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CMS SLHC Upgrade Workshop at Fermilab LYSO: A Radiation Hard Material for the SLHC Ren-Yuan Zhu California Institute of Technology October 29, 2009 (M. Gataullin for R.-Y. Zhu)
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Page 1: LYSO: A Radiation Hard Material for the SLHC · LYSO: A Radiation Hard Material for the SLHC Ren-Yuan Zhu California Institute of Technology October 29, 2009 (M. Gataullin for R.-Y.

CMS SLHC Upgrade Workshop at Fermilab

LYSO: A Radiation Hard Material for the SLHC

Ren-Yuan Zhu California Institute of Technology

October 29, 2009 (M. Gataullin for R.-Y. Zhu)

Page 2: LYSO: A Radiation Hard Material for the SLHC · LYSO: A Radiation Hard Material for the SLHC Ren-Yuan Zhu California Institute of Technology October 29, 2009 (M. Gataullin for R.-Y.

CMS ECAL SLHC Workshop at Fermilab, Ren-yuan Zhu, Caltech

Introduction LSO/LYSO is a bright (200 times of PWO) and fast (40 ns) crystal scintillator. It has been widely used in medical industry for the PET application with mass production capability exits in the world. The Caltech crystal laboratory has been investigating this material for applications in HEP experiment since FY06. It was found that its radiation hardness is excellent against γ–ray and neutron irradiations. The light output loss after 1 Mrad γ–ray irradiation is about 10% for 20 cm long samples. This work is supported by the DOE Advanced Detector R&D program from FY06 to FY08, and also by the US CMS Upgrade R&D Program in FY09.

References: IEEE Trans. Nucl. Sci. NS-52 (2005) 3133-3140, Nucl. Instrum. Meth. A572 (2007) 218-224, IEEE Trans. Nucl. Sci. NS-54 (2007) 718-724, IEEE Trans. Nucl. Sci. NS-54 (2007) 1319-1326, IEEE Trans. Nucl. Sci. NS-55 (2008) 1759-1766 and IEEE Trans. Nucl. Sci. NS-55 (2008) 2425-2341, and paper N69-8 @ NSS08, Dresden.

October 29, 2009 2

Page 3: LYSO: A Radiation Hard Material for the SLHC · LYSO: A Radiation Hard Material for the SLHC Ren-Yuan Zhu California Institute of Technology October 29, 2009 (M. Gataullin for R.-Y.

CMS ECAL SLHC Workshop at Fermilab, Ren-yuan Zhu, Caltech

BGO, LSO & LYSO Samples 2.5 x 2.5 x 20 cm (18 X0)

CPI LYSO

Saint-Gobain LYSO

SIC BGO

CTI LSO

October 29, 2009 3

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CMS ECAL SLHC Workshop at Fermilab, Ren-yuan Zhu, Caltech

LSO/LYSO with PMT Readout 11% FWHM resolution for 22Na source (0.511 MeV) 40 ns, 1,200 p.e./MeV, 5/230 times of BGO/PWO

October 29, 2009 4

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CMS ECAL SLHC Workshop at Fermilab, Ren-yuan Zhu, Caltech

LSO/LYSO with APD Readout L.O.: 1,500 p.e./MeV, 4/200 times of BGO/PWO

Readout Noise: < 40 keV

October 29, 2009 5

Page 6: LYSO: A Radiation Hard Material for the SLHC · LYSO: A Radiation Hard Material for the SLHC Ren-Yuan Zhu California Institute of Technology October 29, 2009 (M. Gataullin for R.-Y.

CMS ECAL SLHC Workshop at Fermilab, Ren-yuan Zhu, Caltech

Excellent Linearity: > 0.511 MeV Observed with APD readout

October 29, 2009 6

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CMS ECAL SLHC Workshop at Fermilab, Ren-yuan Zhu, Caltech

γ-Ray Induced Damage

No damage in photo-luminescence Transmittance recovery slow

October 29, 2009 7

Page 8: LYSO: A Radiation Hard Material for the SLHC · LYSO: A Radiation Hard Material for the SLHC Ren-Yuan Zhu California Institute of Technology October 29, 2009 (M. Gataullin for R.-Y.

CMS ECAL SLHC Workshop at Fermilab, Ren-yuan Zhu, Caltech

γ-Ray Induced Transmittance Damage

300oC thermal annealing effective LT damage: 8% @ 1 Mrad

October 29, 2009 8

Page 9: LYSO: A Radiation Hard Material for the SLHC · LYSO: A Radiation Hard Material for the SLHC Ren-Yuan Zhu California Institute of Technology October 29, 2009 (M. Gataullin for R.-Y.

CMS ECAL SLHC Workshop at Fermilab, Ren-yuan Zhu, Caltech

About 10% L.O. Loss after 1 Mrad

9% - 14% loss by APD 10% - 15% loss by PMT

All samples show consistent radiation resistance

October 29, 2009 9

Page 10: LYSO: A Radiation Hard Material for the SLHC · LYSO: A Radiation Hard Material for the SLHC Ren-Yuan Zhu California Institute of Technology October 29, 2009 (M. Gataullin for R.-Y.

CMS ECAL SLHC Workshop at Fermilab, Ren-yuan Zhu, Caltech

LSO/LYSO ECAL Performance

  Less demanding to the environment because of -0.2%/oC T coefficient.

  This material is expected to survive better the SLHC radiation environment.

  A better energy resolution, σ(E)/E, at low energies than L3 BGO and CMS PWO may be achieved because of its high light output and low readout noise:

2.0 0.5 .001/E

October 29, 2009 10

Page 11: LYSO: A Radiation Hard Material for the SLHC · LYSO: A Radiation Hard Material for the SLHC Ren-Yuan Zhu California Institute of Technology October 29, 2009 (M. Gataullin for R.-Y.

CMS ECAL SLHC Workshop at Fermilab, Ren-yuan Zhu, Caltech

γ–Ray Induced Readout Noise

γ–ray induced PMT anode current can be converted to the photoelectron numbers (Q) integrated in 100 ns gate. Its statistical fluctuation contributes to the readout noise (σ): 0.2 & 1 MeV @ 15 & 500 rad/h.

Sample L.Y. F Q15 rad/h Q500 rad/h σ15 rad/h σ500 rad/h

ID p.e./MeV µA/rad/h p.e. p.e. MeV MeV

CPI 1,480 41 6.98x104 2.33x106 0.18 1.03 SG 1,580 42 7.15x104 2.38x106 0.17 0.97

October 29, 2009 11

Page 12: LYSO: A Radiation Hard Material for the SLHC · LYSO: A Radiation Hard Material for the SLHC Ren-Yuan Zhu California Institute of Technology October 29, 2009 (M. Gataullin for R.-Y.

CMS ECAL SLHC Workshop at Fermilab, Ren-yuan Zhu, Caltech

Issues to be addressed Φ60 ingot may be cut to two crystals, significantly increasing the usage of ingot. A key issue is the light response uniformity, which is crucial to achieve crystal resolution. The distribution of the cerium activator with 0.15 segregation, however, is not uniform along the crystal. Work is needed to achieve designed uniformity.

October 29, 2009 12

Page 13: LYSO: A Radiation Hard Material for the SLHC · LYSO: A Radiation Hard Material for the SLHC Ren-Yuan Zhu California Institute of Technology October 29, 2009 (M. Gataullin for R.-Y.

CMS ECAL SLHC Workshop at Fermilab, Ren-yuan Zhu, Caltech

Light Response Uniformity CTI – L1

SG – L3

SIPAT – L1

SIPAT – L5

SIPAT – L6

SIC – L1

25 x 25 x 200 mm samples measured for their L.R.U. and fit to a

linear function

October 29, 2009 13

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CMS ECAL SLHC Workshop at Fermilab, Ren-yuan Zhu, Caltech

Progress in 2009 (I) �SIPAT-LYSO-L6: Consistent slopes for PMT and APD readout.

They may be compensated by the optical focusing effect.

October 29, 2009 14

Page 15: LYSO: A Radiation Hard Material for the SLHC · LYSO: A Radiation Hard Material for the SLHC Ren-Yuan Zhu California Institute of Technology October 29, 2009 (M. Gataullin for R.-Y.

CMS ECAL SLHC Workshop at Fermilab, Ren-yuan Zhu, Caltech

Progress in 2009 (II)

The 1st Φ61x 310 mm LYSO ingot was successfully grown recently at SIPAT, which may be cut into two 28 cm (25 X0) crystals.

The Caltech crystal laboratory is looking forward to test the 1st 2.5 x 2.5 x 28 cm sample.

October 29, 2009 15

Page 16: LYSO: A Radiation Hard Material for the SLHC · LYSO: A Radiation Hard Material for the SLHC Ren-Yuan Zhu California Institute of Technology October 29, 2009 (M. Gataullin for R.-Y.

CMS ECAL SLHC Workshop at Fermilab, Ren-yuan Zhu, Caltech

News on Hadron Damage from ETH G. Dissertori, D. Luckey, P. Lecomte, Francesca Nessi-

Tedaldi, F. Pauss, Paper N32-3@NSS09, Orlando.

October 29, 2009 16

After 1013 neutrons/cm2 the induced absorption of LYSO is five times less than that of PWO. See talk by Guenther Dissertori in this workshop (30 mins ago).

Page 17: LYSO: A Radiation Hard Material for the SLHC · LYSO: A Radiation Hard Material for the SLHC Ren-Yuan Zhu California Institute of Technology October 29, 2009 (M. Gataullin for R.-Y.

CMS ECAL SLHC Workshop at Fermilab, Ren-yuan Zhu, Caltech

Summary   LYSO crystals with bright, fast

scintillation and excellent radiation hardness are a good candidate material for the forward calorimeter at the SLHC.

  While the quality of LYSO crystals is adequate for low energy applications, such as KLOE-2 and SuperB, work is needed to further develop crystals for the SLHC. A upgrade R&D proposal for CMS is underway. Support from the US CMS upgrade program is crucial for this effort.

October 29, 2009 17

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CMS ECAL SLHC Workshop at Fermilab, Ren-yuan Zhu, Caltech

LSO/LYSO Mass Production CTI: LSO CPI: LYSO Saint-Gobain

LYSO

Additional Capability: SIPAT @ Sichuan and SICCAS @ Shanghai, China 18

Page 19: LYSO: A Radiation Hard Material for the SLHC · LYSO: A Radiation Hard Material for the SLHC Ren-Yuan Zhu California Institute of Technology October 29, 2009 (M. Gataullin for R.-Y.

CMS ECAL SLHC Workshop at Fermilab, Ren-yuan Zhu, Caltech

Sichuan Institute of Piezoelectric and Acousto-optic Technology (SIPAT)

China Electronics Technology Corporation (CETC) No. 26 Research Institute, www.sipat.com

October 29, 2009 19

Page 20: LYSO: A Radiation Hard Material for the SLHC · LYSO: A Radiation Hard Material for the SLHC Ren-Yuan Zhu California Institute of Technology October 29, 2009 (M. Gataullin for R.-Y.

CMS ECAL SLHC Workshop at Fermilab, Ren-yuan Zhu, Caltech

SIPAT Czochralski Furnaces

October 29, 2009 20

Page 21: LYSO: A Radiation Hard Material for the SLHC · LYSO: A Radiation Hard Material for the SLHC Ren-Yuan Zhu California Institute of Technology October 29, 2009 (M. Gataullin for R.-Y.

CMS ECAL SLHC Workshop at Fermilab, Ren-yuan Zhu, Caltech

SIPAT Ø60 x 250 mm LYSO Ingots Sep, 2007

October 29, 2009 21

Page 22: LYSO: A Radiation Hard Material for the SLHC · LYSO: A Radiation Hard Material for the SLHC Ren-Yuan Zhu California Institute of Technology October 29, 2009 (M. Gataullin for R.-Y.

CMS ECAL SLHC Workshop at Fermilab, Ren-yuan Zhu, Caltech

γ–Ray Induced Phosphorescence Phosphorescence peaked at 430 nm

with decay time constant of 2.5 h observed

October 29, 2009 22

Page 23: LYSO: A Radiation Hard Material for the SLHC · LYSO: A Radiation Hard Material for the SLHC Ren-Yuan Zhu California Institute of Technology October 29, 2009 (M. Gataullin for R.-Y.

CMS ECAL SLHC Workshop at Fermilab, Ren-yuan Zhu, Caltech

Scintillation spectrum not affected by irradiation

~8% damage @ 420 nm after 1 Mrad irradiation

Similar γ-Ray Damage in SIPAT LYSO

October 29, 2009 23

Page 24: LYSO: A Radiation Hard Material for the SLHC · LYSO: A Radiation Hard Material for the SLHC Ren-Yuan Zhu California Institute of Technology October 29, 2009 (M. Gataullin for R.-Y.

CMS ECAL SLHC Workshop at Fermilab, Ren-yuan Zhu, Caltech

L.R.U. by PMT & LAAPD: SIPAT-LYSO-L5 Issue: Ce doping was optimized for the uniformities

measured by PMT with two end-couplings, but a large difference observed between the PMT & APD readouts.

October 29, 2009 24

Page 25: LYSO: A Radiation Hard Material for the SLHC · LYSO: A Radiation Hard Material for the SLHC Ren-Yuan Zhu California Institute of Technology October 29, 2009 (M. Gataullin for R.-Y.

CMS ECAL SLHC Workshop at Fermilab, Ren-yuan Zhu, Caltech

L.R.U. by PMT & LAAPD: SG-LYSO-L3 Consistent uniformities between PMT and APD Some difference between two end-couplings

October 29, 2009 25

Page 26: LYSO: A Radiation Hard Material for the SLHC · LYSO: A Radiation Hard Material for the SLHC Ren-Yuan Zhu California Institute of Technology October 29, 2009 (M. Gataullin for R.-Y.

CMS ECAL SLHC Workshop at Fermilab, Ren-yuan Zhu, Caltech

Radio-luminescence for LSO/LYSO

Crystal wrapped with Tyvek paper; ɣ-ray shooting at two ends (1 cm); PMT: XP2254B running @ -1800V.

October 29, 2009 26

Page 27: LYSO: A Radiation Hard Material for the SLHC · LYSO: A Radiation Hard Material for the SLHC Ren-Yuan Zhu California Institute of Technology October 29, 2009 (M. Gataullin for R.-Y.

CMS ECAL SLHC Workshop at Fermilab, Ren-yuan Zhu, Caltech

Found: SIPAT-LYSO-L5 has an extra green emission component at the tail

end, which does not show in other samples. This may explain the large difference observed in uniformities

measured by PMT and APD.

Radio-luminescence

October 29, 2009 27

Page 28: LYSO: A Radiation Hard Material for the SLHC · LYSO: A Radiation Hard Material for the SLHC Ren-Yuan Zhu California Institute of Technology October 29, 2009 (M. Gataullin for R.-Y.

CMS ECAL SLHC Workshop at Fermilab, Ren-yuan Zhu, Caltech

SIPAT-L6: Consistent Emission at two ends�Extra green component at the tail end eliminated

October 29, 2009 28


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