7252019 MA 3000 NIC 600 2233 01 Simplified Operation Manual

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MERCURYMA-3000

Simplified Operation manual

NIC-600-2233-01

Nippon Instruments Corporation

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NIC-600-2233-01

19

1 Preparation

(1) Open the main valve of the Oxygen gas cylinder

and adjust the pressure to 01～05Mpa

(2) Adjust the regulator pressure to 005Mpa on the

backside of MA-3

(3) Confirm whether the drain water is overflowing

from the drain tank

2 Start-up

(1) Start-up Windows and boot ldquoＭＡ３winrdquo by clicking on the desktop

(2) Turn on the main switch of MA-3000

(3) ldquoCheck of flow pathrdquo screen pop up after initialization

Click Yes

Then the checking of a flow rate leak and valve operation is

started

A message will be displayed if abnormal condition is observed Software will be terminated

when OK is clicked Turn off MA-3000 and then fixing them

(4) After the check is completed heat - conditioning start

(H3 is heated for 10 minutes with flowing)

(5) It will be in ready state in 20 minutes Please check that the warning message is not displayed

3 Decreasing the system blanks

Click and perform the blank measurements at least three times until getting stable Or set

SAMPLE_No ldquo0rdquo registers with a tabulation screen and measures

(The mercury which remained in the system comes out in the first several measurements when

MA-3000 starts)

C983148983145983139983147 983156983151 983137983140983140 983139983144983141983139983147 983151983150 983117EA983123 983137983150983140 983145983150983152983157983156 ldquo0rdquo 983145983150983156983151 983123A983117983120983116E983135983118983151

Click or press ldquoF5rdquo to start

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NIC-600-2233-01

29

Pretreatment of sample boat

Sample boats absorb mercury in the air and a blank becomes high In order to measure with

sufficient accuracy heat-treat to remove mercury sample boats before measurement

The way of heat-treatment

(a) Sample boats are repeatedly and measured on MA-3000 to confirm low enough

(b) Sample boats are put into a ceramic crucible which is heated at 750 for 1 hour or more

4 Setting for Measurement Condition

(１) Click and ldquoMeasurement Conditionrdquo is displayed

Select the proper method for ldquoSTDrdquo The defaultmethod is already set for standard solution butselects the proper method for using SRM (StandardReference Materials)

Select ldquoFlow raterdquo

01L min High sensitivity (1pg~10ng)02Lmin usual05Lmin high concentration

(Linear range up to 10000ng)

Enter the proper values in each item of ldquoSTD Checkrdquo

In thermal decomposition mercury analyzing approx1 of the prior measured value is detected as acarryover If a low-concentration sample is measuredafter a high concentration sample it will be affectedwith previous carryover

ldquoBlank Checkrdquo function provides to automatically lowera blank

Please refer this table which number should be

entered

Typical value (02Lmin)

ABS(LOW) ABS(HIGH)

01ng 0002 10ng 0001

1ng 002 100ng 001

5ng 01 1000ng 01

10ng 02 5000ng 04

20ng 03 10000ng 06

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NIC-600-2233-01

39

5 Setting for Table Condition

Click and ldquoTable Condition is displayed Select each item of measuring conditions

PeakArea

Usually select Area

But select PEAK when a peak is smalland AREA value varies

Solid or LiquidSelect a sample feature This is notrelated to Measuring method

Calibration curvey=ax+blank is recommended whenmeasuring the sample near blank

6 Measurements

61 Registration of standard

Click the tab of STDrdquo

(1) Click ldquoSTDrdquo to open the ldquoSTD INPUTrdquo box

Enter the concentration of thestandard solution and the amountof sample

(2) Check the ldquoMeasurementrdquo box to add a checkmark to it

Inject standard solution is put into each sample boat

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NIC-600-2233-01

49

62 Starting a measurement

Click or press ldquoF5rdquo and the measuring starts

At the start set the file name to save the

measurement data

63 Reviewing a calibration curve

Press icon to switch the Analyze screen to review the Calibration curve

Click the icon and switch to the ldquoAnalyzerdquoscreen

Review the calibration curve in ldquoCALIBrdquo tab

When some abnormalities are observed on acalibration curve all values of the calibrationbecome red and WARNING is displayed

Confirm the calibration curves of LOW and HIGH

and reject the abnormal data by marking ldquotimesrdquo in ldquo

timesrdquobox

Each instrument has its own

characteristics and differs on sensitivity

Please refer the optimum sensitivity and

inspection data before shipping

7252019 MA 3000 NIC 600 2233 01 Simplified Operation Manual

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NIC-600-2233-01

59

64 983112983151983159 983156983151 983149983151983157983150983156 983156983144983141 983155983137983149983152983148983141983155983112983151983159 983156983151 983149983151983157983150983156 983156983144983141 983155983137983149983152983148983141983155983112983151983159 983156983151 983149983151983157983150983156 983156983144983141 983155983137983149983152983148983141983155983112983151983159 983156983151 983149983151983157983150983156 983156983144983141 983155983137983149983152983148983141983155

983123983137983149983152983148983141 983137983149983151983157983150983156 983145983155 983140983141983152983141983150983140983145983150983143 983151983150 983156983144983141 983155983137983149983152983148983141 983147983145983150983140 983142983151983154983149 983138983157983156 200983149983143 983142983151983154 983155983151983148983145983140 983137983150983140 200983157983116 983142983151983154 983148983145983153983157983145983140 983137983154983141 983157983155983157983137983148983148983161

983154983141983139983151983149983149983141983150983140983141983140 B983141 983139983137983154983141983142983157983148 983150983151983156 983156983151 983138983141 983155983152983145983148983148983141983140 983151983157983156 983151983142 983156983144983141 983138983151983137983156983155 983140983157983154983145983150983143 983148983151983137983140983145983150983143 983145983150 983156983144983141 983155983137983149983152983148983141 983139983144983137983150983143983141983154

Wear the gloves or use the tweezers when weighing samples and handling sample boats

If the liquid samples may contain organic mercury add additive B or L-cysteine solution not to

vaporize during standby in the sample changer Add small amount of additive B in the boat bottom

or add 10uL of 100ppm L-cycteine solution

When you use additive B please put small amount of additive into sample boat before sample

weighting

① 983124983144983141 volatile high liquid

Add more additive the level of liquid samples

② The sample which melt after measurement

(Ex Aluminum Pyrex and so on)

Put additive at the bottom

③ The sample which burns rapidly

Put additive at the bottom on the boat And put sample

several points on additive and then cover it with another

additive

7252019 MA 3000 NIC 600 2233 01 Simplified Operation Manual

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69

65 Measurement of Unknown samples

(1) Enter the sample name and the sample amount Select the sample form and unit etc on the

ldquoTable Conditionrdquo by clicking

(2) Select the heating method in ldquoMethod Numberrdquo If the moisture content is known as for solid

samples enter it in ldquoMOIST []rdquo so that the concentration is calculated as ldquodry weightrdquo

(3) After checking ldquoSample Numberrdquo with click or press ldquoF5rdquo to start measuring

Selection for (Heating) Method

Select a heating method (12 Methods) can be registered in ldquoRun - Method setrdquo as Heating Method

5 Methods are installed by default as described below

Heating Method table

MethodNo

Kind of sample Heating MethodTypicalamount

0 Liquid sample Standard solutionLiquid sample with additive B STD ~200microL

1Biological sample (Solid)Fish tissue plant tissue

ORGANISM(SOLID)

~200 mg

2 Soil sediment amp sludge SOIL amp SLUDGE ~200 mg

3 Urine Blood URINE amp BLOOD ~200microL

4 Plastics PLASTICS ~100 mg

5MineralsCoal coal ash metal and mineral

MINERAL ~200 mg

6 Waste water WASTE WATER ~100microL

7 Purge PURGE -

Do not measure the sample digested by HNO3 directly This sample may generate heat on the

activated carbon filter Dilute it less than 5wt of HNO3

As for HCL solution dilute it less than 1wt

The above ldquoHeating Methodsrdquo may not cover the samples which contain a lot of halogens or burn

quickly

When the check standard after measuring is lower reduce the sample size

Dilute or reduce the sample size if it contains high mercury Otherwise it contaminates the

plumbing As for the liquid samples containing organic mercury use ldquoAdditive Brdquo on the boat

7252019 MA 3000 NIC 600 2233 01 Simplified Operation Manual

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NIC-600-2233-01

79

66 983123983156983137983154983156983145983150983143 983137 983149983141983137983155983157983154983141983149983141983150983156983123983156983137983154983156983145983150983143 983137 983149983141983137983155983157983154983141983149983141983150983156983123983156983137983154983156983145983150983143 983137 983149983141983137983155983157983154983141983149983141983150983156983123983156983137983154983156983145983150983143 983137 983149983141983137983155983157983154983141983149983141983150983156

C983148983145983139983147 983156983144983141 983145983139983151983150 or press ldquoF5rdquo to start measuring

67 983122983141983158983145983141983159983145983150983143 983149983141983137983155983157983154983141983149983141983150983156 983140983137983156983137983122983141983158983145983141983159983145983150983143 983149983141983137983155983157983154983141983149983141983150983156 983140983137983156983137983122983141983158983145983141983159983145983150983143 983149983141983137983155983157983154983141983149983141983150983156 983140983137983156983137983122983141983158983145983141983159983145983150983143 983149983141983137983155983157983154983141983149983141983150983156 983140983137983156983137

983122983141983158983145983141983159 983156983144983141 983149983141983137983155983157983154983141983149983141983150983156 983154983141983155983157983148983156983155 983137983150983140 983140983141983156983141983154983149983145983150983141 983159983144983141983156983144983141983154 983156983151 983157983155983141 983156983144983141 983140983137983156983137 983151983154 983150983151983156

A983155 983142983151983154 983156983144983141 983137983150983137983148983161983155983145983155 983154983137983150983143983141 983156983144983141 983140983137983156983137 983148983141983155983155 983156983144983137983150 10983150983143 983137983154983141 983137983152983152983148983145983141983140 983142983151983154 983116983119983127 983154983137983150983143983141 983137983150983140 983156983144983141 983140983137983156983137 983143983154983141983137983156983141983154 983156983144983137983150

10983150983143 983137983154983141 983137983152983152983148983145983141983140 983142983151983154 HIGH 983154983137983150983143983141 A983150 983137983150983137983148983161983155983145983155 983154983137983150983143983141 983139983137983150 983138983141 983139983144983137983150983143983141983140 983137983150983140 983145983155 983152983141983154983142983151983154983149983141983140 983145983150 983156983144983141 983122983137983150983143983141

983139983151983148983157983149983150

I983142 983156983144983141 983154983141983139983151983158983141983154983161 983151983142 983156983144983141 983155983156983137983150983140983137983154983140 983155983151983148983157983156983145983151983150 983137983142983156983141983154 983156983144983141 983149983141983137983155983157983154983141983149983141983150983156 983145983155 90 983151983154 983148983141983155983155 983145983156 983149983145983143983144983156 983138983141 983140983157983141 983156983151 983156983144983141

983145983150983156983141983154983142983141983154983141983150983139983141 983139983151983150983156983137983149983145983150983137983156983145983151983150 983124983154983161 983156983151 983154983141983140983157983139983141 983156983144983141 983137983149983151983157983150983156 983151983142 983155983137983149983152983148983141 983151983154 983156983151 983139983144983137983150983143983141 983156983144983141 983144983141983137983156983145983150983143 983139983151983150983140983145983156983145983151983150983155

I983150983146983141983139983156 200micro983116 983151983142 D983145983155983156983145983148983148983141983140 983127983137983156983141983154 983142983151983154 983155983141983158983141983154983137983148 983156983145983149983141983155 983145983142 983144983145983143983144 983139983151983150983139983141983150983156983154983137983156983145983151983150 983155983137983149983152983148983141983155 983137983154983141 983149983141983137983155983157983154983141983140

I983150983146983141983139983156 200micro983116 983151983142 983123983156983137983150983140983137983154983140 983123983151983148983157983156983145983151983150 983154983141983152983141983137983156983141983140983148983161 983145983142 983156983144983141 983155983141983150983155983145983156983145983158983145983156983161 983154983141983140983157983139983141983155 983124983144983145983155 983159983137983161 983154983141983139983151983158983141983154 983156983144983141

983155983141983150983155983145983156983145983158983145983156983161 983137983150983140 983139983137983150 983137983148983155983151 983139983151983150983142983145983154983149

7 Data Save

(１) Press and ldquoSaverdquo screen is displayed

(２) Select the registered folder and save it with entering the file name

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NIC-600-2233-01

89

8 Printing

(１) Press

(２) Select the printing objects and click ldquoPrint Reviewrdquo

(３) Confirm ldquoPrint Reviewrdquo and start printing

983123983141983148983141983139983156 ldquo983124983137983138983148983141rdquo983085ldquo983117983141983149983151 983123983141983156rdquo

983124983144983141 983156983145983156983148983141 983137983150983140 983137 983149983141983137983155983157983154983141983149983141983150983156 983152983141983154983155983151983150 983150983137983149983141 983139983137983150 983138983141 983145983150983152983157983156983156983141983140 983151983150 983156983144983141 983155983139983154983141983141983150

983124983144983141 983152983154983145983150983156983145983150983143 983152983154983151983142983145983148983141983155 983155983139983137983148983141 983145983155 983138983141983145983150983143 983145983150983156983141983154983148983151983139983147983141983140 983159983145983156983144 983156983144983141 983155983139983137983148983141 983151983142 ldquo983120983154983151983142983145983148983141rdquo 983155983139983154983141983141983150 983123983141983156 983157983152 983156983144983141 983155983139983137983148983141 983137983150983140

983156983144983141 983150983157983149983138983141983154 983151983142 983152983154983151983142983145983148983141983155 983151983142 983141983137983139983144 983154983137983150983143983141 983138983161 983123983124D 983137983150983140 983123983117983120 983154983141983155983152983141983139983156983145983158983141983148983161

983124983144983141 983154983151983159 983159983145983140983156983144 983151983142 983152983154983145983150983156983145983150983143 983145983155 983138983141983145983150983143 983145983150983156983141983154983148983151983139983147983141983140 983159983145983156983144 983137 983155983141983156983157983152 983151983142 983124983137983138983148983141 983155983139983154983141983141983150 I983142 983156983144983141 983154983151983159 983159983145983140983156983144 983137983156 983156983144983141 983156983145983149983141

983151983142 983152983154983145983150983156983145983150983143 983145983155 983150983137983154983154983151983159 983152983148983141983137983155983141 983137983140983146983157983155983156 983151983150 983156983144983141 983155983139983154983141983141983150 A983150983140 983156983144983141 983154983151983159 983159983145983148983148 983150983151983156 983138983141 983152983154983145983150983156983141983140 983145983142 983159983145983140983156983144 983151983142 983137 983154983151983159 983145983155

983149983137983140983141 983145983150983156983151 983162983141983154983151

9 Termination

(１) Press the upper right button of MA3win

(２) Close the Windows and turn off the power of PC and Printer

(３) Power off MA-3000

(４) Discharge liquid of a drain tank

(５) Close the main cock of the Oxygen gas cylinder

983116983151983159 983112983113983111983112

983118983157983149983138983141983154

983151983142 983152983154983151983142983145983148983141

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NIC-600-2233-01

99

9 Errors and warning

Measurement can continue even if a warning message has been displayed However if an error

message is displayed measurement will be disabled until the cause of the error has been solved

Please check messages and contact our service

Technical Center

14-8 Akaoji-cho Takatsuki-shi Osaka 569-1146

Japan

Phone +81-72-693-6820

Fax +81-72-694-0663

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19

1 Preparation

(1) Open the main valve of the Oxygen gas cylinder

and adjust the pressure to 01～05Mpa

(2) Adjust the regulator pressure to 005Mpa on the

backside of MA-3

(3) Confirm whether the drain water is overflowing

from the drain tank

2 Start-up

(1) Start-up Windows and boot ldquoＭＡ３winrdquo by clicking on the desktop

(2) Turn on the main switch of MA-3000

(3) ldquoCheck of flow pathrdquo screen pop up after initialization

Click Yes

Then the checking of a flow rate leak and valve operation is

started

A message will be displayed if abnormal condition is observed Software will be terminated

when OK is clicked Turn off MA-3000 and then fixing them

(4) After the check is completed heat - conditioning start

(H3 is heated for 10 minutes with flowing)

(5) It will be in ready state in 20 minutes Please check that the warning message is not displayed

3 Decreasing the system blanks

Click and perform the blank measurements at least three times until getting stable Or set

SAMPLE_No ldquo0rdquo registers with a tabulation screen and measures

(The mercury which remained in the system comes out in the first several measurements when

MA-3000 starts)

C983148983145983139983147 983156983151 983137983140983140 983139983144983141983139983147 983151983150 983117EA983123 983137983150983140 983145983150983152983157983156 ldquo0rdquo 983145983150983156983151 983123A983117983120983116E983135983118983151

Click or press ldquoF5rdquo to start

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NIC-600-2233-01

29

Pretreatment of sample boat

Sample boats absorb mercury in the air and a blank becomes high In order to measure with

sufficient accuracy heat-treat to remove mercury sample boats before measurement

The way of heat-treatment

(a) Sample boats are repeatedly and measured on MA-3000 to confirm low enough

(b) Sample boats are put into a ceramic crucible which is heated at 750 for 1 hour or more

4 Setting for Measurement Condition

(１) Click and ldquoMeasurement Conditionrdquo is displayed

Select the proper method for ldquoSTDrdquo The defaultmethod is already set for standard solution butselects the proper method for using SRM (StandardReference Materials)

Select ldquoFlow raterdquo

01L min High sensitivity (1pg~10ng)02Lmin usual05Lmin high concentration

(Linear range up to 10000ng)

Enter the proper values in each item of ldquoSTD Checkrdquo

In thermal decomposition mercury analyzing approx1 of the prior measured value is detected as acarryover If a low-concentration sample is measuredafter a high concentration sample it will be affectedwith previous carryover

ldquoBlank Checkrdquo function provides to automatically lowera blank

Please refer this table which number should be

entered

Typical value (02Lmin)

ABS(LOW) ABS(HIGH)

01ng 0002 10ng 0001

1ng 002 100ng 001

5ng 01 1000ng 01

10ng 02 5000ng 04

20ng 03 10000ng 06

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NIC-600-2233-01

39

5 Setting for Table Condition

Click and ldquoTable Condition is displayed Select each item of measuring conditions

PeakArea

Usually select Area

But select PEAK when a peak is smalland AREA value varies

Solid or LiquidSelect a sample feature This is notrelated to Measuring method

Calibration curvey=ax+blank is recommended whenmeasuring the sample near blank

6 Measurements

61 Registration of standard

Click the tab of STDrdquo

(1) Click ldquoSTDrdquo to open the ldquoSTD INPUTrdquo box

Enter the concentration of thestandard solution and the amountof sample

(2) Check the ldquoMeasurementrdquo box to add a checkmark to it

Inject standard solution is put into each sample boat

7252019 MA 3000 NIC 600 2233 01 Simplified Operation Manual

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NIC-600-2233-01

49

62 Starting a measurement

Click or press ldquoF5rdquo and the measuring starts

At the start set the file name to save the

measurement data

63 Reviewing a calibration curve

Press icon to switch the Analyze screen to review the Calibration curve

Click the icon and switch to the ldquoAnalyzerdquoscreen

Review the calibration curve in ldquoCALIBrdquo tab

When some abnormalities are observed on acalibration curve all values of the calibrationbecome red and WARNING is displayed

Confirm the calibration curves of LOW and HIGH

and reject the abnormal data by marking ldquotimesrdquo in ldquo

timesrdquobox

Each instrument has its own

characteristics and differs on sensitivity

Please refer the optimum sensitivity and

inspection data before shipping

7252019 MA 3000 NIC 600 2233 01 Simplified Operation Manual

httpslidepdfcomreaderfullma-3000-nic-600-2233-01-simplified-operation-manual 610

NIC-600-2233-01

59

64 983112983151983159 983156983151 983149983151983157983150983156 983156983144983141 983155983137983149983152983148983141983155983112983151983159 983156983151 983149983151983157983150983156 983156983144983141 983155983137983149983152983148983141983155983112983151983159 983156983151 983149983151983157983150983156 983156983144983141 983155983137983149983152983148983141983155983112983151983159 983156983151 983149983151983157983150983156 983156983144983141 983155983137983149983152983148983141983155

983123983137983149983152983148983141 983137983149983151983157983150983156 983145983155 983140983141983152983141983150983140983145983150983143 983151983150 983156983144983141 983155983137983149983152983148983141 983147983145983150983140 983142983151983154983149 983138983157983156 200983149983143 983142983151983154 983155983151983148983145983140 983137983150983140 200983157983116 983142983151983154 983148983145983153983157983145983140 983137983154983141 983157983155983157983137983148983148983161

983154983141983139983151983149983149983141983150983140983141983140 B983141 983139983137983154983141983142983157983148 983150983151983156 983156983151 983138983141 983155983152983145983148983148983141983140 983151983157983156 983151983142 983156983144983141 983138983151983137983156983155 983140983157983154983145983150983143 983148983151983137983140983145983150983143 983145983150 983156983144983141 983155983137983149983152983148983141 983139983144983137983150983143983141983154

Wear the gloves or use the tweezers when weighing samples and handling sample boats

If the liquid samples may contain organic mercury add additive B or L-cysteine solution not to

vaporize during standby in the sample changer Add small amount of additive B in the boat bottom

or add 10uL of 100ppm L-cycteine solution

When you use additive B please put small amount of additive into sample boat before sample

weighting

① 983124983144983141 volatile high liquid

Add more additive the level of liquid samples

② The sample which melt after measurement

(Ex Aluminum Pyrex and so on)

Put additive at the bottom

③ The sample which burns rapidly

Put additive at the bottom on the boat And put sample

several points on additive and then cover it with another

additive

7252019 MA 3000 NIC 600 2233 01 Simplified Operation Manual

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NIC-600-2233-01

69

65 Measurement of Unknown samples

(1) Enter the sample name and the sample amount Select the sample form and unit etc on the

ldquoTable Conditionrdquo by clicking

(2) Select the heating method in ldquoMethod Numberrdquo If the moisture content is known as for solid

samples enter it in ldquoMOIST []rdquo so that the concentration is calculated as ldquodry weightrdquo

(3) After checking ldquoSample Numberrdquo with click or press ldquoF5rdquo to start measuring

Selection for (Heating) Method

Select a heating method (12 Methods) can be registered in ldquoRun - Method setrdquo as Heating Method

5 Methods are installed by default as described below

Heating Method table

MethodNo

Kind of sample Heating MethodTypicalamount

0 Liquid sample Standard solutionLiquid sample with additive B STD ~200microL

1Biological sample (Solid)Fish tissue plant tissue

ORGANISM(SOLID)

~200 mg

2 Soil sediment amp sludge SOIL amp SLUDGE ~200 mg

3 Urine Blood URINE amp BLOOD ~200microL

4 Plastics PLASTICS ~100 mg

5MineralsCoal coal ash metal and mineral

MINERAL ~200 mg

6 Waste water WASTE WATER ~100microL

7 Purge PURGE -

Do not measure the sample digested by HNO3 directly This sample may generate heat on the

activated carbon filter Dilute it less than 5wt of HNO3

As for HCL solution dilute it less than 1wt

The above ldquoHeating Methodsrdquo may not cover the samples which contain a lot of halogens or burn

quickly

When the check standard after measuring is lower reduce the sample size

Dilute or reduce the sample size if it contains high mercury Otherwise it contaminates the

plumbing As for the liquid samples containing organic mercury use ldquoAdditive Brdquo on the boat

7252019 MA 3000 NIC 600 2233 01 Simplified Operation Manual

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NIC-600-2233-01

79

66 983123983156983137983154983156983145983150983143 983137 983149983141983137983155983157983154983141983149983141983150983156983123983156983137983154983156983145983150983143 983137 983149983141983137983155983157983154983141983149983141983150983156983123983156983137983154983156983145983150983143 983137 983149983141983137983155983157983154983141983149983141983150983156983123983156983137983154983156983145983150983143 983137 983149983141983137983155983157983154983141983149983141983150983156

C983148983145983139983147 983156983144983141 983145983139983151983150 or press ldquoF5rdquo to start measuring

67 983122983141983158983145983141983159983145983150983143 983149983141983137983155983157983154983141983149983141983150983156 983140983137983156983137983122983141983158983145983141983159983145983150983143 983149983141983137983155983157983154983141983149983141983150983156 983140983137983156983137983122983141983158983145983141983159983145983150983143 983149983141983137983155983157983154983141983149983141983150983156 983140983137983156983137983122983141983158983145983141983159983145983150983143 983149983141983137983155983157983154983141983149983141983150983156 983140983137983156983137

983122983141983158983145983141983159 983156983144983141 983149983141983137983155983157983154983141983149983141983150983156 983154983141983155983157983148983156983155 983137983150983140 983140983141983156983141983154983149983145983150983141 983159983144983141983156983144983141983154 983156983151 983157983155983141 983156983144983141 983140983137983156983137 983151983154 983150983151983156

A983155 983142983151983154 983156983144983141 983137983150983137983148983161983155983145983155 983154983137983150983143983141 983156983144983141 983140983137983156983137 983148983141983155983155 983156983144983137983150 10983150983143 983137983154983141 983137983152983152983148983145983141983140 983142983151983154 983116983119983127 983154983137983150983143983141 983137983150983140 983156983144983141 983140983137983156983137 983143983154983141983137983156983141983154 983156983144983137983150

10983150983143 983137983154983141 983137983152983152983148983145983141983140 983142983151983154 HIGH 983154983137983150983143983141 A983150 983137983150983137983148983161983155983145983155 983154983137983150983143983141 983139983137983150 983138983141 983139983144983137983150983143983141983140 983137983150983140 983145983155 983152983141983154983142983151983154983149983141983140 983145983150 983156983144983141 983122983137983150983143983141

983139983151983148983157983149983150

I983142 983156983144983141 983154983141983139983151983158983141983154983161 983151983142 983156983144983141 983155983156983137983150983140983137983154983140 983155983151983148983157983156983145983151983150 983137983142983156983141983154 983156983144983141 983149983141983137983155983157983154983141983149983141983150983156 983145983155 90 983151983154 983148983141983155983155 983145983156 983149983145983143983144983156 983138983141 983140983157983141 983156983151 983156983144983141

983145983150983156983141983154983142983141983154983141983150983139983141 983139983151983150983156983137983149983145983150983137983156983145983151983150 983124983154983161 983156983151 983154983141983140983157983139983141 983156983144983141 983137983149983151983157983150983156 983151983142 983155983137983149983152983148983141 983151983154 983156983151 983139983144983137983150983143983141 983156983144983141 983144983141983137983156983145983150983143 983139983151983150983140983145983156983145983151983150983155

I983150983146983141983139983156 200micro983116 983151983142 D983145983155983156983145983148983148983141983140 983127983137983156983141983154 983142983151983154 983155983141983158983141983154983137983148 983156983145983149983141983155 983145983142 983144983145983143983144 983139983151983150983139983141983150983156983154983137983156983145983151983150 983155983137983149983152983148983141983155 983137983154983141 983149983141983137983155983157983154983141983140

I983150983146983141983139983156 200micro983116 983151983142 983123983156983137983150983140983137983154983140 983123983151983148983157983156983145983151983150 983154983141983152983141983137983156983141983140983148983161 983145983142 983156983144983141 983155983141983150983155983145983156983145983158983145983156983161 983154983141983140983157983139983141983155 983124983144983145983155 983159983137983161 983154983141983139983151983158983141983154 983156983144983141

983155983141983150983155983145983156983145983158983145983156983161 983137983150983140 983139983137983150 983137983148983155983151 983139983151983150983142983145983154983149

7 Data Save

(１) Press and ldquoSaverdquo screen is displayed

(２) Select the registered folder and save it with entering the file name

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89

8 Printing

(１) Press

(２) Select the printing objects and click ldquoPrint Reviewrdquo

(３) Confirm ldquoPrint Reviewrdquo and start printing

983123983141983148983141983139983156 ldquo983124983137983138983148983141rdquo983085ldquo983117983141983149983151 983123983141983156rdquo

983124983144983141 983156983145983156983148983141 983137983150983140 983137 983149983141983137983155983157983154983141983149983141983150983156 983152983141983154983155983151983150 983150983137983149983141 983139983137983150 983138983141 983145983150983152983157983156983156983141983140 983151983150 983156983144983141 983155983139983154983141983141983150

983124983144983141 983152983154983145983150983156983145983150983143 983152983154983151983142983145983148983141983155 983155983139983137983148983141 983145983155 983138983141983145983150983143 983145983150983156983141983154983148983151983139983147983141983140 983159983145983156983144 983156983144983141 983155983139983137983148983141 983151983142 ldquo983120983154983151983142983145983148983141rdquo 983155983139983154983141983141983150 983123983141983156 983157983152 983156983144983141 983155983139983137983148983141 983137983150983140

983156983144983141 983150983157983149983138983141983154 983151983142 983152983154983151983142983145983148983141983155 983151983142 983141983137983139983144 983154983137983150983143983141 983138983161 983123983124D 983137983150983140 983123983117983120 983154983141983155983152983141983139983156983145983158983141983148983161

983124983144983141 983154983151983159 983159983145983140983156983144 983151983142 983152983154983145983150983156983145983150983143 983145983155 983138983141983145983150983143 983145983150983156983141983154983148983151983139983147983141983140 983159983145983156983144 983137 983155983141983156983157983152 983151983142 983124983137983138983148983141 983155983139983154983141983141983150 I983142 983156983144983141 983154983151983159 983159983145983140983156983144 983137983156 983156983144983141 983156983145983149983141

983151983142 983152983154983145983150983156983145983150983143 983145983155 983150983137983154983154983151983159 983152983148983141983137983155983141 983137983140983146983157983155983156 983151983150 983156983144983141 983155983139983154983141983141983150 A983150983140 983156983144983141 983154983151983159 983159983145983148983148 983150983151983156 983138983141 983152983154983145983150983156983141983140 983145983142 983159983145983140983156983144 983151983142 983137 983154983151983159 983145983155

983149983137983140983141 983145983150983156983151 983162983141983154983151

9 Termination

(１) Press the upper right button of MA3win

(２) Close the Windows and turn off the power of PC and Printer

(３) Power off MA-3000

(４) Discharge liquid of a drain tank

(５) Close the main cock of the Oxygen gas cylinder

983116983151983159 983112983113983111983112

983118983157983149983138983141983154

983151983142 983152983154983151983142983145983148983141

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NIC-600-2233-01

99

9 Errors and warning

Measurement can continue even if a warning message has been displayed However if an error

message is displayed measurement will be disabled until the cause of the error has been solved

Please check messages and contact our service

Technical Center

14-8 Akaoji-cho Takatsuki-shi Osaka 569-1146

Japan

Phone +81-72-693-6820

Fax +81-72-694-0663

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NIC-600-2233-01

29

Pretreatment of sample boat

Sample boats absorb mercury in the air and a blank becomes high In order to measure with

sufficient accuracy heat-treat to remove mercury sample boats before measurement

The way of heat-treatment

(a) Sample boats are repeatedly and measured on MA-3000 to confirm low enough

(b) Sample boats are put into a ceramic crucible which is heated at 750 for 1 hour or more

4 Setting for Measurement Condition

(１) Click and ldquoMeasurement Conditionrdquo is displayed

Select the proper method for ldquoSTDrdquo The defaultmethod is already set for standard solution butselects the proper method for using SRM (StandardReference Materials)

Select ldquoFlow raterdquo

01L min High sensitivity (1pg~10ng)02Lmin usual05Lmin high concentration

(Linear range up to 10000ng)

Enter the proper values in each item of ldquoSTD Checkrdquo

In thermal decomposition mercury analyzing approx1 of the prior measured value is detected as acarryover If a low-concentration sample is measuredafter a high concentration sample it will be affectedwith previous carryover

ldquoBlank Checkrdquo function provides to automatically lowera blank

Please refer this table which number should be

entered

Typical value (02Lmin)

ABS(LOW) ABS(HIGH)

01ng 0002 10ng 0001

1ng 002 100ng 001

5ng 01 1000ng 01

10ng 02 5000ng 04

20ng 03 10000ng 06

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39

5 Setting for Table Condition

Click and ldquoTable Condition is displayed Select each item of measuring conditions

PeakArea

Usually select Area

But select PEAK when a peak is smalland AREA value varies

Solid or LiquidSelect a sample feature This is notrelated to Measuring method

Calibration curvey=ax+blank is recommended whenmeasuring the sample near blank

6 Measurements

61 Registration of standard

Click the tab of STDrdquo

(1) Click ldquoSTDrdquo to open the ldquoSTD INPUTrdquo box

Enter the concentration of thestandard solution and the amountof sample

(2) Check the ldquoMeasurementrdquo box to add a checkmark to it

Inject standard solution is put into each sample boat

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49

62 Starting a measurement

Click or press ldquoF5rdquo and the measuring starts

At the start set the file name to save the

measurement data

63 Reviewing a calibration curve

Press icon to switch the Analyze screen to review the Calibration curve

Click the icon and switch to the ldquoAnalyzerdquoscreen

Review the calibration curve in ldquoCALIBrdquo tab

When some abnormalities are observed on acalibration curve all values of the calibrationbecome red and WARNING is displayed

Confirm the calibration curves of LOW and HIGH

and reject the abnormal data by marking ldquotimesrdquo in ldquo

timesrdquobox

Each instrument has its own

characteristics and differs on sensitivity

Please refer the optimum sensitivity and

inspection data before shipping

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59

64 983112983151983159 983156983151 983149983151983157983150983156 983156983144983141 983155983137983149983152983148983141983155983112983151983159 983156983151 983149983151983157983150983156 983156983144983141 983155983137983149983152983148983141983155983112983151983159 983156983151 983149983151983157983150983156 983156983144983141 983155983137983149983152983148983141983155983112983151983159 983156983151 983149983151983157983150983156 983156983144983141 983155983137983149983152983148983141983155

983123983137983149983152983148983141 983137983149983151983157983150983156 983145983155 983140983141983152983141983150983140983145983150983143 983151983150 983156983144983141 983155983137983149983152983148983141 983147983145983150983140 983142983151983154983149 983138983157983156 200983149983143 983142983151983154 983155983151983148983145983140 983137983150983140 200983157983116 983142983151983154 983148983145983153983157983145983140 983137983154983141 983157983155983157983137983148983148983161

983154983141983139983151983149983149983141983150983140983141983140 B983141 983139983137983154983141983142983157983148 983150983151983156 983156983151 983138983141 983155983152983145983148983148983141983140 983151983157983156 983151983142 983156983144983141 983138983151983137983156983155 983140983157983154983145983150983143 983148983151983137983140983145983150983143 983145983150 983156983144983141 983155983137983149983152983148983141 983139983144983137983150983143983141983154

Wear the gloves or use the tweezers when weighing samples and handling sample boats

If the liquid samples may contain organic mercury add additive B or L-cysteine solution not to

vaporize during standby in the sample changer Add small amount of additive B in the boat bottom

or add 10uL of 100ppm L-cycteine solution

When you use additive B please put small amount of additive into sample boat before sample

weighting

① 983124983144983141 volatile high liquid

Add more additive the level of liquid samples

② The sample which melt after measurement

(Ex Aluminum Pyrex and so on)

Put additive at the bottom

③ The sample which burns rapidly

Put additive at the bottom on the boat And put sample

several points on additive and then cover it with another

additive

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NIC-600-2233-01

69

65 Measurement of Unknown samples

(1) Enter the sample name and the sample amount Select the sample form and unit etc on the

ldquoTable Conditionrdquo by clicking

(2) Select the heating method in ldquoMethod Numberrdquo If the moisture content is known as for solid

samples enter it in ldquoMOIST []rdquo so that the concentration is calculated as ldquodry weightrdquo

(3) After checking ldquoSample Numberrdquo with click or press ldquoF5rdquo to start measuring

Selection for (Heating) Method

Select a heating method (12 Methods) can be registered in ldquoRun - Method setrdquo as Heating Method

5 Methods are installed by default as described below

Heating Method table

MethodNo

Kind of sample Heating MethodTypicalamount

0 Liquid sample Standard solutionLiquid sample with additive B STD ~200microL

1Biological sample (Solid)Fish tissue plant tissue

ORGANISM(SOLID)

~200 mg

2 Soil sediment amp sludge SOIL amp SLUDGE ~200 mg

3 Urine Blood URINE amp BLOOD ~200microL

4 Plastics PLASTICS ~100 mg

5MineralsCoal coal ash metal and mineral

MINERAL ~200 mg

6 Waste water WASTE WATER ~100microL

7 Purge PURGE -

Do not measure the sample digested by HNO3 directly This sample may generate heat on the

activated carbon filter Dilute it less than 5wt of HNO3

As for HCL solution dilute it less than 1wt

The above ldquoHeating Methodsrdquo may not cover the samples which contain a lot of halogens or burn

quickly

When the check standard after measuring is lower reduce the sample size

Dilute or reduce the sample size if it contains high mercury Otherwise it contaminates the

plumbing As for the liquid samples containing organic mercury use ldquoAdditive Brdquo on the boat

7252019 MA 3000 NIC 600 2233 01 Simplified Operation Manual

httpslidepdfcomreaderfullma-3000-nic-600-2233-01-simplified-operation-manual 810

NIC-600-2233-01

79

66 983123983156983137983154983156983145983150983143 983137 983149983141983137983155983157983154983141983149983141983150983156983123983156983137983154983156983145983150983143 983137 983149983141983137983155983157983154983141983149983141983150983156983123983156983137983154983156983145983150983143 983137 983149983141983137983155983157983154983141983149983141983150983156983123983156983137983154983156983145983150983143 983137 983149983141983137983155983157983154983141983149983141983150983156

C983148983145983139983147 983156983144983141 983145983139983151983150 or press ldquoF5rdquo to start measuring

67 983122983141983158983145983141983159983145983150983143 983149983141983137983155983157983154983141983149983141983150983156 983140983137983156983137983122983141983158983145983141983159983145983150983143 983149983141983137983155983157983154983141983149983141983150983156 983140983137983156983137983122983141983158983145983141983159983145983150983143 983149983141983137983155983157983154983141983149983141983150983156 983140983137983156983137983122983141983158983145983141983159983145983150983143 983149983141983137983155983157983154983141983149983141983150983156 983140983137983156983137

983122983141983158983145983141983159 983156983144983141 983149983141983137983155983157983154983141983149983141983150983156 983154983141983155983157983148983156983155 983137983150983140 983140983141983156983141983154983149983145983150983141 983159983144983141983156983144983141983154 983156983151 983157983155983141 983156983144983141 983140983137983156983137 983151983154 983150983151983156

A983155 983142983151983154 983156983144983141 983137983150983137983148983161983155983145983155 983154983137983150983143983141 983156983144983141 983140983137983156983137 983148983141983155983155 983156983144983137983150 10983150983143 983137983154983141 983137983152983152983148983145983141983140 983142983151983154 983116983119983127 983154983137983150983143983141 983137983150983140 983156983144983141 983140983137983156983137 983143983154983141983137983156983141983154 983156983144983137983150

10983150983143 983137983154983141 983137983152983152983148983145983141983140 983142983151983154 HIGH 983154983137983150983143983141 A983150 983137983150983137983148983161983155983145983155 983154983137983150983143983141 983139983137983150 983138983141 983139983144983137983150983143983141983140 983137983150983140 983145983155 983152983141983154983142983151983154983149983141983140 983145983150 983156983144983141 983122983137983150983143983141

983139983151983148983157983149983150

I983142 983156983144983141 983154983141983139983151983158983141983154983161 983151983142 983156983144983141 983155983156983137983150983140983137983154983140 983155983151983148983157983156983145983151983150 983137983142983156983141983154 983156983144983141 983149983141983137983155983157983154983141983149983141983150983156 983145983155 90 983151983154 983148983141983155983155 983145983156 983149983145983143983144983156 983138983141 983140983157983141 983156983151 983156983144983141

983145983150983156983141983154983142983141983154983141983150983139983141 983139983151983150983156983137983149983145983150983137983156983145983151983150 983124983154983161 983156983151 983154983141983140983157983139983141 983156983144983141 983137983149983151983157983150983156 983151983142 983155983137983149983152983148983141 983151983154 983156983151 983139983144983137983150983143983141 983156983144983141 983144983141983137983156983145983150983143 983139983151983150983140983145983156983145983151983150983155

I983150983146983141983139983156 200micro983116 983151983142 D983145983155983156983145983148983148983141983140 983127983137983156983141983154 983142983151983154 983155983141983158983141983154983137983148 983156983145983149983141983155 983145983142 983144983145983143983144 983139983151983150983139983141983150983156983154983137983156983145983151983150 983155983137983149983152983148983141983155 983137983154983141 983149983141983137983155983157983154983141983140

I983150983146983141983139983156 200micro983116 983151983142 983123983156983137983150983140983137983154983140 983123983151983148983157983156983145983151983150 983154983141983152983141983137983156983141983140983148983161 983145983142 983156983144983141 983155983141983150983155983145983156983145983158983145983156983161 983154983141983140983157983139983141983155 983124983144983145983155 983159983137983161 983154983141983139983151983158983141983154 983156983144983141

983155983141983150983155983145983156983145983158983145983156983161 983137983150983140 983139983137983150 983137983148983155983151 983139983151983150983142983145983154983149

7 Data Save

(１) Press and ldquoSaverdquo screen is displayed

(２) Select the registered folder and save it with entering the file name

7252019 MA 3000 NIC 600 2233 01 Simplified Operation Manual

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NIC-600-2233-01

89

8 Printing

(１) Press

(２) Select the printing objects and click ldquoPrint Reviewrdquo

(３) Confirm ldquoPrint Reviewrdquo and start printing

983123983141983148983141983139983156 ldquo983124983137983138983148983141rdquo983085ldquo983117983141983149983151 983123983141983156rdquo

983124983144983141 983156983145983156983148983141 983137983150983140 983137 983149983141983137983155983157983154983141983149983141983150983156 983152983141983154983155983151983150 983150983137983149983141 983139983137983150 983138983141 983145983150983152983157983156983156983141983140 983151983150 983156983144983141 983155983139983154983141983141983150

983124983144983141 983152983154983145983150983156983145983150983143 983152983154983151983142983145983148983141983155 983155983139983137983148983141 983145983155 983138983141983145983150983143 983145983150983156983141983154983148983151983139983147983141983140 983159983145983156983144 983156983144983141 983155983139983137983148983141 983151983142 ldquo983120983154983151983142983145983148983141rdquo 983155983139983154983141983141983150 983123983141983156 983157983152 983156983144983141 983155983139983137983148983141 983137983150983140

983156983144983141 983150983157983149983138983141983154 983151983142 983152983154983151983142983145983148983141983155 983151983142 983141983137983139983144 983154983137983150983143983141 983138983161 983123983124D 983137983150983140 983123983117983120 983154983141983155983152983141983139983156983145983158983141983148983161

983124983144983141 983154983151983159 983159983145983140983156983144 983151983142 983152983154983145983150983156983145983150983143 983145983155 983138983141983145983150983143 983145983150983156983141983154983148983151983139983147983141983140 983159983145983156983144 983137 983155983141983156983157983152 983151983142 983124983137983138983148983141 983155983139983154983141983141983150 I983142 983156983144983141 983154983151983159 983159983145983140983156983144 983137983156 983156983144983141 983156983145983149983141

983151983142 983152983154983145983150983156983145983150983143 983145983155 983150983137983154983154983151983159 983152983148983141983137983155983141 983137983140983146983157983155983156 983151983150 983156983144983141 983155983139983154983141983141983150 A983150983140 983156983144983141 983154983151983159 983159983145983148983148 983150983151983156 983138983141 983152983154983145983150983156983141983140 983145983142 983159983145983140983156983144 983151983142 983137 983154983151983159 983145983155

983149983137983140983141 983145983150983156983151 983162983141983154983151

9 Termination

(１) Press the upper right button of MA3win

(２) Close the Windows and turn off the power of PC and Printer

(３) Power off MA-3000

(４) Discharge liquid of a drain tank

(５) Close the main cock of the Oxygen gas cylinder

983116983151983159 983112983113983111983112

983118983157983149983138983141983154

983151983142 983152983154983151983142983145983148983141

7252019 MA 3000 NIC 600 2233 01 Simplified Operation Manual

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NIC-600-2233-01

99

9 Errors and warning

Measurement can continue even if a warning message has been displayed However if an error

message is displayed measurement will be disabled until the cause of the error has been solved

Please check messages and contact our service

Technical Center

14-8 Akaoji-cho Takatsuki-shi Osaka 569-1146

Japan

Phone +81-72-693-6820

Fax +81-72-694-0663

7252019 MA 3000 NIC 600 2233 01 Simplified Operation Manual

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NIC-600-2233-01

39

5 Setting for Table Condition

Click and ldquoTable Condition is displayed Select each item of measuring conditions

PeakArea

Usually select Area

But select PEAK when a peak is smalland AREA value varies

Solid or LiquidSelect a sample feature This is notrelated to Measuring method

Calibration curvey=ax+blank is recommended whenmeasuring the sample near blank

6 Measurements

61 Registration of standard

Click the tab of STDrdquo

(1) Click ldquoSTDrdquo to open the ldquoSTD INPUTrdquo box

Enter the concentration of thestandard solution and the amountof sample

(2) Check the ldquoMeasurementrdquo box to add a checkmark to it

Inject standard solution is put into each sample boat

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NIC-600-2233-01

49

62 Starting a measurement

Click or press ldquoF5rdquo and the measuring starts

At the start set the file name to save the

measurement data

63 Reviewing a calibration curve

Press icon to switch the Analyze screen to review the Calibration curve

Click the icon and switch to the ldquoAnalyzerdquoscreen

Review the calibration curve in ldquoCALIBrdquo tab

When some abnormalities are observed on acalibration curve all values of the calibrationbecome red and WARNING is displayed

Confirm the calibration curves of LOW and HIGH

and reject the abnormal data by marking ldquotimesrdquo in ldquo

timesrdquobox

Each instrument has its own

characteristics and differs on sensitivity

Please refer the optimum sensitivity and

inspection data before shipping

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59

64 983112983151983159 983156983151 983149983151983157983150983156 983156983144983141 983155983137983149983152983148983141983155983112983151983159 983156983151 983149983151983157983150983156 983156983144983141 983155983137983149983152983148983141983155983112983151983159 983156983151 983149983151983157983150983156 983156983144983141 983155983137983149983152983148983141983155983112983151983159 983156983151 983149983151983157983150983156 983156983144983141 983155983137983149983152983148983141983155

983123983137983149983152983148983141 983137983149983151983157983150983156 983145983155 983140983141983152983141983150983140983145983150983143 983151983150 983156983144983141 983155983137983149983152983148983141 983147983145983150983140 983142983151983154983149 983138983157983156 200983149983143 983142983151983154 983155983151983148983145983140 983137983150983140 200983157983116 983142983151983154 983148983145983153983157983145983140 983137983154983141 983157983155983157983137983148983148983161

983154983141983139983151983149983149983141983150983140983141983140 B983141 983139983137983154983141983142983157983148 983150983151983156 983156983151 983138983141 983155983152983145983148983148983141983140 983151983157983156 983151983142 983156983144983141 983138983151983137983156983155 983140983157983154983145983150983143 983148983151983137983140983145983150983143 983145983150 983156983144983141 983155983137983149983152983148983141 983139983144983137983150983143983141983154

Wear the gloves or use the tweezers when weighing samples and handling sample boats

If the liquid samples may contain organic mercury add additive B or L-cysteine solution not to

vaporize during standby in the sample changer Add small amount of additive B in the boat bottom

or add 10uL of 100ppm L-cycteine solution

When you use additive B please put small amount of additive into sample boat before sample

weighting

① 983124983144983141 volatile high liquid

Add more additive the level of liquid samples

② The sample which melt after measurement

(Ex Aluminum Pyrex and so on)

Put additive at the bottom

③ The sample which burns rapidly

Put additive at the bottom on the boat And put sample

several points on additive and then cover it with another

additive

7252019 MA 3000 NIC 600 2233 01 Simplified Operation Manual

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NIC-600-2233-01

69

65 Measurement of Unknown samples

(1) Enter the sample name and the sample amount Select the sample form and unit etc on the

ldquoTable Conditionrdquo by clicking

(2) Select the heating method in ldquoMethod Numberrdquo If the moisture content is known as for solid

samples enter it in ldquoMOIST []rdquo so that the concentration is calculated as ldquodry weightrdquo

(3) After checking ldquoSample Numberrdquo with click or press ldquoF5rdquo to start measuring

Selection for (Heating) Method

Select a heating method (12 Methods) can be registered in ldquoRun - Method setrdquo as Heating Method

5 Methods are installed by default as described below

Heating Method table

MethodNo

Kind of sample Heating MethodTypicalamount

0 Liquid sample Standard solutionLiquid sample with additive B STD ~200microL

1Biological sample (Solid)Fish tissue plant tissue

ORGANISM(SOLID)

~200 mg

2 Soil sediment amp sludge SOIL amp SLUDGE ~200 mg

3 Urine Blood URINE amp BLOOD ~200microL

4 Plastics PLASTICS ~100 mg

5MineralsCoal coal ash metal and mineral

MINERAL ~200 mg

6 Waste water WASTE WATER ~100microL

7 Purge PURGE -

Do not measure the sample digested by HNO3 directly This sample may generate heat on the

activated carbon filter Dilute it less than 5wt of HNO3

As for HCL solution dilute it less than 1wt

The above ldquoHeating Methodsrdquo may not cover the samples which contain a lot of halogens or burn

quickly

When the check standard after measuring is lower reduce the sample size

Dilute or reduce the sample size if it contains high mercury Otherwise it contaminates the

plumbing As for the liquid samples containing organic mercury use ldquoAdditive Brdquo on the boat

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NIC-600-2233-01

79

66 983123983156983137983154983156983145983150983143 983137 983149983141983137983155983157983154983141983149983141983150983156983123983156983137983154983156983145983150983143 983137 983149983141983137983155983157983154983141983149983141983150983156983123983156983137983154983156983145983150983143 983137 983149983141983137983155983157983154983141983149983141983150983156983123983156983137983154983156983145983150983143 983137 983149983141983137983155983157983154983141983149983141983150983156

C983148983145983139983147 983156983144983141 983145983139983151983150 or press ldquoF5rdquo to start measuring

67 983122983141983158983145983141983159983145983150983143 983149983141983137983155983157983154983141983149983141983150983156 983140983137983156983137983122983141983158983145983141983159983145983150983143 983149983141983137983155983157983154983141983149983141983150983156 983140983137983156983137983122983141983158983145983141983159983145983150983143 983149983141983137983155983157983154983141983149983141983150983156 983140983137983156983137983122983141983158983145983141983159983145983150983143 983149983141983137983155983157983154983141983149983141983150983156 983140983137983156983137

983122983141983158983145983141983159 983156983144983141 983149983141983137983155983157983154983141983149983141983150983156 983154983141983155983157983148983156983155 983137983150983140 983140983141983156983141983154983149983145983150983141 983159983144983141983156983144983141983154 983156983151 983157983155983141 983156983144983141 983140983137983156983137 983151983154 983150983151983156

A983155 983142983151983154 983156983144983141 983137983150983137983148983161983155983145983155 983154983137983150983143983141 983156983144983141 983140983137983156983137 983148983141983155983155 983156983144983137983150 10983150983143 983137983154983141 983137983152983152983148983145983141983140 983142983151983154 983116983119983127 983154983137983150983143983141 983137983150983140 983156983144983141 983140983137983156983137 983143983154983141983137983156983141983154 983156983144983137983150

10983150983143 983137983154983141 983137983152983152983148983145983141983140 983142983151983154 HIGH 983154983137983150983143983141 A983150 983137983150983137983148983161983155983145983155 983154983137983150983143983141 983139983137983150 983138983141 983139983144983137983150983143983141983140 983137983150983140 983145983155 983152983141983154983142983151983154983149983141983140 983145983150 983156983144983141 983122983137983150983143983141

983139983151983148983157983149983150

I983142 983156983144983141 983154983141983139983151983158983141983154983161 983151983142 983156983144983141 983155983156983137983150983140983137983154983140 983155983151983148983157983156983145983151983150 983137983142983156983141983154 983156983144983141 983149983141983137983155983157983154983141983149983141983150983156 983145983155 90 983151983154 983148983141983155983155 983145983156 983149983145983143983144983156 983138983141 983140983157983141 983156983151 983156983144983141

983145983150983156983141983154983142983141983154983141983150983139983141 983139983151983150983156983137983149983145983150983137983156983145983151983150 983124983154983161 983156983151 983154983141983140983157983139983141 983156983144983141 983137983149983151983157983150983156 983151983142 983155983137983149983152983148983141 983151983154 983156983151 983139983144983137983150983143983141 983156983144983141 983144983141983137983156983145983150983143 983139983151983150983140983145983156983145983151983150983155

I983150983146983141983139983156 200micro983116 983151983142 D983145983155983156983145983148983148983141983140 983127983137983156983141983154 983142983151983154 983155983141983158983141983154983137983148 983156983145983149983141983155 983145983142 983144983145983143983144 983139983151983150983139983141983150983156983154983137983156983145983151983150 983155983137983149983152983148983141983155 983137983154983141 983149983141983137983155983157983154983141983140

I983150983146983141983139983156 200micro983116 983151983142 983123983156983137983150983140983137983154983140 983123983151983148983157983156983145983151983150 983154983141983152983141983137983156983141983140983148983161 983145983142 983156983144983141 983155983141983150983155983145983156983145983158983145983156983161 983154983141983140983157983139983141983155 983124983144983145983155 983159983137983161 983154983141983139983151983158983141983154 983156983144983141

983155983141983150983155983145983156983145983158983145983156983161 983137983150983140 983139983137983150 983137983148983155983151 983139983151983150983142983145983154983149

7 Data Save

(１) Press and ldquoSaverdquo screen is displayed

(２) Select the registered folder and save it with entering the file name

7252019 MA 3000 NIC 600 2233 01 Simplified Operation Manual

httpslidepdfcomreaderfullma-3000-nic-600-2233-01-simplified-operation-manual 910

NIC-600-2233-01

89

8 Printing

(１) Press

(２) Select the printing objects and click ldquoPrint Reviewrdquo

(３) Confirm ldquoPrint Reviewrdquo and start printing

983123983141983148983141983139983156 ldquo983124983137983138983148983141rdquo983085ldquo983117983141983149983151 983123983141983156rdquo

983124983144983141 983156983145983156983148983141 983137983150983140 983137 983149983141983137983155983157983154983141983149983141983150983156 983152983141983154983155983151983150 983150983137983149983141 983139983137983150 983138983141 983145983150983152983157983156983156983141983140 983151983150 983156983144983141 983155983139983154983141983141983150

983124983144983141 983152983154983145983150983156983145983150983143 983152983154983151983142983145983148983141983155 983155983139983137983148983141 983145983155 983138983141983145983150983143 983145983150983156983141983154983148983151983139983147983141983140 983159983145983156983144 983156983144983141 983155983139983137983148983141 983151983142 ldquo983120983154983151983142983145983148983141rdquo 983155983139983154983141983141983150 983123983141983156 983157983152 983156983144983141 983155983139983137983148983141 983137983150983140

983156983144983141 983150983157983149983138983141983154 983151983142 983152983154983151983142983145983148983141983155 983151983142 983141983137983139983144 983154983137983150983143983141 983138983161 983123983124D 983137983150983140 983123983117983120 983154983141983155983152983141983139983156983145983158983141983148983161

983124983144983141 983154983151983159 983159983145983140983156983144 983151983142 983152983154983145983150983156983145983150983143 983145983155 983138983141983145983150983143 983145983150983156983141983154983148983151983139983147983141983140 983159983145983156983144 983137 983155983141983156983157983152 983151983142 983124983137983138983148983141 983155983139983154983141983141983150 I983142 983156983144983141 983154983151983159 983159983145983140983156983144 983137983156 983156983144983141 983156983145983149983141

983151983142 983152983154983145983150983156983145983150983143 983145983155 983150983137983154983154983151983159 983152983148983141983137983155983141 983137983140983146983157983155983156 983151983150 983156983144983141 983155983139983154983141983141983150 A983150983140 983156983144983141 983154983151983159 983159983145983148983148 983150983151983156 983138983141 983152983154983145983150983156983141983140 983145983142 983159983145983140983156983144 983151983142 983137 983154983151983159 983145983155

983149983137983140983141 983145983150983156983151 983162983141983154983151

9 Termination

(１) Press the upper right button of MA3win

(２) Close the Windows and turn off the power of PC and Printer

(３) Power off MA-3000

(４) Discharge liquid of a drain tank

(５) Close the main cock of the Oxygen gas cylinder

983116983151983159 983112983113983111983112

983118983157983149983138983141983154

983151983142 983152983154983151983142983145983148983141

7252019 MA 3000 NIC 600 2233 01 Simplified Operation Manual

httpslidepdfcomreaderfullma-3000-nic-600-2233-01-simplified-operation-manual 1010

NIC-600-2233-01

99

9 Errors and warning

Measurement can continue even if a warning message has been displayed However if an error

message is displayed measurement will be disabled until the cause of the error has been solved

Please check messages and contact our service

Technical Center

14-8 Akaoji-cho Takatsuki-shi Osaka 569-1146

Japan

Phone +81-72-693-6820

Fax +81-72-694-0663

7252019 MA 3000 NIC 600 2233 01 Simplified Operation Manual

httpslidepdfcomreaderfullma-3000-nic-600-2233-01-simplified-operation-manual 510

NIC-600-2233-01

49

62 Starting a measurement

Click or press ldquoF5rdquo and the measuring starts

At the start set the file name to save the

measurement data

63 Reviewing a calibration curve

Press icon to switch the Analyze screen to review the Calibration curve

Click the icon and switch to the ldquoAnalyzerdquoscreen

Review the calibration curve in ldquoCALIBrdquo tab

When some abnormalities are observed on acalibration curve all values of the calibrationbecome red and WARNING is displayed

Confirm the calibration curves of LOW and HIGH

and reject the abnormal data by marking ldquotimesrdquo in ldquo

timesrdquobox

Each instrument has its own

characteristics and differs on sensitivity

Please refer the optimum sensitivity and

inspection data before shipping

7252019 MA 3000 NIC 600 2233 01 Simplified Operation Manual

httpslidepdfcomreaderfullma-3000-nic-600-2233-01-simplified-operation-manual 610

NIC-600-2233-01

59

64 983112983151983159 983156983151 983149983151983157983150983156 983156983144983141 983155983137983149983152983148983141983155983112983151983159 983156983151 983149983151983157983150983156 983156983144983141 983155983137983149983152983148983141983155983112983151983159 983156983151 983149983151983157983150983156 983156983144983141 983155983137983149983152983148983141983155983112983151983159 983156983151 983149983151983157983150983156 983156983144983141 983155983137983149983152983148983141983155

983123983137983149983152983148983141 983137983149983151983157983150983156 983145983155 983140983141983152983141983150983140983145983150983143 983151983150 983156983144983141 983155983137983149983152983148983141 983147983145983150983140 983142983151983154983149 983138983157983156 200983149983143 983142983151983154 983155983151983148983145983140 983137983150983140 200983157983116 983142983151983154 983148983145983153983157983145983140 983137983154983141 983157983155983157983137983148983148983161

983154983141983139983151983149983149983141983150983140983141983140 B983141 983139983137983154983141983142983157983148 983150983151983156 983156983151 983138983141 983155983152983145983148983148983141983140 983151983157983156 983151983142 983156983144983141 983138983151983137983156983155 983140983157983154983145983150983143 983148983151983137983140983145983150983143 983145983150 983156983144983141 983155983137983149983152983148983141 983139983144983137983150983143983141983154

Wear the gloves or use the tweezers when weighing samples and handling sample boats

If the liquid samples may contain organic mercury add additive B or L-cysteine solution not to

vaporize during standby in the sample changer Add small amount of additive B in the boat bottom

or add 10uL of 100ppm L-cycteine solution

When you use additive B please put small amount of additive into sample boat before sample

weighting

① 983124983144983141 volatile high liquid

Add more additive the level of liquid samples

② The sample which melt after measurement

(Ex Aluminum Pyrex and so on)

Put additive at the bottom

③ The sample which burns rapidly

Put additive at the bottom on the boat And put sample

several points on additive and then cover it with another

additive

7252019 MA 3000 NIC 600 2233 01 Simplified Operation Manual

httpslidepdfcomreaderfullma-3000-nic-600-2233-01-simplified-operation-manual 710

NIC-600-2233-01

69

65 Measurement of Unknown samples

(1) Enter the sample name and the sample amount Select the sample form and unit etc on the

ldquoTable Conditionrdquo by clicking

(2) Select the heating method in ldquoMethod Numberrdquo If the moisture content is known as for solid

samples enter it in ldquoMOIST []rdquo so that the concentration is calculated as ldquodry weightrdquo

(3) After checking ldquoSample Numberrdquo with click or press ldquoF5rdquo to start measuring

Selection for (Heating) Method

Select a heating method (12 Methods) can be registered in ldquoRun - Method setrdquo as Heating Method

5 Methods are installed by default as described below

Heating Method table

MethodNo

Kind of sample Heating MethodTypicalamount

0 Liquid sample Standard solutionLiquid sample with additive B STD ~200microL

1Biological sample (Solid)Fish tissue plant tissue

ORGANISM(SOLID)

~200 mg

2 Soil sediment amp sludge SOIL amp SLUDGE ~200 mg

3 Urine Blood URINE amp BLOOD ~200microL

4 Plastics PLASTICS ~100 mg

5MineralsCoal coal ash metal and mineral

MINERAL ~200 mg

6 Waste water WASTE WATER ~100microL

7 Purge PURGE -

Do not measure the sample digested by HNO3 directly This sample may generate heat on the

activated carbon filter Dilute it less than 5wt of HNO3

As for HCL solution dilute it less than 1wt

The above ldquoHeating Methodsrdquo may not cover the samples which contain a lot of halogens or burn

quickly

When the check standard after measuring is lower reduce the sample size

Dilute or reduce the sample size if it contains high mercury Otherwise it contaminates the

plumbing As for the liquid samples containing organic mercury use ldquoAdditive Brdquo on the boat

7252019 MA 3000 NIC 600 2233 01 Simplified Operation Manual

httpslidepdfcomreaderfullma-3000-nic-600-2233-01-simplified-operation-manual 810

NIC-600-2233-01

79

66 983123983156983137983154983156983145983150983143 983137 983149983141983137983155983157983154983141983149983141983150983156983123983156983137983154983156983145983150983143 983137 983149983141983137983155983157983154983141983149983141983150983156983123983156983137983154983156983145983150983143 983137 983149983141983137983155983157983154983141983149983141983150983156983123983156983137983154983156983145983150983143 983137 983149983141983137983155983157983154983141983149983141983150983156

C983148983145983139983147 983156983144983141 983145983139983151983150 or press ldquoF5rdquo to start measuring

67 983122983141983158983145983141983159983145983150983143 983149983141983137983155983157983154983141983149983141983150983156 983140983137983156983137983122983141983158983145983141983159983145983150983143 983149983141983137983155983157983154983141983149983141983150983156 983140983137983156983137983122983141983158983145983141983159983145983150983143 983149983141983137983155983157983154983141983149983141983150983156 983140983137983156983137983122983141983158983145983141983159983145983150983143 983149983141983137983155983157983154983141983149983141983150983156 983140983137983156983137

983122983141983158983145983141983159 983156983144983141 983149983141983137983155983157983154983141983149983141983150983156 983154983141983155983157983148983156983155 983137983150983140 983140983141983156983141983154983149983145983150983141 983159983144983141983156983144983141983154 983156983151 983157983155983141 983156983144983141 983140983137983156983137 983151983154 983150983151983156

A983155 983142983151983154 983156983144983141 983137983150983137983148983161983155983145983155 983154983137983150983143983141 983156983144983141 983140983137983156983137 983148983141983155983155 983156983144983137983150 10983150983143 983137983154983141 983137983152983152983148983145983141983140 983142983151983154 983116983119983127 983154983137983150983143983141 983137983150983140 983156983144983141 983140983137983156983137 983143983154983141983137983156983141983154 983156983144983137983150

10983150983143 983137983154983141 983137983152983152983148983145983141983140 983142983151983154 HIGH 983154983137983150983143983141 A983150 983137983150983137983148983161983155983145983155 983154983137983150983143983141 983139983137983150 983138983141 983139983144983137983150983143983141983140 983137983150983140 983145983155 983152983141983154983142983151983154983149983141983140 983145983150 983156983144983141 983122983137983150983143983141

983139983151983148983157983149983150

I983142 983156983144983141 983154983141983139983151983158983141983154983161 983151983142 983156983144983141 983155983156983137983150983140983137983154983140 983155983151983148983157983156983145983151983150 983137983142983156983141983154 983156983144983141 983149983141983137983155983157983154983141983149983141983150983156 983145983155 90 983151983154 983148983141983155983155 983145983156 983149983145983143983144983156 983138983141 983140983157983141 983156983151 983156983144983141

983145983150983156983141983154983142983141983154983141983150983139983141 983139983151983150983156983137983149983145983150983137983156983145983151983150 983124983154983161 983156983151 983154983141983140983157983139983141 983156983144983141 983137983149983151983157983150983156 983151983142 983155983137983149983152983148983141 983151983154 983156983151 983139983144983137983150983143983141 983156983144983141 983144983141983137983156983145983150983143 983139983151983150983140983145983156983145983151983150983155

I983150983146983141983139983156 200micro983116 983151983142 D983145983155983156983145983148983148983141983140 983127983137983156983141983154 983142983151983154 983155983141983158983141983154983137983148 983156983145983149983141983155 983145983142 983144983145983143983144 983139983151983150983139983141983150983156983154983137983156983145983151983150 983155983137983149983152983148983141983155 983137983154983141 983149983141983137983155983157983154983141983140

I983150983146983141983139983156 200micro983116 983151983142 983123983156983137983150983140983137983154983140 983123983151983148983157983156983145983151983150 983154983141983152983141983137983156983141983140983148983161 983145983142 983156983144983141 983155983141983150983155983145983156983145983158983145983156983161 983154983141983140983157983139983141983155 983124983144983145983155 983159983137983161 983154983141983139983151983158983141983154 983156983144983141

983155983141983150983155983145983156983145983158983145983156983161 983137983150983140 983139983137983150 983137983148983155983151 983139983151983150983142983145983154983149

7 Data Save

(１) Press and ldquoSaverdquo screen is displayed

(２) Select the registered folder and save it with entering the file name

7252019 MA 3000 NIC 600 2233 01 Simplified Operation Manual

httpslidepdfcomreaderfullma-3000-nic-600-2233-01-simplified-operation-manual 910

NIC-600-2233-01

89

8 Printing

(１) Press

(２) Select the printing objects and click ldquoPrint Reviewrdquo

(３) Confirm ldquoPrint Reviewrdquo and start printing

983123983141983148983141983139983156 ldquo983124983137983138983148983141rdquo983085ldquo983117983141983149983151 983123983141983156rdquo

983124983144983141 983156983145983156983148983141 983137983150983140 983137 983149983141983137983155983157983154983141983149983141983150983156 983152983141983154983155983151983150 983150983137983149983141 983139983137983150 983138983141 983145983150983152983157983156983156983141983140 983151983150 983156983144983141 983155983139983154983141983141983150

983124983144983141 983152983154983145983150983156983145983150983143 983152983154983151983142983145983148983141983155 983155983139983137983148983141 983145983155 983138983141983145983150983143 983145983150983156983141983154983148983151983139983147983141983140 983159983145983156983144 983156983144983141 983155983139983137983148983141 983151983142 ldquo983120983154983151983142983145983148983141rdquo 983155983139983154983141983141983150 983123983141983156 983157983152 983156983144983141 983155983139983137983148983141 983137983150983140

983156983144983141 983150983157983149983138983141983154 983151983142 983152983154983151983142983145983148983141983155 983151983142 983141983137983139983144 983154983137983150983143983141 983138983161 983123983124D 983137983150983140 983123983117983120 983154983141983155983152983141983139983156983145983158983141983148983161

983124983144983141 983154983151983159 983159983145983140983156983144 983151983142 983152983154983145983150983156983145983150983143 983145983155 983138983141983145983150983143 983145983150983156983141983154983148983151983139983147983141983140 983159983145983156983144 983137 983155983141983156983157983152 983151983142 983124983137983138983148983141 983155983139983154983141983141983150 I983142 983156983144983141 983154983151983159 983159983145983140983156983144 983137983156 983156983144983141 983156983145983149983141

983151983142 983152983154983145983150983156983145983150983143 983145983155 983150983137983154983154983151983159 983152983148983141983137983155983141 983137983140983146983157983155983156 983151983150 983156983144983141 983155983139983154983141983141983150 A983150983140 983156983144983141 983154983151983159 983159983145983148983148 983150983151983156 983138983141 983152983154983145983150983156983141983140 983145983142 983159983145983140983156983144 983151983142 983137 983154983151983159 983145983155

983149983137983140983141 983145983150983156983151 983162983141983154983151

9 Termination

(１) Press the upper right button of MA3win

(２) Close the Windows and turn off the power of PC and Printer

(３) Power off MA-3000

(４) Discharge liquid of a drain tank

(５) Close the main cock of the Oxygen gas cylinder

983116983151983159 983112983113983111983112

983118983157983149983138983141983154

983151983142 983152983154983151983142983145983148983141

7252019 MA 3000 NIC 600 2233 01 Simplified Operation Manual

httpslidepdfcomreaderfullma-3000-nic-600-2233-01-simplified-operation-manual 1010

NIC-600-2233-01

99

9 Errors and warning

Measurement can continue even if a warning message has been displayed However if an error

message is displayed measurement will be disabled until the cause of the error has been solved

Please check messages and contact our service

Technical Center

14-8 Akaoji-cho Takatsuki-shi Osaka 569-1146

Japan

Phone +81-72-693-6820

Fax +81-72-694-0663

7252019 MA 3000 NIC 600 2233 01 Simplified Operation Manual

httpslidepdfcomreaderfullma-3000-nic-600-2233-01-simplified-operation-manual 610

NIC-600-2233-01

59

64 983112983151983159 983156983151 983149983151983157983150983156 983156983144983141 983155983137983149983152983148983141983155983112983151983159 983156983151 983149983151983157983150983156 983156983144983141 983155983137983149983152983148983141983155983112983151983159 983156983151 983149983151983157983150983156 983156983144983141 983155983137983149983152983148983141983155983112983151983159 983156983151 983149983151983157983150983156 983156983144983141 983155983137983149983152983148983141983155

983123983137983149983152983148983141 983137983149983151983157983150983156 983145983155 983140983141983152983141983150983140983145983150983143 983151983150 983156983144983141 983155983137983149983152983148983141 983147983145983150983140 983142983151983154983149 983138983157983156 200983149983143 983142983151983154 983155983151983148983145983140 983137983150983140 200983157983116 983142983151983154 983148983145983153983157983145983140 983137983154983141 983157983155983157983137983148983148983161

983154983141983139983151983149983149983141983150983140983141983140 B983141 983139983137983154983141983142983157983148 983150983151983156 983156983151 983138983141 983155983152983145983148983148983141983140 983151983157983156 983151983142 983156983144983141 983138983151983137983156983155 983140983157983154983145983150983143 983148983151983137983140983145983150983143 983145983150 983156983144983141 983155983137983149983152983148983141 983139983144983137983150983143983141983154

Wear the gloves or use the tweezers when weighing samples and handling sample boats

If the liquid samples may contain organic mercury add additive B or L-cysteine solution not to

vaporize during standby in the sample changer Add small amount of additive B in the boat bottom

or add 10uL of 100ppm L-cycteine solution

When you use additive B please put small amount of additive into sample boat before sample

weighting

① 983124983144983141 volatile high liquid

Add more additive the level of liquid samples

② The sample which melt after measurement

(Ex Aluminum Pyrex and so on)

Put additive at the bottom

③ The sample which burns rapidly

Put additive at the bottom on the boat And put sample

several points on additive and then cover it with another

additive

7252019 MA 3000 NIC 600 2233 01 Simplified Operation Manual

httpslidepdfcomreaderfullma-3000-nic-600-2233-01-simplified-operation-manual 710

NIC-600-2233-01

69

65 Measurement of Unknown samples

(1) Enter the sample name and the sample amount Select the sample form and unit etc on the

ldquoTable Conditionrdquo by clicking

(2) Select the heating method in ldquoMethod Numberrdquo If the moisture content is known as for solid

samples enter it in ldquoMOIST []rdquo so that the concentration is calculated as ldquodry weightrdquo

(3) After checking ldquoSample Numberrdquo with click or press ldquoF5rdquo to start measuring

Selection for (Heating) Method

Select a heating method (12 Methods) can be registered in ldquoRun - Method setrdquo as Heating Method

5 Methods are installed by default as described below

Heating Method table

MethodNo

Kind of sample Heating MethodTypicalamount

0 Liquid sample Standard solutionLiquid sample with additive B STD ~200microL

1Biological sample (Solid)Fish tissue plant tissue

ORGANISM(SOLID)

~200 mg

2 Soil sediment amp sludge SOIL amp SLUDGE ~200 mg

3 Urine Blood URINE amp BLOOD ~200microL

4 Plastics PLASTICS ~100 mg

5MineralsCoal coal ash metal and mineral

MINERAL ~200 mg

6 Waste water WASTE WATER ~100microL

7 Purge PURGE -

Do not measure the sample digested by HNO3 directly This sample may generate heat on the

activated carbon filter Dilute it less than 5wt of HNO3

As for HCL solution dilute it less than 1wt

The above ldquoHeating Methodsrdquo may not cover the samples which contain a lot of halogens or burn

quickly

When the check standard after measuring is lower reduce the sample size

Dilute or reduce the sample size if it contains high mercury Otherwise it contaminates the

plumbing As for the liquid samples containing organic mercury use ldquoAdditive Brdquo on the boat

7252019 MA 3000 NIC 600 2233 01 Simplified Operation Manual

httpslidepdfcomreaderfullma-3000-nic-600-2233-01-simplified-operation-manual 810

NIC-600-2233-01

79

66 983123983156983137983154983156983145983150983143 983137 983149983141983137983155983157983154983141983149983141983150983156983123983156983137983154983156983145983150983143 983137 983149983141983137983155983157983154983141983149983141983150983156983123983156983137983154983156983145983150983143 983137 983149983141983137983155983157983154983141983149983141983150983156983123983156983137983154983156983145983150983143 983137 983149983141983137983155983157983154983141983149983141983150983156

C983148983145983139983147 983156983144983141 983145983139983151983150 or press ldquoF5rdquo to start measuring

67 983122983141983158983145983141983159983145983150983143 983149983141983137983155983157983154983141983149983141983150983156 983140983137983156983137983122983141983158983145983141983159983145983150983143 983149983141983137983155983157983154983141983149983141983150983156 983140983137983156983137983122983141983158983145983141983159983145983150983143 983149983141983137983155983157983154983141983149983141983150983156 983140983137983156983137983122983141983158983145983141983159983145983150983143 983149983141983137983155983157983154983141983149983141983150983156 983140983137983156983137

983122983141983158983145983141983159 983156983144983141 983149983141983137983155983157983154983141983149983141983150983156 983154983141983155983157983148983156983155 983137983150983140 983140983141983156983141983154983149983145983150983141 983159983144983141983156983144983141983154 983156983151 983157983155983141 983156983144983141 983140983137983156983137 983151983154 983150983151983156

A983155 983142983151983154 983156983144983141 983137983150983137983148983161983155983145983155 983154983137983150983143983141 983156983144983141 983140983137983156983137 983148983141983155983155 983156983144983137983150 10983150983143 983137983154983141 983137983152983152983148983145983141983140 983142983151983154 983116983119983127 983154983137983150983143983141 983137983150983140 983156983144983141 983140983137983156983137 983143983154983141983137983156983141983154 983156983144983137983150

10983150983143 983137983154983141 983137983152983152983148983145983141983140 983142983151983154 HIGH 983154983137983150983143983141 A983150 983137983150983137983148983161983155983145983155 983154983137983150983143983141 983139983137983150 983138983141 983139983144983137983150983143983141983140 983137983150983140 983145983155 983152983141983154983142983151983154983149983141983140 983145983150 983156983144983141 983122983137983150983143983141

983139983151983148983157983149983150

I983142 983156983144983141 983154983141983139983151983158983141983154983161 983151983142 983156983144983141 983155983156983137983150983140983137983154983140 983155983151983148983157983156983145983151983150 983137983142983156983141983154 983156983144983141 983149983141983137983155983157983154983141983149983141983150983156 983145983155 90 983151983154 983148983141983155983155 983145983156 983149983145983143983144983156 983138983141 983140983157983141 983156983151 983156983144983141

983145983150983156983141983154983142983141983154983141983150983139983141 983139983151983150983156983137983149983145983150983137983156983145983151983150 983124983154983161 983156983151 983154983141983140983157983139983141 983156983144983141 983137983149983151983157983150983156 983151983142 983155983137983149983152983148983141 983151983154 983156983151 983139983144983137983150983143983141 983156983144983141 983144983141983137983156983145983150983143 983139983151983150983140983145983156983145983151983150983155

I983150983146983141983139983156 200micro983116 983151983142 D983145983155983156983145983148983148983141983140 983127983137983156983141983154 983142983151983154 983155983141983158983141983154983137983148 983156983145983149983141983155 983145983142 983144983145983143983144 983139983151983150983139983141983150983156983154983137983156983145983151983150 983155983137983149983152983148983141983155 983137983154983141 983149983141983137983155983157983154983141983140

I983150983146983141983139983156 200micro983116 983151983142 983123983156983137983150983140983137983154983140 983123983151983148983157983156983145983151983150 983154983141983152983141983137983156983141983140983148983161 983145983142 983156983144983141 983155983141983150983155983145983156983145983158983145983156983161 983154983141983140983157983139983141983155 983124983144983145983155 983159983137983161 983154983141983139983151983158983141983154 983156983144983141

983155983141983150983155983145983156983145983158983145983156983161 983137983150983140 983139983137983150 983137983148983155983151 983139983151983150983142983145983154983149

7 Data Save

(１) Press and ldquoSaverdquo screen is displayed

(２) Select the registered folder and save it with entering the file name

7252019 MA 3000 NIC 600 2233 01 Simplified Operation Manual

httpslidepdfcomreaderfullma-3000-nic-600-2233-01-simplified-operation-manual 910

NIC-600-2233-01

89

8 Printing

(１) Press

(２) Select the printing objects and click ldquoPrint Reviewrdquo

(３) Confirm ldquoPrint Reviewrdquo and start printing

983123983141983148983141983139983156 ldquo983124983137983138983148983141rdquo983085ldquo983117983141983149983151 983123983141983156rdquo

983124983144983141 983156983145983156983148983141 983137983150983140 983137 983149983141983137983155983157983154983141983149983141983150983156 983152983141983154983155983151983150 983150983137983149983141 983139983137983150 983138983141 983145983150983152983157983156983156983141983140 983151983150 983156983144983141 983155983139983154983141983141983150

983124983144983141 983152983154983145983150983156983145983150983143 983152983154983151983142983145983148983141983155 983155983139983137983148983141 983145983155 983138983141983145983150983143 983145983150983156983141983154983148983151983139983147983141983140 983159983145983156983144 983156983144983141 983155983139983137983148983141 983151983142 ldquo983120983154983151983142983145983148983141rdquo 983155983139983154983141983141983150 983123983141983156 983157983152 983156983144983141 983155983139983137983148983141 983137983150983140

983156983144983141 983150983157983149983138983141983154 983151983142 983152983154983151983142983145983148983141983155 983151983142 983141983137983139983144 983154983137983150983143983141 983138983161 983123983124D 983137983150983140 983123983117983120 983154983141983155983152983141983139983156983145983158983141983148983161

983124983144983141 983154983151983159 983159983145983140983156983144 983151983142 983152983154983145983150983156983145983150983143 983145983155 983138983141983145983150983143 983145983150983156983141983154983148983151983139983147983141983140 983159983145983156983144 983137 983155983141983156983157983152 983151983142 983124983137983138983148983141 983155983139983154983141983141983150 I983142 983156983144983141 983154983151983159 983159983145983140983156983144 983137983156 983156983144983141 983156983145983149983141

983151983142 983152983154983145983150983156983145983150983143 983145983155 983150983137983154983154983151983159 983152983148983141983137983155983141 983137983140983146983157983155983156 983151983150 983156983144983141 983155983139983154983141983141983150 A983150983140 983156983144983141 983154983151983159 983159983145983148983148 983150983151983156 983138983141 983152983154983145983150983156983141983140 983145983142 983159983145983140983156983144 983151983142 983137 983154983151983159 983145983155

983149983137983140983141 983145983150983156983151 983162983141983154983151

9 Termination

(１) Press the upper right button of MA3win

(２) Close the Windows and turn off the power of PC and Printer

(３) Power off MA-3000

(４) Discharge liquid of a drain tank

(５) Close the main cock of the Oxygen gas cylinder

983116983151983159 983112983113983111983112

983118983157983149983138983141983154

983151983142 983152983154983151983142983145983148983141

7252019 MA 3000 NIC 600 2233 01 Simplified Operation Manual

httpslidepdfcomreaderfullma-3000-nic-600-2233-01-simplified-operation-manual 1010

NIC-600-2233-01

99

9 Errors and warning

Measurement can continue even if a warning message has been displayed However if an error

message is displayed measurement will be disabled until the cause of the error has been solved

Please check messages and contact our service

Technical Center

14-8 Akaoji-cho Takatsuki-shi Osaka 569-1146

Japan

Phone +81-72-693-6820

Fax +81-72-694-0663

7252019 MA 3000 NIC 600 2233 01 Simplified Operation Manual

httpslidepdfcomreaderfullma-3000-nic-600-2233-01-simplified-operation-manual 710

NIC-600-2233-01

69

65 Measurement of Unknown samples

(1) Enter the sample name and the sample amount Select the sample form and unit etc on the

ldquoTable Conditionrdquo by clicking

(2) Select the heating method in ldquoMethod Numberrdquo If the moisture content is known as for solid

samples enter it in ldquoMOIST []rdquo so that the concentration is calculated as ldquodry weightrdquo

(3) After checking ldquoSample Numberrdquo with click or press ldquoF5rdquo to start measuring

Selection for (Heating) Method

Select a heating method (12 Methods) can be registered in ldquoRun - Method setrdquo as Heating Method

5 Methods are installed by default as described below

Heating Method table

MethodNo

Kind of sample Heating MethodTypicalamount

0 Liquid sample Standard solutionLiquid sample with additive B STD ~200microL

1Biological sample (Solid)Fish tissue plant tissue

ORGANISM(SOLID)

~200 mg

2 Soil sediment amp sludge SOIL amp SLUDGE ~200 mg

3 Urine Blood URINE amp BLOOD ~200microL

4 Plastics PLASTICS ~100 mg

5MineralsCoal coal ash metal and mineral

MINERAL ~200 mg

6 Waste water WASTE WATER ~100microL

7 Purge PURGE -

Do not measure the sample digested by HNO3 directly This sample may generate heat on the

activated carbon filter Dilute it less than 5wt of HNO3

As for HCL solution dilute it less than 1wt

The above ldquoHeating Methodsrdquo may not cover the samples which contain a lot of halogens or burn

quickly

When the check standard after measuring is lower reduce the sample size

Dilute or reduce the sample size if it contains high mercury Otherwise it contaminates the

plumbing As for the liquid samples containing organic mercury use ldquoAdditive Brdquo on the boat

7252019 MA 3000 NIC 600 2233 01 Simplified Operation Manual

httpslidepdfcomreaderfullma-3000-nic-600-2233-01-simplified-operation-manual 810

NIC-600-2233-01

79

66 983123983156983137983154983156983145983150983143 983137 983149983141983137983155983157983154983141983149983141983150983156983123983156983137983154983156983145983150983143 983137 983149983141983137983155983157983154983141983149983141983150983156983123983156983137983154983156983145983150983143 983137 983149983141983137983155983157983154983141983149983141983150983156983123983156983137983154983156983145983150983143 983137 983149983141983137983155983157983154983141983149983141983150983156

C983148983145983139983147 983156983144983141 983145983139983151983150 or press ldquoF5rdquo to start measuring

67 983122983141983158983145983141983159983145983150983143 983149983141983137983155983157983154983141983149983141983150983156 983140983137983156983137983122983141983158983145983141983159983145983150983143 983149983141983137983155983157983154983141983149983141983150983156 983140983137983156983137983122983141983158983145983141983159983145983150983143 983149983141983137983155983157983154983141983149983141983150983156 983140983137983156983137983122983141983158983145983141983159983145983150983143 983149983141983137983155983157983154983141983149983141983150983156 983140983137983156983137

983122983141983158983145983141983159 983156983144983141 983149983141983137983155983157983154983141983149983141983150983156 983154983141983155983157983148983156983155 983137983150983140 983140983141983156983141983154983149983145983150983141 983159983144983141983156983144983141983154 983156983151 983157983155983141 983156983144983141 983140983137983156983137 983151983154 983150983151983156

A983155 983142983151983154 983156983144983141 983137983150983137983148983161983155983145983155 983154983137983150983143983141 983156983144983141 983140983137983156983137 983148983141983155983155 983156983144983137983150 10983150983143 983137983154983141 983137983152983152983148983145983141983140 983142983151983154 983116983119983127 983154983137983150983143983141 983137983150983140 983156983144983141 983140983137983156983137 983143983154983141983137983156983141983154 983156983144983137983150

10983150983143 983137983154983141 983137983152983152983148983145983141983140 983142983151983154 HIGH 983154983137983150983143983141 A983150 983137983150983137983148983161983155983145983155 983154983137983150983143983141 983139983137983150 983138983141 983139983144983137983150983143983141983140 983137983150983140 983145983155 983152983141983154983142983151983154983149983141983140 983145983150 983156983144983141 983122983137983150983143983141

983139983151983148983157983149983150

I983142 983156983144983141 983154983141983139983151983158983141983154983161 983151983142 983156983144983141 983155983156983137983150983140983137983154983140 983155983151983148983157983156983145983151983150 983137983142983156983141983154 983156983144983141 983149983141983137983155983157983154983141983149983141983150983156 983145983155 90 983151983154 983148983141983155983155 983145983156 983149983145983143983144983156 983138983141 983140983157983141 983156983151 983156983144983141

983145983150983156983141983154983142983141983154983141983150983139983141 983139983151983150983156983137983149983145983150983137983156983145983151983150 983124983154983161 983156983151 983154983141983140983157983139983141 983156983144983141 983137983149983151983157983150983156 983151983142 983155983137983149983152983148983141 983151983154 983156983151 983139983144983137983150983143983141 983156983144983141 983144983141983137983156983145983150983143 983139983151983150983140983145983156983145983151983150983155

I983150983146983141983139983156 200micro983116 983151983142 D983145983155983156983145983148983148983141983140 983127983137983156983141983154 983142983151983154 983155983141983158983141983154983137983148 983156983145983149983141983155 983145983142 983144983145983143983144 983139983151983150983139983141983150983156983154983137983156983145983151983150 983155983137983149983152983148983141983155 983137983154983141 983149983141983137983155983157983154983141983140

I983150983146983141983139983156 200micro983116 983151983142 983123983156983137983150983140983137983154983140 983123983151983148983157983156983145983151983150 983154983141983152983141983137983156983141983140983148983161 983145983142 983156983144983141 983155983141983150983155983145983156983145983158983145983156983161 983154983141983140983157983139983141983155 983124983144983145983155 983159983137983161 983154983141983139983151983158983141983154 983156983144983141

983155983141983150983155983145983156983145983158983145983156983161 983137983150983140 983139983137983150 983137983148983155983151 983139983151983150983142983145983154983149

7 Data Save

(１) Press and ldquoSaverdquo screen is displayed

(２) Select the registered folder and save it with entering the file name

7252019 MA 3000 NIC 600 2233 01 Simplified Operation Manual

httpslidepdfcomreaderfullma-3000-nic-600-2233-01-simplified-operation-manual 910

NIC-600-2233-01

89

8 Printing

(１) Press

(２) Select the printing objects and click ldquoPrint Reviewrdquo

(３) Confirm ldquoPrint Reviewrdquo and start printing

983123983141983148983141983139983156 ldquo983124983137983138983148983141rdquo983085ldquo983117983141983149983151 983123983141983156rdquo

983124983144983141 983156983145983156983148983141 983137983150983140 983137 983149983141983137983155983157983154983141983149983141983150983156 983152983141983154983155983151983150 983150983137983149983141 983139983137983150 983138983141 983145983150983152983157983156983156983141983140 983151983150 983156983144983141 983155983139983154983141983141983150

983124983144983141 983152983154983145983150983156983145983150983143 983152983154983151983142983145983148983141983155 983155983139983137983148983141 983145983155 983138983141983145983150983143 983145983150983156983141983154983148983151983139983147983141983140 983159983145983156983144 983156983144983141 983155983139983137983148983141 983151983142 ldquo983120983154983151983142983145983148983141rdquo 983155983139983154983141983141983150 983123983141983156 983157983152 983156983144983141 983155983139983137983148983141 983137983150983140

983156983144983141 983150983157983149983138983141983154 983151983142 983152983154983151983142983145983148983141983155 983151983142 983141983137983139983144 983154983137983150983143983141 983138983161 983123983124D 983137983150983140 983123983117983120 983154983141983155983152983141983139983156983145983158983141983148983161

983124983144983141 983154983151983159 983159983145983140983156983144 983151983142 983152983154983145983150983156983145983150983143 983145983155 983138983141983145983150983143 983145983150983156983141983154983148983151983139983147983141983140 983159983145983156983144 983137 983155983141983156983157983152 983151983142 983124983137983138983148983141 983155983139983154983141983141983150 I983142 983156983144983141 983154983151983159 983159983145983140983156983144 983137983156 983156983144983141 983156983145983149983141

983151983142 983152983154983145983150983156983145983150983143 983145983155 983150983137983154983154983151983159 983152983148983141983137983155983141 983137983140983146983157983155983156 983151983150 983156983144983141 983155983139983154983141983141983150 A983150983140 983156983144983141 983154983151983159 983159983145983148983148 983150983151983156 983138983141 983152983154983145983150983156983141983140 983145983142 983159983145983140983156983144 983151983142 983137 983154983151983159 983145983155

983149983137983140983141 983145983150983156983151 983162983141983154983151

9 Termination

(１) Press the upper right button of MA3win

(２) Close the Windows and turn off the power of PC and Printer

(３) Power off MA-3000

(４) Discharge liquid of a drain tank

(５) Close the main cock of the Oxygen gas cylinder

983116983151983159 983112983113983111983112

983118983157983149983138983141983154

983151983142 983152983154983151983142983145983148983141

7252019 MA 3000 NIC 600 2233 01 Simplified Operation Manual

httpslidepdfcomreaderfullma-3000-nic-600-2233-01-simplified-operation-manual 1010

NIC-600-2233-01

99

9 Errors and warning

Measurement can continue even if a warning message has been displayed However if an error

message is displayed measurement will be disabled until the cause of the error has been solved

Please check messages and contact our service

Technical Center

14-8 Akaoji-cho Takatsuki-shi Osaka 569-1146

Japan

Phone +81-72-693-6820

Fax +81-72-694-0663

7252019 MA 3000 NIC 600 2233 01 Simplified Operation Manual

httpslidepdfcomreaderfullma-3000-nic-600-2233-01-simplified-operation-manual 810

NIC-600-2233-01

79

66 983123983156983137983154983156983145983150983143 983137 983149983141983137983155983157983154983141983149983141983150983156983123983156983137983154983156983145983150983143 983137 983149983141983137983155983157983154983141983149983141983150983156983123983156983137983154983156983145983150983143 983137 983149983141983137983155983157983154983141983149983141983150983156983123983156983137983154983156983145983150983143 983137 983149983141983137983155983157983154983141983149983141983150983156

C983148983145983139983147 983156983144983141 983145983139983151983150 or press ldquoF5rdquo to start measuring

67 983122983141983158983145983141983159983145983150983143 983149983141983137983155983157983154983141983149983141983150983156 983140983137983156983137983122983141983158983145983141983159983145983150983143 983149983141983137983155983157983154983141983149983141983150983156 983140983137983156983137983122983141983158983145983141983159983145983150983143 983149983141983137983155983157983154983141983149983141983150983156 983140983137983156983137983122983141983158983145983141983159983145983150983143 983149983141983137983155983157983154983141983149983141983150983156 983140983137983156983137

983122983141983158983145983141983159 983156983144983141 983149983141983137983155983157983154983141983149983141983150983156 983154983141983155983157983148983156983155 983137983150983140 983140983141983156983141983154983149983145983150983141 983159983144983141983156983144983141983154 983156983151 983157983155983141 983156983144983141 983140983137983156983137 983151983154 983150983151983156

A983155 983142983151983154 983156983144983141 983137983150983137983148983161983155983145983155 983154983137983150983143983141 983156983144983141 983140983137983156983137 983148983141983155983155 983156983144983137983150 10983150983143 983137983154983141 983137983152983152983148983145983141983140 983142983151983154 983116983119983127 983154983137983150983143983141 983137983150983140 983156983144983141 983140983137983156983137 983143983154983141983137983156983141983154 983156983144983137983150

10983150983143 983137983154983141 983137983152983152983148983145983141983140 983142983151983154 HIGH 983154983137983150983143983141 A983150 983137983150983137983148983161983155983145983155 983154983137983150983143983141 983139983137983150 983138983141 983139983144983137983150983143983141983140 983137983150983140 983145983155 983152983141983154983142983151983154983149983141983140 983145983150 983156983144983141 983122983137983150983143983141

983139983151983148983157983149983150

I983142 983156983144983141 983154983141983139983151983158983141983154983161 983151983142 983156983144983141 983155983156983137983150983140983137983154983140 983155983151983148983157983156983145983151983150 983137983142983156983141983154 983156983144983141 983149983141983137983155983157983154983141983149983141983150983156 983145983155 90 983151983154 983148983141983155983155 983145983156 983149983145983143983144983156 983138983141 983140983157983141 983156983151 983156983144983141

983145983150983156983141983154983142983141983154983141983150983139983141 983139983151983150983156983137983149983145983150983137983156983145983151983150 983124983154983161 983156983151 983154983141983140983157983139983141 983156983144983141 983137983149983151983157983150983156 983151983142 983155983137983149983152983148983141 983151983154 983156983151 983139983144983137983150983143983141 983156983144983141 983144983141983137983156983145983150983143 983139983151983150983140983145983156983145983151983150983155

I983150983146983141983139983156 200micro983116 983151983142 D983145983155983156983145983148983148983141983140 983127983137983156983141983154 983142983151983154 983155983141983158983141983154983137983148 983156983145983149983141983155 983145983142 983144983145983143983144 983139983151983150983139983141983150983156983154983137983156983145983151983150 983155983137983149983152983148983141983155 983137983154983141 983149983141983137983155983157983154983141983140

I983150983146983141983139983156 200micro983116 983151983142 983123983156983137983150983140983137983154983140 983123983151983148983157983156983145983151983150 983154983141983152983141983137983156983141983140983148983161 983145983142 983156983144983141 983155983141983150983155983145983156983145983158983145983156983161 983154983141983140983157983139983141983155 983124983144983145983155 983159983137983161 983154983141983139983151983158983141983154 983156983144983141

983155983141983150983155983145983156983145983158983145983156983161 983137983150983140 983139983137983150 983137983148983155983151 983139983151983150983142983145983154983149

7 Data Save

(１) Press and ldquoSaverdquo screen is displayed

(２) Select the registered folder and save it with entering the file name

7252019 MA 3000 NIC 600 2233 01 Simplified Operation Manual

httpslidepdfcomreaderfullma-3000-nic-600-2233-01-simplified-operation-manual 910

NIC-600-2233-01

89

8 Printing

(１) Press

(２) Select the printing objects and click ldquoPrint Reviewrdquo

(３) Confirm ldquoPrint Reviewrdquo and start printing

983123983141983148983141983139983156 ldquo983124983137983138983148983141rdquo983085ldquo983117983141983149983151 983123983141983156rdquo

983124983144983141 983156983145983156983148983141 983137983150983140 983137 983149983141983137983155983157983154983141983149983141983150983156 983152983141983154983155983151983150 983150983137983149983141 983139983137983150 983138983141 983145983150983152983157983156983156983141983140 983151983150 983156983144983141 983155983139983154983141983141983150

983124983144983141 983152983154983145983150983156983145983150983143 983152983154983151983142983145983148983141983155 983155983139983137983148983141 983145983155 983138983141983145983150983143 983145983150983156983141983154983148983151983139983147983141983140 983159983145983156983144 983156983144983141 983155983139983137983148983141 983151983142 ldquo983120983154983151983142983145983148983141rdquo 983155983139983154983141983141983150 983123983141983156 983157983152 983156983144983141 983155983139983137983148983141 983137983150983140

983156983144983141 983150983157983149983138983141983154 983151983142 983152983154983151983142983145983148983141983155 983151983142 983141983137983139983144 983154983137983150983143983141 983138983161 983123983124D 983137983150983140 983123983117983120 983154983141983155983152983141983139983156983145983158983141983148983161

983124983144983141 983154983151983159 983159983145983140983156983144 983151983142 983152983154983145983150983156983145983150983143 983145983155 983138983141983145983150983143 983145983150983156983141983154983148983151983139983147983141983140 983159983145983156983144 983137 983155983141983156983157983152 983151983142 983124983137983138983148983141 983155983139983154983141983141983150 I983142 983156983144983141 983154983151983159 983159983145983140983156983144 983137983156 983156983144983141 983156983145983149983141

983151983142 983152983154983145983150983156983145983150983143 983145983155 983150983137983154983154983151983159 983152983148983141983137983155983141 983137983140983146983157983155983156 983151983150 983156983144983141 983155983139983154983141983141983150 A983150983140 983156983144983141 983154983151983159 983159983145983148983148 983150983151983156 983138983141 983152983154983145983150983156983141983140 983145983142 983159983145983140983156983144 983151983142 983137 983154983151983159 983145983155

983149983137983140983141 983145983150983156983151 983162983141983154983151

9 Termination

(１) Press the upper right button of MA3win

(２) Close the Windows and turn off the power of PC and Printer

(３) Power off MA-3000

(４) Discharge liquid of a drain tank

(５) Close the main cock of the Oxygen gas cylinder

983116983151983159 983112983113983111983112

983118983157983149983138983141983154

983151983142 983152983154983151983142983145983148983141

7252019 MA 3000 NIC 600 2233 01 Simplified Operation Manual

httpslidepdfcomreaderfullma-3000-nic-600-2233-01-simplified-operation-manual 1010

NIC-600-2233-01

99

9 Errors and warning

Measurement can continue even if a warning message has been displayed However if an error

message is displayed measurement will be disabled until the cause of the error has been solved

Please check messages and contact our service

Technical Center

14-8 Akaoji-cho Takatsuki-shi Osaka 569-1146

Japan

Phone +81-72-693-6820

Fax +81-72-694-0663

7252019 MA 3000 NIC 600 2233 01 Simplified Operation Manual

httpslidepdfcomreaderfullma-3000-nic-600-2233-01-simplified-operation-manual 910

NIC-600-2233-01

89

8 Printing

(１) Press

(２) Select the printing objects and click ldquoPrint Reviewrdquo

(３) Confirm ldquoPrint Reviewrdquo and start printing

983123983141983148983141983139983156 ldquo983124983137983138983148983141rdquo983085ldquo983117983141983149983151 983123983141983156rdquo

983124983144983141 983156983145983156983148983141 983137983150983140 983137 983149983141983137983155983157983154983141983149983141983150983156 983152983141983154983155983151983150 983150983137983149983141 983139983137983150 983138983141 983145983150983152983157983156983156983141983140 983151983150 983156983144983141 983155983139983154983141983141983150

983124983144983141 983152983154983145983150983156983145983150983143 983152983154983151983142983145983148983141983155 983155983139983137983148983141 983145983155 983138983141983145983150983143 983145983150983156983141983154983148983151983139983147983141983140 983159983145983156983144 983156983144983141 983155983139983137983148983141 983151983142 ldquo983120983154983151983142983145983148983141rdquo 983155983139983154983141983141983150 983123983141983156 983157983152 983156983144983141 983155983139983137983148983141 983137983150983140

983156983144983141 983150983157983149983138983141983154 983151983142 983152983154983151983142983145983148983141983155 983151983142 983141983137983139983144 983154983137983150983143983141 983138983161 983123983124D 983137983150983140 983123983117983120 983154983141983155983152983141983139983156983145983158983141983148983161

983124983144983141 983154983151983159 983159983145983140983156983144 983151983142 983152983154983145983150983156983145983150983143 983145983155 983138983141983145983150983143 983145983150983156983141983154983148983151983139983147983141983140 983159983145983156983144 983137 983155983141983156983157983152 983151983142 983124983137983138983148983141 983155983139983154983141983141983150 I983142 983156983144983141 983154983151983159 983159983145983140983156983144 983137983156 983156983144983141 983156983145983149983141

983151983142 983152983154983145983150983156983145983150983143 983145983155 983150983137983154983154983151983159 983152983148983141983137983155983141 983137983140983146983157983155983156 983151983150 983156983144983141 983155983139983154983141983141983150 A983150983140 983156983144983141 983154983151983159 983159983145983148983148 983150983151983156 983138983141 983152983154983145983150983156983141983140 983145983142 983159983145983140983156983144 983151983142 983137 983154983151983159 983145983155

983149983137983140983141 983145983150983156983151 983162983141983154983151

9 Termination

(１) Press the upper right button of MA3win

(２) Close the Windows and turn off the power of PC and Printer

(３) Power off MA-3000

(４) Discharge liquid of a drain tank

(５) Close the main cock of the Oxygen gas cylinder

983116983151983159 983112983113983111983112

983118983157983149983138983141983154

983151983142 983152983154983151983142983145983148983141

7252019 MA 3000 NIC 600 2233 01 Simplified Operation Manual

httpslidepdfcomreaderfullma-3000-nic-600-2233-01-simplified-operation-manual 1010

NIC-600-2233-01

99

9 Errors and warning

Measurement can continue even if a warning message has been displayed However if an error

message is displayed measurement will be disabled until the cause of the error has been solved

Please check messages and contact our service

Technical Center

14-8 Akaoji-cho Takatsuki-shi Osaka 569-1146

Japan

Phone +81-72-693-6820

Fax +81-72-694-0663

7252019 MA 3000 NIC 600 2233 01 Simplified Operation Manual

httpslidepdfcomreaderfullma-3000-nic-600-2233-01-simplified-operation-manual 1010

NIC-600-2233-01

99

9 Errors and warning

Measurement can continue even if a warning message has been displayed However if an error

message is displayed measurement will be disabled until the cause of the error has been solved

Please check messages and contact our service

Technical Center

14-8 Akaoji-cho Takatsuki-shi Osaka 569-1146

Japan

Phone +81-72-693-6820

Fax +81-72-694-0663