorodibenzo-p-dioxin (OCDD)

AIR MN

CAA EPA TO-9A 1,2,3,4,6,7,8,9-Octachlorodibenzofuran(OCDF)

AIR MN

CAA EPA TO-9A 1,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin (1,2,3,4,6,7,8-hpcdd)

AIR MN

CAA EPA TO-9A 1,2,3,4,6,7,8-Heptachlorodibenzofuran(1,2,3,4,6,7,8-hpcdf)

AIR MN

CAA EPA TO-9A 1,2,3,4,7,8,9-Heptachlorodibenzofuran(1,2,3,4,7,8,9-hpcdf)

AIR MN

CAA EPA TO-9A 1,2,3,4,7,8-Hexachlorodibenzo-p-dioxin(1,2,3,4,7,8-Hxcdd)

AIR MN

CAA EPA TO-9A 1,2,3,4,7,8-Hexachlorodibenzofuran(1,2,3,4,7,8-Hxcdf)

AIR MN


AIR MN


AIR MN

Page 7 of 87



ASTM D516-90 Preparation Techniques: N/A

EPA 120.1 Preparation Techniques: N/A


EPA 1664A (HEM) Preparation Techniques: Extraction, separatory funnel liquid-liquid (LLE);



AIR MN


AIR MN

CAA EPA TO-9A 1,2,3,7,8-Pentachlorodibenzo-p-dioxin(1,2,3,7,8-Pecdd)

AIR MN

CAA EPA TO-9A 1,2,3,7,8-Pentachlorodibenzofuran(1,2,3,7,8-Pecdf)

AIR MN

CAA EPA TO-9A 2,3,4,6,7,8-Hexachlorodibenzofuran AIR MN

CAA EPA TO-9A 2,3,4,7,8-Pentachlorodibenzofuran AIR MN

CAA EPA TO-9A 2,3,7,8-Tetrachlorodibenzo- p-dioxin(2,3,7,8-TCDD)

AIR MN

CAA EPA TO-9A 2,3,7,8-Tetrachlorodibenzofuran AIR MN

Clean Water Program


CWP ASTM D516-90 Sulfate NPW MN


CWP EPA 120.1 Conductivity NPW MN


CWP EPA 160.4 Residue-volatile NPW MN

Page 8 of 87



EPA 1664A (SGT-HEM) Preparation Techniques: Extraction, solid phase (SPE);




EPA 350.1


CWP EPA 1664A (HEM) Oil & Grease NPW MN


CWP EPA 1664A (SGT-HEM) Oil & Grease NPW MN


CWP EPA 180.1 Turbidity NPW MN


CWP EPA 300.0 Bromide NPW MN

CWP EPA 300.0 Chloride NPW MN

CWP EPA 300.0 Fluoride NPW MN

CWP EPA 300.0 Nitrate as N NPW MN

CWP EPA 300.0 Nitrite as N NPW MN

CWP EPA 300.0 Sulfate NPW MN


CWP EPA 300.0 Bromide NPW MN

Page 9 of 87



Preparation Techniques: Distillation, MIDI;


EPA 353.2 (calc.) Preparation Techniques: N/A

EPA 410.4 Preparation Techniques: Digestion, hotplate or HotBlock;

EPA 420.4 Preparation Techniques: Distillation, MIDI;

Hach 10360 Preparation Techniques: N/A


CWP EPA 350.1 Ammonia as N NPW MN


CWP EPA 353.2 Nitrate-nitrite NPW MN

CWP EPA 353.2 Nitrite as N NPW MN


CWP EPA 353.2 (calc.) Nitrate as N NPW MN


CWP EPA 410.4 Chemical oxygen demand NPW MN


CWP EPA 420.4 Total Phenolics NPW MN

Page 10 of 87



SM 2320 B-97 Preparation Techniques: N/A




SM 2540 C-97 Preparation Techniques: N/A


CWP Hach 10360 Biochemical oxygen demand NPW MN

CWP Hach 10360 Carbonaceous BOD, CBOD NPW MN

CWP Hach 10360 Oxygen, dissolved NPW MN


CWP SM 2320 B-97 Alkalinity as CaCO3 NPW MN


CWP SM 2340 B-97 Total hardness as CaCO3 NPW MN


CWP SM 2510 B-97 Conductivity NPW MN


CWP SM 2540 B-97 Residue-total NPW MN


CWP SM 2540 C-97 Residue-filterable (TDS) NPW MN

Page 11 of 87



SM 2540 D-97 Preparation Techniques: N/A

SM 2540 F-97 Preparation Techniques: N/A

SM 4500-Cl G-93 Preparation Techniques: N/A

SM 4500-Cl¯ E-97 Preparation Techniques: N/A

SM 4500-CN¯ E-97 Preparation Techniques: Distillation, micro; Distillation, macro; Distillation, MIDI;

SM 4500-CN¯ G-97 Preparation Techniques: Distillation, micro; Distillation, macro; Distillation, MIDI;


CWP SM 2540 D-97 Residue-nonfilterable (TSS) NPW MN


CWP SM 2540 F-97 Residue-settleable NPW MN


CWP SM 4500-Cl G-93 Total residual chlorine NPW MN


CWP SM 4500-Cl¯ E-97 Chloride NPW MN


CWP SM 4500-CN¯ E-97 Total Cyanide NPW MN

Page 12 of 87



SM 4500-F¯ C-97 Preparation Techniques: N/A;

SM 4500-H+ B-96 Preparation Techniques: N/A

SM 4500-NO2¯ B-93 Preparation Techniques: N/A

SM 4500-NO3¯ H-97 Preparation Techniques: N/A

SM 4500-P E-97 Preparation Techniques: N/A


CWP SM 4500-CN¯ G-97 Free cyanide NPW MN


CWP SM 4500-F¯ C-97 Fluoride NPW MN


CWP SM 4500-H+ B-96 pH NPW MN


CWP SM 4500-NO2¯ B-93 Nitrite as N NPW MN


CWP SM 4500-NO3¯ H-97 Nitrate-nitrite NPW MN


CWP SM 4500-P E-97 Orthophosphate as P NPW MN

CWP SM 4500-P E-97 Total Phosphorus NPW MN

Page 13 of 87



SM 4500-P G-1999 Preparation Techniques: N/A

SM 5220 D-97 Preparation Techniques: Digestion, hotplate or HotBlock;



CWP SM 4500-P G-1999 Orthophosphate as P NPW MN


CWP SM 5220 D-97 Chemical oxygen demand NPW MN


CWP EPA 200.7 Aluminum NPW MN

CWP EPA 200.7 Antimony NPW MN

CWP EPA 200.7 Arsenic NPW MN

CWP EPA 200.7 Barium NPW MN

CWP EPA 200.7 Beryllium NPW MN

CWP EPA 200.7 Boron NPW MN

CWP EPA 200.7 Cadmium NPW MN

CWP EPA 200.7 Calcium NPW MN

CWP EPA 200.7 Cobalt NPW MN

CWP EPA 200.7 Copper NPW MN

CWP EPA 200.7 Iron NPW MN

CWP EPA 200.7 Lead NPW MN

CWP EPA 200.7 Magnesium NPW MN

CWP EPA 200.7 Manganese NPW MN

CWP EPA 200.7 Molybdenum NPW MN

CWP EPA 200.7 Nickel NPW MN

CWP EPA 200.7 Potassium NPW MN

CWP EPA 200.7 Selenium NPW MN

CWP EPA 200.7 Silver NPW MN

CWP EPA 200.7 Sodium NPW MN

Page 14 of 87






CWP EPA 200.7 Thallium NPW MN

CWP EPA 200.7 Tin NPW MN

CWP EPA 200.7 Titanium NPW MN

CWP EPA 200.7 Total chromium NPW MN

CWP EPA 200.7 Vanadium NPW MN

CWP EPA 200.7 Zinc NPW MN


CWP EPA 200.7 Total hardness as CaCO3 NPW MN


CWP EPA 200.8 Aluminum NPW MN

CWP EPA 200.8 Antimony NPW MN

CWP EPA 200.8 Arsenic NPW MN

CWP EPA 200.8 Barium NPW MN

CWP EPA 200.8 Beryllium NPW MN

CWP EPA 200.8 Bismuth NPW MN

CWP EPA 200.8 Boron NPW MN

CWP EPA 200.8 Cadmium NPW MN

CWP EPA 200.8 Calcium NPW MN

CWP EPA 200.8 Chromium NPW MN

CWP EPA 200.8 Cobalt NPW MN

CWP EPA 200.8 Copper NPW MN

CWP EPA 200.8 Iron NPW MN

CWP EPA 200.8 Lead NPW MN

CWP EPA 200.8 Lithium NPW MN

CWP EPA 200.8 Magnesium NPW MN

CWP EPA 200.8 Manganese NPW MN

CWP EPA 200.8 Molybdenum NPW MN

Page 15 of 87




EPA 7471B Preparation Techniques: N/A

SM 3500-Cr B-97 Preparation Techniques: N/A


CWP EPA 200.8 Nickel NPW MN

CWP EPA 200.8 Palladium NPW MN

CWP EPA 200.8 Platinum NPW MN

CWP EPA 200.8 Potassium NPW MN

CWP EPA 200.8 Selenium NPW MN

CWP EPA 200.8 Silicon NPW MN

CWP EPA 200.8 Silver NPW MN

CWP EPA 200.8 Sodium NPW MN

CWP EPA 200.8 Strontium NPW MN

CWP EPA 200.8 Thallium NPW MN

CWP EPA 200.8 Tin NPW MN

CWP EPA 200.8 Titanium NPW MN

CWP EPA 200.8 Total chromium NPW MN

CWP EPA 200.8 Uranium NPW MN

CWP EPA 200.8 Vanadium NPW MN

CWP EPA 200.8 Zinc NPW MN


CWP EPA 245.1 Mercury NPW MN


CWP EPA 7471B Mercury NPW MN User Defined S-MN-I-306 Rev. 00


CWP SM 3500-Cr B-97 Chromium VI NPW MN

Page 16 of 87



SM 3500-Fe B-2011 Preparation Techniques: N/A

SM 3500-Fe B-97 Preparation Techniques: N/A

SM 9222 B (M-Endo)-97 Preparation Techniques: N/A

SM 9222 D (m-FC)-97 Preparation Techniques: N/A

SM 9223 B (Colilert® Quanti-Tray®)-97 Preparation Techniques: N/A

EPA 1613B Preparation Techniques: Extraction, solid phase (SPE); Extraction, automated soxhlet; Extraction, separatory funnel liquid-liquid

(LLE);


CWP SM 3500-Fe B-2011 Iron NPW MN


CWP SM 3500-Fe B-97 Iron NPW MN


CWP SM 9222 B (M-Endo)-97 Total coliforms NPW MN


CWP SM 9222 D (m-FC)-97 Fecal coliforms NPW MN


CWP SM 9223 B (Colilert®Quanti-Tray®)-97

Escherichia coli NPW MN

Page 17 of 87



EPA 1668A Preparation Techniques: N/A


CWP EPA 1613B 1,2,3,4,6,7,8,9-Octachlorodibenzo-p-dioxin (OCDD)

NPW MN

CWP EPA 1613B 1,2,3,4,6,7,8,9-Octachlorodibenzofuran(OCDF)

NPW MN

CWP EPA 1613B 1,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin (1,2,3,4,6,7,8-hpcdd)

NPW MN

CWP EPA 1613B 1,2,3,4,6,7,8-Heptachlorodibenzofuran(1,2,3,4,6,7,8-hpcdf)

NPW MN

CWP EPA 1613B 1,2,3,4,7,8,9-Heptachlorodibenzofuran(1,2,3,4,7,8,9-hpcdf)

NPW MN

CWP EPA 1613B 1,2,3,4,7,8-Hexachlorodibenzo-p-dioxin(1,2,3,4,7,8-Hxcdd)

NPW MN

CWP EPA 1613B 1,2,3,4,7,8-Hexachlorodibenzofuran(1,2,3,4,7,8-Hxcdf)

NPW MN


NPW MN


NPW MN


NPW MN


NPW MN

CWP EPA 1613B 1,2,3,7,8-Pentachlorodibenzo-p-dioxin(1,2,3,7,8-Pecdd)

NPW MN

CWP EPA 1613B 1,2,3,7,8-Pentachlorodibenzofuran(1,2,3,7,8-Pecdf)

NPW MN

CWP EPA 1613B 2,3,4,6,7,8-Hexachlorodibenzofuran NPW MN

CWP EPA 1613B 2,3,4,7,8-Pentachlorodibenzofuran NPW MN

CWP EPA 1613B 2,3,7,8-Tetrachlorodibenzo- p-dioxin(2,3,7,8-TCDD)

NPW MN

CWP EPA 1613B 2,3,7,8-Tetrachlorodibenzofuran NPW MN

CWP EPA 1613B Total HpCDD NPW MN

CWP EPA 1613B Total HpCDF NPW MN

CWP EPA 1613B Total HxCDD NPW MN

CWP EPA 1613B Total HxCDF NPW MN

CWP EPA 1613B Total PeCDD NPW MN

CWP EPA 1613B Total PeCDF NPW MN

CWP EPA 1613B Total TCDD NPW MN

CWP EPA 1613B Total TCDF NPW MN

Page 18 of 87




CWP EPA 1668A 2,2',3,3',4,4',5,5',6-Nonachlorobiphenyl(BZ-206)

NPW MN

CWP EPA 1668A 2,2',3,3',4,4',5,5'-Octachlorobiphenyl(BZ-194)

NPW MN


NPW MN

CWP EPA 1668A 2,2',3,3',4,4',5,6,6'-Nonachlorobiphenyl(BZ-207)

NPW MN

CWP EPA 1668A 2,2',3,3',4,4',5,6-Octachlorobiphenyl(BZ-195)

NPW MN

CWP EPA 1668A 2,2',3,3',4,4',5-Heptachlorobiphenyl (BZ-170)

NPW MN

CWP EPA 1668A 2,2',3,3',4,5',6'-Heptachlorobiphenyl(BZ-177)

NPW MN


NPW MN


NPW MN

CWP EPA 1668A 2,2',3,3',4,5'-Hexachlorobiphenyl (BZ-130)

NPW MN

CWP EPA 1668A 2,2',3,3',4,5,5',6,6'-Nonachlorobiphenyl(BZ-208)

NPW MN

CWP EPA 1668A 2,2',3,3',4,5,5'-Heptachlorobiphenyl (BZ-172)

NPW MN


NPW MN


NPW MN


NPW MN

CWP EPA 1668A 2,2',3,3',4,6-Hexachlorobiphenyl (BZ-131)

NPW MN

CWP EPA 1668A 2,2',3,3',4-Pentachlorobiphenyl (BZ-82) NPW MN


NPW MN


NPW MN


NPW MN


NPW MN



NPW MN



NPW MN


NPW MN

Page 19 of 87





NPW MN


NPW MN

CWP EPA 1668A 2,2',3,4'-Tetrachlorobiphenyl (BZ-42) NPW MN

CWP EPA 1668A 2,2',3,4,4',5,5',6-Octachlorobiphenyl(BZ-203)

NPW MN

CWP EPA 1668A 2,2',3,4,4',5,6'-Heptachlorobiphenyl (BZ-182)

NPW MN

CWP EPA 1668A 2,2',3,4,4',5,6,6'-Octachlorobiphenyl(BZ-204)

NPW MN

CWP EPA 1668A 2,2',3,4,4',5,6-Heptachlorobiphenyl (BZ-181)

NPW MN

CWP EPA 1668A 2,2',3,4,4',5-Hexachlorobiphenyl (BZ-137)

NPW MN

CWP EPA 1668A 2,2',3,4,4',6,6'-Heptachlorobiphenyl (BZ-184)

NPW MN

CWP EPA 1668A 2,2',3,4,5',6-Hexachlorobiphenyl (BZ-144)

NPW MN

CWP EPA 1668A 2,2',3,4,5,5'-Hexachlorobiphenyl (BZ-141)

NPW MN

CWP EPA 1668A 2,2',3,4,5,6,6'-Heptachlorobiphenyl (BZ-186)

NPW MN

CWP EPA 1668A 2,2',3,4,5,6-Hexachlorobiphenyl (BZ-142)

NPW MN

CWP EPA 1668A 2,2',3,4,6'-Pentachlorobiphenyl (BZ-89) NPW MN


NPW MN





NPW MN



CWP EPA 1668A 2,2',3-Trichlorobiphenyl (BZ-16) NPW MN


NPW MN



NPW MN


CWP EPA 1668A 2,2',4,5-Tetrachlorobiphenyl (BZ-48) NPW MN



Page 20 of 87







CWP EPA 1668A 2,2'-Dichlorobiphenyl (BZ-4) NPW MN

CWP EPA 1668A 2,3',4,4',5'-Pentachlorobiphenyl (BZ-123)

NPW MN


NPW MN








CWP EPA 1668A 2,3',5'-Trichlorobiphenyl (BZ-34) NPW MN




CWP EPA 1668A 2,3,3',4',5',6-Hexachlorobiphenyl (BZ-164)

NPW MN

CWP EPA 1668A 2,3,3',4',5'-Pentachlorobiphenyl (BZ-122)

NPW MN

CWP EPA 1668A 2,3,3',4',5,5'-Hexachlorobiphenyl (BZ-162)

NPW MN

CWP EPA 1668A 2,3,3',4'-Tetrachlorobiphenyl (BZ-56) NPW MN

CWP EPA 1668A 2,3,3',4,4',5',6-Heptachlorobiphenyl (BZ-191)

NPW MN

CWP EPA 1668A 2,3,3',4,4',5,5',6-Octachlorobiphenyl(BZ-205)

NPW MN

CWP EPA 1668A 2,3,3',4,4',5,5'-Heptachlorobiphenyl (BZ-189)

NPW MN

CWP EPA 1668A 2,3,3',4,4',5,6-Heptachlorobiphenyl (BZ-190)

NPW MN

CWP EPA 1668A 2,3,3',4,4',6-Hexachlorobiphenyl (BZ-158)

NPW MN

CWP EPA 1668A 2,3,3',4,4'-Pentachlorobiphenyl (BZ-105) NPW MN


NPW MN

CWP EPA 1668A 2,3,3',4,5,5',6-Heptachlorobiphenyl (BZ-192)

NPW MN

CWP EPA 1668A 2,3,3',4,5,5'-Hexachlorobiphenyl (BZ-159)

NPW MN

Page 21 of 87




CWP EPA 1668A 2,3,3',4,5,6-Hexachlorobiphenyl (BZ-160)

NPW MN

CWP EPA 1668A 2,3,3',4,5-Pentachlorobiphenyl (BZ-106) NPW MN


CWP EPA 1668A 2,3,3',4-Tetrachlorobiphenyl (BZ-55) NPW MN

CWP EPA 1668A 2,3,3',5'-Tetrachlorobiphenyl (BZ-58) NPW MN


NPW MN

CWP EPA 1668A 2,3,3',5,5'-Pentachlorobiphenyl (BZ-111) NPW MN





CWP EPA 1668A 2,3,4'-Trichlorobiphenyl (BZ-22) NPW MN

CWP EPA 1668A 2,3,4,4',5-Pentachlorobiphenyl (BZ-114) NPW MN

CWP EPA 1668A 2,3,4,4'-Tetrachlorobiphenyl (BZ-60) NPW MN

CWP EPA 1668A 2,3,5-Trichlorobiphenyl (BZ-23) NPW MN


CWP EPA 1668A 2,3-Dichlorobiphenyl (BZ-5) NPW MN







CWP EPA 1668A 2-Chlorobiphenyl (BZ-1) NPW MN


NPW MN











Page 22 of 87





CWP EPA 1668A 3,4,4'-Trichlorobiphenyl (BZ-37) NPW MN






CWP EPA 1668A Decachlorobiphenyl (BZ-209) NPW MN

CWP EPA 1668A PCB-(100/93/102/98) NPW MN

CWP EPA 1668A PCB-(107/124) NPW MN

CWP EPA 1668A PCB-(108/119/86/97/125/87) NPW MN


CWP EPA 1668A PCB-(113/90/101) NPW MN
























Page 23 of 87



EPA 625 Preparation Techniques: Extraction, continuous liquid-liquid (LLE); Extraction, separatory funnel liquid-liquid (LLE);



CWP EPA 1668A PCB-(61/70/74/76) NPW MN





CWP EPA 625 1,2,4-Trichlorobenzene NPW MN

CWP EPA 625 2,4,5-Trichlorophenol NPW MN

CWP EPA 625 2,4,6-Trichlorophenol NPW MN

CWP EPA 625 2,4-Dichlorophenol NPW MN

CWP EPA 625 2,4-Dimethylphenol NPW MN

CWP EPA 625 2,4-Dinitrophenol NPW MN

CWP EPA 625 2,4-Dinitrotoluene (2,4-DNT) NPW MN

CWP EPA 625 2,6-Dinitrotoluene (2,6-DNT) NPW MN

CWP EPA 625 2-Chloronaphthalene NPW MN

CWP EPA 625 2-Chlorophenol NPW MN

CWP EPA 625 2-Methyl-4,6-dinitrophenol (4,6-Dinitro-2-methylphenol)

NPW MN

CWP EPA 625 2-Nitrophenol NPW MN

CWP EPA 625 3,3'-Dichlorobenzidine NPW MN

CWP EPA 625 4-Bromophenyl phenyl ether NPW MN

CWP EPA 625 4-Chloro-3-methylphenol NPW MN

CWP EPA 625 4-Chlorophenyl phenylether NPW MN

CWP EPA 625 4-Nitrophenol NPW MN

CWP EPA 625 Acenaphthene NPW MN

CWP EPA 625 Acenaphthylene NPW MN

CWP EPA 625 Anthracene NPW MN

CWP EPA 625 Benzidine NPW MN

CWP EPA 625 Benzo(a)anthracene NPW MN

CWP EPA 625 Benzo(a)pyrene NPW MN

CWP EPA 625 Benzo(g,h,i)perylene NPW MN

Page 24 of 87



EPA 624 Preparation Techniques: Purge and trap;


CWP EPA 625 Benzo(k)fluoranthene NPW MN

CWP EPA 625 Benzo[b]fluoranthene NPW MN

CWP EPA 625 bis(2-Chloroethoxy)methane NPW MN

CWP EPA 625 bis(2-Chloroethyl) ether NPW MN

CWP EPA 625 bis(2-Chloroisopropyl) ether NPW MN

CWP EPA 625 Butyl benzyl phthalate NPW MN

CWP EPA 625 Chrysene NPW MN

CWP EPA 625 Di(2-ethylhexyl) phthalate (bis(2-Ethylhexyl)phthalate, DEHP)

NPW MN

CWP EPA 625 Di-n-butyl phthalate NPW MN

CWP EPA 625 Di-n-octyl phthalate NPW MN

CWP EPA 625 Dibenz(a,h) anthracene NPW MN

CWP EPA 625 Diethyl phthalate NPW MN

CWP EPA 625 Dimethyl phthalate NPW MN

CWP EPA 625 Fluoranthene NPW MN

CWP EPA 625 Fluorene NPW MN

CWP EPA 625 Hexachlorobenzene NPW MN

CWP EPA 625 Hexachlorobutadiene NPW MN

CWP EPA 625 Hexachlorocyclopentadiene NPW MN

CWP EPA 625 Hexachloroethane NPW MN

CWP EPA 625 Indeno(1,2,3-cd) pyrene NPW MN

CWP EPA 625 Isophorone NPW MN

CWP EPA 625 n-Nitrosodi-n-propylamine NPW MN

CWP EPA 625 n-Nitrosodimethylamine NPW MN

CWP EPA 625 n-Nitrosodiphenylamine NPW MN

CWP EPA 625 Naphthalene NPW MN

CWP EPA 625 Nitrobenzene NPW MN

CWP EPA 625 Pentachlorophenol NPW MN

CWP EPA 625 Phenanthrene NPW MN

CWP EPA 625 Phenol NPW MN

CWP EPA 625 Pyrene NPW MN

Page 25 of 87




CWP EPA 624 1,1,1-Trichloroethane NPW MN

CWP EPA 624 1,1,2,2-Tetrachloroethane NPW MN

CWP EPA 624 1,1,2-Trichloroethane NPW MN

CWP EPA 624 1,1-Dichloroethane NPW MN

CWP EPA 624 1,1-Dichloroethylene NPW MN

CWP EPA 624 1,2,4-Trichlorobenzene NPW MN

CWP EPA 624 1,2-Dichlorobenzene NPW MN

CWP EPA 624 1,2-Dichloroethane (Ethylene dichloride) NPW MN

CWP EPA 624 1,2-Dichloropropane NPW MN



CWP EPA 624 2-Chloroethyl vinyl ether NPW MN

CWP EPA 624 Acrolein (Propenal) NPW MN

CWP EPA 624 Acrylonitrile NPW MN

CWP EPA 624 Benzene NPW MN

CWP EPA 624 Bromodichloromethane NPW MN

CWP EPA 624 Bromoform NPW MN

CWP EPA 624 Carbon tetrachloride NPW MN

CWP EPA 624 Chlorobenzene NPW MN

CWP EPA 624 Chlorodibromomethane NPW MN

CWP EPA 624 Chloroethane (Ethyl chloride) NPW MN

CWP EPA 624 Chloroform NPW MN

CWP EPA 624 cis-1,3-Dichloropropene NPW MN

CWP EPA 624 Ethylbenzene NPW MN

CWP EPA 624 Isopropylbenzene NPW MN

CWP EPA 624 Methyl bromide (Bromomethane) NPW MN

CWP EPA 624 Methyl chloride (Chloromethane) NPW MN

CWP EPA 624 Methylene chloride (Dichloromethane) NPW MN

CWP EPA 624 Tetrachloroethylene (Perchloroethylene) NPW MN

CWP EPA 624 Toluene NPW MN

CWP EPA 624 trans-1,2-Dichloroethylene NPW MN

CWP EPA 624 trans-1,3-Dichloropropylene NPW MN

CWP EPA 624 Trichloroethene (Trichloroethylene) NPW MN

CWP EPA 624 Trichlorofluoromethane(Fluorotrichloromethane, Freon 11)

NPW MN

CWP EPA 624 Vinyl chloride NPW MN

Page 26 of 87



MDA GD24 (Ag List 2) Preparation Techniques: Extraction, microwave; Extraction, separatory funnel liquid-liquid (LLE);

EPA 9045D Preparation Techniques: N/A


EPA 9071B

Resource Conservation Recovery Program


RCRP MDA GD24 (Ag List 2) 2,4-DB NPW MN

RCRP MDA GD24 (Ag List 2) 2,4-DB SCM MN

RCRP MDA GD24 (Ag List 2) Bentazon NPW MN

RCRP MDA GD24 (Ag List 2) Bentazon SCM MN

RCRP MDA GD24 (Ag List 2) Garlon (Triclopyr) NPW MN

RCRP MDA GD24 (Ag List 2) Garlon (Triclopyr) SCM MN

RCRP MDA GD24 (Ag List 2) MCPA NPW MN

RCRP MDA GD24 (Ag List 2) MCPA SCM MN

RCRP MDA GD24 (Ag List 2) Picloram SCM MN

RCRP MDA GD24 (Ag List 2) Picloram NPW MN


RCRP EPA 9045D pH SCM MN


RCRP EPA 9056A Bromide NPW MN

RCRP EPA 9056A Chloride NPW MN

RCRP EPA 9056A Fluoride NPW MN

RCRP EPA 9056A Nitrate NPW MN

RCRP EPA 9056A Nitrite NPW MN

RCRP EPA 9056A Sulfate NPW MN

Page 27 of 87



Preparation Techniques: N/A

EPA 6010B Preparation Techniques: Digestion, hotplate or HotBlock; Extraction, EPA 1311 TCLP, non-volatiles; Extraction, EPA 1312 SPLP,

non-volatiles;


RCRP EPA 9071B n-Hexane Extractable Material (O&G) SCM MN

RCRP EPA 9071B Oil & Grease SCM MN


RCRP EPA 6010B Aluminum NPW MN

RCRP EPA 6010B Aluminum SCM MN

RCRP EPA 6010B Antimony SCM MN

RCRP EPA 6010B Antimony NPW MN

RCRP EPA 6010B Arsenic NPW MN

RCRP EPA 6010B Arsenic SCM MN

RCRP EPA 6010B Barium SCM MN

RCRP EPA 6010B Barium NPW MN

RCRP EPA 6010B Beryllium SCM MN

RCRP EPA 6010B Beryllium NPW MN

RCRP EPA 6010B Boron SCM MN

RCRP EPA 6010B Boron NPW MN

RCRP EPA 6010B Cadmium SCM MN

RCRP EPA 6010B Cadmium NPW MN

RCRP EPA 6010B Calcium SCM MN

RCRP EPA 6010B Calcium NPW MN

RCRP EPA 6010B Chromium SCM MN

RCRP EPA 6010B Cobalt NPW MN

RCRP EPA 6010B Cobalt SCM MN

RCRP EPA 6010B Copper SCM MN

RCRP EPA 6010B Copper NPW MN

RCRP EPA 6010B Iron NPW MN

RCRP EPA 6010B Iron SCM MN

RCRP EPA 6010B Lead SCM MN

RCRP EPA 6010B Lead NPW MN

RCRP EPA 6010B Magnesium SCM MN

Page 28 of 87



EPA 6010C Preparation Techniques: Digestion, hotplate or HotBlock; Extraction, EPA 1311 TCLP, non-volatiles; Extraction, EPA 1312 SPLP,

non-volatiles;


RCRP EPA 6010B Magnesium NPW MN

RCRP EPA 6010B Manganese NPW MN

RCRP EPA 6010B Manganese SCM MN

RCRP EPA 6010B Molybdenum NPW MN

RCRP EPA 6010B Molybdenum SCM MN

RCRP EPA 6010B Nickel SCM MN

RCRP EPA 6010B Nickel NPW MN

RCRP EPA 6010B Potassium SCM MN

RCRP EPA 6010B Potassium NPW MN

RCRP EPA 6010B Selenium SCM MN

RCRP EPA 6010B Selenium NPW MN

RCRP EPA 6010B Silver NPW MN

RCRP EPA 6010B Silver SCM MN

RCRP EPA 6010B Sodium NPW MN

RCRP EPA 6010B Sodium SCM MN

RCRP EPA 6010B Thallium SCM MN

RCRP EPA 6010B Thallium NPW MN

RCRP EPA 6010B Tin SCM MN

RCRP EPA 6010B Tin NPW MN

RCRP EPA 6010B Titanium NPW MN

RCRP EPA 6010B Titanium SCM MN

RCRP EPA 6010B Total chromium NPW MN

RCRP EPA 6010B Vanadium NPW MN

RCRP EPA 6010B Vanadium SCM MN

RCRP EPA 6010B Zinc NPW MN

RCRP EPA 6010B Zinc SCM MN


RCRP EPA 6010C Aluminum SCM MN

RCRP EPA 6010C Aluminum NPW MN

RCRP EPA 6010C Antimony NPW MN

RCRP EPA 6010C Antimony SCM MN

Page 29 of 87




RCRP EPA 6010C Arsenic SCM MN

RCRP EPA 6010C Arsenic NPW MN

RCRP EPA 6010C Barium NPW MN

RCRP EPA 6010C Barium SCM MN

RCRP EPA 6010C Beryllium NPW MN

RCRP EPA 6010C Beryllium SCM MN

RCRP EPA 6010C Boron NPW MN

RCRP EPA 6010C Boron SCM MN

RCRP EPA 6010C Cadmium SCM MN

RCRP EPA 6010C Cadmium NPW MN

RCRP EPA 6010C Calcium SCM MN

RCRP EPA 6010C Calcium NPW MN

RCRP EPA 6010C Chromium NPW MN

RCRP EPA 6010C Chromium SCM MN

RCRP EPA 6010C Cobalt NPW MN

RCRP EPA 6010C Cobalt SCM MN

RCRP EPA 6010C Copper NPW MN

RCRP EPA 6010C Copper SCM MN

RCRP EPA 6010C Iron SCM MN

RCRP EPA 6010C Iron NPW MN

RCRP EPA 6010C Lead NPW MN

RCRP EPA 6010C Lead SCM MN

RCRP EPA 6010C Magnesium SCM MN

RCRP EPA 6010C Magnesium NPW MN

RCRP EPA 6010C Manganese NPW MN

RCRP EPA 6010C Manganese SCM MN

RCRP EPA 6010C Molybdenum NPW MN

RCRP EPA 6010C Molybdenum SCM MN

RCRP EPA 6010C Nickel NPW MN

RCRP EPA 6010C Nickel SCM MN

RCRP EPA 6010C Potassium NPW MN

RCRP EPA 6010C Potassium SCM MN

RCRP EPA 6010C Selenium SCM MN

RCRP EPA 6010C Selenium NPW MN

RCRP EPA 6010C Silver SCM MN

RCRP EPA 6010C Silver NPW MN

Page 30 of 87



EPA 6020 Preparation Techniques: Digestion, hotplate or HotBlock; Extraction, EPA 1311 TCLP, non-volatiles; Extraction, EPA 1312 SPLP,

non-volatiles;


RCRP EPA 6010C Sodium SCM MN

RCRP EPA 6010C Sodium NPW MN

RCRP EPA 6010C Thallium SCM MN

RCRP EPA 6010C Thallium NPW MN

RCRP EPA 6010C Tin SCM MN

RCRP EPA 6010C Tin NPW MN

RCRP EPA 6010C Titanium SCM MN

RCRP EPA 6010C Titanium NPW MN

RCRP EPA 6010C Vanadium NPW MN

RCRP EPA 6010C Vanadium SCM MN

RCRP EPA 6010C Zinc NPW MN

RCRP EPA 6010C Zinc SCM MN


RCRP EPA 6020 Aluminum SCM MN

RCRP EPA 6020 Aluminum NPW MN

RCRP EPA 6020 Antimony SCM MN

RCRP EPA 6020 Antimony NPW MN

RCRP EPA 6020 Arsenic NPW MN

RCRP EPA 6020 Arsenic SCM MN

RCRP EPA 6020 Barium SCM MN

RCRP EPA 6020 Barium NPW MN

RCRP EPA 6020 Beryllium SCM MN

RCRP EPA 6020 Beryllium NPW MN

RCRP EPA 6020 Bismuth SCM MN

RCRP EPA 6020 Bismuth NPW MN

RCRP EPA 6020 Boron NPW MN

RCRP EPA 6020 Boron SCM MN

RCRP EPA 6020 Cadmium SCM MN

RCRP EPA 6020 Cadmium NPW MN

RCRP EPA 6020 Calcium SCM MN

RCRP EPA 6020 Calcium NPW MN

Page 31 of 87




RCRP EPA 6020 Chromium SCM MN

RCRP EPA 6020 Chromium NPW MN

RCRP EPA 6020 Cobalt NPW MN

RCRP EPA 6020 Cobalt SCM MN

RCRP EPA 6020 Copper NPW MN

RCRP EPA 6020 Copper SCM MN

RCRP EPA 6020 Iron NPW MN

RCRP EPA 6020 Iron SCM MN

RCRP EPA 6020 Lead NPW MN

RCRP EPA 6020 Lead SCM MN

RCRP EPA 6020 Lithium SCM MN

RCRP EPA 6020 Lithium NPW MN

RCRP EPA 6020 Magnesium SCM MN

RCRP EPA 6020 Magnesium NPW MN

RCRP EPA 6020 Manganese NPW MN

RCRP EPA 6020 Manganese SCM MN

RCRP EPA 6020 Molybdenum SCM MN

RCRP EPA 6020 Molybdenum NPW MN

RCRP EPA 6020 Nickel SCM MN

RCRP EPA 6020 Nickel NPW MN

RCRP EPA 6020 Palladium NPW MN

RCRP EPA 6020 Platinum NPW MN

RCRP EPA 6020 Potassium SCM MN

RCRP EPA 6020 Potassium NPW MN

RCRP EPA 6020 Selenium SCM MN

RCRP EPA 6020 Selenium NPW MN

RCRP EPA 6020 Silicon NPW MN

RCRP EPA 6020 Silicon SCM MN

RCRP EPA 6020 Silver NPW MN

RCRP EPA 6020 Silver SCM MN

RCRP EPA 6020 Sodium NPW MN

RCRP EPA 6020 Sodium SCM MN

RCRP EPA 6020 Strontium SCM MN

RCRP EPA 6020 Strontium NPW MN

RCRP EPA 6020 Thallium NPW MN

RCRP EPA 6020 Thallium SCM MN

Page 32 of 87



EPA 6020A Preparation Techniques: Digestion, hotplate or HotBlock; Extraction, EPA 1311 TCLP, non-volatiles; Extraction, EPA 1312 SPLP,

non-volatiles;


RCRP EPA 6020 Tin NPW MN

RCRP EPA 6020 Tin SCM MN

RCRP EPA 6020 Titanium NPW MN

RCRP EPA 6020 Titanium SCM MN

RCRP EPA 6020 Total chromium NPW MN

RCRP EPA 6020 Uranium NPW MN

RCRP EPA 6020 Uranium SCM MN

RCRP EPA 6020 Vanadium NPW MN

RCRP EPA 6020 Vanadium SCM MN

RCRP EPA 6020 Zinc SCM MN

RCRP EPA 6020 Zinc NPW MN


RCRP EPA 6020A Aluminum NPW MN

RCRP EPA 6020A Aluminum SCM MN

RCRP EPA 6020A Antimony SCM MN

RCRP EPA 6020A Antimony NPW MN

RCRP EPA 6020A Arsenic NPW MN

RCRP EPA 6020A Arsenic SCM MN

RCRP EPA 6020A Barium NPW MN

RCRP EPA 6020A Barium SCM MN

RCRP EPA 6020A Beryllium SCM MN

RCRP EPA 6020A Beryllium NPW MN

RCRP EPA 6020A Bismuth SCM MN

RCRP EPA 6020A Bismuth NPW MN

RCRP EPA 6020A Boron NPW MN

RCRP EPA 6020A Boron SCM MN

RCRP EPA 6020A Cadmium SCM MN

RCRP EPA 6020A Cadmium NPW MN

RCRP EPA 6020A Calcium SCM MN

RCRP EPA 6020A Calcium NPW MN

RCRP EPA 6020A Chromium NPW MN

Page 33 of 87




RCRP EPA 6020A Chromium SCM MN

RCRP EPA 6020A Cobalt SCM MN

RCRP EPA 6020A Cobalt NPW MN

RCRP EPA 6020A Copper SCM MN

RCRP EPA 6020A Copper NPW MN

RCRP EPA 6020A Iron SCM MN

RCRP EPA 6020A Iron NPW MN

RCRP EPA 6020A Lead SCM MN

RCRP EPA 6020A Lead NPW MN

RCRP EPA 6020A Lithium NPW MN

RCRP EPA 6020A Lithium SCM MN

RCRP EPA 6020A Magnesium NPW MN

RCRP EPA 6020A Magnesium SCM MN

RCRP EPA 6020A Manganese NPW MN

RCRP EPA 6020A Manganese SCM MN

RCRP EPA 6020A Molybdenum NPW MN

RCRP EPA 6020A Molybdenum SCM MN

RCRP EPA 6020A Nickel SCM MN

RCRP EPA 6020A Nickel NPW MN

RCRP EPA 6020A Palladium NPW MN

RCRP EPA 6020A Platinum NPW MN

RCRP EPA 6020A Potassium NPW MN

RCRP EPA 6020A Potassium SCM MN

RCRP EPA 6020A Selenium NPW MN

RCRP EPA 6020A Selenium SCM MN

RCRP EPA 6020A Silicon SCM MN

RCRP EPA 6020A Silicon NPW MN

RCRP EPA 6020A Silver SCM MN

RCRP EPA 6020A Silver NPW MN

RCRP EPA 6020A Sodium NPW MN

RCRP EPA 6020A Sodium SCM MN

RCRP EPA 6020A Strontium SCM MN

RCRP EPA 6020A Strontium NPW MN

RCRP EPA 6020A Thallium NPW MN

RCRP EPA 6020A Thallium SCM MN

RCRP EPA 6020A Tin SCM MN

Page 34 of 87






EPA 1613B Preparation Techniques: Extraction, solid phase (SPE); Extraction, automated soxhlet; Extraction, separatory funnel liquid-liquid

(LLE);


RCRP EPA 6020A Tin NPW MN

RCRP EPA 6020A Titanium SCM MN

RCRP EPA 6020A Titanium NPW MN

RCRP EPA 6020A Uranium SCM MN

RCRP EPA 6020A Uranium NPW MN

RCRP EPA 6020A Vanadium SCM MN

RCRP EPA 6020A Vanadium NPW MN

RCRP EPA 6020A Zinc NPW MN

RCRP EPA 6020A Zinc SCM MN


RCRP EPA 7470A Mercury NPW MN


RCRP EPA 7471A Mercury SCM MN


RCRP EPA 7471B Mercury SCM MN

RCRP EPA 7471B Mercury NPW MN User Defined S-MN-I-490 Rev. 00

Page 35 of 87




RCRP EPA 1613B 1,2,3,4,6,7,8,9-Octachlorodibenzo-p-dioxin (OCDD)

TISSUE MN


SCM MN

RCRP EPA 1613B 1,2,3,4,6,7,8,9-Octachlorodibenzofuran(OCDF)

SCM MN


TISSUE MN

RCRP EPA 1613B 1,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin (1,2,3,4,6,7,8-hpcdd)

TISSUE MN


SCM MN

RCRP EPA 1613B 1,2,3,4,6,7,8-Heptachlorodibenzofuran(1,2,3,4,6,7,8-hpcdf)

SCM MN


TISSUE MN


SCM MN


TISSUE MN

RCRP EPA 1613B 1,2,3,4,7,8-Hexachlorodibenzo-p-dioxin(1,2,3,4,7,8-Hxcdd)

SCM MN


TISSUE MN

RCRP EPA 1613B 1,2,3,4,7,8-Hexachlorodibenzofuran(1,2,3,4,7,8-Hxcdf)

SCM MN


TISSUE MN


SCM MN


TISSUE MN


TISSUE MN


SCM MN


TISSUE MN


SCM MN


SCM MN


TISSUE MN

RCRP EPA 1613B 1,2,3,7,8-Pentachlorodibenzo-p-dioxin(1,2,3,7,8-Pecdd)

TISSUE MN


SCM MN

RCRP EPA 1613B 1,2,3,7,8-Pentachlorodibenzofuran(1,2,3,7,8-Pecdf)

SCM MN

Page 36 of 87






TISSUE MN

RCRP EPA 1613B 2,3,4,6,7,8-Hexachlorodibenzofuran SCM MN

RCRP EPA 1613B 2,3,4,6,7,8-Hexachlorodibenzofuran TISSUE MN

RCRP EPA 1613B 2,3,4,7,8-Pentachlorodibenzofuran TISSUE MN

RCRP EPA 1613B 2,3,4,7,8-Pentachlorodibenzofuran SCM MN

RCRP EPA 1613B 2,3,7,8-Tetrachlorodibenzo- p-dioxin(2,3,7,8-TCDD)

TISSUE MN


SCM MN

RCRP EPA 1613B 2,3,7,8-Tetrachlorodibenzofuran SCM MN

RCRP EPA 1613B 2,3,7,8-Tetrachlorodibenzofuran TISSUE MN

RCRP EPA 1613B Total HpCDD TISSUE MN

RCRP EPA 1613B Total HpCDD SCM MN

RCRP EPA 1613B Total HpCDF TISSUE MN

RCRP EPA 1613B Total HpCDF SCM MN

RCRP EPA 1613B Total HxCDD SCM MN

RCRP EPA 1613B Total HxCDD TISSUE MN

RCRP EPA 1613B Total HxCDF TISSUE MN

RCRP EPA 1613B Total HxCDF SCM MN

RCRP EPA 1613B Total PeCDD SCM MN

RCRP EPA 1613B Total PeCDD TISSUE MN

RCRP EPA 1613B Total PeCDF TISSUE MN

RCRP EPA 1613B Total PeCDF SCM MN

RCRP EPA 1613B Total TCDD SCM MN

RCRP EPA 1613B Total TCDD TISSUE MN

RCRP EPA 1613B Total TCDF TISSUE MN

RCRP EPA 1613B Total TCDF SCM MN


RCRP EPA 1668A 2,2',3,3',4,4',5,5',6-Nonachlorobiphenyl(BZ-206)

SCM MN

RCRP EPA 1668A 2,2',3,3',4,4',5,5',6-Nonachlorobiphenyl(BZ-206)

TISSUE MN

RCRP EPA 1668A 2,2',3,3',4,4',5,5'-Octachlorobiphenyl(BZ-194)

TISSUE MN

Page 37 of 87





SCM MN


TISSUE MN


SCM MN

RCRP EPA 1668A 2,2',3,3',4,4',5,6,6'-Nonachlorobiphenyl(BZ-207)

SCM MN

RCRP EPA 1668A 2,2',3,3',4,4',5,6,6'-Nonachlorobiphenyl(BZ-207)

TISSUE MN

RCRP EPA 1668A 2,2',3,3',4,4',5,6-Octachlorobiphenyl(BZ-195)

SCM MN

RCRP EPA 1668A 2,2',3,3',4,4',5,6-Octachlorobiphenyl(BZ-195)

TISSUE MN

RCRP EPA 1668A 2,2',3,3',4,4',5-Heptachlorobiphenyl (BZ-170)

SCM MN


TISSUE MN

RCRP EPA 1668A 2,2',3,3',4,5',6'-Heptachlorobiphenyl(BZ-177)

TISSUE MN

RCRP EPA 1668A 2,2',3,3',4,5',6'-Heptachlorobiphenyl(BZ-177)

SCM MN


TISSUE MN


SCM MN


SCM MN


TISSUE MN

RCRP EPA 1668A 2,2',3,3',4,5'-Hexachlorobiphenyl (BZ-130)

SCM MN


TISSUE MN

RCRP EPA 1668A 2,2',3,3',4,5,5',6,6'-Nonachlorobiphenyl(BZ-208)

TISSUE MN

RCRP EPA 1668A 2,2',3,3',4,5,5',6,6'-Nonachlorobiphenyl(BZ-208)

SCM MN

RCRP EPA 1668A 2,2',3,3',4,5,5'-Heptachlorobiphenyl (BZ-172)

TISSUE MN


SCM MN


SCM MN


TISSUE MN


SCM MN


TISSUE MN

Page 38 of 87





TISSUE MN


SCM MN

RCRP EPA 1668A 2,2',3,3',4,6-Hexachlorobiphenyl (BZ-131)

SCM MN

RCRP EPA 1668A 2,2',3,3',4,6-Hexachlorobiphenyl (BZ-131)

TISSUE MN

RCRP EPA 1668A 2,2',3,3',4-Pentachlorobiphenyl (BZ-82) TISSUE MN

RCRP EPA 1668A 2,2',3,3',4-Pentachlorobiphenyl (BZ-82) SCM MN


SCM MN


TISSUE MN


SCM MN


TISSUE MN


SCM MN


TISSUE MN


TISSUE MN


SCM MN




SCM MN


TISSUE MN




TISSUE MN


SCM MN


TISSUE MN


SCM MN


TISSUE MN


SCM MN


SCM MN

Page 39 of 87





TISSUE MN

RCRP EPA 1668A 2,2',3,4'-Tetrachlorobiphenyl (BZ-42) SCM MN

RCRP EPA 1668A 2,2',3,4'-Tetrachlorobiphenyl (BZ-42) TISSUE MN

RCRP EPA 1668A 2,2',3,4,4',5,5',6-Octachlorobiphenyl(BZ-203)

SCM MN

RCRP EPA 1668A 2,2',3,4,4',5,5',6-Octachlorobiphenyl(BZ-203)

TISSUE MN

RCRP EPA 1668A 2,2',3,4,4',5,6'-Heptachlorobiphenyl (BZ-182)

TISSUE MN


SCM MN

RCRP EPA 1668A 2,2',3,4,4',5,6,6'-Octachlorobiphenyl(BZ-204)

TISSUE MN

RCRP EPA 1668A 2,2',3,4,4',5,6,6'-Octachlorobiphenyl(BZ-204)

SCM MN

RCRP EPA 1668A 2,2',3,4,4',5,6-Heptachlorobiphenyl (BZ-181)

SCM MN

RCRP EPA 1668A 2,2',3,4,4',5,6-Heptachlorobiphenyl (BZ-181)

TISSUE MN

RCRP EPA 1668A 2,2',3,4,4',5-Hexachlorobiphenyl (BZ-137)

TISSUE MN


SCM MN


SCM MN


TISSUE MN


SCM MN


TISSUE MN

RCRP EPA 1668A 2,2',3,4,5,5'-Hexachlorobiphenyl (BZ-141)

SCM MN


TISSUE MN

RCRP EPA 1668A 2,2',3,4,5,6,6'-Heptachlorobiphenyl (BZ-186)

SCM MN

RCRP EPA 1668A 2,2',3,4,5,6,6'-Heptachlorobiphenyl (BZ-186)

TISSUE MN

RCRP EPA 1668A 2,2',3,4,5,6-Hexachlorobiphenyl (BZ-142)

TISSUE MN

RCRP EPA 1668A 2,2',3,4,5,6-Hexachlorobiphenyl (BZ-142)

SCM MN

RCRP EPA 1668A 2,2',3,4,6'-Pentachlorobiphenyl (BZ-89) TISSUE MN

RCRP EPA 1668A 2,2',3,4,6'-Pentachlorobiphenyl (BZ-89) SCM MN


SCM MN

Page 40 of 87





TISSUE MN








TISSUE MN


SCM MN





RCRP EPA 1668A 2,2',3-Trichlorobiphenyl (BZ-16) TISSUE MN

RCRP EPA 1668A 2,2',3-Trichlorobiphenyl (BZ-16) SCM MN


SCM MN


TISSUE MN




TISSUE MN


SCM MN



RCRP EPA 1668A 2,2',4,5-Tetrachlorobiphenyl (BZ-48) TISSUE MN

RCRP EPA 1668A 2,2',4,5-Tetrachlorobiphenyl (BZ-48) SCM MN









Page 41 of 87






RCRP EPA 1668A 2,2'-Dichlorobiphenyl (BZ-4) TISSUE MN

RCRP EPA 1668A 2,2'-Dichlorobiphenyl (BZ-4) SCM MN

RCRP EPA 1668A 2,3',4,4',5'-Pentachlorobiphenyl (BZ-123)

TISSUE MN


NPW MN


SCM MN


SCM MN


NPW MN


TISSUE MN


RCRP EPA 1668A 2,3',4,4',5-Pentachlorobiphenyl (BZ-118) NPW MN














RCRP EPA 1668A 2,3',5'-Trichlorobiphenyl (BZ-34) SCM MN

RCRP EPA 1668A 2,3',5'-Trichlorobiphenyl (BZ-34) TISSUE MN







Page 42 of 87




RCRP EPA 1668A 2,3,3',4',5',6-Hexachlorobiphenyl (BZ-164)

SCM MN

RCRP EPA 1668A 2,3,3',4',5',6-Hexachlorobiphenyl (BZ-164)

TISSUE MN

RCRP EPA 1668A 2,3,3',4',5'-Pentachlorobiphenyl (BZ-122)

SCM MN

RCRP EPA 1668A 2,3,3',4',5'-Pentachlorobiphenyl (BZ-122)

TISSUE MN

RCRP EPA 1668A 2,3,3',4',5,5'-Hexachlorobiphenyl (BZ-162)

TISSUE MN

RCRP EPA 1668A 2,3,3',4',5,5'-Hexachlorobiphenyl (BZ-162)

SCM MN

RCRP EPA 1668A 2,3,3',4'-Tetrachlorobiphenyl (BZ-56) SCM MN

RCRP EPA 1668A 2,3,3',4'-Tetrachlorobiphenyl (BZ-56) TISSUE MN

RCRP EPA 1668A 2,3,3',4,4',5',6-Heptachlorobiphenyl (BZ-191)

SCM MN

RCRP EPA 1668A 2,3,3',4,4',5',6-Heptachlorobiphenyl (BZ-191)

TISSUE MN

RCRP EPA 1668A 2,3,3',4,4',5'-Hexachlorobiphenyl (BZ-157)

NPW MN

RCRP EPA 1668A 2,3,3',4,4',5'-Hexachlorobiphenyl (BZ-157)

SCM MN

RCRP EPA 1668A 2,3,3',4,4',5,5',6-Octachlorobiphenyl(BZ-205)

TISSUE MN

RCRP EPA 1668A 2,3,3',4,4',5,5',6-Octachlorobiphenyl(BZ-205)

SCM MN

RCRP EPA 1668A 2,3,3',4,4',5,5'-Heptachlorobiphenyl (BZ-189)

NPW MN


TISSUE MN


SCM MN

RCRP EPA 1668A 2,3,3',4,4',5,6-Heptachlorobiphenyl (BZ-190)

SCM MN

RCRP EPA 1668A 2,3,3',4,4',5,6-Heptachlorobiphenyl (BZ-190)

TISSUE MN

RCRP EPA 1668A 2,3,3',4,4',5-Hexachlorobiphenyl (BZ-156)

SCM MN


NPW MN


TISSUE MN


SCM MN

RCRP EPA 1668A 2,3,3',4,4'-Pentachlorobiphenyl (BZ-105) NPW MN

RCRP EPA 1668A 2,3,3',4,4'-Pentachlorobiphenyl (BZ-105) TISSUE MN

RCRP EPA 1668A 2,3,3',4,4'-Pentachlorobiphenyl (BZ-105) SCM MN

Page 43 of 87





TISSUE MN


SCM MN

RCRP EPA 1668A 2,3,3',4,5,5',6-Heptachlorobiphenyl (BZ-192)

SCM MN

RCRP EPA 1668A 2,3,3',4,5,5',6-Heptachlorobiphenyl (BZ-192)

TISSUE MN

RCRP EPA 1668A 2,3,3',4,5,5'-Hexachlorobiphenyl (BZ-159)

SCM MN

RCRP EPA 1668A 2,3,3',4,5,5'-Hexachlorobiphenyl (BZ-159)

TISSUE MN

RCRP EPA 1668A 2,3,3',4,5,6-Hexachlorobiphenyl (BZ-160)

SCM MN

RCRP EPA 1668A 2,3,3',4,5,6-Hexachlorobiphenyl (BZ-160)

TISSUE MN

RCRP EPA 1668A 2,3,3',4,5-Pentachlorobiphenyl (BZ-106) SCM MN

RCRP EPA 1668A 2,3,3',4,5-Pentachlorobiphenyl (BZ-106) TISSUE MN



RCRP EPA 1668A 2,3,3',4-Tetrachlorobiphenyl (BZ-55) SCM MN

RCRP EPA 1668A 2,3,3',4-Tetrachlorobiphenyl (BZ-55) TISSUE MN

RCRP EPA 1668A 2,3,3',5'-Tetrachlorobiphenyl (BZ-58) TISSUE MN

RCRP EPA 1668A 2,3,3',5'-Tetrachlorobiphenyl (BZ-58) SCM MN


SCM MN


TISSUE MN

RCRP EPA 1668A 2,3,3',5,5'-Pentachlorobiphenyl (BZ-111) TISSUE MN

RCRP EPA 1668A 2,3,3',5,5'-Pentachlorobiphenyl (BZ-111) SCM MN









RCRP EPA 1668A 2,3,4'-Trichlorobiphenyl (BZ-22) SCM MN

RCRP EPA 1668A 2,3,4'-Trichlorobiphenyl (BZ-22) TISSUE MN

RCRP EPA 1668A 2,3,4,4',5-Pentachlorobiphenyl (BZ-114) SCM MN

RCRP EPA 1668A 2,3,4,4',5-Pentachlorobiphenyl (BZ-114) NPW MN

Page 44 of 87




RCRP EPA 1668A 2,3,4,4',5-Pentachlorobiphenyl (BZ-114) TISSUE MN

RCRP EPA 1668A 2,3,4,4'-Tetrachlorobiphenyl (BZ-60) SCM MN

RCRP EPA 1668A 2,3,4,4'-Tetrachlorobiphenyl (BZ-60) TISSUE MN

RCRP EPA 1668A 2,3,5-Trichlorobiphenyl (BZ-23) SCM MN

RCRP EPA 1668A 2,3,5-Trichlorobiphenyl (BZ-23) TISSUE MN



RCRP EPA 1668A 2,3-Dichlorobiphenyl (BZ-5) SCM MN

RCRP EPA 1668A 2,3-Dichlorobiphenyl (BZ-5) TISSUE MN













RCRP EPA 1668A 2-Chlorobiphenyl (BZ-1) SCM MN

RCRP EPA 1668A 2-Chlorobiphenyl (BZ-1) TISSUE MN


TISSUE MN


SCM MN


NPW MN

RCRP EPA 1668A 3,3',4,4',5-Pentachlorobiphenyl (BZ-126) NPW MN



RCRP EPA 1668A 3,3',4,4'-Tetrachlorobiphenyl (BZ-77) NPW MN






Page 45 of 87


















RCRP EPA 1668A 3,4,4',5-Tetrachlorobiphenyl (BZ-81) NPW MN


RCRP EPA 1668A 3,4,4'-Trichlorobiphenyl (BZ-37) TISSUE MN

RCRP EPA 1668A 3,4,4'-Trichlorobiphenyl (BZ-37) SCM MN











RCRP EPA 1668A Decachlorobiphenyl (BZ-209) SCM MN

RCRP EPA 1668A Decachlorobiphenyl (BZ-209) TISSUE MN

RCRP EPA 1668A PCB-(100/93/102/98) SCM MN

RCRP EPA 1668A PCB-(100/93/102/98) TISSUE MN

RCRP EPA 1668A PCB-(107/124) SCM MN

RCRP EPA 1668A PCB-(107/124) TISSUE MN

RCRP EPA 1668A PCB-(108/119/86/97/125/87) TISSUE MN

RCRP EPA 1668A PCB-(108/119/86/97/125/87) SCM MN

Page 46 of 87






RCRP EPA 1668A PCB-(113/90/101) TISSUE MN

RCRP EPA 1668A PCB-(113/90/101) SCM MN

































Page 47 of 87



EPA 1668C Preparation Techniques: N/A


















RCRP EPA 1668A PCB-(61/70/74/76) TISSUE MN

RCRP EPA 1668A PCB-(61/70/74/76) SCM MN








RCRP EPA 1668C 2,3',5',6-Tetrachlorobiphenyl (BZ-73) TISSUE MN

RCRP EPA 1668C 2,3',5',6-Tetrachlorobiphenyl (BZ-73) NPW MN

RCRP EPA 1668C 2,3',5',6-Tetrachlorobiphenyl (BZ-73) SCM MN

RCRP EPA 1668C PCB-(100/93/102/98) TISSUE MN

RCRP EPA 1668C PCB-(100/93/102/98) SCM MN

RCRP EPA 1668C PCB-(107/124) NPW MN

Page 48 of 87




RCRP EPA 1668C PCB-(107/124) SCM MN

RCRP EPA 1668C PCB-(107/124) TISSUE MN

RCRP EPA 1668C PCB-(108/119/86/97/125/87) SCM MN

RCRP EPA 1668C PCB-(108/119/86/97/125/87) TISSUE MN




RCRP EPA 1668C PCB-(113/90/101) SCM MN

RCRP EPA 1668C PCB-(113/90/101) NPW MN

RCRP EPA 1668C PCB-(113/90/101) TISSUE MN



























Page 49 of 87








































Page 50 of 87



EPA 8011 Preparation Techniques: Extraction, continuous liquid-liquid (LLE);

EPA 8081B Preparation Techniques: Extraction, ultrasonic; Extraction, separatory funnel liquid-liquid (LLE);












RCRP EPA 1668C PCB-(61/70/74/76) SCM MN

RCRP EPA 1668C PCB-(61/70/74/76) NPW MN

RCRP EPA 1668C PCB-(61/70/74/76) TISSUE MN








RCRP EPA 8011 1,2-Dibromo-3-chloropropane (DBCP) NPW MN

RCRP EPA 8011 1,2-Dibromoethane (EDB, Ethylenedibromide)

NPW MN


RCRP EPA 8081B 4,4'-DDD SCM MN

RCRP EPA 8081B 4,4'-DDD NPW MN

RCRP EPA 8081B 4,4'-DDE SCM MN

Page 51 of 87




RCRP EPA 8081B 4,4'-DDE NPW MN

RCRP EPA 8081B 4,4'-DDT NPW MN

RCRP EPA 8081B 4,4'-DDT SCM MN

RCRP EPA 8081B Aldrin NPW MN

RCRP EPA 8081B Aldrin SCM MN

RCRP EPA 8081B alpha-BHC (alpha-Hexachlorocyclohexane)

SCM MN

RCRP EPA 8081B alpha-BHC (alpha-Hexachlorocyclohexane)

NPW MN

RCRP EPA 8081B alpha-Chlordane NPW MN

RCRP EPA 8081B alpha-Chlordane SCM MN

RCRP EPA 8081B beta-BHC (beta-Hexachlorocyclohexane) NPW MN

RCRP EPA 8081B beta-BHC (beta-Hexachlorocyclohexane) SCM MN

RCRP EPA 8081B Chlordane (tech.) NPW MN

RCRP EPA 8081B Chlordane (tech.) SCM MN

RCRP EPA 8081B delta-BHC NPW MN

RCRP EPA 8081B delta-BHC SCM MN

RCRP EPA 8081B Dieldrin SCM MN

RCRP EPA 8081B Dieldrin NPW MN

RCRP EPA 8081B Endosulfan I SCM MN

RCRP EPA 8081B Endosulfan I NPW MN

RCRP EPA 8081B Endosulfan II NPW MN

RCRP EPA 8081B Endosulfan II SCM MN

RCRP EPA 8081B Endosulfan sulfate SCM MN

RCRP EPA 8081B Endosulfan sulfate NPW MN

RCRP EPA 8081B Endrin SCM MN

RCRP EPA 8081B Endrin NPW MN

RCRP EPA 8081B Endrin aldehyde SCM MN

RCRP EPA 8081B Endrin aldehyde NPW MN

RCRP EPA 8081B Endrin ketone SCM MN

RCRP EPA 8081B Endrin ketone NPW MN

RCRP EPA 8081B gamma-BHC (Lindane, gamma-HexachlorocyclohexanE)

SCM MN

RCRP EPA 8081B gamma-BHC (Lindane, gamma-HexachlorocyclohexanE)

NPW MN

RCRP EPA 8081B gamma-Chlordane NPW MN

RCRP EPA 8081B gamma-Chlordane SCM MN

RCRP EPA 8081B Heptachlor SCM MN

Page 52 of 87



EPA 8082 Preparation Techniques: Extraction, microwave; Extraction, ultrasonic; Extraction, soxhlet; Extraction, separatory funnel liquid-liquid

(LLE);

EPA 8082A Preparation Techniques: Extraction, microwave; Extraction, ultrasonic; Extraction, soxhlet; Extraction, separatory funnel liquid-liquid

(LLE);


RCRP EPA 8081B Heptachlor NPW MN

RCRP EPA 8081B Heptachlor epoxide NPW MN

RCRP EPA 8081B Heptachlor epoxide SCM MN

RCRP EPA 8081B Isodrin NPW MN

RCRP EPA 8081B Isodrin SCM MN

RCRP EPA 8081B Methoxychlor SCM MN

RCRP EPA 8081B Methoxychlor NPW MN

RCRP EPA 8081B Toxaphene (Chlorinated camphene) SCM MN

RCRP EPA 8081B Toxaphene (Chlorinated camphene) NPW MN


RCRP EPA 8082 Aroclor-1016 (PCB-1016) NPW MN

RCRP EPA 8082 Aroclor-1016 (PCB-1016) SCM MN













RCRP EPA 8082 PCBs SCM MN

Page 53 of 87



EPA 8270C Preparation Techniques: Extraction, ultrasonic; Extraction, continuous liquid-liquid (LLE); Extraction, EPA 1311 TCLP, non-

volatiles; Extraction, soxhlet; Extraction, separatory funnel liquid-liquid (LLE); Extraction, EPA 1312 SPLP, non-volatiles;


RCRP EPA 8082A Aroclor-1016 (PCB-1016) SCM MN

RCRP EPA 8082A Aroclor-1016 (PCB-1016) NPW MN














RCRP EPA 8270C 1,2,4-Trichlorobenzene SCM MN

RCRP EPA 8270C 1,2,4-Trichlorobenzene NPW MN

RCRP EPA 8270C 1,2-Dichlorobenzene NPW MN

RCRP EPA 8270C 1,2-Dichlorobenzene SCM MN

RCRP EPA 8270C 1,2-Diphenylhydrazine NPW MN

RCRP EPA 8270C 1,2-Diphenylhydrazine SCM MN





RCRP EPA 8270C 2,4,5-Trichlorophenol NPW MN

RCRP EPA 8270C 2,4,5-Trichlorophenol SCM MN

RCRP EPA 8270C 2,4,6-Trichlorophenol SCM MN

RCRP EPA 8270C 2,4,6-Trichlorophenol NPW MN

RCRP EPA 8270C 2,4-Dichlorophenol SCM MN

Page 54 of 87




RCRP EPA 8270C 2,4-Dichlorophenol NPW MN

RCRP EPA 8270C 2,4-Dimethylphenol SCM MN

RCRP EPA 8270C 2,4-Dimethylphenol NPW MN

RCRP EPA 8270C 2,4-Dinitrophenol SCM MN

RCRP EPA 8270C 2,4-Dinitrophenol NPW MN

RCRP EPA 8270C 2,4-Dinitrotoluene (2,4-DNT) NPW MN

RCRP EPA 8270C 2,4-Dinitrotoluene (2,4-DNT) SCM MN

RCRP EPA 8270C 2,6-Dinitrotoluene (2,6-DNT) NPW MN

RCRP EPA 8270C 2,6-Dinitrotoluene (2,6-DNT) SCM MN

RCRP EPA 8270C 2-Chloronaphthalene NPW MN

RCRP EPA 8270C 2-Chloronaphthalene SCM MN

RCRP EPA 8270C 2-Chlorophenol SCM MN

RCRP EPA 8270C 2-Chlorophenol NPW MN

RCRP EPA 8270C 2-Methyl-4,6-dinitrophenol (4,6-Dinitro-2-methylphenol)

SCM MN

RCRP EPA 8270C 2-Methyl-4,6-dinitrophenol (4,6-Dinitro-2-methylphenol)

NPW MN

RCRP EPA 8270C 2-Methylnaphthalene NPW MN

RCRP EPA 8270C 2-Methylnaphthalene SCM MN

RCRP EPA 8270C 2-Methylphenol (o-Cresol) SCM MN

RCRP EPA 8270C 2-Methylphenol (o-Cresol) NPW MN

RCRP EPA 8270C 2-Nitroaniline SCM MN

RCRP EPA 8270C 2-Nitroaniline NPW MN

RCRP EPA 8270C 2-Nitrophenol SCM MN

RCRP EPA 8270C 2-Nitrophenol NPW MN

RCRP EPA 8270C 3,3'-Dichlorobenzidine NPW MN

RCRP EPA 8270C 3,3'-Dichlorobenzidine SCM MN

RCRP EPA 8270C 3-Methylphenol (m-Cresol) NPW MN

RCRP EPA 8270C 3-Methylphenol (m-Cresol) SCM MN



RCRP EPA 8270C 4-Bromophenyl phenyl ether NPW MN

RCRP EPA 8270C 4-Bromophenyl phenyl ether SCM MN

RCRP EPA 8270C 4-Chloro-3-methylphenol NPW MN

RCRP EPA 8270C 4-Chloro-3-methylphenol SCM MN

RCRP EPA 8270C 4-Chloroaniline NPW MN

RCRP EPA 8270C 4-Chloroaniline SCM MN

Page 55 of 87




RCRP EPA 8270C 4-Chlorophenyl phenylether SCM MN

RCRP EPA 8270C 4-Chlorophenyl phenylether NPW MN

RCRP EPA 8270C 4-Methylphenol (p-Cresol) NPW MN

RCRP EPA 8270C 4-Methylphenol (p-Cresol) SCM MN



RCRP EPA 8270C 4-Nitrophenol NPW MN

RCRP EPA 8270C 4-Nitrophenol SCM MN

RCRP EPA 8270C Acenaphthene SCM MN

RCRP EPA 8270C Acenaphthene NPW MN

RCRP EPA 8270C Acenaphthylene SCM MN

RCRP EPA 8270C Acenaphthylene NPW MN

RCRP EPA 8270C Anthracene SCM MN

RCRP EPA 8270C Anthracene NPW MN

RCRP EPA 8270C Benzidine NPW MN

RCRP EPA 8270C Benzidine SCM MN

RCRP EPA 8270C Benzo(a)anthracene NPW MN

RCRP EPA 8270C Benzo(a)anthracene SCM MN

RCRP EPA 8270C Benzo(a)pyrene NPW MN

RCRP EPA 8270C Benzo(a)pyrene SCM MN

RCRP EPA 8270C Benzo(g,h,i)perylene SCM MN

RCRP EPA 8270C Benzo(g,h,i)perylene NPW MN

RCRP EPA 8270C Benzo(k)fluoranthene SCM MN

RCRP EPA 8270C Benzo(k)fluoranthene NPW MN

RCRP EPA 8270C Benzo[b]fluoranthene SCM MN

RCRP EPA 8270C Benzo[b]fluoranthene NPW MN

RCRP EPA 8270C Benzoic acid NPW MN

RCRP EPA 8270C Benzoic acid SCM MN

RCRP EPA 8270C Benzyl alcohol NPW MN

RCRP EPA 8270C Benzyl alcohol SCM MN

RCRP EPA 8270C bis(2-Chloroethoxy)methane SCM MN

RCRP EPA 8270C bis(2-Chloroethoxy)methane NPW MN

RCRP EPA 8270C bis(2-Chloroethyl) ether NPW MN

RCRP EPA 8270C bis(2-Chloroethyl) ether SCM MN

RCRP EPA 8270C bis(2-Chloroisopropyl) ether NPW MN

RCRP EPA 8270C bis(2-Chloroisopropyl) ether SCM MN

Page 56 of 87




RCRP EPA 8270C Butyl benzyl phthalate SCM MN

RCRP EPA 8270C Butyl benzyl phthalate NPW MN

RCRP EPA 8270C Chrysene SCM MN

RCRP EPA 8270C Chrysene NPW MN

RCRP EPA 8270C Di(2-ethylhexyl) phthalate (bis(2-Ethylhexyl)phthalate, DEHP)

NPW MN

RCRP EPA 8270C Di(2-ethylhexyl) phthalate (bis(2-Ethylhexyl)phthalate, DEHP)

SCM MN

RCRP EPA 8270C Di-n-butyl phthalate NPW MN

RCRP EPA 8270C Di-n-butyl phthalate SCM MN

RCRP EPA 8270C Di-n-octyl phthalate SCM MN

RCRP EPA 8270C Di-n-octyl phthalate NPW MN

RCRP EPA 8270C Dibenz(a,h) anthracene SCM MN

RCRP EPA 8270C Dibenz(a,h) anthracene NPW MN

RCRP EPA 8270C Dibenzofuran NPW MN

RCRP EPA 8270C Dibenzofuran SCM MN

RCRP EPA 8270C Diethyl phthalate SCM MN

RCRP EPA 8270C Diethyl phthalate NPW MN

RCRP EPA 8270C Dimethyl phthalate SCM MN

RCRP EPA 8270C Dimethyl phthalate NPW MN

RCRP EPA 8270C Fluoranthene NPW MN

RCRP EPA 8270C Fluoranthene SCM MN

RCRP EPA 8270C Fluorene NPW MN

RCRP EPA 8270C Fluorene SCM MN

RCRP EPA 8270C Hexachlorobenzene NPW MN

RCRP EPA 8270C Hexachlorobenzene SCM MN

RCRP EPA 8270C Hexachlorobutadiene NPW MN

RCRP EPA 8270C Hexachlorobutadiene SCM MN

RCRP EPA 8270C Hexachlorocyclopentadiene SCM MN

RCRP EPA 8270C Hexachlorocyclopentadiene NPW MN

RCRP EPA 8270C Hexachloroethane NPW MN

RCRP EPA 8270C Hexachloroethane SCM MN

RCRP EPA 8270C Indeno(1,2,3-cd) pyrene NPW MN

RCRP EPA 8270C Indeno(1,2,3-cd) pyrene SCM MN

RCRP EPA 8270C Isophorone NPW MN

RCRP EPA 8270C Isophorone SCM MN

RCRP EPA 8270C n-Nitrosodi-n-propylamine SCM MN

Page 57 of 87



EPA 8270C SIM Preparation Techniques: Extraction, microwave; Extraction, ultrasonic; Extraction, soxhlet; Extraction, separatory funnel liquid-liquid

(LLE);


RCRP EPA 8270C n-Nitrosodi-n-propylamine NPW MN

RCRP EPA 8270C n-Nitrosodimethylamine SCM MN

RCRP EPA 8270C n-Nitrosodimethylamine NPW MN

RCRP EPA 8270C n-Nitrosodiphenylamine SCM MN

RCRP EPA 8270C n-Nitrosodiphenylamine NPW MN

RCRP EPA 8270C Naphthalene SCM MN

RCRP EPA 8270C Naphthalene NPW MN

RCRP EPA 8270C Nitrobenzene SCM MN

RCRP EPA 8270C Nitrobenzene NPW MN

RCRP EPA 8270C Pentachlorophenol NPW MN

RCRP EPA 8270C Pentachlorophenol SCM MN

RCRP EPA 8270C Phenanthrene NPW MN

RCRP EPA 8270C Phenanthrene SCM MN

RCRP EPA 8270C Phenol SCM MN

RCRP EPA 8270C Phenol NPW MN

RCRP EPA 8270C Pyrene SCM MN

RCRP EPA 8270C Pyrene NPW MN

RCRP EPA 8270C Pyridine NPW MN

RCRP EPA 8270C Pyridine SCM MN


RCRP EPA 8270C SIM Benzo(a)anthracene NPW MN

RCRP EPA 8270C SIM Benzo(a)anthracene SCM MN

RCRP EPA 8270C SIM Benzo(a)pyrene NPW MN

RCRP EPA 8270C SIM Benzo(a)pyrene SCM MN

RCRP EPA 8270C SIM Benzo(j)fluoranthene SCM MN

RCRP EPA 8270C SIM Benzo(j)fluoranthene NPW MN

RCRP EPA 8270C SIM Benzo(k)fluoranthene NPW MN

RCRP EPA 8270C SIM Benzo(k)fluoranthene SCM MN

RCRP EPA 8270C SIM Benzo[b]fluoranthene SCM MN

RCRP EPA 8270C SIM Benzo[b]fluoranthene NPW MN

RCRP EPA 8270C SIM Dibenz(a,h) anthracene NPW MN

Page 58 of 87



EPA 8270D Preparation Techniques: Extraction, ultrasonic; Extraction, continuous liquid-liquid (LLE); Extraction, EPA 1311 TCLP, non-

volatiles; Extraction, soxhlet; Extraction, separatory funnel liquid-liquid (LLE); Extraction, EPA 1312 SPLP, non-volatiles;


RCRP EPA 8270C SIM Dibenz(a,h) anthracene SCM MN

RCRP EPA 8270C SIM Fluoranthene SCM MN

RCRP EPA 8270C SIM Fluoranthene NPW MN

RCRP EPA 8270C SIM Indeno(1,2,3-cd) pyrene NPW MN

RCRP EPA 8270C SIM Indeno(1,2,3-cd) pyrene SCM MN

RCRP EPA 8270C SIM Pyrene SCM MN

RCRP EPA 8270C SIM Pyrene NPW MN


RCRP EPA 8270D 1,2,4-Trichlorobenzene SCM MN

RCRP EPA 8270D 1,2,4-Trichlorobenzene NPW MN

RCRP EPA 8270D 1,2-Dichlorobenzene SCM MN

RCRP EPA 8270D 1,2-Dichlorobenzene NPW MN

RCRP EPA 8270D 1,2-Diphenylhydrazine SCM MN

RCRP EPA 8270D 1,2-Diphenylhydrazine NPW MN





RCRP EPA 8270D 2,4,5-Trichlorophenol SCM MN

RCRP EPA 8270D 2,4,5-Trichlorophenol NPW MN

RCRP EPA 8270D 2,4,6-Trichlorophenol SCM MN

RCRP EPA 8270D 2,4,6-Trichlorophenol NPW MN

RCRP EPA 8270D 2,4-Dichlorophenol SCM MN

RCRP EPA 8270D 2,4-Dichlorophenol NPW MN

RCRP EPA 8270D 2,4-Dimethylphenol SCM MN

RCRP EPA 8270D 2,4-Dimethylphenol NPW MN

RCRP EPA 8270D 2,4-Dinitrophenol NPW MN

RCRP EPA 8270D 2,4-Dinitrophenol SCM MN

RCRP EPA 8270D 2,4-Dinitrotoluene (2,4-DNT) NPW MN

RCRP EPA 8270D 2,4-Dinitrotoluene (2,4-DNT) SCM MN

Page 59 of 87




RCRP EPA 8270D 2,6-Dinitrotoluene (2,6-DNT) NPW MN

RCRP EPA 8270D 2,6-Dinitrotoluene (2,6-DNT) SCM MN

RCRP EPA 8270D 2-Chloronaphthalene SCM MN

RCRP EPA 8270D 2-Chloronaphthalene NPW MN

RCRP EPA 8270D 2-Chlorophenol SCM MN

RCRP EPA 8270D 2-Chlorophenol NPW MN

RCRP EPA 8270D 2-Methylnaphthalene SCM MN

RCRP EPA 8270D 2-Methylnaphthalene NPW MN

RCRP EPA 8270D 2-Methylphenol (o-Cresol) NPW MN

RCRP EPA 8270D 2-Methylphenol (o-Cresol) SCM MN

RCRP EPA 8270D 2-Nitroaniline NPW MN

RCRP EPA 8270D 2-Nitroaniline SCM MN

RCRP EPA 8270D 2-Nitrophenol NPW MN

RCRP EPA 8270D 2-Nitrophenol SCM MN

RCRP EPA 8270D 3,3'-Dichlorobenzidine SCM MN

RCRP EPA 8270D 3,3'-Dichlorobenzidine NPW MN

RCRP EPA 8270D 3-Methylcholanthrene NPW MN

RCRP EPA 8270D 3-Methylcholanthrene SCM MN

RCRP EPA 8270D 3-Methylphenol (m-Cresol) SCM MN

RCRP EPA 8270D 3-Methylphenol (m-Cresol) NPW MN



RCRP EPA 8270D 4,6-Dinitro-2-methylphenol NPW MN

RCRP EPA 8270D 4,6-Dinitro-2-methylphenol SCM MN

RCRP EPA 8270D 4-Bromophenyl phenyl ether NPW MN

RCRP EPA 8270D 4-Bromophenyl phenyl ether SCM MN

RCRP EPA 8270D 4-Chloro-3-methylphenol SCM MN

RCRP EPA 8270D 4-Chloro-3-methylphenol NPW MN

RCRP EPA 8270D 4-Chloroaniline SCM MN

RCRP EPA 8270D 4-Chloroaniline NPW MN

RCRP EPA 8270D 4-Chlorophenyl phenylether NPW MN

RCRP EPA 8270D 4-Chlorophenyl phenylether SCM MN

RCRP EPA 8270D 4-Methylphenol (p-Cresol) SCM MN

RCRP EPA 8270D 4-Methylphenol (p-Cresol) NPW MN



Page 60 of 87




RCRP EPA 8270D 4-Nitrophenol SCM MN

RCRP EPA 8270D 4-Nitrophenol NPW MN

RCRP EPA 8270D Acenaphthene SCM MN

RCRP EPA 8270D Acenaphthene NPW MN

RCRP EPA 8270D Acenaphthylene SCM MN

RCRP EPA 8270D Acenaphthylene NPW MN

RCRP EPA 8270D Anthracene NPW MN

RCRP EPA 8270D Anthracene SCM MN

RCRP EPA 8270D Benzidine NPW MN

RCRP EPA 8270D Benzidine SCM MN

RCRP EPA 8270D Benzo(a)anthracene NPW MN

RCRP EPA 8270D Benzo(a)anthracene SCM MN

RCRP EPA 8270D Benzo(a)pyrene NPW MN

RCRP EPA 8270D Benzo(a)pyrene SCM MN

RCRP EPA 8270D Benzo(g,h,i)perylene SCM MN

RCRP EPA 8270D Benzo(g,h,i)perylene NPW MN

RCRP EPA 8270D Benzo(k)fluoranthene SCM MN

RCRP EPA 8270D Benzo(k)fluoranthene NPW MN

RCRP EPA 8270D Benzo[b]fluoranthene NPW MN

RCRP EPA 8270D Benzo[b]fluoranthene SCM MN

RCRP EPA 8270D Benzoic acid SCM MN

RCRP EPA 8270D Benzoic acid NPW MN

RCRP EPA 8270D Benzyl alcohol NPW MN

RCRP EPA 8270D Benzyl alcohol SCM MN

RCRP EPA 8270D bis(2-Chloroethoxy)methane NPW MN

RCRP EPA 8270D bis(2-Chloroethoxy)methane SCM MN

RCRP EPA 8270D bis(2-Chloroethyl) ether SCM MN

RCRP EPA 8270D bis(2-Chloroethyl) ether NPW MN

RCRP EPA 8270D bis(2-Chloroisopropyl) ether SCM MN

RCRP EPA 8270D bis(2-Chloroisopropyl) ether NPW MN

RCRP EPA 8270D Butyl benzyl phthalate NPW MN

RCRP EPA 8270D Butyl benzyl phthalate SCM MN

RCRP EPA 8270D Carbazole SCM MN

RCRP EPA 8270D Carbazole NPW MN

RCRP EPA 8270D Chrysene SCM MN

RCRP EPA 8270D Chrysene NPW MN

Page 61 of 87




RCRP EPA 8270D Di(2-ethylhexyl) phthalate (bis(2-Ethylhexyl)phthalate, DEHP)

NPW MN

RCRP EPA 8270D Di(2-ethylhexyl) phthalate (bis(2-Ethylhexyl)phthalate, DEHP)

SCM MN

RCRP EPA 8270D Di-n-butyl phthalate SCM MN

RCRP EPA 8270D Di-n-butyl phthalate NPW MN

RCRP EPA 8270D Di-n-octyl phthalate NPW MN

RCRP EPA 8270D Di-n-octyl phthalate SCM MN

RCRP EPA 8270D Dibenz(a,h) anthracene SCM MN

RCRP EPA 8270D Dibenz(a,h) anthracene NPW MN

RCRP EPA 8270D Dibenzofuran SCM MN

RCRP EPA 8270D Dibenzofuran NPW MN

RCRP EPA 8270D Diethyl phthalate SCM MN

RCRP EPA 8270D Diethyl phthalate NPW MN

RCRP EPA 8270D Dimethyl phthalate SCM MN

RCRP EPA 8270D Dimethyl phthalate NPW MN

RCRP EPA 8270D Fluoranthene NPW MN

RCRP EPA 8270D Fluoranthene SCM MN

RCRP EPA 8270D Fluorene SCM MN

RCRP EPA 8270D Fluorene NPW MN

RCRP EPA 8270D Hexachlorobenzene NPW MN

RCRP EPA 8270D Hexachlorobenzene SCM MN

RCRP EPA 8270D Hexachlorobutadiene SCM MN

RCRP EPA 8270D Hexachlorobutadiene NPW MN

RCRP EPA 8270D Hexachlorocyclopentadiene SCM MN

RCRP EPA 8270D Hexachlorocyclopentadiene NPW MN

RCRP EPA 8270D Hexachloroethane SCM MN

RCRP EPA 8270D Hexachloroethane NPW MN

RCRP EPA 8270D Indeno(1,2,3-cd) pyrene NPW MN

RCRP EPA 8270D Indeno(1,2,3-cd) pyrene SCM MN

RCRP EPA 8270D Isophorone SCM MN

RCRP EPA 8270D Isophorone NPW MN

RCRP EPA 8270D n-Nitrosodi-n-propylamine SCM MN

RCRP EPA 8270D n-Nitrosodi-n-propylamine NPW MN

RCRP EPA 8270D n-Nitrosodimethylamine NPW MN

RCRP EPA 8270D n-Nitrosodimethylamine SCM MN

RCRP EPA 8270D n-Nitrosodiphenylamine SCM MN

Page 62 of 87



EPA 8270D SIM Preparation Techniques: Extraction, microwave; Extraction, ultrasonic; Extraction, soxhlet; Extraction, separatory funnel liquid-liquid

(LLE);


RCRP EPA 8270D n-Nitrosodiphenylamine NPW MN

RCRP EPA 8270D Naphthalene NPW MN

RCRP EPA 8270D Naphthalene SCM MN

RCRP EPA 8270D Nitrobenzene NPW MN

RCRP EPA 8270D Nitrobenzene SCM MN

RCRP EPA 8270D Pentachlorophenol NPW MN

RCRP EPA 8270D Pentachlorophenol SCM MN

RCRP EPA 8270D Phenanthrene NPW MN

RCRP EPA 8270D Phenanthrene SCM MN

RCRP EPA 8270D Phenol NPW MN

RCRP EPA 8270D Phenol SCM MN

RCRP EPA 8270D Pyrene NPW MN

RCRP EPA 8270D Pyrene SCM MN

RCRP EPA 8270D Pyridine SCM MN

RCRP EPA 8270D Pyridine NPW MN


RCRP EPA 8270D SIM 1-Methylnaphthalene SCM MN

RCRP EPA 8270D SIM 1-Methylnaphthalene NPW MN

RCRP EPA 8270D SIM 2-Chloronaphthalene NPW MN

RCRP EPA 8270D SIM 2-Chloronaphthalene SCM MN

RCRP EPA 8270D SIM 2-Methylnaphthalene SCM MN

RCRP EPA 8270D SIM 2-Methylnaphthalene NPW MN

RCRP EPA 8270D SIM Acenaphthene SCM MN

RCRP EPA 8270D SIM Acenaphthene NPW MN

RCRP EPA 8270D SIM Acenaphthylene SCM MN

RCRP EPA 8270D SIM Acenaphthylene NPW MN

RCRP EPA 8270D SIM Anthracene SCM MN

RCRP EPA 8270D SIM Anthracene NPW MN

RCRP EPA 8270D SIM Benzo(a)anthracene NPW MN

RCRP EPA 8270D SIM Benzo(a)anthracene SCM MN

RCRP EPA 8270D SIM Benzo(a)pyrene SCM MN

Page 63 of 87



EPA 8280B Preparation Techniques: Extraction, separatory funnel liquid-liquid (LLE);


RCRP EPA 8270D SIM Benzo(a)pyrene NPW MN

RCRP EPA 8270D SIM Benzo(g,h,i)perylene SCM MN

RCRP EPA 8270D SIM Benzo(g,h,i)perylene NPW MN

RCRP EPA 8270D SIM Benzo(k)fluoranthene SCM MN

RCRP EPA 8270D SIM Benzo(k)fluoranthene NPW MN

RCRP EPA 8270D SIM Benzo[b]fluoranthene SCM MN

RCRP EPA 8270D SIM Benzo[b]fluoranthene NPW MN

RCRP EPA 8270D SIM Chrysene SCM MN

RCRP EPA 8270D SIM Chrysene NPW MN

RCRP EPA 8270D SIM Dibenz(a,h) anthracene SCM MN

RCRP EPA 8270D SIM Dibenz(a,h) anthracene NPW MN

RCRP EPA 8270D SIM Dibenzofuran NPW MN

RCRP EPA 8270D SIM Dibenzofuran SCM MN

RCRP EPA 8270D SIM Fluoranthene NPW MN

RCRP EPA 8270D SIM Fluoranthene SCM MN

RCRP EPA 8270D SIM Fluorene NPW MN

RCRP EPA 8270D SIM Fluorene SCM MN

RCRP EPA 8270D SIM Indeno(1,2,3-cd) pyrene SCM MN

RCRP EPA 8270D SIM Indeno(1,2,3-cd) pyrene NPW MN

RCRP EPA 8270D SIM Naphthalene SCM MN

RCRP EPA 8270D SIM Naphthalene NPW MN

RCRP EPA 8270D SIM Phenanthrene NPW MN

RCRP EPA 8270D SIM Phenanthrene SCM MN

RCRP EPA 8270D SIM Pyrene SCM MN

RCRP EPA 8270D SIM Pyrene NPW MN

RCRP EPA 8270D SIM Quinoline SCM MN

RCRP EPA 8270D SIM Quinoline NPW MN



NPW MN


SCM MN

Page 64 of 87





NPW MN


SCM MN


NPW MN


SCM MN


SCM MN


NPW MN


SCM MN


NPW MN


SCM MN


NPW MN


NPW MN


SCM MN


SCM MN


NPW MN


SCM MN


NPW MN


NPW MN


SCM MN


NPW MN


SCM MN


SCM MN


NPW MN


NPW MN


SCM MN

RCRP EPA 8280B 2,3,4,6,7,8-Hexachlorodibenzofuran SCM MN

Page 65 of 87



EPA 8290 Preparation Techniques: Extraction, soxhlet; Extraction, separatory funnel liquid-liquid (LLE);


RCRP EPA 8280B 2,3,4,6,7,8-Hexachlorodibenzofuran NPW MN

RCRP EPA 8280B 2,3,4,7,8-Pentachlorodibenzofuran NPW MN

RCRP EPA 8280B 2,3,4,7,8-Pentachlorodibenzofuran SCM MN


SCM MN


NPW MN

RCRP EPA 8280B 2,3,7,8-Tetrachlorodibenzofuran SCM MN

RCRP EPA 8280B 2,3,7,8-Tetrachlorodibenzofuran NPW MN

RCRP EPA 8280B Total HpCDD NPW MN

RCRP EPA 8280B Total HpCDD SCM MN

RCRP EPA 8280B Total HpCDF SCM MN

RCRP EPA 8280B Total HpCDF NPW MN

RCRP EPA 8280B Total HxCDD SCM MN

RCRP EPA 8280B Total HxCDD NPW MN

RCRP EPA 8280B Total HxCDF SCM MN

RCRP EPA 8280B Total HxCDF NPW MN

RCRP EPA 8280B Total PeCDD NPW MN

RCRP EPA 8280B Total PeCDD SCM MN

RCRP EPA 8280B Total PeCDF SCM MN

RCRP EPA 8280B Total PeCDF NPW MN

RCRP EPA 8280B Total TCDD NPW MN

RCRP EPA 8280B Total TCDD SCM MN

RCRP EPA 8280B Total TCDF SCM MN

RCRP EPA 8280B Total TCDF NPW MN


RCRP EPA 8290 1,2,3,4,6,7,8,9-Octachlorodibenzo-p-dioxin (OCDD)

NPW MN


TISSUE MN


SCM MN

RCRP EPA 8290 1,2,3,4,6,7,8,9-Octachlorodibenzofuran(OCDF)

TISSUE MN

Page 66 of 87





SCM MN


NPW MN

RCRP EPA 8290 1,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin (1,2,3,4,6,7,8-hpcdd)

SCM MN


NPW MN


TISSUE MN

RCRP EPA 8290 1,2,3,4,6,7,8-Heptachlorodibenzofuran(1,2,3,4,6,7,8-hpcdf)

NPW MN


TISSUE MN


SCM MN


NPW MN


SCM MN


TISSUE MN

RCRP EPA 8290 1,2,3,4,7,8-Hexachlorodibenzo-p-dioxin(1,2,3,4,7,8-Hxcdd)

TISSUE MN


NPW MN


SCM MN

RCRP EPA 8290 1,2,3,4,7,8-Hexachlorodibenzofuran(1,2,3,4,7,8-Hxcdf)

SCM MN


NPW MN


TISSUE MN


SCM MN


TISSUE MN


NPW MN


TISSUE MN


NPW MN


SCM MN


NPW MN


TISSUE MN

Page 67 of 87





SCM MN


SCM MN


TISSUE MN


NPW MN

RCRP EPA 8290 1,2,3,7,8-Pentachlorodibenzo-p-dioxin(1,2,3,7,8-Pecdd)

NPW MN


SCM MN


TISSUE MN

RCRP EPA 8290 1,2,3,7,8-Pentachlorodibenzofuran(1,2,3,7,8-Pecdf)

SCM MN


TISSUE MN


NPW MN

RCRP EPA 8290 2,3,4,6,7,8-Hexachlorodibenzofuran NPW MN

RCRP EPA 8290 2,3,4,6,7,8-Hexachlorodibenzofuran TISSUE MN

RCRP EPA 8290 2,3,4,6,7,8-Hexachlorodibenzofuran SCM MN

RCRP EPA 8290 2,3,4,7,8-Pentachlorodibenzofuran TISSUE MN

RCRP EPA 8290 2,3,4,7,8-Pentachlorodibenzofuran NPW MN

RCRP EPA 8290 2,3,4,7,8-Pentachlorodibenzofuran SCM MN

RCRP EPA 8290 2,3,7,8-Tetrachlorodibenzo- p-dioxin(2,3,7,8-TCDD)

SCM MN


NPW MN


TISSUE MN

RCRP EPA 8290 2,3,7,8-Tetrachlorodibenzofuran SCM MN

RCRP EPA 8290 2,3,7,8-Tetrachlorodibenzofuran NPW MN

RCRP EPA 8290 2,3,7,8-Tetrachlorodibenzofuran TISSUE MN

RCRP EPA 8290 Total Heptachlorodibenzo-p-dioxin (HpCDD, Total)

TISSUE MN

RCRP EPA 8290 Total Heptachlorodibenzofuran (HpCDF,Total)

TISSUE MN

RCRP EPA 8290 Total Hexachlorodibenzo-p-dioxin (HxCDD, Total)

TISSUE MN

RCRP EPA 8290 Total Hexachlorodibenzofuran (HxCDF,Total)

TISSUE MN

RCRP EPA 8290 Total Hpcdd NPW MN

RCRP EPA 8290 Total Hpcdd SCM MN

RCRP EPA 8290 Total Hpcdf NPW MN

Page 68 of 87



EPA 8290A Preparation Techniques: Extraction, soxhlet; Extraction, separatory funnel liquid-liquid (LLE);


RCRP EPA 8290 Total Hpcdf SCM MN

RCRP EPA 8290 Total Hxcdd NPW MN

RCRP EPA 8290 Total Hxcdd SCM MN

RCRP EPA 8290 Total Hxcdf SCM MN

RCRP EPA 8290 Total Hxcdf NPW MN

RCRP EPA 8290 Total Pecdd SCM MN

RCRP EPA 8290 Total Pecdd NPW MN

RCRP EPA 8290 Total Pecdf SCM MN

RCRP EPA 8290 Total Pecdf NPW MN

RCRP EPA 8290 Total Pentachlorodibenzo-p-dioxin(PeCDD, Total)

TISSUE MN

RCRP EPA 8290 Total Pentachlorodibenzofuran (PeCDF,Total)

TISSUE MN

RCRP EPA 8290 Total TCDD SCM MN

RCRP EPA 8290 Total TCDD NPW MN

RCRP EPA 8290 Total TCDF SCM MN

RCRP EPA 8290 Total TCDF NPW MN

RCRP EPA 8290 Total Tetrachlorodibenzo-p-dioxin (TCDD, Total)

TISSUE MN

RCRP EPA 8290 Total Tetrachlorodibenzofuran (TCDF,Total)

TISSUE MN


RCRP EPA 8290A 1,2,3,4,6,7,8,9-Octachlorodibenzo-p-dioxin (OCDD)

SCM MN


TISSUE MN


NPW MN

RCRP EPA 8290A 1,2,3,4,6,7,8,9-Octachlorodibenzofuran(OCDF)

NPW MN


SCM MN


TISSUE MN

RCRP EPA 8290A 1,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin (1,2,3,4,6,7,8-hpcdd)

TISSUE MN


NPW MN

Page 69 of 87





SCM MN

RCRP EPA 8290A 1,2,3,4,6,7,8-Heptachlorodibenzofuran(1,2,3,4,6,7,8-hpcdf)

TISSUE MN


NPW MN


SCM MN


NPW MN


SCM MN


TISSUE MN

RCRP EPA 8290A 1,2,3,4,7,8-Hexachlorodibenzo-p-dioxin(1,2,3,4,7,8-Hxcdd)

NPW MN


SCM MN


TISSUE MN

RCRP EPA 8290A 1,2,3,4,7,8-Hexachlorodibenzofuran(1,2,3,4,7,8-Hxcdf)

TISSUE MN


SCM MN


NPW MN


NPW MN


SCM MN


TISSUE MN


TISSUE MN


NPW MN


SCM MN


TISSUE MN


SCM MN


NPW MN


TISSUE MN


NPW MN


SCM MN

Page 70 of 87




RCRP EPA 8290A 1,2,3,7,8-Pentachlorodibenzo-p-dioxin(1,2,3,7,8-Pecdd)

TISSUE MN


NPW MN


SCM MN

RCRP EPA 8290A 1,2,3,7,8-Pentachlorodibenzofuran(1,2,3,7,8-Pecdf)

NPW MN


SCM MN


TISSUE MN

RCRP EPA 8290A 2,3,4,6,7,8-Hexachlorodibenzofuran NPW MN

RCRP EPA 8290A 2,3,4,6,7,8-Hexachlorodibenzofuran SCM MN

RCRP EPA 8290A 2,3,4,6,7,8-Hexachlorodibenzofuran TISSUE MN

RCRP EPA 8290A 2,3,4,7,8-Pentachlorodibenzofuran NPW MN

RCRP EPA 8290A 2,3,4,7,8-Pentachlorodibenzofuran SCM MN

RCRP EPA 8290A 2,3,4,7,8-Pentachlorodibenzofuran TISSUE MN

RCRP EPA 8290A 2,3,7,8-Tetrachlorodibenzo- p-dioxin(2,3,7,8-TCDD)

SCM MN


TISSUE MN


NPW MN

RCRP EPA 8290A 2,3,7,8-Tetrachlorodibenzofuran SCM MN

RCRP EPA 8290A 2,3,7,8-Tetrachlorodibenzofuran NPW MN

RCRP EPA 8290A 2,3,7,8-Tetrachlorodibenzofuran TISSUE MN

RCRP EPA 8290A Total Heptachlorodibenzo-p-dioxin (HpCDD, Total)

NPW MN

RCRP EPA 8290A Total Heptachlorodibenzo-p-dioxin (HpCDD, Total)

SCM MN

RCRP EPA 8290A Total Heptachlorodibenzofuran (HpCDF,Total)

SCM MN

RCRP EPA 8290A Total Heptachlorodibenzofuran (HpCDF,Total)

NPW MN

RCRP EPA 8290A Total Hexachlorodibenzo-p-dioxin (HxCDD, Total)

NPW MN

RCRP EPA 8290A Total Hexachlorodibenzo-p-dioxin (HxCDD, Total)

SCM MN

RCRP EPA 8290A Total Hexachlorodibenzofuran (HxCDF,Total)

NPW MN

RCRP EPA 8290A Total Hexachlorodibenzofuran (HxCDF,Total)

SCM MN

RCRP EPA 8290A Total HpCDD TISSUE MN

RCRP EPA 8290A Total HpCDF TISSUE MN

RCRP EPA 8290A Total HxCDD TISSUE MN

Page 71 of 87




EPA 8015B Preparation Techniques: Extraction, ultrasonic; Extraction, separatory funnel liquid-liquid (LLE); Purge and trap;

EPA 8015C


RCRP EPA 8290A Total HxCDF TISSUE MN

RCRP EPA 8290A Total PeCDD TISSUE MN

RCRP EPA 8290A Total PeCDF TISSUE MN

RCRP EPA 8290A Total Pentachlorodibenzo-p-dioxin(PeCDD, Total)

SCM MN

RCRP EPA 8290A Total Pentachlorodibenzo-p-dioxin(PeCDD, Total)

NPW MN

RCRP EPA 8290A Total Pentachlorodibenzofuran (PeCDF,Total)

NPW MN

RCRP EPA 8290A Total Pentachlorodibenzofuran (PeCDF,Total)

SCM MN

RCRP EPA 8290A Total TCDD TISSUE MN

RCRP EPA 8290A Total TCDF TISSUE MN

RCRP EPA 8290A Total Tetrachlorodibenzo-p-dioxin (TCDD, Total)

NPW MN

RCRP EPA 8290A Total Tetrachlorodibenzo-p-dioxin (TCDD, Total)

SCM MN

RCRP EPA 8290A Total Tetrachlorodibenzofuran (TCDF,Total)

NPW MN

RCRP EPA 8290A Total Tetrachlorodibenzofuran (TCDF,Total)

SCM MN


RCRP EPA 9095B Paint Filter Liquids Test SCM MN


RCRP EPA 8015B Diesel range organics (DRO) NPW MN

RCRP EPA 8015B Diesel range organics (DRO) SCM MN

RCRP EPA 8015B Gasoline range organics (GRO) SCM MN

RCRP EPA 8015B Gasoline range organics (GRO) NPW MN

Page 72 of 87



Preparation Techniques: Extraction, ultrasonic; Extraction, separatory funnel liquid-liquid (LLE); Purge and trap;

EPA 8021B Preparation Techniques: Purge and trap;

EPA 8260B Preparation Techniques: Extraction, EPA 1312 SPLP, zero headspace (ZHE); Extraction, EPA 1311 TCLP, zero headspace (ZHE);

Purge and trap;


RCRP EPA 8015C Diesel range organics (DRO) NPW MN

RCRP EPA 8015C Diesel range organics (DRO) SCM MN

RCRP EPA 8015C Gasoline range organics (GRO) SCM MN

RCRP EPA 8015C Gasoline range organics (GRO) NPW MN


RCRP EPA 8021B 1,2,4-Trimethylbenzene NPW MN

RCRP EPA 8021B 1,2,4-Trimethylbenzene SCM MN



RCRP EPA 8021B Benzene SCM MN

RCRP EPA 8021B Benzene NPW MN

RCRP EPA 8021B Ethylbenzene NPW MN

RCRP EPA 8021B Ethylbenzene SCM MN

RCRP EPA 8021B m+p-xylene SCM MN

RCRP EPA 8021B m+p-xylene NPW MN

RCRP EPA 8021B Methyl tert-butyl ether (MTBE) NPW MN

RCRP EPA 8021B Methyl tert-butyl ether (MTBE) SCM MN

RCRP EPA 8021B o-Xylene SCM MN

RCRP EPA 8021B o-Xylene NPW MN

RCRP EPA 8021B Toluene SCM MN

RCRP EPA 8021B Toluene NPW MN


RCRP EPA 8260B 1,1,1,2-Tetrachloroethane NPW MN

RCRP EPA 8260B 1,1,1,2-Tetrachloroethane SCM MN

Page 73 of 87




RCRP EPA 8260B 1,1,1-Trichloroethane SCM MN

RCRP EPA 8260B 1,1,1-Trichloroethane NPW MN

RCRP EPA 8260B 1,1,2,2-Tetrachloroethane SCM MN

RCRP EPA 8260B 1,1,2,2-Tetrachloroethane NPW MN

RCRP EPA 8260B 1,1,2-Trichloro-1,2,2-trifluoroethane(Freon 113)

SCM MN

RCRP EPA 8260B 1,1,2-Trichloroethane SCM MN

RCRP EPA 8260B 1,1,2-Trichloroethane NPW MN

RCRP EPA 8260B 1,1-Dichloroethane SCM MN

RCRP EPA 8260B 1,1-Dichloroethane NPW MN

RCRP EPA 8260B 1,1-Dichloroethylene NPW MN

RCRP EPA 8260B 1,1-Dichloroethylene SCM MN

RCRP EPA 8260B 1,1-Dichloropropene NPW MN

RCRP EPA 8260B 1,1-Dichloropropene SCM MN

RCRP EPA 8260B 1,2,3-Trichlorobenzene NPW MN

RCRP EPA 8260B 1,2,3-Trichlorobenzene SCM MN

RCRP EPA 8260B 1,2,3-Trichloropropane NPW MN

RCRP EPA 8260B 1,2,3-Trichloropropane SCM MN

RCRP EPA 8260B 1,2,4-Trichlorobenzene NPW MN

RCRP EPA 8260B 1,2,4-Trichlorobenzene SCM MN



RCRP EPA 8260B 1,2-Dibromo-3-chloropropane (DBCP) SCM MN

RCRP EPA 8260B 1,2-Dibromo-3-chloropropane (DBCP) NPW MN

RCRP EPA 8260B 1,2-Dibromoethane (EDB, Ethylenedibromide)

NPW MN

RCRP EPA 8260B 1,2-Dibromoethane (EDB, Ethylenedibromide)

SCM MN

RCRP EPA 8260B 1,2-Dichlorobenzene NPW MN

RCRP EPA 8260B 1,2-Dichlorobenzene SCM MN

RCRP EPA 8260B 1,2-Dichloroethane (Ethylene dichloride) NPW MN

RCRP EPA 8260B 1,2-Dichloroethane (Ethylene dichloride) SCM MN

RCRP EPA 8260B 1,2-Dichloropropane SCM MN

RCRP EPA 8260B 1,2-Dichloropropane NPW MN





Page 74 of 87








RCRP EPA 8260B 1,4-Dioxane (1,4- Diethyleneoxide) SCM MN

RCRP EPA 8260B 1,4-Dioxane (1,4- Diethyleneoxide) NPW MN



RCRP EPA 8260B 2-Butanone (Methyl ethyl ketone, MEK) NPW MN

RCRP EPA 8260B 2-Butanone (Methyl ethyl ketone, MEK) SCM MN

RCRP EPA 8260B 2-Chloroethyl vinyl ether NPW MN

RCRP EPA 8260B 2-Chloroethyl vinyl ether SCM MN

RCRP EPA 8260B 2-Chlorotoluene SCM MN

RCRP EPA 8260B 2-Chlorotoluene NPW MN

RCRP EPA 8260B 2-Hexanone NPW MN

RCRP EPA 8260B 2-Hexanone SCM MN

RCRP EPA 8260B 2-Methylnaphthalene SCM MN

RCRP EPA 8260B 2-Nitropropane NPW MN

RCRP EPA 8260B 4-Chlorotoluene SCM MN

RCRP EPA 8260B 4-Chlorotoluene NPW MN

RCRP EPA 8260B 4-Isopropyltoluene (p-Cymene) SCM MN

RCRP EPA 8260B 4-Isopropyltoluene (p-Cymene) NPW MN

RCRP EPA 8260B 4-Methyl-2-pentanone (MIBK) NPW MN

RCRP EPA 8260B 4-Methyl-2-pentanone (MIBK) SCM MN

RCRP EPA 8260B Acetone SCM MN

RCRP EPA 8260B Acetone NPW MN

RCRP EPA 8260B Acetonitrile NPW MN

RCRP EPA 8260B Acrolein (Propenal) NPW MN

RCRP EPA 8260B Acrolein (Propenal) SCM MN

RCRP EPA 8260B Acrylonitrile SCM MN

RCRP EPA 8260B Acrylonitrile NPW MN

RCRP EPA 8260B Allyl chloride (3-Chloropropene) NPW MN

RCRP EPA 8260B Allyl chloride (3-Chloropropene) SCM MN

RCRP EPA 8260B Benzene NPW MN

RCRP EPA 8260B Benzene SCM MN

RCRP EPA 8260B Bromobenzene NPW MN

Page 75 of 87




RCRP EPA 8260B Bromobenzene SCM MN

RCRP EPA 8260B Bromochloromethane SCM MN

RCRP EPA 8260B Bromochloromethane NPW MN

RCRP EPA 8260B Bromodichloromethane SCM MN

RCRP EPA 8260B Bromodichloromethane NPW MN

RCRP EPA 8260B Bromoform NPW MN

RCRP EPA 8260B Bromoform SCM MN

RCRP EPA 8260B Carbon disulfide NPW MN

RCRP EPA 8260B Carbon disulfide SCM MN

RCRP EPA 8260B Carbon tetrachloride NPW MN

RCRP EPA 8260B Carbon tetrachloride SCM MN

RCRP EPA 8260B Chlorobenzene NPW MN

RCRP EPA 8260B Chlorobenzene SCM MN

RCRP EPA 8260B Chlorodibromomethane NPW MN

RCRP EPA 8260B Chlorodibromomethane SCM MN

RCRP EPA 8260B Chloroethane (Ethyl chloride) NPW MN

RCRP EPA 8260B Chloroethane (Ethyl chloride) SCM MN

RCRP EPA 8260B Chloroform SCM MN

RCRP EPA 8260B Chloroform NPW MN

RCRP EPA 8260B Chloroprene (2-Chloro-1,3-butadiene) NPW MN

RCRP EPA 8260B cis & trans-1,2-Dichloroethene SCM MN

RCRP EPA 8260B cis-1,2-Dichloroethylene NPW MN

RCRP EPA 8260B cis-1,2-Dichloroethylene SCM MN

RCRP EPA 8260B cis-1,3-Dichloropropene NPW MN

RCRP EPA 8260B cis-1,3-Dichloropropene SCM MN

RCRP EPA 8260B cis-1,4-Dichloro-2-butene NPW MN

RCRP EPA 8260B Di-isopropylether (DIPE) SCM MN

RCRP EPA 8260B Dibromomethane (Methylene bromide) SCM MN

RCRP EPA 8260B Dibromomethane (Methylene bromide) NPW MN

RCRP EPA 8260B Dichlorodifluoromethane (Freon-12) SCM MN

RCRP EPA 8260B Dichlorodifluoromethane (Freon-12) NPW MN

RCRP EPA 8260B Diethyl ether NPW MN

RCRP EPA 8260B Diethyl ether SCM MN

RCRP EPA 8260B Ethanol NPW MN

RCRP EPA 8260B Ethanol SCM MN

RCRP EPA 8260B Ethyl acetate NPW MN

Page 76 of 87




RCRP EPA 8260B Ethyl methacrylate NPW MN

RCRP EPA 8260B Ethyl-t-butylether (ETBE) (2-Ethoxy-2-methylpropane)

SCM MN


SCM MN User Defined S-MN-O-521 Rev. 27


NPW MN User Defined S-MN-O-521 Rev. 27

RCRP EPA 8260B Ethylbenzene SCM MN

RCRP EPA 8260B Ethylbenzene NPW MN

RCRP EPA 8260B Hexachlorobutadiene SCM MN

RCRP EPA 8260B Hexachlorobutadiene NPW MN

RCRP EPA 8260B Iodomethane (Methyl iodide) SCM MN

RCRP EPA 8260B Iodomethane (Methyl iodide) NPW MN

RCRP EPA 8260B Isobutyl alcohol (2-Methyl-1-propanol) NPW MN

RCRP EPA 8260B Isobutyl alcohol (2-Methyl-1-propanol) SCM MN

RCRP EPA 8260B Isopropyl alcohol (2-Propanol,Isopropanol)

SCM MN

RCRP EPA 8260B Isopropyl alcohol (2-Propanol,Isopropanol)

NPW MN

RCRP EPA 8260B Isopropylbenzene NPW MN

RCRP EPA 8260B Isopropylbenzene SCM MN

RCRP EPA 8260B m+p-xylene NPW MN

RCRP EPA 8260B m+p-xylene SCM MN

RCRP EPA 8260B Methacrylonitrile NPW MN

RCRP EPA 8260B Methyl bromide (Bromomethane) SCM MN

RCRP EPA 8260B Methyl bromide (Bromomethane) NPW MN

RCRP EPA 8260B Methyl chloride (Chloromethane) SCM MN

RCRP EPA 8260B Methyl chloride (Chloromethane) NPW MN

RCRP EPA 8260B Methyl methacrylate NPW MN

RCRP EPA 8260B Methyl tert-butyl ether (MTBE) SCM MN

RCRP EPA 8260B Methyl tert-butyl ether (MTBE) NPW MN

RCRP EPA 8260B Methylene chloride (Dichloromethane) NPW MN

RCRP EPA 8260B Methylene chloride (Dichloromethane) SCM MN

RCRP EPA 8260B n-Butyl alcohol (1-Butanol, n-Butanol) NPW MN

RCRP EPA 8260B n-Butylbenzene SCM MN

RCRP EPA 8260B n-Butylbenzene NPW MN

RCRP EPA 8260B n-Hexane SCM MN

RCRP EPA 8260B n-Hexane NPW MN

RCRP EPA 8260B n-Propylbenzene SCM MN

Page 77 of 87




RCRP EPA 8260B n-Propylbenzene NPW MN

RCRP EPA 8260B Naphthalene SCM MN

RCRP EPA 8260B Naphthalene NPW MN

RCRP EPA 8260B o-Xylene SCM MN

RCRP EPA 8260B o-Xylene NPW MN

RCRP EPA 8260B Propionitrile (Ethyl cyanide) NPW MN

RCRP EPA 8260B sec-Butylbenzene SCM MN

RCRP EPA 8260B sec-Butylbenzene NPW MN

RCRP EPA 8260B Styrene SCM MN

RCRP EPA 8260B Styrene NPW MN

RCRP EPA 8260B T-amylmethylether (TAME) NPW MN User Defined S-MN-O-521 Rev. 27

RCRP EPA 8260B T-amylmethylether (TAME) SCM MN User Defined S-MN-O-521 Rev. 27

RCRP EPA 8260B tert-Butyl alcohol NPW MN

RCRP EPA 8260B tert-Butyl alcohol SCM MN

RCRP EPA 8260B tert-Butylbenzene SCM MN

RCRP EPA 8260B tert-Butylbenzene NPW MN

RCRP EPA 8260B Tetrachloroethylene (Perchloroethylene) SCM MN

RCRP EPA 8260B Tetrachloroethylene (Perchloroethylene) NPW MN

RCRP EPA 8260B Tetrahydrofuran (THF) SCM MN

RCRP EPA 8260B Tetrahydrofuran (THF) NPW MN

RCRP EPA 8260B Toluene SCM MN

RCRP EPA 8260B Toluene NPW MN

RCRP EPA 8260B trans-1,2-Dichloroethylene SCM MN

RCRP EPA 8260B trans-1,2-Dichloroethylene NPW MN

RCRP EPA 8260B trans-1,3-Dichloropropylene SCM MN

RCRP EPA 8260B trans-1,3-Dichloropropylene NPW MN

RCRP EPA 8260B trans-1,4-Dichloro-2-butene SCM MN

RCRP EPA 8260B trans-1,4-Dichloro-2-butene NPW MN

RCRP EPA 8260B Trichloroethene (Trichloroethylene) SCM MN

RCRP EPA 8260B Trichloroethene (Trichloroethylene) NPW MN

RCRP EPA 8260B Trichlorofluoromethane(Fluorotrichloromethane, Freon 11)

NPW MN

RCRP EPA 8260B Trichlorofluoromethane(Fluorotrichloromethane, Freon 11)

SCM MN

RCRP EPA 8260B Vinyl acetate SCM MN

RCRP EPA 8260B Vinyl acetate NPW MN

RCRP EPA 8260B Vinyl chloride NPW MN

Page 78 of 87



EPA RSK-175 (GC/FID) Preparation Techniques: N/A





RCRP EPA 8260B Vinyl chloride SCM MN

RCRP EPA 8260B Xylene (total) SCM MN


RCRP EPA RSK-175 (GC/FID) Ethane NPW MN

RCRP EPA RSK-175 (GC/FID) Ethene NPW MN

RCRP EPA RSK-175 (GC/FID) Methane NPW MN

Safe Drinking Water Program


SDWP EPA 180.1 Turbidity DW MN


SDWP EPA 300.0 Chloride DW MN

SDWP EPA 300.0 Fluoride DW MN

SDWP EPA 300.0 Nitrate DW MN

SDWP EPA 300.0 Nitrite DW MN

SDWP EPA 300.0 Sulfate DW MN


SDWP EPA 353.2 Nitrate DW MN

Page 79 of 87






SM 2540 C-97 Preparation Techniques: N/A

SM 4500-Cl G-93 Preparation Techniques: N/A


SDWP EPA 353.2 Nitrite DW MN


SDWP SM 2320 B-97 Alkalinity as CaCO3 DW MN


SDWP SM 2340 B-97 Hardness DW MN


SDWP SM 2510 B-97 Conductivity DW MN


SDWP SM 2540 C-97 Residue-filterable (TDS) DW MN


SDWP SM 4500-Cl G-93 Total chlorine DW MN

Page 80 of 87



SM 4500-CN¯ E-97 Preparation Techniques: Distillation, micro; Distillation, macro; Distillation, MIDI;

SM 4500-CN¯ G-97 Preparation Techniques: Distillation, micro; Distillation, macro; Distillation, MIDI;

SM 4500-F¯ C-97 Preparation Techniques: N/A;

SM 4500-H+ B-96 Preparation Techniques: N/A

SM 4500-NO2¯ B-93 Preparation Techniques: N/A

SM 4500-P E-97 Preparation Techniques: N/A


SDWP SM 4500-CN¯ E-97 Cyanide DW MN


SDWP SM 4500-CN¯ G-97 Cyanide DW MN


SDWP SM 4500-F¯ C-97 Fluoride DW MN


SDWP SM 4500-H+ B-96 pH DW MN


SDWP SM 4500-NO2¯ B-93 Nitrite DW MN

Page 81 of 87





SM 9215 B (R2A)-94 Preparation Techniques: N/A


SDWP SM 4500-P E-97 Orthophosphate as P DW MN


SDWP EPA 200.8 Aluminum DW MN

SDWP EPA 200.8 Antimony DW MN

SDWP EPA 200.8 Arsenic DW MN

SDWP EPA 200.8 Barium DW MN

SDWP EPA 200.8 Beryllium DW MN

SDWP EPA 200.8 Cadmium DW MN

SDWP EPA 200.8 Chromium DW MN

SDWP EPA 200.8 Copper DW MN

SDWP EPA 200.8 Lead DW MN

SDWP EPA 200.8 Manganese DW MN

SDWP EPA 200.8 Nickel DW MN

SDWP EPA 200.8 Selenium DW MN

SDWP EPA 200.8 Silver DW MN

SDWP EPA 200.8 Thallium DW MN

SDWP EPA 200.8 Uranium DW MN

SDWP EPA 200.8 Zinc DW MN


SDWP EPA 245.1 Mercury DW MN


SDWP SM 9215 B (R2A)-94 Heterotrophic plate count DW MN

Page 82 of 87



SM 9223 B (Colilert®)-97 Preparation Techniques: N/A

EPA 1613 Preparation Techniques: Extraction, solid phase (SPE); Extraction, automated soxhlet; Extraction, separatory funnel liquid-liquid

(LLE);

EPA 524.2 Preparation Techniques: Purge and trap;


SDWP SM 9223 B (Colilert®)-97 Escherichia coli DW MN

SDWP SM 9223 B (Colilert®)-97 Total coliforms DW MN


SDWP EPA 1613 2,3,7,8-Tetrachlorodibenzo- p-dioxin(2,3,7,8-TCDD)

DW MN


SDWP EPA 524.2 1,1,1,2-Tetrachloroethane DW MN

SDWP EPA 524.2 1,1,1-Trichloroethane DW MN

SDWP EPA 524.2 1,1,2,2-Tetrachloroethane DW MN

SDWP EPA 524.2 1,1,2-Trichloroethane DW MN

SDWP EPA 524.2 1,1-Dichloroethane DW MN

SDWP EPA 524.2 1,1-Dichloroethylene DW MN

SDWP EPA 524.2 1,1-Dichloropropene DW MN

SDWP EPA 524.2 1,2,3-Trichlorobenzene DW MN

SDWP EPA 524.2 1,2,3-Trichloropropane DW MN


SDWP EPA 524.2 1,2,4-Trimethylbenzene DW MN

SDWP EPA 524.2 1,2-Dichlorobenzene DW MN

SDWP EPA 524.2 1,2-Dichloroethane (Ethylene dichloride) DW MN

SDWP EPA 524.2 1,2-Dichloropropane DW MN




SDWP EPA 524.2 2,2-Dichloropropane DW MN

Page 83 of 87




SDWP EPA 524.2 2-Chlorotoluene DW MN

SDWP EPA 524.2 4-Chlorotoluene DW MN

SDWP EPA 524.2 Benzene DW MN

SDWP EPA 524.2 Bromobenzene DW MN

SDWP EPA 524.2 Bromochloromethane DW MN

SDWP EPA 524.2 Bromodichloromethane DW MN

SDWP EPA 524.2 Bromoform DW MN

SDWP EPA 524.2 Bromomethane DW MN

SDWP EPA 524.2 Carbon tetrachloride DW MN

SDWP EPA 524.2 Chlorobenzene DW MN

SDWP EPA 524.2 Chlorodibromomethane DW MN

SDWP EPA 524.2 Chloroethane (Ethyl chloride) DW MN

SDWP EPA 524.2 Chloroform DW MN

SDWP EPA 524.2 cis-1,2-Dichloroethylene DW MN

SDWP EPA 524.2 cis-1,3-Dichloropropene DW MN

SDWP EPA 524.2 Dibromomethane (Methylene bromide) DW MN

SDWP EPA 524.2 Dichlorodifluoromethane (Freon-12) DW MN

SDWP EPA 524.2 Ethylbenzene DW MN

SDWP EPA 524.2 Hexachlorobutadiene DW MN

SDWP EPA 524.2 Isopropylbenzene DW MN

SDWP EPA 524.2 Methyl chloride (Chloromethane) DW MN

SDWP EPA 524.2 Methyl tert-butyl ether (MTBE) DW MN

SDWP EPA 524.2 Methylene chloride (Dichloromethane) DW MN

SDWP EPA 524.2 n-Butylbenzene DW MN

SDWP EPA 524.2 n-Propylbenzene DW MN

SDWP EPA 524.2 Naphthalene DW MN

SDWP EPA 524.2 sec-Butylbenzene DW MN

SDWP EPA 524.2 Styrene DW MN

SDWP EPA 524.2 tert-Butylbenzene DW MN

SDWP EPA 524.2 Tetrachloroethylene (Perchloroethylene) DW MN

SDWP EPA 524.2 Toluene DW MN

SDWP EPA 524.2 Total Trihalomethanes DW MN

SDWP EPA 524.2 trans-1,2-Dichloroethylene DW MN

SDWP EPA 524.2 trans-1,3-Dichloropropylene DW MN

SDWP EPA 524.2 Trichloroethene (Trichloroethylene) DW MN

SDWP EPA 524.2 Trichlorofluoromethane(Fluorotrichloromethane, Freon 11)

DW MN

Page 84 of 87



WI(95) DRO Preparation Techniques: N/A

EPA TO-15 Preparation Techniques: N/A


SDWP EPA 524.2 Vinyl chloride DW MN

SDWP EPA 524.2 Xylene (total) DW MN

Underground Storage Tank Program


USTP WI(95) DRO Diesel range organics (DRO) SCM MN

USTP WI(95) DRO Diesel range organics (DRO) NPW MN

USTP WI(95) DRO Diesel range organics (DRO) SCM MN User Defined S-MN-O-466 Rev. Rev.21

USTP WI(95) DRO Diesel range organics (DRO) NPW MN User Defined S-MN-O-466 Rev. Rev.21


USTP EPA TO-15 1,1,1-Trichloroethane AIR MN

USTP EPA TO-15 1,1,2,2-Tetrachloroethane AIR MN

USTP EPA TO-15 1,1,2-Trichloro-1,2,2-trifluoroethane(Freon 113)

AIR MN

USTP EPA TO-15 1,1,2-Trichloroethane AIR MN

USTP EPA TO-15 1,1-Dichloroethane AIR MN

USTP EPA TO-15 1,1-Dichloroethylene AIR MN

USTP EPA TO-15 1,2,4-Trichlorobenzene AIR MN

USTP EPA TO-15 1,2,4-Trimethylbenzene AIR MN

USTP EPA TO-15 1,2-Dibromoethane (EDB, Ethylenedibromide)

AIR MN

USTP EPA TO-15 1,2-Dichloro-1,1,2,2-tetrafluoroethane(Freon-114)

AIR MN

USTP EPA TO-15 1,2-Dichlorobenzene AIR MN

USTP EPA TO-15 1,2-Dichloroethane (Ethylene dichloride) AIR MN

USTP EPA TO-15 1,2-Dichloropropane AIR MN

USTP EPA TO-15 1,3,5-Trimethylbenzene AIR MN

USTP EPA TO-15 1,3-Butadiene AIR MN


Page 85 of 87





USTP EPA TO-15 1-Propene AIR MN

USTP EPA TO-15 2-Butanone (Methyl ethyl ketone, MEK) AIR MN

USTP EPA TO-15 2-Hexanone AIR MN

USTP EPA TO-15 4-Ethyltoluene AIR MN

USTP EPA TO-15 4-Methyl-2-pentanone (MIBK) AIR MN

USTP EPA TO-15 Acetone AIR MN

USTP EPA TO-15 Benzene AIR MN

USTP EPA TO-15 Benzyl chloride AIR MN

USTP EPA TO-15 Bromodichloromethane AIR MN

USTP EPA TO-15 Bromoform AIR MN

USTP EPA TO-15 Carbon disulfide AIR MN

USTP EPA TO-15 Carbon tetrachloride AIR MN

USTP EPA TO-15 Chlorobenzene AIR MN

USTP EPA TO-15 Chlorodibromomethane AIR MN

USTP EPA TO-15 Chloroethane (Ethyl chloride) AIR MN

USTP EPA TO-15 Chloroform AIR MN

USTP EPA TO-15 cis-1,2-Dichloroethylene AIR MN

USTP EPA TO-15 cis-1,3-Dichloropropene AIR MN

USTP EPA TO-15 Cyclohexane AIR MN

USTP EPA TO-15 Dichlorodifluoromethane (Freon-12) AIR MN

USTP EPA TO-15 Ethanol AIR MN

USTP EPA TO-15 Ethyl acetate AIR MN

USTP EPA TO-15 Ethylbenzene AIR MN

USTP EPA TO-15 Hexachlorobutadiene AIR MN

USTP EPA TO-15 Isopropyl alcohol (2-Propanol,Isopropanol)

AIR MN

USTP EPA TO-15 m+p-xylene AIR MN

USTP EPA TO-15 Methyl bromide (Bromomethane) AIR MN

USTP EPA TO-15 Methyl chloride (Chloromethane) AIR MN

USTP EPA TO-15 Methyl tert-butyl ether (MTBE) AIR MN

USTP EPA TO-15 Methylene chloride (Dichloromethane) AIR MN

USTP EPA TO-15 n-Heptane AIR MN

USTP EPA TO-15 n-Hexane AIR MN

USTP EPA TO-15 Naphthalene AIR MN

USTP EPA TO-15 o-Xylene AIR MN

USTP EPA TO-15 Styrene AIR MN

Page 86 of 87



WI(95) GRO Preparation Techniques: N/A

WI(95) GRO Preparation Techniques: N/A

Note: Method beginning with "SM" refer to the approved editions of Standard methods for the Examination of Water and Wastes. Approved

methods are listed in the applicable parts of Title 40 of the Code of Federal Regulations (including its subsequent Federal Register updates),

MN Statutes and Rules, and state-issued permits.


USTP EPA TO-15 Tetrachloroethylene (Perchloroethylene) AIR MN

USTP EPA TO-15 Tetrahydrofuran (THF) AIR MN

USTP EPA TO-15 Toluene AIR MN

USTP EPA TO-15 trans-1,2-Dichloroethylene AIR MN

USTP EPA TO-15 trans-1,3-Dichloropropylene AIR MN

USTP EPA TO-15 Trichloroethene (Trichloroethylene) AIR MN

USTP EPA TO-15 Trichlorofluoromethane(Fluorotrichloromethane, Freon 11)

AIR MN

USTP EPA TO-15 Vinyl acetate AIR MN

USTP EPA TO-15 Vinyl chloride AIR MN

USTP EPA TO-15 Xylene (total) AIR MN


USTP WI(95) GRO Gasoline range organics (GRO) NPW MN

USTP WI(95) GRO Gasoline range organics (GRO) SCM MN


USTP WI(95) GRO Petroleum Volatile Organic Compounds(PVOC)

SCM MN

USTP WI(95) GRO Petroleum Volatile Organic Compounds(PVOC)

NPW MN

Page 87 of 87


Appendix E Sampling Methodologies and Analysis


Potable drinking water samples for determining lead content in water were obtained using 950 cubic centimeters (0.95 liters) plastic bottles to collect water. The collection bottles were provided by the analyzing laboratory; Pace Analytical. First draw samples were collected after each potable drinking water source was not used for a minimum of six hours prior to sample collection. Sample were collected from the cold water side if the faucets had both hot and cold water. Prior to collecting water samples, nitrile gloves were donned by the person collecting the water sample to prevent cross contamination. The cap was removed from the 950 cc sample bottle and the bottle was filled with water at the rate it would be used by the consumer. The bottle was not allowed to overfill. The bottle was closed tightly with the cap and a unique sample number was written on the side of the sample bottle. The sample number was recorded on the chain of custody and stored in a cooler for transport to the analyzing laboratory. Field notes documented each sample number, type of fixture, the location and any additional comments. Pace Analytical Services (PACE) analyzed the potable drinking water samples for lead content. PACE used EPA Method 200.8 to analyze for lead concentrations in each water sample. EPA Method 200.8 is a well-established method promulgated by the U.S. Environmental Protection Agency (EPA) for the analysis of ground waters, surface waters, drinking waters, and wastewaters by inductively coupled plasma mass spectrometry (ICP-MS). The method was first published in 1990 to support the National Primary Drinking Water Regulations (NPDWR), which specified maximum contaminant levels (MCL) for 12 primary elemental contaminants in public water systems as part of the Safe Drinking Water Act (SDWA) of 1986. There have been many iterations of Method 200.8, including the addition of 9 secondary contaminants under the National Secondary Drinking Water Regulations (NSDWR). The version in use today is Revision 5.4 of the Method, which was approved for drinking water in 1994 and became effective in January, 1995. In addition, Method 200.8 was also recommended in 1992 for the monitoring of wastewaters under the National Pollutant Discharge Elimination System (NPDES) permit program to control the discharge of pollutants into navigable water systems, as part of the amended Clean Water Act (CWA) of 1977. It was approved on a nation-wide basis for this matrix in 2007.1

1 http://www.perkinelmer.com/CMSResources/Images/44-134581APP_NexION300Q-US-EPA200-8-Drinking-Water.pdf

AET Project No. 03-06427 Page E1 of 1

http://www.perkinelmer.com/CMSResources/Images/44-134581APP_NexION300Q-US-EPA200-8-Drinking-Water.pdf

Appendix F Supporting Documents


Introduction to Lead

Page 1 of 1

Lead naturally occurs in small amounts in nature and is found in soil, rocks and water. However, lead can be toxic to humans in higher concentrations when ingested or inhaled. Lead exposure occurs from lead containing products such as fossil fuels, plumbing, paint, batteries, ammunition and cosmetics. Lead from industrial manufacturing sites contaminates the environment and workers when using incorrect work practices, using inadequate personal protective equipment, and improper handing lead containing waste products. Industrial facilities, automobiles, and small aircraft release lead in to the atmosphere which settles on surfaces; contaminating structures, soil, and water. Federal and state regulatory standards have reduced lead content in products and significantly decreased lead exposure in humans.

Lead exposure poses the greatest risk for children since Lead is more easily absorbed and incorporated into their growing bodies. At high concentrations, lead interferes with growth, results in hearing problems, mental development, behavior problems, and lower intelligence. Children may absorb 50% of the lead from an exposure. Lead ingested or inhaled from contaminated soil in their playground, lead dust in the paint on their house or toys, and lead contaminated water are a few sources that children are exposed to lead. Adults are less affected by lead since physical growth has generally stopped. With the exception of pregnant mothers and their unborn child, adults do not absorb lead as readily as children may only absorb 25% of the lead from an exposure. However, lead exposure at higher concentrations for adults can cause health symptoms such as nerve disorders, decreased kidney function and cardiovascular deficiencies, Organic lead compounds, such as tetraethyl lead and tetramethyl lead (TEL) which is an additive to avgas, behave as gases in the respiratory tract and are absorbed to a greater extent than are inorganic lead particles. Organic lead compounds are also absorbed through the skin of both humans and experimental animals.

AET Project No. 03-06427 Page F1 of 1

Date post:	23-Mar-2022
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